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February 5, 2013Volume 85, Issue 3Pages 1257-1964

EDITORIAL FEATURES LETTERS TO ANALYTICAL CHEMISTRY

TECHNICAL NOTES ARTICLES

In this issue:

About the Cover: The cover image illustrates several single molecule detection techniques described in the Feature article written by David R. Walt. The center graphic depicts a femto-liter microwell array etched at the tip of a fiber-optic bundle. Art designer: Huaibin (Eli) Zhang. View the article.

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EDITORIAL

Meet the Analytical Chemistry Editorial Advisory BoardJonathan V. Sweedler

pp 1257–1257Publication Date (Web): January 18, 2013 (Editorial)DOI: 10.1021/ac4001173

First Page

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FEATURES

Section: Biochemical Methods

Optical Methods for Single Molecule Detection and AnalysisDavid R. Walt

pp 1258–1263Publication Date (Web): December 10, 2012 (Feature)DOI: 10.1021/ac3027178

Abstract

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Figure 1 of 4

Laboratory Analysis of StardustErnst Zinner

pp 1264–1270Publication Date (Web): December 11, 2012 (Feature)DOI: 10.1021/ac303052p

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Page 1 of 13Analytical Chemistry: Volume 85, Issue 3 (ACS Publications)

23/5/2548http://pubs.acs.org/toc/ancham/85/3

Section: Mineralogical and Geological Chemistry

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LETTERS TO ANALYTICAL CHEMISTRY


Dipolar Direct Current Driven Collision-Induced Dissociation in a Digital Ceramic-Based Rectilinear Ion Trap Mass SpectrometerLiang Wang, Fuxing Xu, and Chuan-Fan Ding

pp 1271–1275Publication Date (Web): January 8, 2013 (Letter)DOI: 10.1021/ac3031256

Abstract | Supporting Info

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Desorption Electrospray Ionization Imaging Mass Spectrometry as a Tool for Investigating Model Prebiotic Reactions on Mineral Surfaces.Rachel V. Bennett, H. James Cleaves, II, Jeffrey M. Davis, Denis A. Sokolov, Thomas M. Orlando, Jeffrey L. Bada, and Facundo M. Fernández

pp 1276–1279Publication Date (Web): January 3, 2013 (Letter)DOI: 10.1021/ac303202n


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Detection of Glutathione in Vitro and in Cells by the Controlled Self-Assembly of NanoringsYue Yuan, Jia Zhang, Mengjing Wang, Bin Mei, Yafeng Guan, and Gaolin Liang

pp 1280–1284Publication Date (Web): January 7, 2013 (Letter)DOI: 10.1021/ac303183v


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Interfacing Droplet Microfluidics with Matrix-Assisted Laser Desorption/Ionization Mass Spectrometry: Label-Free Content Analysis of Single DropletsSimon K. Küster, Stephan R. Fagerer, Pascal E. Verboket, Klaus Eyer, Konstantins Jefimovs, Renato Zenobi, and Petra S. Dittrich



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Illuminating the Lateral Organization of Cell-Surface CD24 and CD44 through Plasmon Coupling between Au Nanoparticle ImmunolabelsXinwei Yu, Jing Wang, Amin Feizpour, and Björn M. Reinhard

pp 1290–1294Publication Date (Web): January 15, 2013 (Letter)DOI: 10.1021/ac303310j


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Section: Air Pollution and Industrial Hygiene

Investigation of Gas Exchange Processes in Peat Bog Ecosystems by Means of Innovative Raman Gas SpectroscopyTorsten Frosch, Robert Keiner, Beate Michalzik, Bernhard Fischer, and Jürgen Popp


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Section: Inorganic Analytical Chemistry

Sensing and Imaging of Oxygen with Parts per Billion Limits of Detection and Based on the Quenching of the Delayed Fluorescence of 13C70 Fullerene in Polymer HostsSven Kochmann, Carlos Baleizão, Mário N. Berberan-Santos, and Otto S. Wolfbeis

pp 1300–1304Publication Date (Web): January 15, 2013 (Letter)DOI: 10.1021/ac303486f

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TECHNICAL NOTES

Section: Organic Analytical Chemistry

Argon Direct Analysis in Real Time Mass Spectrometry in Conjunction with Makeup Solvents: A Method for Analysis of Labile CompoundsHongmei Yang, Debin Wan, Fengrui Song, Zhiqiang Liu, and Shuying Liu

pp 1305–1309Publication Date (Web): December 20, 2012 (Technical Note)DOI: 10.1021/ac3026543


