Northfield Road, Netherton (J17035/01)
CONTENTS
1.0 INTRODUCTION
2.0 GROUND INVESTIGATION
2.1 Site Works
2.2 Insitu Testing
2.2.1 Standard Penetration Tests
2.2.2 Dynamic Probing
2.2.3 Photoionisation Device (PID) Screening
2.3 Instrumentation
2.4 Laboratory Testing
2.4.1 Contamination Testing
2.4.2 Geotechnical Testing
3.0 GROUND CONDITIONS
3.1 Made Ground
3.2 Weathered Etruria Formation
3.3 Groundwater
4.0 CONTAMINATION ASSESSMENT
4.1 Visual and Olfactory Evidence
4.2 Human Health
4.2.1 Metals
4.2.2 Cyanide and Phenols
4.2.3 Polycyclic Aromatic Hydrocarbons (PAH)
4.2.4 Total Petroleum Hydrocarbons (TPH)
4.2.5 Asbestos
4.3 Contamination Recommendations
5.0 GROUND GASES
Northfield Road, Netherton (J17035/01)
6.0 ENGINEERING CONSIDERATIONS
6.1 Mining
6.2 Foundations
6.3 Building Near Trees
6.4 Floor Slabs
6.5 Excavations
6.6 Groundwater
6.7 Buried Concrete
6.8 Water Pipes
Northfield Road, Netherton (J17035/01)
TABLES
Table No Table Title
1 Summary of Contamination Results
FIGURES
Figure No Figure Title
1 Borehole Location Plan
2 SPT N Value vs Depth (BH1 & BH2)
3 SPT N Value vs Depth (BH3 & BH4)
4 Dynamic Probe Results (BH1)
5 Dynamic Probe Results (BH2)
6 Dynamic Probe Results (BH3)
7 Dynamic Probe Results (BH4)
8 Plasticity Chart
APPENDICES
Appendix No Appendix Title
A Borehole Records
B Trial Pit Records
C Summary of SPT Results
D PID Screening Results
E Gas Monitoring Results
F Contamination Test Results
G Geotechnical Test Results
Northfield Road, Netherton (J17035/01)
1
1.0 INTRODUCTION
Spilman Associates Limited have been appointed by Mr Tony Walker to
carry out a ground investigation for a proposed residential development on
land at 57 Northfield Road, Netherton, Dudley, West Midlands, DY2 9JD.
This report should be read in conjunction with Spilman Associates Limited
“Desk Study & Initial Site Assessment” dated July 2015 (Report No
J15092/01) which presents background information on the site.
The current report presents the findings of an intrusive investigation and
associated monitoring and laboratory testing.
The outline scope of the investigation was discussed and agreed with
Dudley MBC (Anita Metelko) in respect of contamination and ground gas
issues.
2.0 GROUND INVESTIGATION
2.1 Site Works
The site works were carried out on 5th April 2017 and comprised the drilling
of four mini-rig boreholes and the excavation of 7 no machine dug trial pits
at locations shown on Figure 1.
The mini-rig boreholes were advanced by percussive techniques in 1m
intervals. All boreholes and trial pits were logged by a Geotechnical
Engineer and detailed records are reproduced at Appendix A (boreholes)
and B (trial pits).
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2.2 Insitu Testing
2.2.1 Standard Penetration Tests
Standard Penetration Tests (SPTs) were carried out at variable
intervals in all mini-rig boreholes. The test results are shown in full
at Appendix C, on the borehole records at Appendix A and
graphically on Figure 2 (BH1 and BH2) and Figure 3 (BH3 and
BH4).
2.2.2 Dynamic Probing
Super heavy dynamic probing was carried out adjacent to all
borehole positions and the results are shown graphically on Figures
4, 5, 6 and 7.
2.2.3 Photoionisation Device (PID) Screening
Selected soil samples were screened for volatile organic
compounds (VOCs) using a portable Photoionisation Device (PID)
and the test results are detailed on Appendix D.
2.3 Instrumentation
Combined gas and groundwater monitoring standpipes were installed in all
boreholes. The installation details are shown on the borehole records at
Appendix A and are summarised below:
Borehole Response Zone (m)
BH1 0.50 – 4.00
BH2 0.50 – 4.00
BH3 0.50 – 3.00
BH4 0.50 – 3.00
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Gas and groundwater level monitoring was carried out on six occasions at
weekly intervals. Monitoring was carried out with a portable infrared gas
analyser (Gas Data GFM 436). Groundwater depths were determined with
an electronic dipmeter.
The monitoring results are presented at Appendix E.
2.4 Laboratory Testing
2.4.1 Contamination Testing
Fourteen near surface soil samples were tested for the following
determinands:
Former ICRCL Suite
Speciated Polycyclic Aromatic Hydrocarbons (PAH)
Total Petroleum Hydrocarbons (TPH) with an
Aromatic/Aliphatic Split
Asbestos Screen
The test results are reproduced in full at Appendix F and are
summarised on Table 1.
2.4.2 Geotechnical Testing
Selected soil samples were tested for the following parameters:
Moisture Content
Liquid Limit
Plastic Limit
Soluble Sulphate
pH
Particle Size Distribution
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The test results are reproduced at Appendix G. Index properties
are shown on the plasticity chart at Figure 8.
3.0 GROUND CONDITIONS
3.1 Made Ground
Made ground was encountered in all trial pits and boreholes. In the
northwest part of the site (area to northwest of the retaining wall) the made
ground comprised predominantly very loose to loose very sandy gravel of
ash and clinker. The base of the made ground was proved in BH1 and
BH2 at 7.10m and 7.00m respectively.
In the southeast part of the site (area to southeast of the retaining wall) the
made ground comprised loose to medium dense sandy gravel of ash and
clinker with some to much brick rubble. The base of the made ground was
proved at 2.40m in BH3 and 2.10m in BH4.
3.2 Weathered Etruria Formation
Weathered Etruria Formation strata was encountered in all boreholes and
generally comprised firm clay, although in BH4 sand was recorded from
2.60m to the base of the borehole at 3.45m.
3.3 Groundwater
Groundwater was not encountered in any of the trial pits or boreholes
during excavation or drilling. Subsequent monitoring in the boreholes
identified groundwater in BH1 only at depths between 2.52m and 2.57m.
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4.0 CONTAMINATION ASSESSMENT
4.1 Visual and Olfactory Evidence
No visual or olfactory evidence of soil contamination was identified during
the current investigation. PID screening of selected samples showed as
absence of volatile organic compounds.
4.2 Human Health
4.2.1 Metals
The soil test results have been assessed against the published
CLEA Soil Guideline Values (SGVs). Where no SGVs are available
the results have been assessed against the LQM/CIEH S4ULs.
Lead has been assessed against the potential Category 4
Screening Level (C4SL) of 200mg/kg in the absence of any updated
CLEA SGVs. All results are based on a residential end-use. The
test results are summarised below and detailed in full on Table 1
and Appendix F:-
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Determinand
Range of Values
Detected
(mg/kg)
Screening
Value
(mg/kg)
No of Results
Exceeding
Screening Value*
Arsenic 14 – 68 32 8
Boron <1 – 1 291 0
Cadmium <1 – 78 10 3
Chromium 15 – 220 910 0
Chromium VI <1 6 0
Copper 68 – 1400 2330 0
Lead 64 – 2000 200 9
Mercury <1 – 1 170 0
Nickel 30 – 260 130 4
Selenium <3 350 0
Zinc 160 – 9300 3750 2
* 14 no samples tested
4.2.2 Cyanide and Phenols
Concentrations of free cyanide and phenols were below the
laboratory detection limit of 1.0mg/kg in all samples. Free cyanide
concentrations were significantly below the screening value of
20mg/kg and phenol concentrations were below the screening value
of 780mg/kg.
4.2.3 Polycyclic Aromatic Hydrocarbons (PAH)
Total PAH concentrations ranged from <1.0mg/kg to 180mg/kg.
Concentrations of benzo(a)pyrene exceeded the screening value of
2.2mg/kg in 9 of the 14 samples tested with concentrations up to a
maximum of 11mg/kg in TP4 at 0.20m. Other exceedances
occurred for naphthalene (1no), benzo(a)anthracene (1no),
chrysene (1no), benzo(b/k)fluoranthene (10no),
dibenzo(ah)anthracene (10no).
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4.2.4 Total Petroleum Hydrocarbons (TPH)
TPH concentrations for both aromatic and aliphatic compounds over
all carbon ranges were below the appropriate screening value in all
samples.
BTEX compounds were at concentrations below the appropriate
screening value in all samples.
4.2.5 Asbestos
Asbestos fibres were identified in four of the fourteen samples
screened. Where asbestos fibres were positively identified then
asbestos quantification testing was carried out and the results are
reproduced at Appendix F. The proportion of asbestos present was
recorded as <0.001% in all four samples and at this level does not
require specific remediation.
4.3 Contamination Recommendations
A qualitative risk assessment has been carried out based on the accepted
source-pathway-receptor pollutant linkages methodology. The
assessment considers a site specific conceptual model designed from
information obtained from the current investigation.
The principal receptors at the site are considered to be humans and
controlled waters.
Elevated concentration of arsenic, cadmium, lead, nickel, zinc and PAH
compounds have been identified at the site. These elevated
concentrations pose a potential hazard with respect to human health
without appropriate remedial measures.
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Appropriate remedial measures should be designed to sever the identified
pollutant linkage. This could be achieved by the provision of a clean cover
layer as the removal of the impacted soil would not be practical or cost-
effective.
The cover layer should comprise a minimum 600mm of clean topsoil
and/or subsoil which will effectively isolate any residual contaminants from
the site end-users thus breaking the identified pollutant linkage. No
special measures are considered necessary beneath buildings, parking
areas and other areas of hardstanding.
Care should be taken to ensure that all imported materials are
uncontaminated. Appropriate testing and validation of the remedial works
should be carried out to the satisfaction of the Local Authority and
Warranty Provider. The remedial works should be completed and
validated before the development is first occupied.
The risk of the site having any significant impact on the controlled waters
(surface and groundwater) is assessed to be low for the following reasons:
The contaminants identified are unlikely to be significantly leachable
There are no sensitive groundwater receptors close to the site
The potential for any contaminants to impact the adjacent canal to
the northwest of the site would be prevented by the puddle clay liner
to the canal
Consequently no specific remedial measures are considered necessary
with respect to controlled waters.
