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QUEENSLAND UNIVERSITY OF TECHNOLOGY SCHOOL OF ENGINEERING SYSTEMS WEAR REDUCING ADDITIVES FOR LUBRICANTS CONTAINING SOLID CONTAMINANTS SUBHASH CHANDRA SHARMA B.E. (Mech.), M. Tech. (Mech.) Principal supervisor: Prof. Doug Hargreaves Associate Supervisor: Prof. Will Scott Submitted to Queensland University of Technology for the Degree of Doctor of Philosophy 2008
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Page 1: Principal supervisor: Associate Supervisor: Prof. Will Scott · SUBHASH CHANDRA SHARMA B.E. (Mech.), M. Tech. (Mech.) Principal supervisor: Prof. Doug Hargreaves Associate Supervisor:

QUEENSLAND UNIVERSITY OF TECHNOLOGY

SCHOOL OF ENGINEERING SYSTEMS

WEAR REDUCING ADDITIVES FOR LUBRICANTS CONTAINING SOLID

CONTAMINANTS

SUBHASH CHANDRA SHARMA

B.E. (Mech.), M. Tech. (Mech.)

Principal supervisor: Prof. Doug Hargreaves

Associate Supervisor: Prof. Will Scott

Submitted to Queensland University of Technology for the Degree of

Doctor of Philosophy

2008

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ABSTRACT

Machines operating in dusty environments, such as mining and civil works, are prone

to premature failure, leading to production losses. To address this problem, this

research project examines the interaction between solid contaminants and the bearing

micro-geometry, in lubricated surface contacts. In particular, it seeks to identify anti-

wear additives that are effective in reducing wear under abrasive conditions, making

machine elements more dirt tolerant.

In general, the influence of antiwear additive is so small that it is difficult to isolate

it. Manufactures often make claims about their antiwear products, which are difficult

to verify. Hence, there is a need to characterising the antiwear additives available

with a well-defined parameter, making it easier for consumers to compare the

efficacy of various additives, and be able to select the most suitable additive for a

given environment.

Effect of micro-geometry parameters such as radial clearance, out-of-roughness and

surface roughness was examined and a Film Shape Factor (FSF) – also termed

gamma ratio – has been proposed for ensuring adequate separation of journal

bearings operating in hydrodynamic lubrication regime, where the out-of-roundness

values are higher than the surface roughness values.

In this research, an experimental study has been conducted on journal bearings, to

examine the influence of five antiwear additives on the bearing wear and micro-

geometry. The test additives were provided by the industry partner without revealing

their chemical identity or composition; however, these included some of the most

commonly used antiwear additives. The tests were performed under three conditions:

pure base oil, base oil containing contaminants, and base oil containing contaminants

treated with five different additives.

The experiments were aimed at choosing one wear measuring technique that

evaluates the performance of an individual additive reliably, and based on this

technique the additives were characterised. To achieve these objectives, a multi-wear

parameter approach (MWPA) was developed, which employed three main wear

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measurement methodologies, i.e. weight loss, micro-geometry and particle counts –to

examine the effect of the antiwear additives. Minimum oil film thickness was also

measured to study the lubrication status in the bearing contacts. The MWPA helped

in comparing different wear measuring methods, and in selecting the most reliable

one. This approach also helped in developing short duration wear tests, thereby

saving time, while still getting reliable results without repeating these.

Wear experiments were performed on seven sets of bronze bearings and steel sleeve

shafts. The test contaminant was 16 micron Aluminium oxide Al2O3 powder mixed

in oil with 4% concentration by weight. These solid contaminants were treated with

five different antiwear additives to study their influence on the bearings. Bearings

were operated such that the minimum oil film thickness in the bearing was equal to

the size of the contaminants. These tests were run for a constant sliding distance of

7536m.

The results showed that most of the wear measuring techniques do not suit heavily

contaminated test conditions. However, the out-of-roundness technique proved to be

the most reliable and practical. Based on this technique a methodology was

developed which gave a wear characteristic number (N). A unique value of N can be

derived for each additive, thereby ranking the additives for their efficacy.

The finding of this research provides a better understanding of the methodologies

used for measuring wear in journal bearings subjected to dusty environments, and

examines the efficacy of each one of these. The wear characteristic number (N) can

be used by manufacturers with support from international standards organisations, so

that the users can confidently choose the most appropriate antiwear additive for their

application.

Machines operating in a dusty environment, such as mining industry and civil works

are prone to premature failure with subsequent production losses. In response to this

problem, this research project examines the interaction between solid contaminant

particles and the lubricant film micro-geometry in lubricated surface contacts. In

particular, it seeks to identify lubricant anti-wear additives, which are effective in

reducing wear under abrasive conditions and thus making machine elements more

dirt tolerant.

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Table of Contents

ABSTRACT ......................................................................................................................... iii

LIST OF PUBLICATIONS.................................................................................................xiv

STATEMENT OF ORIGINALITY.......................................................................................xv

KEY WORDS .....................................................................................................................xvi

ACKNOWLEDGEMENT..................................................................................................xvii

NOMENCLATURE AND SYMBOLS.............................................................................. xviii

CHAPTER-1 .......................................................................................................................................... 1

1. INTRODUCTION ............................................................................................................ 1

1.1 Rationale................................................................................................................................. 1

1.2 Background Research ............................................................................................................. 2

1.3 Project Motivation .................................................................................................................. 2

1.4 Current Scenario ..................................................................................................................... 4

1.5 Knowledge Gaps..................................................................................................................... 4

1.6 Aims and Objectives of the Research ..................................................................................... 4

1.7 Research Methodology ........................................................................................................... 5

1.7.1 Effect of anti-wear additives on bearing wear ................................................................ 6

1.7.2 Effect of micro-geometry on tribological performance .................................................. 7

1.7.3 Characterisation of anti-wear additives........................................................................... 8

1.8 Contribution to the Body of Knowledge................................................................................. 8

1.9 Organisation of the Thesis .................................................................................................... 10

CHAPTER 2 ........................................................................................................................................ 11

2. LITERATURE REVIEW................................................................................................. 11

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2.1 Overview ...............................................................................................................................11

2.2 Contaminant Effects on Wear................................................................................................12

2.2.1 A general view of abrasive wear....................................................................................14

2.2.2 Abrasive wear in sliding bearings..................................................................................17

2.2.3 Micro polar lubricant effects in bearing lubrication ......................................................17

2.3 Effect of Solid Contaminants on Journal Bearing Performance ............................................18

2.3.1 Effects of abrasive hardness on wear.............................................................................25

2.3.2 Contaminant motion in lubricated contact .....................................................................27

2.4 Anti-wear Additives and Performance Characterisation .......................................................29

2.4.1 Commonly used antiwear additives ...............................................................................31

2.4.2 Lubricated wear and characterisation of additives.........................................................38

2.4.3 Bearing performance measurement techniques .............................................................40

2.5 Effects of Micro-geometry on Bearing Performance.............................................................41

2.5.1 Roughness effects in hydrodynamic bearings................................................................41

2.5.2 Worn journal bearing analysis .......................................................................................44

2.6 Knowledge gaps ....................................................................................................................48

2.7 Conclusion.............................................................................................................................48

CHAPTER-3 .........................................................................................................................................51

3. EXPERIMENT DESIGN AND DEVELOPMENT..........................................................51

3.1 Overview ...............................................................................................................................51

3.2 Identification of Performance Parameters .............................................................................52

3.2.1 Parameters as measure of energy conservation..............................................................53

3.2.2 Parameters as a measure of bearing life.........................................................................54

3.3 Journal Bearing Design .................................................................................................................. 55

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3.4 Contaminant Selection and Characterization........................................................................ 59

3.5 Lubricant and Additive Selection ......................................................................................... 60

3.5.1 Base oil ......................................................................................................................... 61

3.5.2 Additives selection........................................................................................................ 61

3.6 Test Rig and Instrumentation................................................................................................ 63

3.7 Multi-Wear Parameter Approach (MWPA).......................................................................... 66

3.7.1 Weight loss ................................................................................................................... 67

3.7.2 Out-of-roundness .......................................................................................................... 67

3.7.3 Radial clearance measurements .................................................................................... 68

3.7.3.1 Metrological issues .................................................................................................... 72

3.7.4 Gamma ratio for film thickness measurement .............................................................. 76

3.7.5 Bearing Component Roughness.................................................................................... 82

3.7.6 Maximum Wear Depth ................................................................................................. 82

3.7.7 Particle Counts in Oil Sample....................................................................................... 83

3.7.8 Minimum Oil Film Thickness Measurement ................................................................ 83

3.8 Trigonometric Solution of Film Thickness Measurement .................................................... 92

3.9 Test Procedure and Experiment Design................................................................................ 95

3.10 Conclusion .......................................................................................................................... 96

CHAPTER-4 ........................................................................................................................................ 99

4. EXPERIMENTAL RESULTS AND ANALYSIS............................................................. 99

4.1 Overview .............................................................................................................................. 99

4.2 Weight Loss........................................................................................................................ 103

4.3. Out-of-roundness ............................................................................................................... 106

4.4 Radial Clearance................................................................................................................. 113

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4.5 Change in Roughness ..........................................................................................................117

4.5.1 Bearing roughness........................................................................................................118

4.5.2 Shaft sleeve roughness.................................................................................................121

4.5.3 Individual additive effects............................................................................................123

4.5.4 Roughness traces of bearing elements .........................................................................128

4. 6 Particle Counts (PC) ...........................................................................................................132

4.6.1 Gravimetric change (PCg) ............................................................................................140

4.7 Maximum Wear Depth (WDmax) .........................................................................................142

4.8 Changes in Minimum Oil Film Thickness (Hmin) ................................................................144

4.9 Comparative Analysis of Techniques and Results...............................................................147

4.9.1 Methodologies .............................................................................................................148

4.9.2 Additive performance ..................................................................................................150

4.10 Conclusion.........................................................................................................................151

CHAPTER 5 .......................................................................................................................................153

5. CHARACTERISATION OF ANTIWEAR ADDITIVES.................................................153

5.1 Overview .............................................................................................................................153

5.2 Wear Measurement by Weight Loss....................................................................................154

5.2.1 Wear Computation from Out-of-roundness Trace .......................................................155

5.2.2 Computation of Cross Sectional Wear Area (CSWA).................................................157

5.2.3 Wear Characteristic Equation ......................................................................................165

5.2.4 Area measurement by Newton Cotes method..............................................................167

5.3 Wear Assessment from Out-of-roundness Traces ...............................................................169

5.3.1 Maximum wear depth ..................................................................................................169

5.3.2 Computed wear volume (V) .......................................................................................................171

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5.3.3 Computed weight loss (W).......................................................................................... 172

5.4 Characterisation of Additives ............................................................................................. 174

5.4.1 Wear Characteristic Number (N) ................................................................................ 175

5.5 Discussion on Results ......................................................................................................... 177

5.6 Conclusion.......................................................................................................................... 178

CHAPTER 6 ...................................................................................................................................... 181

6. CONCLUSIONS .......................................................................................................... 181

6.1 Problem Statement.............................................................................................................. 181

6.2 Literature Review ............................................................................................................... 182

6.3 Experiment Design and Development ................................................................................ 184

6.4 Results and Analysis........................................................................................................... 186

6.5 Characterisation of Antiwear Additives.............................................................................. 187

6.6 Research Contributions....................................................................................................... 188

CHAPTER 7 ...................................................................................................................................... 191

7. SCOPE FOR FUTURE WORK ................................................................................... 191

8.0 REFERENCES........................................................................................................... 193

APPENDICES ................................................................................................................................... 203