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Combination of Liquid Chromatography–Fourier Transform Ion Cyclotron Resonance-Mass Spectrometry with 13C-Labeling for Chemical Assignment of Sulfur-Containing Metabolites in Onion BulbsRyo Nakabayashi, Yuji Sawada, Yutaka Yamada, Makoto Suzuki, Masami Yokota Hirai, Tetsuya Sakurai, and Kazuki Saito

pp 1310–1315Publication Date (Web): January 17, 2013 (Technical Note)DOI: 10.1021/ac302733c


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Speciation of Silver Nanoparticles and Silver(I) by Reversed-Phase Liquid Chromatography Coupled to ICPMSJuan Soto-Alvaredo, María Montes-Bayón, and Jörg Bettmer

pp 1316–1321Publication Date (Web): January 11, 2013 (Technical Note)DOI: 10.1021/ac302851d


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Section: Electrochemistry

A Leveling Method Based on Current Feedback Mode of Scanning Electrochemical MicroscopyLianhuan Han, Ye Yuan, Jie Zhang, Xuesen Zhao, Yongzhi Cao, Zhenjiang Hu, Yongda Yan, Shen Dong, Zhong-Qun Tian, Zhao-Wu Tian, and Dongping, Zhan

pp 1322–1326Publication Date (Web): January 5, 2013 (Technical Note)DOI: 10.1021/ac303122v

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Section: Radiation Chemistry, Photochemistry, and Photographic and Other Reprographic Processes

Method for Fabrication of Paper-Based Microfluidic Devices by Alkylsilane Self-Assembling and UV/O3-PatterningQiaohong He, Cuicui Ma, Xianqiao Hu, and Hengwu Chen

pp 1327–1331Publication Date (Web): December 17, 2012 (Technical Note)DOI: 10.1021/ac303138x


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Non-Severinghaus Potentiometric Dissolved CO2 Sensor with Improved CharacteristicsXiaojiang Xie and Eric Bakker

pp 1332–1336Publication Date (Web): January 10, 2013 (Technical Note)DOI: 10.1021/ac303534v


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Section: Optical, Electron, and Mass Spectroscopy and Other Related Properties

Chromatic Aberration Short-Wave Infrared Spectroscopy: Nanoparticle Spectra without a SpectrometerJason K. Streit, Sergei M. Bachilo, and R. Bruce Weisman

pp 1337–1341Publication Date (Web): January 3, 2013 (Technical Note)DOI: 10.1021/ac303713z


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ARTICLES




Nanoclustered Gold Honeycombs for Surface-Enhanced Raman ScatteringWeinan Leng and Peter J. Vikesland

pp 1342–1349Publication Date (Web): December 4, 2012 (Article)DOI: 10.1021/ac301028w


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Fuel Cell Virus Sensor Using Virus Capture within Antibody-Coated NanochannelsYanyan Wei, Lai Peng Wong, and Chee-Seng Toh

pp 1350–1357Publication Date (Web): January 11, 2013 (Article)DOI: 10.1021/ac302942y


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Section: Biochemical Genetics

Direct and Freely Switchable Detection of Target Genes Engineered by Reduced Graphene Oxide-Poly(m-Aminobenzenesulfonic Acid) Nanocomposite via Synchronous Pulse ElectrosynthesisTao Yang, Qian Guan, Xiuhong Guo, Le Meng, Meng Du, and Kui Jiao

pp 1358–1366Publication Date (Web): December 20, 2012 (Article)DOI: 10.1021/ac3030009


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Section: Enzymes

Genetically Encoded Protease Substrate Based on Lanthanide-Binding Peptide for Time-Gated Fluorescence DetectionJohanna Vuojola, Markku Syrjänpää, Urpo Lamminmäki, and Tero Soukka

pp 1367–1373Publication Date (Web): December 31, 2012 (Article)DOI: 10.1021/ac302030q


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Investigation of Free Fatty Acid Associated Recombinant Membrane Receptor Protein Expression in HEK293 Cells Using Raman Spectroscopy, Calcium Imaging, and Atomic Force MicroscopyJuqiang Lin, Han Xu, Yangzhe Wu, Mingjie Tang, Gerald D. McEwen, Pin Liu, Dane R. Hansen, Timothy A. Gilbertson, and Anhong Zhou



