+ All Categories
Home > Documents > METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent...

METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent...

Date post: 05-Jun-2018
Category:
Upload: ngonhi
View: 227 times
Download: 0 times
Share this document with a friend
18
.~ , REPORT No: NMLIMST/IAF/t.13/80/2007 Restricted Circulation October, 2007 - METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL HUBS OF A VRO HS-748 H-1517 Sponsored by Air Force Station Borjhar Kamrup District Guwahati -781017 Assa m l I ~ "h~~ Materials Science & Technology Division National Metallurgical Laboratory (Council of Scientific and Industrial Research) Jamshedpur - 831007 \
Transcript
Page 1: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

.~,REPORT No: NMLIMST/IAF/t.13/80/2007 Restricted Circulation

October, 2007-

METALLURGICAL ANALYSIS OF THE DAMAGED

WHEEL HUBS OF A VRO HS-748 H-1517

Sponsored by

Air Force Station BorjharKamrup District

Guwahati -781017Assa m

l I~

"h~~

Materials Science & Technology Division

National Metallurgical Laboratory

(Council of Scientific and Industrial Research)

Jamshedpur - 831007

\

Page 2: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

, NATIONAL METALLURGICAL LABORATORY(Council of Scientific & Industrial Research)

JAMSHEDPUR..,PROJECT COMPLETION REPORT

Project Title: METALLURGICAL ANALYSIS OF Project No. :THE DAMAGED WHEEL HUBS OF AVRO HS-748 H- Report No. NML/MST/IAFIl. I3/80/2007, Oct' 20071517 Date of Project Initiation:27.08.2007

Date of Completion: 05.10.2007Project Team Members: Class: Publ ic document (Free/Priced)Dr. M. Ghosh (PL) Restricted circulation (X)Dr. S. R. Singh (Co PL) Only to clientMr. S. K. Das SecretCustomer / Client's name and address: Classification:

Wg. Cdr. V. Mathur In-house

Technical Member of Court of Enquiry Grant-in-aid

Air Force Station, Borjhar Sponsored (X)Kamrup District, Guwahati - 78\ 0 17 ConsultancyAssam Collaborati ve

Date of Report: 05.10.2007Area: Material Characterization. Specify Type:Sub Area: Failure analysis Ongoing Area: (X)

New Area Initiated:

Key Words: Avro aircraft, wheel hub, aluminium alloy, precipitation, dispersoid, fusion, flow lines.Abstract: There was a Cat-D accident to Avro aircraft HS-748 H-1517 at Dimapur in July'07. In thataccident as soon as STBD side touches the ground, both the tyres bursted along with one of the tyres onports ide. It causes rubbing and scraping of the wheel hubs leading to permanent damage to thecomponent. It has been explored after the incident that, the brake unit and the bearings of the wheel huhswere perfectly all right.Chemical composition of base metal of wheel hub of the aircraft is close to British specification BS 2L77 of AI base alloys; however, Cu concentration is marginally higher for both the samples in comparisonto the specification. Microstructure of the base alloy exhibits grain size of ] 5-20lm with fine dispersionof AI-Cu intermetallic phases. 2nd phase occurs pre-dominantly at the grain boundary. Apart from theselarge dispersoid of Cu-O and AI-Si-Cu-O are also found. The deformed part of the wheel hub consists ofthe substrate, bend and flow region. The substrate contains both precipitate free and dencely precipitatedregion. Dissolution of precipitate is caused by localised heat generation owing to friction. Co-existenceof both grain boundary and without grain boundary region is also observed. With grain boundary regioncontains dispersoid of Cu-O and AI-Si rich phase. The bend and flow regions consist of precipitate freeregion, dencely precipitated region, finer distribution of AI-Cu phase and large 2nd phase of AI-Si andCu-O. Minor structural difference or loss of directionality at the three regions could be attributed to thelocalised incipient fusion of the alloy due to excessive fricti6nal heat. The root cause of the accident iswheel jamming during landing. Jamming is evident from the flow lines on the deformed part of the hub.Jamming results in excessive stress over the wheel hub. Hence the wheel hub deformed immediatelyafter the tire burst. The jamming is also evident from the dissolution of 2nd phases and microstructure ofthe deformed region. Actual chemical composition, processing root, mechanical properties, heattreatment schedule of that particular wheel hub were not available; hence it is difficult to remarkconclusively the exact reason of structural heterogeneity found in the investigation.Details of IPRs (PI tick): NA If no IPR taken, reasons: NAPatent

CopyrightTrade Marks

Report Issuance Authority: Dr.S.R.Singh Signature: .R.

