Material Testing Report
MAT9695
EH119HPB
Prepared for:
Borealis Brasil S.A.
Av. Osvaldo Berto 700 - Distrito Industrial Alfredo Rela
Sao Paulo, - 13255-840
Brazil
Prepared by:
Beaumont Advanced Processing
6100 West Ridge Rd
Erie, PA 16506
USA
Prepared on:
12 December, 2019
Report Created By:
David Schmidt
Materials Lab Engineer
12 December, 2019
© Beaumont Advanced Processing 2019. This report may not be reproduced.
Test results relate only to the item tested. Autodesk disclaims all warranties express or implied, including warranties of merchantability and fitness for a particular purpose. Beaumont Advanced Processing expressly disclaims all incidental and consequential damages that may arise from the use of this information.
Contents
Summary ......................................................................................................................... 4
Viscosity ........................................................................................................................ 10
Thermal conductivity ..................................................................................................... 16
Specific heat .................................................................................................................. 18
Pressure-Volume-Temperature ..................................................................................... 20
Shrinkage ...................................................................................................................... 23
Mechanical .................................................................................................................... 29
Elastic modulus and Poisson's ratio ........................................................................... 29
Shear modulus .......................................................................................................... 30
Nonlinear Mechanical Model .................................................................................... 31
Coefficient of linear thermal expansion .................................................................... 33
Mold verification ........................................................................................................... 34
Contact details .............................................................................................................. 37
mat9695 Summary
Beaumont Advanced Processing EH119HPB Page 4 of 37
Summary
Description
Family name POLYPROPYLENES (PP)
Trade name EH119HPB
Manufacturer Borealis South America
Family abbreviation PP
Material structure Crystalline
Data source Beaumont Advanced Processing : pvT-Measured : mech-Measured
Date last modified 12-DEC-19
Date tested 12-DEC-19
Data status Non-Confidential
Material ID 60695
Grade code mat9695
Supplier code BOREALSA
Fibers/fillers 12% Talc Filled
Recommended Processing
Mold surface temperature 45.00 °C
Melt temperature 240.00 °C
Mold temperature range (recommended)
Minimum 30.00 °C
Maximum 60.00 °C
Melt temperature range (recommended)
Minimum 220.00 °C
Maximum 260.00 °C
Absolute maximum melt temperature 280.00 °C
Ejection temperature 121.00 °C
Maximum shear stress 0.25 MPa
Maximum shear rate 100000 1/s
Maximum shear stress and maximum shear rate values have been supplemented with generic estimates.
mat9695 Summary
Beaumont Advanced Processing EH119HPB Page 5 of 37
Rheological Properties
Cross WLF Viscosity Model
n 0.26492
Tau 31124.2 Pa
D1 1.70305e+015 Pa-s
D2 263.15 K
D3 0 K/Pa
A1 34.890
A2 51.600 K
Juncture loss method coefficients
C1 4.862e-005 Pa^(1-c2)
C2 2.098
Transition temperature