SUMMARY OF APPENDICES ....................................................................................... 203

APPENDIX A- PUBLICATIONS..................................................................................... 205

APPENDIX –B BEARING FORTRAN PROGRAM........................................................ 215

APPENDIX –C EXAMPLES OF ESDU BEARING OUTPUT)....................................... 225

APPENDIX-D MICROGRAPHS (SURFACE IMAGES ........................................................ 235

APPENDIX-E OUT–OF–ROUNDNESS TRACES)........................................................ 242

APPENDIX F –ROUGHNESS TRACES OF BEARINGS AND SHAFT SLEEVE........... 251

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LIST OF FIGURES

Figure 2.1 Classification of abrasive wear, Misra & Finnie (1980) .......................................15 Figure.2.2 Effect of abrasive hardness on wear rate, Czichos (1978) ..................................26 Figure.2.3 Particle Motion in bearing contact (William and Hyncica (1992) ......................28 Figure 2.4 Clearance ratio and film thickness relationship Chu (1974).................................45 Figure 2.5 Out of roundness magnified part of the edge, Bagnel (1978) ...............................46 Figure 3.1 Bearing and journal drawing.................................................................................56 Figure 3.2 SEM micrograph of Aluminium Oxide particles .................................................60 Figure 3.3 EDAX elemental analysis of Al2 O3 .....................................................................61 Figure 3.4 Test rig assembly ..................................................................................................62 Figure 3.5 Loading System ....................................................................................................64 Figure 3.6 Oil Circuit .............................................................................................................65 Figure 3.7 Multi-Wear Parameter Approach (MWPA)..........................................................68 Figure 3.8 Talyrond 100.........................................................................................................69 Figure 3.9 Metroscope for bearing ID measurements ............................................................70 Figure 3.10a Bearing ID profile by Vernier measurements .................................................73 Figure 3.10b Bearing ID profile by Sigmascope....................................................................73 Figure 3.10c Bearing ID profile by Hole-test-gauge..............................................................74 Figure 3.10d Bearing ID profile by Metroscope ....................................................................74 Figure 3.10e Concentric bearing and shaft sleeve diameter graphs .......................................75 Figure 3.11a Oil film thickness between the surfaces ............................................................77 Figure 3.11b Oil film thickness based on composite roughness ............................................77 Figure 3.12 Film thickness based on composite out-of-roundness concept ...........................79 Figure 3.13 Film thickness based on out-of-roundness concept ............................................80 Figure 3.14 Quant Alert..........................................................................................................84 Figure 3.15 Flow chart ...........................................................................................................87 Figure 3.16a Probe calibration fixture....................................................................................90 Figure 3.16b Calibration setup ...............................................................................................91 Figure 3.17a Calibration chart of probe 1 ..............................................................................91 Figure 3.17b Calibration chart of probe -2.............................................................................92 Figure 3.18 Geometrical representation of film thickness measurement ...............................94 Figure 4.1 Weight loss in bearings .......................................................................................103 Figure 4.2a After Test A2 bearing surface (X50)................................................................104 Figure 4.2b Micrograph of bearing surface after Test A7 (X100) .......................................105

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Figure 4.3 Weight loss in shaft sleeves................................................................................ 105 Figure 4.4 Change in out-of-roundness of bearings............................................................. 107 Figure 4.5a Bottom end out-of-roundness before Test A2 ................................................. 109 Figure 4.5b Bottom end out-of-roundness (convex graph) after Test A2........................... 109 Figure 4.5c Top end out-of-roundness before Test A3....................................................... 110 Figure 4.5d Middle position out-of-roundness before Test A6........................................... 110 Figure 4.5e Bottom end out-of-roundness before Test A6 ................................................ 111 Figure 4.5f Top end out-of-roundness of bearing after Test A6 ........................................ 111 Figure 4.5g Middle position out-of-roundness of bearing after Test A6 ............................ 112 Figure 4.5h Bottom end out-of-roundness Test A6 ............................................................ 112 Figure 4.6 Shaft sleeve trace inside the bearing out-of-roundness trace............................. 113 Figure 4.7 Change in radial clearance of bearings.............................................................. 115 Figure 4.8 Changes in bearing element geometry................................................................ 116 Figure 4.9a Change in bearing circumferential roughness.................................................. 119 Figure 4.9b Change in bearing transverse roughness.......................................................... 120 Figure 4.10a Change in shaft sleeve circumferential roughness........................................ 121 Figure 4.10 b Change in shaft sleeve transverse roughness................................................ 122 Figure 4.11a Roughness effects after Test A1 ................................................................... 123 Figure 4.11b Roughness effects after Test A2..................................................................... 124 Figure 4.11c Roughness effects after Test A3 .................................................................... 125 Figure 4.11d Roughness effects after Test A4................................................................... 126 Figure 4.11e Roughness effects after Test A5 .................................................................... 126 Figure 4.11f Roughness effects after Test A6..................................................................... 127 Figure 4.11g Roughness effects after Test A7.................................................................... 127 Figure 4.12a Bearing circumferential roughness before Test A5 ...................................... 128 Figure 4.12b Bearing circumferential roughness after Test A5........................................... 128 Figure 4.12c Bearing transverse roughness before Test A5 ............................................... 129 Figure 4.12d Bearing transverse roughness after Test A5 .................................................. 129 Figure 4.12e Shaft sleeve roughness before Test A5.......................................................... 130 Figure 4.12f Shaft sleeve roughness after Test A5 ............................................................ 131 Figure 4.12 g Shaft sleeve transverse roughness before TestA5 ....................................... 131 Figure 4.12 h Shaft sleeve transverse roughness after Test A5 ......................................... 132 Figure 4.13 Comparison of change in counts for different tests ......................................... 134 Figure 4.13a Change in counts after Test A1...................................................................... 135 Figure 4.13b Changes in counts after Test A2.................................................................... 136 Figure 4.13c Changes in counts after Test A3 .................................................................... 137

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Figure 4.13d Changes in Counts After Test A4 ..................................................................137 Figure 4.13e Changes in counts after Test A5 ....................................................................138 Figure 4.13f Change in counts after Test A6 ......................................................................138 Figure 4.13g Changes in counts after Test A7 ....................................................................139 Figure 4.13h Change in total particle count .........................................................................139 Figure 4.14 Comparison of wear particles changes.............................................................140 Figure 4.15 Changes in total weight of contaminants ..........................................................142 Figure 4.16 Changes in maximum wear depth....................................................................143 Figure 4.17 Reduction in minimum oil film thickness........................................................146 Figure 5.1 Wear profile of a worn bearing ...........................................................................155 Figure 5.2 Roundness measurements locations....................................................................156 Figure 5.3 Wear zone shape .................................................................................................157 Figure 5.4 Out-of-roundness ‘before test trace’ .................................................................159 Figure 5.5 Out-of-roundness ‘after test trace’ .....................................................................160 Figure 5.6 Computed out-of-roundness shape of a worn bearing ........................................161 Figure 5.7 Actual trace of a test bearing with redrawn shape .............................................162 Figure 5.8 Wear depth measurement at different nodes (wndn)...........................................163 Figure 5.9 Wear Characteristic Equation for Test A2..........................................................167 Figure 5.10 Wear Characteristic Equation for Test A3........................................................167 Figure 5.11 Comparison of maximum wear depth..............................................................171 Figure 5.12 Comparison of computed weight loss and measured weight loss.....................174

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LIST OF TABLES

Table 2.1: Sources of Solid Contaminants, Dwyer-Joyce (1993).......................................... 13 Table 2.2 Wear reducing properties of various lubricants, Zheng (1986) ............................. 32 Table 2.3 Results for infinitely wide bearing (Christensen 1969-70) .................................... 42 Table 3.1 Sample of test parameters ...................................................................................... 57 Table 3.2 Hardness measurements on bearing and shaft sleeves........................................... 58 Table 3.3 Antiwear additive properties.................................................................................. 63 Table 3.4 Bearing ID measurements...................................................................................... 71 Table 3.5 Bearing ID measurements: statistical analysis...................................................... 72 Table 3.6 Roughness and out-of-roundness data of test bearings .......................................... 81 Table 3.7 Operating parameters and experiment design........................................................ 96 Table 4.1 Initial measurements before the tests ................................................................... 101 Table 4.2 Experimental results ............................................................................................ 103 Table 4.3 Rise in particle counts of different sizes ............................................................. 133 Table 4.4 Changes in measured minimum oil film thickness ............................................ 145 Table 4.5 Comparison of performance of antiwear additives .............................................. 150 Table 5.1 Computed maximum wear depth data ................................................................. 164 Table 5.2 Comparison of maximum wear depth.................................................................. 170 Table 5.3 Wear Volume....................................................................................................... 173 Table 5.4 Wear Coefficients of antiwear additives.............................................................. 177

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LIST OF PUBLICATIONS

1. Sharma, S., C. and Hargreaves, D (2001), “Effect of Solid Contaminants on Journal Bearing Performance”, World Tribology Conference, Vienna, pp.1-4

2. Sharma, S. C., Hargreaves, D. and Scott, W., (2004), Influence of Errors in Measuring the Radial Clearance of Journal Bearing Performance. 1st International Conference on Advanced Tribology, Singapore. pp.1

3. Sharma, S., Hargreaves, D., Scott, W., (2008), “Journal bearing metrology and manufacturing issues”, 9th Global Congress on Manufacturing and management (GCMM 2008), 12-14 November 2008, pp (paper accepted).

4. Sharma, S., Hargreaves, D., Scott, W., (2008), “Characterisation of antiwear additives”, 9th Global Congress on Manufacturing and management (GCMM 2008), 12-14 November 2008, pp. (abstract accepted- paper to be published in The Journal of Computational materials and Surface Engineering).

5. Sharma, S., Hargreaves, D., Scott, W. (2008), “Characterisation of additives using out-of roundness traces”, 2nd International Conference on Advance Tribology 2008 (ICAT 2008), 3-5 December 2008, Singapore (paper accepted)

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STATEMENT OF ORIGINALITY

The work contained in this thesis has not been previously submitted to meet

requirements for an award at this or any other higher education institution. To the

best of my knowledge and belief, the thesis contains no material previously

published or written by another person except where due reference is made.

Signed ……………………………….

(Subhash Chandra Sharma)

Date ……………………………..

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KEY WORDS

Journal bearing, Contaminants, Antiwear additives, Worn journal bearings, Bearing

metrology, Hydrodynamic lubrication, Sliding bearing wear, Micro-geometry,

specific film thickness.

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ACKNOWLEDGEMENT

I would like to express deep gratitude to my principal supervisor, Prof. Doug

Hargreaves for his consistent academic and administrative support. I am thankful to

my former principal supervisor and current Associate Supervisor, Professor Will

Scott who introduced me to the field of contamination in lubrication and motivated

me to find innovative experimental techniques to solve the problems encountered

throughout the project.

I am thankful to our industry partners Fuchs Australia and specifically Mr. Phil

Leeming who supported the project throughout its duration by supplying additives

and information related to industrial applications.

I am thankful to Mr. David McIntosh for providing me full technical support and a

jovial environment in the laboratory during the testing work. I am thankful to Mr.

Terry Beach and Mr. Mark Haynes for helping me in fabrication and instrumentation

work required for the test rig. Thanks are due to Mr. David Allen, Mr Steve Behari,

Mr Erwin Schilling and Mr. Alf Small for their technical support in instrumentation

and testing time to time.

I am thankful to Prof. Eric Hahn, University of New South Wales for his valuable

suggestions in modelling and to Prof. Nalin Sharda, of Victoria University for the

useful discussions in presenting the results and giving the final shape to this thesis.

Finally, thanks to my wife Pallavi, sons Vyom and Vihang who supported me

emotionally to complete this work.

I would like to dedicate this thesis to my late parents Shri Nathu Ram Sharma,

Shrimati Bhagwan Devi Sharma and grand mother Shrimati Rani Devi for

inculcating in me the spirit of higher learning, over and above any other worldly

gain.