Page 3: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

NATIONAL METALLURGICAL LABORATORY, JAMSHEDPURMETALLURGICAL ANALYSIS OFTHE DAMAGED WHEEL HUBS OF AVRO HS-748 H-1517.

REPORTNo. NML/MST/IAF/I .13/80/2007, OCTOBER 2007

BACKGROUND

There was a Cat-D accident to Avro aircraft HS-748 H-1517 at Dimapur in July'07. In

that accident as soon as STBD side touched the ground, both the tyres bursted along

with one of the tyres on ports ide. It causes rubbing and scraping of the wheel hubs

leading to permanent damage to the component. It has been told that, such kind of

accident i.e, in which three wheels was burst at a time, is very rare all over the world.

Moreover, it has been explored after the incident that, the brake unit and the bearings

of the wheel hubs were perfectly all right. The cause of failure could not be

ascertained at the operating base. Hence the two wheel hubs of STBD side have been

sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H-

1517/16 Aug 07/FS, dated 22ndAug, 2007 through Sgt. R.N. Tripathy of 59th Sqn of

IAF. The damaged components were received at NML on 27.08.2007 for the

investigation.

SCOPE OF WORK

Based on the information provided and discussions held at NML, it is decided to carry

out following assignments for detailed investigation of the wheel hubs:

I. Visual observation, photographic recording and determination of sampling

locations.

2. Microstructural analysis of the wheel hub by optical and scanning electron

microscopy.

3. Determination of chemical composition of the materials by spark erosion

technique.

4. SEM characterization of the deformed region of the failed component.

5. Hardness measurement.

6. Find out the root cause of failure.

COMPONENT'S MATERIAL AND SERVICE EXPOSURE

The Avro HS-748 H-1517 aircraft has two sets of wheel hubs, one set is on portside

and the other set on the STBD side. At the time of landing, the STBD side wheels

touched the ground ahead of few fractions of seconds than portside. The maximum

landing weight of the aircraft is 4.3x I041bs and the hubs are capable enough to

withstand the static as well as impact load during touch down. The life completed

Page 4: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

NATIONAL METALLURGICAL LABORATORY, JAMSHEDPURMETALLURGICAL ANALYSIS OFTHE DAMAGED WHEEL HUBS OF AVRO HS-748 H-1517.

REPORT No. NMLlMST/IAF/I.13/80/2007,OCTOBER 2007

since new is 124:45hrs with 101LOGS and the TBO of the same components is

1500hrs with 1500LOGS. Life completed since O/H is also 124:45hrs with 101LOGS

for the wheel hub. The under carriage of the main wheel assembly has the serial

number 5057EX and 5216EY for the damaged two wheel hubs. It has been also

reported that, the hub is made off Mg-base alloys. As per their inspection report tyre

burst during landing causes rubbing of the wheel hubs leading to severe damage to the

components.

EXPERIMENT AL RESULTS & DISCUSSIONS

From the as received damaged wheel hubs, sampling was done from one of the

components considering the symmetry for the location of failure. The sampling

location for fractographic and microstructural analysis with their nomenclature are

shown in Figs.! (a-f). All the deformed/rubbed surfaces along with the periphery of

the hubs were examined visually in reflected light to find out the appearance of the

affected regions with the extent of damage on macro scale. Bulk chemical

composition of the wheel hub was determined by Spark Erosion Technique (PMI

Master Plus). The samples were prepared by conventional metallographic technique

and etched with Keller's reagent. The samples were observed in optical microscope

(Correct SOME TRS) and scanning electron microscope (JEOL JSM 840A) to reveal

the microstructural features of the service exposed alloy. The hardness of the samples

was measured in Vickers scale (Leica) using 200gf load with ISsecs dwelling time.

The deformed region of the hubs was examined in scanning electron microscope

(SEM) to reveal the characteristics of deformation. The details of the investigation are

presented in the following subsections.