Ttrans 131.00 °C
Moldflow Viscosity Index VI(240)56
Melt mass-flow rate (MFR)
Temperature 230 °C
Load 2.16 kg
Measured MFR 35.0 g/10min
mat9695 Summary
Beaumont Advanced Processing EH119HPB Page 6 of 37
Thermal Properties
Specific heat data
Temperature (T)
°C
Specific heat (Cp)
J/kg-°C
Heating/Cooling rate
°C/s
248.93 3068.1 -0.33
239.67 3049.1 -0.33
191.19 2855.0 -0.33
139.61 2646.4 -0.33
136.52 2641.2 -0.33
134.46 2690.8 -0.33
131.42 3503.2 -0.33
129.53 6513.6 -0.33
127.92 12333.0 -0.33
127.15 13432.0 -0.33
126.25 12436.0 -0.33
122.9 6297.5 -0.33
120.45 4028.6 -0.33
117.07 3093.9 -0.33
114.95 2883.3 -0.33
109.76 2730.1 -0.33
102.53 2709.5 -0.33
92.18 2504.1 -0.33
80.804 2359.6 -0.33
58.089 2182.0 -0.33
30.235 1967.2 -0.33
Thermal conductivity data
Temperature (T)
°C
Thermal conductivity
(k) W/m-°C
Heating/Cooling rate
°C/s
260.00 0.244 0.0
240.00 0.250 0.0
220.00 0.256 0.0
200.00 0.260 0.0
180.00 0.267 0.0
160.00 0.272 0.0
140.00 0.377 0.0
120.00 0.391 0.0
100.00 0.402 0.0
80.00 0.404 0.0
65.00 0.404 0.0
mat9695 Summary
Beaumont Advanced Processing EH119HPB Page 7 of 37
PVT Properties
Melt density 0.8287 g/cm3
Solid density 1.0098 g/cm3
2-domain Tait PVT model coefficients
b5 431.15 K
b6 1.285e-007 K/Pa
b1m 0.001139 m3/kg
b2m 8.263e-007 m3/kg-K
b3m 9.89742e+007 Pa
b4m 0.005883 1/K
b1s 0.001067 m3/kg
b2s 5.790e-007 m3/kg-K
b3s 1.58688e+008 Pa
b4s 0.004609 1/K
b7 0.000072 m3/kg
b8 0.2098 1/K
b9 3.153e-008 1/Pa
mat9695 Summary
Beaumont Advanced Processing EH119HPB Page 8 of 37
Mechanical Properties
Mechanical properties data Elastic modulus, 1st principal direction [E1] 1720 MPa
Elastic modulus, 2nd principal direction [E2] 1472.75 MPa
Poisson's ratio [v12] 0.3620
Poisson's ratio [v23] 0.3620
Shear modulus [G12] 592.900 MPa
Transversely isotropic coefficient of thermal expansion [CTE] data Alpha1 6.480e-005 1/°C
Alpha2 8.180e-005 1/°C
Nonlinear Mechanical property data
Sigma Zero 12.1947 MPa
N 7.54463
Alpha 1
Beta 1
Eig 0
Matrix Modulus 1665.23 MPa
Matrix Poisson’s Ratio 0
Fiber Modulus 0 MPa
Fiber Poisson’s Ratio 0
Maximum Von Mises matrix stress at failure 15.5463 MPa
A1 0 1/ MPa2
A2 0 1/ MPa2
A4 0 1/ MPa2
Temperature 23.0 C
Relative Humidity 50.0 %
Strain rate 0.000833 1/s
The nonlinear mechanical data are derived from RO Library Version 2.
mat9695 Summary
Beaumont Advanced Processing EH119HPB Page 9 of 37
Shrinkage Properties
Corrected residual in-mold stress (CRIMS) model coefficients A1 0.634249
A2 -0.194852
A3 -0.000295
A4 0.512682
A5 -0.340556
A6 0.001569
Residual strain model coefficients Parallel Perpendicular
A1 0.072685 0.063712
A2 0.000482 0.000896
A3 -0.000169 -0.000116
A4 5.374e-008 1.2652e-007
A5 0.002461 0.003879
The shrinkage models shown above are valid for Autodesk Moldflow Insight 2018 Revision 2 and later. Shrinkage models for previous software versions are included in the 21000.udb file.
Filler Properties
Filler data Description Weight %
Talc 12
mat9695 Viscosity
Beaumont Advanced Processing EH119HPB Page 10 of 37
Viscosity
Method: AMPL Test Method
Instrument: Arburg Allrounder 270S Injection Molding Machine
Test Specifications: Sample Form: Pellets
Pre-Processing: Dried at 90°C for 2 hours in a hopper dryer
Moisture Level: 0.0026 %
Capillary A: Length: 31.9693 mm
L/D: 15.98465
Die Entry Angle: 90 degrees
Capillary B: Length: 7.9731 mm
L/D: 3.98655
Die Entry Angle: 90 degrees
Barrel Diameter: 30 mm
Plastication Time: 20 sec
Dwell Time: 20 sec
Corrections: Bagley, Rabinowitsch and shear heating
Date Received: 14-NOV-19
Date Tested: 27-NOV-19
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing.
