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Table of Contents
Organics ................................................................................................... 10
Thermospray High Performance Liquid Chromatography/Mass Spectrometry Methods Development ....... 12
Investigation of Improved Performance in High Performance Liquid Chromatography/Particle Beam/Mass Spectrometry Systems .................................................................................................... 19
Liquid Chromatography/Mass Spectrometry Methods for the Analysis of Aromatic Sulfonic Acids in Hazardous Waste Leachates and Groundwater Monitoring Well Samples ......................................... 21
LC/MS Data Compared to Traditional Methods Data ................................................................. 37
Analysis of Environmental Samples for Polynuclear Aromatic Hydrocarbons by Particle Beam High Performance Liquid Chromatography/Mass Spectrometry .......................................................... 47
Current Status of Infrared and Combined Infrared/Mass Spectrometry Techniques for Environmental Analysis ...................................................................................................................... 50
Method Performance Data from EMSL-LV .............................................................................. 53
Supercritical Fluid Extraction ............................................................................................ 56
The Utilization of Quantitative Supercritical Fluid Extraction for Environmental Applications .............. 59
Quantitative Supercritical Fluid Extraction (SFE) and Coupled SFE-GC Analysis of Environmental Solids and Sorbent Resins .............................................................................................................. 68
The Determination of Selected Priority Pollutants in Soils by Supercritical Fluid and Gas Chromatography/Mass Spectrometry (SFE/GC/MS) .................................................................. 84
The Application of Supercritical Fluid Chromatography-Mass Spectrometry to the Analysis of Appendix-VIII and IX Compounds ........................................................................................................100
Azeotropic Distillation: A continuing Evaluation for the Determination of Polar, Water-soluble Organics ....................................................................................................................115
A Method for the Concentration and Analysis of Trace Methanol in Water by Gas Chromatography .......117
Adaptation of SW-846 Methodology for the Organic Analysis of Radioactive Mixed Wastes ..................131
A Method to Improve the Column Cleanup Efficiency and Throughput of Oily Waste Extracts Through a Nitrogen Pressurized Alumina Column (a Modification of SW-846 Method 3611) ...............................143
New and Improved Techniques for Speciation and Quantitation of Aroclors in Hazardous Wastes..........151
The Determination of Part Per Trillion Levels of Nitroaromatics in Ground and Drinking Water by Wide-Bore Capillary Gas Chromatography ...................................................................................167
A Performance Evaluation of the CLP High Concentration Organic Protocol....................................170
Oxidation of Acid Surrogates and Target Analytes in Environmental Water Samples Using EPA GC/MS Methods ....................................................................................................................172
The Use of High Performance Liquid Chromatography Techniques in the Screening for Priority Pollutants ..................................................................................................................178
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July 16 – 20, 1990 Table of Contents cont.
Optimization of Continuous Liquid-Liquid Extraction Procedures for Semivolatile and Pesticide Analysis .....................................................................................................................180
Extraction of Contaminated Soils with Cosolvents ..................................................................182
High Performance Thin Layer Chromatographic Analysis of Anilines and Phenols .............................195
An Interlaboratory Comparison of a SW-846 Method for the Analysis of the Chlorinated Phenoxyacid Herbicides by LC/MS .....................................................................................................199
The Distribution of Target Compound List Analytes in Superfund Samples .....................................210
Dual-Column/Dual-Detector Approach to Gas Chromatographic Analysis of Environmental Pollutants ....213
Off-Line Supercritical Fluid Extraction Technique for Difficult Environmental Matrices Contaminated with Compounds of Environmental Significance ...........................................................................215
A Retention Index System for Improving the Reliability of GC/MS Tentative Identifications ................217
A Multi-Laboratory Determination of Method Detection Limits and Practical Quantitation Limits for EPA regulated Volatile Organics in Incinerator Ash ......................................................... (Not Included)
On-Line Supercritical Fluid Extraction/Gas Chromatographic (SFE/GC) Method Suitable for Use with Modified Carbon Dioxide .................................................................................................221
Analysis of Environmental Samples for Polynuclear Aromatic Hydrocarbons by Particle Beam HPLC/MS ..................................................................................................... (Not Included)
A Multi-Laboratory Determination of Method Detection Limits for EPA Regulated Semi-Volatile Organic Compounds in Incinerator Ash ............................................................................ (Not Included)