The contamination conclusions and recommendations detailed in this
report should be submitted to and approved by the Local Authority prior to
commencement of any development works.
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In the event of actual or suspected contamination not identified by this
investigation being encountered during site development works then further
advice should be sought and the Local Authority should be informed.
5.0 GROUND GASES
Ground gas monitoring was carried out in all four boreholes on six
occasions. Methane was absent in all boreholes on all monitoring visits.
Carbon dioxide concentrations ranged from 0.4% to 4.8%.
Borehole gas flow rates were less than 0.5 litres per hour on all monitoring
visits in all boreholes. Atmospheric pressures during the monitoring
ranged from 999 to 1019 millibars with one reading less than 1000
millibars.
In accordance with CIRIA C665 (2007) Assessing Risks Posed by
Hazardous Ground Gases to Buildings a classification of Characteristic
Situation 1 (CS1) would be appropriate for the site. Under this
classification no formal gas protection measures are considered
necessary.
6.0 ENGINEERING CONSIDERATIONS
6.1 Mining
Mining for coal and ironstone is recorded beneath the site at depths
between 40m and 140m. However, the age and depth of the workings are
such that they are not considered to have the potential to significantly
impact surface stability. The site does not lie in an area where a potential
for shallow unrecorded coal workings has been identified. Accordingly no
further mining investigation or stabilisation works are required for the
proposed residential development.
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There are no recorded mineshafts on the site or within 20m of the site
boundary. However, as in all mining areas there is a slight risk of
unrecorded mineshafts being present. Any suspicious features identified
during site development works should be appropriately investigated and
treated as necessary.
6.2 Foundations
The made ground is unsuitable as a founding medium due to its variability
and poor geotechnical characteristics.
In the southeast part of the site (to the southeast of the retaining wall)
made ground depths are between 2.10m and 2.40m. At these depths it
may be feasible to utilise deep trench fill foundations extending through the
full depth of the made ground into competent natural strata. Foundation
depths may be of the order 2.50m to 3.00m. If deep trench fill foundations
are employed then at a nominal foundation depth of 2.5m an allowable
bearing pressure of 100kN/m2 would be appropriate for foundation design.
At this loading intensity settlements would be limited to acceptable levels.
In the northwest part of the site around 7m of made ground has been
identified which would preclude the use of deep trench fill foundation. It is
anticipated that the most economic foundation solution would be to
improve the made ground by the use of vibro-replacement stone columns
through the full depth of the made ground. The stone columns should be
designed to by a specialist contractor, although it is anticipated that an
allowable bearing pressure of around 100kN/m2 could be achieved
following treatment. Conventional strip foundations could then be used on
the stone columns although reinforcement would be required within the
strip footings.
It may be cost-effective to adopt a similar foundation solution in the
southeast part of the site in lieu of deep trench fill foundations.
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An alternative to the use of vibro stone columns would be piled
foundations to transfer building loads to competent strata at depth.
All foundation proposals should be inspected and approved by the Building
Inspector.
In the event of ground conditions differing from those identified by this
investigation then further geotechnical advice should be sought.
6.3 Building Near Trees
There are trees adjacent to the electricity substation in the central part of
the site which could have the potential to cause heave or shrinkage of the
clay soils.
One clay sample from BH3 indicated a plasticity index of 28 which equates
to modified plasticity index of 12 when taking into account the proportion of
material passing the 0.425mm sieve.
In accordance with the NHBC Standards (2016) Chapter 4.2 Building Near
Trees the clay soils would be classified as being of Low Volume Change
(Shrinkage) Potential.
Foundation depths can be determined in accordance with NHBC Design
Charts (or other similar guidance) taking into account the proximity, type
and size of nearby trees.
Where necessary further advice on foundation design should be obtained
from a Structural Engineer.
6.4 Floor Slabs
Due to the depth of made ground fully suspended beam and block type
ground floor slabs are recommended.
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6.5 Excavations
Excavations are anticipated to be of varying stability in the made ground
and some excavation overbreak and instability should be anticipated.
Where man entry is required the excavation sides should be appropriately
battered or shored in accordance with Health & Safety Executive
Guidance.
6.6 Groundwater
No shallow groundwater has been identified by the current investigation
and consequently significant groundwater ingress into shallow excavations
is not anticipated. Excavations below around 2.5m may encounter
groundwater.
It should be noted that groundwater levels can be subject to seasonal
fluctuations and longer term groundwater monitoring has not been carried
out.
6.7 Buried Concrete
Sulphate and pH test results indicate an appropriate design class for
buried concrete of DS-1 in accordance with BRE Special Digest 1 (2005).
The Aggressive Chemical Environment for Concrete (ACEC) class for the
site would be AC-1s assuming static groundwater conditions.
6.8 Water Pipes
Contaminants identified at the site may have the potential to impact
conventional polyethylene water supply pipes. Accordingly, the water
supply company should be contacted to confirm their precise
requirements.
TABLES
Northfield Road, Netherton (J17035/01)
0.20 0.30 0.30 0.20 0.40 0.30 0.40
mg/kg 44 26 25 35 14 54 40 32
mg/kg <1 <1 <1 <1 1 <1 <1 291
mg/kg 2 <1 <1 19 <1 10 7 10
mg/kg 220 29 28 24 15 79 38 910 1
mg/kg <1 <1 <1 <1 <1 <1 <1 6
mg/kg 290 130 110 160 68 1400 680 2330
mg/kg 300 170 130 650 64 2000 460 200 2
mg/kg <1 <1 <1 <1 <1 <1 <1 170 3
mg/kg 140 35 46 51 30 140 76 130
mg/kg <3 <3 <3 <3 <3 <3 <3 350
mg/kg 960 210 350 9300 160 3300 1400 3750
mg/kg <1 <1 <1 <1 <1 <1 <1 20 4
mg/kg <1 <1 <1 <1 <1 <1 <1 780
mg/kg <0.1 1.2 <1.0 8.4 <1.0 0.1 0.2 2.3
mg/kg 0.1 0.3 <1.0 <1.0 <1.0 0.2 0.5 170
mg/kg <0.1 0.5 <1.0 4.7 <1.0 0.1 0.2 210
mg/kg <0.1 0.6 <1.0 5.2 <1.0 0.1 0.3 170
mg/kg 0.6 4.8 <1.0 30 <1.0 1.6 2.8 95
mg/kg 0.1 1.8 <1.0 10 <1.0 0.4 1.2 2400
mg/kg 1.2 5.2 <1.0 28 <1.0 4.6 4 280
mg/kg 1.2 4.2 <1.0 23 <1.0 4.5 3.9 620
mg/kg 0.6 3.5 <1.0 15 <1.0 2.2 3.7 7.2
mg/kg 0.9 4 <1.0 16 <1.0 2.9 3.9 15
mg/kg 1.8 4.9 <1.0 19 <1.0 7.8 13 2.6/77 5
mg/kg 1.1 2.8 <1.0 11 <1.0 3.6 5.9 2.2
mg/kg 0.7 1.2 <1.0 4.8 <1.0 2.5 4 27
mg/kg 0.3 0.5 <1.0 1.7 <1.0 0.6 1.3 0.24
mg/kg 0.8 1.1 <1.0 4.1 <1.0 2.3 4.1 320
mg/kg 9.6 37 <1.0 180 <1.0 33 49 N/A
ug/kg <10 <10 <10 <20 <20 <10 <10 330
ug/kg <10 <10 <10 <20 <20 <10 <10 350,000
ug/kg <10 <10 <10 <20 <20 <10 <10 240,000 6
ug/kg <10 <10 <10 <20 <20 <10 <10 250,000
ug/kg <10 <10 <10 <20 <20 <10 <10 610,000
mg/kg <0.1 <0.1 <0.1 <0.2 <0.2 <0.1 <0.1 42
mg/kg <0.1 <0.1 <0.1 <0.2 <0.2 <0.1 <0.1 100
mg/kg <0.1 <0.1 <0.1 <0.2 <0.2 <0.1 <0.1 27
mg/kg <10 <1 <10 <10 <10 <10 <1 130
