Precision Data working product wise for various modes of transport

8/7/2019 Precision Data working product wise for various modes of transport

1/25

Characteristic

770 7100.5

Distillation:(E-70), % v 45 10 1

Distillation:(E-100), % v 70 40 1

Distillation:(E-180), % v 90 1

215 1

88 0

88 0.2

4011.87

0.05

0.01

60 350.02

1 0.04

3 0.03

0.01

0

Application of Precision D

Test

MethodRequirements

LimitsRepetabilit

yUpper

Lower

Density @ 15oC, Kg/m3

P:16

P:18/ D:86

RON

Existent Gum, g/m3 P:29

Sulphur, Total % mass P:34

(RVP) at 38oC kPa P:39Benzene, % by Vol. D:3606

Lead, g/lit IP:352


2/25

1.2 769.29 710.71 770.71 709.29 769.29 710.71

3 43.23 11.77 46.77 8.23 43.23 11.77

3 68.23 41.77 71.77 38.23 68.23 41.77

3 91.77 88.23 #VALUE! 91.77

4 212.64 217.36 212.64 #VALUE!

1 88.59 87.41 #VALUE! 88.59

0.7 88.41 87.59 #VALUE! 88.41

23.33 26.24 53.76 26.24#VALUE!

0.01 0.04 0.06 0.0434#VALUE!

0.04 59.98 35.02 60.02 34.98 59.98 35.02

0.18 0.89 1.11 0.89#VALUE!

0.84 2.5 3.5 2.50#VALUE!

0.01 0.01 0.02 0.008#VALUE!

ata MS BSII IS 2796

Reproduci

bilityA1-A2>4R;

A1,A2>2R

Acceptable Margins,Supplier ,

Not OK Margins,Recipient ,

RemarksA1-0.59RA2+0.59RA1+0.59RA2-0.59R

60>4.8 OK35>12 OK30>12 OK90>6 OK

215>8 OK88>2 OK

88>1.4 OK

40>46.66 NOT OK

0.5>0.224 OK

25>0.16 OK1>0.36 OK3>1.68 OK. .

5 OK


3/25

770.71 709.29

46.77 8.23

71.77 38.23

#VALUE! 88.23

217.36 #VALUE!

#VALUE! 87.41

#VALUE! 87.59

53.76#VALUE!

0.0566#VALUE!

60.02 34.98

1.11#VALUE!

3.50#VALUE!

0.018#VALUE!


4/25

Characteristic

775 720 0.5 1.2

Distill:(E-70), % v 45 10 1 3

Distill:(E-100), % v 70 40 1 3Distill:(E-150), % v 75 1 3

210 1 8

91 0.2 0.7

5 2.1 4.04

0.02

0.01 0.01

60 0.02 0.04

1 0.04 0.18

42 1.6 3.5

21 1.6 6.80.01

0 0.01

Application of Precision Data

Test

MethodRequirements

Repetability

Reproduci

bilityUpper

Lower

Den @ 15oC, Kg/m3

P:18/ D:86

Sulphur, Total % m D:4294

o

Lead, g/lit IP:352


5/25

774.29 720.71 775.71 719.29

43.23 11.77 46.77 8.23

68.23 41.77 71.77 38.2376.77 73.23

205.28 214.72

91.41 90.59

2.62 7.38

0.01 0.02

59.98 60.02

0.89 1.11

39.94 44.07

16.99 25.01

0 0.01

S BSIII IS 2796

A1-A2>4R;

A1,A2>2R

Acceptable Margins,Supplier

Not OK Margins,Recipient

RemarksA1-0.59RA2+0.59RA1+0.59RA2-0.59R55>4.8 OK35>12 OK

30>12 OK75>6 OK210>16 OK91>1.4 OK5>8.08 NOT OK. .