Multilaboratory Validation Study of PCBs in Soils Using SOXTEC Extraction Technique .......................235
Inorganics ................................................................................................ 243
Pre-concentration Techniques for Trace Metals .....................................................................245
Analysis of Waste Water ICP-AES with Ultrasonic Nebulization ...................................................248
A Study of the Linear Ranges of Several Acid Digestion Procedures ..............................................262
The “Art” of Successful Analyses of Inorganic CLP Performance Evaluation Samples .........................278
State-of-the-Art Sample Preparation Methods for Environmental Inorganic Analysis .........................284
Analysis of Arsenic, Selenium, and Mercury in TCLP Extracts of Stabilized Hazardous Waste by Hydride Generation/Multi-Element ICP Optical Emission Spectroscopy....................................................287
X-Ray Fluorescence Spectroscopy in Hazardous Waste and Contaminated Soil Analysis ......................303
Recent Advances in Measuring Mercury at Trace Levels in the Environment ...................................319
The Use of Ion Chromatography in Solid Waste Matrices: Method 300 ...........................................323
The Determination of the Effects of Preservation of Nitrite and Nitrate in Three Types of Water Samples Using TRAACS 800 AutoAnalyzer and Single Column Ion Chromatography .......................................334
A Study of the Effectiveness of SW-846 Method 9010 for the Determination of Total and Amenable Cyanide in Hazardous Waste Matrices ...........................................................................................344
Microwave Digestion: Pressure Control and Monitoring ............................................................359
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July 16 – 20, 1990 Table of Contents cont.
Comparison of Chromatographic and Colorimetric Techniques for Analyzing Chloride and Sulfate in Ground and Surface Waters .......................................................................................................361
Metals Digestion: A Comparative Study ...............................................................................366
Using Flow Injection to Meet QA Criteria for ICPMS Method 6020 .................................. (Not Included)
Comparison of the Determination of Hexavalent Chromium by Ion Chromatography Coupled with ICP-MS or with Colorimetry ..........................................................................................................377
Mobility .................................................................................................. 388
A Proposed Waste Component Mobility Scale ........................................................................390
Contaminated Soils Leaching Part 1- Mobility of Soluble Species .................................................392
Contaminated Soils Leaching Part 2- Mobility of Lead from Contaminated Soils ...............................401
Mobility of Contaminants from Municipal Waste Combustion Ash ................................................406
The Waste Interface Leaching Test: A Long-Term Static Leaching Method for Solidified/Stabilized Waste .......................................................................................................................411
Alternative Methods for Estimating Leaching of Inorganic Constituents from Coal-Combustion Residues ....................................................................................................................413
Air/Groundwater ....................................................................................... 427
Determination of Target Organics in Air Using Ion Trap Mass Spectrometry ....................................429
Ion Chromatography for the Detection of Formic Acid in Incineratory Emissions and Ash from the Use of Formic Acid as a POHC ...................................................................................................431
Ambient Air Monitoring for Benzene and Ethylene Oxide at Texaco Conroe Chemical Plant Conroe Texas .......................................................................................................................434
United States Environmental Protection Agency Method 25D for Determining the Volatile Organic Content of Wastes: Evaluation on Real World Waste Samples ...............................................................458
Groundwater Sampling Procedures Necessary to Obtain Defensible Analytical Data ..........................474
Techniques and Quality Control in Groundwater Sampling ........................................................488
Adaptation of a Simple Colorimetric Method for Formaldehyde for Use with Groundwater Matrices ......503
A Dual Bio-Monitoring System for the Genotoxicity of Air and Water at the Site of Hazardous Waste Mixtures ....................................................................................................................505
Enforcement ............................................................................................ 515
Use of Waste Stream Audits to Determine the Regulatory Status of Surface Impoundments ................517
Designing a LIMS to Meet Enforcement Requirements ..............................................................528
The Use of Confirmed, “Tentatively Identified Compounds” to Build a Case Against the Primary Responsible Party at a Superfund Site ................................................................................530
Evidence Audits: A Case Study and Overview of Audit Findings ...................................................532
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July 16 – 20, 1990 Table of Contents cont.