Subhash Chandra Sharma

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NOMENCLATURE AND SYMBOLS

ASTM = American Society for Testing and Materials

ASME = American Society of Mechanical Engineers

Al2O3 = Aluminium Oxide

ASI = American Standards Institute

ha = Contaminant average height/diameter (microns)

C = Radial clearance (m)

ΔC = Change in radial clearance (microns)

ha = Contaminant average size (microns)

CSWA = Cross Sectional Wear Area (mm2)

D = Bearing diameter (m)

e = Eccentricity (microns)

e o = Eccentricity at no load (microns)

Eox = Eccentricity at no load in the direction of Probe ‘X’

Eoy = Eccentricity at no load in the direction of Probe ‘Y’

ESDU = Engineering Science Data Unit

f0 = Wear depth at the first node (microns)

f1 = Sum of all the WD’s at odd nodes (i.e. 3, 5, 7,….17), (microns)

f2 = Sum of all the wd’s at even nodes (i.e. 2, 4, 6…16), (microns)

F = Frictional force (N)

FSF = Film Shape Factor

Ha = Hardness of the abrasive (Kgf/mm2)

Hb = Hardness of the bearing

Ho = Film thickness at no load (ho/RB)

h = Oil film thickness at any angular position (microns)

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hmin = Minimum oil film thickness in the bearing contact (microns)

Δh = Nodal distance along the outer crescent (microns)

HB = Brinell hardness

HRB = Rockwell hardness at ‘B’ scale

HRC = Rockwell hardness at ‘C’ scale

Hmin = Minimum oil film thickness (microns) (hmin/RB)

Δhmin = Change in minimum oil film thickness (microns)

Hxps = Measured minimum oil film thickness – start of test (microns)

Hxpm = Measured minimum oil film thickness – during test (microns)

Hxpe = Measured minimum oil film thickness – end of test (microns)

H esdu = Minimum oil film thickness from ESDU 84031 chart (microns)

H = Non dimensional film thickness (at any location) (H=h/RB)

hhdl = Film thickness value required for λ = 10 , (microns)

Hhdl = Film thickness required for γ = 10 , (microns)

IDmax = Maximum ID of bearing (mm)

ISO = International Standards Organisation

ID = Internal diameter

K ratio = Film thickness to particle size ratio (‘K’ ratio), K= hmin/ha)

l = Sliding distance (m)

L = Bearing length (m)

L = Bearing length in mm

L/D = Bearings length to diameter ratio

Lc = Cut off length (microns)

MWPA = Multi-wear parameter approach

N = Speed (rpm)

OD = Outer diameter of shaft sleeve (m)

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ΔOD = Change in Shaft sleeve OD (microns)

OR = Out-of-roundness (microns)

ΔORb = Change in out-of-roundness (microns)

ΔODs = Change in outer diameter of Shaft sleeve shaft (microns)

Orb = Out-of- roundness of bearing (microns)

Ors = Out-of –roundness of shaft sleeve (microns)

Ori = Localised or instantaneous out-of-roundness (microns)

Or1 and Or2 = Out-of-roundness of surface 1 and 2 respectively (microns)

Pi,j = Non dimensional pressure at i,j node (ph2/ηoL.Us)

Px = Distance measured with Probe X (microns)

Py = Distance measured with Probe Y (microns)

Pox = Distance measured with Probe ‘X’ at no load and full speed (microns)

Poy = Distance measured with Probe ‘Y’ at no load and full speed (microns)

Pc = Particle count (counts /ml)

Pcg = Gravimetric particle (g/l)

ΔPc = Change in particle count (counts/ml)

Rsk = Roughness skewness

RB = Bearing radius (m)

Rs = Shaft sleeve radius (m)

Rb = Bearing circumferential roughness (microns)

ΔRb = Change in bearing circumferential roughness (microns)

Rs = Change in shaft sleeve circumferential roughness (microns)

ΔRs = Change in Shaft sleeve roughness circumferential (microns)

Rbt = Bearing transverse roughness (microns)

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ΔRbt = Change in bearing axial or transverse roughness (microns)

Rst = Shaft sleeve transverse roughness (microns)

ΔRst = Change in transverse roughness of shaft sleeve (microns)

Ra = Average roughness (microns)

Rp = Highest peak (microns)

Rt = Maximum upward excursion (microns)

Rq = Root mean square roughness (microns)

S = Sommerfeld number (S = (ημ/Wap).(Wap/C)2 )

SEM = Scanning Electron Microscope

SF = Scale Factor

t = Time (s)

Τ = Cross Sectional Wear Area (m2)

Us = Bearing velocity (m/s)

V = Wear volume (m3)

V = Computed wear volume (mm3)

W = Normal load (N)

Wz = Load component in Z direction

W = Non dimensional load wz/(ηoub). (C/RB)

W = Computed weight loss (mg)

Wapp. = Applied load (N)

Wcal = Non dimensional Load calculate (N)

WCE = Wear Characteristic Equations

wndn = Computed wear depth at nth node (microns)

WD = Computed maximum wear depth (microns)

WZW = Wear Zone Width (microns)

Wx = Load component in x direction (N)

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Wy = Load component in y direction in thesis z direction (N)

Wb = Bearing weight (g)

ΔWb = Measured weight loss in bearing (mg)

Ws = Weight of shaft sleeve (g)

ΔWs = Measured weight loss in shaft sleeve shaft (mg)

WD = Computed maximum wear depth (microns)

WDmax = Measured maximum wear depth (microns)

ω = Cross sectional wear area (CSWA), (mm2)

X = Linear coordinate in the direction of circumference (mm)

X1 = Coordinates in space as distance from the tip of the X probe (m)

Y1 = Coordinates in space as distance from the tip of the Y probe (m)

y = War depth calculated at X distance using WCE (mm)

β = Angle subtended by SN and NB lines

ρ = bearing material density g/cm3

ε = Eccentricity ratio (εce

= )

φ = Angle MNS considered in probe geometry (degrees)

Φ = Attitude angle assumed (degrees)

Ψ = Calculated attitude angle (degrees)

η = Oil viscosity (Pa.s-1)

ηo = Inlet oil viscosity (Pa.s-1)

λ = Lambda ratio or Film parameter or specific film thickness (hmin/σcomp)

θ = Angle MNB in probe geometry (in this thesis)

σ1 and σ2 = RMS roughness values of surface 1 and 2 (microns)

γ ratio = Film Shape Factor (FSF)

σb and σs = RMS roughness of bearing and shaft sleeve (microns)

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CHAPTER-1

1. INTRODUCTION

1.1 Rationale

Bearings are used for transmitting forces between machine components in relative

motion. One of the objectives of a machine designer is to incorporate efficient

bearings that minimise power consumption due to friction, and achieve longer life in

face of wear. A lubricant layer between the mating surfaces of a bearing often helps

in reducing frictional force, and thus, minimises wear. However, the machines

working in dusty environment are prone to higher wear rate; hence the effect of

contaminants in bearings lubrication is an important topic of study.

Machines working in dusty environment often fail prematurely and incur high

maintenance costs. To minimise such failures, operators change the lubricant

frequently, thus aggravating the hazardous waste disposal problem, which is a threat

to the ecological system. If machines can be designed to be more dust tolerant,

bearing life will be extended and thus reduce hazardous waste material (Scott and

Hargreaves, 1991). Thus, tribologists face simultaneous challenges of energy

conservation, environmental protection and machine reliability.

Bourne (2002) reported on the British army exercise in the Saif Sareea deserts of

Oman in year 2001. In this exercise, sixty-six Challenger-2 tanks were deployed at a

cost of A$230 million, but half of the tank engines seized due to dust. During the

Iraq war, Offley (2003) reported that Jessica Lynch was captured as her gun jammed

due to CLP lubricant failure in dusty environment. During the very first dust-storm

more than 200 infantry vehicles and 70 helicopters were disabled, and, as a result,

coalition forces faced heavy casualties. To conclude, failure of lubricants can lead to

loss of life as well; therefore, research into the performance of lubricants and wear

reducing additives in dusty environments is more important than ever before.

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1.2 Background Research

Given the importance of lubricants in smooth machine operation, substantial research

has been conducted on the effect of contaminants in journal bearings. Such research

has emphasised the importance of using clean oils and given strategies for

controlling the contaminants. The most widely applied strategy is the application of

filters. Duchowski (1998) recommended that the filtration requirements for journal

bearing should be more stringent, and that ISO 4406 cleanliness level must be adhere

to using the ISO 16/14/12 cleanliness code; additionally, filtration requirements for

six micron contaminants (β6 ratio) should also be met. However, as the costs of

filtration increase exponentially with cleanliness, unduly high cleanliness is not

always economically viable.

Another strategy to minimise wear is to use antiwear additives, to mitigate the effect

of contaminants. Many such additives are commercially available; however, little

information is supplied by manufacturers about their efficacy. Manufacturers often

make unsubstantiated claims that users have no way to confirm.

However, in most machine components the wear is so small that it is difficult to

distinguish between the improvement due to additives, and the effect of operating

parameters such as speed, load and misalignment. Rowe (1980) has conducted

research to characterise additives in dust free environments. Furthermore, he used

elasto-hydrodynamic concentrated lubricated contacts. He suggested that further

research be conducted in this area. However, since the 1980s not much research has

been carried out on the efficacy of antiwear additives. Consequently this research is

filling a long standing knowledge gap.

1.3 Project Motivation

Professor W. Scott at Queensland University of Technology received requests from

the mining industry to investigate the effect of contaminants on oil change period.

Subsequently, Hirstch and Scott (1980) conducted an experimental study on journal

bearing lubricated with oil containing contaminants and found that bearing journals

with rough surfaces do not wear as rapidly as their smoother counterparts. A logical

explanation for this phenomenon – as given by Hirstch et. al. – is that the

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contaminant particles take a preferential path through the lubricant film (i.e. valley-

to-valley of the rough surfaces) and hence reduces three-body abrasive wear. Martin

(1991) also supported Hirstch’s hypothesis, but could not provide any empirical

evidence. These researchers concluded that the surface topography (roughness /

waviness) of mating surfaces is important in almost every facet of machine

operation; nonetheless, there is no clear-cut evidence as to which topography works

the best. This is partly due to the difficulty in uniquely defining the micro-geometry

in quantitative terms. A "smooth is the best" attitude has developed which results in

the pursuit of expensive finishing processes, which are not only uneconomical but

may, in fact, impair the part performance.

Later, the mining industry also raised the issue of efficacy of the additives for

selecting appropriate additives for dusty applications. As a result this project was

developed as an Australian Postgraduate Award (Industry) (APAI) with the support

of Fuch Australia lubricant company.

After reviewing the literature and analysing the problem it was realised that rolling

element bearings used in the machines are either sealed or shielded, whereas sliding

bearings are often exposed, and hence need special attention. Since journal bearings

are the most widely used sub category of sliding bearings, these were chosen for this

study. This resulted in an experimental study on the effect of solid contaminants on

the wear of journal bearing and specifically on its micro-geometry, which includes

surface roughness, roundness, wear-depth and radial clearance.

Furthermore, there is a need to develop a systematic methodology for determining

the efficacy of the antiwear additives. Though, the tribological performance of an

additive can be judged by its ability to save energy and resist wear; it is easier to

measure wear than frictional losses. Therefore, this research project has placed

greater emphasis on wear measurements.

There are several antiwear additives available in the market; these additives are sold

separately or are blended with lubricants. The chemical composition of these

additives is mostly confidential. Five antiwear additives were supplied by Fuchs

Australia for this research, as these additives are used commercially. Some of these

additives are commercial products, while the others are experimental products with

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proprietary composition. This experimental research is aims to using materials and

operating conditions as close to field conditions as possible.

1.4 Current Scenario

Moon (2007) has recently reported the detrimental effects of lubricants containing

solid contaminants. He concludes that solid contaminants reduce the life of

tribological components by 15%, cause 35% of downtime, and 82% of the wear.

Moon emphasises that particles smaller than the minimum oil film thickness in the

bearing contact do not cause much harm; however, the particles equal to the size of

the film thickness are highly detrimental.

Maru (2006) has studied the effect of antiwear additives on lubricants containing

solid contaminants on a tribometer in rotary and reciprocating motions. But his study

was confined to boundary lubrication regimes, and the focus was on the wear

mechanisms rather than characterisation of lubricants.

The available literature indicates that no significant research has been conducted on

oils containing solid contaminants treated with antiwear additives since 1980s, hence

this research is timely.

1.5 Knowledge Gaps

While much research has been carried on bearing wear, the literature review revealed

the following knowledge gaps:

• The effect of solid contaminants treated with antiwear additives on journal bearing wear has not been fully studied.