1. Visual Examination

Figs.1(a-f) exhibit the damaged wheel hubs of the aircraft. Shining deep scratch marks

along the periphery of the hubs clearly indicates heavy rubbing action (Fig.] a and b).

The span of the rubbed surface exists over a curvature length of -285mm for both the

hubs. The rubbing also causes change of plane over the periphery and the length of

each segment varies with in the range of 40-80mm (Fig.l e and f). Thus the rubbed

area consists of multiple number of planes having an angularity of 10-15° with respect

to the tangent at that location of the hub. The change of plane in rubbed zone indicates

that, wheels have been undergone rotational motion of few degrees while it dragged

2

Page 5: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

NATIONAL METALLURGICAL LABORATORY, JAMSHEDPURMETALLURGICAL ANALYSIS OF THE DAMAGED WHEEL HUBS OF AVRO HS-748 H-ISI7.

REpORTNo. NML/MST/IAF/1.I3/80/2007, OCTOBER 2007

on the runway. Both the end portion of the rubbed surface has been folded (Fig.1c and

d). The shining edge of the folded region is wavy / serrated in nature having cracks of

2-4mm length. The cracks are perpendicular to the edge of the folded region. Fig. 1a

and c shows the sampling location for fractography and metallography.

"'"

Figs. 1(a- f): Photographs of wheel hubs (5057 Ex and 5216 Ey) showing (a) and (b) asreceived damaged components having scratch marks over the periphery, (c) and (d)

folded edges at end of the failed component, (e) and (f) change of plane over theperiphery of the rubbed surface.

3

Page 6: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

NATIONAL METALLURGICAL LABORATORY, JAMSHEDPURMETALLtJRGICAL ANALYSIS OF TI-IE DAMAGED WI-IEEL I-IUBS OF AVRO I-IS-748 1-1-1517.

REPORTNo. NML/MST/IAF/113/80/2007, OCTOBER 2007

2. Chemical Composition

The concentration of major alloying elements present in the alloy is determined by

spark erosion technique. The data is furnished in Table-I. The chemical composition

resemblances with British specification of BS 2L 77 and Indian specification of IS

7902, Grade 24345.

Table 1: Chemical composition of the wheel hub (wt%).

Though it has been told that, the affected wheel hubs are made off Mg alloys, yet

chemical composition exhibits that, the alloy belongs to 2XXX series of AI-alloys.

For both the samples concentration of alloying elements varies insignificantly.

However, Cu concentration is marginally higher for both the samples in comparison

to the BS specification. Si content of sample A I is little higher with respect to

specification. Compositional deviation cannot be assessed owing non-availability of

actual alloy specification as per the OEM.

3. Microstructural Analysis

The microstructure of the base alloy as well as deformed region of the wheel hub was

examined in optical and scanning electron microscopy. Optical microstructure

(Figs.2a and b) of the base alloy exhibits fine grain structure (l5-20~m) with the

dispersion of the second phase both at grain body and grain boundary. Some shaded

and gray chunky islands were also found within the matrix. At higher resolution in

SEM. grain boundary thickening (Figs.2c and d) is quiet evident owing to second

phase precipitation. Within the grain body the second phases are finer in nature. These

4

Elements As per British Sample Al Sample A2specification of BS2L 77

AI Bal Bal BalSi 0.5-0.9 0.95 0.87Fe 0.5 max 0.42 0.42Cu 3.9-5.0 5.04 5.06Mn 0.4-1.2 0.73 0.68Mg 0.2-0.8 0.45 0.49Zn 0.2 max 0.078 0.091Cr 0.1 max 0.021 0.024Ni 0.2 max 0.008 0.004Ti Not specified 0.049 0.058Ti + Zr 0.2 max Zr not found Zr not foundPb 0.05 max 0.01 0.018Sn 0.05 max 0.043 0.040

Page 7: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

NATIONAL METALLURGICAL LABORATORY, JAMSHEDPURMETALLURGICAL ANALYSIS OFTHE DAMAGED WHEEL HUBS OF AVRO HS-748 H-1517.