EPA Oversight of Federal Facility Cleanup of Radiologically Contaminated Mixed Waste Sites Under the Superfund and RCRA Programs .........................................................................................534
Hazardous Waste Identification Enforcement Program .............................................................536
Evaluation of the Draft High Concentration, Multi-media Protocol Versus an Historical Database .........538
Author Index ............................................................................................ 541
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Sixth Annual Waste Testing and Quality Assurance Symposium Vol. II, Washington D.C, July 16 – 20, 1990
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Fifth Annual Waste Testing and Quality Assurance Symposium
July 24-28, 1989
Index
Ainsworth, Calvin C ......................................... 413
Alforque, Maricia M ......................................... 377
Alm, Patti M .................................................. 431
Anderson, Diane W. .......................................... 37
Atwood, Rita A .............................................. 287
Baldin, E ...................................................... 213
Barger, Melanie S............................................ 534
Bayne, Charles K ............................................ 235
Beckert, W.F ...................................... 56, 213, 215
Behymer, Thomas D .......................................... 19
Bellar, Thomas A ............................................. 19
Benedicto, J ................................................. 213
Berges, Jack ................................................. 210
Betowski, L.D ....................................... 12, 47, 199
Bisson, Debra L .............................................. 411
Bone, Larry I ................................................. 458
Bour, Ed ...................................................... 538
Boyer, D.S ..................................................... 59
Bradford, A. Anderson ....................................... 37
Brockhoff, Carol A .......................................... 323
Brown, Mark A ................................................ 21
Bruce, Mark L ................................................ 117
Buchanan, Michelle V ....................................... 429
Budde, William L. ............................................ 19
Buhle, Harald G ............................................. 170
Campbell, A.M ................................................ 84
Caton, J.E .................................................... 131
Chan, Shi-Kit ................................................. 248
Chen, Paul H ................................................. 172
Comeau, Rich ................................................ 319
Cornet, Hans ................................................. 178
Cramer, Paul H .............................................. 115
Cross, K. ....................................................... 59
Cucherini, Brenda A ......................................... 458
Davis, William R ............................................. 517
Dawson, Thomas L .......................................... 458
DeWald, John .......................................... 180, 503
Dias, Frank ............................................. 334, 361
Dodhiwala, N.S .............................................. 215
Dovi, Robert ........................................... 334, 361
Downs, J ...................................................... 390
Draper, William M ........................................... 151
DuBose, G.J ...................................... 392, 401, 406
Dymerski, Mark .............................................. 143
Edwards, M.D ................................................ 131
Eichelberger, James W ..................................... 115
Erickson, David C ............................................ 182
Ferro, Sam ................................................... 195
Fleming, G.S ........................................... 131, 217
Fletcher, Tim ................................................ 366
Floyd, Terry ................................................. 359
Garcia, M.E .................................................. 131
Griest, W.H .................................................. 131
Grillo, Angelo C ............................................. 359
Guerin, Michael R ........................................... 429
Gurka, Donald F ............................................... 50
Guterriez, J ...................................... 392, 401, 406
Hable, Michaek .............................................. 167
Hansen, G ........................................ 392, 401, 406
Harmon, S.H ........................................... 131, 217
Hartwell, S ............................................. 392, 401
Hawthorne, Stephen B ....................................... 68
Hecht, Charles .............................................. 100
Heithmar, E.M ............................................... 245
Hinners, T.A ................................................. 245
Ho, James S .................................................... 19
House, Arthur ............................................... 319
Hsu, John S .................................................... 21
Hull, Donald R ............................................... 287
Huppert, H ................................................... 401
Ilgner, Ralph H .............................................. 429
Jackson, Danny R ........................................... 411
Jarke, Frank H............................................... 488
Jones, T.L ................................................ 12, 199
