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Making Measurements  · Web view2015. 11. 6. · 3.880.227. 7.383.618. 5.980.839. 1 ... In the...

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Topic 0 - Practical Skills Name:_____________________________________ Date: _________________ Assess yourself with these criteria Teacher Comments What you need to do to improve Making measurements and resolution Micrometer Vernier callipers Use of fiducial marks Improving Precision Improving Accuracy Improving Reproducability and repeatability A simple measurement (really simple) Sources of Uncertainty – random and systematic errors Handling Uncertainty Absolute, fractional and percentage uncertainties Combining uncertainties Drawing Graphs and interpreting graphs Using error bars on a graph Determining uncertainties in the gradient and intercept # Assignment Title Student Self- Assessment Teacher Comment Grade (1-4) (1 = high) 0 . Sources of error – 1
Transcript

Topic 0 - Practical Skills

Name:_____________________________________ Date: _________________

Assess yourself with these criteria

Teacher Comments

What you need to do to improve

Making measurements and resolution

· Micrometer

· Vernier callipers

· Use of fiducial marks

· Improving Precision

· Improving Accuracy

· Improving Reproducability and repeatability

A simple measurement (really simple)

Sources of Uncertainty – random and systematic errors

Handling Uncertainty

· Absolute, fractional and percentage uncertainties

· Combining uncertainties

Drawing Graphs and interpreting graphs

· Using error bars on a graph

· Determining uncertainties in the gradient and intercept

#

Assignment Title

Student Self-Assessment

Teacher Comment

Grade (1-4)

(1 = high)

0.1

Sources of error – pendulum timing

0.2

Uncertainty in Readings

0.3

Handling Uncertainty

0.4

Practical measurements with errors

0.5

Drawing and interpreting graphs

0.6

Assessed Experiment

/ 20 marks

Making Measurements

Resolution is the fineness to which an instrument can be read. e.g. the resolution of a stop watch is 0.01 s

The uncertainty in a measurement is at best equal to the resolution. e.g. the uncertainty in any reading of a stop watch is +/– 0.01 s

The resolution is taken as the smallest division capable of being read. (This may be different to the uncertainty)

Vernier Calliper

The vernier calliper contains a vernier scale. This scale enables readings to be made with a much greater resolution. As a result, the precision of readings can be increased.

With a pair of vernier callipers, you can measure short lengths i.e. 0 to 15 cm. It has a resolution of 0.002 cm, or 0.02mm. A pair of vernier calipers consists of a Main Scale (top) and a Vernier Scale (bottom / moving) as shown in the diagram to the right.

The outside jaws, are used to measure the outer dimensions of an object and the inner jaws for the inner ones. The stem is used to measure the depth of a hole.

To take measurements

1. To measure, gently grip the object with the straight edges of the outside or inside jaws.

2. First read the main scale, and note down the reading before the 0 on the vernier scale, as shown in the diagram right. The reading on it is 2.8 cm, as the .8 after the 2 on the main scale is before the 0 on the vernier scale.

3. For the second place of decimal, look at the vernier scale. Find a marking on the vernier scale that coincides exactly with the reading on the main scale. In the diagram below, the 6 on the vernier scale coincides exactly with a line on the main scale (it does not matter with which line on the main scale this line coincides). So the second place of the decimal would 6.0, ie .060cm or 0.6mm.

4. To get the total reading, add the two readings i-e 2.8+.060. The final reading is 2.860cm or 28.60mm.

Lab Work – Vernier Scale Practise

Determine the measurement of the following examples, and then have a go at measuring some objects yourself using a pair of Vernier Callipers. Make sure you compare your measurements to those that other students of the teacher can take. You could also check your reading with a digital calliper. You must take at least seven correct readings.

Object

Your reading

Comparison reading

Correct?

Screwgauge Micrometer

A screwgauge micrometer is used to measure very short readings i.e. 0 to 2.5cm. It has a resolution of 0.001cm or 0.01 mm. Like the vernier scale, the micrometer has two scales, main scale (on the sleeve) and the circular scale (on the thimble). Each division on the main scale represents 1 mm. Each division on the thimble represents a distance of 0.01mm.