REPORTNo. NML/MST/IAF/I .13/8012007, OCTOBER 2007

2ndphases are the intermetallics of Cu-AI combination. The large islands within the

matrix are of two types; one is bright (Fig.2c, marked as 'I') and the other is gray

(Fig.2d, marked as 'II') in appearance. In qualitative EDS analysis, it has been found

that bright islands is the combination of Cu and 0, whereas gray regions are the

complex combination of Al-Si-Cu-O.

f."r~r,~,

''"1 I

ii

'-IUI

..., I

iii

"'1

)1 (.f.,

,l:'i:';.,:;:", '--"'-"-.,...,--,..~,,~~-\~, ,.,._,~~.,i,,...:.;!t:_--,-, I , , , , . , , .I..

'f'(.l"-li'I

"'1

.i "I'f-

j

, !!j:1Ii"Ii

.~..

.Ko

'.j IiI

Figs.2 (a-f): Microstructure of base material [a] and [b] optical microscopy, [c]and [d] scanning electron microscopy, [e] EDS from region marked 'I' of

Fig.2c and [fJ EDS from area 'II' marked on Fig.2d.

5

Page 8: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

NATIONAL METALLURGICAL LABORATORY,JAMSHEDPURMETALLURGICAL ANALYSIS OF THE DAMAGED WHEEL HUBS OF AVRO HS-748 H-1517.

REPORTNo. NMLlMST/IAF/1.l3/80/2007, OCTOBER 2007

From the deformed region, two samples, i.e, A I and BI have been chosen and their

overall appearance in transverse section is shown at low'magnification in Fig.3a and

b. In each sample three regions have been identified, i.e, substrate, bend and flow

region. Substrate indicate the region attached to the main part of the wheel hub, bend

means along which material deformation took place during accident and flow region

refers to the area of thin section owing to plastic flow of the alloy. These three

sections have been examined separately and salient features are given below.

Figs.3 (a & b): Transverse SEM micrograph of deformed part of the wheel hub[a] sample A I and [b] sample B I

The substrate microstructure of sample A I and BI exhibits more or less same

morphology (FigsAa and b). The matrix is decorated with bright and shaded islands.

Directionality is evident owing to mechanical working of the alloy during fabrication.

For sample BI, the microstructure exhibits a marked difference at the opposite side of

the bend with respect to the area near the bend. In case of the former, increment in the

number quantity of white islands with irregular shape occurred in comparison to the

streaking like appearance of the white islands of the latter.

6

Page 9: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

NATIONAL METALLURGICAL LABORATORY, JAMSHEDPURMETALLURGICAL ANALYSIS OFTHE DAMAGED WHEEL HUBS OF AVRO HS-748 H-1517.

REPORTNO. NML/MST/IAF/I. I3/80/2007, OCTOBER 2007

Figs. 4(a-c): Optical micrographsof the substrate of deformed wheel

hub showing [a] sample A I withbright elongated islands in theshaded matrix [b] sample B Iexhibiting same bright elongatedislands in the shaded matrixadjacent to the bend and [c]sample B1 irregular shaped brightislands in combination with shaded

region opposite to the bend region..

The general view of the bend region is exhibited in Figs.Sa and b. Heavy deformation

is evident from the curvature of the material flow. For sample A I (Fig. Sa) the volume

fraction of bright regions is more than the sample B I (Fig.5b).

Figs. S(a & b): Optical microstructure of the bend region of the wheel hub [a]sample A I showing material flowing owing to heavy deformation and [b]

sample B 1 exhibiting less pronounced material flow.

Figs. 6a and b shows the flow region of the two samples. In case of the sample B 1, the

bright regions are few in number quantity with respect to the sample A I. From the

alignment of bright region in sample AI (Fig.6a), the direction of the material flow is

found to be diametrically parallel to the wheel hub. In case of sample B] (Fig.6b), no

such clear alignment has been found, rather the bright islands are distributed in a

scattered fashion.

SEM micrographs of the sample A I are illustrated in Figs.7a-h. The substrate

microstructure is heterogeneous in nature. Two distinct regions are evident in the

substrate; one is densely precipitated zone and the other is precipitate free zone where

7

Page 10: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

NATIONAL METALLlRGICAL LABORATORY,JAMSHEDPURMETALLURGICAL ANALYSIS OFTHE DAMAGED WHEEL HUBS OF AVRO HS-748 H-ISI7,

REPORTNo. NM L/MST/IAF/\. I3/80/2007, OCTOBER 2007

the second phases have dissolved completely (Figs,7a and b), The size of the

precipitate free region is -I O-151lm,

Figs, 6(a & b): Optical microstructure of the wheel hub on the flow region [a]sample Al showing alignment of bright region and [b] sample 81 exhibiting

scattered distribution of bright region.