• Characterisation of antiwear additives based on their efficacy for dusty applications under hydrodynamic lubrication has not been carried out.

• The effect of solid contaminants on the bearing micro-geometry, and its effect on the bearing’s tribological performance is not well understood.

• There is no standard numerical parameter for classifying the performance of antiwear additives operating in dusty hydrodynamic lubrication conditions.

1.6 Aims and Objectives of the Research

The main aims of this research project are to conduct experiments on journal

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bearings lubricated with oil containing solid contaminants treated with antiwear

additives, and study the following aspects:

a) The effect of contaminants –treated with antiwear additives– on journal bearing

wear

b) The effect of antiwear additives on the wear of journal bearings operating with

oils containing solid contaminants

c) The effect of change in micro-geometry on bearing’s tribological performance

d) Characterisation of additives using the most suitable wear measuring technique

The research objectives (deliverables) were derived from a literature review in

consultation with the project’s industrial partner (Fuchs Lubricants Australia). The

main objectives are as follows:

1. Compare the tribological performance of: a) journal bearings lubricated with

pure base oil, b) base oil containing solid contaminants, and c) oils containing

solid contaminants treated with different antiwear additives.

2. Determine the effect of solid contaminants on wear and micro-geometry of a

journal bearing.

3. Evaluate different wear measurement techniques for their suitability to

identifying a methodology for characterising the antiwear additives.

4. Study the effect of micro-geometry on the tribological performance by

measuring the change in minimum oil film thickness.

5. Characterise antiwear additives using a unique number, and rank them for

their efficacy.

1.7 Research Methodology

Before conducting the wear tests on the test bearings, micro-geometry parameters

and their effect on lubrication were examined. This required verification of micro-

geometry parameters including their metrology. Micro-geometry parameters i.e.

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out-of-roundness, surface roughness and radial clearance were measured carefully

before conducting the tests. While measuring the radial clearance it was found that

ID of the bearings varies at different locations along the circumference. This is

mainly due to out-of-roundness, and hence, it is proposed that out-of-roundness

should also be specified along with the radial clearance, just like cut-off length is

specified along with the surface roughness. Further investigations revealed that the

out-of-roundness values are higher than the surface roughness values. This resulted

in proposing a new design parameter called Film Shape Factor (FSF) or gamma ratio.

This research has three main components that are:

1) The efficacy of anti-wear additives on bearing wear

2) Effect of micro-geometry on tribological performance

3) Characterisation of anti-wear additives

1.7.1 Effect of anti-wear additives on bearing wear

The research problem predicates the need for experimental studies that measures the

effect of antiwear additives on bearings lubricated with oil containing solid

contaminants. Therefore, a series of wear tests were planned on the pairs of 40mm

ID bronze bearings and steel shaft sleeve. The bearings were designed using

Engineering Science Data Unit method (ESDU 84031) and were tested under

simulated dusty conditions.

Wear tests generally suffer from poor repeatability. If factors influencing the wear

are not controlled then the wear results can vary by as much as a factor of 10 or more

(Bayer, 2004). The experiments were designed for best utilisation of the available

resources, which led to the following strategic decisions:

• The test should be conduct for short duration without repeating them.

• The wear results obtained from different methods need to be compared to

find out the level of accuracy of each method, and select the most reliable

method to obtain reliable results.

• Environment and procedures must be consistent, because the tests are not to

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be repeated.

• Test must be conducted for K=1, sliding distance (l) = 7536m, and all other

operating and environmental parameters must be kept the same.

A performance parameter selection process based on weight loss, micro-

geometry and particle counts called multi wear parameter approach (MWPA)

was developed, this comprised fourteen parameters. Wherever appropriate

multiple observations were recorded, and average of these was used for analysis.

The following six measurement parameters were used in the MWPA:

1. Weight loss

2. Out-of-roundness

3. Roughness

4. Radial clearance

5. Wear depth

6. Particle count

1.7.2 Effect of micro-geometry on tribological performance

The effect of change in micro-geometry on the tribological performance was also

measured, by recording the change in minimum oil film thickness. However, the

tribological performance of test bearings was affected not only due to change in

micro-geometry but also as a result of: a) combined effect of change in bearing

geometry, b) influence of antiwear additives, and c) the oil flow restrictions due to

concentration of the solid contaminants in and around the bearing contact.

The change in minimum oil film thickness was recorded at three intervals i.e. at the

beginning, middle and at the end of each test. Each measurement technique was

examined critically, merits and demerits of these techniques were compared, and the

most suitable measurement technique was chosen for characterising the antiwear

additives.

Bearings were designed using ESDU 84031 method and seven test bearing sets were

fabricated for this experimental study. First test used pure base oil, and the second

test used oil containing 4% (by weight of 16 micron) Al2O3 powder. Subsequent, five

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tests used contaminated oil treated with antiwear additives.

To make sure that the measurement system used in this study works satisfactorily,

the results obtained with pure base oils were compared with the values predicted by

the on-line ESDU A 9305 software program, as well as by using a FORTRAN

program based on the algorithm proposed by Pai and Mazumdar (1992).

1.7.3 Characterisation of anti-wear additives

Wear test results were analysed for accuracy of the measurement technique as well as

for the efficacy of the antiiwear additives. The out-of-roundness technique was found

to be the most suitable. Using this technique, an antiwear additive characterisation

method was developed. In this method the out-of-roundness traces were used for

computing the weight loss, and by using this weight loss a number called wear

characteristic number (N) was derived. This number represents the efficacy of an

additive and hence users can select an additive for their applications using this

number.

1.8 Contribution to the Body of Knowledge

In this experimental research, various wear measurement techniques were evaluated

to examine their suitability for studying wear in bearings lubricated with oil

containing solid contaminants, and treated with antiwear additives. Effect of solid

contaminants with and without additives was studied on the wear of journal bearing

components; and specifically on the micro-geometry of the bearings. The effect of

change in micro-geometry on minimum oil film thickness was also studied. Different

wear measurement techniques were compared and the best technique was chosen for

characterising the antiwear additives – specifically for dusty applications.

Out-of-roundness was found to be the most reliable and suitable micro-geometry

parameter for characterising antiwear additives. This parameter was used to develop

a method for characterising the antiwear additives. A wear characteristic number (N),

was derived to rank the additives based on their efficacy.

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The main contributions of this research to the existing body of knowledge include:

• Developed a clear understanding of the effect of antiwear additives on the

wear of a journal bearing lubricated with oils containing solid contaminants;

and in particular, on the change in bearing micro-geometry.

• Established a process for comparative analysis of different wear measuring

methods –for characterising antiwear additives.

• Developed a novel geometrical method for improving the precision of oil film

thickness measurement –using floating proximity probes.

• Demonstrated the inadequacy of the current metrological practices for

measuring the radial clearance in journal bearings; and as a result predicated

the need to review the current bearing design heuristic –that the lambda ratio

should be close to 10.

• A Film Shape Factor (FSF or gamma ratio) has been proposed as a design

parameter for ensuring adequate separation of bearing surfaces of a journal

bearing working in hydrodynamic lubrication regime where out-of-roundness

value is higher than the surface roughness.

• Derived wear characteristic equations (WCE) to obtain a unique wear

signature for individual antiwear additives.

• Derived a wear characteristic number (N) to characterise antiwear additives

and facilitate the selection of the most suitable antiwear additive for a given

dusty environment.

These contributions to the existing body of knowledge for the tribology of machine

elements will help in extending the life of journal bearings, minimise downtime, save

energy, benefit the environment –by reducing hazardous waste of contaminated oils–

and help lubricant users to select the most suitable antiwear additive for dusty

applications.

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1.9 Organisation of the Thesis

This thesis comprises seven chapters and six appendices. A brief introduction to each

chapter is given in the following:

Chapter 1 gives an introduction to the thesis, including problem statement, objectives

and contribution to the body of knowledge.

Chapter 2 provides a detailed literature review concerning the various aspects of this

research and highlights knowledge gaps.

Chapter 3 details the experimental design and tests set up. It explains the issues

related to metrology of radial clearance, limitations of the current concept of specific

film thickness and a proposed gamma ratio for hydrodynamic bearing design. The

chapter also gives the details of a proposed geometrical method for measuring oil

film thickness with proximity probes mounted on a floating bearing housing.

Chapter 4 presents the results and their detailed analysis, which is used to identify the

most suitable wear measurement technique for characterising antiwear additives. It

also provides a discussion of the influence of each anti-wear additive on the wear of

test bearings.

Chapter 5 gives the methodology for characterising the additives, and the wear

characteristic number for selecting an additive based on its antiwear performance.

Chapter 6 presents the main conclusions of this research project.

Chapter 7 suggests directions for future research.

Appendices A to F are summarised and included at the end of the main thesis body.

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CHAPTER 2

2. LITERATURE REVIEW

2.1 Overview

This research project required an in-depth knowledge of various components of the

problem, which included contaminants, wear measurements, antiwear additives,

miro-geometry and characterisation of antiwear additives. Thus the literature review

was guided by the following three main areas connected to each other:

a) The effect of contaminants –treated with antiwear additives– on journal bearing

wear

b) The effect of change in micro-geometry on bearing’s tribological performance

c) Characterisation of additives using the most suitable wear measuring technique

The literature review was further classified, and a search was conducted on the

following topics:

• Contaminants’ effect on wear

• Effect of solid contaminants on journal bearings

• Tribological performance and criteria for its measurement

• Micro-geometry parameters and their effect on bearing lubrication

• Antiwear additives and their characterisation

The literature on antiwear additive gives more emphasis on additive chemistry, only

limited information is available on additive characterisation. In this context, literature

on applications of commonly used antiwear additives was reviewed.

Appendices A to F are summarised and included at the end of the main thesis body.

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2.2 Contaminant Effects on Wear

Bearings are usually prone to solids contamination at the lubricated contacts and they

tend to damage the bearing. In fact even the cleanest of lubricants carry some

contaminants as it is impossible to remove all particulate matter, which passes

through the filter Khonsari et al. (1999). The need for cleanliness of lubricants was

emphasised by Douglas (1989) who suggested that cleanliness standards need to be

reviewed from time to time in view of changing requirements of machinery. Godfrey

(1989) highlighted the relationship between lubricant cleanliness and bearing life.

Dufrane et.al. (1983) reported on a turbine bearing survey where 54% failures were

attributed to contamination of lubricants.

Duchowski (1998) defined a contaminant as an unwanted foreign element or

substance that can have adverse effects on the lubrication system of an operating

machine. These adverse effects are; efficiency, service life and reliability of the

machine components. Contamination can take place in either form of matter such as

gas, liquid or solid. Gases normally dissolve in the liquid lubricant or form bubbles;

liquids are either directly dissolved or form an emulsion but solids are always found

in the form of suspended particles. In the present study only contamination of the

lubricant by solid particles is considered.

Dwyer-Joyce et al. (1990) has indicated that lubricant contamination may be by the

three forms of matter: solid, liquid and gas either individually or in combination.

There are three main sources of solids contamination in machinery:

1. Implanted contaminants: The contaminant particles are introduced at the time of

manufacturing including the process itself, assembly, handling, packaging, and

transportation.

2. Ingested Contaminants: Particles may enter the system from environment

through seals or air filters etc.

3. Self-Generated Contaminants: These are mainly due to wear of mating surfaces

in the lubricated contacts. There may be different forms of wear mechanisms

responsible for the generation of these contaminants. Though rare, it also

includes erosive wear mechanism, which is caused by high flow rate of lubricant

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through pipes and seals.

Knowing the concentration, size distribution, and material properties such as

geometry, hardness, etc., the severity of contamination can be assessed in a

lubrication system. It is easy to determine the first two parameters in comparison to

hardness and material type of an individual particle. The hardness of particles can be

assumed to be the hardness of the bulk material, which is reported in any standard

handbook. The material type can be determined with the help of energy dispersive X-

ray micro analysis and Infra Red (IR) emission (Kuhnell (1992)) or any other

technique used for elemental analysis. These methods are complex in nature but well

accepted by modern researchers.

