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Professional Service Industries, Inc. 4161 Ridgemoor Avenue Memphis, Tennessee 38118 Phone (901) 365-1802 October 30, 2014 Triple Z Development, Inc. and K3C2 Investments, LLC 7730 Trinity Road Suite 107 Cordova, Tennessee 38018 Attn: Keith Saunders Subject: Phase II Environmental Site Assessment Former Christie Cut Stone 2029 Elzey Avenue Memphis, Shelby County, Tennessee PSI Project # 05021106 Dear Mr. Saunders: In general accordance with our agreement, Professional Service Industries, Inc. (PSI) performed a Phase II Environmental Site Assessment for the above referenced property. Thank you for choosing PSI as your environmental consultant for this project. If you have any questions, or if we can be of additional service, please contact us at (901) 365-1802. Respectfully Submitted, PROFESSIONAL SERVICE INDUSTRIES, INC. Richard M. Reynolds Patricia St. Peter, LPG (IN) Project Manager Principal Consultant Environmental Services Environmental Services Attachments
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Page 1: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802

October 30, 2014 Triple Z Development, Inc. and K3C2 Investments, LLC 7730 Trinity Road – Suite 107 Cordova, Tennessee 38018 Attn: Keith Saunders Subject: Phase II Environmental Site Assessment Former Christie Cut Stone 2029 Elzey Avenue Memphis, Shelby County, Tennessee PSI Project # 05021106 Dear Mr. Saunders: In general accordance with our agreement, Professional Service Industries, Inc. (PSI) performed a Phase II Environmental Site Assessment for the above referenced property. Thank you for choosing PSI as your environmental consultant for this project. If you have any questions, or if we can be of additional service, please contact us at (901) 365-1802. Respectfully Submitted, PROFESSIONAL SERVICE INDUSTRIES, INC. Richard M. Reynolds Patricia St. Peter, LPG (IN) Project Manager Principal Consultant Environmental Services Environmental Services Attachments

Page 2: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

Report of

Phase II Environmental Site Assessment

Former Christie Cut Stone

2029 Elzey Avenue Memphis, Tennessee

Prepared for

Triple Z Development, Inc. and

K3C2 Investments, LLC

7730 Trinity Road – Suite 107

Cordova, Tennessee 38018

Prepared by

Professional Service Industries, Inc.

4161 Ridgemoor Avenue

Memphis, Tennessee 38118

October 30, 2014

PSI Project: 05021106

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

TABLE OF CONTENTS

1 EXECUTIVE SUMMARY ....................................................................................................... 1 1.1 FINDINGS ................................................................................................................ 2 1.2 CONCLUSIONS ...................................................................................................... 3 1.3 RECOMMENDATIONS ........................................................................................... 3

2 INTRODUCTION ................................................................................................................... 4 2.1 OVERVIEW OF ASTM E1903-11 STANDARD PRACTICE .................................... 4 2.2 OBJECTIVES .......................................................................................................... 4 2.3 DEVIATIONS FROM CONTRACT .......................................................................... 5

3 BACKGROUND ..................................................................................................................... 6 3.1 SITE DESCRIPTION AND FEATURES .................................................................. 6 3.2 PHYSICAL SETTING .............................................................................................. 6 3.3 SITE HISTORY AND LAND USE ............................................................................ 7 3.4 CURRENT AND HISTORIC ADJACENT LAND USE.............................................. 7 3.5 SUMMARY OF PREVIOUS ASSESSMENTS ......................................................... 7

4 SCOPE OF WORK AND SAMPLING RATIONALE ............................................................. 8 4.1 SITE CONCEPTUAL MODEL AND HYPOTHESIS STATEMENT(S) ..................... 8 4.2 FIELD INVESTIGATION SUMMARY ...................................................................... 8 4.3 SAMPLING RATIONALE AND METHODOLOGY ................................................... 9 4.4 INVESTIGATION DERIVED WASTES .................................................................... 9

5 DATA ANALYSIS & INTERPRETATION ............................................................................ 10 5.1 REGULATORY GUIDANCE CONCENTRATIONS ............................................... 10 5.2 SITE HYDROGEOLOGICAL CHARACTERISTICS .............................................. 10 5.3 DATA VALIDATION ............................................................................................... 10 5.4 SUMMARY OF FIELD SCREENING AND ANALYTICAL RESULTS .................... 10

6 CONCLUSIONS AND RECOMMENDATIONS ................................................................... 12 6.1 CONCLUSIONS FOR AREA OF CONCERN #1 ................................................... 12 6.2 RECOMMENDATIONS ......................................................................................... 13

7 WARRANTY ........................................................................................................................ 14 7.1 WARRANTY .......................................................................................................... 14 7.2 USE BY THIRD PARTIES ..................................................................................... 15

8 REFERENCES .................................................................................................................... 16 FIGURES

FIGURE 1 – SITE LOCATION MAP FIGURE 2 – SITE LAYOUT SKETCH FIGURE 3 – BORING LOCATION SKETCH TABLE

TABLE 1 – SOIL ANALYTICAL DATA SUMMARY APPENDICES

APPENDIX A – LABORATORY ANALYTICAL DATA REPORT

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

1

1 EXECUTIVE SUMMARY

Professional Service Industries, Inc. (PSI) has conducted a Phase II Environmental Site Assessment (ESA) at the former Christie Cut Stone property located at 2029 Elzey Avenue in Memphis, Shelby County, Tennessee (subject property). The assessment was performed in general accordance with the scope and limitations of the American Society for Testing and Materials (ASTM) Standard E 1903-11. The assessment was performed to address specific recognized environmental conditions (RECs) and objectives that were stated by the client. Exceptions or deletions from the contracted scope of work are described in Section 2.4 of this report. The approximately 2.32-acre subject property is improved with an approximately 3,900-square-foot two-story, office building on the southeast portion. The building, which formerly served as an office for Christie Cut Stone, is currently being used by the property owner for storage of building materials, furniture, and other miscellaneous items. The remainder of the subject property is a gravel-covered and partially paved lot/laydown yard that is overgrown with vegetation. The storage yard area consists of multiple piles of stone, rock, wood, and other debris left from the former owner/operator. A Phase I ESA was prepared by PSI and issued on June 26, 2014. The Phase I ESA identified the following REC in connection with the subject property:

Based on the historical research obtained, the types of current and former structures on-site, and previous knowledge from similar site assessments, the subject property appears to have most likely been originally developed as a small manufactured gas plant (MGP). These types of facilities produced gas for lighting, heating, and cooking in a localized area, prior to the mass distribution of natural gas via pipelines. The production process typically involved heating coal or oil to generate gas. However, in addition to producing the desired gas, various toxic by-products were often produced, including coal tar, sludge, metals, cyanide, light oils, spent oxide wastes, phenols, cresols, and other hydrocarbon products. Some of these products would have typically been stored in subsurface containers or disposed of in dump areas on-site. Significant amounts of contamination usually occur at MGP sites due to the nature of the operation and waste by-products generated. In addition, the generated wastes contain a number of known or suspected carcinogens and other potentially hazardous chemicals to both human health and the environment. Therefore, the likely former use of the subject property as a MGP represents a REC.

The scope of the Phase II ESA was intended to address the RECs listed above. The Phase II ESA was conducted to address the following objectives which were defined through a discussion between the assessor and the client:

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

2

Assess whether there has been a release of hazardous substances or petroleum products.

Provide information relevant to identifying, defining, and evaluating property conditions associated with target analytes that may pose a risk to human health or the environment, risk of bodily injury to persons on the property, and thereby give rise to potential liability.

The assessment included the following general scope of services:

Health & Safety Plan Preparation

Installation of Soil Borings

Collection of Soil Samples

Data Analysis and Report Preparation *Note: Although anticipated, groundwater was not encountered during the drilling activities. Therefore, groundwater samples were not collected as part of the field work activities for this Phase II ESA.

1.1 FINDINGS

A total of ten (10) soil borings were advanced at the subject property using direct-push technology drilling methods to investigate the historical development of a manufactured gas plant on the property. Soil samples were collected for laboratory analysis of volatile organic compounds (VOCs), semi-volatile organic compounds (SVOCs), polychlorinated biphenyls (PCBs), cyanide, sulfate, sulfide, pH, and priority pollutant metals (including antimony, arsenic, beryllium, cadmium, chromium, copper, lead, mercury, nickel, selenium, silver, thallium, zinc). Laboratory analysis for the collected soil samples indicated various concentrations of acenapthalene; acenapthylene; anthracene; benzo(a)anthracene; benzo(a)pyrene; benzo(b)fluoranthene; benzo(g,h,i)perylene; benzo(k)fluoranthene; carbazole; chrysene; dibenz(a,h)anthracene; dibenzofuran; fluorathene; fluorene; indeno(1,2,3-cd)pyrene; 2-methylnapthalene; naphthalene; phenanthrene; pyrene; sulfate; arsenic; beryllium; cadmium; chromium; copper; lead; mercury; nickel; and zinc above laboratory reporting limits. Of the detected analytes, all were below the appropriate USEPA screening value with the exception of benzo(a)anthracene; benzo(a)pyrene; benzo(b)fluoranthene; benzo(k)fluoranthene; dibenz(a,h)anthracene; indeno(1,2,3-cd)pyrene; and arsenic. The detected arsenic levels ranged from 1.62 mg/kg to 8.62 mg/kg, which are above the USEPA RSL of 0.39 mg/kg. However, arsenic is a natural occurring metal at high levels in the soils of this region and the concentrations of arsenic identified in the soil samples are below the accepted background level of 10 mg/kg for arsenic in the Mid-South. Therefore, no further investigation of arsenic in soil appears warranted at this time.

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

3

The analytes benzo(a)anthracene; benzo(a)pyrene; benzo(b)fluoranthene; benzo(k)fluoranthene; dibenz(a,h)anthracene; indeno(1,2,3-cd)pyrene are SVOCs that contain carbon and hydrogen. These analytes are components, byproducts, or waste products resulting from the production process of manufacturing gas, which typically involved heating coal or oil to generate gas. Laboratory analyses for these constituents, which exceeded the appropriate screening levels, were identified at the following concentrations:

Benzo(a)anthracene at 1.97 mg/kg in SB-7 (8-12’) and 4.7 mg/kg in SB-8 (0-4’), which is above the USEPA RSL of 0.15 mg/kg

Benzo(a)pyrene at 2.36 mg/kg in SB-7 (8-12’) and 4.59 mg/kg in SB-8 (0-4’), which is above the USEPA RSL of 0.015 mg/kg

Benzo(b)fluoranthene at 1.82 mg/kg in SB-7 (8-12’) and 4.79 mg/kg in SB-8 (0-4’), which is above the USEPA RSL of 0.015 mg/kg

Benzo(k)fluoranthene at 2.43 mg/kg in SB-8 (0-4’), which is above the USEPA RSL of 1.5 mg/kg

Dibenz(a,h)anthracene at 0.257 mg/kg in SB-7 (8-12’) and 0.656 mg/kg in SB-8 (0-4’), which is above the USEPA RSL of 0.015 mg/kg

Indeno(1,2,3-cd)pyrene at 1.14 mg/kg in SB-7 (8-12’) and 2.48 mg/kg in SB-8 (0-4’), which is above the USEPA RSL of 0.015 mg/kg

1.2 CONCLUSIONS

This Phase II ESA has provided sufficient information to conclude that isolated subsurface soils at the subject property have been adversely impacted by components, byproducts, and/or waste products that would have been used or generated from the former manufactured gas plant that historically operated at the property. However, the areas appear relatively shallow and site-wide or broad scale soil contamination is not expected. In addition, groundwater was not encountered and it not expected to be impacted by the former site operations.

1.3 RECOMMENDATIONS

Based on the isolated nature of the detected constituents in the subsurface soil at the subject property, an additional site-wide assessment to better delineate the extent of subsurface impacts is not warranted at this time. However, isolated areas of impacted soil can be expected to be encountered during future site activities that may require additional investigation and/or remediation. These areas, if discovered, can be addressed during site development. If suspect environmental conditions, are encountered during future site activities, an environmental professional should be contacted for oversight and remediation recommendations.

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

4

2 INTRODUCTION

PSI conducted a Phase II ESA at the former Christie Cut Stone property located at 2029 Elzey Avenue in Memphis, Shelby County, Tennessee. This report documents the user objectives, the scope of work and sampling rationale, field and laboratory methodologies, an evaluation of data, and conclusions.

2.1 OVERVIEW OF ASTM E1903-11 STANDARD PRACTICE

This Phase II ESA was conducted in general accordance with ASTM Standard E 1903-11, Standard Practice for Environmental Site Assessments: Phase II Environmental Site Assessment Process. This practice covers a process for conducting a Phase II ESA of a parcel of property with respect to evaluating the presence or likely presence of substances defined as “hazardous substances under the Comprehensive Environmental Response Compensation Act (CERCLA or Superfund), and petroleum products. The Standard Practice specifies procedures based on the scientific method to characterize property conditions in an objective, representative, repeatable, and defensible manner. The Standard Practice contemplates that the user (i.e., the client) and the assessor will consult to define the scope and objectives of the investigation in light of relevant factors, such as the portion of the property or specific concerns to be investigated, the specific questions to be answered to satisfy the user’s business needs, the degree of confidence needed or desired in the results, the degree of investigatory sampling needed to achieve such confidence, and any time and resource constraints. The scope of the Phase II ESA investigation is directly related to the user’s objectives. The Standard Practice does not require full site characterization in every instance, but may be used to conduct an investigation that is sufficient to meet the user’s objective.

As stated above, the Standard Practice utilizes the scientific method, which includes defining a problem for which a solution is sought, formulating a hypothesis that might resolve the problem, conducting investigation and collecting data to test the hypothesis, and evaluating the data to confirm or refute the hypothesis. The Standard Practice requires the Phase II assessor to define a hypothesis based on the user’s objectives for each area of investigation (e.g., HYPOTHESIS – A release of petroleum products exceeding regulatory limits has impacted the soil in the vicinity of the petroleum storage tank system). The investigation is designed to test the hypothesis. Once data are collected, the assessor must evaluate whether the hypothesis has been confirmed or refuted and whether the user’s objectives have been met.

2.2 OBJECTIVES

The purpose of performing the Phase II ESA in accordance with the Standard Practice was to acquire and evaluate information sufficient to achieve the objectives outlined below, which were developed through consultation between PSI and the client.

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

5

PSI performed the Phase II ESA at the subject property in conformance with the scope and limitations of the ASTM Standard Practice E1903-11 and for the following objectives:

Assess whether there has been a release of hazardous substances or petroleum products.

Provide information relevant to identifying, defining, and evaluating property conditions associated with target analytes that may pose a risk to human health or the environment, risk of bodily injury to persons on the property, and thereby give rise to potential liability.

The scope of work outlined in Section 4 was developed specifically to satisfy the objectives outlined above. Any areas where the data are insufficient to satisfy the objectives are discussed in the report conclusions.

2.3 DEVIATIONS FROM CONTRACT

PSI completed the work in accordance with the scope of work outlined in the proposal with the following exceptions:

The proposed scope also indicated the collection of two (2) groundwater samples; however, due to subsurface soil conditions, groundwater was not encountered during drilling activities. Therefore, groundwater was not sampled as part of this Phase II ESA.

Page 9: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

6

3 BACKGROUND

3.1 SITE DESCRIPTION AND FEATURES

The subject property is located at 2029 Elzey Avenue in Memphis, Shelby County, Tennessee. The site vicinity is primarily developed with residential, commercial, warehouse, and light industrial/manufacturing properties. Figure 1 is a Site Location Map that illustrates the general location of the subject property. The approximately 2.32-acre subject property is improved with an approximately 3,900-square-foot two-story, office building on the southeast portion. The building, which formerly served as an office for Christie Cut Stone, is currently being used for storage of building materials, furniture, and other miscellaneous items. The remainder of the subject property is a gravel-covered and partially paved lot/laydown yard that is overgrown with vegetation. The storage yard area consists of multiple piles of stone, rock, wood, and other debris left from the former owner/operator.

3.2 PHYSICAL SETTING

PSI reviewed U.S. Geological Survey (USGS) topographic maps, U.S. Department of Agriculture (USDA) soil surveys, Federal Emergency Management Agency (FEMA) flood maps, and other information regarding the physical setting of the subject property to assist with the interpretation of subsurface water movement near the subject property.

Summary

Source Name Year Published/Issued

“Southeast Memphis” Quadrangle, 7.5-Minute Series USGS Topographic Map

1999

FEMA Flood Maps - #47157C0430F 2007

USDA Web Soil Survey – Shelby County, Tennessee 2013

According to its Online Mapping Center, FEMA maps the subject property in Other Areas Zone X, which is defined as "areas determined to be outside the 0.2% annual chance flood plain." According to the USDA Web Soil Survey, soils at the subject property consist of Memphis silt loam, which is a well-drained soil in hydrologic class B with moderate infiltration rates. Field observations were generally consistent with expected soil conditions with silty clay loam observed throughout the depth of the soil borings.

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

7

3.3 SITE HISTORY AND LAND USE

Historically, the subject property appears to have been developed as a small manufactured gas plant for Memphis Power & Light (later Memphis Light, Gas, & Water) from at least 1927 to the 1940’s. Originally, the subject property was improved with the present-day site building on the southeast corner and a ‘gas holder’ tank on the central portion. The site building was most likely originally used in the MGP process. The ‘gas holder’ was a telescopic tank used to store manufactured gas for distribution throughout the area. Later, the site building was reportedly used as a utility substation (rectifying station) for changing alternating current (AC) to direct current (DC) for street cars in the area and by 1964, the ‘gas holder’ tank was no longer depicted on the subject property. After street cars were no longer used in the area, the property became a transformer storage facility through the late 1980’s. By 1990, the subject property had been purchased for use as Christie Cut Stone, which operated a storage yard and mill facility for various types of stone, rock, and concrete. Christie Cut Stone also used the site building on the southeast portion of the property as an office. Christie Cut Stone operated at the subject property through circa 2007, when they closed and moved to a new facility. From circa 2008 to present, the subject property has been a vacant gravel-covered and partially paved property that is overgrown with vegetation and has scattered piles of stone, rock, wood, and other miscellaneous debris.

3.4 CURRENT AND HISTORIC ADJACENT LAND USE

The site vicinity is primarily developed with residential, commercial, warehouse, and light industrial/manufacturing properties. The subject property is bordered on the north by Graham’s Lighting Fixtures warehouse at 2020 York Avenue; on the east by Memphis Metal Manufacturing Company at 795 Tanglewood Street, the dead end of Elzey Avenue, and residential properties; and on the south and west by multiple residential properties. Historically, the adjoining and surrounding area properties were primarily developed as residential with scattered warehouse and light industrial/manufacturing properties from at least 1927 to the mid-1960’s. By the mid-1960’s, additional warehouse and light manufacturing operations had been developed. The site vicinity remains as mix of residential, warehouse, and light manufacturing properties, which is much as it appeared during the 2014 site visit.

3.5 SUMMARY OF PREVIOUS ASSESSMENTS

The Phase II ESA was performed based on information provided in a Phase I ESA conducted by PSI and dated June 26, 2014. The Phase I ESA identified one REC in connection with the subject property’s historical development as a manufactured gas plant.

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

8

4 SCOPE OF WORK AND SAMPLING RATIONALE

The scope of work and sampling rationale described below was intended to satisfy the data needs to meet the client’s objectives for the Phase II ESA, which are described in Section 2 of this report.

4.1 SITE CONCEPTUAL MODEL AND HYPOTHESIS STATEMENT(S)

PSI has prepared a site conceptual model for each area that is to be investigated where target analytes are likely to be present. The conceptual model was developed in order to evaluate what target analytes are most likely to be present and where the target analytes are likely to be currently located, in light of the environmental behavior, fate and transport characteristics of the potential target analytes. The conceptual model was based upon available information and assumptions regarding physical conditions, such as relative permeability, depth to the water table, and groundwater flow direction, as well as available information regarding the nature and physical properties of the target analytes. The conceptual model also takes into account potential release mechanisms and preferential pathways for contaminant travel at each area of concern. The conceptual model was utilized to determine the sampling rationale, including most appropriate sampling locations and media to be sampled, sampling methodologies, and target analytes.

4.1.1 AREA OF CONCERN #1 – FORMER ON-SITE MANUFACTURED GAS PLANT

Target Analyte(s) Release Mechanism Media and Locations Most Likely To Be Impacted

Coal Tar Derivatives, Metals, VOCs/SVOCs, PCBs, and Other Hydrocarbons

Former on-site production of manufactured gas

Soils at the subject property as well as localized/regional groundwater

The Standard Practice requires the assessor to develop a hypothesis based on the user’s objectives for each area of concern. The following hypothesis was developed for Area of Concern #1, which was tested during the Phase II ESA:

Hypothesis: Coal tar derivatives and other hydrocarbons from the historical on-site manufactured gas plant that have impacted subsurface soils and groundwater beneath the subject property at concentrations exceeding the applicable regulatory action criteria.

4.2 FIELD INVESTIGATION SUMMARY

Field investigation and sampling activities were conducted on September 17 and 18, 2014, under the field supervision of Ricky Reynolds, Environmental Services Project Manager for PSI. The Phase II ESA was conducted under the direction of a qualified professional who meets the requirements of a “Phase II Assessor” under the ASTM Standard Practice E1527.

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

9

Prior to the commencement of assessment activities, Tennessee One-Call Systems, Inc., a utility locating service, was contacted to locate all utilities on the subject property or entering the subject property from adjacent properties. Drilling of ten (10) soil borings was performed by Professional Service Industries, Inc. and McCray Drilling Services in accordance with USEPA Standard protocols. Upon completion of the investigation, all soil borings were abandoned by filling the boreholes with native material and bentonite-enriched grout in accordance with local requirements. Locations of the soil borings are shown on Figure 3.

Field screening was conducted during the investigation by monitoring organic vapors in the soil samples using a photoionization detector (PID). Soil samples were collected at 4-foot intervals to the termination depth of the boring. Samples were placed in Ziploc® bags and retained on ice for preservation during field activities. Based on field observations, samples were selected, packed in laboratory provided jars, and placed on ice for transport to an approved laboratory for analysis. If obvious field variables were not identified at a boring location, then the soil sample was collected form the termination depth interval for that boring. Soil samples collected for analysis were submitted to Environmental Testing and Consulting, Inc. under chain of custody by hand delivery. A summary of laboratory soil data is included in Table 1 and a complete copy of the laboratory analytical report is provided in Appendix B.

4.3 SAMPLING RATIONALE AND METHODOLOGY

Based on the conceptual model for Area of Concern #1 described above, PSI conducted the following investigation to determine whether a release had occurred: Media Sampled Location(s) Target Analytes

Soil Ten soil borings were advanced in various areas across the subject property.

VOCs, SVOCs, Metals, Cyanide, Sulfate/Sulfide, PCBs, and pH

Ten (10) soil borings (SB-1 through SB-10) were advanced by direct-push drilling methods at the subject property. Two (2) borings were advanced to an average depth of 65 feet bgs. The remaining eight (8) borings were advanced to an average depth of approximately 24 feet bgs. New acetate liners inside stainless steel rods were used to collect the soil samples from all borings. Soil samples were collected from each boring for laboratory analysis based on field observations.

4.4 INVESTIGATION DERIVED WASTES

Investigation derived wastes were limited due to the sampling methodology and were returned to the boreholes along with bentonite-enriched grout.