mat9695 Viscosity
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Apparent Viscosity Data
Temperature
(°C)
Apparent Shear Rate
(sec-1)
Apparent Viscosity (Pa-s)
Die Diameter
(mm)
Die L/D (-)
208.7 25588 12.09 2.00 15.98
208.8 196 243.36 2.00 15.98
209.7 1352 85.37 2.00 15.98
209.8 319 194.75 2.00 15.98
209.8 773 118.85 2.00 15.98
209.8 2589 57.31 2.00 15.98
209.8 12760 18.98 2.00 15.98
209.8 64538 6.62 2.00 15.98
210.8 6476 31.10 2.00 15.98
223.8 203 166.78 2.00 15.98
223.8 319 138.56 2.00 15.98
224.8 781 87.95 2.00 15.98
224.8 1351 65.59 2.00 15.98
224.8 2601 44.73 2.00 15.98
224.8 12744 16.96 2.00 15.98
224.8 25587 10.72 2.00 15.98
224.8 64429 5.96 2.00 15.98
225.8 6474 25.97 2.00 15.98
237.8 201 141.86 2.00 15.98
238.7 64080 5.50 2.00 15.98
238.8 320 114.44 2.00 15.98
238.8 25582 9.68 2.00 15.98
239.8 771 74.44 2.00 15.98
239.8 1349 54.89 2.00 15.98
239.8 2592 38.17 2.00 15.98
239.8 6468 22.51 2.00 15.98
239.8 12784 14.91 2.00 15.98
252.8 199 137.14 2.00 15.98
253.8 322 110.79 2.00 15.98
253.8 778 72.38 2.00 15.98
253.8 25545 8.79 2.00 15.98
253.8 64144 5.04 2.00 15.98
254.7 12801 13.28 2.00 15.98
254.8 1351 54.64 2.00 15.98
254.8 2606 37.44 2.00 15.98
254.8 6476 22.31 2.00 15.98
217.9 319 272.30 2.00 3.99
218.9 1352 120.19 2.00 3.99
219.0 196 343.34 2.00 3.99
219.0 773 165.78 2.00 3.99
219.0 2589 80.25 2.00 3.99
219.0 12760 30.79 2.00 3.99
219.0 25588 20.61 2.00 3.99
219.9 64538 11.89 2.00 3.99
mat9695 Viscosity
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Temperature
(°C)
Apparent Shear Rate
(sec-1)
Apparent Viscosity (Pa-s)
Die Diameter
(mm)
Die L/D (-)
221.0 6476 45.75 2.00 3.99
236.0 319 187.62 2.00 3.99
236.0 781 121.14 2.00 3.99
236.0 1351 91.82 2.00 3.99
236.0 2601 63.71 2.00 3.99
236.0 12744 25.49 2.00 3.99
236.0 25587 17.19 2.00 3.99
236.0 64429 10.48 2.00 3.99
236.4 6474 38.29 2.00 3.99
237.0 203 230.86 2.00 3.99
251.0 1349 74.57 2.00 3.99
251.0 2592 52.58 2.00 3.99
251.0 6468 32.07 2.00 3.99
251.9 12784 21.87 2.00 3.99
251.9 64080 9.55 2.00 3.99
252.0 771 98.76 2.00 3.99
252.0 25582 14.97 2.00 3.99
253.0 320 151.29 2.00 3.99
254.0 201 193.28 2.00 3.99
266.0 2606 45.74 2.00 3.99
267.0 778 84.42 2.00 3.99
267.0 1351 64.12 2.00 3.99
267.0 6476 28.01 2.00 3.99
267.0 25545 13.42 2.00 3.99
267.1 12801 19.41 2.00 3.99
268.0 322 132.18 2.00 3.99
268.0 64144 8.56 2.00 3.99
269.0 199 170.98 2.00 3.99
mat9695 Viscosity
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Calculated Viscosity
Temperature
(°C)
Shear Rate (sec-1)
Calculated Viscosity
(Pa-s)
208.7 25588 7.02
208.8 196 199.66
209.7 1352 57.19
209.8 319 147.75
209.8 773 83.59
209.8 2589 36.33
209.8 12760 11.57
209.8 64538 3.54
210.8 6476 18.76
217.9 319 136.95
218.9 1352 53.40
219.0 196 179.81
219.0 773 77.67
219.0 25588 6.57
219.0 12760 10.89
219.0 2589 34.05
219.9 64538 3.32
221.0 6476 17.54
223.8 203 167.99
223.8 319 129.94
224.8 781 73.78
224.8 2601 32.65
224.8 12744 10.52
224.8 1351 51.25
224.8 25587 6.34
224.8 64429 3.23
225.8 6474 17.02
236.0 781 67.82
236.0 25587 5.95
236.0 1351 47.42
236.0 319 116.51
236.0 2601 30.38
236.0 64429 3.03
236.0 12744 9.85
236.4 6474 15.96
237.0 203 147.45
237.8 201 147.13
238.7 64080 3.00
238.8 320 113.42
238.8 25582 5.86