As shown in Table 2.1, Beghini et al. (1992), Dwyer-Joyce et al. (1990), Dwyer-

Joyce (1992) and Hamer et al. (1989) have reported the following solid contaminant

concentration results after analysis of used lubricant collected from different type of

machines.

Table 2.1: Sources of Solid Contaminants, Dwyer-Joyce (1993)

Investigator Sample Source

Concentration g/l

Size range μm

Materials present

Dwyer-Joyce(1983)

Paper mill 0.4 0-150 Cu, Sn, silicates

Dwyer-Joyce (1983)

Motor vehicle sump

1-2 0-250 Al, Cu, Fe, Fe, Pb

SKF ERC (Beghini 1992)

Various bearing lubricants

0.3-1.5 0-250 Fe, Al, Cu, Sn, SiC, sand

Dwyer-Joyce (1993)

Aircraft gas turbines

1-2 0-200 Fe, C, silicates

Fuchs Australia *

Mining industry

2-5g/l 0-200 Depending upon the mining industry

* Data from Fuchs Australia (personal communication)

Effect of contaminants on bearings can be correlated with abrasive wear. It is

important to understand abrasive wear in general and its effect on different

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tribological elements.

A bearing may wear out faster due to presence of solid contaminants present in the

oil. The gradual wear affects the bearing performance in terms of load carrying

capacity and subsequently accelerates the increase in friction and wear. These effects

have been very recently studied by Fillon (2002).

2.2.1 A general view of abrasive wear

Friction and wear are inevitable in tribological components of machines. The

Institution of Mechanical Engineers, U.K., has defined wear as;

“The progressive loss of substance from the surface of a body brought about by

mechanical action. Usually it reduces the serviceability of a body, but it can be

beneficial in its early stages.” Dwyer- Joyce (1993).

There are different types of wear mechanisms (Halling (1975), Rabinowicz (1965)).

Archard (1953) introduced the first mathematical equation to quantify out wear of

metals as follows:

V= kW l/3H (2.1)

Where ‘V’ is the wear volume, ‘K’ is known as wear coefficient, ‘W’ is normal load,

‘l ’ is sliding distance and ‘H’ is hardness of the substrate. The model was developed

for adhesive wear but Rabinowicz (1965) modified it for abrasive wear and modified

the above equation to;

HWlV

πθcot

= (2.2)

Where θ is the angle of the cone used as an indenter and all other terms are same as

in Equation 2.1. This equation was derived for an abrasive wear process, where an

indenter of a cone shape of radius r and cone angle θ was used. In this model k/3 is

replaced by (cot (θ)/π).

Rabinowicz et al. (1961) carried out an experimental study on three-body wear with

different sizes of grits and found that smaller grits lead to low wear rates. Later

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Rabinowicz (1965) investigated a threshold limit of grit size above which wear did

not increase when silicon carbide was used as an abrasive mixed with oil and water

in a sliding bearing.

Misra and Finnie (1980), Misra and Finnie (1981), Misra and Finnie (1982) Misra

and Finnie (1983) published a series of research papers based on several three-body

abrasive wear experiments and concluded that a critical particle size affects the

abrasive wear severely. Misra and Finnie (1980) divided abrasive wear into three

groups; two-body, three- body and two and a half body wear. They further

subdivided three-body wear as shown in Figure 2.1

Figure 2.1 Classification of abrasive wear, Misra & Finnie (1980)

They defined open three-body wear system as wear occurring in two opposing

surfaces which are apart whereas closed three-body wear occurs where wear particles

are trapped between the surfaces, such as bearings lubricated with an oil containing

solid contaminants. Similarly stressed situations are those where particles are crushed

into small pieces as in the case of ball mills. In the case of low stress, wear particles

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do not break into small particles.

Larsen-Basse (1975) found that moisture is responsible for an increase in wear in

presence of silicon carbide and aluminium oxide abrasives in a sliding contact up to

65%.Chandrasekaran et al. (1985) studied the effect of abrasive particles on wear in a

four ball test machine under boundary lubrication regimes and determined the size of

grits on scuffing in the contact.

Fodor (1980); Fodor (1987); Fodor and Ling (1987) studied the effects of abrasive

particle size on internal combustion engine components and demonstrated that by

using correct filtration system, up to 4% energy can be saved and the oil change

period can be extended up to 10000 km. Odi-Owei and Roylance (1987) performed

some experiments with a four-ball test machine under sliding conditions. They

observed that the contaminants were embedded in the inlet zone on the ball surfaces

and restricted the oil flow, which results in ploughing action. Concentration and

particle size both were damaging in the boundary lubrication regime as adhesive

wear dominated the abrasive wear and leads to scuffing. They presented a simple

mathematical model to predict friction under abrasive containing lubricant

conditions.

In an experimental study on a pin-on-disk machine, Mehan (1988) compared the

wear behaviour of different materials and coatings under contaminated lubricant

conditions. The study revealed that 2g/ l concentration of Al2O3 particles in white

mineral oil caused less wear. Furthermore, cemented tungsten carbide (WC) cermets

as well as WC coating displayed less than that for chromium-plated pins when

rubbed against cast iron in an uncontaminated lubricant. The study also revealed that

the increase in surface roughness from 0.15 micron to 0.8 micron caused 10 times

more wear.

The geometry of abrasive particles influences the wear pattern. Defining the

geometry of their irregular shape has been a challenge for researchers. A number of

researchers have suggested numerical methods and imaging techniques to determine

the shape of the particles mathematically Kuhnell (1992).

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2.2.2 Abrasive wear in sliding bearings

Solid contaminants are the enemy of lubricated surfaces of both sliding and rolling

bearings. They not only increase friction between the two moving surfaces but also

cause accelerated wear. The lubrication mechanism and especially the ratio between

lubricant film thickness and contaminant size is important in determining the wear

severity in bearings (Douglas, 1989).

Journal bearings normally operate in hydrodynamic lubrication regime where fluid

properties influence the fluid flow through the contact. Particles mixed with

lubricants in any form influence the flow and hence the oil film thickness, which is

directly related to their performance (Das, et. al., 2004).

2.2.3 Micro polar lubricant effects in bearing lubrication

The effect of particles mixed with lubricant has been a major concern in bearing

performance for practicing engineers since they understood hydrodynamic

lubrication theory Allen and Kline (1971). These particles may be long chain

polymers due to additives, dust particles, or other solid contaminants. The concept of

micro-polar effects has also been applied to bearings lubricated with oils containing

excessive solid contaminants in colloidal form and it was found that under dynamic

loading their stability improved Das et al. (2004).

Viscosity is a major criterion for satisfactory bearing performance. This topic has

been discussed by several bearing designers such as; Eringer (1964), Allen and

Kiline (1971) and Khonsari and Brewe (1989). These studies have who contributed

significantly to lubrication theory where large quantities of polymeric additives are

used.

A common assumption in bearing design is that lubricants are Newtonian. However

this is not the case when polymeric substances are mixed with the lubricant. Many

researchers, Prakash and Sinha (1975),Prakash and Sinha (1977), Mahanti (1976) ,

Zaheeruddin and Isa (1978), Tipei(1979), Sinha et al.(1981), Prakash and Kumar

(1987) have done extensive work in the field of journal bearings. They recognized

that the effect of synthetic lubricants can be significant depending upon the

concentration of solid particles in the lubricants. They found that polymers in the

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lubricants affect the friction, viscosity and load carrying capacity. Other researchers

Khonsari and Kim (1989), Dai and Khonsari (1992) have presented theoretical

models to incorporate micropolar effects in journal bearings under different

operating conditions. 3-dimensional roughness effects were considered by Tsann-

Rong (1996).

The theory of micropolar lubrication is governed by continuum mechanics. The

continuous media is considered as a set of structured particles possessing individual

mass and velocity. The definition by Eringer (1964) a simple micro-fluid is a

viscous medium whose behaviour and properties are affected by the local motion of

the particles in its micro-volume. This theory may be applied to contaminant effects

in journal bearings. But Ronen and Malkin (1981) considered that the concentration

of solid contaminants is usually too low to be worth considering. This resulted from

an experimental study of performance evaluation of a journal bearing lubricated with

solid contaminated fluids.

In recent years experimental results show that the Newtonian viscous lubricant

blended with small amount of long chained additives improve lubricant properties.

Furthermore Allen and Kilne (1971) demonstrated that the micro-continuum model

can be used for first approximation for modelling bearings lubricated with the oil

containing dirt and metal particles. Das (2002) studied the effect of contaminants of

different length micro-polar fluids on journal bearing performance.

2.3 Effect of Solid Contaminants on Journal Bearing Performance

Journal bearing contamination is very common because these bearings are normally

not sealed like rolling element bearings. The mechanism of contaminant ingestion

into journal bearing contacts is different from rolling element bearings mainly due to

difference in the order of minimum oil film thickness in their contacts. The order of

minimum film thickness is 10-100 times higher in journal bearings in comparison to

rolling element bearings.

Sliding and rolling element bearings operate under thick film lubrication called

hydrodynamic (HDL) and Elasto-hydrodynamic lubrication (EHL) regimes

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respectively and each exhibit low friction and wear. Though journal bearings are

much simpler in construction than rolling element bearings, the theory of their

lubrication mechanism is equally complex. An enormous amount of research on

bearing design has contributed to the development of high performance bearings.

McKee (1927) conducted a study on a journal bearing set-up to determine the effect

of contaminants on bearing performance. Friction was measured as a function of

bearing characteristic number (ZN/P), where Z is viscosity, N is speed and P is

specific load. He observed that solid contaminants are responsible for increased

coefficient of friction and bearings made of softer materials wear faster than the hard

material shafts.

Roach and Mich (1950) reported that in year 1945 Rosenfield investigated the effect

of particle size on bearing wear and found that the particles of the size of minimum

film thickness in the bearing are the most dangerous for elevated wear in bearings.

Roach and Mich (1950) conducted a study to examine the effect of solid

contaminants mixed with oil on temperature rise in journal bearings which is a

crucial parameter for monitoring the satisfactory performance of a bearing. The rise

in temperature was observed for different material combinations. They also

investigated the influence of solid contaminants on other bearing performance

parameters such as wear and embedability of the material pair. They identified three

basic situations with regard to the ratio between particle size and minimum film

thickness: the size of the abrasive particles is larger, smaller or equal to the height of

the film thickness in the contact. These can be mathematically represented by ‘K’

ratios;

K = 1, K > 1, and K < 1, where K = ha/hmin, where ha = height of the abrasive

particle and hmin = minimum lubricant film thickness.

The following conclusions were drawn from his study:

1. Particles of size smaller than the minimum film thickness in the contact are not

harmful to journal bearings.

2. Operating bearings at a high flow rate and a small l /d ratio where l is the length

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of the bearing and d is the diameter of the journal is a better way to avoid

embeddability problem.

3. Presence of abrasives in a lubricated contact is responsible for high friction

resulting in more resistance to achieve higher speeds without temperature rise.

Running such bearings with a larger film thickness is advisable to achieve longer

bearing life and low frictional losses.

In order to be more realistic, Rylander (1952) considered different types of solid

contaminants and examined their effect on the size of the contaminant in comparison

to minimum oil film thickness in the bearing and found that:

• The concentration of graphite particles reduced the lubricant flow rate in the

contact,

• Concentration of contaminants and coefficient of friction are linked,

• A hard shaft wears faster than the soft bearing because wear particles embedded

in the soft bearing surface act as a cutting tool, and

• Particles smaller than the minimum film thickness do not harm the bearing

performance as they pass through the minimum clearance without creating any

obstruction in flow of the lubricant through the contact.

Broeder and Hejnekamp (1965) measured the wear distribution (around the

circumference) in a hydrodynamic bearing with stationary radial load. Analysis of

Broeder and Hejnekamp results showed that significant liner wear occurs at the

circumferential locations where the local film thickness is less than the abrasive

particle size and that the wear rate is more intensive at locations of smaller oil film

thickness. They also observed different types of wear mechanisms such as pitting,

ploughing, and cutting in the test bearings.