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

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5 DATA ANALYSIS & INTERPRETATION

The results of the field investigation and laboratory analyses of soil samples collected are presented in Table 1. The full laboratory report is provided in Appendix B. Where appropriate, the results are compared with regulatory limits for the chemicals and compounds identified in the applicable media.

5.1 REGULATORY GUIDANCE CONCENTRATIONS

Analyte concentrations in all media were compared to applicable or relevant and appropriate requirements. TDEC does not currently publish guidelines for subsurface investigations as related to chemicals of concern other than for UST closures. Instead, each site is evaluated using risk-based calculations and ultimately defaults to the USEPA Regional Screening Levels (RSLs) for comparison values. Therefore, PSI compared the constituents of concern to the USEPA RSLs published in November 2012. The RSL table is a guidance document to be used when determining the need for further investigation at a site.

5.2 SITE HYDROGEOLOGICAL CHARACTERISTICS

The subsurface conditions were derived from on-site observations of soil samples and cuttings collected only from the locations where borings were installed. The soil stratigraphy at the subject site was generally constant between soil borings.

5.3 DATA VALIDATION

Based on the sample methodology of collecting only soil media, a duplicate sample was not required, and therefore, not collected during the sampling event.

5.4 SUMMARY OF FIELD SCREENING AND ANALYTICAL RESULTS

5.4.1 AREA OF CONCERN #1

Soil borings were advanced at various locations across the subject property to investigate the historical presence of a manufactured gas plant. Soil samples were selected based on field observations. Results of the laboratory analysis for the soil samples indicate various concentrations of acenapthalene; acenapthylene; anthracene; benzo(a)anthracene; benzo(a)pyrene; benzo(b)fluoranthene; benzo(g,h,i)perylene; benzo(k)fluoranthene; carbazole; chrysene; dibenz(a,h)anthracene; dibenzofuran; fluorathene; fluorene; indeno(1,2,3-cd)pyrene; 2-methylnapthalene; naphthalene; phenanthrene; pyrene; sulfate; arsenic; beryllium; cadmium; chromium; copper; lead; mercury; nickel; and zinc above laboratory reporting limits.

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

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Of the detected analytes, all were below the appropriate USEPA screening value with the exception of benzo(a)anthracene; benzo(a)pyrene; benzo(b)fluoranthene; benzo(k)fluoranthene; dibenz(a,h)anthracene; indeno(1,2,3-cd)pyrene; and arsenic. A summary of the soil analytical results is included in Table 1 and the full laboratory analytical report is included in Appendix B. Based on the field observations and sampling results the conceptual model appears validated.

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

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6 CONCLUSIONS AND RECOMMENDATIONS

PSI has performed a Phase II Environmental Site Assessment in general conformance with the scope and limitations of the ASTM Standard E 1903-11 Standard Practice and PSI Proposal for the former Christie Cut Stone property located at 2029 Elzey Avenue in Memphis, Shelby County, Tennessee. Based on an evaluation of our findings, the following conclusions have been developed.

6.1 CONCLUSIONS FOR AREA OF CONCERN #1

Hypothesis Statement Was the Hypothesis Confirmed?

Coal tar derivatives and other hydrocarbons from the historical on-site manufactured gas plant that have impacted subsurface soils and groundwater beneath the subject property at concentrations exceeding the applicable regulatory action criteria.

Yes. But only for the soil; groundwater was not encountered.

Laboratory analysis for the collected soil samples indicated various concentrations of acenapthalene; acenapthylene; anthracene; benzo(a)anthracene; benzo(a)pyrene; benzo(b)fluoranthene; benzo(g,h,i)perylene; benzo(k)fluoranthene; carbazole; chrysene; dibenz(a,h)anthracene; dibenzofuran; fluorathene; fluorene; indeno(1,2,3-cd)pyrene; 2-methylnapthalene; naphthalene; phenanthrene; pyrene; sulfate; arsenic; beryllium; cadmium; chromium; copper; lead; mercury; nickel; and zinc above laboratory reporting limits. Of the detected analytes, all were below the appropriate USEPA screening value with the exception of benzo(a)anthracene; benzo(a)pyrene; benzo(b)fluoranthene; benzo(k)fluoranthene; dibenz(a,h)anthracene; indeno(1,2,3-cd)pyrene; and arsenic. Benzo(a)anthracene; benzo(a)pyrene; benzo(b)fluoranthene; benzo(k)fluoranthene; dibenz(a,h)anthracene; indeno(1,2,3-cd)pyrene are SVOCs that contain carbon and hydrogen. These analytes are components, byproducts, or waste products resulting from the production process of manufacturing gas, which typically involved heating coal or oil to generate gas. Laboratory analyses for these constituents, which exceeded the appropriate screening levels, were identified at the following concentrations:

Benzo(a)anthracene at 1.97 mg/kg in SB-7 (8-12’) and 4.7 mg/kg in SB-8 (0-4’), which is above the USEPA RSL of 0.15 mg/kg

Benzo(a)pyrene at 2.36 mg/kg in SB-7 (8-12’) and 4.59 mg/kg in SB-8 (0-4’), which is above the USEPA RSL of 0.015 mg/kg

Benzo(b)fluoranthene at 1.82 mg/kg in SB-7 (8-12’) and 4.79 mg/kg in SB-8 (0-4’), which is above the USEPA RSL of 0.015 mg/kg

Benzo(k)fluoranthene at 2.43 mg/kg in SB-8 (0-4’), which is above the USEPA RSL of 1.5 mg/kg

Dibenz(a,h)anthracene at 0.257 mg/kg in SB-7 (8-12’) and 0.656 mg/kg in SB-8 (0-4’), which is above the USEPA RSL of 0.015 mg/kg

Indeno(1,2,3-cd)pyrene at 1.14 mg/kg in SB-7 (8-12’) and 2.48 mg/kg in SB-8 (0-4’), which is above the USEPA RSL of 0.015 mg/kg

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

13

The detected arsenic levels ranged from 1.62 mg/kg to 8.62 mg/kg, which are above the USEPA RSL of 0.39 mg/kg. However, arsenic is a natural occurring metal at high levels in the soils of this region and the concentrations of arsenic identified in the soil samples are below the accepted background level of 10 mg/kg for arsenic in the Mid-South. Therefore, no further investigation of arsenic in soil appears warranted at this time. This Phase II ESA has provided sufficient information to conclude that isolated subsurface soils at the subject property have been adversely impacted by components, byproducts, and/or waste products that would have been used or generated from the former manufactured gas plant that historically operated at the property. However, the areas appear relatively shallow and site-wide or broad scale soil contamination is not expected. In addition, groundwater was not encountered and it not expected to be impacted by the former site operations.

6.2 RECOMMENDATIONS

Based on the isolated nature of the detected constituents in the subsurface soil at the subject property, an additional site-wide assessment to better delineate the extent of subsurface impacts is not warranted at this time. However, isolated areas of impacted soil can be expected to be encountered during future site activities that may require additional investigation and/or remediation. These areas, if discovered, can be addressed during site development. If suspect environmental conditions, are encountered during future site activities, an environmental professional should be contacted for oversight and remediation recommendations.

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

14

7 WARRANTY

7.1 WARRANTY

PSI warrants that the findings and conclusions reported herein were conducted in general accordance with ASTM E 1903-11 Standard Practice. These methodologies are described by the Standard Practice as representing good commercial and customary practice for conducting a Phase II ESA of a parcel of property for the purpose of evaluating recognized environmental conditions. However, these findings and conclusions contain all of the limitations inherent in these methodologies which are referred to in the Standard Practice and some of which are more specifically set forth below. The conclusions presented in the report are based solely on the services described herein and not on scientific tasks or procedures beyond the scope of agreed upon services. The Phase II ESA has been developed to provide the client with information regarding apparent indications of recognized environmental conditions relating to the subject property. It is necessarily limited to the conditions observed and to the information available at the time of the work. The assessment and conclusions presented herein were based upon the subjective evaluation of limited data. They may not represent all conditions at the subject site as they reflect the information gathered from specific locations. PSI warrants that the findings and conclusions contained herein have been promulgated in accordance with generally accepted environmental investigation methodology and only for the site described in this report. The findings set forth in this report are strictly limited to the date of the evaluation. The scope of the Phase II ESA was developed specifically to meet the client’s stated objectives and the data that was developed may not be suitable for use to satisfy other objectives. Any limitations on the data to meet the client’s stated objectives are described in the report.

Due to the limited nature of the work, there is a possibility that there may exist conditions which could not be identified within the scope of the assessment or which were not apparent at the time of report preparation. It is also possible that the testing methods employed at the time of the report may later be superseded by other methods. The description, type, and composition of what are commonly referred to as "hazardous materials or conditions" can also change over time. PSI does not accept responsibility for changes in the state of the art, nor for changes in the scope of various lists of hazardous materials or conditions. PSI believes that the findings and conclusions provided in this report are reasonable. However, no other warranties are implied or expressed. The Phase II ESA did not include a quantitative human health risk assessment.

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

15

The findings of this investigation are partially based on data provided by others. PSI cannot guarantee the accuracy of data provided by others. No warranty is expressed or implied with the usage of such data. Analytical data contained in this report is limited to the corresponding sampling location, depth, sampled material, selected range of analyses and laboratory reporting limits. Additional chemical constituents not searched for during the current study, may be present in soil, soil gas, and/or groundwater at the site. The location and concentration of contaminants can vary over time due to seasonal water table fluctuations, past disposal practices, the passage of time, and other factors. The Phase II ESA is intended to develop and present sound, scientifically valid data concerning actual site conditions. It is not the role of the Phase II Assessor to provide legal or business advice.

7.2 USE BY THIRD PARTIES

This report was prepared pursuant to the contract PSI has with Triple Z Development, Inc. and K3C2 Investments, LLC. That contractual relationship included an exchange of information about the subject site that was unique and between PSI and its client and serves as the basis upon which this report was prepared. Because of the importance of the communication between PSI and its client, reliance or any use of this report by anyone other than Triple Z Development, Inc. and K3C2 Investments, LLC, for whom it was prepared, is prohibited and therefore not foreseeable to PSI. Reliance or use by any such third party without explicit authorization in the report does not make said third party a third party beneficiary to PSI’s contract with Triple Z Development, Inc. and K3C2 Investments, LLC. Any such unauthorized reliance on or use of this report, including any of its information or conclusions, will be at third party’s risk. For the same reasons, no warranties or representations, expressed or implied in this report, are made to any such third party. Third party reliance letters may be issued on request and payment of the, then current fee for such letters. All third parties relying on PSI’s reports, by such reliance, agree to be bound by the proposal and PSI’s General Conditions. No reliance by any party is permitted without such agreement, regardless of the content of the reliance letter itself.

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Phase II ESA October 30, 2014

Former Christie Cut Stone – Memphis, TN

PSI Project #05021106

16

8 REFERENCES

ASTM E 1527-05 Standard Practice for Environmental Site Assessments: Phase I Environmental Site Assessment Process

ASTM E 1903-11 Standard Practice for Environmental Site Assessments: Phase II

Environmental Site Assessment Process Professional Service Industries, Inc., Phase I ESA Report, Former Christie Cut Stone,

2029 Elzey Avenue, Memphis, Tennessee, June 26, 2014 USEPA SW-846 - Recommended Analytical Procedures, Test Methods for Evaluating

Solid Waste-Physical/Chemical Methods USEPA Regional Screening Levels (RSLs) Summary Table – November 2012

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FIGURES

Page 21: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

FIGURE 1

SITE LOCATION MAP

Former Christie Cut Stone 2029 Elzey Avenue

Memphis, Tennessee

PSI PROJECT # 05021106

Subject Property

Page 22: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

FIGURE 2

SITE SKETCH

Former Christie Cut Stone 2029 Elzey Avenue

Memphis, Tennessee

PSI PROJECT # 05021106

Page 23: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

FIGURE 3

BORING LOCATION SKETCH

Former Christie Cut Stone 2029 Elzey Avenue

Memphis, Tennessee

PSI PROJECT # 05021106

Page 24: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

TABLE

Page 25: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

Analyte

USEPA

Remediation  

Screening Levels

(Residential)

SB-1

(60-65')

SB-2

(60-65')

SB-3

(8-12')

SB-4

(12-16')

SB-5

(20-24')

SB-6

(20-24')

SB-7

(8-12')

SB-8

(0-4')

SB-8

(20-24')

SB-9

(20-24')

SB-10

(12-16')

pH NV 6.0 5.6 6.9 6.9 5.9 5.2 7.2 7.1 6.8 6.3 6.5

mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Cyanide NV <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00

Sulfide NV <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10

Sulfate NV <10 20.1 57.5 65.2 11.1 15 73 12.1 14 29.8 <10

VOCs mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Acetone 61,000 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400

Acetonitrile 870 <0.100 <0.100 <0.100 <0.100 <0.100 <0.100 <0.100 <0.100 <0.100 <0.100 <0.100

Acrolein 0.15 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400

Acrylonitrile 0.24 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400

Benzene 1.10 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Bromobenzene 300 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Bromochloromethane 160 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Bromodichloromethane 0.27 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Bromoform 61 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Bromomethane 7.3 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

2-Butanone (MEK) 28,000 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400

n-Butylbenzene 3,900 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

sec-Butyl Benzene NV <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

tert-Butyl Benzene NV <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Carbon Disulfide 820 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Carbon Tetrachloride 0.61 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Chlorobenzene 290 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Chlorodibromomethane 0.68 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Chloroethane (Ethyl Chloride) 15,000 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

2-Chloroethylvinyl Ether NV <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Chloroform 0.29 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Chloromethane 120 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

2-Chlorotoluene 1,600 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

4-Chlorotoluene 1,600 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,2-Dibromo-3-chloropropane 0.0054 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100

1,2-Dibromoethane (EDB) 0.034 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Dibromomethane (Methylene Bromide) 25 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Dichlorodifluoromethane 94 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,2-Dichlorobenzene 1,900 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,3-Dichlorobenzene 70.4 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,4-Dichlorobenzene 2.4 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,1-Dichloroethane 3.3 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,2-Dichloroethane 0.43 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,1-Dichloroethylene (1,1-DCE) 240 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

cis-1,2-Dichloroethylene 160 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

trans-1,2-Dichloroethylene 150 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,2-Dichloroethene (Total) 700 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,2-Dichloropropane 0.94 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,3-Dichloropropane 1,600 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

2,2-Dichloropropane NV <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,1-Dichloropropene NV <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

cis-1,3-Dichloropropene 1.7 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

trans-1,3-Dichloropropene 1.7 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Ethyl Acetate 70,000 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400

Ethylbenzene 5.4 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Hexachlorobutadiene 6.2 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

2-Hexanone 210 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Iodomethane (Methyl Iodide) NV <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Isopropylbenzene (Cumene) 2,100 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

4-Isopropyl Toluene NV <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Methyl Tert-Butyl Ether (MTBE) 43 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

4-Methyl-2-Pentanone 5,300 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Methylene Chloride 56 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Naphthalene 3.6 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100

n-Propyl Benzene 3,400 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Styrene 6,300 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,1,1,2-Tetrachloroethane 1.9 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,1,2,2-Tetrachloroethane 0.56 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Tetrachloroethene (PERC) 2.2 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Toluene 5,000 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100 <0.0100

1,2,3-Trichlorobenzene 49 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,2,4-Trichlorobenzene 22 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,1,1-Trichloroethane 8,700 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,1,2-Trichloroethane 1.1 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Trichloroethene (TCE) 0.91 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

Trichlorofluoromethane 790 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,2,3-Trichloropropane 0.005 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,2,4-Trimethylbenzene 62 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

1,3,5-Trimethylbenzene 780 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

mg/kg - millograms per kilogram

NV - No Value listed in USEPA RSL table

Chemical identified above laboratory reporting limit, but below the USEPA Screening Value

Concentration exceeds the USEPA Screening Value for the Chemical of Concern.

Table 1

Soil Analylitcal Data Summary

Elzey Avenue Property

2029 Elzey Avenue

Memphis, Tennessee

Page 26: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

Analyte

USEPA

Remediation  

Screening Levels

(Residential)

SB-1

(60-65')

SB-2

(60-65')

SB-3

(8-12')

SB-4

(12-16')

SB-5

(20-24')

SB-6

(20-24')

SB-7

(8-12')

SB-8

(0-4')

SB-8

(20-24')

SB-9

(20-24')

SB-10

(12-16')

VOCs mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Vinyl Acetate 970 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400 <0.0400

Vinyl Chloride 0.06 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

o-Xylene 690 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

m,p-Xylene 600 <0.0040 <0.0040 <0.0040 <0.0040 <0.0040 <0.0040 <0.0040 <0.0040 <0.0040 <0.0040 <0.0040

Xylenes (Total) 630 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020

SVOCs mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Acenaphthene 3,400 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 0.243 0.543 <0.066 <0.066 <0.066

Acenaphthylene 4,690 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 0.607 0.805 <0.066 <0.066 <0.066

Acetophenone 7,800 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Aniline 85 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Anthracene 17,000 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 0.286 0.961 <0.066 <0.066 <0.066

Benzidine 0.0005 <0.670 <0.670 <0.670 <0.670 <0.670 <0.670 <0.670 <0.670 <0.670 <0.670 <0.670

Benzo(a)anthracene 0.15 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 1.97 4.7 <0.066 <0.066 <0.066

Benzo(a)pyrene 0.015 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 2.36 4.59 <0.066 <0.066 <0.066

Benzo(b)fluoranthene 0.15 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 1.82 4.79 <0.066 <0.066 <0.066

Benzo(g,h,i)perylene 2,350 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 1.21 2.83 <0.066 <0.066 <0.066

Benzo(k)fluoranthene 1.5 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 0.862 2.43 <0.066 <0.066 <0.066

Benzoic Acid 240,000 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330

Benzyl Alcohol 6,100 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330

Bis(2-Chloroethoxy)methane 180 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Bis(2-Chloroethyl)ether 0.21 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Bis(2-Chloroisopropyl)ether NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Bis(2-ethylhexyl)phthalate NV <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330

4-Bromophenyl Phenyl Ether NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Butyl Benzyl Phthalate 260 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Carbazole NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 0.51 <0.170 <0.170 <0.170

4-Chloro-3-Methylphenol NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

4-Chloroaniline NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

2-Chloronaphthalene NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

2-Chlorophenol NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

4-Chlorophenyl Phenyl Ether NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Chrysene 15 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 2.04 4.92 <0.066 <0.066 <0.066

Dibenz(a,h)anthracene 0.015 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 0.257 0.656 <0.066 <0.066 <0.066

Dibenzofuran NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 0.28 <0.170 <0.170 <0.170

1,2-Dichlorobenzene 1,900 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

1,3-Dichlorobenzene NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

1,4-Dichlorobenzene 2.4 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

3,3-Dichlorobenzidine 1.1 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330

2,4-Dichlorophenol 180 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

2,6-Dichlorophenol NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Diethyl Phthalate 49,000 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Dimethyl Phthalate NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

3,3-Dimethylbenzidine 35 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330

2,4-Dimethylphenol 1,200 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Di-n-butyl Phthalate NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

4,6-Dinitro-2-Methylphenol NV <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330

2,4-Dinitrophenol 120 <1.67 <1.67 <1.67 <1.67 <1.67 <1.67 <1.67 <1.67 <1.67 <1.67 <1.67

2,4-Dinitrotoluene 1.6 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

2,6-Dinitrotoluene 61 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Di-n-octyl Phthalate NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Fluoranthene 2,300 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 3.01 5.46 <0.066 <0.066 <0.066

Fluorene 2,300 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 0.250 0.422 <0.066 <0.066 <0.066

Hexachlorobenzene 0.3 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Hexachlorobutadiene 6.2 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Hexachlorocyclopentadiene 370 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Hexachloroethane 12 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Indeno(1,2,3-cd)pyrene 0.15 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 1.14 2.48 <0.066 <0.066 <0.066

Isophorone 510 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

2-Methylnaphthalene 310 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 0.311 0.42 <0.066 <0.066 <0.066

2-Methylphenol NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

3&4 Methylphenol NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Naphthalene 3.9 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 0.845 0.984 <0.066 <0.066 <0.066

2-Nitroaniline 610 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

3-Nitroaniline NV <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330

4-Nitroaniline 24 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Nitrobenzene 4.8 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

2-Nitrophenol NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

4-Nitrophenol NV <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

N-Nitrosodimethylamine 0.0023 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

N-Nitrosodiphenylamine 99 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330

N-Nitrosodiethylamine 0.00077 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

N-Nitroso-di-n-butylamine 0.087 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

N-Nitroso-di-n-propylamine 0.069 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

mg/kg - millograms per kilogram

NV - No Value listed in USEPA RSL table

Chemical identified above laboratory reporting limit, but below the USEPA Screening Value

Concentration exceeds the USEPA Screening Value for the Chemical of Concern.

Table 1

Soil Analylitcal Data Summary

Elzey Avenue Property

2029 Elzey Avenue

Memphis, Tennessee

Page 27: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

Analyte

USEPA

Remediation  

Screening Levels

(Residential)

SB-1

(60-65')

SB-2

(60-65')

SB-3

(8-12')

SB-4

(12-16')

SB-5

(20-24')

SB-6

(20-24')

SB-7

(8-12')

SB-8

(0-4')

SB-8

(20-24')

SB-9

(20-24')

SB-10

(12-16')

SVOCs mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Pentachlorophenol 0.89 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330

Phenanthrene 2,350 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 0.746 <0.066 3.7 <0.066 <0.066

Phenol 18,000 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Pyrene 1,700 <0.066 <0.066 <0.066 <0.066 <0.066 <0.066 5.85 <0.066 8.09 <0.066 <0.066

Pyridine 1,500 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330 <0.330

1,2,4,5-Tetrachlorobenzene 18 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

2,3,4,6-Tetrachlorophenol 1,800 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

1,2,4-Trichlorobenzene 22 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

2,4,5-Trichlorophenol 6,100 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

2,4,6-Trichlorophenol 44 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170

Metals mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Antimony 31 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.250 <0.500 <0.500 <0.500 <0.500

Arsenic 0.39 1.62 6.42 7.33 3.95 4.06 5.17 8.62 5.87 6.65 4.24 6.81

Beryllium 2,000 0.156 0.807 0.376 0.478 0.416 0.440 <0.250 0.411 0.303 0.385 0.314

Cadmium 70 <0.100 <0.100 0.121 <0.100 <0.100 <0.100 <0.500 0.263 0.144 <0.100 0.133

Chromium 180,000 5.92 16.7 8.80 11.3 11.7 10.6 10.2 7.64 7.52 9.59 7.94

Copper 3,100 1.16 4.85 12.1 9.02 8.85 9.98 17.2 34.3 11.0 8.56 11.7

Lead 400 0.721 3.22 7.87 25.9 5.73 7.11 11.5 49.1 46.1 6.49 6.55

Mercury 10 <0.0133 <0.0133 0.0157 0.0209 0.0190 0.0203 0.0319 0.100 <0.0133 0.0163 0.0237

Nickel 3,800 1.79 4.06 12.1 9.28 9.10 10.8 15.1 11.1 11.3 10 11.5

Selenium 390 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00

Silver 390 <0.250 <0.250 <0.250 <0.250 <0.250 <0.250 <1.25 <0.250 <0.250 <0.250 <0.250

Thallium 0.55 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00

Zinc 23,000 5.57 16.5 39.7 27.2 24 30.9 48.8 50.8 32 25.3 32.6

mg/kg - millograms per kilogram

NV - No Value listed in USEPA RSL table

Chemical identified above laboratory reporting limit, but below the USEPA Screening Value

Concentration exceeds the USEPA Screening Value for the Chemical of Concern.