Kell, Roger A .......................................... 344, 366
Kendall, Douglas S .......................................... 303
Kim, In Suk ..................................................... 21
Kimborough, David E ....................................... 262
Kittikul, P .................................................... 434
Kotus, Matt A ................................................ 100
Labor, Leigh ................................................. 431
Lammerts van Bueren, Daan .............................. 178
Lane, Willam F .............................................. 182
Langenfeld, J .................................................. 68
Lawson, Ty ................................................... 143
Lee, Y. Joyce ................................................ 210
Lee, Richard P ............................................... 117
Levy, J.M ....................................................... 59
Loehr, Raymond C .......................................... 182
Lopez-Avila, V ..................................... 56, 213, 215
Lowry, Joe ................................................... 538
Ma, Te-Hsiu .................................................. 505
Marcus, Mark F .............................................. 100
Marsden, P.J .............................................. 47, 53
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Maskarinec, M.P ............................................. 217
Mayahi, Mostafa ............................................. 180
McKee, Terry M .............................................. 474
McPherson, Craig ............................................ 474
Meenihan, G. Shawn ........................................ 474
Meszaros, Timothy J ........................................ 538
Milancus, J ................................................... 213
Miller, David J ................................................ 68
Moul, Robert ................................................. 143
Muraka, Ishwar P. ........................................... 413
Northington, D.J............................................. 374
Osborn, Ronald J ............................................ 344
Pace, C.M ..................................................... 47
Perugini, Frank .............................................. 488
Pfaff, John D ................................................. 323
Polanski, G ................................................... 406
Pospisil, Peter A. ...................................... 100, 287
Prange, Neil E ............................................... 458
Rai, Dhanpat ................................................. 413
Raymer, James H ............................................ 221
Richards, M .................................................... 84
Riviello, J.M .................................................. 245
Roberts, Dwight F ........................................... 172
Robertson, Gary L ..................................... 170, 210
Roby, M.R ..................................................... 47
Roehl, Raimund .............................................. 377
Roman, Miriam ........................................ 334, 361
Rose, Stephan ............................................... 178
Rosselli, A.C................................................... 59
Rowan, J.T ................................................... 245
Sasinos, Fassil I. .............................................. 21
Sauter, A.D ................................................... 390
Schenley, R.L ................................................ 131
Sheldon, Linda S ............................................. 221
Shelton, Michael ............................................. 374
Smith, Paula ................................................. 532
Smith, Turner ................................................ 503
Spurlin, Stan R ............................................... 431
Stephens, Marvin W ......................................... 117
Stephens, Robert D .......................................... 21
Stern, Catherine ............................................. 167
Stewart, Joseph H ........................................... 235
Stewart, Ralph R ............................................ 517
Stockwell, Peter ............................................. 319
Surdo, Tony Lo ............................................... 530
Syslo, John ................................................... 530
Tatro, Mark E .......................................... 278, 284
Tellez, Daniel ................................................ 180
Tomkins, B.A. ................................................ 131
Van Ausdale, William A ..................................... 172
Velez, George R ............................................. 221
Wakakuwa, Janice .......................................... 262
Warden, Bruce ......................................... 334, 361
Weston, Roy F ............................................... 530
White, P ................................................ 401, 406
Wiggenhauser, Gary ........................................ 366
Wijekoon, Donald ........................................... 151
Williams, Kenneth .................................... 167, 411
Wilner, Jay .................................................. 115
Wise, Marcus B. ............................................. 429
Worthington, Jeffrey C............................... 528, 532
Yanak, Michael M ........................................... 248
Yoder, Rhonda............................................... 334
Zechmann, Cecilia A........................................ 248
Zully, Romana ............................................... 344
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