Apart from the above, the substrate contains bright large 2nd phases having size -1-

IOllm and small grey phase having size -1-5Ilm within the matrix (Fig.7c), The

qualitative EDS analysis indicates that the former is basically copper oxide (Fig,8a)

and the latter is AI-Si rich phase in association with Cu and 0 (Fig,8b).

i/::-'. f.'~;~;':):};;i~/.~;.;;0> .::.~;/:}\)~/:'t}~:.:. tj)l~ "','..;,:, ;j.~. .'".f .1'" '.. , . ' ,',": :"'" ,jP".' "'., ..;.'f:':"':' ;,.}~.. 1't; ..;";)i:'.":",~:,/,;~:~",,;,"":X';;"'>' {' ,\:,.t.>(;{~''''.':/ ".,':, ,:;',:,""

,;(;~)..\::,:J ,::; ;.~::~.;/:,: "\J~.;'.:~;;'0:;::'\':~, .'Ir"'.. ! ,;" '.j (""'~.J'( , ,\'",; ,,'\", , '...'> ,

:\:.:;:Y;',~ :,,}.,'. " ?}:,\<~: ::U,~ :,;'~':\~(f

~"\" ", .j' \ "", {' '" Itf'

~?:!~~'~h;*~~~.~~}./lii.''-. "" 'f.' Q.",

",

'\0,,

\\:',

" ' ''''':"

..,. 7. .,.',>.,:::,ri'J", :'~."~::'\'C"\,I"'rc.::;" ~i..,V';,:~{'::'/

,~!~'!))iss~ivclf.:~'I)liascta,~ion: <,'r:<~(" ,,:;: :"';;< 0,";';r:',~.':;,:: ,',~ "'.\:;:i",'.)3z"':,J:iKU",:ti,.;" ':';.. '-;d,':!JWri,,~D~9 'i: ';: ~ : :...",'1'::." ,~'.: ';:.;,,:, . ,..,...\~: " ,~ : ::C"; :

8

Page 11: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

NATIONAL METALLURGICAL LABORATORY,JAMSHEDPURMETALLURGICAL ANALYSIS OFTHE DAMAGED WHEEL HUBS OF AVRO HS-748 H-1517.

REPORTNo, NML/MST/IAF/l,13/80/2007, OCTOBER 2007

.' j" ,d.." "',.'," :', '", ''', ., -', '

, ,(~, '.\-, '.""'1 "~'.' ~,;

~,i,,,,,'j' " \;::.. 'f,,,!.;: .,/" "';'1\""V""'" '." t..""'~'>'" ,.'

!;~,~~{~;;;;~:;~~:~Y:~~,:~;[:r-.~}J;~~~,

-':~'!:';H:~~:~t;I~~~~~:;f t 1'3~4;,:,:t~U.:'::~ ~~i?t~~d:g)lj~~:>;.:;~,.. ~;.,~~;,.''.~<'.,. , ' J,,'. ':.s'.;~. <'-,>"~~,~'i,,,>:I,.:,.'':'<:;.'.(''"

,. ,. """""

,

', ." X"CO """,''''''h

,~''''''''''''''' ...,',

. "'\<~'" ,~.' ~',~.',:\'~'.; ,.. . "':~ .::. -. itC'~1~:,".." "

Figs. 7(a-h): SEM micrograph of the sample A I (a) BSE image of the substrateexhibiting dissolved second phase in the matrix (b) Same region as indicated inFig.7a in SE mode (c) BSE image ofCu distribution on the substrate (d) BSEimage of 2ndphase distribution in the bend region (e) BSE image of large Cu

2ndphase with the fine distribution of8' precipitate at bend region (f) SE imageof precipitate free region at the bend (g) SE image at bend exhibiting secondphase distribution and (h) BSE image showing 2ndphases in the flow part,

As stated before, the bend region is also consists of densely precipitated zone

(Fig.7h),precipitate free region (Fig.7h),Cu-O rich phase (Figs.7d and e), AI-Si rich..." ~". "''''..r'

[a]1 l,'"

..~"

.,L,

~"

,1, ,I A

"'",I.,

., ,_m , ,,,"

l,.,.