239.8 6468 15.67
239.8 1349 46.26
mat9695 Viscosity
Beaumont Advanced Processing EH119HPB Page 14 of 37
Temperature
(°C)
Shear Rate (sec-1)
Calculated Viscosity
(Pa-s)
239.8 2592 29.74
239.8 771 66.48
239.8 12784 9.62
251.0 2592 27.79
251.0 6468 14.72
251.0 1349 42.97
251.9 64080 2.80
251.9 12784 9.01
252.0 771 60.91
252.0 25582 5.46
252.8 199 127.93
253.0 320 100.35
253.8 322 99.41
253.8 778 59.80
253.8 25545 5.42
253.8 64144 2.78
254.0 201 125.93
254.7 12801 8.88
254.8 1351 41.93
254.8 6476 14.41
254.8 2606 27.09
266.0 2606 25.43
267.0 6476 13.53
267.0 25545 5.09
267.0 778 54.61
267.0 1351 38.86
267.1 12801 8.35
268.0 322 88.33
268.0 64144 2.60
269.0 199 109.98
mat9695 Viscosity
Beaumont Advanced Processing EH119HPB Page 15 of 37
Rheological Data
Cross WLF Viscosity Model
n 0.26492
Tau 31124.2 Pa
D1 1.70305e+015 Pa-s
D2 263.15 K
D3 0 K/Pa
A1 34.890
A2 51.600 K
Juncture loss method coefficients
C1 4.862e-005 Pa^(1-c2)
C2 2.098
1.0E+0
1.0E+1
1.0E+2
1.0E+3
1.0E+1 1.0E+2 1.0E+3 1.0E+4 1.0E+5
Vis
cosi
ty (
Pa
-s)
Shear rate (1/s)
Viscosity vs shear rate
T = 220 °C T = 240 °C T = 260 °C
mat9695 Thermal conductivity
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Thermal conductivity
Method: ISO 22007-2, Plastics - Determination of thermal conductivity and thermal diffusivity - Part 2: Transient plane heat source (hot disc) method
Instrument: Hot Disk TPS 2500 S Thermal Constants Analyser
Test Specifications: Sample Form: 19 mm disks (2) machined from molded plaque
Pre-Processing: N/A
Moisture Level: DAM (Dry As Molded)
Sensor Specification Hot Disk 5465 3.189mm Kapton sensor
Measurement Time 10 sec
Heating Power 47 mW
Date Received: 14-NOV-19
Date Tested: 11-DEC-19
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing.
mat9695 Thermal conductivity
Beaumont Advanced Processing EH119HPB Page 17 of 37
Thermal conductivity data
Temperature (T) °C
Thermal conductivity (k) W/m-°C
Heating/Cooling rate °C/s
260.00 0.244 0.0
240.00 0.250 0.0
220.00 0.256 0.0
200.00 0.260 0.0
180.00 0.267 0.0
160.00 0.272 0.0
140.00 0.377 0.0
120.00 0.391 0.0
100.00 0.402 0.0
80.00 0.404 0.0
65.00 0.404 0.0
0.00
0.10
0.20
0.30
0.40
0.50
0.60
0 50 100 150 200 250 300
Ther
mal
co
nd
uct
ivit
y, k
(W
/m-°
C)
Temperature (°C)
Thermal conductivity vs temperature
mat9695 Specific heat
Beaumont Advanced Processing EH119HPB Page 18 of 37
Specific heat
Method: ASTM E 1269, Standard Test Method for Determining Specific Heat Capacity by Differential Scanning Calorimetry ASTM D 3418, Standard Test Method for Transition Temperatures and Enthalpies of Fusion and Crystallization of Polymers by Differential Scanning Calorimetry
Instrument: TA Instruments Discovery Differential Scanning Calorimeter
Test Specifications: Sample Form: Pellets
Pre-Processing: Dried at 90°C for 2 hours in a hopper dryer
Moisture Level: 0.0061 %
Initial Temperature: 260°C
Final Temperature: 20°C
Cooling Rate: -20°C/min
Equilibrium Time: 3 min
Sample holder material: Aluminum
Sample holder volume: 40 µl
Sample holder mass: 53 mg (pan+lid)
Purge gas: 99.99% pure nitrogen
Purge gas flow rate: 50 ml/min
Date Received: 14-NOV-19
Date Tested: 21-NOV-19
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing.