Elwell (1977) used steel-weld spatters and fly ash as abrasive contaminants and

observed that the smaller particles liberated from the shaft as a result of large

particles striking the shaft with high force were more damaging than the large

particles themselves. Fly ash does not harm the surfaces but it creates a lapping

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action and makes surfaces smooth. However, this happened at only low speeds. At

high speed, the wear was high and surfaces were rougher.

Several lubricated wear models were developed by Rowe (1967); Rowe (1970);

Rowe (1986) for different types of additives in different wear modes. However the

performance of individual additives was presented mathematically without

considering the effects of abrasive particles. Ronen et al. (1980) prompted by the

high frequency of engine bearing failures on vehicles operating in the deserts of

Israel, conducted an experimental study on journal bearings and confirmed the

findings of Broeder and Heijnekamp (1965) in their preliminary studies.

Hirstch et al. (1980) considered roughness effects in their experimental studies on

bearings lubricated with oils containing solid contaminants. They used rough and

smooth bearings with particles of different sizes and confirmed that large abrasive

particles caused a greater amount of wear than the smaller particles. They also

observed a unique phenomenon of journal wear; in the presence of abrasive particles,

initially there was low wear in rougher journals as compared to smoother ones. The

rough journals became smoother during the wear process when the abrasive particle

size was smaller than the minimum film thickness. However, the bearing surface

roughness increased in the vicinity of minimum film thickness in presence of

contaminants in the lubricant. Their finding of low initial wear with the rough

journals is an important finding. They explained this phenomenon by a preferential

path theory. According to preferential path theory, particles find an easy way to flow

through valleys of rough surfaces in the contact zone, hence three-body abrasive

wear does not occur and that is why the wear rate is lower in the shaft at the initial

stage. Frith and Scott (1993) and Martin (1991) also supported this phenomenon but

they could not provide reliable experimental evidence.

Ronen and Malkin (1981); Ronen and Malkin (1983); Ronen et al. (1980) continued

their experimental work using contaminants with automotive filter testing such as

engine crank case sludge and Arizona dusts. Initially they confirmed that wear of

journal and liner under dynamic loading conditions depends upon the minimum film

thickness where large particles are primarily responsible for the wear. They also

emphasised that so called ‘clean oil’ contained wear particles which may be system

generated or ingested from other sources not taken into account initially. In

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another part of their experimental study they considered hardness of journal and

liners and studied six different combinations of journals and bearings and observed

that smaller shaft to liner hardness ratio causes relatively more liner wear and less

shaft wear. In their first mathematical model Ronen and Malkin (1981), they

explained that abrasive particles are either locked due to embedding in the soft

bearing material or they may roll. The shaft-to-liner hardness ratio of 3-4 is more

dangerous than higher hardness ratios. By controlling the minimum film thickness,

partial embedding of the particles can be avoided. They also concluded that

irrespective of size and hardness, contaminants increase the friction in bearings.

Their experimental work is quite comprehensive in nature and gives a solid base for

further research in this area.

In another experimental study on journal bearings, Dufrane (1983) and Dufrane and

Kannel (1989) confirmed that hydrodynamic bearings lubricated with clean oil

should be operated at a lambda ratio greater than 10, where lambda ratio is the ratio

of the minimum oil film thickness and composite roughness of the surfaces in

contact. They also warned that this ratio is not enough for bearings lubricated with

solid contaminants.

Contaminant effects on journal bearings were also examined by other researchers

Dufrane et al (1983), Watanabe et al. (1985), Dufrane and Kannel (1989). They used

five different grades of SiO2 abrasive particles with different hardness ratios (bearing

to abrasive). Their observations confirmed the findings of other researchers that wear

tends to be serious when particle size approaches minimum film thickness.

Prakash and Kumar (1987) studied the effect of contaminant size on unfilled PTFE

bearings, phosphor bronze and Al-Si alloy bearings under boundary lubrication. The

experimental study revealed that smaller particles (7-micron cut-off) caused

maximum wear in phosphor bronze whereas large size (25-micron cut-off) particles

were harmful for PTFE bearings. In general 15-micron particles caused maximum

wear in metallic bearings in comparison to 7 and 25-micron particles. Their results

are valid only in the boundary lubrication regime and therefore cannot be applied to

hydrodynamic bearings.

Fodor (1987), Fodor and Ling (1987) used Air Cleaner Fine Test Dust (ACFTD) and

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silica particles and studied the effect of their size and concentration on friction and

wear of hydrodynamic bearings. They found that friction and wear increase with

increase in size and concentration of the particles. They designed new filters based

on their previous studies on I.C. engines in a contaminated environment and

demonstrated that the oil change periods in these engines can be extended

significantly.

Xuan (1989) conducted experiments on a journal bearing test rig and found the effect

of different hardness ratios between journal, bearing and abrasives on wear of

individual bearing parts. They defined the limits of hardness ratios to achieve low

wear in the bearings.

Effect of abrasives and flash temperature considerations in contact zone are also

important from a scuffing point of view. Khonsari and Wang (1990) studied this

problem in depth and developed a model by which critical temperature and critical

abrasive size can be calculated for a given bearing by a governing equation. Their

model is very basic in nature and useful for further research on scuffing in bearings.

The following conclusions drawn from their studies are useful for research into the

abrasive wear of bearings.

• The size of particles, the hardness of the overlay and penetration depth of the

solid particle into the overlay influences the scuffing of the bearing,

• The flash temperature rises with rise in hardness of the overlay, and

• At higher speeds the critical size of the particle beyond which the chance of

scuffing is remote approaches the order of the minimum film thickness.

In continuation of their research, Khonsari et al. (1999) demonstrated that a particle

partially embedded in the bearing overlay can cause scuffing if the flash temperature

exceeds a critical value. They emphasized that the other factors which may influence

the scuffing are operating speed, hardness ratio, diameter of the particle, thermal

diffusibility of the slider and orientation of the particle when they are embedded

within the surfaces. The study led to a theoretical model in which the filter rating

required to minimise the failure rate can be determined. However this model is

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rudimentary and based on many assumptions and therefore requires experimental

confirmation.

The effect of speed on friction and wear was studied by Wlkstrom et al. (1993). They

used bronze and babbitt journal bearings with lubricants containing quartz and iron

particles and found that friction did not increase as significantly as the wear. At low

speeds the shaft surfaces were smoothed due to wear. They also confirmed that a

hard particle embedded in the overlay acted as a cutting tool for the journal.

Researchers Narayanan et. al. (1995) have shown that solid contaminants are not

only the foreign particles or wear debris but are also found in the form of additives.

Most lubricants contain different additives which are introduced to enhance certain

characteristics of the lubricant. Added to these, there exist undesirable contaminants

in the lubricant which along with additives form a dilute suspension in the oil. An

important effect of the solid particles suspended in the oil is to produce a thickening

effect. Also, it is found that there is an increase in the viscosity in the part of the

lubricant film which is in the vicinity of the journal and bearing surfaces due to

adhesion and other surface phenomena which have not been fully explained. This

results in a lubricant film with variable viscosity. Also, non-uniform distribution of

the solid suspended particles builds up concentration gradients which result in mass

transfer of these particles predominantly across the film thickness from the journal

surface, which results in a reduction of the thickening effect. In their study they

found that the results reveal enhanced load-carrying capacity and improved stability

characteristics for the micro polar lubricant as against the single-phase Newtonian

lubricant.

Among recent studies, Duchowski's (1998) experimental findings are very important

from the point of view of filtration requirements in journal bearings. He

demonstrated experimentally that the damaging particles are of the size approaching

minimum film thickness or bigger. He stressed that the existing filtration practices

need to be reviewed. In the light of his experimental findings he recommended that

the users of journal bearings (5.1 to 20.3 cm in diameter) should maintain cleanliness

level on the ISO 4406 scale below 16/14/12 and filter elements rated at 6 micron

(β6> 200) or finer must be used to minimise failures in journal bearings.

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Din and Kassfeldt (1999) performed experiments on a journal bearing in mixed

lubrication regime where self-generated solid contaminants were mixed with

environmentally friendly lubricants. The results showed that even though friction

was high, wear rate was low. The results obtained were influenced more by the

lubricant rather than the contaminant itself.

In a recent experimental study Mizuhara et al. (2000) showed that speed plays a vital

role in the wear of bearings when solid contaminants are present in the lubricant.

The increased friction due to contaminants when operating at low speeds disappears

at high speeds. The rate of change in friction reduces at higher concentrations.

Moreover, the friction depends upon the number of particles entering the contact.

Velocity dependence is mainly governed by the interfering time (the duration of the

particles staying in the contact) and load supported by the particles. A theoretical

model has been developed based on these findings.

2.3.1 Effects of abrasive hardness on wear

Hardness of the mating surfaces and abrasive particles influences the wear of bearing

elements severely and the wear of an individual component depends upon the

hardness ratios of the three bodies in contact. Researchers have examined the effects

of hardness of different constituents in the bearing contact and recommended some

hardness ratios for journals and bearings operating with lubricants containing

abrasives. The experimental studies conducted by Roach and Mich (1950), Rylander

(1952) were of a very basic in nature. Subsequently Broeder (1965) investigated the

tribological wear of HV 700 hardness mating with various bearing sleeves. The

mating pair was lubricated with oil contaminated by silicon carbide grain of an

average diameter of 21 micron. The wear of the shaft that mated with same hardness

HV 700 was three times less than the shaft that was mated with bronze sleeve with

HV80 hardness.

An important study in this area was carried out by Czichos (1978) who suggested a

systems approach to solve tribological problems and proposed three wear regimes

based on the hardness ratios between abrasive hardness Ha and hardness of the metal

surface subjected to wear Hm. These regimes are shown in Figure 2.2. Truscott

(1972) confirmed these models by experimental studies. The experiments were based

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on hydraulic systems and different critical ratios of particle to surface hardness ratios

for the three regimes of wear were determined.

Rigney (1994) demonstrated experimentally that in three-body abrasive wear, cutting

and deformation co-exist. He demonstrated that when hardness of the materials

changes, the ratio of cutting to plastic deformation also changes. The theoretical

model developed by him satisfies the experimental findings.

Figure.2.2 Effect of abrasive hardness on wear rate, Czichos (1978)

Xuan et. al. (1989) performed an exhaustive experimental study on a journal bearing

test rig and established relationships between the journal hardness-Hj, bearing

hardness-Hb and abrasive hardness-Ha. They conducted wear test for Hb/Hj ratios

0.75, 0.6 and 0.3. The bearing and shaft pairs were subjected to four types of

abrasive particles, with Hj/Ha ratio ranging from 0.14 to 2.75. From these

experiments empirical constants of the wear function were obtained. The critical

hardness ratio and the wear coefficients were also analysed. They concluded from

their study that the wear rate in journal bearings is maximum, when Hb/Hj ratio is

higher than one and Hj/Ha ratio is lower than one. The wear rate is the lowest when

Hb/Hj is low and Hj/Ha is high.

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2.3.2 Contaminant motion in lubricated contact

It is well known that under dry condition sliding motion causes more friction than

rolling motion. In a three body wear situation where solid particles are suspended in

oil, it is difficult to monitor the motion of these particles. A theoretical model was

presented by Ronen and Malkin (1983) for three body wear. This model was

rudimentary in nature; nonetheless it gave a new direction to other researchers to

explain the motion of abrasives in a lubricated contact. Berthier and Godet (1989)

have defined velocity and friction zones in sliding wear, and Fang et. al. (1991, 1992,

1993) gave a seminal theory entailing the motion of particles in three-body wear.

William and Hyncica (1992) extended this work by performing abrasive wear

experiments using abrasives in a foil bearing. They observed the motion of abrasive

particles when the size of particles was small in comparison to lubricant film

thickness. They also found that these particles tumble and leave erosive wear marks

on the surface and at higher ratios of abrasive size to film thickness, grooving of

surfaces occurred. The critical particle size to film thickness ratio in sliding contacts

is given by:

βsec/ =hD (2.3)

Where; D, h and β are defined in the Figure 2.3.