mg/kg <10 <2 <10 <10 <10 <10 3 1100
mg/kg <10 2 <10 <10 <10 <10 8 65,000 7
mg/kg 49 10 82 <10 11 34 26 65,000 7
mg/kg 11 4 <10 12 <10 18 9 65,000
mg/kg <0.1 <0.1 <0.1 <0.2 <0.2 <0.1 <0.1 70
mg/kg <0.1 <0.1 <0.1 <0.2 <0.2 <0.1 <0.1 130
mg/kg <0.1 <0.1 <0.1 <0.2 <0.2 <0.1 <0.1 34
mg/kg <10 <1 <10 <10 <10 <10 <1 74
mg/kg <10 9 <10 10 <10 <10 13 140
mg/kg <10 44 <10 61 <10 76 110 260
mg/kg <10 110 <10 79 <10 250 320 1100
mg/kg <10 <1 <10 <10 <10 <10 6 11001 S4UL quoted is for Chromium III2 Results assessed against Category 4 Screening Level3 Total Mercury concentration assessed against SGV for inorganic mercury4 Assessed against Dutch Intervention Value5 Analysis does not separate benzo(b)fluoranthene and benzo(k)fluoranthene6 SGV for m-xylene 240mg/kg and for p-xylene 230mg/kg7 S4UL of 65,000mg/kg for aliphatic C16 - C35
Chrysene
Benzo(b/k)Fluoranthene
Benzo(a)Pyrene
Indeno(123-cd)Pyrene
Toluene
Dibenzo(ah)Anthracene
Benzo(ghi)Perylene
PAH (Total)
Benzene
TPH (C35 - C44 Aliphatic)
TPH (C21 - C35 Aromatic)
TPH (C16 - C21 Aromatic)
TPH (C35 - C44 Aromatic)
TPH (C10 - C12 Aromatic)
TPH (C12 - C16 Aromatic)
TABLE 1: SUMMARY OF SOIL CONTAMINATION RESULTS (Page 1 of 2)
TPH (C7 - C8 Aromatic)
TPH (C8 - C10 Aromatic)
TPH (C12 - C16 Aliphatic)
TPH (C16 - C21 Aliphatic)
TPH (C21 - C35 Aliphatic)
TPH (C6 - C7 Aromatic)
TPH (C5 - C6 Aliphatic)
TPH (C6 - C8 Aliphatic)
TPH (C8 - C10 Aliphatic)
TPH (C10 - C12 Aliphatic)
EthylBenzene
Meta/Para-Xylene
Ortho-Xylene
Anthracene
Fluoranthene
Pyrene
Benzo(a)Anthracene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Lead
Mercury
Nickel
Copper
LQM/CIEH S4UL
Chromium
Cadmium
Chromium VI
Boron
Arsenic
Selenium
Cyanide (free)
Phenols
Naphthalene
Zinc
CLEA SGVBorehole
Depth (m)orTP5 TP6 TP7TP1 TP2 TP3 TP4
Northfield Road, Netherton (J17035/01)
1.20 2.00 1.80 0.20 0.40 0.30 0.30
mg/kg 68 30 27 52 54 19 37 32
mg/kg <1 <1 <1 <1 <1 <1 <1 291
mg/kg 2 <1 6 3 3 2 78 10
mg/kg 210 35 26 68 26 18 61 9101
mg/kg <1 <1 <1 <1 <1 <1 <1 6
mg/kg 480 120 500 250 210 160 950 2330
mg/kg 210 160 320 510 430 110 770 2002
mg/kg <1 <1 <1 <1 1 <1 <1 1703
mg/kg 260 42 47 77 49 30 170 130
mg/kg <3 <3 <3 <3 <3 <3 <3 350
mg/kg 990 430 910 1300 4200 190 1300 3750
mg/kg <1 <1 <1 <1 <1 <1 <1 204
mg/kg <1 <1 <1 <1 <1 <1 <1 780
mg/kg 1 0.4 0.1 0.4 1 0.4 <0.1 2.3
mg/kg 0.4 <0.1 0.1 0.4 0.3 <0.1 0.1 170
mg/kg 0.2 0.2 <0.1 0.1 0.5 0.7 <0.1 210
mg/kg 0.2 0.1 <0.1 0.1 0.7 0.5 <0.1 170
mg/kg 1.9 1.2 1.1 1.6 6.1 3.6 1.1 95
mg/kg 0.5 0.4 0.5 0.5 1.8 1.3 0.5 2400
mg/kg 2.4 1.9 2.2 1.8 7 3.9 2.1 280
mg/kg 2.2 1.7 2.3 1.6 5.9 3.4 2.1 620
mg/kg 1.2 1.1 1.8 1.3 4.1 2.3 1.9 7.2
mg/kg 2.2 1.2 2.1 1.5 4.3 2.3 2 15
mg/kg 4.6 2.5 8 3.5 8.8 5.1 5.8 2.6/775
mg/kg 2.4 1.1 3.7 1.5 3.9 2.2 2.6 2.2
mg/kg 1.8 0.6 2.9 1 2.3 1.2 1.9 27
mg/kg <0.1 <0.1 0.9 0.3 0.9 0.4 0.6 0.24
mg/kg 1.9 0.6 3.2 1 2.2 1.2 2 320
mg/kg 23 13 29 17 50 28 23 N/A
ug/kg <10 <10 <10 <20 <20 <20 <20 330
ug/kg <10 <10 17 <20 <20 20 27 350,000
ug/kg <10 <10 13 20 <20 <20 29 240,0006
ug/kg <10 <10 <10 <20 <20 <20 <20 250,000
ug/kg <10 <10 <10 <20 <20 <20 <20 610,000
mg/kg <0.1 <0.1 <0.1 <0.2 <0.2 <0.2 <0.2 42
mg/kg <0.1 <0.1 <0.1 <0.2 <0.2 <0.2 <0.2 100
mg/kg <0.1 <0.1 <0.1 <0.2 <0.2 <0.2 <0.2 27
mg/kg <10 <10 <10 <1 <10 <1 <1 130
mg/kg <10 <10 <10 5 <10 <2 <2 1100
mg/kg 34 <10 14 22 17 2 4 65,0007
mg/kg <10 20 65 20 39 4 28 65,0007
mg/kg 10 <10 18 <1 57 4 <1 65,000
mg/kg <0.1 <0.1 <0.1 <0.2 <0.2 <0.2 <0.2 70
mg/kg <0.1 <0.1 <0.1 <0.2 <0.2 <0.2 <0.2 130
mg/kg <0.1 <0.1 <0.1 <0.2 <0.2 <0.2 <0.2 34
mg/kg <10 <10 <10 2 <1 <1 <1 74
mg/kg <10 <10 <10 30 18 3 4 140
mg/kg <10 <10 120 31 160 16 32 260
mg/kg <10 27 550 81 420 41 130 1100
mg/kg <10 <10 <10 <1 <10 <1 <1 11001
S4UL quoted is for Chromium III2
Results assessed against Category 4 Screening Level3
Total Mercury concentration assessed against SGV for inorganic mercury4
Assessed against Dutch Intervention Value5
Analysis does not separate benzo(b)fluoranthene and benzo(k)fluoranthene6
SGV for m-xylene 240mg/kg and for p-xylene 230mg/kg7
S4UL of 65,000mg/kg for aliphatic C16 - C35
CLEA SGVBorehole
Depth (m)
orBH2 BH3 BH4TP1 TP3 TP7 BH1
Selenium
Cyanide (free)
Phenols
Naphthalene
Zinc
Lead
Mercury
Nickel
Copper
LQM/CIEH S4UL
Chromium
Cadmium
Chromium VI
Boron
Arsenic
Anthracene
Fluoranthene
Pyrene
Benzo(a)Anthracene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
TABLE 1: SUMMARY OF SOIL CONTAMINATION RESULTS (Page 2 of 2)
TPH (C7 - C8 Aromatic)
TPH (C8 - C10 Aromatic)
TPH (C12 - C16 Aliphatic)
TPH (C16 - C21 Aliphatic)
TPH (C21 - C35 Aliphatic)
TPH (C6 - C7 Aromatic)
TPH (C5 - C6 Aliphatic)
TPH (C6 - C8 Aliphatic)
TPH (C8 - C10 Aliphatic)
TPH (C10 - C12 Aliphatic)
EthylBenzene
Meta/Para-Xylene
Ortho-Xylene
TPH (C35 - C44 Aliphatic)
TPH (C21 - C35 Aromatic)
TPH (C16 - C21 Aromatic)
TPH (C35 - C44 Aromatic)
TPH (C10 - C12 Aromatic)
TPH (C12 - C16 Aromatic)
Chrysene
Benzo(b/k)Fluoranthene
Benzo(a)Pyrene
Indeno(123-cd)Pyrene
Toluene
Dibenzo(ah)Anthracene
Benzo(ghi)Perylene
PAH (Total)
Benzene
FIGURES
APPENDIX A
Page 1 of 1
40
MADE GROUND
Spilman Associates 38 South Avenue Stourbridge West Midlands DY8 3XY 01384 820578 tel
BH No.
BH1
Job No.J17035
Site Location
Strata Depth
(m)
Sample Depth (m)
Strata Description Legend Casing and Test Record
Water/ Reduced
Levels (m)
0.00
3.00
7.10
7.45
SPT N = 1
SPT N = 3
SPT N = 4
SPT N = 12
SPT N = 24
Remarks:- 1. No groundwater encountered during drilling 2. Borehole unstable below 3.00m 3. For dynamic probe results see Figure 4 4. 50mm ID HDPE slotted pipe from 0.50m to 4.00m with pea gravel surround. Plain pipe from
surface to 0.50m with bentonite seal. Pipe capped with bung and gas tap within stopcock cover
Very loose black silty very sandy gravel of ash and clinker with occasional brick fragments (MADE GROUND) … with band of soft grey sandy gravelly clay from 1.90m to 2.30m (possible puddle clay lining to former canal) Very loose to loose occasionally medium dense dark grey clayey very sandy gravel (MADE GROUND)
Firm yellow brown and grey slightly sandy CLAY (WEATHERED ETRURIA FORMATION)
MINI RIG BOREHOLE RECORD
Client Name
Date of Drilling 05/04/17 Grid Ref
BH continued
Key to samples/in situ tests:- D Disturbed B Bulk U Undisturbed W Water SPT Standard Penetration Test CPT Cone Penetration Test N N value
1
2
3
4
5
6
7
8
9
Mr Tony Walker
Northfield Road, Netherton
1
2
3
4
5
6
7
8
9
Page 1 of 1
40
MADE GROUND
Spilman Associates 38 South Avenue Stourbridge West Midlands DY8 3XY 01384 820578 tel
BH No.
BH2
Job No.J17035
Site Location
Strata Depth
(m)
Sample Depth (m)
Strata Description Legend Casing and Test Record
Water/ Reduced
Levels (m)
0.00
0.30
3.00
7.00
7.30
SPT N = 1
SPT N = 4
SPT N = 4
SPT N = 12
Remarks:- 1. No groundwater encountered during drilling 2. Borehole unstable below 3.00m 3. For dynamic probe results see Figure 5 4. 50mm ID HDPE slotted pipe from 0.50m to 3.00m with pea gravel surround. Plain pipe from
surface to 0.50m with bentonite seal. Pipe capped with bung and gas tap within stopcock cover
Tarmac over roadstone (MADE GROUND) Very loose to loose black silty very sandy gravel of ash and clinker (MADE GROUND) … becoming medium dense below 4.00m
Firm mottled yellow brown and grey slightly sandy CLAY (WEATHERED ETRURIA FORMATION)
MINI RIG BOREHOLE RECORD
Client Name
Date of Drilling 05/04/17 Grid Ref
BH continued
Key to samples/in situ tests:- D Disturbed B Bulk U Undisturbed W Water SPT Standard Penetration Test CPT Cone Penetration Test N N value
1
2
3
4
5
6
7
8
9
Mr Tony Walker
Northfield Road, Netherton
1
2
3
4
5
6
7
8
9
Page 1 of 1
40
MADE GROUND
Spilman Associates 38 South Avenue Stourbridge West Midlands DY8 3XY 01384 820578 tel
BH No.