How to take measurements

1. Turn the thimble until the object is nearly gripped. Then use the ratchet knob to fully close the anvil and spindle. DO NOT overtighten. This can cause two problems; the object you are measuring becomes squashed slightly, so the reading is reduced; the thread of the screwgauge becomes warped, so all future measurements have a zero-error (more on this later).

2. Read the main scale on the sleeve. This reading would be in millimeters. In the diagram below, the reading is 5.5mm. The top row of the sleeve gives whole mm, and the bottom row of the sleeve gives half mm. These ½ mm are only read if they are clearly visible (they become clearly visible when the thimble has rotated fully past 49).

3. Then read the line on the circular scale that coincides with the line on the main scale. In the diagram below, the 28th line on the circular scale coincides with the line. So, the reading would be 0.28mm.

4. Then add 5.5 with 0.28 and you will obtain your answer in millimeters.

How to avoid error

When fully closed with no object to measure, the zero on the vernier scale i.e. circular scale coincides exactly the horizontal line then no error exists (a). This should be the case for all new micrometers, though older ones may, through misuse, have zero error.

If the zero is below the horizontal line than a positive zero error exists and can be avoided by subtracting the error from the final reading (b)

While if the zero is above the horizontal line than a negative zero error exists and can be avoided by measuring the error and adding the error into the final reading (c).

Lab Work – Micrometer Scale Practise

Determine the measurement of the following examples, then have a go at measuring some objects yourself using a screwgauge micrometer. Make sure you compare your measurements to those that other students of the teacher can take. You must take at least seven correct readings.

Object

Your reading

Comparison reading

Correct?

(Answers from previous page6.146. 3.880.227. 7.383.618. 5.980.839. 1.57 8.08)

The space below has been left for you to make further note regarding the use of and measurements with Vernier Calipers and the Screwgauge Micrometer.

Lab Work – Using a fiducial mark – increasing accuracy and reliability

In this experiment a fiducial mark is going to be used to help increase the accuracy of measurements.

In the broadest sense, a fiducial marker or fiducial is an object placed in the field of view of an imaging system which appears in the image produced, for use as a point of reference or a measure. It may be either something placed into or on the imaging subject, or a mark or set of marks in the reticle of an optical instrument.

Within the practicals you will undertake on this course, fiducial markers are used to create a fixed reference point against which measurements can be taken, be it measurements of length or timing.

(bulldog clippendulum bob)Equipment needed

· Retort stand, clamp and boss

· Pendulum bob attached to a length of string

· Bulldog clip (which will act as our fiducial mark)

· Stopwatch

Set up the equipment as shown in the diagram to the right.

The length of the string is not important, but do record the length.

1. Remove the bulldog clip and swing the pendulum.

2. Record the time for one complete swing. time for one swing =

3. Record the time for 20 complete swings and find the average time for one swing.

average time for one swing =

4. Add the bulldog clip. This will act as a fiducial mark to provide a fixed reference point.

5. Observe the time it takes for the pendulum to pass the bulldog clip and record the time for one complete swing.

time for one swing =

6. Record the time for 20 complete swings and find the average time for one swing.

average time for one swing =

7. Comment on the impact that using a fiducial mark had upon the measurement.

8. Comment on the impact that taking multiple readings and finding the average had upon the measurement.

9. If you have a digital camera (e.g. a camera phone, iPad, table etc) with the capability of advancing a video one frame at a time, repeat the experiment and record the swings with the timer in the picture. You should be able to achieve very high precision (down to 1ms) in your measurements.

Apps such as CMV (CoachMyVideo.com) for iPad/iPhone and AndroVid Video Trimmer (for Android) are useful and free.

Sources of Uncertainty

In metrology, physics, and engineering, the uncertainty or margin of error of a measurement, is a range of values likely to enclose the true value. There are a variety of origins of uncertainty summarised below:

19

1. Personal Careless Error (Human error)

· introduced by experimenter.