..

'uJ~ x,....1.1

9

Page 12: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

---,,".lIlllil;l~ ---+-~;.::r"~"""!:fJl"":;:;' .~r~:-:::::""".,,;:'~.: ....".,_.. .- "",-~,,,,,.," '...,,..",,,

"""""""'= ..~... ". ..,,-.. " ,-

NATIONAL METALLURGICAL LABORATORY, JAMSHEDPURMETALLURGICAL ANALYSIS OFTHE DAMAGED WHEEL HUBS OF AVRO HS-748 H-lSI7.

REPORTNo. NMLlMST/IAF/J.l3/80/2007. OCTOBER 2007

.,1.",.",,-", 8 ',...[c]"". ("..

..."..,,,0".

I"'~

X (.~I

,I.V

,..",,,

[d]I .

...

*' '[I!].~I 'II.V

Figs. 8 (a-d): Qualitative EDS analysis (a) Cu-rich phase containing oxygen ofFig.7c and e, (b) Fe-Si rich phase in association with Cu and 0 of Fig.7d, (c)EDS of a complex compound consisting ofCu-AI-Si-Mg-O ofFig.7fand (d)Aluminium oxide as shown in Fig.7h.

2ndphase. One marked difference has been observed for the bend region with respect

to substrate that the number density of copper oxide particles are quiet large having

more or less same size distribution as stated before for the substrate. At an enlarged

magnification for a single copper oxide dispersoid, it has found that around the

particle near about IJ..lmarea is free from any 2ndphase (Fig.7e), however outside of

the region dence distribution of the same occurred. The bend region also contains

complex combination of Cu-Al-Si-Mg-O as shown in Figs.7f and 8c. However they

are few in number and occurred as clusters of small size distribution.

The flow region of sample Al (Fig.7h) contains both precipitate free and with

precipitate zone along with the distribution of bright copper oxide phase (-1-7J..lm),

AI-Si rich phase (-2-8J..lm)and grey aluminium oxide phase (1-3J..lm).

Page 13: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

NATIONAL METALLURGICAL LABORATORY,JAMSHEDPURMETALLlIRGICAL ANALYSIS OFTHE DAMAGED WHEEL HUBS OF AYRO HS-748 H-1517.

REPORTNo. NML/MST/IAF/113/80/2007, OCTOBER 2007

,."".I...".~", 8 ',...[c],,",. ,-.1.,

....

",. .,.m.,,,..,

"'~

'j\ (.~,,..,

...",,,

[d]I .

0..

I.,

"

,

'

~

'I1

"" '"

i!\. ,l~ '-r, I \

I.,

Figs. 8 (a-d): Qualitative EDS analysis (a) Cu-rich phase containing oxygen ofFig.7c and e, (b) Fe-Si rich phase in association with Cu and 0 of Fig.7d, (c)EDS of a complex compound consisting ofCu-AI-Si-Mg-O ofFig.7fand (d)Aluminium oxide as shown in Fig.7h.

2nd phase. One marked difference has been observed for the bend region with respect

to substrate that the number density of copper oxide particles are quiet large having

more or less same size distribution as stated before for the substrate. At an enlarged

magnification for a single copper oxide dispersoid, it has found that around the

particle near about] I-lmarea is free from any 2ndphase (Fig. 7e), however outside of

the region dence distribution of the same occurred. The bend region also contains

complex combination of Cu-AI-Si-Mg-O as shown in Figs.7f and 8c. However they

are few in number and occurred as clusters of small size distribution.

The flow region of sample A] (Fig.7h) contains both precipitate free and with

precipitate zone along with the distribution of bright copper oxide phase (-l-htm),

AI-Si rich phase (-2-8I-lm) and grey aluminium oxide phase (1-3I-lm).

10

Page 14: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

NATIONAL METALLURGICAL LABORATORY, JAMSHEDPURMETALLURGICAL ANALYSIS OF THE DAMAGED WHEEL HUBS OF AVRO HS-748 H-tSt7.