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Section: Surface Chemistry and Colloids

High-Resolution Length Fractionation of Surfactant-Dispersed Carbon NanotubesConstantine Y. Khripin, Xiaomin Tu, John M. Heddleston, Carlos Silvera-Batista, Angela R. Hight Walker, Jeffrey Fagan, and Ming Zheng



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Section: Electrochemistry

Impact of a Surfactant on the Electroactivity of Proteins at an Aqueous–Organogel Microinterface ArrayShane O’Sullivan and Damien W. M. Arrigan

pp 1389–1394Publication Date (Web): December 22, 2012 (Article)DOI: 10.1021/ac302222u


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Characterization of the Mechanodynamic Response of Cardiomyocytes with Atomic Force MicroscopyWei-Tien Chang, David Yu, Yu-Cheng Lai, Kuen-You Lin, and Ian Liau


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Section: Pharmaceuticals

Gene Delivery to Cultured Embryonic Stem Cells Using Nanofiber-Based Sandwich ElectroporationZhengzheng Fei, Yun Wu, Sadhana Sharma, Daniel Gallego-Perez, Natalia Higuita-Castro, Derek Hansford, John J. Lannutti, and Ly James Lee

pp 1401–1407Publication Date (Web): December 13, 2012 (Article)DOI: 10.1021/ac302140p

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SERS Primers and Their Mode of Action for Pathogen DNA DetectionDanny van Lierop, Iain A. Larmour, Karen Faulds, and Duncan Graham

pp 1408–1414Publication Date (Web): January 11, 2013 (Article)DOI: 10.1021/ac302254h


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Hyperspectral Visualization of Mass Spectrometry Imaging DataJudith M. Fonville, Claire L. Carter, Luis Pizarro, Rory T. Steven, Andrew D. Palmer, Rian L. Griffiths, Patricia F. Lalor, John C. Lindon, Jeremy K. Nicholson, Elaine Holmes, and Josephine Bunch

pp 1415–1423Publication Date (Web): December 18, 2012 (Article)DOI: 10.1021/ac302330a


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Graphene Signal Amplification for Sensitive and Real-Time Fluorescence Anisotropy Detection of Small MoleculesJinhua Liu, Changyao Wang, Ying Jiang, Yaping Hu, Jishan Li, Sheng Yang, Yinhui Li, Ronghua Yang, Weihong Tan, and Cheng Zhi Huang

pp 1424–1430Publication Date (Web): January 2, 2013 (Article)DOI: 10.1021/ac3023982


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Magnetic Nanoparticle Mediated Enhancement of Localized Surface Plasmon Resonance for Ultrasensitive Bioanalytical Assay in Human Blood PlasmaLiang Tang, Justin Casas, and Meenakshi Venkataramasubramani

pp 1431–1439Publication Date (Web): December 25, 2012 (Article)DOI: 10.1021/ac302422k


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Limitations of Surface Enhanced Raman Scattering in Sensing DNA Hybridization Demonstrated by Label-Free DNA Oligos as Molecular Rulers of Distance-Dependent EnhancementNicole E. Marotta, Kelsey R. Beavers, and Lawrence A. Bottomley

pp 1440–1446Publication Date (Web): December 22, 2012 (Article)DOI: 10.1021/ac302454j

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Directly Functionalizable Surface Platform for Protein Arrays in Undiluted Human Blood PlasmaNorman D. Brault, Andrew D. White, Allen D. Taylor, Qiuming Yu, and Shaoyi Jiang

pp 1447–1453Publication Date (Web): January 8, 2013 (Article)DOI: 10.1021/ac303462u


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Multiple and Sequential Data Acquisition Method: An Improved Method for Fragmentation and Detection of Cross-Linked Peptides on a Hybrid Linear Trap Quadrupole Orbitrap Velos Mass SpectrometerElena L. Rudashevskaya, Florian P. Breitwieser, Marie L. Huber, Jacques Colinge, André C. Müller, and Keiryn L. Bennett

pp 1454–1461Publication Date (Web): January 9, 2013 (Article)DOI: 10.1021/ac302251f


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Section: General Biochemistry

