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�
Material: SDVBParticleSize: 5,10,�0µmPorosities: 50Åto106Å,andmixedbedsTypicalPressure: 5µm:350psi10µm:�00psiMaximumPressure: 1000psiMaximumTemperature: 140°CMinimumEfficiency*: 5µm: 45,000p/m** 10µm: 35,000p/m**TypicalFlowRates: 4.6mmID: 0.35mL/min 7.8mmID: 1.0mL/min�1.�mmID: 8.0mL/minEndFittings: Valco®Compatible* Tested in THF ** For 300 x 7.8 mm ID columns
ElutionVolume/Column(mL)
Poly
styr
ene
Mol
ecul
arW
eigh
t
Highlycross-linkedformechanicalandchemicalstability
Narrowbore(4.6mmID)solvent-savertopreparativecolumnsavailable
Temperaturestableto140°C/�05°C*
Phenogel packing materials are madefrom styrene-divinylbenzene by emulsionpolymerization under conditions to optimizepore size, total pore volume, particle size,and degree of cross-linking. The resultsyield GPC materials that provide very highresolution,ruggeddurability,andwidesolventcompatibility.
Phenogelisavailableinsevendifferentporesizesrangingfrom50Åto106Å,andauniqueLinear(�)configuration.Poresizedistributionand pore volume are closely controlledparameters in the manufacturing process;attentiontothesedetailsaccountsforthehighresolutionandtightlinearcalibrationcurvesassociated with Phenogel, as well as theexcellentcolumn-to-columnreproducibility.
*PhenogelUltraTempcolumnsavailableuponrequest.
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Column Selection by Molecular Weight
Sample Type Molecular Weight Phenogel Column
SmallOrganics 100-3K 50Å 500-6K 100Å 1K-15K 500ÅResins 1K-75K 103Å 5K-500K 104Å 10K-1,000K 105ÅHighMWPolymers 60K-10,000K 106Å 100-10,000K Linear(�)
Column Molecular Weight Calibration Curves
SEM Photos of Phenogel Polymer Beads
103 Å 106 Å
Technical Specifications
If Phenogel does not provide at least equivalent separation as compared to a competing column of the similar particle size, phase, and dimensions, send in your comparitive data within 45 days and keep the column for FREE.
Phenogel™ GPC Materials
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N = Not Compatible
Y = Compatible
Phenogel Pore Size: LInear Suggested Mobile Phase Solvent 50 Å 100 Å 500 Å 103 Å 104 Å 105 Å 106 Å & Mixed Operating Temp.
Acetone Y Y Y Y Y Y Y Y
Benzene Y Y Y Y Y Y Y Y
CarbonTetrachloride Y Y Y Y Y Y Y Y
Chloroform Y Y Y Y Y Y Y Y
30%HFIP/Chloroform Y Y Y Y YY Y Y
DiethylEther Y Y Y Y Y Y Y Y
Dimethylacetamide(DMAC) Y* Y Y Y Y Y Y Y 60°C
Dimethylformamide(DMF) Y* Y Y Y Y Y Y Y 60°C
Dioxane Y Y Y Y Y Y Y Y
DMSO Y* Y Y Y Y Y Y Y 60°C
EthylAcetate Y Y Y Y Y Y Y Y
Hexafluoroisopropanol(HFIP) Y Y Y Y Y Y Y Y
Hexane Y Y Y Y Y Y Y Y
M-Cresol Y* Y Y Y Y Y Y Y 100°C
MethylEthylKetone Y Y Y Y Y Y Y Y
MethyleneChloride Y Y Y Y Y Y Y Y
0-Chlorophenol Y* Y Y Y Y Y Y Y 100°C
0-Dichlorobenzene Y* Y Y Y Y Y Y Y 135°C
Quinolin Y* Y Y Y Y Y Y Y 60°C
Tetrahydrofuran Y Y Y Y Y Y Y Y
Toluene Y Y Y Y Y Y Y Y
Trichlorobenzene Y* Y Y Y Y Y Y Y 135°C
Water N N N N N N N N
Xylene Y Y Y Y Y Y Y Y
*Not recommended on 5 µm 50 Å columns.