· while discussing this was sometimes acceptable at GCSE level, do not cite this as a source of error at A level. Rather, take care with your experiment to ensure that you do not introduce error. You will be assessed on your ability to do this.

2. Determinate (Systematic) Error

· uncertainty that is inherent in the measurement devices (hard to read scales, etc.) – i.e. the resolution of the instrument

· often caused by poorly or mis-calibrated instruments

· cannot reduce by repeated measurements

3. Indeterminate (Random) Errors

· may be natural variations in measurements caused by factors beyond reasonable control

· may be result of operator bias, variation in experimental conditions (e.g. temperature), or other factors not easily accounted for.

· may be minimized by repeated measurement and using an arithmetic mean (average) as the best estimate of the true value.

Practical Steps to take to minimise uncertainty

Bookmark or otherwise this guide so that you can easily refer to it when doing investigations

· First look at your measuring instrument. What is its precision (resolution)? (Usually this is the smallest scale division on the instrument, but sometimes you can do better than this e.g. reading a typical temperature to ± 0.5 ºC between the divisions of a thermometer – you can still use your common sense!) This is your best case scenario.

· Then ask yourself: “Are my readings really that good?” Consider whether there are other factors (other random errors) restricting the precision further? This may be obvious with a single reading, but does become obvious over multiple readings. Again use your common sense!

· Generally you will have instinctively realised if your measurements are less reliable and you will have done repeat readings. (There are rare occasions where repeat readings are unnecessary, or even daft.)

· With repeat readings the range of your readings will usually be bigger than the precision of the instrument and this gives you a better idea of the uncertainty in your measurements (the precision is then ignored and the range from the repeats is considered).

Example: timing a trolley rolling a fixed distance from rest down a slope using a manual stopwatch

· Initial reading: 1.27 sec. Precision of stopwatch: ± 0.01 sec

· Clearly it is very unlikely that your measurement is this precise –– your reaction time is involved. So you will do repeat measurements and find a mean value as the best estimate of the true value.

· Readings: 1.27 s; 1.28 s; 1.35 s. Mean value = 1.30 s.

· In fact the ‘true result’ is likely to lie somewhere between 1.27 and 1.35 s.

· The uncertainty is ± 0.4s. This is half the range (1.35 -1.27 = 0.08) of the readings so we write: mean value = 1.30 ± 0.4s.

Assignment 0.1 – Sources of error – pendulum timing – due ……………

First, categorise the following sources of error according to whether they are random, systematic or both.

· Lag time and hysteresis – some measuring devices require time to reach equilibrium and display a stable figure (such as thermometers), and taking a measurement before the instrument is stable will result in a measurement that is generally too low

· Instrument drift – most electronic instruments have readings that drift over time.

· Parallax – this error can occur whenever there is some distance between the measuring scale and the indicator used to obtain a measurement. If the observer's eye is not squarely aligned with the pointer and scale, the reading may be too high or low (some analogue meters have mirrors to help with this alignment).

· Physical or environmental variations

· Failure to calibrate or check zero of instrument

· Instrument resolution – all instruments have finite precision that limits the ability to resolve small measurement differences.

· Failure to account for a factor – the most challenging part of designing an experiment is trying to control or account for all possible factors except the one independent variable that is being analyzed. For instance, you may inadvertently ignore air resistance when measuring free-fall acceleration.

· Incomplete method – one reason that it is impossible to make exact measurements is that the measurement is not always clearly defined. For example, if two different people measure the length of the same rope, they would probably get different results because each person may stretch the rope with a different tension

Secondly, referring back to the Pendulum Timing experiment conducted earlier. On a single side of A4 discuss the potential sources of error that contributed to the uncertainty of the period of the pendulum. Discuss whether each source of error was random or systematic and how each source of error affected the accuracy, repeatability and reproducibility of the measurement. Discuss how the precision and accuracy differ.

You may need to read up further on the meaning and use of the underlined terms. Hand in a well presented document.

Affix your final version of the essay here.