Temperature Dependence of Electrochemical DNA Charge Transport: Influence of a MismatchChris H. Wohlgamuth, Marc A. McWilliams, and Jason D. Slinker

pp 1462–1467Publication Date (Web): December 20, 2012 (Article)DOI: 10.1021/ac302508f


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Simple and Efficient Strategy for Site-Specific Dual Labeling of Proteins for Single-Molecule Fluorescence Resonance Energy Transfer AnalysisJihyo Kim, Moon-Hyeong Seo, Sangsik Lee, Kyukwang Cho, Aerin Yang, Kyunghwa Woo, Hak-Sung Kim, and Hee-Sung Park

pp 1468–1474Publication Date (Web): December 31, 2012 (Article)DOI: 10.1021/ac303089v


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Impedimetric Detection of Histamine in Bowel Fluids Using Synthetic Receptors with pH-Optimized Binding CharacteristicsMarloes Peeters, Freddy J. Troost, Roel H.G. Mingels, Tina Welsch, Bart van Grinsven, Tom Vranken, Sven Ingebrandt, Ronald Thoelen, Thomas Jan Cleij, and Patrick Wagner



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A Microfluidic Liquid Phase Nucleic Acid Purification Chip to Selectively Isolate DNA or RNA from Low Copy/Single Bacterial Cells in Minute Sample Volume Followed by Direct On-Chip Quantitative PCR AssayRui Zhang, Hai-Qing Gong, Xudong Zeng, ChaoPing Lou, and ChunChau Sze



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An Optimized Calibration Procedure for Determining Elemental Ratios Using Laser-Induced Breakdown SpectroscopyJens Frydenvang, Kjartan Münster Kinch, Søren Husted, and Morten Bo Madsen


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Section: General Biochemistry

Cu(II) Affinity for the Alzheimer’s Peptide: Tyrosine Fluorescence Studies RevisitedBruno Alies, Emelyne Renaglia, Malgorzata Rózga, Wojciech Bal, Peter Faller, and Christelle Hureau

pp 1501–1508Publication Date (Web): December 18, 2012 (Article)DOI: 10.1021/ac302629u


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Spectral Multivariate Calibration without Laboratory Prepared or Determined Reference Analyte ValuesJosh Ottaway, Jeremy A. Farrell, and John H. Kalivas

pp 1509–1516Publication Date (Web): December 31, 2012 (Article)DOI: 10.1021/ac302705m


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Separation of Fatty Acid Methyl Esters by GC-Online Hydrogenation × GCPierluigi Delmonte, Ali Reza Fardin-Kia, and Jeanne I. Rader

pp 1517–1524Publication Date (Web): December 20, 2012 (Article)DOI: 10.1021/ac302707z

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Capillary Electrophoresis–SELEX Selection of Catalytic DNA Aptamers for a Small-Molecule Porphyrin TargetJing Yang and Michael T. Bowser



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Direct Approach for Qualitative and Quantitative Characterization of Glycoproteins Using Tandem Mass Tags and an LTQ Orbitrap XL Electron Transfer Dissociation Hybrid Mass SpectrometerHongping Ye, Michael T. Boyne, II, Lucinda F. Buhse, and John Hill



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Mechanistic Evaluation of the Pros and Cons of Digital RT-LAMP for HIV-1 Viral Load Quantification on a Microfluidic Device and Improved Efficiency via a Two-Step Digital ProtocolBing Sun, Feng Shen, Stephanie E. McCalla, Jason E. Kreutz, Mikhail A. Karymov, and Rustem F. Ismagilov



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Ring-Oven Based Preconcentration Technique for Microanalysis: Simultaneous Determination of Na, Fe, and Cu in Fuel Ethanol by Laser Induced Breakdown SpectroscopyJuliana Cortez and Celio Pasquini

pp 1547–1554Publication Date (Web): December 20, 2012 (Article)DOI: 10.1021/ac302755h

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Solid-Contact Ion-Selective Electrodes with Highly Selective Thioamide Derivatives of p-tert-Butylcalix[4]arene for the Determination of Lead(II) in Environmental SamplesMarcin Guziński, Grzegorz Lisak, Tomasz Sokalski, Johan Bobacka, Ari Ivaska, Maria Bocheńska, and Andrzej Lewenstam

pp 1555–1561Publication Date (Web): January 2, 2013 (Article)DOI: 10.1021/ac302772v