BH3
Job No.
J17035
Site Location
Strata Depth
(m)
Sample
Depth (m) Strata Description Legend Casing and
Test Record
Water/ Reduced
Levels (m)
0.00
2.40
3.45
SPT N = 4
SPT N = 11
SPT N = 17
Remarks:- 1. No groundwater encountered during drilling 2. For dynamic probe results see Figure 6 3. 50mm ID HDPE slotted pipe from 0.50m to 3.00m with pea gravel surround. Plain pipe from
surface to 0.50m with bentonite seal. Pipe capped with bung and gas tap
Loose becoming medium dense dark grey silty very sandy gravel of ash and clinker and some brick rubble (MADE GROUND) Firm friable mottled red brown, dark brown, light brown and grey sandy CLAY (WEATHERED ETRURIA FORMATION)
MINI RIG BOREHOLE RECORD
Client Name
Date of Drilling 05/04/17 Grid Ref
BH continued
Key to samples/in situ tests:- D Disturbed B Bulk U Undisturbed W Water SPT Standard Penetration Test CPT Cone Penetration Test N N value
1
2
3
4
5
6
7
8
9
Mr Tony Walker
Northfield Road, Netherton
1
2
3
4
5
6
7
8
9
Page 1 of 1
40
MADE GROUND
Spilman Associates 38 South Avenue Stourbridge West Midlands DY8 3XY 01384 820578 tel
BH No.
BH4
Job No.
J17035
Site Location
Strata Depth
(m)
Sample
Depth (m) Strata Description Legend Casing and
Test Record
Water/ Reduced
Levels (m)
0.00
2.10
2.60
3.45
SPT N = 0
SPT N = 5
SPT N = 37
Remarks:- 1. No groundwater encountered during drilling 2. For dynamic probe results see Figure 7 3. 50mm ID HDPE slotted pipe from 0.50m to 3.00m with pea gravel surround. Plain pipe from
surface to 0.50m with bentonite seal. Pipe capped with bung and gas tap within stopcock cover
Very loose black silty very sandy gravel of ash and clinker with much brick rubble (MADE GROUND)
Firm mottled light grey and light brown slightly sandy slight gravelly CLAY (WEATHERED ETRURIA FORMATION)
Medium dense becoming dense brown slightly clayey gravelly SAND (WEATHERED ETRURIA FORMATION)
MINI RIG BOREHOLE RECORD
Client Name
Date of Drilling 05/04/17 Grid Ref
BH continued
Key to samples/in situ tests:- D Disturbed B Bulk U Undisturbed W Water SPT Standard Penetration Test CPT Cone Penetration Test N N value
1
2
3
4
5
6
7
8
9
Mr Tony Walker
Northfield Road, Netherton
1
2
3
4
5
6
7
8
9
APPENDIX B
SPILMAN ASSOCIATES
TRIAL PIT NO: TP1
Geotechnical and Environmental Engineers 38 South Avenue Stourbridge West Midlands DY8 3XY Tel: 01384 820578 TRIAL PIT RECORD
Client: Mr Tony Walker Excavation Method: Wheeled Excavator Site: Northfield Road, Netherton Logged By: HDS
Date: 05/04/17 Job Number: J17035
Depth (m)
Strata Description
0 – 2.20
Loose black silty very sandy gravel of ash and clinker with much brick rubble and occasional metal fragments (MADE GROUND) No visual or olfactory evidence of contamination
Stability of Excavation: Unstable throughout Groundwater Observations: Dry Samples Taken: SD @ 0.20m; SB @ 1.20m; SB @ 1.00 – 2.00m Insitu Testing: None
SPILMAN ASSOCIATES
TRIAL PIT NO: TP2
Geotechnical and Environmental Engineers 38 South Avenue Stourbridge West Midlands DY8 3XY Tel: 01384 820578 TRIAL PIT RECORD
Client: Mr Tony Walker Excavation Method: Wheeled Excavator Site: Northfield Road, Netherton Logged By: HDS
Date: 05/04/17 Job Number: J17035
Depth (m)
Strata Description
0 – 0.10 0.10 – 1.95
Crushed brick hardcore with occasional concrete fragments (MADE GROUND) Loose black and dark grey slightly silty very sandy gravel of ash and clinker (MADE GROUND) No visual or olfactory evidence of contamination
Stability of Excavation: Slightly unstable Groundwater Observations: Dry Samples Taken: SD @ 0.30m; SB @ 1.50m; B @ 1.70m Insitu Testing: None
SPILMAN ASSOCIATES
TRIAL PIT NO: TP3
Geotechnical and Environmental Engineers 38 South Avenue Stourbridge West Midlands DY8 3XY Tel: 01384 820578 TRIAL PIT RECORD
Client: Mr Tony Walker Excavation Method: Wheeled Excavator Site: Northfield Road, Netherton Logged By: HDS
Date: 05/04/17 Job Number: J17035
Depth (m)
Strata Description
0 – 0.20 0.20 – 2.00
Brick rubble hardcore with occasional concrete fragments (MADE GROUND) Loose black slightly silty very sandy gravel of ash and clinker (MADE GROUND) No visual or olfactory evidence of contamination
Stability of Excavation: Slightly unstable Groundwater Observations: Dry Samples Taken: SD @ 0.30m; SB @ 2.00m Insitu Testing: None
SPILMAN ASSOCIATES
TRIAL PIT NO: TP4
Geotechnical and Environmental Engineers 38 South Avenue Stourbridge West Midlands DY8 3XY Tel: 01384 820578 TRIAL PIT RECORD
Client: Mr Tony Walker Excavation Method: Wheeled Excavator Site: Northfield Road, Netherton Logged By: HDS
Date: 05/04/17 Job Number: J17035
Depth (m)
Strata Description
0 – 2.30
Loose black slightly silty very sandy gravel of ash and clinker (MADE GROUND) No visual or olfactory evidence of contamination
Stability of Excavation: Slightly unstable Groundwater Observations: Dry Samples Taken: SD @ 0.20m; SB @ 2.00m; B @ 2.20m Insitu Testing: None
SPILMAN ASSOCIATES
TRIAL PIT NO: TP5
Geotechnical and Environmental Engineers 38 South Avenue Stourbridge West Midlands DY8 3XY Tel: 01384 820578 TRIAL PIT RECORD
Client: Mr Tony Walker Excavation Method: Wheeled Excavator Site: Northfield Road, Netherton Logged By: HDS
Date: 05/04/17 Job Number: J17035
Depth (m)
Strata Description
0 – 0.10 0.10 – 0.30 0.30 – 2.00
Crushed brick hardcore (MADE GROUND) Firm grey sandy slightly gravelly clay (colliery spoil). Gravel is angular mudstone (MADE GROUND) Loose black slightly silty very sandy gravel of ash and clinker (MADE GROUND) No visual or olfactory evidence of contamination
Stability of Excavation: Slightly unstable Groundwater Observations: Dry Samples Taken: SD @ 0.20m; SB @ 0.40m; SB @ 1.80m Insitu Testing: None
SPILMAN ASSOCIATES
TRIAL PIT NO: TP6
Geotechnical and Environmental Engineers 38 South Avenue Stourbridge West Midlands DY8 3XY Tel: 01384 820578 TRIAL PIT RECORD
Client: Mr Tony Walker Excavation Method: Wheeled Excavator Site: Northfield Road, Netherton Logged By: HDS
Date: 05/04/17 Job Number: J17035
Depth (m)
Strata Description
0 – 0.20 0.20 – 1.70
Roadstone over crushed concrete (MADE GROUND) Medium dense dark brown and grey clayey gravelly sand with much brick rubble (MADE GROUND) No visual or olfactory evidence of contamination
Stability of Excavation: Stable Groundwater Observations: Dry Samples Taken: SD @ 0.30m; SB @ 1.50m Insitu Testing: None
SPILMAN ASSOCIATES
TRIAL PIT NO: TP7
Geotechnical and Environmental Engineers 38 South Avenue Stourbridge West Midlands DY8 3XY Tel: 01384 820578 TRIAL PIT RECORD
Client: Mr Tony Walker Excavation Method: Wheeled Excavator Site: Northfield Road, Netherton Logged By: HDS
Date: 05/04/17 Job Number: J17035
Depth (m)
Strata Description
0 – 1.80
Loose to medium dense red brown and grey gravelly sand with much brick rubble (MADE GROUND) No visual or olfactory evidence of contamination
Stability of Excavation: Stable Groundwater Observations: Dry Samples Taken: SD @ 0.40m; SB @ 1.80m Insitu Testing: None
APPENDIX C
Northfield Road, Netherton (J17035/01)
N Value1.00 - 1.45 1 1 0 0 0 0 12.00 - 2.45 3 2 1 0 0 1 23.00 - 3.45 4 0 0 0 0 2 25.00 - 5.45 12 5 5 5 2 3 27.00 - 7.45 24 3 4 5 7 5 7