mat9695 Specific heat
Beaumont Advanced Processing EH119HPB Page 19 of 37
Specific heat data
Temperature (T)
°C
Specific heat (Cp)
J/kg-°C
Heating/Cooling
rate °C/s
248.93 3068.1 -0.33
239.67 3049.1 -0.33
191.19 2855.0 -0.33
139.61 2646.4 -0.33
136.52 2641.2 -0.33
134.46 2690.8 -0.33
131.42 3503.2 -0.33
129.53 6513.6 -0.33
127.92 12333.0 -0.33
127.15 13432.0 -0.33
126.25 12436.0 -0.33
122.9 6297.5 -0.33
120.45 4028.6 -0.33
117.07 3093.9 -0.33
114.95 2883.3 -0.33
109.76 2730.1 -0.33
102.53 2709.5 -0.33
92.18 2504.1 -0.33
80.804 2359.6 -0.33
58.089 2182.0 -0.33
30.235 1967.2 -0.33
Ttrans 131.00 °C
Ejection temperature 121.00 °C
0
2000
4000
6000
8000
10000
12000
14000
16000
0 50 100 150 200 250 300
Spec
ific
hea
t, C
p (
J/kg
-°C
)
Temperature (°C)
Specific heat vs temperature
mat9695 Pressure-Volume-Temperature
Beaumont Advanced Processing EH119HPB Page 20 of 37
Pressure-Volume-Temperature
Method: High Pressure Indirect Dilatometry Instrument: Gnomix pvT Apparatus Test Specifications:
Sample Form: Molded Plaque
Pre-Processing: Not required
Scan type: Isothermal Cooling
Date Received: 14-NOV-19
Date Tested: 22-NOV-19
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing.
mat9695 Pressure-Volume-Temperature
Beaumont Advanced Processing EH119HPB Page 21 of 37
pvT Experimental Data
Temperature (°C)
Pressure (MPa)
0MPa 50MPa 100MPa 150MPa 200MPa
36.66 0.9987 0.9846 0.9721 0.9614 0.9516
49.97 1.0060 0.9904 0.9773 0.9662 0.9560
63.99 1.0120 0.9959 0.9820 0.9704 0.9599
77.92 1.0200 1.0020 0.9868 0.9746 0.9637
92.48 1.0280 1.0080 0.9918 0.9789 0.9677
106.70 1.0370 1.0150 0.9976 0.9839 0.9719
121.20 1.0470 1.0220 1.0030 0.9888 0.9762
136.30 1.0600 1.0310 1.0110 0.9948 0.9814
151.70 1.0810 1.0430 1.0190 1.0020 0.9874
166.70 1.1470 1.0990 1.0430 1.0120 0.9952
182.10 1.1600 1.1080 1.0760 1.0520 1.0320
197.70 1.1720 1.1160 1.0830 1.0580 1.0380
213.60 1.1850 1.1260 1.0900 1.0640 1.0430
228.90 1.1980 1.1340 1.0970 1.0700 1.0490
238.90 1.2060 1.1390 1.1010 1.0740 1.0520
248.80 1.2150 1.1450 1.1060 1.0780 1.0560
263.40 1.2270 1.1510 1.1090 1.0790 1.0570
mat9695 Pressure-Volume-Temperature
Beaumont Advanced Processing EH119HPB Page 22 of 37
Melt density 0.8287 g/cm3
Solid density 1.0098 g/cm3
2-domain Tait PVT model coefficients
b5 431.15 K
b6 1.285e-007 K/Pa
b1m 0.001139 m3/kg
b2m 8.263e-007 m3/kg-K
b3m 9.89742e+007 Pa
b4m 0.005883 1/K
b1s 0.001067 m3/kg
b2s 5.790e-007 m3/kg-K
b3s 1.58688e+008 Pa
b4s 0.004609 1/K
b7 0.000072 m3/kg
b8 0.2098 1/K
b9 3.153e-008 1/Pa
0.89
0.94
0.99
1.04
1.09
1.14
1.19
1.24
1.29
20 70 120 170 220 270
Spec
ific
vo
lum
e (c
m^3
/g)
Temperature (°C)
Specific volume vs temperature
0 MPa 50 MPa 100 MPa 150 MPa 200 MPa
mat9695 Shrinkage
Beaumont Advanced Processing EH119HPB Page 23 of 37
Shrinkage
Method: AMPL Shrinkage Test Method (QOP-17-M)
Instrument: Krauss Maffei KM160-750CX Injection molding machine Test mold inscribed with a fine grid pattern Temperature and Humidity Controlled Room OGP Smartscope Flash 400 metrology system
Test Specifications: Sample Form: Pellets
Pre-Processing: Dried at 90°C for 2 hours in a hopper dryer
Moisture Level: 0.0061 %
Date Molded: 21-NOV-19
Post-Processing: Conditioned at 23°C / 50% relative humidity for 7 days
Date Measured: 02-DEC-19
Shrinkage Data Correlated With: Moldflow Insight 2018 Revision 2
Default Shrinkage Model: Residual Stress (CRIMS)
Date Received: 14-NOV-19
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing. Shrinkage measurements have been corrected to account for mold thermal expansion. Data for some process conditions may have been removed in the determination of the favored model.