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Effect of Microculture on Cell Metabolism and Biochemistry: Do Cells Get Stressed in Microchannels?Xiaojing Su, Ashleigh B. Theberge, Craig T. January, and David J. Beebe



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Influence of Surface Adsorption on the Interfacial Electron Transfer of Flavin Adenine Dinucleotide and Glucose Oxidase at Carbon Nanotube and Nitrogen-Doped Carbon Nanotube ElectrodesJacob M. Goran, Sandra M. Mantilla, and Keith J. Stevenson



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Section: Pharmaceutical Analysis

Electrochemical Study of the Anticancer Drug Daunorubicin at a Water/Oil Interface: Drug Lipophilicity and QuantificationJosé A. Ribeiro, F. Silva, and Carlos M. Pereira


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Section: Enzymes

Studies of pH-Dependent Self-Association of a Recombinant Form of Arylsulfatase A with Electrospray Ionization Mass Spectrometry and Size-Exclusion ChromatographyRinat R. Abzalimov, Cedric E. Bobst, Paul A. Salinas, Philip Savickas, John J. Thomas, and Igor A. Kaltashov

pp 1591–1596Publication Date (Web): December 19, 2012 (Article)DOI: 10.1021/ac302829k

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Section: Immunochemistry

Structural Model of Lymphocyte Receptor NKR-P1C Revealed by Mass Spectrometry and Molecular ModelingDaniel Rozbesky, Zofie Sovova, Julien Marcoux, Petr Man, Rudiger Ettrich, Carol V. Robinson, and Petr Novak

pp 1597–1604Publication Date (Web): December 18, 2012 (Article)DOI: 10.1021/ac302860m

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Using Optical Anisotropy as a Quality Factor To Rapidly Characterize Structural Qualities of Large-Area Graphene FilmsYu-Lun Liu, Chen-Chieh Yu, Cheng-Yi Fang, Hsuen-Li Chen, Chun-Wei Chen, Chun-Chiang Kuo, Cheng-Kai Chang, Li-Chyong Chen, and Kuei-Hsien Chen

pp 1605–1614Publication Date (Web): January 16, 2013 (Article)DOI: 10.1021/ac302863w


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Maximizing Mismatch Discrimination by Surface-Tethered Locked Nucleic Acid Probes via Ionic TuningSourav Mishra, Srabani Ghosh, and Rupa Mukhopadhyay



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A Label-Free Biosensor for Electrochemical Detection of Femtomolar MicroRNAsZhiqiang Gao, Huimin Deng, Wei Shen, and Yuqian Ren

pp 1624–1630Publication Date (Web): January 16, 2013 (Article)DOI: 10.1021/ac302883c


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Hydroquinone Diphosphate as a Phosphatase Substrate in Enzymatic Amplification Combined with Electrochemical–Chemical–Chemical Redox Cycling for the Detection of E. coli O157:H7Md. Rajibul Akanda, Vellaiappillai Tamilavan, Seonhwa Park, Kyungmin Jo, Myung Ho Hyun, and Haesik Yang



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Flow-Through Comb Electroporation Device for Delivery of MacromoleculesAndrea Adamo, Alessandro Arione, Armon Sharei, and Klavs F. Jensen


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Stable Isotope Probing and Raman Spectroscopy for Monitoring Carbon Flow in a Food Chain and Revealing Metabolic PathwayMengqiu Li, Wei E. Huang, Christopher M. Gibson, Patrick W. Fowler, and Alexandre Jousset

pp 1642–1649Publication Date (Web): December 22, 2012 (Article)DOI: 10.1021/ac302910x


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Section: History, Education, and Documentation

Beyond the Great Wall: Gold of the Silk Roads and the First Empire of the SteppesMartin Radtke, Ina Reiche, Uwe Reinholz, Heinrich Riesemeier, and Maria F. Guerra



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Digital Polymerase Chain Reaction Measured pUC19 Marker as Calibrant for HPLC Measurement of DNA QuantityDaniel G. Burke, Lianhua Dong, Somanath Bhat, Michael Forbes-Smith, Shuang Fu, Leonardo Pinheiro, Wang Jing, and Kerry R. Emslie



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Section: Water

Sensitive and Selective Redox, Chromogenic, and “Turn-On” Fluorescent Probe for Pb(II) in Aqueous EnvironmentArunabha Thakur, Dipendu Mandal, and Sundargopal Ghosh