1.00 - 1.45 1 1 0 0 1 0 02.00 - 2.45 4 1 1 1 1 1 13.00 - 3.45 4 2 1 1 1 1 14.00 - 4.45 10 2 1 2 2 3 3
1.00 - 1.45 4 1 0 0 1 0 02.00 - 2.45 11 1 1 1 1 1 13.00 - 3.45 17 2 1 1 1 1 1 1.00 - 1.45 0 1 0 0 0 0 02.00 - 2.45 5 2 1 1 1 1 23.00 - 3.45 37 6 10 9 10 8 10
BH3
BH4
BH1
BH2
SUMMARY OF SPT 'N' RESULTS
Blows for 75mm PenetrationDepth (m)Borehole
APPENDIX D
Northfield Road, Netherton (J17035/01)
Trial Pit/Borehole Depth (m) PID Reading (ppm)
TP1 0.20 0.0
1.20 0.0
1.00 - 2.00 0.0
0.30 0.0
1.50 0.0
1.70 0.0
TP3 0.30 0.0
2.00 0.0
TP4 0.20 0.0
2.20 0.0
TP5 0.20 0.0
0.40 0.0
1.80 0.0
TP6 0.30 0.0
1.50 0.0
TP7 0.40 0.0
1.80 0.0
0.20 0.2
1.50 0.0
3.00 - 6.00 0.0
0.40 0.0
1.50 0.0
2.00 - 6.00 0.0
7.00 0.0
BH3 0.30 0.0
2.60 - 3.00 0.0
0.30 0.0
1.20 0.0
2.30 0.0
2.80 0.0
PID SCREENING RESULTS
TP2
BH1
BH2
BH4
APPENDIX E
SPILMAN ASSOCIATES Geotechnical and Environmental Engineers 38 South Avenue Stourbridge West Midlands DY8 3XY Tel: 01384 820578
Gas Monitoring Record Form Job No: Northfield Road, Netherton (J17035/01) Date: 07/04/17 Operator: HDS
Weather Conditions: Sunny
Barometric Pressure Trend (24 hr):
Surface Ground Conditions: Dry
Ambient Air Concentration (% Vol)
Methane
Carbon Dioxide
Oxygen
Barometric Pressure, Mb
Before 0.0 0.0 20.9 1009
During
After 0.0 0.0 20.9 1006
Monitoring Point
Gas Concentration (%)
Peak Steady
BH No
Depth to Water (m bgl)
CH4
CO2
O2
CH4
CO2
O2
Gas Emission Rate (l/hr)
Observations/ Comments
BH1 2.54 0.0 0.7 18.6 <0.5
BH2 Dry 0.0 0.7 20.0 <0.5
BH3 Dry 0.0 2.2 18.4 <0.5
BH4 Dry 0.0 1.5 19.1 <0.5
SPILMAN ASSOCIATES Geotechnical and Environmental Engineers 38 South Avenue Stourbridge West Midlands DY8 3XY Tel: 01384 820578
Gas Monitoring Record Form Job No: Northfield Road, Netherton (J17035/01) Date: 13/04/17 Operator: HDS
Weather Conditions: Overcast
Barometric Pressure Trend (24 hr):
Surface Ground Conditions: Dry
Ambient Air Concentration (% Vol)
Methane
Carbon Dioxide
Oxygen
Barometric Pressure, Mb
Before 0.0 0.0 20.5 1002
During
After 0.0 0.0 20.5 1002
Monitoring Point
Gas Concentration (%)
Peak Steady
BH No
Depth to Water (m bgl)
CH4
CO2
O2
CH4
CO2
O2
Gas Emission Rate (l/hr)
Observations/ Comments
BH1 2.56 0.0 2.2 18.3 <0.5
BH2 Dry 0.0 0.7 19.8 <0.5
BH3 Dry 0.0 2.7 17.6 <0.5
BH4 Dry 0.0 2.0 18.2 <0.5
SPILMAN ASSOCIATES Geotechnical and Environmental Engineers 38 South Avenue Stourbridge West Midlands DY8 3XY Tel: 01384 820578
Gas Monitoring Record Form Job No: Northfield Road, Netherton (J17035/01) Date: 20/04/17 Operator: HDS
Weather Conditions: Sunny
Barometric Pressure Trend (24 hr):
Surface Ground Conditions: Dry
Ambient Air Concentration (% Vol)
Methane
Carbon Dioxide
Oxygen
Barometric Pressure, Mb
Before 0.0 0.0 20.4 1019
During
After 0.0 0.0 20.4 1019
Monitoring Point
Gas Concentration (%)
Peak Steady
BH No
Depth to Water (m bgl)
CH4
CO2
O2
CH4
CO2
O2
Gas Emission Rate (l/hr)
Observations/ Comments
BH1 2.57 0.0 2.3 17.0 <0.5
BH2 Dry 0.0 3.4 16.8 <0.5
BH3 Dry 0.0 1.9 18.5 <0.5
BH4 Dry 0.0 2.6 17.2 <0.5
SPILMAN ASSOCIATES Geotechnical and Environmental Engineers 38 South Avenue Stourbridge West Midlands DY8 3XY Tel: 01384 820578
Gas Monitoring Record Form Job No: Northfield Road, Netherton (J17035/01) Date: 28/04/17 Operator: HDS
Weather Conditions: Sunny
Barometric Pressure Trend (24 hr):
Surface Ground Conditions: Damp
Ambient Air Concentration (% Vol)
Methane
Carbon Dioxide
Oxygen
Barometric Pressure, Mb
Before 0.0 0.0 20.4 999
During
After 0.0 0.0 20.4 999
Monitoring Point
Gas Concentration (%)
Peak Steady
BH No
Depth to Water (m bgl)
CH4
CO2
O2
CH4
CO2
O2
Gas Emission Rate (l/hr)
Observations/ Comments
BH1 2.58 0.0 2.0 18.7 <0.5
BH2 Dry 0.0 4.8 15.6 <0.5
BH3 Dry 0.0 0.8 19.8 <0.5
BH4 Dry 0.0 1.7 18.2 <0.5
SPILMAN ASSOCIATES Geotechnical and Environmental Engineers 38 South Avenue Stourbridge West Midlands DY8 3XY Tel: 01384 820578
Gas Monitoring Record Form Job No: Northfield Road, Netherton (J17035/01) Date: 05/05/17 Operator: HDS
Weather Conditions: Sunny
Barometric Pressure Trend (24 hr):
Surface Ground Conditions: Dry
Ambient Air Concentration (% Vol)
Methane
Carbon Dioxide
Oxygen
Barometric Pressure, Mb
Before 0.0 0.0 20.6 1007
During
After 0.0 0.0 20.6 1007
Monitoring Point
Gas Concentration (%)
Peak Steady
BH No
Depth to Water (m bgl)
CH4
CO2
O2
CH4
CO2
O2
Gas Emission Rate (l/hr)
Observations/ Comments
BH1 2.52 0.0 2.0 18.9 <0.5
BH2 Dry 0.0 4.7 15.9 <0.5
BH3 Dry 0.0 0.4 20.2 <0.5
BH4 Dry 0.0 0.9 19.3 <0.5
SPILMAN ASSOCIATES Geotechnical and Environmental Engineers 38 South Avenue Stourbridge West Midlands DY8 3XY Tel: 01384 820578
Gas Monitoring Record Form Job No: Northfield Road, Netherton (J17035/01) Date: 15/05/17 Operator: HDS
Weather Conditions: Overcast
Barometric Pressure Trend (24 hr):
Surface Ground Conditions: Wet
Ambient Air Concentration (% Vol)
Methane
Carbon Dioxide
Oxygen
Barometric Pressure, Mb
Before 0.0 0.0 20.4 1003
During
After 0.0 0.0 20.4 1003
Monitoring Point
Gas Concentration (%)
Peak Steady
BH No
Depth to Water (m bgl)
CH4
CO2
O2
CH4
CO2
O2
Gas Emission Rate (l/hr)
Observations/ Comments
BH1 2.57 0.0 0.8 19.6 <0.5
BH2 Dry 0.0 4.4 15.9 <0.5
BH3 Dry 0.0 1.3 18.2 <0.5
BH4 Dry 0.0 4.2 15.0 <0.5
APPENDIX F
Concept Life Sciences
Certificate of Analysis
Hadfield HouseHadfield Street
CornbrookManchester
M16 9FETel : 0161 874 2400Fax : 0161 874 2468
Report Number: 646143-1
Date of Report: 26-Apr-2017
Customer: Spilman Associates38 South AvenueStourbridge. WEST MIDLANDSDY8 3XY
Customer Contact: Mr Harry Spilman
Customer Job Reference: J17035Customer Site Reference: Northfield Road, Netherton
Date Job Received at Concept: 07-Apr-2017Date Analysis Started: 11-Apr-2017
Date Analysis Completed: 25-Apr-2017
The results reported relate to samples received in the laboratory and may not be representative of a wholebatch.Opinions and interpretations expressed herein are outside the scope of UKAS accreditationThis report should not be reproduced except in full without the written approval of the laboratoryTests covered by this certificate were conducted in accordance with Concept SOPs
This document has been printed from a digitally signed master copy
Concept Life Sciences is a trading name of
Scientific Analysis Laboratories registered in England and
Wales (No 2514788)
1549
Report checkedand authorised by :Muhammad WaqasProject Manager
Issued by :Muhammad WaqasProject Manager
Page 1 of 8
646143-1
Concept Reference: 646143
Project Site: Northfield Road, Netherton
Customer Reference: J17035
Soil Analysed as Soil
MCERTS Preparation
Concept Reference 646143 001 646143 002 646143 003 646143 004 646143 005
Customer Sample Reference TP1 TP2 TP3 TP4 TP5
Bottom Depth 0.20 0.30 0.30 0.20 0.40
Date Sampled 05-APR-2017 05-APR-2017 05-APR-2017 05-APR-2017 05-APR-2017
Type Sandy Soil Sandy Soil Sandy Soil Sandy Soil Sandy Soil
Determinand Method TestSample LOD Units
Retained on 10mm sieve T2 M40 0.1 % <0.1 <0.1 <0.1 <0.1 <0.1
Moisture @105C T162 AR 0.1 % 12 21 26 25 21
Asbestos ID T27 AR Chrysotile FibresDetected
N.D. N.D. N.D. N.D.