Solvent Compatibility Table
Recommended Suggested GPC Solvent Sample Temp.THF Polystyrenes Ambient
Polybutadienes
PolyethyleneOxide 50°C
EpoxyResins
PhenolicResins Ambient
Polymethacrylates
PolyethyleneGlycol
HFIP** Polyamides(Nylon) 30°C
PETP (polyethyleneterephthalate)
Dichloromethane Naphthalene
DiethylhexylPhthalate Ambient
Toluene Polyisobutlylene Ambient
Polyisoprene
SiliconeOils
DMF ChlorinatedRubber
**HFIP (hexafluoroisopropanol) allows polymers such as polyamides and PET that are analyzed at temperature of 135 °C and higher to be analyzed at temperatures below 100 °C. The narrow particle distribution of Phenogel columns eliminates the problem of overlapping peaks and brand broadening that is typically associated with using this solvent with traditional GPC columns.
Solvent Selection Table
Phenogelcolumnsarepackedintetrahydrofuran(THF)
ColumnscanalsobeshippedinsolventssuchasDMF,MethyleneChloride,NMP,ando-CP,tohelpminimizeequilibrationtime
Phenogelcolumnsmaintainexcellentsolventcompatibility and high efficiency duringsequentialsolventswitchesfrom:
THFËDMFËTolueneËCHCI3ËDMF
(ambienttemp)ËDMF(50°C)Ë THFËNMP
Ë DMSOË THF Ë DMSOË Methanol
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Althoughstyrene-divinylbenzenematerialsareexceptionally inert, interaction between thecolumnpackingandsamplematerials(especiallyverypolarsolutes)occasionallyoccursandthemobilephasemustbemodified toeliminatethiseffect.Phenogelcolumnscantolerateupto0.1%lowMWamines,0.5%glacialaceticacid,orupto1%waterinthemobilephaseasmodifiers.
Phenogelcolumnsaretemperaturestableto140°Cto�05°C(PhenogelUltraTemp)whichisimportantforapplicationsinvolvingsoluteswithlimitedsolubilityatambienttemperatures
or where solubility considerations demandtheuseofviscoussolventssuchasDMForDMSO.Athighertemperatures,eluentviscosityisdecreasedandmasstransferisenhanced,withtheeffectofincreasingsampleresolution.Thistemperaturestabilityisparticularlyusefulwhenanalyzingpolymerssuchaspolyethyleneand polypropylene which require highertemperatures.
Solvent and Temperature Compatibility
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Solvent Miscibility Table
AlthoughPhenogel columnsare ruggedandcan withstand strong solvent changes, careshould be exercised when switching fromhigh-swellsolvents(A)tolow-swellsolvents(B,C,andD),seediagramatright.Impropersolvent switches can result in a void. Bestresults are attained when an intermediate-swell solvent is used, and column lifetimeis improved.ContactPhenomenexregardingsolventsnotlistedbelow.
Columnlifecanbemaximizedbydedicatingcertaincolumnstocertainsolvents.Thiswillalsominimizesolventswitches.Ifcareisnottaken,avoidmayoccur.
Reduceflowrateto0.�mL/min
BackpressuremustNEVERexceed1000psi
AlwayschecksolventmiscibilityinabeakerorfollowthesolventmiscibilitytablebelowbeforeproceedingwithANYsolventswitch.
Comparetheswellcharacteristicsofsolvent1(oldsolvent)tosolvent�(newsolvent)andfollowtheguidelinesatright.
Ifsolvent1andsolvent2belongtothesameswellcategory(seetableatright),checkthesolventmiscibilityandproceedwiththeswitch.
Ifsolvent1andsolvent2belongtosuccessiveswellcategoriesasindicated bythearrowsinthetableatright,checkthemiscibilityandproceedwiththeswitch.
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Ifsolvent1andsolvent2DONOTbelongtothesameORsuccessiveswellcategories,switchtoanintermediatesolventFIRST,asindicatedbythearrowsinthetable.