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Ambient Surface Mass Spectrometry Using Plasma-Assisted Desorption Ionization: Effects and Optimization of Analytical Parameters for Signal Intensities of Molecules and PolymersT. L. Salter, I. S. Gilmore, A. Bowfield, O. T. Olabanji, and J. W. Bradley

pp 1675–1682Publication Date (Web): January 8, 2013 (Article)DOI: 10.1021/ac302677m


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Microcirculation System with a Dialysis Part for Bioassays Evaluating Anticancer Activity and RetentionYuki Imura, Etsuro Yoshimura, and Kiichi Sato


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Modulation of Glycan Detection on Specific Glycoproteins by Lectin MultimerizationZheng Cao, Katie Partyka, Mitchell McDonald, Elizabeth Brouhard, Marina Hincapie, Randall E. Brand, William S. Hancock, and Brian B. Haab

pp 1689–1698Publication Date (Web): January 3, 2013 (Article)DOI: 10.1021/ac302826a


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Development of a Native Nanoelectrospray Mass Spectrometry Method for Determination of the Drug-to-Antibody Ratio of Antibody–Drug ConjugatesJia Chen, Sheng Yin, Yongjian Wu, and Jun Ouyang

pp 1699–1704Publication Date (Web): January 4, 2013 (Article)DOI: 10.1021/ac302959p

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Estimation of the Deamidation Rates of Major Deamidation Sites in a Fab Fragment of Mouse IgG1-κ by Capillary Isoelectric Focusing of Mutated Fab FragmentsKiyohito Shimura, Makoto Hoshino, Keiichiro Kamiya, Manabu Enomoto, Sunao Hisada, Hiroyuki Matsumoto, Mark Novotny, and Ken-ichi Kasai


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Quenching of the Electrochemiluminescence of Tris(2,2′-bipyridine)ruthenium(II)/Tri-n-propylamine by Pristine Carbon Nanotube and Its Application to Quantitative Detection of DNAXiaofeng Tang, Dan Zhao, Jinchao He, Fengwang Li, Jiaxi Peng, and Meining Zhang

pp 1711–1718Publication Date (Web): January 13, 2013 (Article)DOI: 10.1021/ac303025y


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Sequential Protein and Peptide Immunoaffinity Capture for Mass Spectrometry-Based Quantification of Total Human β-Nerve Growth FactorHendrik Neubert, David Muirhead, Musarat Kabir, Chris Grace, Adriaan Cleton, and Rosalin Arends



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Screening and Identification of Glyceollins and Their Metabolites by Electrospray Ionization Tandem Mass Spectrometry with Precursor Ion ScanningSyeda S. Quadri, Robert E. Stratford, Stephen M. Boué, and Richard B. Cole


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Spherical Nucleic Acid Enhanced FO-SPR DNA Melting for Detection of Mutations in Legionella pneumophilaKarel Knez, Kris P. F. Janssen, Dragana Spasic, Priscilla Declerck, Louise Vanysacker, Carla Denis, Dinh T. Tran, and Jeroen Lammertyn

pp 1734–1742Publication Date (Web): January 3, 2013 (Article)DOI: 10.1021/ac303008f


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Multiplex Analysis of Novel Urinary Lyso-Gb3-Related Biomarkers for Fabry Disease by Tandem Mass SpectrometryPamela Lavoie, Michel Boutin, and Christiane Auray-Blais



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Cell Surface-Fluorescence Immunosorbent Assay for Real-Time Detection of Hybridomas with Efficient Antibody Secretion at the Single-Cell LevelAkiko Kida, Masumi Iijima, Tomoaki Niimi, Andrés D. Maturana, Nobuo Yoshimoto, and Shun’ichi Kuroda

pp 1753–1759Publication Date (Web): January 8, 2013 (Article)DOI: 10.1021/ac303067k

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Torsional and Lateral Resonant Modes of Cantilevers as Biosensors: Alternatives to Bending ModesBlake N. Johnson, Harsh Sharma, and Raj Mutharasan



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Synchronized Discharge Ionization for Analysis of Volatile Organic Compounds Using a Hand-Held Ion Trap Mass SpectrometerTsung-Chi Chen and Zheng Ouyang

pp 1767–1772Publication Date (Web): December 20, 2012 (Article)DOI: 10.1021/ac303112d