Elzey Avenue Property

2029 Elzey Avenue

Table 1

Soil Analylitcal Data Summary

Memphis, Tennessee

Page 28: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

APPENDIX A – LABORATORY DATA REPORT

Page 29: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

 

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Alabama  #40750      Louisiana      #04015    VA NELAP  #460181    Texas          #T104704180‐11‐6  Arkansas  #88‐0650 Mississippi   California      #2904    NC  #415                           Oklahoma          #9311                             Virginia  #00106 Kentucky  #90047  Tennessee     #TN02027  EPA             #TN00012                 Kentucky UST   #41                        Kansas  #E‐10396 

 

9/26/2014 PSI Mr. Ricky Reynolds 4161 Ridgemoor Ave Memphis, TN, 38118 Ref: Analytical Testing

ETC Report Number: 14-262-0305 Client Project Description: 2029 Elzey Avenue Memphis, TN Project No. 05021106 Project Number: 2029 Elzey Avenue

Dear Mr. Ricky Reynolds: Environmental Testing and Consulting, Inc. received sample(s) on 9/19/2014 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '~' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Per EPA Methods Update Rule (May 2012), all methods from Standard Methods for the Examination of Water and Wastewater are reported to include the year of approval. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,

Andy Parrish Project Manager

Page 1 of 119

Page 30: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

  Client: PSI CASE NARRATIVE Project: 2029 Elzey Avenue Lab Report Number: 14-262-0305 Date: 9/26/2014 Poly chlorinated Biphenyls (PCB's) Method SW-8082 Sample 95409 (SB-8 (0-4')) QC Batch No: L213328 Surrogate(s) was flagged for recovery outside QC limits in this project sample. This sample was re-analyzed for verification, and/or dilution of target analytes. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits. Volatile Organic Compounds - GC/MS Method SW-8260B Several project samples are flagged as follows: Analyte: 2-Chloroethyl vinyl ether QC Batch No: L212859

This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged 'M' to indicate that results should be considered estimated concentration due to the potential for a low bias.

Page 2 of 119

Page 31: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-1 (60-65')

95402 Matrix:

9/17/2014 11:30

Solids

Test Results Units MQL By AnalyticalMethod

Date / TimeAnalyzed

DF

<1.00 mg/Kg 1.00Cyanide, Total 1 09/25/14 11:15 SW-9014EWB

6.0 s.u.pH 1 09/24/14 13:45 9045CSNS

<10.0 mg/Kg 10.0Sulfide 1 09/23/14 10:35 4500S2F-2011KM2

<0.500 mg/Kg 0.500Total Antimony 1 09/22/14 21:55 6010BBKN

1.62 mg/Kg 1.00Total Arsenic 1 09/22/14 21:55 6010BBKN

0.156 mg/Kg 0.0500Total Beryllium 1 09/22/14 21:55 6010BBKN

<0.100 mg/Kg 0.100Total Cadmium 1 09/22/14 21:55 6010BBKN

5.92 mg/Kg 0.250Total Chromium 1 09/22/14 21:55 6010BBKN

1.16 mg/Kg 0.250Total Copper 1 09/22/14 21:55 6010BBKN

0.721 mg/Kg 0.300Total Lead 1 09/22/14 21:55 6010BBKN

<0.0133 mg/Kg 0.0133Mercury (Total) 1 09/22/14 13:11 7471AJRS

1.79 mg/Kg 0.250Total Nickel 1 09/23/14 18:12 6010BBKN

<1.00 mg/Kg 1.00Total Selenium 1 09/22/14 21:55 6010BBKN

<0.250 mg/Kg 0.250Total Silver 1 09/22/14 21:55 6010BBKN

<1.00 mg/Kg 1.00Total Thallium 1 09/22/14 21:55 6010BBKN

5.57 mg/Kg 0.500Total Zinc 1 09/22/14 21:55 6010BBKN

<10.0 mg/Kg 10.0Sulfate 1 09/23/14 19:08 9056CGC

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Method Quantitation LimitMQLMinimum valueM

Page 3 of 119

Page 32: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-1 (60-65')

95402 Matrix:

9/17/2014 11:30

Solids

Analytical Method: 8082

Prep Method: 3546 Date/Time Prepped: 9/25/2014 09:00:00Prep Batch(es): L213208

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0066 mg/Kg 0.0066Aroclor 1016 1 09/25/14 22:43 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1221 1 09/25/14 22:43 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1232 1 09/25/14 22:43 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1242 1 09/25/14 22:43 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1248 1 09/25/14 22:43 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1254 1 09/25/14 22:43 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1260 1 09/25/14 22:43 L213328VIC

Surrogate: Decachlorobiphenyl 60.3 Limits: 25-125% 09/25/14 22:431 VIC L213328

Surrogate: Tetrachloro-m-xylene 51.8 Limits: 25-125% 09/25/14 22:431 VIC L213328

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0400 mg/Kg 0.0400Acetone 1 09/22/14 14:14 L212859SEB

<0.100 mg/Kg 0.100Acetonitrile 1 09/22/14 14:14 L212859SEB

<0.0400 mg/Kg 0.0400Acrolein 1 09/22/14 14:14 L212859SEB

<0.0400 mg/Kg 0.0400Acrylonitrile 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Benzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Bromobenzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Bromochloromethane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Bromodichloromethane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Bromoform 1 09/22/14 14:14 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 4 of 119

Page 33: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-1 (60-65')

95402 Matrix:

9/17/2014 11:30

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Bromomethane 1 09/22/14 14:14 L212859SEB

<0.0400 mg/Kg 0.0400Methyl Ethyl Ketone (MEK) 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020n-Butylbenzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020sec-Butyl benzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020tert-Butyl benzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Disulfide 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Tetrachloride 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Chlorobenzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Chlorodibromomethane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Chloroethane 1 09/22/14 14:14 L212859SEB

<0.0020 M mg/Kg 0.00202-Chloroethylvinyl Ether 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Chloroform 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Chloromethane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00202-Chlorotoluene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00204-Chlorotoluene 1 09/22/14 14:14 L212859SEB

<0.0100 mg/Kg 0.01001,2-Dibromo-3-Chloropropane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dibromoethane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Dibromomethane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichlorobenzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichlorobenzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,4-Dichlorobenzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Dichlorodifluoromethane 1 09/22/14 14:14 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 5 of 119

Page 34: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-1 (60-65')

95402 Matrix:

9/17/2014 11:30

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.00201,1-Dichloroethane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloroethene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,2-Dichloroethene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,2-Dichloroethene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethene (Total) 1 09/22/14 14:14 L212859

<0.0020 mg/Kg 0.00201,2-Dichloropropane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichloropropane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00202,2-Dichloropropane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloropropene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,3-Dichloropropene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,3-Dichloropropene 1 09/22/14 14:14 L212859SEB

<0.0400 mg/Kg 0.0400Ethyl Acetate 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Ethylbenzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Hexachlorobutadiene 1 09/22/14 14:14 L212859SEB

<0.0100 mg/Kg 0.01002-Hexanone 1 09/22/14 14:14 L212859SEB

<0.0100 mg/Kg 0.0100Iodomethane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Isopropylbenzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00204-Isopropyl toluene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Methyl tert-butyl ether (MTBE) 1 09/22/14 14:14 L212859SEB

<0.0100 mg/Kg 0.01004-Methyl-2-Pentanone 1 09/22/14 14:14 L212859SEB

<0.0100 mg/Kg 0.0100Methylene Chloride 1 09/22/14 14:14 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 6 of 119

Page 35: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-1 (60-65')

95402 Matrix:

9/17/2014 11:30

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0100 mg/Kg 0.0100Naphthalene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020n-Propylbenzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Styrene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,1,1,2-Tetrachloroethane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,1,2,2-Tetrachloroethane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Tetrachloroethene 1 09/22/14 14:14 L212859SEB

<0.0100 mg/Kg 0.0100Toluene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichlorobenzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trichlorobenzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,1,1-Trichloroethane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,1,2-Trichloroethane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Trichloroethene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Trichlorofluoromethane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichloropropane 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trimethylbenzene 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.00201,3,5-Trimethylbenzene 1 09/22/14 14:14 L212859SEB

<0.0400 mg/Kg 0.0400Vinyl Acetate 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020Vinyl Chloride 1 09/22/14 14:14 L212859SEB

<0.0020 mg/Kg 0.0020o-Xylene 1 09/22/14 14:14 L212859SEB

<0.0040 mg/Kg 0.0040m,p-Xylene 1 09/22/14 14:14 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 7 of 119

Page 36: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-1 (60-65')

95402 Matrix:

9/17/2014 11:30

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Xylene (Total) 1 09/22/14 14:14 L212859

Surrogate: 4-Bromofluorobenzene 108 Limits: 60-130% 09/22/14 14:141 SEB L212859

Surrogate: 1,2-Dichloroethane - d4 112 Limits: 60-132% 09/22/14 14:141 SEB L212859

Surrogate: Toluene-d8 95.2 Limits: 70-122% 09/22/14 14:141 SEB L212859

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.066 mg/Kg 0.066Acenaphthene 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Acenaphthylene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Acetophenone 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Aniline 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Anthracene 1 09/22/14 21:35 L213162BMP

<0.670 mg/Kg 0.670Benzidine 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)anthracene 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)pyrene 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Benzo(b)fluoranthene 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Benzo(g,h,i)perylene 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Benzo(k)fluoranthene 1 09/22/14 21:35 L213162BMP

<0.330 mg/Kg 0.330Benzoic Acid 1 09/22/14 21:35 L213162BMP

<0.330 mg/Kg 0.330Benzyl alcohol 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroethoxy)methane 1 09/22/14 21:35 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 8 of 119

Page 37: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-1 (60-65')

95402 Matrix:

9/17/2014 11:30

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.170Bis(2-Chloroethyl)ether 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroisopropyl)ether 1 09/22/14 21:35 L213162BMP

<0.330 mg/Kg 0.330Bis(2-ethylhexyl)phthalate 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1704-Bromophenyl phenyl ether 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Butyl benzyl phthalate 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Carbazole 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1704-Chloro-3-methylphenol 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1704-Chloroaniline 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1702-Chloronaphthalene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1702-Chlorophenol 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1704-Chlorophenyl phenyl ether 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Chrysene 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Dibenz(a,h)anthracene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Dibenzofuran 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1701,2-Dichlorobenzene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1701,3-Dichlorobenzene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1701,4-Dichlorobenzene 1 09/22/14 21:35 L213162BMP

<0.330 mg/Kg 0.3303,3'-Dichlorobenzidine 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1702,4-Dichlorophenol 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1702,6-Dichlorophenol 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Diethyl phthalate 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Dimethyl phthalate 1 09/22/14 21:35 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 9 of 119

Page 38: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-1 (60-65')

95402 Matrix:

9/17/2014 11:30

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.330 mg/Kg 0.3303,3' Dimethylbenzidine 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1702,4-Dimethylphenol 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Di-n-butyl phthalate 1 09/22/14 21:35 L213162BMP

<0.330 mg/Kg 0.3304,6-Dinitro-2-methylphenol 1 09/22/14 21:35 L213162BMP

<1.67 mg/Kg 1.672,4-Dinitrophenol 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1702,4-Dinitrotoluene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1702,6-Dinitrotoluene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Di-n-Octyl Phthalate 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Fluoranthene 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Fluorene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobenzene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobutadiene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Hexachlorocyclopentadiene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Hexachloroethane 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Indeno(1,2,3-cd)pyrene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Isophorone 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.0662-Methylnaphthalene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1702-Methylphenol 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1703&4 Methylphenol 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Naphthalene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1702-Nitroaniline 1 09/22/14 21:35 L213162BMP

<0.330 mg/Kg 0.3303-Nitroaniline 1 09/22/14 21:35 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 10 of 119

Page 39: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-1 (60-65')

95402 Matrix:

9/17/2014 11:30

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1704-Nitroaniline 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Nitrobenzene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1702-Nitrophenol 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1704-Nitrophenol 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodimethylamine 1 09/22/14 21:35 L213162BMP

<0.330 mg/Kg 0.330N-Nitrosodiphenylamine 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodiethylamine 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-butylamine 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-propylamine 1 09/22/14 21:35 L213162BMP

<0.330 mg/Kg 0.330Pentachlorophenol 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Phenanthrene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.170Phenol 1 09/22/14 21:35 L213162BMP

<0.066 mg/Kg 0.066Pyrene 1 09/22/14 21:35 L213162BMP

<0.330 mg/Kg 0.330Pyridine 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1701,2,4,5-Tetrachlorobenzene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1702,3,4,6-Tetrachlorophenol 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1701,2,4-Trichlorobenzene 1 09/22/14 21:35 L213162BMP

<0.170 mg/Kg 0.1702,4,5-Trichlorophenol 1 09/22/14 21:35 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 11 of 119

Page 40: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-1 (60-65')

95402 Matrix:

9/17/2014 11:30

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1702,4,6-Trichlorophenol 1 09/22/14 21:35 L213162BMP

Surrogate: 2-Fluorobiphenyl 67.5 Limits: 33-115% 09/22/14 21:351 BMP L213162

Surrogate: 2-Fluorophenol 68.9 Limits: 10-119% 09/22/14 21:351 BMP L213162

Surrogate: Nitrobenzene-d5 63.0 Limits: 29-110% 09/22/14 21:351 BMP L213162

Surrogate: Phenol-d6 74.1 Limits: 11-125% 09/22/14 21:351 BMP L213162

Surrogate: 4-Terphenyl-d14 82.2 Limits: 33-122% 09/22/14 21:351 BMP L213162

Surrogate: 2,4,6-Tribromophenol 95.2 Limits: 9-134% 09/22/14 21:351 BMP L213162

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 12 of 119

Page 41: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-2 (60-65')

95403 Matrix:

9/17/2014 14:00

Solids

Test Results Units MQL By AnalyticalMethod

Date / TimeAnalyzed

DF

<1.00 mg/Kg 1.00Cyanide, Total 1 09/25/14 11:15 SW-9014EWB

5.6 s.u.pH 1 09/24/14 13:45 9045CSNS

<10.0 mg/Kg 10.0Sulfide 1 09/23/14 10:35 4500S2F-2011KM2

<0.500 mg/Kg 0.500Total Antimony 1 09/22/14 22:07 6010BBKN

6.42 mg/Kg 1.00Total Arsenic 1 09/22/14 22:07 6010BBKN

0.807 mg/Kg 0.0500Total Beryllium 1 09/22/14 22:07 6010BBKN

<0.100 mg/Kg 0.100Total Cadmium 1 09/22/14 22:07 6010BBKN

16.7 mg/Kg 0.250Total Chromium 1 09/22/14 22:07 6010BBKN

4.85 mg/Kg 0.250Total Copper 1 09/22/14 22:07 6010BBKN

3.22 mg/Kg 0.300Total Lead 1 09/22/14 22:07 6010BBKN

<0.0133 mg/Kg 0.0133Mercury (Total) 1 09/22/14 13:18 7471AJRS

4.06 mg/Kg 0.250Total Nickel 1 09/23/14 18:17 6010BBKN

<1.00 mg/Kg 1.00Total Selenium 1 09/22/14 22:07 6010BBKN

<0.250 mg/Kg 0.250Total Silver 1 09/22/14 22:07 6010BBKN

<1.00 mg/Kg 1.00Total Thallium 1 09/22/14 22:07 6010BBKN

16.5 mg/Kg 0.500Total Zinc 1 09/22/14 22:07 6010BBKN

20.1 mg/Kg 10.0Sulfate 1 09/23/14 19:26 9056CGC

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Method Quantitation LimitMQLMinimum valueM

Page 13 of 119

Page 42: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-2 (60-65')

95403 Matrix:

9/17/2014 14:00

Solids

Analytical Method: 8082

Prep Method: 3546 Date/Time Prepped: 9/25/2014 09:00:00Prep Batch(es): L213208

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0066 mg/Kg 0.0066Aroclor 1016 1 09/25/14 23:44 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1221 1 09/25/14 23:44 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1232 1 09/25/14 23:44 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1242 1 09/25/14 23:44 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1248 1 09/25/14 23:44 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1254 1 09/25/14 23:44 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1260 1 09/25/14 23:44 L213328VIC

Surrogate: Decachlorobiphenyl 46.2 Limits: 25-125% 09/25/14 23:441 VIC L213328

Surrogate: Tetrachloro-m-xylene 53.1 Limits: 25-125% 09/25/14 23:441 VIC L213328

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0400 mg/Kg 0.0400Acetone 1 09/22/14 14:55 L212859SEB

<0.100 mg/Kg 0.100Acetonitrile 1 09/22/14 14:55 L212859SEB

<0.0400 mg/Kg 0.0400Acrolein 1 09/22/14 14:55 L212859SEB

<0.0400 mg/Kg 0.0400Acrylonitrile 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Benzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Bromobenzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Bromochloromethane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Bromodichloromethane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Bromoform 1 09/22/14 14:55 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 14 of 119

Page 43: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-2 (60-65')

95403 Matrix:

9/17/2014 14:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Bromomethane 1 09/22/14 14:55 L212859SEB

<0.0400 mg/Kg 0.0400Methyl Ethyl Ketone (MEK) 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020n-Butylbenzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020sec-Butyl benzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020tert-Butyl benzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Disulfide 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Tetrachloride 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Chlorobenzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Chlorodibromomethane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Chloroethane 1 09/22/14 14:55 L212859SEB

<0.0020 M mg/Kg 0.00202-Chloroethylvinyl Ether 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Chloroform 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Chloromethane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00202-Chlorotoluene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00204-Chlorotoluene 1 09/22/14 14:55 L212859SEB

<0.0100 mg/Kg 0.01001,2-Dibromo-3-Chloropropane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dibromoethane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Dibromomethane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichlorobenzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichlorobenzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,4-Dichlorobenzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Dichlorodifluoromethane 1 09/22/14 14:55 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 15 of 119

Page 44: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-2 (60-65')

95403 Matrix:

9/17/2014 14:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.00201,1-Dichloroethane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloroethene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,2-Dichloroethene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,2-Dichloroethene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethene (Total) 1 09/22/14 14:55 L212859

<0.0020 mg/Kg 0.00201,2-Dichloropropane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichloropropane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00202,2-Dichloropropane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloropropene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,3-Dichloropropene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,3-Dichloropropene 1 09/22/14 14:55 L212859SEB

<0.0400 mg/Kg 0.0400Ethyl Acetate 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Ethylbenzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Hexachlorobutadiene 1 09/22/14 14:55 L212859SEB

<0.0100 mg/Kg 0.01002-Hexanone 1 09/22/14 14:55 L212859SEB

<0.0100 mg/Kg 0.0100Iodomethane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Isopropylbenzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00204-Isopropyl toluene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Methyl tert-butyl ether (MTBE) 1 09/22/14 14:55 L212859SEB

<0.0100 mg/Kg 0.01004-Methyl-2-Pentanone 1 09/22/14 14:55 L212859SEB

<0.0100 mg/Kg 0.0100Methylene Chloride 1 09/22/14 14:55 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 16 of 119

Page 45: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-2 (60-65')

95403 Matrix:

9/17/2014 14:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0100 mg/Kg 0.0100Naphthalene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020n-Propylbenzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Styrene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,1,1,2-Tetrachloroethane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,1,2,2-Tetrachloroethane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Tetrachloroethene 1 09/22/14 14:55 L212859SEB

<0.0100 mg/Kg 0.0100Toluene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichlorobenzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trichlorobenzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,1,1-Trichloroethane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,1,2-Trichloroethane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Trichloroethene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Trichlorofluoromethane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichloropropane 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trimethylbenzene 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.00201,3,5-Trimethylbenzene 1 09/22/14 14:55 L212859SEB

<0.0400 mg/Kg 0.0400Vinyl Acetate 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020Vinyl Chloride 1 09/22/14 14:55 L212859SEB

<0.0020 mg/Kg 0.0020o-Xylene 1 09/22/14 14:55 L212859SEB

<0.0040 mg/Kg 0.0040m,p-Xylene 1 09/22/14 14:55 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 17 of 119

Page 46: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-2 (60-65')

95403 Matrix:

9/17/2014 14:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Xylene (Total) 1 09/22/14 14:55 L212859

Surrogate: 4-Bromofluorobenzene 101 Limits: 60-130% 09/22/14 14:551 SEB L212859

Surrogate: 1,2-Dichloroethane - d4 117 Limits: 60-132% 09/22/14 14:551 SEB L212859

Surrogate: Toluene-d8 90.1 Limits: 70-122% 09/22/14 14:551 SEB L212859

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.066 mg/Kg 0.066Acenaphthene 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Acenaphthylene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Acetophenone 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Aniline 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Anthracene 1 09/25/14 12:26 L213162BMP

<0.670 mg/Kg 0.670Benzidine 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)anthracene 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)pyrene 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Benzo(b)fluoranthene 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Benzo(g,h,i)perylene 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Benzo(k)fluoranthene 1 09/25/14 12:26 L213162BMP

<0.330 mg/Kg 0.330Benzoic Acid 1 09/25/14 12:26 L213162BMP

<0.330 mg/Kg 0.330Benzyl alcohol 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroethoxy)methane 1 09/25/14 12:26 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 18 of 119

Page 47: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-2 (60-65')

95403 Matrix:

9/17/2014 14:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.170Bis(2-Chloroethyl)ether 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroisopropyl)ether 1 09/25/14 12:26 L213162BMP

<0.330 mg/Kg 0.330Bis(2-ethylhexyl)phthalate 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1704-Bromophenyl phenyl ether 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Butyl benzyl phthalate 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Carbazole 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1704-Chloro-3-methylphenol 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1704-Chloroaniline 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1702-Chloronaphthalene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1702-Chlorophenol 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1704-Chlorophenyl phenyl ether 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Chrysene 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Dibenz(a,h)anthracene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Dibenzofuran 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1701,2-Dichlorobenzene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1701,3-Dichlorobenzene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1701,4-Dichlorobenzene 1 09/25/14 12:26 L213162BMP

<0.330 mg/Kg 0.3303,3'-Dichlorobenzidine 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1702,4-Dichlorophenol 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1702,6-Dichlorophenol 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Diethyl phthalate 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Dimethyl phthalate 1 09/25/14 12:26 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 19 of 119

Page 48: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-2 (60-65')

95403 Matrix:

9/17/2014 14:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.330 mg/Kg 0.3303,3' Dimethylbenzidine 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1702,4-Dimethylphenol 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Di-n-butyl phthalate 1 09/25/14 12:26 L213162BMP

<0.330 mg/Kg 0.3304,6-Dinitro-2-methylphenol 1 09/25/14 12:26 L213162BMP

<1.67 mg/Kg 1.672,4-Dinitrophenol 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1702,4-Dinitrotoluene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1702,6-Dinitrotoluene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Di-n-Octyl Phthalate 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Fluoranthene 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Fluorene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobenzene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobutadiene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Hexachlorocyclopentadiene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Hexachloroethane 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Indeno(1,2,3-cd)pyrene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Isophorone 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.0662-Methylnaphthalene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1702-Methylphenol 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1703&4 Methylphenol 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Naphthalene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1702-Nitroaniline 1 09/25/14 12:26 L213162BMP