8 NOT OK60>0.08 OK1>0.36 OK42>7.0 OK

21>13.6 OK. .5 NOT OK


6/25

Characteristic

1 860 820 0.5 1.2

2 0.01

0 0.01

3 0.3

0.04 0.06

4 0.25 0.04 0.05

5 0.05

0.01 0.05

6 Pour Point,oC,winter 3 3 6

7 Pour,oC,summer 15 3 6

8 48 0 2

9 35 1 1.5

10 5 2 0.02 0.04

5 2 0.01 0.01

11 Distill(E-350), % v 85 2 5

Distill:(E-370), % v 95 2 5

12 0.2 0.1 0.2

13 0.05 0.1 0.2

14 0.05

0.03 0.05

Application of Precision Data HSD

Sl. TestMethod

Requirements

Repetability

Reproduci

bilityUpper

Lower

Density @ 15oC, Kg/m3 Ash, % by Mass P:4

RCR, %by mass P:8

Sulphur, Total % m IP:336

K V, cSt at 40

o

C P:25P:18/ D:86

-

Sediment P:30


7/25

859.29 820.71 860.71 819.29

0.01 0.01

0.26 0.34

0.22 0.28

0.02 0.08

0 6.54

11.46 18.54

49.18 46.82

35.89 34.12

4.98 2.02 5.02 1.98

4.99 2.01 5.01 1.99

87.95 82.05

97.95 92.05

0.08 0.32

-0.07 0.17

0.02 0.08

IS 1460 BSII

A1-A2>4R;

A1,A2>2R

Acceptable Margins,Supplier

Not OK Margins,Recipient

RemarksA1-0.59RA2+0.59RA1+0.59RA2-0.59R40>4.8 OK

0.01=0.01 BORDER

0.3>0.124 OK0.25>0.1 OK

0.05>0.094 NOT OK15>12 OK3>12 NOT OK48>4 OK35>3 OK

3>0.14 OK3>0.06 OK85>10 OK95>10 OK

0.2>0.4 NOT OK0.05>0.4 NOT OK

0.05=0.05 BORDER


8/25

Characteristic

845 820 0.5 1.2

0.01 0

0 0.01

0.3 0

0.04 0.06

0.04 0

0.01 0.01

0 51 0 2

0 35 1 1.5

4.5 2 0.02 0.03

4.5 2 0.01 0.01

Distillation(E-360), % v 0 95 2 5

Water Content, %(v/v) 0.02 0

0 0.01CFPP,oC,winter 6 0 1 2

CFPP,oC,summer 18 0 0.5 1

0 25 6.7 13.1

11 0 1.77 3.83

0 460 63 120

Application of Precision Data HSD IS 1460 Test

MethodRequirements

Repetability

Reproduci

bilityA1-A2>4R;

A1,A2>2RUpper

Lower

Density @ 15oC, Kg/m3 25>4.8

Ash, % by Mass P:4 0.01=0.01

RCR, %by mass P:8 0.3>0.124

Sulphur, Total % mass D:4294. .

2

51>4

35>3

K V, cSt at 40 oC P:25 3>0.143>0.06

95>10

P:40 0.02=0.02 6>4

18>2

25>26.2

11>7.66

460>204


9/25

844.29 820.71 845.71 819.29

0.01 0.01 0.01 0.01

0.26 0.34 0.34 0.26

0.03 0.04 0.04 0.03

49.82 52.18 1.18 49.82

34.12 35.89 35.89 34.12

4.48 2.02 4.52 1.98

4.49 2.01 4.51 1.99

92.05 97.95 97.95 92.05

0.01 0.01 0.03 -0.01

4.82 7.18 7.18 4.82

17.41 18.59 18.59 17.41

17.27 32.73 32.73 17.27

8.74 13.26 13.26 8.74

389.2 530.8 530.8 389.2

SIIIAcceptable Margins,

SupplierNot OK Margins,

Recipient

RemarksA1-0.59RA2+0.59RA1+0.59RA2-0.59ROK

BORDER

OK

OKOKOKOKOKOK

BORDEROKOK

NOT OKOKOK


10/25

Characteristic

Nov-38 Nov-38

75 76 76

90 91.8 91 92

215 210 212 200 200 200

88 91 88.42 88.2 91.2 91.2

500 150 225 480 145 125

60 58 58

Benz, % v. Max. 1 1 0.89 0.9 0.9 0.9

3 0.03/.84 2.5 2.8

Cu Corr, Max.