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Solvent Switching Considerations
Solvent Switching
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Cyclic Polymer CharacterizationColumn: Phenogel 10 µm Linear(2) Dimensions: 600 x 7.8 mmPart No: 00K-3260-K0Mobile Phase: THF with 1 % TEAFlow Rate: 1.3 mL/minDetection: UV @ 268 nmInjection Volume: 40 µL 0.2 % w/vTemperature: AmbientSample: Poly-(2-Vinylpyridine) [0.05 % - 0.25 % (w/v)]
App
ID 5
441
Fractionated
13 14 15 16 17 18
Crude
10 11 12
Elution Vol (mL) SEC traces of solutions of cyclic P2VP which contain the indicated percentages of added linear precursor (dotted line is ‘pure’ cyclic P2VP)
Cyclic Polymer Characterization Column: Phenogel 10 µm Linear(2)Dimensions: 600 x 7.8 mmPart No: 00K-3260-K0Mobile Phase: THF with 1 % TEAFlow Rate: 1.3 mL/minDetection: UV @ 268 nmInjection Volume: 7 µL 1.25 % w/vTemperature: AmbientSample: Poly-(2-Vinylpyridine) [0.05 % - 0.25 % (w/v)]
App
ID 5
440
Nylon 6 in HFIP Column: Phenogel 10 µm Linear(2) x 2Dimensions: 300 x 7.8 mmPart No: 00H-3260-K0Mobile Phase: HFIP (0.01 M NATFAT)Flow Rate: 1.0 mL/minDetection: Differential RefractometerInjection Volume: 100 µL 0.025 % w/vTemperature: 30 °CSample: 14,500 MW
App
ID 5
445
MIxed Polystyrene Standard on Linear (2) Column
Column: Phenogel 5 µm Linear(2)Dimensions: 300 x 7.8 mmPart No: 00H-3259-K0Mobile Phase: THFFlow Rate: 1.0 mL/minDetection: RlInjection Volume: 50 µL Temperature: 35 °CSample: Polystyrene standards injected 1. 2,860,000 MW 2. 277,000 MW 3. 9,350 MW
App
ID 5
444
Linearcalibrationto10millionDaltons
Excellentmechanicalstability
Excellentforanalyzingawiderangeofmolecularweights
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Phenogel Linear Columns
Applications on Phenogel Linear Non-Aqueous GPC Columns
Calibration Curve: Linear(2)Phenogel 5 µm 300 x 7.8 mm
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Polyvinyl Butyral Column: Phenogel 5 µm 500 Å, 103 Å, 104 Å, 105 ÅDimensions: 300 x 7.8 mmSolvent: THFFlow Rate: 1.0 mL/minDetection: Differential RefractometerInjection Volume: 100 µL 0.25 % w/v Temperature: 25 °CSample: 300,000 MW
App
ID 5
438
Organic Compounds Column: Phenogel 10 µm 100 ÅDimensions: 250 x 21.2 mmOrder No: 00G-0642-P0Mobile Phase: DichloromethaneFlow Rate: 4.0 mL/minDetection: UV @254 nmTemperature: AmbientSample: 1. Diethylhexyl Phthalate 2. Biphenyl 3. Naphthalene 4. Coronene 5. Sulfur
App
ID 5
430
Polyethylene Oxide (PEO) Column: Phenogel 10 µm 105 Å, 104 Å, 103 ÅDimensions: 300 x 7.8 mmMobile Phase: DMF (0.1M LiBr)Flow Rate: 1.0 mL/minDetection: Differential RefractometerInjection Volume: 100 µL 0.125 % w/v Temperature: 50 °CSample: 400,000 MW
App
ID 5
434
Polyethylene Glycol 330Column: Phenogel 5 µm 50 Å, 100 Å, 500 ÅDimensions: 300 x 7.8 mmSolvent: THFFlow Rate: 1.0 mL/minDetection: Differential RefractometerInjection Volume: 100 µL 0.25 % w/v Temperature: AmbientSample: 1. dp7 546 MW 5. dp3 194 MW 2. dp6 458 MW 6. dp2 106 MW 3. dp5 370 MW 7. dp1 62 MW 4. dp4 282 MW
App
ID 5
433
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
Rel I
nten
X10
-1
20.00 21.00 22.00 23.00 24.00 25.00 26.00 27.00
Ret Vol (mL)
1
2
3
6
7
45
Refrac Chromatogram