As shown in Figure 2.3, a particle of height D with grit angle β (always less than 90

and greater than 45 degree angle) and bigger than the film thickness gap h is

entrapped. The transition typically occurred for a ratio of about two. Using the force

equilibrium and geometry of a single abrasive grit they modelled the tumbling and

ploughing processes caused by the abrasives and showed the conditions of a particle

to be trapped in the soft body cutting the harder body. The model also demonstrated

how a harder material might wear more than its softer counter face.

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Figure.2.3 Particle Motion in bearing contact (William and Hyncica (1992)

Some researchers Fang et al. (1993); Fang et al. (1992); Fang et al. (1991); Kragelski

et al. (1992); Kragelski (1982) investigated the particle motion in a lubricated contact

and a new relationship for the motion of a particle in the contact zone was proposed

Fang et al. (1993):

V = αV1 ± βV2 where α + β= 1 ( 2.4)

21

2

HHH+

=α and 21

1

HHH+

=β (2.5)

Where V1 and V2 are the velocities of surface one and two respectively, and V is the

linear velocity of the particle with respect to the stationery surface. Factors α and β

are derived from the hardness ratios H1 and H2 of the two surfaces in relative motion

as shown in Equation 2.5. The sum of factors α and β is equal to one, thus their

individual value is always less than one. The relationship indicates that the velocity

of the particle is mainly governed by the harder material. This model was developed

considering a spherical abrasive particle moving at velocity V relative to the

stationery lubricated surface. Volumes of the deformed components of the abrasive

particles as well as the surfaces were calculated based on the geometry of the

particles.

Fang et al. (1991), Fang et al. (1992), Fang et al. (1993) developed a new apparatus

and conducted an extensive study on the motion of abrasive particles. In three body

wear they found a relationship in terms of coefficient of friction and particle

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dimensions, which helps to determine the type of motion occurring (sliding or

rolling). The sliding motion leaves scratches on the surfaces whilst rolling motion

creates pits. Wilkstrom et al. (1993) conducted some experiments at low speed and

low concentration (0.02%) of solid contaminants and found that the friction rise in

journal bearings was very low, and the surfaces were smooth due to lapping effect.

They emphasised the effect of the critical contaminant size to minimum oil film

thickness ratios (K ratios) on the wear of the bearing liner and established that K

ratios equal to one causes severe wear.

2.4 Anti-wear Additives and Performance Characterisation

The use of additives in lubricants began as early as 19th century when fatty oil and

sulfur were added to mineral oils to acquire higher load carrying capacities from

lubricants Booser (1983). As such lubricants perform several functions other than

keeping two mating surfaces of a machine component apart. The most important of

all is to reduce wear and friction to meet the tribological goals, which means

conservation of energy and material. The other functions are needs based and vary

from one application to the other such as corrosion, anti-oxidant, extreme pressure

(EP), viscosity index improvers (VI), pour point depressant, anti-foams,

detergent/dispersant etc. The world’s total lubricant production of more than 40

million metric ton Khorramian et al. (1993) all contain one additive or another.

Additives are chemicals added to a carrier lubricant to harness any one or more

properties mentioned above.

In hydrodynamic bearings, film thickness to roughness ratio (lambda ratio) is more

than four to ensure that there is no asperity interaction in the lubricated contact.

Hence ideally there is no wear in this regime of lubrication. However, this cannot be

assured due to two main reasons: firstly, machines start and stop, thus speeds vary

from zero to maximum during start and vice versa when stopping. Secondly,

unintentional changes in operating conditions do occur. In both cases it is the

minimum oil film thickness which is affected. These operating conditions, which can

affect the film thickness, are load, temperature, misalignment, contaminants, undue

vibrations, etc. Under these situations, bearings are lubricated with either no

lubricant film or only a few molecular layers thick as in boundary lubrication regime,

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Dorinson and Ludema (1985).

In an experimental study of vane pump wear Tao and Appeldoorn (1969)

investigated the effects of oleic acid and stearyl amine on different metal parts of the

pump. They observed that oleic acid performed best on iron oxide, which is basic in

nature, whilst stearyl amine is best on silica which is acidic in nature. No reduction in

abrasive wear by oleic acid was observed when a steel ball was loaded against a

grinding wheel. The experimental study revealed that the reactivity of additives

depends on the acidic or basic nature of the mating surfaces. They also observed that

the abrasives coated with antiwear additives do not adhere to surfaces and remain

loose in the contact thus preventing cutting action.

Metal-to-metal contact may occur due to low film thickness as a result of change in

operating parameters or due to entrapment of solid contaminants in the lubricant. As

explained earlier, the main sources of solid contaminants are either self-generated

wear particles or environmental dust particles. Metal-to-metal contact can be reduced

by adding film forming antiwear agent to the carrier lubricant which helps to reduce

friction between the abrasive and the contacting surfaces and prevent adherence

between them.

Friction is directly responsible for wear of metals. There are two types of friction –

surface-to-surface friction and fluid friction. Surface-to-surface friction is due to

asperity contact between the two mating surfaces and fluid friction is caused by the

resistance to motion between the molecules of the fluid. Friction reducing additives

better known as friction modifiers help to reduce the coefficient of friction, which is

the best indicator of low wear. Viscosity index and pressure-viscosity coefficient are

two important properties of the lubricant responsible for low fluid friction.

The other factors responsible for low friction are Lansdown (1982):

• material combination and their miscibility in each other

• their solubility in base oil

• atomic size of metals contained in lubricants

• valency of elements

• molecular structure of materials

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• electrochemical activity

• intermolecular forces

There are many antiwear additives available in the market but very few are available

in pure chemical form (generic). Most are sold in the form of an additive package

comprised of different chemicals to achieve desired properties of a lubricant. Each

constituent of the package is committed to perform its intended duty. Additive

technology is very complex and package design is the domain of chemical engineers

and chemists. Efforts have been made to find wear coefficients of several antiwear

additives and base oils Rowe (1970), Klaus and Bieber (1965); Forbes and Battersby

(1974); Forbes (1974) A number of wear models by Rowe (1967), Rowe (1970) and

Groszek (1962) under lubricated conditions were developed where the role of

temperature in adsorption and chemical reactivity of additives were taken into

account.

Din and Kassfeldt (1999) used environmental friendly rapeseed with synthetic ester

oil in a journal bearing lubricated under contaminated conditions. They recorded

high friction in these bearings but wear rate was very low. The possible explanation

for these results was that the abrasive particle size contained in the oil was large

compared to the film thickness in the bearings, which operated under mixed

lubrication.

2.4.1 Commonly used antiwear additives

The most commonly used additive packages in industry are identified by the name

of the prominent chemical group they contain, the most popular antiwear additives

known by the name of their chemical groups are: phosphate esters, sulfurized olefins,

sulfurized sperm oil, metal dithiophosphates, borates, phosphites and metal

dithiocarbamates. Properties of these additives are reviewed in brief to develop a

basic understanding of additives in this section.

Phosphate esters

The general formula of phosphate ester is O=P(OR)3 where R is alkyl group having

4 to 20 carbon atoms and a molecular weight between 200 to 1000 daltons. Zheng et

al. (1986) have measured the values of coefficient of friction and scar diameter on

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a Falex test machine of some of the lubricants and compared them with O-tricresyl

phosphate ester (TCP). These lubricants are: molybdenum dithiophosphate

(MoDTP), Zincdithiophosphate (ZDTP) and sulphurised olefins (SO). The results

revealed that TCP is the second best wear reducing additive as shown in the Table-

2.2.

This synthetic ester has the advantage of being neutral, ash less and stable at high

temperature. As far as their effectiveness in reducing wear is concerned, it was

reported that a 2% (by weight) sample of triaryl phosphate (TAP) in base oil

produces a scar diameter of 0.43 mm and load wear index of 25.2 under the test

conditions specified by ASTMD2266 (2004) and ASTMD2596 (2004) standards

respectively. Warne (1985) reported that TCP is hazardous for health, which prevents

its further use as an antiwear additive.

Table 2.2 Wear reducing properties of various lubricants, Zheng (1986)

Sulfurised olefins (SO)

Sulfurised olefins form a sulphide film on the lubricated surface and act similar to

other antiwear additives like MoDTP, TCP and ZDTP but their coefficient of friction

is low Zheng (1986). The SO mainly act as an extreme pressure additive. However,

they also act as an antiwear and antioxidant. Due to the presence of sulphur, this

additive is useful for high temperature applications but free sulphur poses a risk of

forming acids when in contact with copper or its alloys.

Sulfurized sperm oil

Sulfurised sperm is well known for increasing the load carrying capacity of

lubricated contacting surfaces, but it is not generally used alone. By adding

chemicals like chlorine or sulphur compounds, they form iron sulphide and sulphur-

chlorinated fatty material which are softer and act like a solid lubricant. These added

compounds help to form a good lubricating film on a surface due to the affinity of

halla
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the polar part of the molecules. The sulphur and chlorine react better under pressure

and elevated temperatures; therefore at higher loads prove to be better load carrying

agents. When these additives are used with ZDTP they act as effective friction

modifiers.

The use of sulphurised sperm oil was very common before 1970 but now they are

banned. Their use has been replaced by certain alkyl esters. As stated above, the

effectiveness of this additive increases many fold when added with chlorine and

sulphur compounds but they pose a threat in terms of corrosion of the surfaces due to

formation of hydrochloric and sulphuric acids.

Metal dithiophosphates

The use of lead salts in lubricants has been known to be toxic, hence lead

dithiophoshate has been replaced with other compounds Jiusheng (2003). Currently

metal dithiophosphates are popular, as they are better in terms of their antiwear and

toxicity properties. These are available in different forms of dithiophosphates such as

dialkyl, diaryl and alkyl type of compounds. Some of the most commonly used

additives of this family are discussed below:

Zincdialkyldithiophosphate (ZDDP)

ZDDP additives are very popular in industry today, not only as antiwear additives

but their antioxidant and anticorrosive properties against copper-lead bearings are of

equal importance for the users Klamann (1985). These additives are also used in

combination with other additives such as TCP, amine salts of phosphate esters,

sulphur fats and olefins. These were originally used in automotive lubricants as an

antioxidant but their usefulness as anti-scuffing and antiwear additives was identified

later from experience in service. The antiwear activity of these additives is an

important factor which needs to be considered when temperatures are high, Jahanmir

(1986). Kulczycki (1994) studied the effect of viscosity on ZDDP tribological

performance and characterised the additive according to their thermal stability.

Though the mechanism by which ZDDPs reduce wear and the process by which wear

occurs in their presence is not well understood, Bell et al. (1992). Marina et al.

(1997) have investigated the ZDDP film formation mechanism in relation to a stable

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film deposition of colloidal polyphosphate material. It was also found that at low

loads and temperatures, wear reduces two orders of magnitude whereas at increased

loads and temperature it increases by one order of magnitude, Jahanmir (1987).

Keeping in view the application of antiwear additives in fire hazard situations such

as: mining and metal working industry, aqueous antiwear additives were developed.

Most antiwear agents were oil soluble agents, which were dispersed in water using

surfactants. Two such long chain slats of zinc; polyoxyethelyne glycol phosphate and

polyethylene glycol thiophosphate (ZOP and ZTP) developed by Feng et al (1995)

showed good wear resistance in fire resistant lubricants. However, in the presence of

water, ZDDP is less effective as an antiwear additive due to hydrolysis.

Winer (1967) indicated that zinc is the secret to ZDDP’s performance; however the

dithiophosphate part of the molecule is equally, if not more, important. This additive

can be classified in two groups: neutral and basic. For primary and secondary ZDDP,

the former is mainly responsible for thermal stability whereas secondary ZDDP is

more effective as an antiwear additive. In fact it decomposes to hydrogenperoxides

and thus inhibits oxidation and modifies the surfaces in contact. In an experimental

study Liston (1992) has demonstrated that three types of ZDDP discussed above can

be chosen as either EP, antiwear or antioxidant additive depending upon the

application.

A number of researchers Khorramian et al. (1993) and Kapsa (1981) have

investigated antiwear properties of ZDDP of different types in combination with

different types of other additives such as detergents and antioxidants. They found

that these additives hamper the effectiveness of ZDDP.