mat9695 Shrinkage
Beaumont Advanced Processing EH119HPB Page 24 of 37
Shrinkage Experimental Data
Process Condition
Melt Temperature
(°C)
Mold Temperature
(°C)
Flow Rate (cc/sec)
Part Thickness (mm)
Packing Pressure
(MPa)
Packing Time (sec)
Cooling Time (sec)
1 220.5 47.9 37.4 2 37.3 15.5 10
2 217.9 45.4 37.4 2 51.7 15.5 10
3 218.4 45.7 37.4 2 66.3 15.5 10
4 218.6 47.4 19.0 2 51.6 15.5 10
5 219.7 46.0 63.5 2 51.7 15.5 10
6 240.9 45.3 39.7 2 27.5 16.5 10
7 241.3 46.8 38.5 2 46.8 16.5 10
8 240.9 47.8 42.3 2 66.2 16.5 10
9 240.9 45.4 18.4 2 46.6 16.5 10
10 240.9 46.7 55.2 2 46.8 16.5 10
11 240.7 47.1 21.0 1 46.9 6.5 10
12 241.1 47.8 21.0 1 66.3 6.5 10
13 242.1 47.9 22.4 1 85.8 6.5 10
14 241.0 46.7 10.2 1 66.1 6.5 10
15 241.4 47.2 32.5 1 66.4 6.5 10
16 240.5 48.0 41.8 3 27.4 31 10
17 240.9 44.8 41.8 3 41.9 31 10
18 240.7 46.7 41.8 3 56.3 31 10
19 240.2 46.1 19.8 3 41.7 31 10
20 240.3 46.4 76.9 3 41.9 31 10
21 260.7 46.5 39.7 2 27.4 17.5 10
22 262.8 47.5 39.7 2 41.9 17.5 10
23 260.2 48.4 41.0 2 56.5 17.5 10
24 261.8 48.8 18.7 2 41.8 17.5 10
25 261.1 49.7 57.7 2 42.0 17.5 10
mat9695 Shrinkage
Beaumont Advanced Processing EH119HPB Page 25 of 37
Part Shrinkage
Process Condition Average Measured Parallel
Average Measured Perpendicular
Average Predicted Volumetric
1 0.533% 0.670% 5.144%
2 0.458% 0.594% 4.094%
3 0.357% 0.494% 3.230%
4 0.463% 0.618% 4.043%
5 0.446% 0.564% 4.046%
6 0.574% 0.717% 5.749%
7 0.456% 0.608% 4.299%
8 0.361% 0.489% 3.101%
9 0.463% 0.635% 4.243%
10 0.466% 0.588% 4.293%
11 0.570% 0.604% 6.850%
12 0.468% 0.504% 5.549%
13 0.342% 0.392% 4.819%
14 0.510% 0.541% 4.732%
15 0.450% 0.502% 5.579%
16 0.591% 0.768% 4.741%
17 0.498% 0.662% 3.767%
18 0.413% 0.579% 2.968%
19 0.516% 0.690% 3.861%
20 0.504% 0.650% 3.692%
21 0.579% 0.732% 5.666%
22 0.507% 0.642% 4.569%
23 0.421% 0.568% 3.624%
24 0.494% 0.679% 4.492%
25 0.508% 0.647% 4.540%
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Residual Stress Coefficients
Corrected residual in-mold stress (CRIMS) model coefficients
A1 0.634249
A2 -0.194852
A3 -0.000295
A4 0.512682
A5 -0.340556
A6 0.001569
Residual Strain Coefficients
Parallel
Coefficient Lower Limit Upper Limit Centroid
1 0.072685 0.025727 0.085079 0.044199
2 0.000482 0.013278 0.77153 0.34305
3 -0.000169 5.1235 24.752 11.721
4 5.374e-008 3423.00 48639.00 17677.00
5 0.002461 0 0 0
Perpendicular
Coefficient Lower Limit Upper Limit Centroid
1 0.063712 0.025727 0.085079 0.044199
2 0.000896 0.013278 0.77153 0.34305
3 -0.000116 5.1235 24.752 11.721
4 1.2652e-007 2154.30 6624.70 3506.10
5 0.003879 0 0 0
The shrinkage models shown above are valid for Autodesk Moldflow Insight 2018 Revision 2 and later. Shrinkage models for previous software versions are included in the 21000.udb file.