Closely Related Hydrocarbons Column: Phenogel 5 µm 50 Å, 100 Å, 500 ÅDimensions: 300 x 7.8 mmSolvent: THFFlow Rate: 1.0 mL/minDetection: Differential RefractometerInjection Volume: 100 µL 0.25 % w/v Temperature: AmbientSample: 1. C40 562 MW 4. C20 282 MW 2. C32 450 MW 5. C16 226 MW 3. C24 338 MW 6. C13 184 MW
App
ID 5
432
Phenogel Non-Aqueous GPC/SEC 50 Å - 106 Å Columns
Highresolutionatlowcost
Customizeyouranalysisbycouplingdifferentpore-sizecolumns
Widerangeofsolventcompatibility
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Phenolic ResinsColumn: Phenogel 5 µm 500 Å x 2, 103 Å, 104 ÅDimensions: 300 x 7.8 mmSolvent: THFFlow Rate: 1.0 mL/minDetection: RlInjection Volume: 5 µL Temperature: 25 °CSample: Phenolic Aldehyde Resin, MW 500 to 470 K
App
ID 5
429
Applications on Phenogel Non-Aqueous GPC/SEC Columns
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Polystyrenes (Wide MW Range) Column: Phenogel 10 µm 105 Å, 104 Å, 103 ÅDimensions: 300 x 7.8 mmSolvent: THFFlow Rate: 1.0 mL/minDetection: Differential RefractometerInjection Volume: 100 µL 0.25 % w/v Temperature: AmbientSample: 1. 1,560,000 MW 5. 6,100 MW 2. 260,000 MW 6. 854 MW 3. 94,000 MW 7. 146 MW 4. 30,000 MW
App
ID 5
435
Poly - (a)-Metahyl Styrene) (Wide MW Range)Column: Phenogel 5 µm 105 Å, 104 Å, 103 Å, 500 ÅDimensions: 300 x 7.8 mmSolvent: THFFlow Rate: 1.0 mL/minDetection: Differential RefractometerInjection Volume: 100 µL 0.25 % w/v Sample: 1. 680,000 MW 2. 90,000 MW 3. 30,000 MW 4. 6,000 MW
App
ID 5
439
Polybutadines (Wide MW Range) Column: Phenogel 5 µm 105 Å, 104 Å, 103 Å, 500 ÅDimensions: 300 x 7.8 mmSolvent: THFFlow Rate: 1.0 mL/minDetection: Differential RefractometerInjection Volume: 100 µL 0.25 % w/v Sample: 1. 420,000 MW 2. 24,000 MW 3. 2,500 MW 4. 500 MW
App
ID 5
437
Polymethyl Methacrylates (Wide MW Range)Column: Phenogel 5 µm 105 Å, 104 Å, 103 Å, 500 ÅDimensions: 300 x 7.8 mmSolvent: THFFlow Rate: 1.0 mL/minDetection: Differential RefractometerInjection Volume: 100 µL 0.25 % w/v Sample: 1. 700,000 MW 2. 107,000 MW 3. 27,000 MW
App
ID 5
431
Isoprenes from In Vitro Translation on Products Column: Phenogel 5 µm 50 Å, 100 Å in series Dimensions: 300 x 7.8 mm Mobile Phase: THF Flow Rate: 0.25 mL/min Detection: Differential Refractometer Sample: 1. Squalene C30 (2, 6, 10, 15, 19, 23-Hexamethyltetracosane) 2. Phytane C20 (2, 6, 10, 14-Tetramethylhexadane) 3. Farnesne C15 (2, 6, 10-Trimethyldodecane)
App
ID 5
436The columns were used in tandem to characterize
isoprenechainlengthsremovedfromlabeledinvitro
translationproductsorcellproteins.Theisoprenoids
were removed by treatment with Raney nickel and
extracted into pentane. The pentane extractable
materialwashydrogenatedoverplatinumcatalystand
injectedontothecolumn.Fractionswerecollectedat
0.5minuteintervalsandradioactivitywasmonitoredby
liquidscintillation.Thesesaturatedhydrocarbonchains
werecharacterizedbycomparingradioactivepeaksto
standardretentiontimes.
ChromatogramcourtesyofW.MalteseandR.Erdman,
WeisCenterforResearch,GeisingerClinic.
3
21
45 50 55 min
0 10 20 30 40 min
2
1
3
4
Phenogel Non-Aqueous GPC/SEC 50 Å - 106 Å Columns (continued)
Applications on Phenogel Non-Aqueous GPC/SEC Columns
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Decreasesolventconsumption
Retainsameelutionprofile
Reducesolventdisposalcosts
Phenogel-NB (NarrowBore) columns areoptimizedtoreducesolventconsumption.ThePhenogel-NBcolumnshavea4.6mmcolumnIDandrunat0.35mL/minute,reducingsolventconsumptionanddisposalcostsupto65%!