<0.330 mg/Kg 0.3303-Nitroaniline 1 09/25/14 12:26 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 20 of 119

Page 49: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-2 (60-65')

95403 Matrix:

9/17/2014 14:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1704-Nitroaniline 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Nitrobenzene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1702-Nitrophenol 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1704-Nitrophenol 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodimethylamine 1 09/25/14 12:26 L213162BMP

<0.330 mg/Kg 0.330N-Nitrosodiphenylamine 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodiethylamine 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-butylamine 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-propylamine 1 09/25/14 12:26 L213162BMP

<0.330 mg/Kg 0.330Pentachlorophenol 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Phenanthrene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.170Phenol 1 09/25/14 12:26 L213162BMP

<0.066 mg/Kg 0.066Pyrene 1 09/25/14 12:26 L213162BMP

<0.330 mg/Kg 0.330Pyridine 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1701,2,4,5-Tetrachlorobenzene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1702,3,4,6-Tetrachlorophenol 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1701,2,4-Trichlorobenzene 1 09/25/14 12:26 L213162BMP

<0.170 mg/Kg 0.1702,4,5-Trichlorophenol 1 09/25/14 12:26 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 21 of 119

Page 50: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-2 (60-65')

95403 Matrix:

9/17/2014 14:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1702,4,6-Trichlorophenol 1 09/25/14 12:26 L213162BMP

Surrogate: 2-Fluorobiphenyl 62.8 Limits: 33-115% 09/25/14 12:261 BMP L213162

Surrogate: 2-Fluorophenol 58.8 Limits: 10-119% 09/25/14 12:261 BMP L213162

Surrogate: Nitrobenzene-d5 56.4 Limits: 29-110% 09/25/14 12:261 BMP L213162

Surrogate: Phenol-d6 63.5 Limits: 11-125% 09/25/14 12:261 BMP L213162

Surrogate: 4-Terphenyl-d14 76.5 Limits: 33-122% 09/25/14 12:261 BMP L213162

Surrogate: 2,4,6-Tribromophenol 85.5 Limits: 9-134% 09/25/14 12:261 BMP L213162

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 22 of 119

Page 51: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-3 (8-12')

95404 Matrix:

9/18/2014 9:45

Solids

Test Results Units MQL By AnalyticalMethod

Date / TimeAnalyzed

DF

<1.00 mg/Kg 1.00Cyanide, Total 1 09/25/14 11:15 SW-9014EWB

6.9 s.u.pH 1 09/24/14 13:45 9045CSNS

<10.0 mg/Kg 10.0Sulfide 1 09/23/14 10:35 4500S2F-2011KM2

<0.500 mg/Kg 0.500Total Antimony 1 09/22/14 22:11 6010BBKN

7.33 mg/Kg 1.00Total Arsenic 1 09/22/14 22:11 6010BBKN

0.376 mg/Kg 0.0500Total Beryllium 1 09/22/14 22:11 6010BBKN

0.121 mg/Kg 0.100Total Cadmium 1 09/22/14 22:11 6010BBKN

8.80 mg/Kg 0.250Total Chromium 1 09/22/14 22:11 6010BBKN

12.1 mg/Kg 0.250Total Copper 1 09/22/14 22:11 6010BBKN

7.87 mg/Kg 0.300Total Lead 1 09/22/14 22:11 6010BBKN

0.0157 mg/Kg 0.0133Mercury (Total) 1 09/22/14 13:20 7471AJRS

12.1 mg/Kg 0.250Total Nickel 1 09/23/14 18:21 6010BBKN

<1.00 mg/Kg 1.00Total Selenium 1 09/22/14 22:11 6010BBKN

<0.250 mg/Kg 0.250Total Silver 1 09/22/14 22:11 6010BBKN

<1.00 mg/Kg 1.00Total Thallium 1 09/22/14 22:11 6010BBKN

39.7 mg/Kg 0.500Total Zinc 1 09/22/14 22:11 6010BBKN

57.5 mg/Kg 10.0Sulfate 1 09/23/14 19:43 9056CGC

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Method Quantitation LimitMQLMinimum valueM

Page 23 of 119

Page 52: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-3 (8-12')

95404 Matrix:

9/18/2014 9:45

Solids

Analytical Method: 8082

Prep Method: 3546 Date/Time Prepped: 9/25/2014 09:00:00Prep Batch(es): L213208

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0066 mg/Kg 0.0066Aroclor 1016 1 09/26/14 00:04 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1221 1 09/26/14 00:04 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1232 1 09/26/14 00:04 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1242 1 09/26/14 00:04 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1248 1 09/26/14 00:04 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1254 1 09/26/14 00:04 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1260 1 09/26/14 00:04 L213328VIC

Surrogate: Decachlorobiphenyl 55.8 Limits: 25-125% 09/26/14 00:041 VIC L213328

Surrogate: Tetrachloro-m-xylene 37.2 Limits: 25-125% 09/26/14 00:041 VIC L213328

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0400 mg/Kg 0.0400Acetone 1 09/22/14 15:36 L212859SEB

<0.100 mg/Kg 0.100Acetonitrile 1 09/22/14 15:36 L212859SEB

<0.0400 mg/Kg 0.0400Acrolein 1 09/22/14 15:36 L212859SEB

<0.0400 mg/Kg 0.0400Acrylonitrile 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Benzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Bromobenzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Bromochloromethane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Bromodichloromethane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Bromoform 1 09/22/14 15:36 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 24 of 119

Page 53: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-3 (8-12')

95404 Matrix:

9/18/2014 9:45

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Bromomethane 1 09/22/14 15:36 L212859SEB

<0.0400 mg/Kg 0.0400Methyl Ethyl Ketone (MEK) 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020n-Butylbenzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020sec-Butyl benzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020tert-Butyl benzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Disulfide 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Tetrachloride 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Chlorobenzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Chlorodibromomethane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Chloroethane 1 09/22/14 15:36 L212859SEB

<0.0020 M mg/Kg 0.00202-Chloroethylvinyl Ether 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Chloroform 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Chloromethane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00202-Chlorotoluene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00204-Chlorotoluene 1 09/22/14 15:36 L212859SEB

<0.0100 mg/Kg 0.01001,2-Dibromo-3-Chloropropane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dibromoethane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Dibromomethane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichlorobenzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichlorobenzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,4-Dichlorobenzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Dichlorodifluoromethane 1 09/22/14 15:36 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 25 of 119

Page 54: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-3 (8-12')

95404 Matrix:

9/18/2014 9:45

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.00201,1-Dichloroethane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloroethene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,2-Dichloroethene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,2-Dichloroethene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethene (Total) 1 09/22/14 15:36 L212859

<0.0020 mg/Kg 0.00201,2-Dichloropropane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichloropropane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00202,2-Dichloropropane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloropropene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,3-Dichloropropene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,3-Dichloropropene 1 09/22/14 15:36 L212859SEB

<0.0400 mg/Kg 0.0400Ethyl Acetate 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Ethylbenzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Hexachlorobutadiene 1 09/22/14 15:36 L212859SEB

<0.0100 mg/Kg 0.01002-Hexanone 1 09/22/14 15:36 L212859SEB

<0.0100 mg/Kg 0.0100Iodomethane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Isopropylbenzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00204-Isopropyl toluene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Methyl tert-butyl ether (MTBE) 1 09/22/14 15:36 L212859SEB

<0.0100 mg/Kg 0.01004-Methyl-2-Pentanone 1 09/22/14 15:36 L212859SEB

<0.0100 mg/Kg 0.0100Methylene Chloride 1 09/22/14 15:36 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 26 of 119

Page 55: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-3 (8-12')

95404 Matrix:

9/18/2014 9:45

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0100 mg/Kg 0.0100Naphthalene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020n-Propylbenzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Styrene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,1,1,2-Tetrachloroethane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,1,2,2-Tetrachloroethane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Tetrachloroethene 1 09/22/14 15:36 L212859SEB

<0.0100 mg/Kg 0.0100Toluene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichlorobenzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trichlorobenzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,1,1-Trichloroethane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,1,2-Trichloroethane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Trichloroethene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Trichlorofluoromethane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichloropropane 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trimethylbenzene 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.00201,3,5-Trimethylbenzene 1 09/22/14 15:36 L212859SEB

<0.0400 mg/Kg 0.0400Vinyl Acetate 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020Vinyl Chloride 1 09/22/14 15:36 L212859SEB

<0.0020 mg/Kg 0.0020o-Xylene 1 09/22/14 15:36 L212859SEB

<0.0040 mg/Kg 0.0040m,p-Xylene 1 09/22/14 15:36 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 27 of 119

Page 56: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-3 (8-12')

95404 Matrix:

9/18/2014 9:45

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Xylene (Total) 1 09/22/14 15:36 L212859

Surrogate: 4-Bromofluorobenzene 105 Limits: 60-130% 09/22/14 15:361 SEB L212859

Surrogate: 1,2-Dichloroethane - d4 106 Limits: 60-132% 09/22/14 15:361 SEB L212859

Surrogate: Toluene-d8 87.2 Limits: 70-122% 09/22/14 15:361 SEB L212859

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.066 mg/Kg 0.066Acenaphthene 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Acenaphthylene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Acetophenone 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Aniline 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Anthracene 1 09/25/14 13:02 L213162BMP

<0.670 mg/Kg 0.670Benzidine 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)anthracene 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)pyrene 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Benzo(b)fluoranthene 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Benzo(g,h,i)perylene 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Benzo(k)fluoranthene 1 09/25/14 13:02 L213162BMP

<0.330 mg/Kg 0.330Benzoic Acid 1 09/25/14 13:02 L213162BMP

<0.330 mg/Kg 0.330Benzyl alcohol 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroethoxy)methane 1 09/25/14 13:02 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 28 of 119

Page 57: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-3 (8-12')

95404 Matrix:

9/18/2014 9:45

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.170Bis(2-Chloroethyl)ether 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroisopropyl)ether 1 09/25/14 13:02 L213162BMP

<0.330 mg/Kg 0.330Bis(2-ethylhexyl)phthalate 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1704-Bromophenyl phenyl ether 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Butyl benzyl phthalate 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Carbazole 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1704-Chloro-3-methylphenol 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1704-Chloroaniline 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1702-Chloronaphthalene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1702-Chlorophenol 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1704-Chlorophenyl phenyl ether 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Chrysene 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Dibenz(a,h)anthracene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Dibenzofuran 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1701,2-Dichlorobenzene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1701,3-Dichlorobenzene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1701,4-Dichlorobenzene 1 09/25/14 13:02 L213162BMP

<0.330 mg/Kg 0.3303,3'-Dichlorobenzidine 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1702,4-Dichlorophenol 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1702,6-Dichlorophenol 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Diethyl phthalate 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Dimethyl phthalate 1 09/25/14 13:02 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 29 of 119

Page 58: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-3 (8-12')

95404 Matrix:

9/18/2014 9:45

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.330 mg/Kg 0.3303,3' Dimethylbenzidine 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1702,4-Dimethylphenol 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Di-n-butyl phthalate 1 09/25/14 13:02 L213162BMP

<0.330 mg/Kg 0.3304,6-Dinitro-2-methylphenol 1 09/25/14 13:02 L213162BMP

<1.67 mg/Kg 1.672,4-Dinitrophenol 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1702,4-Dinitrotoluene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1702,6-Dinitrotoluene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Di-n-Octyl Phthalate 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Fluoranthene 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Fluorene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobenzene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobutadiene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Hexachlorocyclopentadiene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Hexachloroethane 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Indeno(1,2,3-cd)pyrene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Isophorone 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.0662-Methylnaphthalene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1702-Methylphenol 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1703&4 Methylphenol 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Naphthalene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1702-Nitroaniline 1 09/25/14 13:02 L213162BMP

<0.330 mg/Kg 0.3303-Nitroaniline 1 09/25/14 13:02 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 30 of 119

Page 59: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-3 (8-12')

95404 Matrix:

9/18/2014 9:45

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1704-Nitroaniline 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Nitrobenzene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1702-Nitrophenol 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1704-Nitrophenol 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodimethylamine 1 09/25/14 13:02 L213162BMP

<0.330 mg/Kg 0.330N-Nitrosodiphenylamine 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodiethylamine 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-butylamine 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-propylamine 1 09/25/14 13:02 L213162BMP

<0.330 mg/Kg 0.330Pentachlorophenol 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Phenanthrene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.170Phenol 1 09/25/14 13:02 L213162BMP

<0.066 mg/Kg 0.066Pyrene 1 09/25/14 13:02 L213162BMP

<0.330 mg/Kg 0.330Pyridine 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1701,2,4,5-Tetrachlorobenzene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1702,3,4,6-Tetrachlorophenol 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1701,2,4-Trichlorobenzene 1 09/25/14 13:02 L213162BMP

<0.170 mg/Kg 0.1702,4,5-Trichlorophenol 1 09/25/14 13:02 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 31 of 119

Page 60: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-3 (8-12')

95404 Matrix:

9/18/2014 9:45

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1702,4,6-Trichlorophenol 1 09/25/14 13:02 L213162BMP

Surrogate: 2-Fluorobiphenyl 58.1 Limits: 33-115% 09/25/14 13:021 BMP L213162

Surrogate: 2-Fluorophenol 52.8 Limits: 10-119% 09/25/14 13:021 BMP L213162

Surrogate: Nitrobenzene-d5 55.4 Limits: 29-110% 09/25/14 13:021 BMP L213162

Surrogate: Phenol-d6 57.5 Limits: 11-125% 09/25/14 13:021 BMP L213162

Surrogate: 4-Terphenyl-d14 65.7 Limits: 33-122% 09/25/14 13:021 BMP L213162

Surrogate: 2,4,6-Tribromophenol 69.7 Limits: 9-134% 09/25/14 13:021 BMP L213162

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 32 of 119

Page 61: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-4 (12-16')

95405 Matrix:

9/18/2014 10:20

Solids

Test Results Units MQL By AnalyticalMethod

Date / TimeAnalyzed

DF

<1.00 mg/Kg 1.00Cyanide, Total 1 09/25/14 11:15 SW-9014EWB

6.9 s.u.pH 1 09/24/14 13:45 9045CSNS

<10.0 mg/Kg 10.0Sulfide 1 09/23/14 10:35 4500S2F-2011KM2

<0.500 mg/Kg 0.500Total Antimony 1 09/22/14 22:16 6010BBKN

3.95 mg/Kg 1.00Total Arsenic 1 09/22/14 22:16 6010BBKN

0.478 mg/Kg 0.0500Total Beryllium 1 09/22/14 22:16 6010BBKN

<0.100 mg/Kg 0.100Total Cadmium 1 09/22/14 22:16 6010BBKN

11.3 mg/Kg 0.250Total Chromium 1 09/22/14 22:16 6010BBKN

9.02 mg/Kg 0.250Total Copper 1 09/22/14 22:16 6010BBKN

25.9 mg/Kg 0.300Total Lead 1 09/22/14 22:16 6010BBKN

0.0209 mg/Kg 0.0133Mercury (Total) 1 09/22/14 13:22 7471AJRS

9.28 mg/Kg 0.250Total Nickel 1 09/23/14 18:25 6010BBKN

<1.00 mg/Kg 1.00Total Selenium 1 09/22/14 22:16 6010BBKN

<0.250 mg/Kg 0.250Total Silver 1 09/22/14 22:16 6010BBKN

<1.00 mg/Kg 1.00Total Thallium 1 09/22/14 22:16 6010BBKN

27.2 mg/Kg 0.500Total Zinc 1 09/22/14 22:16 6010BBKN

65.2 mg/Kg 10.0Sulfate 1 09/23/14 20:00 9056CGC

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Method Quantitation LimitMQLMinimum valueM

Page 33 of 119

Page 62: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-4 (12-16')

95405 Matrix:

9/18/2014 10:20

Solids

Analytical Method: 8082

Prep Method: 3546 Date/Time Prepped: 9/25/2014 09:00:00Prep Batch(es): L213208

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0066 mg/Kg 0.0066Aroclor 1016 1 09/26/14 00:25 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1221 1 09/26/14 00:25 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1232 1 09/26/14 00:25 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1242 1 09/26/14 00:25 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1248 1 09/26/14 00:25 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1254 1 09/26/14 00:25 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1260 1 09/26/14 00:25 L213328VIC

Surrogate: Decachlorobiphenyl 55.8 Limits: 25-125% 09/26/14 00:251 VIC L213328

Surrogate: Tetrachloro-m-xylene 50.7 Limits: 25-125% 09/26/14 00:251 VIC L213328

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0400 mg/Kg 0.0400Acetone 1 09/22/14 16:58 L212859SEB

<0.100 mg/Kg 0.100Acetonitrile 1 09/22/14 16:58 L212859SEB

<0.0400 mg/Kg 0.0400Acrolein 1 09/22/14 16:58 L212859SEB

<0.0400 mg/Kg 0.0400Acrylonitrile 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Benzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Bromobenzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Bromochloromethane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Bromodichloromethane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Bromoform 1 09/22/14 16:58 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 34 of 119

Page 63: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-4 (12-16')

95405 Matrix:

9/18/2014 10:20

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Bromomethane 1 09/22/14 16:58 L212859SEB

<0.0400 mg/Kg 0.0400Methyl Ethyl Ketone (MEK) 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020n-Butylbenzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020sec-Butyl benzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020tert-Butyl benzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Disulfide 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Tetrachloride 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Chlorobenzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Chlorodibromomethane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Chloroethane 1 09/22/14 16:58 L212859SEB

<0.0020 M mg/Kg 0.00202-Chloroethylvinyl Ether 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Chloroform 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Chloromethane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00202-Chlorotoluene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00204-Chlorotoluene 1 09/22/14 16:58 L212859SEB

<0.0100 mg/Kg 0.01001,2-Dibromo-3-Chloropropane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dibromoethane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Dibromomethane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichlorobenzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichlorobenzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,4-Dichlorobenzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Dichlorodifluoromethane 1 09/22/14 16:58 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 35 of 119

Page 64: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-4 (12-16')

95405 Matrix:

9/18/2014 10:20

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.00201,1-Dichloroethane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloroethene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,2-Dichloroethene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,2-Dichloroethene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethene (Total) 1 09/22/14 16:58 L212859

<0.0020 mg/Kg 0.00201,2-Dichloropropane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichloropropane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00202,2-Dichloropropane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloropropene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,3-Dichloropropene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,3-Dichloropropene 1 09/22/14 16:58 L212859SEB

<0.0400 mg/Kg 0.0400Ethyl Acetate 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Ethylbenzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Hexachlorobutadiene 1 09/22/14 16:58 L212859SEB

<0.0100 mg/Kg 0.01002-Hexanone 1 09/22/14 16:58 L212859SEB

<0.0100 mg/Kg 0.0100Iodomethane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Isopropylbenzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00204-Isopropyl toluene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Methyl tert-butyl ether (MTBE) 1 09/22/14 16:58 L212859SEB

<0.0100 mg/Kg 0.01004-Methyl-2-Pentanone 1 09/22/14 16:58 L212859SEB

<0.0100 mg/Kg 0.0100Methylene Chloride 1 09/22/14 16:58 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 36 of 119

Page 65: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-4 (12-16')

95405 Matrix:

9/18/2014 10:20

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0100 mg/Kg 0.0100Naphthalene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020n-Propylbenzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Styrene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,1,1,2-Tetrachloroethane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,1,2,2-Tetrachloroethane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Tetrachloroethene 1 09/22/14 16:58 L212859SEB

<0.0100 mg/Kg 0.0100Toluene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichlorobenzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trichlorobenzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,1,1-Trichloroethane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,1,2-Trichloroethane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Trichloroethene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Trichlorofluoromethane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichloropropane 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trimethylbenzene 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.00201,3,5-Trimethylbenzene 1 09/22/14 16:58 L212859SEB

<0.0400 mg/Kg 0.0400Vinyl Acetate 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020Vinyl Chloride 1 09/22/14 16:58 L212859SEB

<0.0020 mg/Kg 0.0020o-Xylene 1 09/22/14 16:58 L212859SEB

<0.0040 mg/Kg 0.0040m,p-Xylene 1 09/22/14 16:58 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 37 of 119

Page 66: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-4 (12-16')

95405 Matrix:

9/18/2014 10:20

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Xylene (Total) 1 09/22/14 16:58 L212859

Surrogate: 4-Bromofluorobenzene 88.7 Limits: 60-130% 09/22/14 16:581 SEB L212859

Surrogate: 1,2-Dichloroethane - d4 113 Limits: 60-132% 09/22/14 16:581 SEB L212859

Surrogate: Toluene-d8 99.9 Limits: 70-122% 09/22/14 16:581 SEB L212859

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.066 mg/Kg 0.066Acenaphthene 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Acenaphthylene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Acetophenone 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Aniline 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Anthracene 1 09/26/14 11:12 L213162BMP

<0.670 mg/Kg 0.670Benzidine 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)anthracene 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)pyrene 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Benzo(b)fluoranthene 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Benzo(g,h,i)perylene 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Benzo(k)fluoranthene 1 09/26/14 11:12 L213162BMP

<0.330 mg/Kg 0.330Benzoic Acid 1 09/26/14 11:12 L213162BMP

<0.330 mg/Kg 0.330Benzyl alcohol 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroethoxy)methane 1 09/26/14 11:12 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 38 of 119

Page 67: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-4 (12-16')

95405 Matrix:

9/18/2014 10:20

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.170Bis(2-Chloroethyl)ether 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroisopropyl)ether 1 09/26/14 11:12 L213162BMP

<0.330 mg/Kg 0.330Bis(2-ethylhexyl)phthalate 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1704-Bromophenyl phenyl ether 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Butyl benzyl phthalate 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Carbazole 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1704-Chloro-3-methylphenol 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1704-Chloroaniline 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1702-Chloronaphthalene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1702-Chlorophenol 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1704-Chlorophenyl phenyl ether 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Chrysene 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Dibenz(a,h)anthracene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Dibenzofuran 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1701,2-Dichlorobenzene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1701,3-Dichlorobenzene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1701,4-Dichlorobenzene 1 09/26/14 11:12 L213162BMP

<0.330 mg/Kg 0.3303,3'-Dichlorobenzidine 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1702,4-Dichlorophenol 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1702,6-Dichlorophenol 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Diethyl phthalate 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Dimethyl phthalate 1 09/26/14 11:12 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 39 of 119

Page 68: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-4 (12-16')

95405 Matrix:

9/18/2014 10:20

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.330 mg/Kg 0.3303,3' Dimethylbenzidine 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1702,4-Dimethylphenol 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Di-n-butyl phthalate 1 09/26/14 11:12 L213162BMP

<0.330 mg/Kg 0.3304,6-Dinitro-2-methylphenol 1 09/26/14 11:12 L213162BMP

<1.67 mg/Kg 1.672,4-Dinitrophenol 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1702,4-Dinitrotoluene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1702,6-Dinitrotoluene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Di-n-Octyl Phthalate 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Fluoranthene 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Fluorene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobenzene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobutadiene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Hexachlorocyclopentadiene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Hexachloroethane 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Indeno(1,2,3-cd)pyrene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Isophorone 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.0662-Methylnaphthalene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1702-Methylphenol 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1703&4 Methylphenol 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Naphthalene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1702-Nitroaniline 1 09/26/14 11:12 L213162BMP