Arsenic T6 M40 2 mg/kg 44 26 25 35 14
Boron (water-soluble) T6 AR 1 mg/kg <1 <1 <1 <1 1
Cadmium T6 M40 1 mg/kg 2 <1 <1 19 <1
Chromium T6 M40 1 mg/kg 220 29 28 24 15
Chromium VI T6 AR 1 mg/kg <1 <1 <1 <1 <1
Copper T6 M40 1 mg/kg 290 130 110 160 68
Lead T6 M40 1 mg/kg 300 170 130 650 64
Mercury T6 M40 1 mg/kg <1 <1 <1 <1 <1
Nickel T6 M40 1 mg/kg 140 35 46 51 30
Selenium T6 M40 3 mg/kg <3 <3 <3 <3 <3
Zinc T6 M40 1 mg/kg 960 210 350 9300 160
Cyanide(free) T546 AR 1 mg/kg <1 <1 <1 <1 <1
Phenols(Mono) T546 AR 1 mg/kg <1 <1 <1 <1 <1
Cyanide(Complex) T85 AR 1 mg/kg <1 <1 <1 <1 <1
Cyanide(Total) T546 AR 1 mg/kg <1 <1 <1 <1 <1
SO4(Total) T6 A40 0.01 % 0.16 0.15 0.22 0.11 0.21
Sulphur(Free) T2 AR 500 mg/kg <500 <500 <500 <500 <500
pH T7 AR 8.0 8.1 8.1 7.8 7.7
Sulphide T4 AR 10 mg/kg 12 86 100 75 20
Naphthalene T207 M105 0.1 mg/kg <0.1 1.2 (100) <1.0 8.4 (100) <1.0
Acenaphthylene T207 M105 0.1 mg/kg 0.1 0.3 (100) <1.0 (100) <1.0 (100) <1.0
Acenaphthene T207 M105 0.1 mg/kg <0.1 0.5 (100) <1.0 4.7 (100) <1.0
Fluorene T207 M105 0.1 mg/kg <0.1 0.6 (100) <1.0 5.2 (100) <1.0
Phenanthrene T207 M105 0.1 mg/kg 0.6 4.8 (100) <1.0 30 (100) <1.0
Anthracene T207 M105 0.1 mg/kg 0.1 1.8 (100) <1.0 10 (100) <1.0
Fluoranthene T207 M105 0.1 mg/kg 1.2 5.2 (100) <1.0 28 (100) <1.0
Pyrene T207 M105 0.1 mg/kg 1.2 4.2 (100) <1.0 23 (100) <1.0
Benzo(a)Anthracene T207 M105 0.1 mg/kg 0.6 3.5 (100) <1.0 15 (100) <1.0
Chrysene T207 M105 0.1 mg/kg 0.9 4.0 (100) <1.0 16 (100) <1.0
Benzo(b/k)Fluoranthene T207 M105 0.1 mg/kg 1.8 4.9 (100) <1.0 19 (100) <1.0
Benzo(a)Pyrene T207 M105 0.1 mg/kg 1.1 2.8 (100) <1.0 11 (100) <1.0
Indeno(123-cd)Pyrene T207 M105 0.1 mg/kg 0.7 1.2 (100) <1.0 4.8 (100) <1.0
Dibenzo(ah)Anthracene T207 M105 0.1 mg/kg 0.3 0.5 (100) <1.0 1.7 (100) <1.0
Benzo(ghi)Perylene T207 M105 0.1 mg/kg 0.8 1.1 (100) <1.0 4.1 (100) <1.0
PAH(total) T207 M105 0.1 mg/kg 9.6 37 (100) <1.0 180 (100) <1.0
Benzene T209 M105 10 µg/kg (13) <10 (13) <10 (13) <10 (13,110) <20 (110,13) <20
Toluene T209 M105 10 µg/kg <10 <10 <10 (110) <20 (110) <20
EthylBenzene T209 M105 10 µg/kg <10 <10 <10 (110) <20 (110) <20
Methyl tert-Butyl Ether T209 M105 10 µg/kg <10 <10 <10 (110) <20 (110) <20
O Xylene T209 M105 10 µg/kg <10 <10 <10 (110) <20 (110) <20
M/P Xylene T209 M105 10 µg/kg <10 <10 <10 (110) <20 (110) <20
TPH (C5-C6 aliphatic) T209 M105 0.100 mg/kg <0.100 <0.100 <0.100 (110) <0.200 (110) <0.200
TPH (C6-C8 aliphatic) T209 M105 0.10 mg/kg <0.10 <0.10 <0.10 (110) <0.20 (110) <0.20
TPH (C8-C10 aliphatic) T209 M105 0.10 mg/kg <0.10 <0.10 <0.10 (110) <0.20 (110) <0.20
TPH (C10-C12 aliphatic) T206 M105 1 mg/kg (13,9) <10 (13) <1 (100,13) <10 (13,100) <10 (13,100) <10
TPH (C12-C16 aliphatic) T206 M105 2 mg/kg (9,13) <10 (13) <2 (100,13) <10 (100,13) <10 (100,13) <10
TPH (C16-C21 aliphatic) T206 M105 1 mg/kg (9,13) <10 (13) 2 (13,100) <10 (100,13) <10 (100,13) <10
TPH (C21-C35 aliphatic) T206 M105 4 mg/kg (13) 49 (13) 10 (13) 82 (100,13) <10 (13) 11
TPH (C35-C44 aliphatic) T8 M105 1 mg/kg (13) 11 (13) 4 (13,100) <10 (13) 12 (13,100) <10
TPH (Aliphatic) total T85 M105 mg/kg 60 (13) 12 (13) 82 (13) <10 (13) 11
TPH (C6-C7 aromatic) T209 M105 0.10 mg/kg <0.10 <0.10 <0.10 (110) <0.20 (110) <0.20
This document has been printed from a digitally signed master copy
Produced by Concept Life Sciences, Hadfield House, Hadfield Street, Cornbrook, Manchester, M16 9FE Page 2 of 8
646143-1
Concept Reference: 646143
Project Site: Northfield Road, Netherton
Customer Reference: J17035
Soil Analysed as Soil
MCERTS Preparation
Concept Reference 646143 001 646143 002 646143 003 646143 004 646143 005
Customer Sample Reference TP1 TP2 TP3 TP4 TP5
Bottom Depth 0.20 0.30 0.30 0.20 0.40
Date Sampled 05-APR-2017 05-APR-2017 05-APR-2017 05-APR-2017 05-APR-2017
Type Sandy Soil Sandy Soil Sandy Soil Sandy Soil Sandy Soil
Determinand Method TestSample LOD Units
TPH (C7-C8 aromatic) T209 M105 0.10 mg/kg <0.10 <0.10 <0.10 (110) <0.20 (110) <0.20
TPH (C8-C10 aromatic) T209 M105 0.10 mg/kg <0.10 <0.10 <0.10 (110) <0.20 (110) <0.20
TPH (C10-C12 aromatic) T206 M105 1 mg/kg (9,13) <10 (13) <1 (100,13) <10 (100,13) <10 (13,100) <10
TPH (C12-C16 aromatic) T206 M105 1 mg/kg (13,9) <10 (13) 9 (100,13) <10 (13) 10 (13,100) <10
TPH (C16-C21 aromatic) T206 M105 1 mg/kg (13,9) <10 (13) 44 (100,13) <10 (13) 61 (13,100) <10
TPH (C21-C35 aromatic) T206 M105 1 mg/kg (13,9) <10 (13) 110 (100,13) <10 (13) 79 (100,13) <10
TPH (C35-C44 aromatic) T8 M105 1 mg/kg (13,9) <10 (13) <1 (100,13) <10 (100,13) <10 (13,100) <10
TPH (Aromatic) total T85 M105 mg/kg <10 (13) 170 (13) <10 (13) 150 (13) <10
TPH (Aliphatic+Aromatic) (sum) T85 M105 mg/kg 60 (13) 180 (13) 82 (13) 150 (13) 11
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646143-1
Concept Reference: 646143
Project Site: Northfield Road, Netherton
Customer Reference: J17035
Soil Analysed as Soil
MCERTS Preparation
Concept Reference 646143 006 646143 007 646143 008 646143 009 646143 010
Customer Sample Reference TP6 TP7 TP1 TP3 TP7
Bottom Depth 0.30 0.40 1.20 2.00 1.80
Date Sampled 05-APR-2017 05-APR-2017 05-APR-2017 05-APR-2017 05-APR-2017
Type Sandy Soil Sandy Soil Sandy Soil Sandy Soil Sandy Soil
Determinand Method TestSample LOD Units
Retained on 10mm sieve T2 M40 0.1 % <0.1 <0.1 <0.1 <0.1 <0.1
Moisture @105C T162 AR 0.1 % 13 5.4 16 25 17
Asbestos ID T27 AR N.D. N.D. Amosite FibresDetected
N.D. Amosite FibresDetected
Arsenic T6 M40 2 mg/kg 54 40 68 30 27
Boron (water-soluble) T6 AR 1 mg/kg <1 <1 <1 <1 <1
Cadmium T6 M40 1 mg/kg 10 7 2 <1 6
Chromium T6 M40 1 mg/kg 79 38 210 35 26
Chromium VI T6 AR 1 mg/kg <1 <1 <1 <1 <1
Copper T6 M40 1 mg/kg 1400 680 480 120 500
Lead T6 M40 1 mg/kg 2000 460 210 160 320
Mercury T6 M40 1 mg/kg <1 <1 <1 <1 <1
Nickel T6 M40 1 mg/kg 140 76 260 42 47
Selenium T6 M40 3 mg/kg <3 <3 <3 <3 <3
Zinc T6 M40 1 mg/kg 3300 1400 990 430 910
Cyanide(free) T546 AR 1 mg/kg <1 <1 <1 <1 <1
Phenols(Mono) T546 AR 1 mg/kg <1 <1 <1 <1 <1
Cyanide(Complex) T85 AR 1 mg/kg <1 <1 3 <1 <1
Cyanide(Total) T546 AR 1 mg/kg <1 <1 3 <1 <1
SO4(Total) T6 A40 0.01 % 0.30 0.18 0.23 0.33 0.20
Sulphur(Free) T2 AR 500 mg/kg <500 <500 <500 <500 <500
pH T7 AR 7.9 8.2 7.9 8.1 8.0
Sulphide T4 AR 10 mg/kg 110 120 34 120 120
Naphthalene T207 M105 0.1 mg/kg 0.1 0.2 1.0 0.4 0.1
Acenaphthylene T207 M105 0.1 mg/kg 0.2 0.5 0.4 <0.1 0.1
Acenaphthene T207 M105 0.1 mg/kg 0.1 0.2 0.2 0.2 <0.1
Fluorene T207 M105 0.1 mg/kg 0.1 0.3 0.2 0.1 <0.1
Phenanthrene T207 M105 0.1 mg/kg 1.6 2.8 1.9 1.2 1.1
Anthracene T207 M105 0.1 mg/kg 0.4 1.2 0.5 0.4 0.5
Fluoranthene T207 M105 0.1 mg/kg 4.6 4.0 2.4 1.9 2.2
Pyrene T207 M105 0.1 mg/kg 4.5 3.9 2.2 1.7 2.3
Benzo(a)Anthracene T207 M105 0.1 mg/kg 2.2 3.7 1.2 1.1 1.8
Chrysene T207 M105 0.1 mg/kg 2.9 3.9 2.2 1.2 2.1
Benzo(b/k)Fluoranthene T207 M105 0.1 mg/kg 7.8 13 4.6 2.5 8.0
Benzo(a)Pyrene T207 M105 0.1 mg/kg 3.6 5.9 2.4 1.1 3.7
Indeno(123-cd)Pyrene T207 M105 0.1 mg/kg 2.5 4.0 1.8 0.6 2.9
Dibenzo(ah)Anthracene T207 M105 0.1 mg/kg 0.6 1.3 <0.1 <0.1 0.9
Benzo(ghi)Perylene T207 M105 0.1 mg/kg 2.3 4.1 1.9 0.6 3.2
PAH(total) T207 M105 0.1 mg/kg 33 49 23 13 29
Benzene T209 M105 10 µg/kg (13) <10 (13) <10 (13) <10 (13) <10 (13) <10