Loading
WithnarrowboreGPC/SECcolumns,thevolumein which the sample elutes is significantlydecreased, thus increasing the effectiveconcentrationof thesample.This increase insensitivityisexploitedinHPLC,butinGPCitleadstooverloadingeffectsandproportionallylowersampleloadingsmustbeused.
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High-temperaturecolumnstabilityupto�05°C
Improvedanalysisofultra-highmolecularweightpolymers
Virtuallyfreefromsheardegradation
Excellentchemicalstability
Custom-packinginothersolvents
PhenogelUltraTempisaseriesofthreehighefficiency,extremelyrugged,nonaqueousGPCcolumns forultra-high temperatureanalysis
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ChromatographicScienceSeriesVol.69.Chi-SanWu.1995.453pp.
Thissingle-sourcereferencedetailsthepracticaluseofsizeexclusionchromatography(SEC)incharacterizingthemolecularweightdistributionofimportantpolymericmaterialsaddressingproblemsencounteredinSECofspecificsubstances,includingcopolymers,polyamides,polyvinylalcoholandacetate,ligninderivative,proteinsandstarch.SECcolumntechnologyisthoroughlyreviewed,andtheuseofsemi-rigidpolymergelsandmodifiedsilica-basedpackingmaterialsisclearlydelineated.Writtenbymorethan�5internationallyrenownedauthoritiesintheirrespectivefields,theHandbook of Size Exclusion Chromatographyisaninvaluableresourceforpolymerchromatographers.
Part No.: AA0-3346
ofpolymers.Theresinsarebasedonhighlycross linked poly (styrene-divinylbenzene),resulting in excellent mechanical, chemicaland thermal stability.The result is a robustcolumnvirtuallyfreefromsheardegradation,with exceptional solvent compatibility, andprolonged operational life at ultra-hightemperatures.Analysisattemperaturesfrom100upto�05°Carepossible,makingthesecolumnsanexcellentchoicefortheanalysisofrefractorypolymersofultra-highmolecular
Phenogel-Narrow Bore: An Improved Dimension in GPC Analysis
weight, such as high-density polyethyleneand polypropylene. Columns are highlyresistanttomostaggressiveorganicsandcantoleratefrequentmobilephasechangeovers,with nominal gel shrinking and swelling.Custom co lumns packed wi th o thersolvents such as o-dichlorobenzene,tetrachloroethaneanddimethylformamideareavailableuponrequest.
Phenogel UltraTemp Columns
Handbook of Size Exclusion Chromatography
Reduced Solvent and High Temperature Stability
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Othercolumndimensionsavailable.PhenogelcolumnsareroutinelyshippedinTHF.However,columnsarealsoavailablein
commonlyusedsolventssuchasTolueneandChloroformaswellasDMF,NMP,andothersolvents.Refertothechartatthe
rightfortheadditionalchargefortheseshippingsolvents.Pleasespecifyshippingsolventwhenordering.
5 µm Columns (mm) GuardsPore Size MW Range 300 x 7.8 600 x 7.8 300 x 21.2 50 x 7.8 I I I I 50 Å 100-3 K 00H-0441-K0 — — 03B-2088-K0100 Å 500-6 K 00H-0442-K0 00K-0442-K0 — 03B-2088-K0500 Å 1 K-15 K 00H-0443-K0 00K-0443-K0 — 03B-2088-K010-3 Å 1 K-75 K 00H-0444-K0 — — 03B-2088-K010-4 Å 5 K-500 K 00H-0445-K0 00K-0445-K0 00H-0445-P0 03B-2088-K010-5 Å 10 K-1,000 K 00H-0446-K0 00K-0446-K0 00H-0446-P0 03B-2088-K010-6 Å 60 K-10,000 K 00H-0447-K0 00K-0447-K0 00H-0447-P0 03B-2088-K0
Mixed Beds I I I I — Linear (2) 100-10,000 K 00H-3259-K0 00K-3259-K0 — 03B-2088-K0
Other Shipping Solvents:
Methanol,MethyleneChloride,Cyclohexane,EthylAcetate,
NMP,DMAC,DMF
Size (mm) Price
30 x 4.650 x 4.6300 x 4.6300 x 7.8600 x 7.8300 x 21.2600 x 21.2
NOTE: Phenogel columns are routinely shipped in THF. Columns can be shipped in Toluene and Chloroform upon request at no additional charge.