Percentage uncertainties

Clearly a ± 1mm uncertainty in a length of 12mm has more effect than a ± 1mm uncertainty in a length of 123mm and a ± 0.1mA uncertainty in a current of 0.5mA is more worrying than a ± 0.1mA uncertainty in a current of 50.0 mA.

This is why we work out the percentage uncertainty of a measurement. This is the most useful indicator of uncertainty.

Small percentage uncertainties (<5%) are typically excellent results, especially in a school science lab. Larger than 20% uncertainties are poor results.

The rules for combining uncertainties

· When measurements are added, subtracted, you can add their absolute uncertainties or their percentage uncertainties.

· When measurements are multiplied together or divided you can ONLY add their percentage uncertainties.

· If a measurement is raised to a power then you multiply the percentage uncertainty by the power.

· Using these rules enables you to work out the overall percentage uncertainty in a quantity that you have calculated from your measurements. This can then be converted into an actual ± value of uncertainty in your final value.

Uncertainties in gradients of graphs

· If there is very little scatter in your points, so that you can be highly certain of the position of your best fit line, then the uncertainty in your gradient is due to your precision in measuring the lengths of the sides of your triangle. Here, using larger triangles, (minimum 80mm sides) helps reduce uncertainty. Again, selecting scales such that your data points cover the maximum space on your A4 paper helps to reduce uncertainty.

· Measure the actual lengths of the horizontal and vertical sides of your gradient triangle; assume that you can measure them to a precision of ±1mm; work out the corresponding percentage uncertainty for each side; then add those 2 percentage uncertainties together to get the percentage uncertainty in your gradient.

· If there is a lot of scatter then you should probably draw another likely best fit line at a steeper/shallower angle and compare its gradient with your original line to give you the likely uncertainty.

Assignment 0.2: Uncertainty in Readings – due …………………

1. What is the minimum resolution of each of the following apparatus:

a. Metre rule

b. 25ml measuring cylinder

c. 50 N spring balance

d. 25 N spring balance

e. Thermometer

f. Analogue ammeter

2. What is the minimum uncertainty when using:

a. Metre rule

b. 25ml measuring cylinder

c. 50 N spring balance

d. Thermometer

3. John uses a metre rule to measure the width of the room by repeatedly drawing a pencil line at the 100cm mark then moving the ruler to measure from there. He gets a value of 4677 mm

Suggest an estimated uncertainty

calculate the percentage uncertainty:

%

4. What is minimum percentage uncertainty in the following measurements:

a. Standard Lab Thermometer reading 26°

b. Thermometer reading 76°

c. Metre rule reading 3 mm

d. Metre rule reading 320 mm

e. 50 N spring balance reading 20N

Assignment 0.3 – Handling Uncertainty due …………………..

It is suggested that working out is completed on a separate piece of paper and the final answers are copied to the spaces below. Hand in the working out with the answers, ensuring the working out is well organised and easy to follow.