Toluene T209 M105 10 µg/kg <10 <10 <10 <10 <10
EthylBenzene T209 M105 10 µg/kg <10 <10 <10 <10 17
Methyl tert-Butyl Ether T209 M105 10 µg/kg <10 <10 <10 <10 <10
O Xylene T209 M105 10 µg/kg <10 <10 <10 <10 <10
M/P Xylene T209 M105 10 µg/kg <10 <10 <10 <10 13
TPH (C5-C6 aliphatic) T209 M105 0.100 mg/kg <0.100 <0.100 <0.100 <0.100 <0.100
TPH (C6-C8 aliphatic) T209 M105 0.10 mg/kg <0.10 <0.10 <0.10 <0.10 <0.10
TPH (C8-C10 aliphatic) T209 M105 0.10 mg/kg <0.10 <0.10 <0.10 <0.10 <0.10
TPH (C10-C12 aliphatic) T206 M105 1 mg/kg (9,13) <10 (13) <1 (13,9) <10 (100,13) <10 (13,9) <10
TPH (C12-C16 aliphatic) T206 M105 2 mg/kg (13,9) <10 (13) 3 (9,13) <10 (13,100) <10 (9,13) <10
TPH (C16-C21 aliphatic) T206 M105 1 mg/kg (13,9) <10 (13) 8 (13) 34 (100,13) <10 (13) 14
TPH (C21-C35 aliphatic) T206 M105 4 mg/kg (13) 34 (13) 26 (9,13) <10 (13) 20 (13) 65
TPH (C35-C44 aliphatic) T8 M105 1 mg/kg (13) 18 (13) 9 (13) 10 (13,100) <10 (13) 18
TPH (Aliphatic) total T85 M105 mg/kg 52 (13) 37 44 (13) 20 98
TPH (C6-C7 aromatic) T209 M105 0.10 mg/kg <0.10 <0.10 <0.10 <0.10 <0.10
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646143-1
Concept Reference: 646143
Project Site: Northfield Road, Netherton
Customer Reference: J17035
Soil Analysed as Soil
MCERTS Preparation
Concept Reference 646143 006 646143 007 646143 008 646143 009 646143 010
Customer Sample Reference TP6 TP7 TP1 TP3 TP7
Bottom Depth 0.30 0.40 1.20 2.00 1.80
Date Sampled 05-APR-2017 05-APR-2017 05-APR-2017 05-APR-2017 05-APR-2017
Type Sandy Soil Sandy Soil Sandy Soil Sandy Soil Sandy Soil
Determinand Method TestSample LOD Units
TPH (C7-C8 aromatic) T209 M105 0.10 mg/kg <0.10 <0.10 <0.10 <0.10 <0.10
TPH (C8-C10 aromatic) T209 M105 0.10 mg/kg <0.10 <0.10 <0.10 <0.10 <0.10
TPH (C10-C12 aromatic) T206 M105 1 mg/kg (13,9) <10 (13) <1 (13,9) <10 (100,13) <10 (13,9) <10
TPH (C12-C16 aromatic) T206 M105 1 mg/kg (9,13) <10 (13) 13 (9,13) <10 (100,13) <10 (9,13) <10
TPH (C16-C21 aromatic) T206 M105 1 mg/kg (13) 76 (13) 110 (13,9) <10 (100,13) <10 (13) 120
TPH (C21-C35 aromatic) T206 M105 1 mg/kg (13) 250 (13) 320 (9,13) <10 (13) 27 (13) 550
TPH (C35-C44 aromatic) T8 M105 1 mg/kg (9,13) <10 (13) 6 (9,13) <10 (13,100) <10 (13,9) <10
TPH (Aromatic) total T85 M105 mg/kg 330 (13) 440 <10 (13) 27 670
TPH (Aliphatic+Aromatic) (sum) T85 M105 mg/kg 380 (13) 480 44 (13) 46 760
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646143-1
Concept Reference: 646143
Project Site: Northfield Road, Netherton
Customer Reference: J17035
Soil Analysed as Soil
MCERTS Preparation
Concept Reference 646143 011 646143 012 646143 013 646143 014
Customer Sample Reference BH1 BH2 BH3 BH4
Bottom Depth 0.20 0.40 0.30 0.30
Date Sampled 05-APR-2017 05-APR-2017 05-APR-2017 05-APR-2017
Type Sandy Soil Sandy Soil Sandy Soil Sandy Soil
Determinand Method TestSample LOD Units
Retained on 10mm sieve T2 M40 0.1 % <0.1 <0.1 <0.1 <0.1
Moisture @105C T162 AR 0.1 % 16 24 27 18
Asbestos ID T27 AR Amosite FibresDetected
N.D. N.D. N.D.
Arsenic T6 M40 2 mg/kg 52 54 19 37
Boron (water-soluble) T6 AR 1 mg/kg <1 <1 <1 <1
Cadmium T6 M40 1 mg/kg 3 3 2 78
Chromium T6 M40 1 mg/kg 68 26 18 61
Chromium VI T6 AR 1 mg/kg <1 <1 <1 <1
Copper T6 M40 1 mg/kg 250 210 160 950
Lead T6 M40 1 mg/kg 510 430 110 770
Mercury T6 M40 1 mg/kg <1 1 <1 <1
Nickel T6 M40 1 mg/kg 77 49 30 170
Selenium T6 M40 3 mg/kg <3 <3 <3 <3
Zinc T6 M40 1 mg/kg 1300 4200 190 1300
Cyanide(free) T546 AR 1 mg/kg <1 <1 <1 <1
Phenols(Mono) T546 AR 1 mg/kg <1 <1 <1 <1
Cyanide(Complex) T85 AR 1 mg/kg <1 <1 <1 <1
Cyanide(Total) T546 AR 1 mg/kg <1 <1 <1 <1
SO4(Total) T6 A40 0.01 % 0.18 0.14 0.10 0.24
Sulphur(Free) T2 AR 500 mg/kg <500 <500 <500 <500
pH T7 AR 7.9 8.0 7.9 8.1
Sulphide T4 AR 10 mg/kg 54 20 80 140
Naphthalene T207 M105 0.1 mg/kg 0.4 1.0 0.4 <0.1
Acenaphthylene T207 M105 0.1 mg/kg 0.4 0.3 <0.1 0.1
Acenaphthene T207 M105 0.1 mg/kg 0.1 0.5 0.7 <0.1
Fluorene T207 M105 0.1 mg/kg 0.1 0.7 0.5 <0.1
Phenanthrene T207 M105 0.1 mg/kg 1.6 6.1 3.6 1.1
Anthracene T207 M105 0.1 mg/kg 0.5 1.8 1.3 0.5
Fluoranthene T207 M105 0.1 mg/kg 1.8 7.0 3.9 2.1
Pyrene T207 M105 0.1 mg/kg 1.6 5.9 3.4 2.1
Benzo(a)Anthracene T207 M105 0.1 mg/kg 1.3 4.1 2.3 1.9
Chrysene T207 M105 0.1 mg/kg 1.5 4.3 2.3 2.0
Benzo(b/k)Fluoranthene T207 M105 0.1 mg/kg 3.5 8.8 5.1 5.8
Benzo(a)Pyrene T207 M105 0.1 mg/kg 1.5 3.9 2.2 2.6
Indeno(123-cd)Pyrene T207 M105 0.1 mg/kg 1.0 2.3 1.2 1.9
Dibenzo(ah)Anthracene T207 M105 0.1 mg/kg 0.3 0.9 0.4 0.6
Benzo(ghi)Perylene T207 M105 0.1 mg/kg 1.0 2.2 1.2 2.0
PAH(total) T207 M105 0.1 mg/kg 17 50 28 23
Benzene T209 M105 10 µg/kg (13,110) <20 (110,13) <20 (110,13) <20 (13,110) <20
Toluene T209 M105 10 µg/kg (110) <20 (110) <20 (110) <20 (110) <20
EthylBenzene T209 M105 10 µg/kg (110) <20 (110) <20 20 27
Methyl tert-Butyl Ether T209 M105 10 µg/kg (110) <20 (110) <20 (110) <20 (110) <20
O Xylene T209 M105 10 µg/kg (110) <20 (110) <20 (110) <20 (110) <20
M/P Xylene T209 M105 10 µg/kg 20 (110) <20 (110) <20 29
TPH (C5-C6 aliphatic) T209 M105 0.100 mg/kg (110) <0.200 (110) <0.200 (110) <0.200 (110) <0.200
TPH (C6-C8 aliphatic) T209 M105 0.10 mg/kg (110) <0.20 (110) <0.20 (110) <0.20 (110) <0.20
TPH (C8-C10 aliphatic) T209 M105 0.10 mg/kg (110) <0.20 (110) <0.20 (110) <0.20 (110) <0.20
TPH (C10-C12 aliphatic) T206 M105 1 mg/kg (13) <1 (100,13) <10 (13) <1 (13) <1
TPH (C12-C16 aliphatic) T206 M105 2 mg/kg (13) 5 (100,13) <10 (13) <2 (13) <2
TPH (C16-C21 aliphatic) T206 M105 1 mg/kg (13) 22 (13) 17 (13) 2 (13) 4
TPH (C21-C35 aliphatic) T206 M105 4 mg/kg (13) 20 (13) 39 (13) 4 (13) 28
TPH (C35-C44 aliphatic) T8 M105 1 mg/kg (13) <1 (13) 57 (13) 4 (13) <1
TPH (Aliphatic) total T85 M105 mg/kg (13) 47 (13) 55 (13) 6.1 (13) 33
TPH (C6-C7 aromatic) T209 M105 0.10 mg/kg (110) <0.20 (110) <0.20 (110) <0.20 (110) <0.20
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646143-1
Index to symbols used in 646143-1
Notes
Method Index
Accreditation Summary
Concept Reference: 646143
Project Site: Northfield Road, Netherton
Customer Reference: J17035
Soil Analysed as Soil
MCERTS Preparation
Concept Reference 646143 011 646143 012 646143 013 646143 014
Customer Sample Reference BH1 BH2 BH3 BH4
Bottom Depth 0.20 0.40 0.30 0.30
Date Sampled 05-APR-2017 05-APR-2017 05-APR-2017 05-APR-2017
Type Sandy Soil Sandy Soil Sandy Soil Sandy Soil
Determinand Method TestSample LOD Units
TPH (C7-C8 aromatic) T209 M105 0.10 mg/kg (110) <0.20 (110) <0.20 (110) <0.20 (110) <0.20
TPH (C8-C10 aromatic) T209 M105 0.10 mg/kg (110) <0.20 (110) <0.20 (110) <0.20 (110) <0.20
TPH (C10-C12 aromatic) T206 M105 1 mg/kg (13) 2 (13) <1 (13) <1 (13) <1
TPH (C12-C16 aromatic) T206 M105 1 mg/kg (13) 30 (13) 18 (13) 3 (13) 4
TPH (C16-C21 aromatic) T206 M105 1 mg/kg (13) 31 (13) 160 (13) 16 (13) 32
TPH (C21-C35 aromatic) T206 M105 1 mg/kg (13) 81 (13) 420 (13) 41 (13) 130
TPH (C35-C44 aromatic) T8 M105 1 mg/kg (13) <1 (13,100) <10 (13) <1 (13) <1
TPH (Aromatic) total T85 M105 mg/kg (13) 140 (13) 610 (13) 60 (13) 160
TPH (Aliphatic+Aromatic) (sum) T85 M105 mg/kg (13) 190 (13) 660 (13) 67 (13) 190
Value Description
M40 Analysis conducted on sample assisted dried at no morethan 40C. Results are reported on a dry weight basis.