Company Column
Jordi Associates Jordi™ GPC-DVBPolymer Labs PLgel™
Waters Styragel®
µStryagel®
Ultrastyragel®
Styragel HT®
Styragel HR®
Phenogel Columns are a Direct Equivalent to:
Ordering Information
If Phenogel does not provide at least equivalent separation as compared to a competing column of the similar particle size, phase, and dimensions, send in your comparitive data within 45 days and keep the column for FREE.
5 µm Narrow Bore (NB) Columns (mm) GuardsPore Size MW Range 300 x 4.6 30 x 4.6 I I 50 Å 100-3 K 00H-0441-E0 03A-2088-E0100 Å 500-6 K 00H-0442-E0 03A-2088-E0500 Å 1 K-15 K 00H-0443-E0 03A-2088-E010-3 Å 1 K-75 K 00H-0444-E0 03A-2088-E010-4 Å 5 K-500 K 00H-0445-E0 03A-2088-E0
10 µm Columns (mm) GuardsPore Size MW Range 300 x 7.8 600 x 7.8 300 x 21.2 600 x 21.2 50 x 7.8 I I I I I 50 Å 100-3 K 00H-0641-K0 00K-0641-K0 00H-0641-P0 00K-0641-P0 03B-2090-K0100 Å 500-6 K 00H-0642-K0 00K-0642-K0 00H-0642-P0 00K-0642-P0 03B-2090-K0500 Å 1 K-15 K 00H-0643-K0 00K-0643-K0 — 00K-0643-P0 03B-2090-K010-3 Å 1 K-75 K 00H-0644-K0 00K-0644-K0 00H-0644-P0 00K-0644-P0 03B-2090-K010-4 Å 5 K-500 K 00H-0645-K0 00K-0645-K0 00H-0645-P0 00K-0645-P0 03B-2090-K010-5 Å 10 K-1,000 K 00H-0646-K0 00K-0646-K0 00H-0646-P0 00K-0646-P0 03B-2090-K010-6 Å 60 K-10,000 K 00H-0647-K0 00K-0647-K0 00H-0647-P0 00K-0647-P0 03B-2090-K0
Mixed Beds I I I I I Linear (2) 100-10,000 K 00H-3260-K0 00K-3260-K0 00H-3260-P0 — 03B-2090-K0
PhenogelandThermaSpherearetrademarksofPhenomenex,Inc.
Styragel,µStyragel,Ultrastyragel,andStyragelHTareregisteredtrademarksofWatersCorporation.PLgelisatrademarkofPolymerLabs.JordiisatrademarkofJordiAssociates.PhenomenexisinnowayaffiliatedwithWatersCorporation,PolymerLabs,orJordiAssociates.©2008Phenomenex,Inc.Allrightsreserved.
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Aqueousandorganicstandards
Low,medium,high,andultra-highmolecularweightsavailable
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Aqueous SEC (GFC) Calibration Kits
Polystyrenes Part No. MW Kit Description Mp Range Unit PriceALO-2761 I Low MW Narrow MWD Kit I 8 Standards I 100-10,000 I 250 mg/standard I
ALO-2762 Medium MW Narrow MWD Kit 6 Standards 10,000-100,000 250 mg/standard
ALO-2763 High MW Narrow MWD Kit 6 Standards 120,000-1,850,000 250 mg/standard
ALO-2765 Broad MW Narrow MWD Kit 7 Standards 500-250,000 1.0 g/standard
Narrow,mediumandbroadmolecularweightdistribution
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Dextrans (Polysaccharides) Part No. MW Kit Description Mp Range Unit PriceALO-2771 I Branched, Kit I 7 Standards I 200-50,000 I 250 mg/standard I
ALO-2772 Branched, Broad MWD Kit 8 Standards 10-2,000,000 1.0 g/standard
Polyethylene Glycols Part No. MW Kit Description Mp Range Unit PriceALO-2774 I Narrow MWD Kit I 10 Standards I 100-22,500 I 1.0 g/standard I
Polystyrene Sulfonates Part No. MW Kit Description Mp Range Unit PriceALO-4423 I Broad MWD Kit I 10 Standards I 1,000-2,000,000 I 250 mg/standard I
Polyethylene Oxides Part No. MW Kit Description Mp Range Unit PriceALO-2775 I Narrow MWD Kit I 6 Standards I 20,000-1,000,000 I 250 mg/standard I
Organic SEC (GPC) Calibration Kits
AllcalibrationkitscontainstandardsthatareuniformlyseparatedlogarithmicallytogiveequallydistributeddatapointsonacalibrationcurveovertheMp(peakmolecularweight)rangestated.