<0.330 mg/Kg 0.3303-Nitroaniline 1 09/26/14 11:12 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 40 of 119

Page 69: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-4 (12-16')

95405 Matrix:

9/18/2014 10:20

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1704-Nitroaniline 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Nitrobenzene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1702-Nitrophenol 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1704-Nitrophenol 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodimethylamine 1 09/26/14 11:12 L213162BMP

<0.330 mg/Kg 0.330N-Nitrosodiphenylamine 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodiethylamine 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-butylamine 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-propylamine 1 09/26/14 11:12 L213162BMP

<0.330 mg/Kg 0.330Pentachlorophenol 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Phenanthrene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.170Phenol 1 09/26/14 11:12 L213162BMP

<0.066 mg/Kg 0.066Pyrene 1 09/26/14 11:12 L213162BMP

<0.330 mg/Kg 0.330Pyridine 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1701,2,4,5-Tetrachlorobenzene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1702,3,4,6-Tetrachlorophenol 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1701,2,4-Trichlorobenzene 1 09/26/14 11:12 L213162BMP

<0.170 mg/Kg 0.1702,4,5-Trichlorophenol 1 09/26/14 11:12 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 41 of 119

Page 70: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-4 (12-16')

95405 Matrix:

9/18/2014 10:20

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1702,4,6-Trichlorophenol 1 09/26/14 11:12 L213162BMP

Surrogate: 2-Fluorobiphenyl 61.9 Limits: 33-115% 09/26/14 11:121 BMP L213162

Surrogate: 2-Fluorophenol 53.8 Limits: 10-119% 09/26/14 11:121 BMP L213162

Surrogate: Nitrobenzene-d5 54.7 Limits: 29-110% 09/26/14 11:121 BMP L213162

Surrogate: Phenol-d6 57.5 Limits: 11-125% 09/26/14 11:121 BMP L213162

Surrogate: 4-Terphenyl-d14 67.6 Limits: 33-122% 09/26/14 11:121 BMP L213162

Surrogate: 2,4,6-Tribromophenol 71.6 Limits: 9-134% 09/26/14 11:121 BMP L213162

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 42 of 119

Page 71: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-5 (20-24')

95406 Matrix:

9/18/2014 11:05

Solids

Test Results Units MQL By AnalyticalMethod

Date / TimeAnalyzed

DF

<1.00 mg/Kg 1.00Cyanide, Total 1 09/25/14 11:15 SW-9014EWB

5.9 s.u.pH 1 09/24/14 13:45 9045CSNS

<10.0 mg/Kg 10.0Sulfide 1 09/23/14 10:35 4500S2F-2011KM2

<0.500 mg/Kg 0.500Total Antimony 1 09/22/14 22:20 6010BBKN

4.06 mg/Kg 1.00Total Arsenic 1 09/22/14 22:20 6010BBKN

0.416 mg/Kg 0.0500Total Beryllium 1 09/22/14 22:20 6010BBKN

<0.100 mg/Kg 0.100Total Cadmium 1 09/22/14 22:20 6010BBKN

11.7 mg/Kg 0.250Total Chromium 1 09/22/14 22:20 6010BBKN

8.85 mg/Kg 0.250Total Copper 1 09/22/14 22:20 6010BBKN

5.73 mg/Kg 0.300Total Lead 1 09/22/14 22:20 6010BBKN

0.0190 mg/Kg 0.0133Mercury (Total) 1 09/22/14 13:28 7471AJRS

9.10 mg/Kg 0.250Total Nickel 1 09/23/14 18:30 6010BBKN

<1.00 mg/Kg 1.00Total Selenium 1 09/22/14 22:20 6010BBKN

<0.250 mg/Kg 0.250Total Silver 1 09/22/14 22:20 6010BBKN

<1.00 mg/Kg 1.00Total Thallium 1 09/22/14 22:20 6010BBKN

24.0 mg/Kg 0.500Total Zinc 1 09/22/14 22:20 6010BBKN

11.1 mg/Kg 10.0Sulfate 1 09/23/14 20:18 9056CGC

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Method Quantitation LimitMQLMinimum valueM

Page 43 of 119

Page 72: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-5 (20-24')

95406 Matrix:

9/18/2014 11:05

Solids

Analytical Method: 8082

Prep Method: 3546 Date/Time Prepped: 9/25/2014 09:00:00Prep Batch(es): L213208

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0066 mg/Kg 0.0066Aroclor 1016 1 09/26/14 00:45 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1221 1 09/26/14 00:45 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1232 1 09/26/14 00:45 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1242 1 09/26/14 00:45 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1248 1 09/26/14 00:45 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1254 1 09/26/14 00:45 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1260 1 09/26/14 00:45 L213328VIC

Surrogate: Decachlorobiphenyl 70.8 Limits: 25-125% 09/26/14 00:451 VIC L213328

Surrogate: Tetrachloro-m-xylene 61.5 Limits: 25-125% 09/26/14 00:451 VIC L213328

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0400 mg/Kg 0.0400Acetone 1 09/22/14 17:39 L212859SEB

<0.100 mg/Kg 0.100Acetonitrile 1 09/22/14 17:39 L212859SEB

<0.0400 mg/Kg 0.0400Acrolein 1 09/22/14 17:39 L212859SEB

<0.0400 mg/Kg 0.0400Acrylonitrile 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Benzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Bromobenzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Bromochloromethane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Bromodichloromethane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Bromoform 1 09/22/14 17:39 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 44 of 119

Page 73: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-5 (20-24')

95406 Matrix:

9/18/2014 11:05

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Bromomethane 1 09/22/14 17:39 L212859SEB

<0.0400 mg/Kg 0.0400Methyl Ethyl Ketone (MEK) 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020n-Butylbenzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020sec-Butyl benzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020tert-Butyl benzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Disulfide 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Tetrachloride 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Chlorobenzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Chlorodibromomethane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Chloroethane 1 09/22/14 17:39 L212859SEB

<0.0020 M mg/Kg 0.00202-Chloroethylvinyl Ether 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Chloroform 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Chloromethane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00202-Chlorotoluene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00204-Chlorotoluene 1 09/22/14 17:39 L212859SEB

<0.0100 mg/Kg 0.01001,2-Dibromo-3-Chloropropane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dibromoethane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Dibromomethane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichlorobenzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichlorobenzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,4-Dichlorobenzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Dichlorodifluoromethane 1 09/22/14 17:39 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 45 of 119

Page 74: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-5 (20-24')

95406 Matrix:

9/18/2014 11:05

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.00201,1-Dichloroethane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloroethene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,2-Dichloroethene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,2-Dichloroethene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethene (Total) 1 09/22/14 17:39 L212859

<0.0020 mg/Kg 0.00201,2-Dichloropropane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichloropropane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00202,2-Dichloropropane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloropropene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,3-Dichloropropene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,3-Dichloropropene 1 09/22/14 17:39 L212859SEB

<0.0400 mg/Kg 0.0400Ethyl Acetate 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Ethylbenzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Hexachlorobutadiene 1 09/22/14 17:39 L212859SEB

<0.0100 mg/Kg 0.01002-Hexanone 1 09/22/14 17:39 L212859SEB

<0.0100 mg/Kg 0.0100Iodomethane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Isopropylbenzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00204-Isopropyl toluene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Methyl tert-butyl ether (MTBE) 1 09/22/14 17:39 L212859SEB

<0.0100 mg/Kg 0.01004-Methyl-2-Pentanone 1 09/22/14 17:39 L212859SEB

<0.0100 mg/Kg 0.0100Methylene Chloride 1 09/22/14 17:39 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 46 of 119

Page 75: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-5 (20-24')

95406 Matrix:

9/18/2014 11:05

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0100 mg/Kg 0.0100Naphthalene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020n-Propylbenzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Styrene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,1,1,2-Tetrachloroethane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,1,2,2-Tetrachloroethane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Tetrachloroethene 1 09/22/14 17:39 L212859SEB

<0.0100 mg/Kg 0.0100Toluene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichlorobenzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trichlorobenzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,1,1-Trichloroethane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,1,2-Trichloroethane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Trichloroethene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Trichlorofluoromethane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichloropropane 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trimethylbenzene 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.00201,3,5-Trimethylbenzene 1 09/22/14 17:39 L212859SEB

<0.0400 mg/Kg 0.0400Vinyl Acetate 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020Vinyl Chloride 1 09/22/14 17:39 L212859SEB

<0.0020 mg/Kg 0.0020o-Xylene 1 09/22/14 17:39 L212859SEB

<0.0040 mg/Kg 0.0040m,p-Xylene 1 09/22/14 17:39 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 47 of 119

Page 76: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-5 (20-24')

95406 Matrix:

9/18/2014 11:05

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Xylene (Total) 1 09/22/14 17:39 L212859

Surrogate: 4-Bromofluorobenzene 112 Limits: 60-130% 09/22/14 17:391 SEB L212859

Surrogate: 1,2-Dichloroethane - d4 112 Limits: 60-132% 09/22/14 17:391 SEB L212859

Surrogate: Toluene-d8 86.0 Limits: 70-122% 09/22/14 17:391 SEB L212859

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.066 mg/Kg 0.066Acenaphthene 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Acenaphthylene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Acetophenone 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Aniline 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Anthracene 1 09/25/14 13:37 L213162BMP

<0.670 mg/Kg 0.670Benzidine 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)anthracene 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)pyrene 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Benzo(b)fluoranthene 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Benzo(g,h,i)perylene 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Benzo(k)fluoranthene 1 09/25/14 13:37 L213162BMP

<0.330 mg/Kg 0.330Benzoic Acid 1 09/25/14 13:37 L213162BMP

<0.330 mg/Kg 0.330Benzyl alcohol 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroethoxy)methane 1 09/25/14 13:37 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 48 of 119

Page 77: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-5 (20-24')

95406 Matrix:

9/18/2014 11:05

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.170Bis(2-Chloroethyl)ether 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroisopropyl)ether 1 09/25/14 13:37 L213162BMP

<0.330 mg/Kg 0.330Bis(2-ethylhexyl)phthalate 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1704-Bromophenyl phenyl ether 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Butyl benzyl phthalate 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Carbazole 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1704-Chloro-3-methylphenol 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1704-Chloroaniline 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1702-Chloronaphthalene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1702-Chlorophenol 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1704-Chlorophenyl phenyl ether 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Chrysene 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Dibenz(a,h)anthracene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Dibenzofuran 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1701,2-Dichlorobenzene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1701,3-Dichlorobenzene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1701,4-Dichlorobenzene 1 09/25/14 13:37 L213162BMP

<0.330 mg/Kg 0.3303,3'-Dichlorobenzidine 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1702,4-Dichlorophenol 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1702,6-Dichlorophenol 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Diethyl phthalate 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Dimethyl phthalate 1 09/25/14 13:37 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 49 of 119

Page 78: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-5 (20-24')

95406 Matrix:

9/18/2014 11:05

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.330 mg/Kg 0.3303,3' Dimethylbenzidine 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1702,4-Dimethylphenol 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Di-n-butyl phthalate 1 09/25/14 13:37 L213162BMP

<0.330 mg/Kg 0.3304,6-Dinitro-2-methylphenol 1 09/25/14 13:37 L213162BMP

<1.67 mg/Kg 1.672,4-Dinitrophenol 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1702,4-Dinitrotoluene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1702,6-Dinitrotoluene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Di-n-Octyl Phthalate 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Fluoranthene 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Fluorene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobenzene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobutadiene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Hexachlorocyclopentadiene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Hexachloroethane 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Indeno(1,2,3-cd)pyrene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Isophorone 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.0662-Methylnaphthalene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1702-Methylphenol 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1703&4 Methylphenol 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Naphthalene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1702-Nitroaniline 1 09/25/14 13:37 L213162BMP

<0.330 mg/Kg 0.3303-Nitroaniline 1 09/25/14 13:37 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 50 of 119

Page 79: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-5 (20-24')

95406 Matrix:

9/18/2014 11:05

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1704-Nitroaniline 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Nitrobenzene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1702-Nitrophenol 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1704-Nitrophenol 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodimethylamine 1 09/25/14 13:37 L213162BMP

<0.330 mg/Kg 0.330N-Nitrosodiphenylamine 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodiethylamine 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-butylamine 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-propylamine 1 09/25/14 13:37 L213162BMP

<0.330 mg/Kg 0.330Pentachlorophenol 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Phenanthrene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.170Phenol 1 09/25/14 13:37 L213162BMP

<0.066 mg/Kg 0.066Pyrene 1 09/25/14 13:37 L213162BMP

<0.330 mg/Kg 0.330Pyridine 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1701,2,4,5-Tetrachlorobenzene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1702,3,4,6-Tetrachlorophenol 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1701,2,4-Trichlorobenzene 1 09/25/14 13:37 L213162BMP

<0.170 mg/Kg 0.1702,4,5-Trichlorophenol 1 09/25/14 13:37 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 51 of 119

Page 80: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-5 (20-24')

95406 Matrix:

9/18/2014 11:05

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1702,4,6-Trichlorophenol 1 09/25/14 13:37 L213162BMP

Surrogate: 2-Fluorobiphenyl 62.8 Limits: 33-115% 09/25/14 13:371 BMP L213162

Surrogate: 2-Fluorophenol 55.1 Limits: 10-119% 09/25/14 13:371 BMP L213162

Surrogate: Nitrobenzene-d5 58.2 Limits: 29-110% 09/25/14 13:371 BMP L213162

Surrogate: Phenol-d6 57.4 Limits: 11-125% 09/25/14 13:371 BMP L213162

Surrogate: 4-Terphenyl-d14 69.8 Limits: 33-122% 09/25/14 13:371 BMP L213162

Surrogate: 2,4,6-Tribromophenol 76.3 Limits: 9-134% 09/25/14 13:371 BMP L213162

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 52 of 119

Page 81: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-6 (20-24')

95407 Matrix:

9/18/2014 12:00

Solids

Test Results Units MQL By AnalyticalMethod

Date / TimeAnalyzed

DF

<1.00 mg/Kg 1.00Cyanide, Total 1 09/25/14 11:15 SW-9014EWB

5.2 s.u.pH 1 09/24/14 13:45 9045CSNS

<10.0 mg/Kg 10.0Sulfide 1 09/23/14 10:35 4500S2F-2011KM2

<0.500 mg/Kg 0.500Total Antimony 1 09/22/14 22:24 6010BBKN

5.17 mg/Kg 1.00Total Arsenic 1 09/22/14 22:24 6010BBKN

0.440 mg/Kg 0.0500Total Beryllium 1 09/22/14 22:24 6010BBKN

<0.100 mg/Kg 0.100Total Cadmium 1 09/22/14 22:24 6010BBKN

10.6 mg/Kg 0.250Total Chromium 1 09/22/14 22:24 6010BBKN

9.98 mg/Kg 0.250Total Copper 1 09/22/14 22:24 6010BBKN

7.11 mg/Kg 0.300Total Lead 1 09/22/14 22:24 6010BBKN

0.0203 mg/Kg 0.0133Mercury (Total) 1 09/22/14 13:30 7471AJRS

10.8 mg/Kg 0.250Total Nickel 1 09/23/14 18:35 6010BBKN

<1.00 mg/Kg 1.00Total Selenium 1 09/22/14 22:24 6010BBKN

<0.250 mg/Kg 0.250Total Silver 1 09/22/14 22:24 6010BBKN

<1.00 mg/Kg 1.00Total Thallium 1 09/22/14 22:24 6010BBKN

30.9 mg/Kg 0.500Total Zinc 1 09/22/14 22:24 6010BBKN

15.0 mg/Kg 10.0Sulfate 1 09/23/14 21:10 9056CGC

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Method Quantitation LimitMQLMinimum valueM

Page 53 of 119

Page 82: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-6 (20-24')

95407 Matrix:

9/18/2014 12:00

Solids

Analytical Method: 8082

Prep Method: 3546 Date/Time Prepped: 9/25/2014 09:00:00Prep Batch(es): L213208

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0066 mg/Kg 0.0066Aroclor 1016 1 09/26/14 01:06 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1221 1 09/26/14 01:06 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1232 1 09/26/14 01:06 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1242 1 09/26/14 01:06 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1248 1 09/26/14 01:06 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1254 1 09/26/14 01:06 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1260 1 09/26/14 01:06 L213328VIC

Surrogate: Decachlorobiphenyl 62.8 Limits: 25-125% 09/26/14 01:061 VIC L213328

Surrogate: Tetrachloro-m-xylene 46.7 Limits: 25-125% 09/26/14 01:061 VIC L213328

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0400 mg/Kg 0.0400Acetone 1 09/22/14 18:20 L212859SEB

<0.100 mg/Kg 0.100Acetonitrile 1 09/22/14 18:20 L212859SEB

<0.0400 mg/Kg 0.0400Acrolein 1 09/22/14 18:20 L212859SEB

<0.0400 mg/Kg 0.0400Acrylonitrile 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Benzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Bromobenzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Bromochloromethane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Bromodichloromethane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Bromoform 1 09/22/14 18:20 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 54 of 119

Page 83: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-6 (20-24')

95407 Matrix:

9/18/2014 12:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Bromomethane 1 09/22/14 18:20 L212859SEB

<0.0400 mg/Kg 0.0400Methyl Ethyl Ketone (MEK) 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020n-Butylbenzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020sec-Butyl benzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020tert-Butyl benzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Disulfide 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Tetrachloride 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Chlorobenzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Chlorodibromomethane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Chloroethane 1 09/22/14 18:20 L212859SEB

<0.0020 M mg/Kg 0.00202-Chloroethylvinyl Ether 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Chloroform 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Chloromethane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00202-Chlorotoluene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00204-Chlorotoluene 1 09/22/14 18:20 L212859SEB

<0.0100 mg/Kg 0.01001,2-Dibromo-3-Chloropropane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dibromoethane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Dibromomethane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichlorobenzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichlorobenzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,4-Dichlorobenzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Dichlorodifluoromethane 1 09/22/14 18:20 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 55 of 119

Page 84: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-6 (20-24')

95407 Matrix:

9/18/2014 12:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.00201,1-Dichloroethane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloroethene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,2-Dichloroethene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,2-Dichloroethene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethene (Total) 1 09/22/14 18:20 L212859

<0.0020 mg/Kg 0.00201,2-Dichloropropane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichloropropane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00202,2-Dichloropropane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloropropene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,3-Dichloropropene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,3-Dichloropropene 1 09/22/14 18:20 L212859SEB

<0.0400 mg/Kg 0.0400Ethyl Acetate 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Ethylbenzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Hexachlorobutadiene 1 09/22/14 18:20 L212859SEB

<0.0100 mg/Kg 0.01002-Hexanone 1 09/22/14 18:20 L212859SEB

<0.0100 mg/Kg 0.0100Iodomethane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Isopropylbenzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00204-Isopropyl toluene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Methyl tert-butyl ether (MTBE) 1 09/22/14 18:20 L212859SEB

<0.0100 mg/Kg 0.01004-Methyl-2-Pentanone 1 09/22/14 18:20 L212859SEB

<0.0100 mg/Kg 0.0100Methylene Chloride 1 09/22/14 18:20 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 56 of 119

Page 85: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-6 (20-24')

95407 Matrix:

9/18/2014 12:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0100 mg/Kg 0.0100Naphthalene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020n-Propylbenzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Styrene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,1,1,2-Tetrachloroethane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,1,2,2-Tetrachloroethane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Tetrachloroethene 1 09/22/14 18:20 L212859SEB

<0.0100 mg/Kg 0.0100Toluene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichlorobenzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trichlorobenzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,1,1-Trichloroethane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,1,2-Trichloroethane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Trichloroethene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Trichlorofluoromethane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichloropropane 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trimethylbenzene 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.00201,3,5-Trimethylbenzene 1 09/22/14 18:20 L212859SEB

<0.0400 mg/Kg 0.0400Vinyl Acetate 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020Vinyl Chloride 1 09/22/14 18:20 L212859SEB

<0.0020 mg/Kg 0.0020o-Xylene 1 09/22/14 18:20 L212859SEB

<0.0040 mg/Kg 0.0040m,p-Xylene 1 09/22/14 18:20 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 57 of 119

Page 86: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-6 (20-24')

95407 Matrix:

9/18/2014 12:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Xylene (Total) 1 09/22/14 18:20 L212859

Surrogate: 4-Bromofluorobenzene 94.6 Limits: 60-130% 09/22/14 18:201 SEB L212859

Surrogate: 1,2-Dichloroethane - d4 108 Limits: 60-132% 09/22/14 18:201 SEB L212859

Surrogate: Toluene-d8 88.6 Limits: 70-122% 09/22/14 18:201 SEB L212859

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.066 mg/Kg 0.066Acenaphthene 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Acenaphthylene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Acetophenone 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Aniline 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Anthracene 1 09/25/14 14:13 L213162BMP

<0.670 mg/Kg 0.670Benzidine 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)anthracene 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)pyrene 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Benzo(b)fluoranthene 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Benzo(g,h,i)perylene 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Benzo(k)fluoranthene 1 09/25/14 14:13 L213162BMP

<0.330 mg/Kg 0.330Benzoic Acid 1 09/25/14 14:13 L213162BMP

<0.330 mg/Kg 0.330Benzyl alcohol 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroethoxy)methane 1 09/25/14 14:13 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 58 of 119

Page 87: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-6 (20-24')

95407 Matrix:

9/18/2014 12:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.170Bis(2-Chloroethyl)ether 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroisopropyl)ether 1 09/25/14 14:13 L213162BMP

<0.330 mg/Kg 0.330Bis(2-ethylhexyl)phthalate 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1704-Bromophenyl phenyl ether 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Butyl benzyl phthalate 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Carbazole 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1704-Chloro-3-methylphenol 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1704-Chloroaniline 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1702-Chloronaphthalene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1702-Chlorophenol 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1704-Chlorophenyl phenyl ether 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Chrysene 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Dibenz(a,h)anthracene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Dibenzofuran 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1701,2-Dichlorobenzene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1701,3-Dichlorobenzene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1701,4-Dichlorobenzene 1 09/25/14 14:13 L213162BMP

<0.330 mg/Kg 0.3303,3'-Dichlorobenzidine 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1702,4-Dichlorophenol 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1702,6-Dichlorophenol 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Diethyl phthalate 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Dimethyl phthalate 1 09/25/14 14:13 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 59 of 119

Page 88: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-6 (20-24')

95407 Matrix:

9/18/2014 12:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.330 mg/Kg 0.3303,3' Dimethylbenzidine 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1702,4-Dimethylphenol 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Di-n-butyl phthalate 1 09/25/14 14:13 L213162BMP

<0.330 mg/Kg 0.3304,6-Dinitro-2-methylphenol 1 09/25/14 14:13 L213162BMP

<1.67 mg/Kg 1.672,4-Dinitrophenol 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1702,4-Dinitrotoluene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1702,6-Dinitrotoluene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Di-n-Octyl Phthalate 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Fluoranthene 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Fluorene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobenzene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobutadiene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Hexachlorocyclopentadiene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Hexachloroethane 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Indeno(1,2,3-cd)pyrene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Isophorone 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.0662-Methylnaphthalene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1702-Methylphenol 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1703&4 Methylphenol 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Naphthalene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1702-Nitroaniline 1 09/25/14 14:13 L213162BMP