REPORT No. NML/MST/IAF/l.13/80/2007,OCTOBER2007

Figs. 9 (a-g): SEM micrograph of the sample B1 (a) Fine grain and without grainboundary region co-existence in the substrate (b) junk Cu rich and other 2nd

phases in the no grain boundary region of the substrate (c) BSE image ofFig.9b(d) on bend region exhibiting grain boundary (e) co-existence of precipitate freeand densely precipitated region on the flow part (f) Distribution ofCu bearing

phase.

The SEM micrographs of different parts of sample B 1 is shown in Figs.9a-g. The

presence of without grain boundary and with grain boundary region is clearly revealed

(Fig.9a). The size of the former is -5-7j..lm containing fine distribution of 2nd phase

mainly at the grain boundary. However like sample A I (Fig.7b) precipitate free region

in the substrate has not been found. Without grain boundary region contains bulky

copper oxide phase (-5-20j..lm), tiny AI-Si rich phase (-I-2j..lm) and clusters of AI-

oxide phase (Figs.9b and c). Definite alignment of these two regions indicates

direction of material flow during forming operation.

The SEM microstructure of bend region of sample B1 resemblances with the bend

region of sample A I exhibiting Cu-O, Al-Si rich second phase distribution in the

II

Page 15: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

NATIONAL METALLURGICAL LABORATORY, JAMSHEDPURMETALLURGICAL ANAL YSIS OF THE DAMAGED WHEEL HUBS OF AVRO HS-748 H-1517.

REPORTNo. NMLlMST/IAF/\.l3/80/2007, OCTOBER2007

heterogeneous matrix of precipitate free and dencely precipitated region (Fig.9d). The

flow region of sample B I does not reveal any grain boundary region; rather the zone

contains denced distribution of 2nd phase and precipitate free region (Fig.ge). The

flow region also contains Cu-O and Cu-Al-Si-Mg-O phase as shown in Fig.9f.

4. SEM Characterization of Deformed Surface

The micrographs of A I and BI are shown in Figs.IO(a-d). Scratch marks over the

periphery once again endorses rubbing action (Fig.1Oaand c). At the folded region the

direction of scratches changes and makes an angel of 60-70° with the original scratch

marks (Fig.l Ob). Intense impact causes bending of the component at the edges and the

residual stress causes cracking (Fig.l Ocand d). Material flow near the edge of the hub

is evident (Fig.1Ob). The flow lines indicates that at the moment of the accident, the

wheel was not in rotation, i.e. may be due to some mechanical reason wheel was

jammed.

Figs. 10(a-d): SEM micrographs of the deformed wheel hubs (a) scratch marks

12

Page 16: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

NATIONAL METALU'RGICAL LABORATORY, .JAMSHEDP1:RMETALLURGICAL ANALYSIS OFTHE DAMAGED WHEEL HUBS OF AVRO HS-748 H-ISI7.

REPORT No, NML/MST/IAF/l13/80/2007. OCTOBER2007

over the surface of sample A I (b) multiple flow lines at the edge of fold ofsample A I, (c) scratch mark and cracking over the surface of B I and (d)

scratches and flow lines over the 'surface of B I.

5. Hardness Evaluation

Hardness is measured on the transverse section of the as-received service exposed

wheel hub and the data are collated in Table-2. The data exhibits wide variation

between the substrate and the bend region, whereas the flow region and the bend

exhibits more or less same value. As per specification. for AI alloy of BS 2L 77 at T6

condition, the specified hardness is minimum 134 BHN. With respect to that, base

material hardness is as per speci fication. The hardness of the substrate of sample A I

and Blare more or less at par with the base alloy, However lower values (as compared

with the specified limit) are observed for bend as well as flow region. In both the

regions. from the microstructure it is evident that dissolution of precipitate takes place

which indicates loss of strength and hence the lowering of the hardness. More over

localised grain boundary free regions on the deformed region indicates

recrystallization of the alloy owing to frictional heat. In the recrystallized region new

strain free grains are formed, which are also responsible for the reduction in hardness.