Polymer Calibration Standards Kits
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Features
Compactandlightweight
Transparentcompartmentcover
Micro-fanprovidesrapidthermalequilibration
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Specifications:
Column Sizes Accommodated:Fitsuptoone30cmlengthcolumn,or�5cmcolumnwithguardcolumn.Multipleinletandoutletslotsallowtheshortestlengthoftubingtobeusedwithanylengthcolumn.
Temperature Range:From�5to90°Cin0.1°Cincrements.
Temperature Stability:±0.1°CCalibrationtwo-point,electronic,factoryset.
Power:1�voltDCuniversalpowersupplytakesvoltageinputsfrom95VACto�65VAC,50/60Hz.CEapproved.
Over-Temperature Alarm:Audiblewithautomaticheatershutoffifcolumntemperatureexceeds10°Coftargettemperature.
Auto-Off Timer:Countdowntimerwithaudiblealarmturnsoffheater,settableto30daysindays,hours,minutesandseconds
Injection Counter:Triggeronexternalswitchclosure
Essential For
Polymeranalysisandcharacterization
Controllingpolymerformulations
Qualitysystemsassurance(GLP,GMP,ISO)
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Benefits
ImprovesGPCchromatographicreproducibility
Increasessamplethrough-put(fasterrun-time)
Improvespeakefficiencyandcomponentresolution
Improvesbaselineandoveralldetectorperformance
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1.TheThermaSphereTS-130iswarrantedforoneyearparts
andlabor.Eachunitisindividuallycalibratedandcomeswitha
CertificateofPerformance.Noadjustmentorre-calibrationis
evernecessary.CEapproved,ULandCSAapprovalpending.
�.PleasespecifyLineCordifotherthanU.S.(Australia,Germany,
ItalyandU.K.areavailable)
ThermaSphere TS-130 Column Heater
Part No. Description Price
EH0-7057 ThermaSphere TS-130 HPLC Column Heater 25-90 °C, 95 to 265 VAC, 50/60 Hz
EH0-7058 Stand for ThermaSphere TS-130 HPLC Column Heater
Use a ThermaSphere™ TS-130 Column Heateryou need constant temperature.
For Improved GPC Reproducibility,
If you are not completely satisfied with the performance of your new TS-130 column heater, simply return the unit within 60 days of purchase for A FULL REFUND.
www.phenomenex.com¢
5488
_I
AustraliaPO Box 4084Lane Cove, NSW 2066Australia
mail:
tel.:fax:
email:
mail:
tel.:fax:
email:
AustriaZeppelinstr. 563741 AschaffenburgGermany
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(800) 543-3681(310) [email protected]
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01 247 5405+44 [email protected]
ItalyVia Serenari, 15/D40013 Castel Maggiore (BO)Italy
051 6327511051 [email protected]
New ZealandP O Box 31-601Milford 0741North Shore CityNew Zealand
DenmarkGydevang 39-413450 AllerødDenmark
4824 80484810 [email protected]
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01 30 09 21 1001 30 09 21 [email protected]
GermanyZeppelinstr. 563741 AschaffenburgGermany
Puerto Rico273 Sierra Morena,Suite #104San Juan,Puerto Rico 00926
(800) 541-HPLC(310) [email protected]
United KingdomQueens Avenue,Hurds�eld Ind. Est.,Maccles�eld, Cheshire SK10 2BN, UK
USA411 Madrid Ave.Torrance, CA90501-1430USA
(310) 212-0555(310) [email protected]
www.phenomenex.comPhenomenex products are available worldwide. For the distributor in your country, contact Phenomenex USA, International Department by telephone, fax or email: [email protected].