<0.330 mg/Kg 0.3303-Nitroaniline 1 09/25/14 14:13 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 60 of 119

Page 89: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-6 (20-24')

95407 Matrix:

9/18/2014 12:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1704-Nitroaniline 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Nitrobenzene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1702-Nitrophenol 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1704-Nitrophenol 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodimethylamine 1 09/25/14 14:13 L213162BMP

<0.330 mg/Kg 0.330N-Nitrosodiphenylamine 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodiethylamine 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-butylamine 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-propylamine 1 09/25/14 14:13 L213162BMP

<0.330 mg/Kg 0.330Pentachlorophenol 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Phenanthrene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.170Phenol 1 09/25/14 14:13 L213162BMP

<0.066 mg/Kg 0.066Pyrene 1 09/25/14 14:13 L213162BMP

<0.330 mg/Kg 0.330Pyridine 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1701,2,4,5-Tetrachlorobenzene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1702,3,4,6-Tetrachlorophenol 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1701,2,4-Trichlorobenzene 1 09/25/14 14:13 L213162BMP

<0.170 mg/Kg 0.1702,4,5-Trichlorophenol 1 09/25/14 14:13 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 61 of 119

Page 90: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-6 (20-24')

95407 Matrix:

9/18/2014 12:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1702,4,6-Trichlorophenol 1 09/25/14 14:13 L213162BMP

Surrogate: 2-Fluorobiphenyl 62.4 Limits: 33-115% 09/25/14 14:131 BMP L213162

Surrogate: 2-Fluorophenol 57.5 Limits: 10-119% 09/25/14 14:131 BMP L213162

Surrogate: Nitrobenzene-d5 60.9 Limits: 29-110% 09/25/14 14:131 BMP L213162

Surrogate: Phenol-d6 60.5 Limits: 11-125% 09/25/14 14:131 BMP L213162

Surrogate: 4-Terphenyl-d14 78.2 Limits: 33-122% 09/25/14 14:131 BMP L213162

Surrogate: 2,4,6-Tribromophenol 78.5 Limits: 9-134% 09/25/14 14:131 BMP L213162

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 62 of 119

Page 91: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-7 (8-12')

95408 Matrix:

9/18/2014 13:25

Solids

Test Results Units MQL By AnalyticalMethod

Date / TimeAnalyzed

DF

<1.00 mg/Kg 1.00Cyanide, Total 1 09/25/14 11:15 SW-9014EWB

7.2 s.u.pH 1 09/24/14 13:45 9045CSNS

<10.0 mg/Kg 10.0Sulfide 1 09/23/14 10:35 4500S2F-2011KM2

<2.50 mg/Kg 2.50Total Antimony 5 09/23/14 18:39 6010BBKN

8.62 mg/Kg 5.00Total Arsenic 5 09/23/14 18:39 6010BBKN

<0.250 mg/Kg 0.250Total Beryllium 5 09/23/14 18:39 6010BBKN

<0.500 mg/Kg 0.500Total Cadmium 5 09/23/14 18:39 6010BBKN

10.2 mg/Kg 1.25Total Chromium 5 09/23/14 18:39 6010BBKN

17.2 mg/Kg 1.25Total Copper 5 09/23/14 18:39 6010BBKN

11.5 mg/Kg 1.50Total Lead 5 09/23/14 18:39 6010BBKN

0.0319 mg/Kg 0.0133Mercury (Total) 1 09/22/14 13:32 7471AJRS

15.1 mg/Kg 1.25Total Nickel 5 09/23/14 18:39 6010BBKN

<5.00 mg/Kg 5.00Total Selenium 5 09/23/14 18:39 6010BBKN

<1.25 mg/Kg 1.25Total Silver 5 09/23/14 18:39 6010BBKN

<5.00 mg/Kg 5.00Total Thallium 5 09/23/14 18:39 6010BBKN

48.8 mg/Kg 2.50Total Zinc 5 09/23/14 18:39 6010BBKN

73.0 mg/Kg 10.0Sulfate 1 09/23/14 21:27 9056CGC

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Method Quantitation LimitMQLMinimum valueM

Page 63 of 119

Page 92: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-7 (8-12')

95408 Matrix:

9/18/2014 13:25

Solids

Analytical Method: 8082

Prep Method: 3546 Date/Time Prepped: 9/25/2014 09:00:00Prep Batch(es): L213208

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0066 mg/Kg 0.0066Aroclor 1016 1 09/26/14 01:26 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1221 1 09/26/14 01:26 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1232 1 09/26/14 01:26 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1242 1 09/26/14 01:26 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1248 1 09/26/14 01:26 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1254 1 09/26/14 01:26 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1260 1 09/26/14 01:26 L213328VIC

Surrogate: Decachlorobiphenyl 47.2 Limits: 25-125% 09/26/14 01:261 VIC L213328

Surrogate: Tetrachloro-m-xylene 43.1 Limits: 25-125% 09/26/14 01:261 VIC L213328

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0400 mg/Kg 0.0400Acetone 1 09/22/14 19:01 L212859SEB

<0.100 mg/Kg 0.100Acetonitrile 1 09/22/14 19:01 L212859SEB

<0.0400 mg/Kg 0.0400Acrolein 1 09/22/14 19:01 L212859SEB

<0.0400 mg/Kg 0.0400Acrylonitrile 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Benzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Bromobenzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Bromochloromethane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Bromodichloromethane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Bromoform 1 09/22/14 19:01 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 64 of 119

Page 93: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-7 (8-12')

95408 Matrix:

9/18/2014 13:25

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Bromomethane 1 09/22/14 19:01 L212859SEB

<0.0400 mg/Kg 0.0400Methyl Ethyl Ketone (MEK) 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020n-Butylbenzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020sec-Butyl benzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020tert-Butyl benzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Disulfide 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Tetrachloride 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Chlorobenzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Chlorodibromomethane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Chloroethane 1 09/22/14 19:01 L212859SEB

<0.0020 M mg/Kg 0.00202-Chloroethylvinyl Ether 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Chloroform 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Chloromethane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00202-Chlorotoluene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00204-Chlorotoluene 1 09/22/14 19:01 L212859SEB

<0.0100 mg/Kg 0.01001,2-Dibromo-3-Chloropropane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dibromoethane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Dibromomethane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichlorobenzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichlorobenzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,4-Dichlorobenzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Dichlorodifluoromethane 1 09/22/14 19:01 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 65 of 119

Page 94: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-7 (8-12')

95408 Matrix:

9/18/2014 13:25

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.00201,1-Dichloroethane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloroethene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,2-Dichloroethene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,2-Dichloroethene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethene (Total) 1 09/22/14 19:01 L212859

<0.0020 mg/Kg 0.00201,2-Dichloropropane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichloropropane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00202,2-Dichloropropane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloropropene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,3-Dichloropropene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,3-Dichloropropene 1 09/22/14 19:01 L212859SEB

<0.0400 mg/Kg 0.0400Ethyl Acetate 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Ethylbenzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Hexachlorobutadiene 1 09/22/14 19:01 L212859SEB

<0.0100 mg/Kg 0.01002-Hexanone 1 09/22/14 19:01 L212859SEB

<0.0100 mg/Kg 0.0100Iodomethane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Isopropylbenzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00204-Isopropyl toluene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Methyl tert-butyl ether (MTBE) 1 09/22/14 19:01 L212859SEB

<0.0100 mg/Kg 0.01004-Methyl-2-Pentanone 1 09/22/14 19:01 L212859SEB

<0.0100 mg/Kg 0.0100Methylene Chloride 1 09/22/14 19:01 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 66 of 119

Page 95: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-7 (8-12')

95408 Matrix:

9/18/2014 13:25

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0100 mg/Kg 0.0100Naphthalene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020n-Propylbenzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Styrene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,1,1,2-Tetrachloroethane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,1,2,2-Tetrachloroethane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Tetrachloroethene 1 09/22/14 19:01 L212859SEB

<0.0100 mg/Kg 0.0100Toluene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichlorobenzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trichlorobenzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,1,1-Trichloroethane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,1,2-Trichloroethane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Trichloroethene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Trichlorofluoromethane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichloropropane 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trimethylbenzene 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.00201,3,5-Trimethylbenzene 1 09/22/14 19:01 L212859SEB

<0.0400 mg/Kg 0.0400Vinyl Acetate 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020Vinyl Chloride 1 09/22/14 19:01 L212859SEB

<0.0020 mg/Kg 0.0020o-Xylene 1 09/22/14 19:01 L212859SEB

<0.0040 mg/Kg 0.0040m,p-Xylene 1 09/22/14 19:01 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 67 of 119

Page 96: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-7 (8-12')

95408 Matrix:

9/18/2014 13:25

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Xylene (Total) 1 09/22/14 19:01 L212859

Surrogate: 4-Bromofluorobenzene 111 Limits: 60-130% 09/22/14 19:011 SEB L212859

Surrogate: 1,2-Dichloroethane - d4 118 Limits: 60-132% 09/22/14 19:011 SEB L212859

Surrogate: Toluene-d8 95.0 Limits: 70-122% 09/22/14 19:011 SEB L212859

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

0.243 mg/Kg 0.066Acenaphthene 1 09/25/14 14:49 L213162BMP

0.607 mg/Kg 0.066Acenaphthylene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Acetophenone 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Aniline 1 09/25/14 14:49 L213162BMP

0.286 mg/Kg 0.066Anthracene 1 09/25/14 14:49 L213162BMP

<0.670 mg/Kg 0.670Benzidine 1 09/25/14 14:49 L213162BMP

1.97 mg/Kg 0.066Benzo(a)anthracene 1 09/25/14 14:49 L213162BMP

2.36 mg/Kg 0.066Benzo(a)pyrene 1 09/25/14 14:49 L213162BMP

1.82 mg/Kg 0.066Benzo(b)fluoranthene 1 09/25/14 14:49 L213162BMP

1.21 mg/Kg 0.066Benzo(g,h,i)perylene 1 09/25/14 14:49 L213162BMP

0.862 mg/Kg 0.066Benzo(k)fluoranthene 1 09/25/14 14:49 L213162BMP

<0.330 mg/Kg 0.330Benzoic Acid 1 09/25/14 14:49 L213162BMP

<0.330 mg/Kg 0.330Benzyl alcohol 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroethoxy)methane 1 09/25/14 14:49 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 68 of 119

Page 97: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-7 (8-12')

95408 Matrix:

9/18/2014 13:25

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.170Bis(2-Chloroethyl)ether 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroisopropyl)ether 1 09/25/14 14:49 L213162BMP

<0.330 mg/Kg 0.330Bis(2-ethylhexyl)phthalate 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1704-Bromophenyl phenyl ether 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Butyl benzyl phthalate 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Carbazole 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1704-Chloro-3-methylphenol 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1704-Chloroaniline 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1702-Chloronaphthalene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1702-Chlorophenol 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1704-Chlorophenyl phenyl ether 1 09/25/14 14:49 L213162BMP

2.04 mg/Kg 0.066Chrysene 1 09/25/14 14:49 L213162BMP

0.257 mg/Kg 0.066Dibenz(a,h)anthracene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Dibenzofuran 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1701,2-Dichlorobenzene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1701,3-Dichlorobenzene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1701,4-Dichlorobenzene 1 09/25/14 14:49 L213162BMP

<0.330 mg/Kg 0.3303,3'-Dichlorobenzidine 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1702,4-Dichlorophenol 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1702,6-Dichlorophenol 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Diethyl phthalate 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Dimethyl phthalate 1 09/25/14 14:49 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 69 of 119

Page 98: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-7 (8-12')

95408 Matrix:

9/18/2014 13:25

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.330 mg/Kg 0.3303,3' Dimethylbenzidine 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1702,4-Dimethylphenol 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Di-n-butyl phthalate 1 09/25/14 14:49 L213162BMP

<0.330 mg/Kg 0.3304,6-Dinitro-2-methylphenol 1 09/25/14 14:49 L213162BMP

<1.67 mg/Kg 1.672,4-Dinitrophenol 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1702,4-Dinitrotoluene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1702,6-Dinitrotoluene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Di-n-Octyl Phthalate 1 09/25/14 14:49 L213162BMP

3.01 mg/Kg 0.066Fluoranthene 1 09/25/14 14:49 L213162BMP

0.250 mg/Kg 0.066Fluorene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobenzene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobutadiene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Hexachlorocyclopentadiene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Hexachloroethane 1 09/25/14 14:49 L213162BMP

1.14 mg/Kg 0.066Indeno(1,2,3-cd)pyrene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Isophorone 1 09/25/14 14:49 L213162BMP

0.311 mg/Kg 0.0662-Methylnaphthalene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1702-Methylphenol 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1703&4 Methylphenol 1 09/25/14 14:49 L213162BMP

0.845 mg/Kg 0.066Naphthalene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1702-Nitroaniline 1 09/25/14 14:49 L213162BMP

<0.330 mg/Kg 0.3303-Nitroaniline 1 09/25/14 14:49 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 70 of 119

Page 99: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-7 (8-12')

95408 Matrix:

9/18/2014 13:25

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1704-Nitroaniline 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Nitrobenzene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1702-Nitrophenol 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1704-Nitrophenol 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodimethylamine 1 09/25/14 14:49 L213162BMP

<0.330 mg/Kg 0.330N-Nitrosodiphenylamine 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodiethylamine 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-butylamine 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-propylamine 1 09/25/14 14:49 L213162BMP

<0.330 mg/Kg 0.330Pentachlorophenol 1 09/25/14 14:49 L213162BMP

0.746 mg/Kg 0.066Phenanthrene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.170Phenol 1 09/25/14 14:49 L213162BMP

5.85 mg/Kg 0.066Pyrene 1 09/25/14 14:49 L213162BMP

<0.330 mg/Kg 0.330Pyridine 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1701,2,4,5-Tetrachlorobenzene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1702,3,4,6-Tetrachlorophenol 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1701,2,4-Trichlorobenzene 1 09/25/14 14:49 L213162BMP

<0.170 mg/Kg 0.1702,4,5-Trichlorophenol 1 09/25/14 14:49 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 71 of 119

Page 100: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-7 (8-12')

95408 Matrix:

9/18/2014 13:25

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1702,4,6-Trichlorophenol 1 09/25/14 14:49 L213162BMP

Surrogate: 2-Fluorobiphenyl 61.7 Limits: 33-115% 09/25/14 14:491 BMP L213162

Surrogate: 2-Fluorophenol 58.6 Limits: 10-119% 09/25/14 14:491 BMP L213162

Surrogate: Nitrobenzene-d5 55.7 Limits: 29-110% 09/25/14 14:491 BMP L213162

Surrogate: Phenol-d6 61.2 Limits: 11-125% 09/25/14 14:491 BMP L213162

Surrogate: 4-Terphenyl-d14 72.3 Limits: 33-122% 09/25/14 14:491 BMP L213162

Surrogate: 2,4,6-Tribromophenol 84.8 Limits: 9-134% 09/25/14 14:491 BMP L213162

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 72 of 119

Page 101: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (0-4')

95409 Matrix:

9/18/2014 14:00

Solids

Test Results Units MQL By AnalyticalMethod

Date / TimeAnalyzed

DF

<1.00 mg/Kg 1.00Cyanide, Total 1 09/25/14 11:15 SW-9014EWB

7.1 s.u.pH 1 09/24/14 13:45 9045CSNS

<10.0 mg/Kg 10.0Sulfide 1 09/23/14 10:35 4500S2F-2011KM2

<0.500 mg/Kg 0.500Total Antimony 1 09/22/14 22:33 6010BBKN

5.87 mg/Kg 1.00Total Arsenic 1 09/22/14 22:33 6010BBKN

0.411 mg/Kg 0.0500Total Beryllium 1 09/22/14 22:33 6010BBKN

0.263 mg/Kg 0.100Total Cadmium 1 09/22/14 22:33 6010BBKN

7.64 mg/Kg 0.250Total Chromium 1 09/22/14 22:33 6010BBKN

34.3 mg/Kg 0.250Total Copper 1 09/22/14 22:33 6010BBKN

49.1 mg/Kg 0.300Total Lead 1 09/22/14 22:33 6010BBKN

0.100 mg/Kg 0.0133Mercury (Total) 1 09/22/14 13:33 7471AJRS

11.1 mg/Kg 0.250Total Nickel 1 09/23/14 18:52 6010BBKN

<1.00 mg/Kg 1.00Total Selenium 1 09/22/14 22:33 6010BBKN

<0.250 mg/Kg 0.250Total Silver 1 09/22/14 22:33 6010BBKN

<1.00 mg/Kg 1.00Total Thallium 1 09/22/14 22:33 6010BBKN

50.8 mg/Kg 0.500Total Zinc 1 09/22/14 22:33 6010BBKN

12.1 mg/Kg 10.0Sulfate 1 09/23/14 21:45 9056CGC

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Method Quantitation LimitMQLMinimum valueM

Page 73 of 119

Page 102: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (0-4')

95409 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8082

Prep Method: 3546 Date/Time Prepped: 9/25/2014 09:00:00Prep Batch(es): L213208

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0066 mg/Kg 0.0066Aroclor 1016 1 09/26/14 01:47 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1221 1 09/26/14 01:47 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1232 1 09/26/14 01:47 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1242 1 09/26/14 01:47 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1248 1 09/26/14 01:47 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1254 1 09/26/14 01:47 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1260 1 09/26/14 01:47 L213328VIC

Surrogate: Decachlorobiphenyl 27.3 Limits: 25-125% 09/26/14 01:471 VIC L213328

Surrogate: Tetrachloro-m-xylene 10.2 * Limits: 25-125% 09/26/14 01:471 VIC L213328

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0400 mg/Kg 0.0400Acetone 1 09/22/14 19:42 L212859SEB

<0.100 mg/Kg 0.100Acetonitrile 1 09/22/14 19:42 L212859SEB

<0.0400 mg/Kg 0.0400Acrolein 1 09/22/14 19:42 L212859SEB

<0.0400 mg/Kg 0.0400Acrylonitrile 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Benzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Bromobenzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Bromochloromethane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Bromodichloromethane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Bromoform 1 09/22/14 19:42 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 74 of 119

Page 103: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (0-4')

95409 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Bromomethane 1 09/22/14 19:42 L212859SEB

<0.0400 mg/Kg 0.0400Methyl Ethyl Ketone (MEK) 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020n-Butylbenzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020sec-Butyl benzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020tert-Butyl benzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Disulfide 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Tetrachloride 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Chlorobenzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Chlorodibromomethane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Chloroethane 1 09/22/14 19:42 L212859SEB

<0.0020 M mg/Kg 0.00202-Chloroethylvinyl Ether 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Chloroform 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Chloromethane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00202-Chlorotoluene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00204-Chlorotoluene 1 09/22/14 19:42 L212859SEB

<0.0100 mg/Kg 0.01001,2-Dibromo-3-Chloropropane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dibromoethane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Dibromomethane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichlorobenzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichlorobenzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,4-Dichlorobenzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Dichlorodifluoromethane 1 09/22/14 19:42 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 75 of 119

Page 104: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (0-4')

95409 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.00201,1-Dichloroethane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloroethene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,2-Dichloroethene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,2-Dichloroethene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethene (Total) 1 09/22/14 19:42 L212859

<0.0020 mg/Kg 0.00201,2-Dichloropropane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichloropropane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00202,2-Dichloropropane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloropropene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,3-Dichloropropene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,3-Dichloropropene 1 09/22/14 19:42 L212859SEB

<0.0400 mg/Kg 0.0400Ethyl Acetate 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Ethylbenzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Hexachlorobutadiene 1 09/22/14 19:42 L212859SEB

<0.0100 mg/Kg 0.01002-Hexanone 1 09/22/14 19:42 L212859SEB

<0.0100 mg/Kg 0.0100Iodomethane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Isopropylbenzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00204-Isopropyl toluene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Methyl tert-butyl ether (MTBE) 1 09/22/14 19:42 L212859SEB

<0.0100 mg/Kg 0.01004-Methyl-2-Pentanone 1 09/22/14 19:42 L212859SEB

<0.0100 mg/Kg 0.0100Methylene Chloride 1 09/22/14 19:42 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 76 of 119

Page 105: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (0-4')

95409 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0100 mg/Kg 0.0100Naphthalene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020n-Propylbenzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Styrene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,1,1,2-Tetrachloroethane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,1,2,2-Tetrachloroethane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Tetrachloroethene 1 09/22/14 19:42 L212859SEB

<0.0100 mg/Kg 0.0100Toluene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichlorobenzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trichlorobenzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,1,1-Trichloroethane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,1,2-Trichloroethane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Trichloroethene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Trichlorofluoromethane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichloropropane 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trimethylbenzene 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.00201,3,5-Trimethylbenzene 1 09/22/14 19:42 L212859SEB

<0.0400 mg/Kg 0.0400Vinyl Acetate 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020Vinyl Chloride 1 09/22/14 19:42 L212859SEB

<0.0020 mg/Kg 0.0020o-Xylene 1 09/22/14 19:42 L212859SEB

<0.0040 mg/Kg 0.0040m,p-Xylene 1 09/22/14 19:42 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 77 of 119

Page 106: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (0-4')

95409 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Xylene (Total) 1 09/22/14 19:42 L212859

Surrogate: 4-Bromofluorobenzene 99.4 Limits: 60-130% 09/22/14 19:421 SEB L212859

Surrogate: 1,2-Dichloroethane - d4 114 Limits: 60-132% 09/22/14 19:421 SEB L212859

Surrogate: Toluene-d8 83.1 Limits: 70-122% 09/22/14 19:421 SEB L212859

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

0.543 mg/Kg 0.066Acenaphthene 1 09/25/14 15:23 L213162BMP

0.805 mg/Kg 0.066Acenaphthylene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Acetophenone 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Aniline 1 09/25/14 15:23 L213162BMP

0.961 mg/Kg 0.066Anthracene 1 09/25/14 15:23 L213162BMP

<0.670 mg/Kg 0.670Benzidine 1 09/25/14 15:23 L213162BMP

4.70 mg/Kg 0.066Benzo(a)anthracene 1 09/25/14 15:23 L213162BMP

4.59 mg/Kg 0.066Benzo(a)pyrene 1 09/25/14 15:23 L213162BMP

4.79 mg/Kg 0.667Benzo(b)fluoranthene 10 09/25/14 15:59 L213162BMP

2.83 mg/Kg 0.066Benzo(g,h,i)perylene 1 09/25/14 15:23 L213162BMP

2.43 mg/Kg 0.066Benzo(k)fluoranthene 1 09/25/14 15:23 L213162BMP

<0.330 mg/Kg 0.330Benzoic Acid 1 09/25/14 15:23 L213162BMP

<0.330 mg/Kg 0.330Benzyl alcohol 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroethoxy)methane 1 09/25/14 15:23 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 78 of 119

Page 107: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (0-4')

95409 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.170Bis(2-Chloroethyl)ether 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroisopropyl)ether 1 09/25/14 15:23 L213162BMP

<0.330 mg/Kg 0.330Bis(2-ethylhexyl)phthalate 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1704-Bromophenyl phenyl ether 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Butyl benzyl phthalate 1 09/25/14 15:23 L213162BMP