Observed Shrinkage
Observed nominal shrinkage
Parallel 0.478%
Perpendicular 0.605%
Observed shrinkage
Minimum Parallel 0.342%
Maximum Parallel 0.591%
Minimum Perpendicular 0.392%
Maximum Perpendicular 0.768%
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Residual Stress Plots
0.00%
0.20%
0.40%
0.60%
0.80%
1.00%
1.20%
1.40%
0 5 10 15 20 25 30
Shri
nka
ge (%
)
Process conditions
Parallel shrinkage
Experimental value Predicted (with CRIMS) Predicted (without CRIMS)
0.00%
0.20%
0.40%
0.60%
0.80%
1.00%
1.20%
1.40%
1.60%
0 5 10 15 20 25 30
Shri
nka
ge (%
)
Process conditions
Perpendicular shrinkage
Experimental value Predicted (with CRIMS) Predicted (without CRIMS)
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Residual Strain Plots
0.00%
0.10%
0.20%
0.30%
0.40%
0.50%
0.60%
0.70%
0 10 20 30 40 50 60 70 80 90 100
Shri
nka
ge (%
)
Process conditions
Parallel shrinkage
Experimental Prediction
0.00%
0.10%
0.20%
0.30%
0.40%
0.50%
0.60%
0.70%
0.80%
0.90%
0 10 20 30 40 50 60 70 80 90 100
Shri
nka
ge (%
)
Process conditions
Perpendicular shrinkage
Experimental Prediction
mat9695 Mechanical
Beaumont Advanced Processing EH119HPB Page 29 of 37
Mechanical
Elastic modulus and Poisson's ratio
Method: ASTM D 638, Standard Test Method for Tensile Properties of Plastics ASTM E 132, Standard Test Method for Poisson's Ratio at Room Temperature
Instrument: MTS Sintech 5/G Universal Testing Machine
Test Specifications: Specimens Tested: 8 (per direction)
Pre-Processing: 23°C +/-2°C at 50% +/-5% relative humidity for a minimum of 40 hours
Sample Form: Machined from molded plaques
Test Speed: 5 mm/min
Date Received: 14-NOV-19
Date Tested: 26-NOV-19
Operator’s Notes: Testing was performed per standard testing procedures. Inconsistent results seen for V23. V23 made equal to V12 for isotropic behavior.
Elastic modulus
Elastic modulus, 1st principal direction [E1] 1720 MPa
Elastic modulus, 2nd principal direction [E2] 1472.75 MPa
Poisson's ratio
Poisson's ratio [v12] 0.3620
Poisson's ratio [v23] 0.3620
mat9695 Mechanical
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Shear modulus
Method: ASTM D 638, Standard Test Method for Tensile Properties of Plastics
Instrument: MTS Sintech 5/G Universal Testing Machine
Test Specifications: Specimens Tested: 8
Pre-Processing: 23°C +/-2°C at 50% +/-5% relative humidity for a minimum of 40 hours
Sample Form: Machined from molded plaques
Test Speed: 5 mm/min
Date Received: 14-NOV-19
Date Tested: 26-NOV-19
Operator’s Notes: Shear modulus is calculated using orthotropic elasticity from the tensile modulus measured on a sample cut at an angle of 45° with the flow direction. Testing was performed per standard testing procedures. No anomalies were noted during testing.
Shear modulus
Shear modulus [G12] 592.900 MPa
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Nonlinear Mechanical Model
Method: ASTM D 638, Standard Test Method for Tensile Properties of Plastics
Instrument: MTS Sintech 5/G Universal Testing Machine
Test Specifications: Specimens Tested: 8 (per direction)
Pre-Processing: 23°C +/-2°C at 50% +/-5% relative humidity for a minimum of 40 hours
Sample Form: Machined from molded plaques
Test Speed: 5 mm/min
Date Received: 14-NOV-19
Date Tested: 26-NOV-19
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing.