A40 Assisted dried < 40C
AR As Received
M105 Analysis conducted on an "as received" aliquot. Resultsare reported on a dry weight basis where moisture contentwas determined by assisted drying of sample at 105C
N.D. Not Detected
9 LOD raised due to dilution of sample
13 Results have been blank corrected.
100 LOD determined by sample aliquot used for analysis
110 LOD raised due to low internal standard recovery.
S Analysis was subcontracted
M Analysis is MCERTS accredited
U Analysis is UKAS accredited
N Analysis is not UKAS accredited
These samples have been analysed exceeding recommended holding times for pH. It is possible therefore that the results provided may be compromised.
Asbestos subcontracted to REC Asbestos
Value Description
T4 Colorimetry
T207 GC/MS (MCERTS)
T162 Grav (1 Dec) (105 C)
T546 Colorimetry (CF)
T2 Grav
T6 ICP/OES
T27 PLM
T85 Calc
T209 GC/MS (Head Space)(MCERTS)
T206 GC/FID (MCERTS)
T7 Probe
T8 GC/FID
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646143-1
Determinand Method TestSample LOD Units Symbol Concept References
Retained on 10mm sieve T2 M40 0.1 % N 001-014
Moisture @105C T162 AR 0.1 % N 001-014
Asbestos ID T27 AR SU 001-014
Arsenic T6 M40 2 mg/kg M 001-014
Boron (water-soluble) T6 AR 1 mg/kg N 001-014
Cadmium T6 M40 1 mg/kg M 001-014
Chromium T6 M40 1 mg/kg M 001-014
Chromium VI T6 AR 1 mg/kg N 001-014
Copper T6 M40 1 mg/kg M 001-014
Lead T6 M40 1 mg/kg M 001-014
Mercury T6 M40 1 mg/kg M 001-014
Nickel T6 M40 1 mg/kg M 001-014
Selenium T6 M40 3 mg/kg M 001-014
Zinc T6 M40 1 mg/kg M 001-014
Cyanide(free) T546 AR 1 mg/kg M 001-014
Phenols(Mono) T546 AR 1 mg/kg M 001-014
Cyanide(Complex) T85 AR 1 mg/kg N 001-014
Cyanide(Total) T546 AR 1 mg/kg M 001-014
SO4(Total) T6 A40 0.01 % N 001-014
Sulphur(Free) T2 AR 500 mg/kg N 001-014
pH T7 AR M 001-014
Sulphide T4 AR 10 mg/kg N 001-014
Naphthalene T207 M105 0.1 mg/kg M 001-014
Acenaphthylene T207 M105 0.1 mg/kg U 001-014
Acenaphthene T207 M105 0.1 mg/kg M 001-014
Fluorene T207 M105 0.1 mg/kg M 001-014
Phenanthrene T207 M105 0.1 mg/kg M 001-014
Anthracene T207 M105 0.1 mg/kg U 001-014
Fluoranthene T207 M105 0.1 mg/kg M 001-014
Pyrene T207 M105 0.1 mg/kg M 001-014
Benzo(a)Anthracene T207 M105 0.1 mg/kg M 001-014
Chrysene T207 M105 0.1 mg/kg M 001-014
Benzo(b/k)Fluoranthene T207 M105 0.1 mg/kg M 001-014
Benzo(a)Pyrene T207 M105 0.1 mg/kg M 001-014
Indeno(123-cd)Pyrene T207 M105 0.1 mg/kg M 001-014
Dibenzo(ah)Anthracene T207 M105 0.1 mg/kg M 001-014
Benzo(ghi)Perylene T207 M105 0.1 mg/kg M 001-014
PAH(total) T207 M105 0.1 mg/kg U 001-014
Benzene T209 M105 10 µg/kg M 001-014
Toluene T209 M105 10 µg/kg M 001-014
EthylBenzene T209 M105 10 µg/kg M 001-014
Methyl tert-Butyl Ether T209 M105 10 µg/kg M 001-014
O Xylene T209 M105 10 µg/kg M 001-014
M/P Xylene T209 M105 10 µg/kg M 001-014
TPH (C5-C6 aliphatic) T209 M105 0.100 mg/kg N 001-014
TPH (C6-C8 aliphatic) T209 M105 0.10 mg/kg N 001-014
TPH (C8-C10 aliphatic) T209 M105 0.10 mg/kg N 001-014
TPH (C10-C12 aliphatic) T206 M105 1 mg/kg N 001-014
TPH (C12-C16 aliphatic) T206 M105 2 mg/kg M 001-014
TPH (C16-C21 aliphatic) T206 M105 1 mg/kg M 001-014
TPH (C21-C35 aliphatic) T206 M105 4 mg/kg M 001-014
TPH (C35-C44 aliphatic) T8 M105 1 mg/kg N 001-014
TPH (Aliphatic) total T85 M105 mg/kg N 001-014
TPH (C6-C7 aromatic) T209 M105 0.10 mg/kg N 001-014
TPH (C7-C8 aromatic) T209 M105 0.10 mg/kg N 001-014
TPH (C8-C10 aromatic) T209 M105 0.10 mg/kg N 001-014
TPH (C10-C12 aromatic) T206 M105 1 mg/kg M 001-014
TPH (C12-C16 aromatic) T206 M105 1 mg/kg M 001-014
TPH (C16-C21 aromatic) T206 M105 1 mg/kg M 001-014
TPH (C21-C35 aromatic) T206 M105 1 mg/kg M 001-014
TPH (C35-C44 aromatic) T8 M105 1 mg/kg N 001-014
TPH (Aromatic) total T85 M105 mg/kg N 001-014
TPH (Aliphatic+Aromatic) (sum) T85 M105 mg/kg N 001-014
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646143-1
Concept Life Sciences
Certificate of Analysis
Hadfield HouseHadfield Street
CornbrookManchester
M16 9FETel : 0161 874 2400Fax : 0161 874 2468
Report Number: 650539-1
Date of Report: 11-May-2017
Customer: Spilman Associates38 South AvenueStourbridge. WEST MIDLANDSDY8 3XY
Customer Contact: Mr Harry Spilman
Customer Job Reference: J17035Customer Site Reference: Northfield Road, Netherton
Date Job Received at Concept: 07-Apr-2017Date Analysis Started: 02-May-2017
Date Analysis Completed: 11-May-2017
The results reported relate to samples received in the laboratory and may not be representative of a wholebatch.This report should not be reproduced except in full without the written approval of the laboratoryTests covered by this certificate were conducted in accordance with Concept SOPs
This document has been printed from a digitally signed master copy
Concept Life Sciences is a trading name of
Scientific Analysis Laboratories registered in England and
Wales (No 2514788)
Report checkedand authorised by :Sara Abou-ShakraProject Manager
Issued by :Sara Abou-ShakraProject Manager
Page 1 of 2
650539-1
Index to symbols used in 650539-1
Notes
Method Index
Accreditation Summary
Concept Reference: 650539
Project Site: Northfield Road, Netherton
Customer Reference: J17035
Soil Analysed as Soil
Miscellaneous
Concept Reference 650539 001 650539 002 650539 003 650539 004
Customer Sample Reference TP1 (646143/001) TP1 (646143/008) TP7 (646143/010) BH1 (646143/011)
Date Sampled 05-APR-2017 05-APR-2017 05-APR-2017 05-APR-2017
Determinand Method TestSample LOD Units
Asbestos Quantification T27 AR 0.001 % Chrysotile FibresDetected
<0.001
Amosite Fibres Detected
<0.001
Amosite Fibres Detected
<0.001
Amosite Fibres Detected
<0.001
Value Description
AR As Received
S Analysis was subcontracted
U Analysis is UKAS accredited
Asbestos subcontracted to REC Asbestos
Asbestos type for all 4 samples consistent with Loose fibres.
Value Description
T27 PLM
Determinand Method TestSample LOD Units Symbol Concept References
Asbestos Quantification T27 AR 0.001 % SU 001-004
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650539-1
APPENDIX G