0.510 mg/Kg 0.170Carbazole 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1704-Chloro-3-methylphenol 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1704-Chloroaniline 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1702-Chloronaphthalene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1702-Chlorophenol 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1704-Chlorophenyl phenyl ether 1 09/25/14 15:23 L213162BMP

4.92 mg/Kg 0.066Chrysene 1 09/25/14 15:23 L213162BMP

0.656 mg/Kg 0.066Dibenz(a,h)anthracene 1 09/25/14 15:23 L213162BMP

0.280 mg/Kg 0.170Dibenzofuran 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1701,2-Dichlorobenzene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1701,3-Dichlorobenzene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1701,4-Dichlorobenzene 1 09/25/14 15:23 L213162BMP

<0.330 mg/Kg 0.3303,3'-Dichlorobenzidine 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1702,4-Dichlorophenol 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1702,6-Dichlorophenol 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Diethyl phthalate 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Dimethyl phthalate 1 09/25/14 15:23 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 79 of 119

Page 108: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (0-4')

95409 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.330 mg/Kg 0.3303,3' Dimethylbenzidine 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1702,4-Dimethylphenol 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Di-n-butyl phthalate 1 09/25/14 15:23 L213162BMP

<0.330 mg/Kg 0.3304,6-Dinitro-2-methylphenol 1 09/25/14 15:23 L213162BMP

<1.67 mg/Kg 1.672,4-Dinitrophenol 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1702,4-Dinitrotoluene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1702,6-Dinitrotoluene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Di-n-Octyl Phthalate 1 09/25/14 15:23 L213162BMP

5.46 mg/Kg 0.066Fluoranthene 1 09/25/14 15:23 L213162BMP

0.422 mg/Kg 0.066Fluorene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobenzene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobutadiene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Hexachlorocyclopentadiene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Hexachloroethane 1 09/25/14 15:23 L213162BMP

2.48 mg/Kg 0.066Indeno(1,2,3-cd)pyrene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Isophorone 1 09/25/14 15:23 L213162BMP

0.420 mg/Kg 0.0662-Methylnaphthalene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1702-Methylphenol 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1703&4 Methylphenol 1 09/25/14 15:23 L213162BMP

0.984 mg/Kg 0.066Naphthalene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1702-Nitroaniline 1 09/25/14 15:23 L213162BMP

<0.330 mg/Kg 0.3303-Nitroaniline 1 09/25/14 15:23 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 80 of 119

Page 109: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (0-4')

95409 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1704-Nitroaniline 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Nitrobenzene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1702-Nitrophenol 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1704-Nitrophenol 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodimethylamine 1 09/25/14 15:23 L213162BMP

<0.330 mg/Kg 0.330N-Nitrosodiphenylamine 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodiethylamine 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-butylamine 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-propylamine 1 09/25/14 15:23 L213162BMP

<0.330 mg/Kg 0.330Pentachlorophenol 1 09/25/14 15:23 L213162BMP

3.70 mg/Kg 0.066Phenanthrene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.170Phenol 1 09/25/14 15:23 L213162BMP

8.09 mg/Kg 0.667Pyrene 10 09/25/14 15:59 L213162BMP

<0.330 mg/Kg 0.330Pyridine 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1701,2,4,5-Tetrachlorobenzene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1702,3,4,6-Tetrachlorophenol 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1701,2,4-Trichlorobenzene 1 09/25/14 15:23 L213162BMP

<0.170 mg/Kg 0.1702,4,5-Trichlorophenol 1 09/25/14 15:23 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 81 of 119

Page 110: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (0-4')

95409 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1702,4,6-Trichlorophenol 1 09/25/14 15:23 L213162BMP

Surrogate: 2-Fluorobiphenyl 60.4 Limits: 33-115% 09/25/14 15:231 BMP L213162

Surrogate: 2-Fluorophenol 52.4 Limits: 10-119% 09/25/14 15:231 BMP L213162

Surrogate: Nitrobenzene-d5 56.4 Limits: 29-110% 09/25/14 15:231 BMP L213162

Surrogate: Phenol-d6 57.5 Limits: 11-125% 09/25/14 15:231 BMP L213162

Surrogate: 4-Terphenyl-d14 73.8 Limits: 33-122% 09/25/14 15:231 BMP L213162

Surrogate: 2,4,6-Tribromophenol 76.0 Limits: 9-134% 09/25/14 15:231 BMP L213162

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 82 of 119

Page 111: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (20-24')

95410 Matrix:

9/18/2014 14:00

Solids

Test Results Units MQL By AnalyticalMethod

Date / TimeAnalyzed

DF

<1.00 mg/Kg 1.00Cyanide, Total 1 09/25/14 11:15 SW-9014EWB

6.8 s.u.pH 1 09/24/14 13:45 9045CSNS

<10.0 mg/Kg 10.0Sulfide 1 09/23/14 10:35 4500S2F-2011KM2

<0.500 mg/Kg 0.500Total Antimony 1 09/22/14 22:38 6010BBKN

6.65 mg/Kg 1.00Total Arsenic 1 09/22/14 22:38 6010BBKN

0.303 mg/Kg 0.0500Total Beryllium 1 09/22/14 22:38 6010BBKN

0.144 mg/Kg 0.100Total Cadmium 1 09/22/14 22:38 6010BBKN

7.52 mg/Kg 0.250Total Chromium 1 09/22/14 22:38 6010BBKN

11.0 mg/Kg 0.250Total Copper 1 09/22/14 22:38 6010BBKN

46.1 mg/Kg 0.300Total Lead 1 09/22/14 22:38 6010BBKN

<0.0133 mg/Kg 0.0133Mercury (Total) 1 09/22/14 13:35 7471AJRS

11.3 mg/Kg 0.250Total Nickel 1 09/23/14 18:56 6010BBKN

<1.00 mg/Kg 1.00Total Selenium 1 09/22/14 22:38 6010BBKN

<0.250 mg/Kg 0.250Total Silver 1 09/22/14 22:38 6010BBKN

<1.00 mg/Kg 1.00Total Thallium 1 09/22/14 22:38 6010BBKN

32.0 mg/Kg 0.500Total Zinc 1 09/22/14 22:38 6010BBKN

14.0 mg/Kg 10.0Sulfate 1 09/23/14 22:02 9056CGC

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Method Quantitation LimitMQLMinimum valueM

Page 83 of 119

Page 112: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (20-24')

95410 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8082

Prep Method: 3546 Date/Time Prepped: 9/25/2014 09:00:00Prep Batch(es): L213208

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0066 mg/Kg 0.0066Aroclor 1016 1 09/26/14 02:07 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1221 1 09/26/14 02:07 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1232 1 09/26/14 02:07 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1242 1 09/26/14 02:07 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1248 1 09/26/14 02:07 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1254 1 09/26/14 02:07 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1260 1 09/26/14 02:07 L213328VIC

Surrogate: Decachlorobiphenyl 51.8 Limits: 25-125% 09/26/14 02:071 VIC L213328

Surrogate: Tetrachloro-m-xylene 44.3 Limits: 25-125% 09/26/14 02:071 VIC L213328

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0400 mg/Kg 0.0400Acetone 1 09/22/14 20:23 L212859SEB

<0.100 mg/Kg 0.100Acetonitrile 1 09/22/14 20:23 L212859SEB

<0.0400 mg/Kg 0.0400Acrolein 1 09/22/14 20:23 L212859SEB

<0.0400 mg/Kg 0.0400Acrylonitrile 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Benzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Bromobenzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Bromochloromethane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Bromodichloromethane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Bromoform 1 09/22/14 20:23 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 84 of 119

Page 113: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (20-24')

95410 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Bromomethane 1 09/22/14 20:23 L212859SEB

<0.0400 mg/Kg 0.0400Methyl Ethyl Ketone (MEK) 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020n-Butylbenzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020sec-Butyl benzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020tert-Butyl benzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Disulfide 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Carbon Tetrachloride 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Chlorobenzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Chlorodibromomethane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Chloroethane 1 09/22/14 20:23 L212859SEB

<0.0020 M mg/Kg 0.00202-Chloroethylvinyl Ether 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Chloroform 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Chloromethane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00202-Chlorotoluene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00204-Chlorotoluene 1 09/22/14 20:23 L212859SEB

<0.0100 mg/Kg 0.01001,2-Dibromo-3-Chloropropane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dibromoethane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Dibromomethane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichlorobenzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichlorobenzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,4-Dichlorobenzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Dichlorodifluoromethane 1 09/22/14 20:23 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 85 of 119

Page 114: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (20-24')

95410 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.00201,1-Dichloroethane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloroethene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,2-Dichloroethene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,2-Dichloroethene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethene (Total) 1 09/22/14 20:23 L212859

<0.0020 mg/Kg 0.00201,2-Dichloropropane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,3-Dichloropropane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00202,2-Dichloropropane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,1-Dichloropropene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020cis-1,3-Dichloropropene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020trans-1,3-Dichloropropene 1 09/22/14 20:23 L212859SEB

<0.0400 mg/Kg 0.0400Ethyl Acetate 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Ethylbenzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Hexachlorobutadiene 1 09/22/14 20:23 L212859SEB

<0.0100 mg/Kg 0.01002-Hexanone 1 09/22/14 20:23 L212859SEB

<0.0100 mg/Kg 0.0100Iodomethane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Isopropylbenzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00204-Isopropyl toluene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Methyl tert-butyl ether (MTBE) 1 09/22/14 20:23 L212859SEB

<0.0100 mg/Kg 0.01004-Methyl-2-Pentanone 1 09/22/14 20:23 L212859SEB

<0.0100 mg/Kg 0.0100Methylene Chloride 1 09/22/14 20:23 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 86 of 119

Page 115: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (20-24')

95410 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0100 mg/Kg 0.0100Naphthalene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020n-Propylbenzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Styrene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,1,1,2-Tetrachloroethane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,1,2,2-Tetrachloroethane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Tetrachloroethene 1 09/22/14 20:23 L212859SEB

<0.0100 mg/Kg 0.0100Toluene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichlorobenzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trichlorobenzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,1,1-Trichloroethane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,1,2-Trichloroethane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Trichloroethene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Trichlorofluoromethane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,2,3-Trichloropropane 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,2,4-Trimethylbenzene 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.00201,3,5-Trimethylbenzene 1 09/22/14 20:23 L212859SEB

<0.0400 mg/Kg 0.0400Vinyl Acetate 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020Vinyl Chloride 1 09/22/14 20:23 L212859SEB

<0.0020 mg/Kg 0.0020o-Xylene 1 09/22/14 20:23 L212859SEB

<0.0040 mg/Kg 0.0040m,p-Xylene 1 09/22/14 20:23 L212859SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 87 of 119

Page 116: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (20-24')

95410 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/22/2014 10:22:00Prep Batch(es): L212857

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Xylene (Total) 1 09/22/14 20:23 L212859

Surrogate: 4-Bromofluorobenzene 102 Limits: 60-130% 09/22/14 20:231 SEB L212859

Surrogate: 1,2-Dichloroethane - d4 115 Limits: 60-132% 09/22/14 20:231 SEB L212859

Surrogate: Toluene-d8 102 Limits: 70-122% 09/22/14 20:231 SEB L212859

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.066 mg/Kg 0.066Acenaphthene 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Acenaphthylene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Acetophenone 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Aniline 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Anthracene 1 09/25/14 16:35 L213162BMP

<0.670 mg/Kg 0.670Benzidine 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)anthracene 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)pyrene 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Benzo(b)fluoranthene 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Benzo(g,h,i)perylene 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Benzo(k)fluoranthene 1 09/25/14 16:35 L213162BMP

<0.330 mg/Kg 0.330Benzoic Acid 1 09/25/14 16:35 L213162BMP

<0.330 mg/Kg 0.330Benzyl alcohol 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroethoxy)methane 1 09/25/14 16:35 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 88 of 119

Page 117: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (20-24')

95410 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.170Bis(2-Chloroethyl)ether 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroisopropyl)ether 1 09/25/14 16:35 L213162BMP

<0.330 mg/Kg 0.330Bis(2-ethylhexyl)phthalate 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1704-Bromophenyl phenyl ether 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Butyl benzyl phthalate 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Carbazole 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1704-Chloro-3-methylphenol 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1704-Chloroaniline 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1702-Chloronaphthalene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1702-Chlorophenol 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1704-Chlorophenyl phenyl ether 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Chrysene 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Dibenz(a,h)anthracene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Dibenzofuran 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1701,2-Dichlorobenzene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1701,3-Dichlorobenzene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1701,4-Dichlorobenzene 1 09/25/14 16:35 L213162BMP

<0.330 mg/Kg 0.3303,3'-Dichlorobenzidine 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1702,4-Dichlorophenol 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1702,6-Dichlorophenol 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Diethyl phthalate 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Dimethyl phthalate 1 09/25/14 16:35 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 89 of 119

Page 118: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (20-24')

95410 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.330 mg/Kg 0.3303,3' Dimethylbenzidine 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1702,4-Dimethylphenol 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Di-n-butyl phthalate 1 09/25/14 16:35 L213162BMP

<0.330 mg/Kg 0.3304,6-Dinitro-2-methylphenol 1 09/25/14 16:35 L213162BMP

<1.67 mg/Kg 1.672,4-Dinitrophenol 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1702,4-Dinitrotoluene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1702,6-Dinitrotoluene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Di-n-Octyl Phthalate 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Fluoranthene 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Fluorene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobenzene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobutadiene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Hexachlorocyclopentadiene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Hexachloroethane 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Indeno(1,2,3-cd)pyrene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Isophorone 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.0662-Methylnaphthalene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1702-Methylphenol 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1703&4 Methylphenol 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Naphthalene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1702-Nitroaniline 1 09/25/14 16:35 L213162BMP

<0.330 mg/Kg 0.3303-Nitroaniline 1 09/25/14 16:35 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 90 of 119

Page 119: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (20-24')

95410 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1704-Nitroaniline 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Nitrobenzene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1702-Nitrophenol 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1704-Nitrophenol 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodimethylamine 1 09/25/14 16:35 L213162BMP

<0.330 mg/Kg 0.330N-Nitrosodiphenylamine 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodiethylamine 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-butylamine 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-propylamine 1 09/25/14 16:35 L213162BMP

<0.330 mg/Kg 0.330Pentachlorophenol 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Phenanthrene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.170Phenol 1 09/25/14 16:35 L213162BMP

<0.066 mg/Kg 0.066Pyrene 1 09/25/14 16:35 L213162BMP

<0.330 mg/Kg 0.330Pyridine 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1701,2,4,5-Tetrachlorobenzene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1702,3,4,6-Tetrachlorophenol 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1701,2,4-Trichlorobenzene 1 09/25/14 16:35 L213162BMP

<0.170 mg/Kg 0.1702,4,5-Trichlorophenol 1 09/25/14 16:35 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 91 of 119

Page 120: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-8 (20-24')

95410 Matrix:

9/18/2014 14:00

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1702,4,6-Trichlorophenol 1 09/25/14 16:35 L213162BMP

Surrogate: 2-Fluorobiphenyl 52.9 Limits: 33-115% 09/25/14 16:351 BMP L213162

Surrogate: 2-Fluorophenol 49.6 Limits: 10-119% 09/25/14 16:351 BMP L213162

Surrogate: Nitrobenzene-d5 48.3 Limits: 29-110% 09/25/14 16:351 BMP L213162

Surrogate: Phenol-d6 48.9 Limits: 11-125% 09/25/14 16:351 BMP L213162

Surrogate: 4-Terphenyl-d14 59.9 Limits: 33-122% 09/25/14 16:351 BMP L213162

Surrogate: 2,4,6-Tribromophenol 66.8 Limits: 9-134% 09/25/14 16:351 BMP L213162

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 92 of 119

Page 121: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-9 (20-24')

95411 Matrix:

9/18/2014 14:50

Solids

Test Results Units MQL By AnalyticalMethod

Date / TimeAnalyzed

DF

<1.00 mg/Kg 1.00Cyanide, Total 1 09/25/14 11:15 SW-9014EWB

6.3 s.u.pH 1 09/24/14 13:45 9045CSNS

<10.0 mg/Kg 10.0Sulfide 1 09/23/14 10:35 4500S2F-2011KM2

<0.500 mg/Kg 0.500Total Antimony 1 09/22/14 22:43 6010BBKN

4.24 mg/Kg 1.00Total Arsenic 1 09/22/14 22:43 6010BBKN

0.385 mg/Kg 0.0500Total Beryllium 1 09/22/14 22:43 6010BBKN

<0.100 mg/Kg 0.100Total Cadmium 1 09/22/14 22:43 6010BBKN

9.59 mg/Kg 0.250Total Chromium 1 09/22/14 22:43 6010BBKN

8.56 mg/Kg 0.250Total Copper 1 09/22/14 22:43 6010BBKN

6.49 mg/Kg 0.300Total Lead 1 09/22/14 22:43 6010BBKN

0.0163 mg/Kg 0.0133Mercury (Total) 1 09/22/14 13:37 7471AJRS

10.0 mg/Kg 0.250Total Nickel 1 09/23/14 19:01 6010BBKN

<1.00 mg/Kg 1.00Total Selenium 1 09/22/14 22:43 6010BBKN

<0.250 mg/Kg 0.250Total Silver 1 09/22/14 22:43 6010BBKN

<1.00 mg/Kg 1.00Total Thallium 1 09/22/14 22:43 6010BBKN

25.3 mg/Kg 0.500Total Zinc 1 09/22/14 22:43 6010BBKN

29.8 mg/Kg 10.0Sulfate 1 09/23/14 22:20 9056CGC

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Method Quantitation LimitMQLMinimum valueM

Page 93 of 119

Page 122: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-9 (20-24')

95411 Matrix:

9/18/2014 14:50

Solids

Analytical Method: 8082

Prep Method: 3546 Date/Time Prepped: 9/25/2014 09:00:00Prep Batch(es): L213208

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0066 mg/Kg 0.0066Aroclor 1016 1 09/26/14 02:27 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1221 1 09/26/14 02:27 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1232 1 09/26/14 02:27 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1242 1 09/26/14 02:27 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1248 1 09/26/14 02:27 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1254 1 09/26/14 02:27 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1260 1 09/26/14 02:27 L213328VIC

Surrogate: Decachlorobiphenyl 40.8 Limits: 25-125% 09/26/14 02:271 VIC L213328

Surrogate: Tetrachloro-m-xylene 45.5 Limits: 25-125% 09/26/14 02:271 VIC L213328

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/23/2014 09:22:00Prep Batch(es): L212904

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0400 mg/Kg 0.0400Acetone 1 09/23/14 14:47 L212905SEB

<0.100 mg/Kg 0.100Acetonitrile 1 09/23/14 14:47 L212905SEB

<0.0400 mg/Kg 0.0400Acrolein 1 09/23/14 14:47 L212905SEB

<0.0400 mg/Kg 0.0400Acrylonitrile 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Benzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Bromobenzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Bromochloromethane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Bromodichloromethane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Bromoform 1 09/23/14 14:47 L212905SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 94 of 119

Page 123: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-9 (20-24')

95411 Matrix:

9/18/2014 14:50

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/23/2014 09:22:00Prep Batch(es): L212904

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Bromomethane 1 09/23/14 14:47 L212905SEB

<0.0400 mg/Kg 0.0400Methyl Ethyl Ketone (MEK) 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020n-Butylbenzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020sec-Butyl benzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020tert-Butyl benzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Carbon Disulfide 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Carbon Tetrachloride 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Chlorobenzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Chlorodibromomethane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Chloroethane 1 09/23/14 14:47 L212905SEB

<0.0020 M mg/Kg 0.00202-Chloroethylvinyl Ether 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Chloroform 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Chloromethane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00202-Chlorotoluene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00204-Chlorotoluene 1 09/23/14 14:47 L212905SEB

<0.0100 mg/Kg 0.01001,2-Dibromo-3-Chloropropane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,2-Dibromoethane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Dibromomethane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,2-Dichlorobenzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,3-Dichlorobenzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,4-Dichlorobenzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Dichlorodifluoromethane 1 09/23/14 14:47 L212905SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 95 of 119

Page 124: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-9 (20-24')

95411 Matrix:

9/18/2014 14:50

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/23/2014 09:22:00Prep Batch(es): L212904

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.00201,1-Dichloroethane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,1-Dichloroethene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020cis-1,2-Dichloroethene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020trans-1,2-Dichloroethene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethene (Total) 1 09/23/14 14:47 L212905

<0.0020 mg/Kg 0.00201,2-Dichloropropane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,3-Dichloropropane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00202,2-Dichloropropane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,1-Dichloropropene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020cis-1,3-Dichloropropene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020trans-1,3-Dichloropropene 1 09/23/14 14:47 L212905SEB

<0.0400 mg/Kg 0.0400Ethyl Acetate 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Ethylbenzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Hexachlorobutadiene 1 09/23/14 14:47 L212905SEB

<0.0100 mg/Kg 0.01002-Hexanone 1 09/23/14 14:47 L212905SEB

<0.0100 mg/Kg 0.0100Iodomethane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Isopropylbenzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00204-Isopropyl toluene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Methyl tert-butyl ether (MTBE) 1 09/23/14 14:47 L212905SEB

<0.0100 mg/Kg 0.01004-Methyl-2-Pentanone 1 09/23/14 14:47 L212905SEB

<0.0100 mg/Kg 0.0100Methylene Chloride 1 09/23/14 14:47 L212905SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 96 of 119

Page 125: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-9 (20-24')

95411 Matrix:

9/18/2014 14:50

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/23/2014 09:22:00Prep Batch(es): L212904

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0100 mg/Kg 0.0100Naphthalene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020n-Propylbenzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Styrene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,1,1,2-Tetrachloroethane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,1,2,2-Tetrachloroethane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Tetrachloroethene 1 09/23/14 14:47 L212905SEB

<0.0100 mg/Kg 0.0100Toluene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,2,3-Trichlorobenzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,2,4-Trichlorobenzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,1,1-Trichloroethane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,1,2-Trichloroethane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Trichloroethene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Trichlorofluoromethane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,2,3-Trichloropropane 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,2,4-Trimethylbenzene 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.00201,3,5-Trimethylbenzene 1 09/23/14 14:47 L212905SEB

<0.0400 mg/Kg 0.0400Vinyl Acetate 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020Vinyl Chloride 1 09/23/14 14:47 L212905SEB

<0.0020 mg/Kg 0.0020o-Xylene 1 09/23/14 14:47 L212905SEB

<0.0040 mg/Kg 0.0040m,p-Xylene 1 09/23/14 14:47 L212905SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 97 of 119

Page 126: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-9 (20-24')

95411 Matrix:

9/18/2014 14:50

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/23/2014 09:22:00Prep Batch(es): L212904

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Xylene (Total) 1 09/23/14 14:47 L212905

Surrogate: 4-Bromofluorobenzene 103 Limits: 60-130% 09/23/14 14:471 SEB L212905

Surrogate: 1,2-Dichloroethane - d4 109 Limits: 60-132% 09/23/14 14:471 SEB L212905

Surrogate: Toluene-d8 102 Limits: 70-122% 09/23/14 14:471 SEB L212905

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.066 mg/Kg 0.066Acenaphthene 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Acenaphthylene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Acetophenone 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Aniline 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Anthracene 1 09/25/14 17:11 L213162BMP