Seven Critical Parameters for MS BSII- Rail/Road and PipelineBIS BSII

SpecsBIS BSIII

SpecsPrecision

Limits(Repet./Repro)

TestMarginsas per

ISO 4259based on

singletest

result

Rail/RoadMfg

Specs

BSII

Rail/RoadMfg

Specs

BSIII

P/L MfgSpecsBSIII

{2000ppm SKOinterface

}

Density @ 15oC,Kg/m3

710 770720-7750.5/0.12710.72-711-768*721-773721-773

Distill-Rec, 70oC , % v10 4510 45 - 11.8-43.211-38*

100oC , % v40 7040 70 - 41.8-68.241-70 41-70 41-70

150oC , % v-

180o

C , % v Min - FBP, oC, Max.

-

Sul % m, Max. 145/467

RVP at 38oC kPa 35 60 3.2/5.237.1-57.638-58*

0.04/0.18

- - - -


11/25

To take care of test margin

To take care of Testing Margin

Justification/Remarks

ethanolo a e care o s orage an

handling impact and upper limitto take care of addition of

ethanol

handling impact.

handling impact.

margin. UL to facilitate

absorption of ethanol


and production constraints


12/25

Characteristic

1 46 47.98 47

2 95 96.2 96

3 35 36.8 37

4 0.05 0.7 225 450

5 460 388 420

7 1

Seven Critical Parameters for HSD- Rail/Road and Pipeline

Sl. BISSpecs

PrecisionLimits

(Repetability/

Reproducibility)

Test Margins asper ISO 4259

based on single

test result

Rail/RoadMfg

Specs

Distillation :Recovery up to

370oC (E-370), % by Vol. Min-

Flash Point, Deg C, Min 1/1.5Sulphur, Total Percent by

Copper Strip Corrosion, for3hrs at 50oC, Max.

NA Qualitative test. NoPrecision limit

1a


13/25


To take care of Test marginrecovery higher than 95% to

To take care of test margin

To take care of TestingMargin

To take care of TestingTo improve product quality

further


14/25

Characteristic

1 Smoke Point, mm, Min. 18 2-Jan 19.8 19

2 300 297 290

4 2500 2160 2400

Four Critical Parameters for SKO- Rail/Road and Pipe

Sl. BISSpecs

PrecisionLimits

(Repetability/

Reproducibility)

TestMarginsas per

ISO 4259based on

singletest

result

Rail/RoadMfg

Specs

Distillation : FBP, Deg C,

-

Sulphur, Total % mass,

175/580


15/25


line


To take care of test margin. 20

for Rlys and 22 for Defence

owing to production difficulty.


16/25

Eight Critical parameters for ATF- RaiCharacteristic

1

25 23.2 20

2

0 0

3

3000 2700 2500

4 300 297 290

5 38 38.9 40

6 -47 -48.38 -49

8

Lubricity: WSD, mm, Max 0.78 0.65

Sl. BISS ecs

PrecisionLimits

TestMargins

Rail/Road

Mf S ecsAromatics, percent byvolume, Max 1.4/3.0Sulphur mercaptan, percent

by mass, Max

0.003/0.0

NA

Sulphur Total, ppm by mass,Max 50/175Final Boiling Point, oC, Max

-Flash point ( Abel ), oC, Min Freezing point, oC, Max

0.85/ 0.65 -


17/25

l/Road


Def Reqmt 20. Since product cannot be segregated

Def Reqmt 0.002

Def Reqmt 2500To take care of Test MarginTo take care of Test MarginTo take care of Test Margin

Def reqmnt-0.65


18/25

S Prod Characteristic Road/Rail Movement Coastal

1 MS Density

RON 0.5 unit > BS-II -88 0.5 unit > BS-II -88

BS-III-91 BS-III-91

Distillation 1% above of Min Range 1% above of Min Range

FBP

Benzene

RVP BS-I:38 Min; 58 Max BS-I:38 Min; 58 Max

BS-II: 58 Max BS-II: 58 Max

Sulfur 20 ppm < BS-II:500 ppm; 20 ppm < BS-II:500 ppm;