Ramberg Osgood Parameter (Tension)
Sigma Zero 12.1947 MPa
n 7.54463
Alpha 1
Beta 1
Eig 0
Matrix Modulus 1665.23 MPa
Matrix Poisson’s Ratio 0
Fiber Modulus 0 MPa
Fiber Poisson’s Ratio 0
Maximum Von Mises matrix Stress at failure 15.5463 MPa
A1 0 1/MPa2
A2 0 1/MPa2
A4 0 1/MPa2
Temperature 23.0 C
Relative Humidity 50.0 %
Strain Rate 0.000833 1/s
The nonlinear mechanical data are derived from RO Library Version 2.
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0
2
4
6
8
10
12
14
16
18
0 0.01 0.02 0.03 0.04 0.05 0.06
Stre
ss (
MP
a)
Strain (-)
Nonlinear Mechanical Stress vs Strain
0° Measured 0° Fitted
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Coefficient of linear thermal expansion
Method: QOP-11, Coefficient of Linear Thermal Expansion of Plastics
Instrument: Quartz tube dilatometer per ASTM
Test Specifications: Specimens Tested: 2 (per direction): test repeated 2 times per specimen
Pre-Processing: 23°C +/-2°C at 50% +/-5% relative humidity for a minimum of 40 hours
Sample Form: Machined from molded plaques
Specimen Geometry: Rectangular, 8mm x 50mm, full thickness
Temperature Range: 0°C to 60°C
Date Received: 14-NOV-19
Date Tested: 26-NOV-19
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing.
Transversely isotropic coefficient of thermal expansion [CTE] data
Alpha 1 6.480e-005 1/°C
Alpha 2 8.180e-005 1/°C
mat9695 Mold verification
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Mold verification
Method: AMPL Mold Verification Test Method (QOP-16-M)
Instrument: Krauss Maffei KM160-750CX Injection molding machine
Test Specifications: Sample Form: Pellets
Pre-Processing: Dried at 90°C for 2 hours in a hopper dryer
Moisture Level: 0.0061 %
Date Received: 14-NOV-19
Date Tested: 21-NOV-19
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing.
mat9695 Mold verification
Beaumont Advanced Processing EH119HPB Page 35 of 37
1mm tag die
Experiment Number
Flow Rate (cc/sec)
Melt Temperature
Mold Temperature
Cyc0069 6.5 240.2 45.9
Cyc0081 38.3 241.7 48
0
10
20
30
40
50
60
70
0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0
Pre
ssu
re (M
Pa)
Time (s)
Cavity Pressure vs Time
Experimental data AMI2018R2 simulation
Part thickness : 1.0 mmFlow rate : 6.5 cc/secMelt temperature : 240.2 °CMold temperature : 45.9 °C
0
10
20
30
40
50
60
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7
Pre
ssu
re (M
Pa)
Time (s)
Cavity Pressure vs Time
Experimental data AMI2018R2 simulation
Part thickness : 1.0 mmFlow rate : 38.3 cc/secMelt temperature : 241.7 °CMold temperature : 48.0 °C
mat9695 Mold verification
Beaumont Advanced Processing EH119HPB Page 36 of 37
2mm tag die
Experiment Number
Flow Rate (cc/sec)
Melt Temperature
Mold Temperature
Cyc0033 13.5 239.4 45.8
Cyc0042 55.2 241.6 48.4
0
2
4
6
8
10
12
14
0.0 0.5 1.0 1.5 2.0 2.5
Pre
ssu
re (M
Pa)
Time (s)
Cavity Pressure vs Time
Experimental data AMI2018R2 simulation
Part thickness : 2.0 mmFlow rate : 13.5 cc/secMelt temperature : 239.4 °CMold temperature : 45.8 °C
0
2
4
6
8
10
12
14
16
0.0 0.1 0.2 0.3 0.4 0.5 0.6
Pre
ssu
re (M
Pa)
Time (s)
Cavity Pressure vs Time
Experimental data AMI2018R2 simulation
Part thickness : 2.0 mmFlow rate : 55.2 cc/secMelt temperature : 241.6 °CMold temperature : 48.4 °C
Contact details
Beaumont Advanced Processing Page 37 of 37
Contact details
Beaumont Advanced Processing
6100 West Ridge Rd
Erie, PA 16506
USA
Phone: +1-814-899-6390
Fax: +1-814-899 7117
Email: [email protected]
Testing enquiries: [email protected]
Beaumont Advanced Processing website: www.bapmolding.com