<0.670 mg/Kg 0.670Benzidine 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)anthracene 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)pyrene 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Benzo(b)fluoranthene 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Benzo(g,h,i)perylene 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Benzo(k)fluoranthene 1 09/25/14 17:11 L213162BMP

<0.330 mg/Kg 0.330Benzoic Acid 1 09/25/14 17:11 L213162BMP

<0.330 mg/Kg 0.330Benzyl alcohol 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroethoxy)methane 1 09/25/14 17:11 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 98 of 119

Page 127: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-9 (20-24')

95411 Matrix:

9/18/2014 14:50

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.170Bis(2-Chloroethyl)ether 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroisopropyl)ether 1 09/25/14 17:11 L213162BMP

<0.330 mg/Kg 0.330Bis(2-ethylhexyl)phthalate 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1704-Bromophenyl phenyl ether 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Butyl benzyl phthalate 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Carbazole 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1704-Chloro-3-methylphenol 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1704-Chloroaniline 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1702-Chloronaphthalene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1702-Chlorophenol 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1704-Chlorophenyl phenyl ether 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Chrysene 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Dibenz(a,h)anthracene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Dibenzofuran 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1701,2-Dichlorobenzene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1701,3-Dichlorobenzene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1701,4-Dichlorobenzene 1 09/25/14 17:11 L213162BMP

<0.330 mg/Kg 0.3303,3'-Dichlorobenzidine 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1702,4-Dichlorophenol 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1702,6-Dichlorophenol 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Diethyl phthalate 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Dimethyl phthalate 1 09/25/14 17:11 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 99 of 119

Page 128: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-9 (20-24')

95411 Matrix:

9/18/2014 14:50

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.330 mg/Kg 0.3303,3' Dimethylbenzidine 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1702,4-Dimethylphenol 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Di-n-butyl phthalate 1 09/25/14 17:11 L213162BMP

<0.330 mg/Kg 0.3304,6-Dinitro-2-methylphenol 1 09/25/14 17:11 L213162BMP

<1.67 mg/Kg 1.672,4-Dinitrophenol 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1702,4-Dinitrotoluene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1702,6-Dinitrotoluene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Di-n-Octyl Phthalate 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Fluoranthene 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Fluorene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobenzene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobutadiene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Hexachlorocyclopentadiene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Hexachloroethane 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Indeno(1,2,3-cd)pyrene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Isophorone 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.0662-Methylnaphthalene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1702-Methylphenol 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1703&4 Methylphenol 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Naphthalene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1702-Nitroaniline 1 09/25/14 17:11 L213162BMP

<0.330 mg/Kg 0.3303-Nitroaniline 1 09/25/14 17:11 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 100 of 119

Page 129: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-9 (20-24')

95411 Matrix:

9/18/2014 14:50

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1704-Nitroaniline 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Nitrobenzene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1702-Nitrophenol 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1704-Nitrophenol 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodimethylamine 1 09/25/14 17:11 L213162BMP

<0.330 mg/Kg 0.330N-Nitrosodiphenylamine 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodiethylamine 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-butylamine 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-propylamine 1 09/25/14 17:11 L213162BMP

<0.330 mg/Kg 0.330Pentachlorophenol 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Phenanthrene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.170Phenol 1 09/25/14 17:11 L213162BMP

<0.066 mg/Kg 0.066Pyrene 1 09/25/14 17:11 L213162BMP

<0.330 mg/Kg 0.330Pyridine 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1701,2,4,5-Tetrachlorobenzene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1702,3,4,6-Tetrachlorophenol 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1701,2,4-Trichlorobenzene 1 09/25/14 17:11 L213162BMP

<0.170 mg/Kg 0.1702,4,5-Trichlorophenol 1 09/25/14 17:11 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 101 of 119

Page 130: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-9 (20-24')

95411 Matrix:

9/18/2014 14:50

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1702,4,6-Trichlorophenol 1 09/25/14 17:11 L213162BMP

Surrogate: 2-Fluorobiphenyl 57.7 Limits: 33-115% 09/25/14 17:111 BMP L213162

Surrogate: 2-Fluorophenol 53.5 Limits: 10-119% 09/25/14 17:111 BMP L213162

Surrogate: Nitrobenzene-d5 52.2 Limits: 29-110% 09/25/14 17:111 BMP L213162

Surrogate: Phenol-d6 56.1 Limits: 11-125% 09/25/14 17:111 BMP L213162

Surrogate: 4-Terphenyl-d14 76.2 Limits: 33-122% 09/25/14 17:111 BMP L213162

Surrogate: 2,4,6-Tribromophenol 77.7 Limits: 9-134% 09/25/14 17:111 BMP L213162

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 102 of 119

Page 131: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-10 (12-16')

95412 Matrix:

9/18/2014 16:15

Solids

Test Results Units MQL By AnalyticalMethod

Date / TimeAnalyzed

DF

<1.00 mg/Kg 1.00Cyanide, Total 1 09/25/14 11:15 SW-9014EWB

6.5 s.u.pH 1 09/24/14 13:45 9045CSNS

<10.0 mg/Kg 10.0Sulfide 1 09/23/14 10:35 4500S2F-2011KM2

<0.500 mg/Kg 0.500Total Antimony 1 09/22/14 22:47 6010BBKN

6.81 mg/Kg 1.00Total Arsenic 1 09/22/14 22:47 6010BBKN

0.314 mg/Kg 0.0500Total Beryllium 1 09/22/14 22:47 6010BBKN

0.133 mg/Kg 0.100Total Cadmium 1 09/22/14 22:47 6010BBKN

7.94 mg/Kg 0.250Total Chromium 1 09/22/14 22:47 6010BBKN

11.7 mg/Kg 0.250Total Copper 1 09/22/14 22:47 6010BBKN

6.55 mg/Kg 0.300Total Lead 1 09/22/14 22:47 6010BBKN

0.0237 mg/Kg 0.0133Mercury (Total) 1 09/22/14 13:39 7471AJRS

11.5 mg/Kg 0.250Total Nickel 1 09/23/14 19:06 6010BBKN

<1.00 mg/Kg 1.00Total Selenium 1 09/22/14 22:47 6010BBKN

<0.250 mg/Kg 0.250Total Silver 1 09/22/14 22:47 6010BBKN

<1.00 mg/Kg 1.00Total Thallium 1 09/22/14 22:47 6010BBKN

32.6 mg/Kg 0.500Total Zinc 1 09/22/14 22:47 6010BBKN

<10.0 mg/Kg 10.0Sulfate 1 09/23/14 22:37 9056CGC

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Method Quantitation LimitMQLMinimum valueM

Page 103 of 119

Page 132: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-10 (12-16')

95412 Matrix:

9/18/2014 16:15

Solids

Analytical Method: 8082

Prep Method: 3546 Date/Time Prepped: 9/25/2014 09:00:00Prep Batch(es): L213208

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0066 mg/Kg 0.0066Aroclor 1016 1 09/26/14 02:48 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1221 1 09/26/14 02:48 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1232 1 09/26/14 02:48 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1242 1 09/26/14 02:48 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1248 1 09/26/14 02:48 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1254 1 09/26/14 02:48 L213328VIC

<0.0066 mg/Kg 0.0066Aroclor 1260 1 09/26/14 02:48 L213328VIC

Surrogate: Decachlorobiphenyl 45.9 Limits: 25-125% 09/26/14 02:481 VIC L213328

Surrogate: Tetrachloro-m-xylene 54.5 Limits: 25-125% 09/26/14 02:481 VIC L213328

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/23/2014 09:22:00Prep Batch(es): L212904

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0400 mg/Kg 0.0400Acetone 1 09/23/14 15:28 L212905SEB

<0.100 mg/Kg 0.100Acetonitrile 1 09/23/14 15:28 L212905SEB

<0.0400 mg/Kg 0.0400Acrolein 1 09/23/14 15:28 L212905SEB

<0.0400 mg/Kg 0.0400Acrylonitrile 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Benzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Bromobenzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Bromochloromethane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Bromodichloromethane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Bromoform 1 09/23/14 15:28 L212905SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 104 of 119

Page 133: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-10 (12-16')

95412 Matrix:

9/18/2014 16:15

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/23/2014 09:22:00Prep Batch(es): L212904

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Bromomethane 1 09/23/14 15:28 L212905SEB

<0.0400 mg/Kg 0.0400Methyl Ethyl Ketone (MEK) 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020n-Butylbenzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020sec-Butyl benzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020tert-Butyl benzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Carbon Disulfide 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Carbon Tetrachloride 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Chlorobenzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Chlorodibromomethane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Chloroethane 1 09/23/14 15:28 L212905SEB

<0.0020 M mg/Kg 0.00202-Chloroethylvinyl Ether 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Chloroform 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Chloromethane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00202-Chlorotoluene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00204-Chlorotoluene 1 09/23/14 15:28 L212905SEB

<0.0100 mg/Kg 0.01001,2-Dibromo-3-Chloropropane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,2-Dibromoethane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Dibromomethane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,2-Dichlorobenzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,3-Dichlorobenzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,4-Dichlorobenzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Dichlorodifluoromethane 1 09/23/14 15:28 L212905SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 105 of 119

Page 134: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-10 (12-16')

95412 Matrix:

9/18/2014 16:15

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/23/2014 09:22:00Prep Batch(es): L212904

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.00201,1-Dichloroethane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,1-Dichloroethene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020cis-1,2-Dichloroethene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020trans-1,2-Dichloroethene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,2-Dichloroethene (Total) 1 09/23/14 15:28 L212905

<0.0020 mg/Kg 0.00201,2-Dichloropropane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,3-Dichloropropane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00202,2-Dichloropropane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,1-Dichloropropene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020cis-1,3-Dichloropropene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020trans-1,3-Dichloropropene 1 09/23/14 15:28 L212905SEB

<0.0400 mg/Kg 0.0400Ethyl Acetate 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Ethylbenzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Hexachlorobutadiene 1 09/23/14 15:28 L212905SEB

<0.0100 mg/Kg 0.01002-Hexanone 1 09/23/14 15:28 L212905SEB

<0.0100 mg/Kg 0.0100Iodomethane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Isopropylbenzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00204-Isopropyl toluene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Methyl tert-butyl ether (MTBE) 1 09/23/14 15:28 L212905SEB

<0.0100 mg/Kg 0.01004-Methyl-2-Pentanone 1 09/23/14 15:28 L212905SEB

<0.0100 mg/Kg 0.0100Methylene Chloride 1 09/23/14 15:28 L212905SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 106 of 119

Page 135: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-10 (12-16')

95412 Matrix:

9/18/2014 16:15

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/23/2014 09:22:00Prep Batch(es): L212904

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0100 mg/Kg 0.0100Naphthalene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020n-Propylbenzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Styrene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,1,1,2-Tetrachloroethane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,1,2,2-Tetrachloroethane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Tetrachloroethene 1 09/23/14 15:28 L212905SEB

<0.0100 mg/Kg 0.0100Toluene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,2,3-Trichlorobenzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,2,4-Trichlorobenzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,1,1-Trichloroethane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,1,2-Trichloroethane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Trichloroethene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Trichlorofluoromethane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,2,3-Trichloropropane 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,2,4-Trimethylbenzene 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.00201,3,5-Trimethylbenzene 1 09/23/14 15:28 L212905SEB

<0.0400 mg/Kg 0.0400Vinyl Acetate 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020Vinyl Chloride 1 09/23/14 15:28 L212905SEB

<0.0020 mg/Kg 0.0020o-Xylene 1 09/23/14 15:28 L212905SEB

<0.0040 mg/Kg 0.0040m,p-Xylene 1 09/23/14 15:28 L212905SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 107 of 119

Page 136: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-10 (12-16')

95412 Matrix:

9/18/2014 16:15

Solids

Analytical Method: 8260B

Prep Method: 5030A Date/Time Prepped: 9/23/2014 09:22:00Prep Batch(es): L212904

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0020 mg/Kg 0.0020Xylene (Total) 1 09/23/14 15:28 L212905

Surrogate: 4-Bromofluorobenzene 108 Limits: 60-130% 09/23/14 15:281 SEB L212905

Surrogate: 1,2-Dichloroethane - d4 106 Limits: 60-132% 09/23/14 15:281 SEB L212905

Surrogate: Toluene-d8 90.6 Limits: 70-122% 09/23/14 15:281 SEB L212905

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.066 mg/Kg 0.066Acenaphthene 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Acenaphthylene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Acetophenone 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Aniline 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Anthracene 1 09/25/14 17:47 L213162BMP

<0.670 mg/Kg 0.670Benzidine 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)anthracene 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Benzo(a)pyrene 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Benzo(b)fluoranthene 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Benzo(g,h,i)perylene 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Benzo(k)fluoranthene 1 09/25/14 17:47 L213162BMP

<0.330 mg/Kg 0.330Benzoic Acid 1 09/25/14 17:47 L213162BMP

<0.330 mg/Kg 0.330Benzyl alcohol 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroethoxy)methane 1 09/25/14 17:47 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 108 of 119

Page 137: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-10 (12-16')

95412 Matrix:

9/18/2014 16:15

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.170Bis(2-Chloroethyl)ether 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Bis(2-Chloroisopropyl)ether 1 09/25/14 17:47 L213162BMP

<0.330 mg/Kg 0.330Bis(2-ethylhexyl)phthalate 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1704-Bromophenyl phenyl ether 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Butyl benzyl phthalate 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Carbazole 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1704-Chloro-3-methylphenol 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1704-Chloroaniline 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1702-Chloronaphthalene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1702-Chlorophenol 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1704-Chlorophenyl phenyl ether 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Chrysene 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Dibenz(a,h)anthracene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Dibenzofuran 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1701,2-Dichlorobenzene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1701,3-Dichlorobenzene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1701,4-Dichlorobenzene 1 09/25/14 17:47 L213162BMP

<0.330 mg/Kg 0.3303,3'-Dichlorobenzidine 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1702,4-Dichlorophenol 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1702,6-Dichlorophenol 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Diethyl phthalate 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Dimethyl phthalate 1 09/25/14 17:47 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 109 of 119

Page 138: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-10 (12-16')

95412 Matrix:

9/18/2014 16:15

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.330 mg/Kg 0.3303,3' Dimethylbenzidine 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1702,4-Dimethylphenol 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Di-n-butyl phthalate 1 09/25/14 17:47 L213162BMP

<0.330 mg/Kg 0.3304,6-Dinitro-2-methylphenol 1 09/25/14 17:47 L213162BMP

<1.67 mg/Kg 1.672,4-Dinitrophenol 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1702,4-Dinitrotoluene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1702,6-Dinitrotoluene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Di-n-Octyl Phthalate 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Fluoranthene 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Fluorene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobenzene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Hexachlorobutadiene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Hexachlorocyclopentadiene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Hexachloroethane 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Indeno(1,2,3-cd)pyrene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Isophorone 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.0662-Methylnaphthalene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1702-Methylphenol 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1703&4 Methylphenol 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Naphthalene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1702-Nitroaniline 1 09/25/14 17:47 L213162BMP

<0.330 mg/Kg 0.3303-Nitroaniline 1 09/25/14 17:47 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 110 of 119

Page 139: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-10 (12-16')

95412 Matrix:

9/18/2014 16:15

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1704-Nitroaniline 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Nitrobenzene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1702-Nitrophenol 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1704-Nitrophenol 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodimethylamine 1 09/25/14 17:47 L213162BMP

<0.330 mg/Kg 0.330N-Nitrosodiphenylamine 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170N-Nitrosodiethylamine 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-butylamine 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170N-Nitroso-di-n-propylamine 1 09/25/14 17:47 L213162BMP

<0.330 mg/Kg 0.330Pentachlorophenol 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Phenanthrene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.170Phenol 1 09/25/14 17:47 L213162BMP

<0.066 mg/Kg 0.066Pyrene 1 09/25/14 17:47 L213162BMP

<0.330 mg/Kg 0.330Pyridine 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1701,2,4,5-Tetrachlorobenzene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1702,3,4,6-Tetrachlorophenol 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1701,2,4-Trichlorobenzene 1 09/25/14 17:47 L213162BMP

<0.170 mg/Kg 0.1702,4,5-Trichlorophenol 1 09/25/14 17:47 L213162BMP

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 111 of 119

Page 140: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:SB-10 (12-16')

95412 Matrix:

9/18/2014 16:15

Solids

Analytical Method: 8270C

Prep Method: 3546 Date/Time Prepped: 9/22/2014 09:30:00Prep Batch(es): L213161

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.170 mg/Kg 0.1702,4,6-Trichlorophenol 1 09/25/14 17:47 L213162BMP

Surrogate: 2-Fluorobiphenyl 64.6 Limits: 33-115% 09/25/14 17:471 BMP L213162

Surrogate: 2-Fluorophenol 62.0 Limits: 10-119% 09/25/14 17:471 BMP L213162

Surrogate: Nitrobenzene-d5 64.3 Limits: 29-110% 09/25/14 17:471 BMP L213162

Surrogate: Phenol-d6 62.8 Limits: 11-125% 09/25/14 17:471 BMP L213162

Surrogate: 4-Terphenyl-d14 79.6 Limits: 33-122% 09/25/14 17:471 BMP L213162

Surrogate: 2,4,6-Tribromophenol 89.3 Limits: 9-134% 09/25/14 17:471 BMP L213162

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 112 of 119

Page 141: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:Trip Blank

95413 Matrix:

9/18/2014 0:00

Aqueous

Analytical Method: 8260B

Prep Method: 5030B Date/Time Prepped: 9/24/2014 08:57:00Prep Batch(es): L213148

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.0200 mg/L 0.0200Acetone 1 09/24/14 13:45 L213151SEB

<0.0500 mg/L 0.0500Acetonitrile 1 09/24/14 13:45 L213151SEB

<0.0200 mg/L 0.0200Acrolein 1 09/24/14 13:45 L213151SEB

<0.0200 mg/L 0.0200Acrylonitrile 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Benzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Bromobenzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Bromochloromethane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Bromodichloromethane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Bromoform 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Bromomethane 1 09/24/14 13:45 L213151SEB

<0.0200 mg/L 0.0200Methyl Ethyl Ketone (MEK) 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100n-Butylbenzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100sec-Butyl benzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100tert-Butyl benzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Carbon Disulfide 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Carbon Tetrachloride 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Chlorobenzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Chlorodibromomethane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Chloroethane 1 09/24/14 13:45 L213151SEB

<0.00500 M mg/L 0.005002-Chloroethylvinyl Ether 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Chloroform 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Chloromethane 1 09/24/14 13:45 L213151SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 113 of 119

Page 142: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:Trip Blank

95413 Matrix:

9/18/2014 0:00

Aqueous

Analytical Method: 8260B

Prep Method: 5030B Date/Time Prepped: 9/24/2014 08:57:00Prep Batch(es): L213148

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.00100 mg/L 0.001002-Chlorotoluene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001004-Chlorotoluene 1 09/24/14 13:45 L213151SEB

<0.00500 mg/L 0.005001,2-Dibromo-3-Chloropropane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,2-Dibromoethane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Dibromomethane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,2-Dichlorobenzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,3-Dichlorobenzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,4-Dichlorobenzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Dichlorodifluoromethane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,1-Dichloroethane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,2-Dichloroethane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,1-Dichloroethene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100cis-1,2-Dichloroethene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100trans-1,2-Dichloroethene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,2-Dichloroethene (Total) 1 09/24/14 13:45 L213151

<0.00100 mg/L 0.001001,2-Dichloropropane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,3-Dichloropropane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001002,2-Dichloropropane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,1-Dichloropropene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100cis-1,3-Dichloropropene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100trans-1,3-Dichloropropene 1 09/24/14 13:45 L213151SEB

<0.0100 mg/L 0.0100Ethyl Acetate 1 09/24/14 13:45 L213151SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 114 of 119

Page 143: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:Trip Blank

95413 Matrix:

9/18/2014 0:00

Aqueous

Analytical Method: 8260B

Prep Method: 5030B Date/Time Prepped: 9/24/2014 08:57:00Prep Batch(es): L213148

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.00100 mg/L 0.00100Ethylbenzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Hexachlorobutadiene 1 09/24/14 13:45 L213151SEB

<0.00500 mg/L 0.005002-Hexanone 1 09/24/14 13:45 L213151SEB

<0.00500 mg/L 0.00500Iodomethane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Isopropylbenzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001004-Isopropyl toluene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Methyl tert-butyl ether (MTBE) 1 09/24/14 13:45 L213151SEB

<0.00500 mg/L 0.005004-Methyl-2-Pentanone 1 09/24/14 13:45 L213151SEB

<0.00500 mg/L 0.00500Methylene Chloride 1 09/24/14 13:45 L213151SEB

<0.00500 mg/L 0.00500Naphthalene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100n-Propylbenzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Styrene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,1,1,2-Tetrachloroethane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,1,2,2-Tetrachloroethane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Tetrachloroethene 1 09/24/14 13:45 L213151SEB

<0.00500 mg/L 0.00500Toluene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,2,3-Trichlorobenzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,2,4-Trichlorobenzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,1,1-Trichloroethane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,1,2-Trichloroethane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Trichloroethene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Trichlorofluoromethane 1 09/24/14 13:45 L213151SEB

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 115 of 119

Page 144: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

,

REPORT OF ANALYSISReport Number :

Project

Information :

TN 38118

14-262-0305

04897

PSI

4161 Ridgemoor Ave

Mr. Ricky Reynolds

Memphis

Memphis, TN

Project No. 05021106

Project ID :

2029 Elzey Avenue

Report Date :

Received :

09/26/2014

9/19/2014

Sample ID :

Lab No :

Sampled:Trip Blank

95413 Matrix:

9/18/2014 0:00

Aqueous

Analytical Method: 8260B

Prep Method: 5030B Date/Time Prepped: 9/24/2014 08:57:00Prep Batch(es): L213148

Test Results Units MQL By AnalyticalBatch

Date / TimeAnalyzed

DF

<0.00100 mg/L 0.001001,2,3-Trichloropropane 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,2,4-Trimethylbenzene 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.001001,3,5-Trimethylbenzene 1 09/24/14 13:45 L213151SEB

<0.0100 mg/L 0.0100Vinyl Acetate 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100Vinyl Chloride 1 09/24/14 13:45 L213151SEB

<0.00100 mg/L 0.00100o-Xylene 1 09/24/14 13:45 L213151SEB

<0.00200 mg/L 0.00200m,p-Xylene 1 09/24/14 13:45 L213151SEB

<0.0010 mg/L 0.0010Xylene (Total) 1 09/24/14 13:45 L213151

Surrogate: 4-Bromofluorobenzene 108 Limits: 71-137% 09/24/14 13:451 SEB L213151

Surrogate: Dibromofluoromethane 88.4 Limits: 70-128% 09/24/14 13:451 SEB L213151

Surrogate: 1,2-Dichloroethane - d4 109 Limits: 63-136% 09/24/14 13:451 SEB L213151

Surrogate: Toluene-d8 94.6 Limits: 70-130% 09/24/14 13:451 SEB L213151

Qualifiers/Definitions

Dilution FactorDFOutside QC limit*

Minimum valueMRecovery out of rangeI

Method Quantitation LimitMQL

Page 116 of 119

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Page 117 of 119

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Page 118 of 119

Page 147: October 30, 2014 Triple Z Development, Inc. and …...Professional Service Industries, Inc. – 4161 Ridgemoor Avenue Memphis, Tennessee 38118 – Phone (901) 365-1802 October 30,

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