5 ppmBS-II: 95% Vol

Cetane Index -

Cetane No - 0.4>BS-II:48;BS-III:51

Flash Point

Lubricity 40< BS-II/BS-III: 460 mu 40< BS-II/BS-III: 460 mu

Oxidation stabili ty 3 35 oC

+/-0.002 @ 15 oC +/-0.002 @ 15 oParticulate Visual inspection- free from Visual inspection- free
mailto:+/-0.0025@%2015mailto:+/-0.002@%2015mailto:+/-0.002@%2015mailto:+/-0.0025@%2015mailto:+/-0.0025@%2015mailto:+/-0.0025@%2015mailto:+/-0.002@%2015mailto:+/-0.002@%2015mailto:+/-0.002@%2015mailto:+/-0.002@%2015mailto:+/-0.0025@%2015mailto:+/-0.0025@%2015


19/25

Water

Silver Strip Corr.

Copper Strip Corro

Lubricity Def- 0.65; Civil-0.85 Def- 0.65; Civil-0.85

Conductivity 250-450 PS/M

Using conductivity meter

S Test E:

1 Appearance

2

3 Flash Point

4 Existent Gum

5 Copper Strip Corrosion Test

6 Distillation

7 Doctor Test

8 Water Reaction

9 Freezing Point

30 ppm through Aquadischeck

Free from dissolved waterusing aquadis check

Test H after loading TT /Tank Wagon

Test E after loading

Test H after loading TT /Tank Wagon

Def-1; Civil-1 as perTestE after loading

250-450 PS/M usingconductivity meter

Density @ 15 oC

Note: The Customer may take product Coastally and push into cross country pipelinto take care of the Max/Min limits of the most stringent requirement. In ATF conductiTanks it has to be in the range of 350 + as per our experience factor.


20/25

Pipeline Transfers Guarantee to Customer

BS-II -88

BS-III-91

1% above of Min Range

BS-I:38 Min; 58 Max

BS-II: 58 Max

50 ppm < BS-II:500 ppm;

25 ppm 2 Cst for BS-II, BS-III BS-II: 2-5 Cst;

BS-III: 2-4.5 Cst

0.5>BS-II: 95% Vol

0.5 unit > BS-II: 46; BS-III 51 BS-II: 46;

BS-III 51

0.4>BS-II:48;BS-III:51 BS-II: 48;

BS-III 51

40< BS-II/BS-III: 460 mu BS-II: 460;

BS-III 460

3 BSII -88(93); BSIII-91 {whenSKO is intermediate Product}

BS-II Rec@70:10-45%;@100:40-70%@180: 90% Min

BS-III Rec@70:10-45%;@100:40-70%@150: 75% Min

Min 20 oC < BS-II:215 oC; BS-III:210 oC{when SKO is intermediate Product}

BS-II:215 oC;

BS-III:210 oC

0.2 35 oC BS-II/BS-III: 35o

C Min

BS-III: 25 g/m3, Max

+/-0.002 @ 15 oC
mailto:+/-0.002@%2015mailto:+/-0.0025@%2015mailto:+/-0.003@%2015mailto:+/-0.0025@%2015mailto:+/-0.0025@%2015mailto:+/-0.003@%2015mailto:+/-0.0025@%2015mailto:+/-0.002@%2015


21/25

(Qtly Millipore gravimetric test)

15 ppm using aquadis check

Def-1; Civil-2

Def-1; Civil-1

Def- 0.65; Civil-0.85 Def- 0.65; Civil-0.85

250-450 PS/M 50-450 PS/M

Using conductivity meter

Sr Test H:

1

2 Temperature

3 Appearance

4 Water / Sediments

Free from dissolved water using aquadischeck

Test H after commencement of PLT

Test H after commencement of PLT

Density @ 15 oC

We are producing only one Grade of ATF. Since the Defence Grade is morestringent, the Defence specs needs to be met so that we can supply to both civil aswell as defence requirements.

s at the destination. In such a eventuality, the manufacturing specs will haveity insisted ex Mktg Company is 250 PSM Min by OMCs. Therefore at ref