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Quantifying the Cluster of Differentiation 4 Receptor Density on Human T Lymphocytes Using Multiple Reaction Monitoring Mass SpectrometryMeiyao Wang, Hua-Jun He, Illarion V. Turko, Karen W. Phinney, and Lili Wang



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Section: Toxicology

Antipyrine Based Arsenate Selective Fluorescent Probe for Living Cell ImagingSisir Lohar, Animesh Sahana, Arnab Banerjee, Avishek Banik, Subhra Kanti Mukhopadhyay, Jesús Sanmartín Matalobos, and Debasis Das



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Increased Electrocatalyzed Performance through Dendrimer-Encapsulated Gold Nanoparticles and Carbon Nanotube-Assisted Multiple Bienzymatic Labels: Highly Sensitive Electrochemical Immunosensor for Protein DetectionBongjin Jeong, Rashida Akter, Oc Hee Han, Choong Kyun Rhee, and Md. Aminur Rahman

pp 1784–1791Publication Date (Web): January 4, 2013 (Article)DOI: 10.1021/ac303142e

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Selective Diagnosis of Diabetes Using Pt-Functionalized WO3 Hemitube Networks As a Sensing Layer of Acetone in Exhaled BreathSeon-Jin Choi, Inkun Lee, Bong-Hoon Jang, Doo-Young Youn, Won-Hee Ryu, Chong Ook Park, and Il-Doo Kim



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Fabrication of High-Quality Microfluidic Solid-Phase Chromatography ColumnsJens Huft, Charles A. Haynes, and Carl L. Hansen



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Investigation of the Human Brain Metabolome to Identify Potential Markers for Early Diagnosis and Therapeutic Targets of Alzheimer’s DiseaseStewart F. Graham, Olivier P. Chevallier, Dominic Roberts, Christian Hölscher, Christopher T. Elliott, and Brian D. Green



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Section: Electric Phenomena

Contactless Surface Conductivity Mapping of Graphene Oxide Thin Films Deposited on Glass with Scanning Electrochemical MicroscopyJoel Azevedo, Céline Bourdillon, Vincent Derycke, Stéphane Campidelli, Christine Lefrou, and Renaud Cornut

pp 1812–1818Publication Date (Web): December 22, 2012 (Article)DOI: 10.1021/ac303173d


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Structural Analysis of Low Molecular Weight Heparin by Ultraperformance Size Exclusion Chromatography/Time of Flight Mass Spectrometry and Capillary Zone ElectrophoresisQianqian Zhang, Xi Chen, Zhijia Zhu, Xueqiang Zhan, Yanfang Wu, Lankun Song, and Jingwu Kang



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Section: Magnetic Phenomena

Iterative Thresholding Algorithm for Multiexponential Decay Applied to PGSE NMR DataMateusz Urbańczyk, Diana Bernin, Wiktor Koźmiński, and Krzysztof Kazimierczuk



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Determination of Percent Hemoglobin A1c Using a Potentiometric MethodHong Liu and Richard M. Crooks



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Section: Surface Chemistry and Colloids

Chemically Irreversible Redox Mediator for SECM Kinetics Investigations: Determination of the Absolute Tip–Sample DistanceSebastien Lhenry, Yann R. Leroux, and Philippe Hapiot

pp 1840–1845Publication Date (Web): January 3, 2013 (Article)DOI: 10.1021/ac303226e


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Toward the Development of Raman Spectroscopy as a Nonperturbative Online Monitoring Tool for Gasoline AdulterationKhay M. Tan, Ishan Barman, Narahara C. Dingari, Gajendra P. Singh, Tet F. Chia, and Wee L. Tok


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Section: Food and Feed Chemistry

Characterization of Triacylglycerol Enantiomers Using Chiral HPLC/APCI-MS and Synthesis of Enantiomeric TriacylglycerolsMiroslav Lísa and Michal Holčapek

pp 1852–1859Publication Date (Web): January 8, 2013 (Article)DOI: 10.1021/ac303237a


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Paper-Based Solid-Phase Nucleic Acid Hybridization Assay Using Immobilized Quantum Dots as Donors in Fluorescence Resonance Energy TransferM. Omair Noor, Anna Shahmuradyan, and Ulrich J. Krull



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Automated Circular Dichroism Spectroscopy for Medium-Throughput Analysis of Protein ConformationSebastian Fiedler, Lindsay Cole, and Sandro Keller

pp 1868–1872Publication Date (Web): December 19, 2012 (Article)DOI: 10.1021/ac303244g