Sample ID

169 ::t2170 + I

112::t3128+ I

115::t2127+ 2

Base

Sample AISamole BI

From the above observation it may be inferred that, the root cause of the accident is

wheel jamming during landing. The flow lines at the edge of the folded region

indicate the phenomena. Jamming raises the frictional force over the wheel hub

assembly. The frictional stress perhaps exceeds the load bearing ability of the

component. Thus. during landing excessive load causes deformation of the wheel hub

after tire burst. The alloy of the wheel hub contains dispersoid of Cu-O and AI-Si-Cu-

0 within the matrix. This dispersoid are large in size hard in nature. Hence ductility of

the alloy becomes limited. The same features are also found at the deformed region of

the wheel hub. Hence, this microstructural heterogeneity is not caused by the

accident; rather it has been in-herited during processing. This structural heterogeneity

is responsible for the formation of cracks in the deformed region. The jamming of the

13

Page 17: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

NATIONAL MET ALLlJRGICAL LABORATORY. JAMSHEDPlJRMETALLURGICAL ANALYSIS OFTHE DAMAGED WHEEL HUBS OF AVRO HS-748 H-ISt7.

REPORTNo. NML/MST/IAF/ 1.13/80/2007. OCTOBER 2007

hub also increases friction against the ground manifold and temperature is raised. This

localised heating causes dissolution of precipitates in localised region as it may be

presumed that the temperature reaches near the solvus temperature of the 2ndphases

(-550°C). The frictional heat also promotes the formation of new strain free grains in

bend and flow region, which is manifested by the reduction in hardness at the bend

and flow region.

CONCLUSIONS

I. Chemical composition of base metal of wheel hub of Avro aircraft HS-748 H-

1517 is close to British specification of BS 2L 77; however, Cu concentration is

marginally higher for both the samples in comparison to the BS specification. Si

content of sample A I is Iittle higher with respect to specification. The exact alloy

specification is not available; hence it is not possible to compare the data obtained

in the present investigation.

2. Microstructure of the base alloy exhibits grain size of 15-20~m having fine

dispersion of AI-Cu intermetallic phases. 2ndphase occurs pre-dominantly at the

grain boundary and is responsible for grain boundary thickening. Apart from these

large dispersoid consisting of Cu-O and AI-Si-Cu-O are also found.

3. The deformed region of the wheel hub consists of three regions; the substrate, the

bend and the flow region. The substrate contains both precipitate free and dencely

precipitated region. Dissolution of precipitate is caused by localised heat

generation owing to friction. Co-existence of both grain boundary and without

grain boundary region is also observed. The grain size of the with grain boundary

region is :<:;:IO~Lm,i.e., lower than the base alloy. It also indicates localised heating

promotes recrystallization and new strain free grains are formed. With grain

boundary region contains large dispersoid of Cu-O and AI~Si rich phase.

4. The bend as well as flow regions consist of precipitate free region, dencely

precipitated region, finer distribution of AI-Cu phase and large 2ndphase of AI-Si

and Cu-O. Minor structural difference or loss of directionality at the three regions

could be attributed to the localised overheating leading to dissolution of

precipitate and recrystallization.

5. The root cause of the accident is wheel jamming during landing. Jamming is

evident from the flow lines on the deformed part of the hub. Jamming results in

14

Page 18: METALLURGICAL ANALYSIS OF THE DAMAGED WHEEL …library.nmlindia.org/FullText/2007/292.pdf · sent to NML for metallurgical failure analysis vide letter No. 19W/S.IO/9/HS-748/H- ...

<, NATIONAL METALLURGICAL LABORATORY, JAMSHEDPURMETALLlJRGICAL ANALYSIS OFTHE DAMAGED WHEEL HUBS OF AVRO HS-748 H-1517.

REPORTNo. NMLlMST/lAF/1.13/80/2007. OCTOBER 2007

,.

excessive stress over the wheel hub. Hence the wheel hub deformed immediately

after the tire burst. The jamm ing is also evident from the microstructure of the

deformed region as it raises frictional force and causes dissolution of 2ndphases

with in the matrix in a scattered fashion and recrystallization.

Actual chemical composition, processing root, mechanical properties, heat treatment

schedule of that particular wheel hub were not available; hence it is difficult to remark

conclusively the exact reason of structural heterogeneity found in the investigation.

###################

,

15


Recommended