1. Convert the following to relative uncertainties:

a. 2.70 ± 0.05 cm /1

b. 12.02 ± 0.08 cm/1

2. Convert the following to absolute uncertainties:

a. 3.5 cm ± 10 % /1

b. 16 s ± 8 %/1

3. Complete the following, determining the appropriate uncertainty:

a. (2.70 ± 0.05 cm) + (12.02 ± 0.08 cm)/1

b. (2.70 ± 0.05 cm) − (12.02 ± 0.08 cm)/1

c. (2.70 ± 0.05 cm) + (3.5 cm ± 10 %)/1

4. Complete the following, determining the appropriate uncertainty:

a. (2.70 ± 0.05 cm) × (12.02 ± 0.08 cm)/1

b. (12.02 ± 0.08 cm) ÷ (16 s ± 8 %)/1

c. (3.5 cm ± 10 %) × (2.70 ± 0.05 cm) ÷ (16 s ± 8 %)/1

5. Complete the following, determining the appropriate uncertainty:

a. 2 × (2.70 ± 0.05 cm)/1

b. 2 × (16 s ± 8 %)/1

c. (12.02 ± 0.08 cm)2/1

6. Complete the following determining the appropriate uncertainty:

a. (12.02 ± 0.08 cm)2 ÷ (3.5 cm ± 10 %)/1

b. (12.02 ± 0.08 cm)2 + (3.5 cm ± 10 %) × (2.70 ± 0.05 cm)/1

c. [(3.5 cm ± 10%) + (2.70 ± 0.05 cm)] / (16 s ± 8%)/1

d. 4π2/(0.034 ± 0.004 s2/cm)/1

7. Determine the perimeter and area of a rectangle of length 9.2 ± 0.05 cm and width 4.33 ± 0.01 cm, stating the percentage and absolute uncertainty.

/1 Mark: /19

Assignment 0.4: Using a micrometer screw gauge and Vernier callipers, digital balance and combining errors

Tip: Show all raw measurements clearly. Show all subsequent steps in your working clearly. Underline final answer with units, to a suitable number of significant figures. Include the percentage error for all final answers. Marks awarded for presentation.

1. Find the volume of the Perspex block

2. Find the density of Perspex

3. Find the mean diameter of the ball bearing.

4. Calculate the volume of the ball bearing.

5. Calculate the density of the steel of the ball bearing.

6. Find the area of a sheet of A4 paper.

7. Find the volume of a sheet of A4 paper. Explain how you did this to make it accurate.

8. Find the density of water. (Tip – use a measuring cylinder)

9. Copper has a density of 8.0 g cm-3. By measurement find the volume of copper in the copper pipe, and calculate the mass of the pipe.

10. Use a top pan balance to find the mass of the copper pipe.Account for any discrepancy between the measured and calculated mass.

Drawing and interpreting graphs

The standard for drawing graphs in A level Physics is set out here (adapted from AQA GCE Physics A Teacher Resource Bank ISA/PSA Guidance). Please ensure all graphs drawn meet this standard. Regularly refer to this page until you are familiar with the standard required and confident at producing suitable graphs.

· Graphs should be plotted on A4 graph paper with either 1 mm or 2 mm squares (it is advisable that you purchase a pad of suitable graph paper).

· Graph scales should have sensible divisions on which points can be easily plotted and read multiples of 1, 2, 5, 8 (i.e. not generally in multiples of 3, 4, 6, 7, 9 etc).

· Axes should be labelled with the plotted quantity and unit, ie quantity/unit.

· The scale should be chosen so that the plotted points occupy as large an area of the paper as possible. A scale would be deemed too small if the plotted points do not occupy at least half the length of each axis. In some cases this will require starting either or both axes at a suitable non-zero value.

· Notwithstanding the previous point, ensure that a y-intercept (i.e. 0, c) can be plotted, therefore an x-axis with a non-zero start point should be an extremely rare exception.

· It is good practice to ensure that all graphs have an appropriate title that describes the data shown.

· The plotted points should be represented as a small horizontal cross ‘+’ (preferred) or a small diagonal cross ‘×’ (less accurate). Generally, a plotted point would be deemed as correctly plotted if it is a distance of 0.5 mm or less from the correct position. A sharp pencil is needed.

· Lines of best fit:

· Where the plotted points suggest a straight line, the line should be drawn with approximately equal numbers of points on either side of the line. Points which are obviously anomalous should not unduly influence the line (do indicate that an anomalous point has been ignored when drawing the line of best fit).

· If the plotted points suggest a curve, a smooth curve should be drawn.

· Where a gradient is to be calculated, a suitably large triangle should be used (at least 8cm on the smallest side).

· Where a gradient is taken from two points on the graph, the points must be sufficiently far apart to be equivalent to a ‘large’ triangle as defined above.

· Where the line of best fit is a smooth curve, the gradient at a point may be found by drawing a tangent to the curve at that point.

· Where an intercept is required this can either be read directly from the axis or, in the case of axes not starting from zero, a suitable calculation may be required.

Plotting Error Bars on graphs

Data that you plot on a graph will have experimental uncertainties. These should be shown on a graph with error bars, and used to determine uncertainties in the slope and intercept.