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Liquid Chromatography, Chemical Oxidation, and Online Carbon Isotope Dilution Mass Spectrometry as a Universal Quantification System for Nonvolatile Organic CompoundsSergio Cueto Díaz, Jorge Ruiz Encinar, Alfredo Sanz-Medel, and J. Ignacio García Alonso


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Top Down Proteomics of Human Membrane Proteins from Enriched Mitochondrial FractionsAdam D. Catherman, Mingxi Li, John C. Tran, Kenneth R. Durbin, Philip D. Compton, Bryan P. Early, Paul M. Thomas, and Neil L. Kelleher



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Section: Radiation Biochemistry

Method for Determination of Neptunium in Large-Sized Urine Samples Using Manganese Dioxide Coprecipitation and 242Pu as Yield TracerJixin Qiao, Xiaolin Hou, and Per Roos


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Section: Pharmacology

Development and Validation of the First Liquid Chromatography-Tandem Mass Spectrometry Assay for Simultaneous Quantification of Multiple Antiretrovirals in MeconiumSarah K. Himes, Karl B. Scheidweiler, Katherine Tassiopoulos, Deborah Kacanek, Rohan Hazra, Kenneth Rich, Marilyn A. Huestis, and Pediatric HIV/AIDS Cohort Study



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Sub 2-μm Macroporous Silica Particles Derivatized for Enhanced Lectin Affinity Enrichment of GlycoproteinsBenjamin F. Mann, Amanda K. P. Mann, Sara E. Skrabalak, and Milos V. Novotny

pp 1905–1912Publication Date (Web): January 1, 2013 (Article)DOI: 10.1021/ac303274w


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Glutathione-Protected Silver Nanoclusters as Cysteine-Selective Fluorometric and Colorimetric ProbeXun Yuan, Yuanqi Tay, Xinyue Dou, Zhentao Luo, David Tai Leong, and Jianping Xie



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Room-Temperature Phosphorescent Discrimination of Catechol from Resorcinol and Hydroquinone Based on Sodium Tripolyphosphate Capped Mn-Doped ZnS Quantum DotsHe-Fang Wang, Ye-Yu Wu, and Xiu-Ping Yan

pp 1920–1925Publication Date (Web): December 27, 2012 (Article)DOI: 10.1021/ac303374s


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Novel Monoisotopic 109AgNPET for Laser Desorption/Ionization Mass SpectrometryJoanna Nizioł, Wojciech Rode, Barbara Laskowska, and Tomasz Ruman

pp 1926–1931Publication Date (Web): December 30, 2012 (Article)DOI: 10.1021/ac303770y


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Direct Detection of Bacterial Genomic DNA at Sub-Femtomolar Concentrations Using Single Molecule ArraysLinan Song, Dandan Shan, Mingwei Zhao, Brian A. Pink, Kaitlin A. Minnehan, Lyndsey York, Melissa Gardel, Sean Sullivan, Aaron F. Phillips, Ryan B. Hayman, David R. Walt, and David C. Duffy

pp 1932–1939Publication Date (Web): January 18, 2013 (Article)DOI: 10.1021/ac303426b


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Appropriate Solvent NaVO3 for Composition Analysis of LiNbO3 Crystal Using Chemical MethodDe-Long Zhang, Jian Gao, Ping-Rang Hua, Dao-Yin Yu, and Edwin Yue-Bun Pun


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Polymeric Membrane Neutral Phenol-Sensitive Electrodes for Potentiometric G-Quadruplex/Hemin DNAzyme-Based BiosensingXuewei Wang, Zhaofeng Ding, Qingwei Ren, and Wei Qin



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Picking up the Pieces: A Generic Porous Si Biosensor for Probing the Proteolytic Products of EnzymesGiorgi Shtenberg, Naama Massad-Ivanir, Oren Moscovitz, Sinem Engin, Michal Sharon, Ljiljana Fruk, and Ester Segal



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Section: Enzymes


Inaccuracies of Nitric Oxide Measurement Methods in Biological MediaRebecca A. Hunter, Wesley L. Storm, Peter N. Coneski, and Mark H. Schoenfisch

pp 1957–1963Publication Date (Web): January 3, 2013 (Article)DOI: 10.1021/ac303787p


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