22/25

S Prod Characteristic Refinery to Mkt Coastal

1 MS Density

RON(AKI) - 0.5 unit > B

BS-III-91 BS-III-91FBP - -

Sulfur - 20 ppm B

Sulfur - -

4 ATF Density

1.0 mg/lit

Water

Silver Strip Corr. Def-0; Civil-1

Def-1; Civil-1

Road/RailMovement

BS-II-88(93)

Min 10oC <

III:210 oC

20 ppm < BS-II:500 ppm;

5 ppm


23/25

Lubricity Def- 0.65; Civil-0.85 Def- 0.65;

Conductivity 250-450 P

Using cond

s Test E:

1 Appearance

2

3 Flash Point

4 Existent Gum

5 Copper Strip Corrosion Test

6 Distillation

7 Doctor Test

8 Water Reaction

9 Freezing Point

Def- 0.65; Civil-0.85

300-450 PS/M usingconductivity meter

250-450 PS/Musing conductivity

Density @ 15 oC

Note: The Customer may take product Coastally and push into cross countryspecs will have to take care of the Max/Min limits of the most stringent requirMin by OMCs. Therefore at ref Tanks it has to be in the range of 350 + as per


24/25

Pipeline Transfers

S-II -88(93) BS-II -88(93)

BS-III-91(95)

S-II:500 ppm; 50 ppm < BS-II:500 ppm;

III:150 ppm 25 ppm 2 Cst for BS-II, BS-IIIBS-III: 2-4.5 Cst

S-II: 48; BS-III 51 0.5 unit > BS-II: 48; BS-III 51

BS-III 51

BS-III:350 ppm

775-840

0.22 mg/lit

Def-1; Civil-2

Def-1; Civil-1

Guarantee toCustomer

15 oC +/-0.0025 @ 15 oC BS-II :710-770;BS-III: 720-

1 unit > BSII -88(93); BSIII-91{when SKO is intermediate

Product}

BS-II:215 oC; BS-

Min 15 oC < BS-II:215 oC; BS-III:210 oC {when SKO isintermediate Product}

BS-II:215 oC;

BS-III:210 oC

BS-II:500 ppm;BS-III:150

ppm

{when SKO is intermediateProduct}

15 oC +/-0.0025 @ 15 oC

42 oC Min {when interfacedwith MS/ Naphtha}

35 oC Min

15 oC +/-0.0025 @ 15 oC BS-II: 820-860;

BS-II: 2-5 Cst;

BS-II: 48;

S-II:500 ppm;BS-

50 ppm < BS-II:500 ppm;BS-III:350 ppm

BS-II:500 ppm;

15 oC +/-0.0025@ 15 oC

ction- free from Visual inspection- free fromsediments (Qtly Millipore

gravimetric test)issolved water usingck

Free from dissolved waterusing aquadis check

15 ppm usingaquadis check

r loading Test H after commencementof PLT

1 as perTest E afterTest H after commencementof PLT
mailto:+/-0.0025@%2015mailto:+/-0.002@%2015mailto:+/-0.0025@%2015mailto:+/-0.002@%2015mailto:+/-0.003@%2015mailto:+/-0.0025@%2015mailto:+/-0.0025@%2015mailto:+/-0.0025@%2015mailto:+/-0.003@%2015mailto:+/-0.002@%2015mailto:+/-0.0025@%2015mailto:+/-0.002@%2015mailto:+/-0.0025@%2015mailto:+/-0.0025@%2015


25/25

ivil-0.85 Def- 0.65; Civil-0.85 Def- 0.65; Civil-0.85

/M 250-450 PS/M 50-450 PS/M

uctivity meter Using conductivity meter

sr Test H:

1

2 Temperature

3 Appearance

4 Water / Sediments

Density @ 15 oC

We are producing only one Grade of ATF. Since the Defence Grade ismore stringent, the Defence specs needs to be met so that we can supplyto both civil as well as defence requirements.

pipelines at the destination. In such a eventuality, the manufacturingment. In ATF conductivity insisted ex Mktg Company is 250 PSMur experience factor.

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