Consider a point with coordinates and. Often does not have an error to plot, but be sure before you make this assumption.

(a) Plot a point, circled, at the point

(b) Draw lines from the circle to (if relevant , ), , and and put bars on the lines, as shown in the diagram right. These are called error bars.

http://www.rit.edu/cos/uphysics/graphing/graphingpart1.html

Use the space below to make further notes regarding drawing graphs and determining the error of their gradients.

Assignment 0.5 – Graphing and interpreting data due ……………………

For each of the following sets of data, you need to do the following:

1. Process the data (if relevant) by calculating average values, absolute and percentage errors. EXT: Dataset 4 requires the natural log ln(x) to be calculated of one of the variables to be plotted.

2. Plot a suitable graph on A4 graph paper, including (if relevant) error bars.

3. Calculate gradient and intercept.

4. EXT: Determine the equation of the graph in the form y = mx + c

All work should be neatly presented, with clear titles, properly laid out tables, appropriately drawn graphs. Work should be secured together ready for submission.

Space has been left for you to complete working out and attach your graphs. Graphs should be completed on A4.

Data set 1 – simple linear relationship (no error bars needed on points)

Current /mA

Voltage /V

0

1.49

2

1.47

5

1.44

8

1.41

10

1.39

13

1.36

16

1.33

20

1.29

22

1.27

25

1.24

28

1.21

Data set 2 – data with multiple repeats, requires average to be calculated and then plotted with error bars

Height to fall /m

Time /s

1

2

3

0.2

0.25

0.22

0.20

0.4

0.72

0.30

0.27

0.6

0.72

0.37

0.35

0.8

0.04

0.42

0.40

1.0

0.56

0.43

0.43

1.2

0.31

0.50

0.50

1.4

0.46

0.53

0.55

1.6

0.50

0.58

0.58

1.8

0.19

0.60

0.59

2.0

0.62

0.63

0.64

For this, calculate the average time and then calculate time2. Plot height vs time2.

Data set 3 – data with a large scatter

Hubble’s 1929 Cepheid Variable data

Distance /Mpc

Recessional velocity /km s-1

0.032

170

0.034

290

0.45

200

0.5

290

0.5

270

0.63

200

0.8

300

0.9

650

0.9

150

0.9

500

1

920

1.1

450

1.1

500

1.4

500

1.7

960

2

500

2

850

2

1090

EXTENSION: Data set 4 – data with an exponential relationship

Radioactive Decay of Protactinium-234

Time /s

Activity /count

1

2

3

0

382

510

530

10

445

372

320

20

381

461

431

30

413

377

366

40

236

388

332

50

249

309

311

60

166

243

201

70

167

246

156

80

132

290

266

90

247

183

199

100

79

95

196

Plot a graph of time vs. ln (average activity)

For further reading and activities have a look at http://www.batesville.k12.in.us/physics/apphynet/Measurement/Measurement_Intro.html

1

Topic 0

-

Practical Skills

Name:_____________________________________ Date: _________________

Assess yourself with these

criteria

Teacher Comments

L

K

J

What you need to do to

improve

Making measurements

and resolution

·

Micrometer

·

Vernier callipers

·

U

se of fiducial marks

·

Improving Precision

·

Improving Accuracy

·

Improving R

eproducability and repeatability

A simple measurement (really simple)

Sources of Uncertainty

random and systematic

errors

Handling

Uncertainty

·

Absolute, fractional and p

ercentage uncertainties

·

Combining uncertainties

Drawing Graphs and

interpreting

graphs

·

Using error bars on a graph

·

Determining uncertainties in the gradient and

intercept

#

Assignment Title

Student

Self

-

Assessment

Teacher Comment

Grade (1

-

4)

(1 =

high)

0.

1

Sources of error

pendulum timing

0.

2

Uncertainty in Readings

0.3

Handling Uncertainty

0.4

Practical measurements

with errors

0.5

Drawing and interpreting

graphs

0.6

Assessed Experiment

/ 20 marks


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