Researchers have used Scanning Electron Microscope (SEM) and Scanning Auger

Microprobes (SAM) test rig; Marina (1997), to find out the antiwear mechanism of

ZDDP. They observed that it reacts with the contacting surface and forms a thin

layer. In another study the antiwear property of ZDDP was attributed to adsorption of

these additives, forming a layer of a friction polymer (Kawamura ,1983).

High contents of phosphorus in ZDDP can cause deterioration problems in the

presence of other additives. Researchers recommend that in the case of crank case

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oils where catalysts are present, the percentage of phosphorus needs to be below 0.1

% by weight, Khorramian, Iyer et al. (1993)

In an experimental study Glaeser (1992) concluded that sub-micron wear particles

found in many lubricated wear conditions represent a large surface area in a

lubricated wear situation, which can become a major factor in the depletion of the

lubricant antiwear additive.

In an experimental study Kano et al (2003) have found that ZDDP forms a higher

shear strength film than MoDTP. They also found that the film thickness depends

upon the type of additive, its concentration, the contact temperature and the rate of

heat removal due to wear. The antiwear property of these additives is associated with

the film thickness formed and scuffing occurs when the protective films have been

worn off.

Molybdenum dithiophosphate( MoDTP )

It was in 1878 that molybdenum was finally and clearly distinguished from its base

metal but it was readily available with reasonable purity in 1918. The real turning

point came in 1934, when low friction properties of molybdenum disulfide were

evident. Bell and Findlay (1941) reported the first successful operation of this

additive. A number of reviews have been published on this topic of growing interest,

for example Winer (1967) and Lansdown (1999) who recently published a book on

this subject. Mo S2 is used in dry powder, dispersion and compound chemical forms.

It is very widely used in the space industry as a solid lubricant and as a dispersed

additive in greases and oils for automotive and industrial applications. There are

many other forms in which MoS2 can be used, such as burnished coatings, sputtered

films, bonded films, composites and pastes.

According to Bell and Findlay (1941) the coefficient of friction of MoS2 varies with

several factors such as gaseous environment, humidity, temperature, load and purity,

state of orientation and consolidation of the film. It is not possible to incorporate

these parameters simultaneously while measuring the coefficient of friction

experimentally. There is controversy about repeatability of coefficient of friction

values reported by experimenters. However, the friction is at its lowest for fully

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ordered surface films in dry air or vacuum at high load and highest for randomly-

oriented films in the presence of water vapour or certain other vapours at low load.

This proves that MoS2 is less effective in moist conditions. However, it is almost

impossible in most cases to compare the results published by different investigators.

MoDTP is the most popular form of MoS2 to be used as a friction modifier in

industrial and automotive industry. Experimental studies by Zheng (1986) have

demonstrated that in engine oils, fuel consumption can be reduced by 2-5% with the

use of MoS2. This additive is better known as a friction modifier than an antiwear

additive. MoDTP decomposes with time and forms a MoS2 film on the contacting

surface, which is a low shear strength film and hence reduces friction significantly.

However, under dynamic conditions, these films are effective when, the contact

pressure between the two surfaces is below the critical pressure.

In Falex tests, Zheng (1986) found that the oil-soluble sulfurized oxymolybdenum

di-(2-ethylhexyl)-phosphorodithioate (MoDTP) has excellent friction-reducing

behaviour. He also observed that when MoDTP is used as an additive, the asperity

tips of the rubbing surfaces wear gradually and many micro-terraces, occur on the

surfaces, thus the rubbing surface becomes smoother

Antimony dialkyldithiophosphate (SbDTP)

The basic structure of SbDTP is similar to ZDDP and MoDTP, except that Sb

replaces the metal part of the molecule. This additive has better antiwear and

antioxidant properties (Khorramian et al, 1993) than ZDDP and MoDTP. It can also

act as an EP additive but requires a higher number of carbon molecules in the

lubricant to ensure its solubility.

Gold dihydrocarbylphosphorodithioate (AuDPD)

AuDPD prolongs the antiwear property of lubricating oils as reported by Khorramian

et al (1993). The salts deposit close strongly bonded metallic coatings of gold

directly on the metal surface being lubricated as a fixed, almost permanent, solid

lubricant. These solid films formed on the surfaces prevent the wear of the substrate

when moving one with respect to the other. It has been found that gold

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phosphorodithioate is superior to the corresponding zinc salt.

Phosphite Compounds

Phosphites are a derived form of phosphorous compounds and have proved to be

good antiwear agents. However, the mechanism of their wear reducing property is

not yet well understood. Researchers observed that phosphates or phosphites

containing long chain alkyl groups, formed smaller wear scar diameters than those

containing branched or aryl groups in a wear test (Khorramian et.al., 1993).

Metal Dithiocarbomate (DTC)

It is observed in automotive applications that in the presence of some catalysts,

phosphorous causes deterioration of the surfaces. In order to overcome this problem

dithiocarbomates (DTC) of some metals were developed. The general chemical

formula of these chemicals is (R2NCS2)x M where M represents Metal such as

Mo,Zn, Sb, Pb and R is alkyl group of 1-22 carbon atoms and x is the integer 1,2 or 3

depending upon the metal used. The main advantage of DTC’s is that they contain

reduced or no phosphorous and some are excellent copper corrosion inhibitors.

The antiwear mechanism of these additives is explained by Yuji and Gondo (1989)

MoDTC forms a film-composed mainly of MoS2. The coefficient of friction

decreases with increase in the percentage of MoS2 on the surface film. MoDTC has

better film forming capability than MoDTP and is therefore superior. A lubricant

containing ester of a polycarboxylic acid and glycol or glycerol with the selected

metal DTC derivative enhances friction-reducing properties even further. Zn DTC

helps inhibit corrosion and wear more effectively when combined with detergents.

Borates

Various types of borates are used, mainly as EP additives. However there are a

number of borate additive compositions which are useful as friction modifiers,

antioxidants and corrosion inhibitors. In general borates compounded with little or no

phosphorous are preferred as antiwear additives. In low phosphorous containing

lubricants it is preferable to use boron-containing compounds derived from hydroxy-

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containing ester, Kawamura (1983) and Khorramian et al (1993).

Borate containing additives are limited if they are to be used in the presence of

moisture as they crystallise and form solid hard granules. These hard granules act as

abrasive particles and cause severe wear of the surfaces. Experience has shown that

alkali metal borate dispersion slowly forms solid deposits on the shafts near the seals.

Thus during the motion, seals get abraded causing leakage of lubricant which may

lead to severe damage. Borates also create a compatibility problem when used in the

presence of other additives such as phenates, sulphurised fats and ZDDP.

In a study manometer zinc borate of 20-50 micron, antiwear, antifriction properties

have been examined by Dong and Hu (1998). It was found that this additive gave

low wear and friction coefficient and a significant increase in load carrying capacity.

He examined the surfaces under SEM and found that Diboron trioxide, FeB and FeB2

films were formed which helped to reduce the friction between the surfaces.

2.4.2 Lubricated wear and characterisation of additives

The primary function of a liquid lubricant is to reduce friction and wear. The

secondary functions are to carry wear debris and heat away from the contacting

surfaces. However, the acceptable liquid lubricant must have many other properties

which may be tailored by selecting a suitable additive package. A lubricant prevents

metal-to-metal contact between the asperities of two mating surfaces either by

forming a thick film in the hydrodynamic or elastohydrodynamic regimes, surface

films by physical or chemisorption, tenacious surface films by chemical reaction or

by prior treatment of the surfaces with some low friction material to form a solid film

or coating. The total load on the bearing surfaces is shared by the lubricant film,

surface film and by metal to metal contact depending upon the type of lubrication

mechanism, Thompson (1971).

Significant research has been carried out on the mechanism of surface interaction

between lubricants and additives. Many additives react with metal surfaces and the

energy of desorption of the surface reaction product becomes the controlling factor in

the effectiveness of the additive. There is a sufficient evidence Groszek (1962) that

energy of adsorption and desorption is responsible for the effectiveness of polar

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additives in preventing wear. Wear results for graphite in the presence of various

gases also were described by Rowe (1967). Later, the model was extended to the

competitive adsorption of lubricant additive and base oil molecules Rowe (1970).

Researchers were attracted towards wear in 1950s when first mathematical

relationship Archard (1953) was established between wear volumes and operating

parameters; load, sliding distance (l)and hardness as shown in Equation 2.1.

There have been controversies about this equation as this was preliminary or

rudimentary in nature. The same model has been extended with modified wear

coefficient ‘K’ as wear in boundary lubrication regime. There is a school of thought

who feels that the friction in the boundary regime needs to be considered in

conjunction with viscous shearing of the substance where asperity contact does not

exist. Hence the lubricated ‘Km’ value needs to be some fixed fraction of K value of

dry sliding. The modified reactive lubrication is commonly used for lubricated wear

and is a modified Archard’s equation:

m

m

PK

DV α

= (2.6)

Where comparing in Archard’s Equation 2.1; Pm is the hardness, and

KK m =α.

0UtRT

EXs

e ⎟⎠⎞⎜

⎝⎛−

=α (2.7)

Xe = diameter of area associated with an adsorbed lubricant molecule

to = fundamental time of oscillation of the molecule in adsorbed state

E = energy adsorption

U = sliding speed

Ts = surface temperature

R = gas constant

The new components wear faster because initially there are more asperity contacts

and the temperature is not enough to let the additive film form, Peterson (1980).

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There is no standard method developed to characterise an additive. However,

depending upon the purpose, an index may be derived of the additive. This may not

be possible for an antiwear additive because different antiwear behaviour is difficult

to predict. However lubricated wear of different metal pairs has been expressed in

terms of a wear coefficient, Peterson (1980).

Wear coefficients for different lubricants and additives have been reported in the

Wear Control Handbook (Peterson and Winer, 1980) with data obtained from a four

ball test. The values of K vary from 10 -6 to 10 -8. The pressure and speed for the test

conditions were far greater than that for sliding bearings so the values may not be

suitable for journal bearings. Blau (1997) reviewed 70 years research on the subject

of wear. He concluded that wear is broad in nature and the process itself very

complex with the variables chosen being either insufficient or not directly relevant to

the designer.

2.4.3 Bearing performance measurement techniques

Literature revealed that there are various methods for reporting the tribological

performance of machine components. Frictional losses and the loss of material due to

wear are the two main tribological performance aspects. There are various indicators

by which the performance of a machine can be represented, such as; temperature rise,

vibration level, and pressure drop in oil feed system. Tribological performance of a

machine can be determined either by loss of energy due to friction between the

machine components, or by the loss of material due to wear in them Peterson and

Winer (1980).

The wear in a journal bearing relates to its life, and there are several methods by

which this wear can be expressed. Weight loss is a direct method by which wear in

bearings can be expressed. However, there are several other methods by which wear

in bearings can be expressed qualitatively, such as: change in bearing dimensions

such as radial clearance, change in surface roughness, wear particle count, and wear

scar diameter. However, minimum oil film thickness is one of the key bearing

performance parameters that gives the tribological history of a lubricated contact,

and closely correlates to the wear and friction status in the bearing Peterson and

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Winer (1980).

In recent years, a number of non-conventional methods have been used for

determining the wear performance of a bearing, especially in bearings lubricated

with oils containing solid contaminants. Yuan et. al., (2004) have used vibration

analysis to correlate the concentration of the contaminants with the bearing vibration

level. Peng et.al. (2005) have also studied the problem on a worm gear test rig and

monitored and compared the wear debris analysis results with the vibration level.

They found that there is a strong relationship with the mode of wear and wear

severity with the vibration spectra. In a recent experimental study Maru and Castillo

et. al. (2007) used vibration measurement technique for correlating the damage in

rolling element bearings, due to solid contaminants. They recorded a change in root

mean square (rms) values in high-band frequency range of 600-10,000 Hz,

depending upon the type of contaminants and the wear damage. The tests were

simulated on a tribometer.

2.5 Effects of Micro-geometry on Bearing Performance

Micro-geometry of a journal bearing refers to radial clearance, surface roughness and

the out-of-roundness. These parameters change as wear progresses in the bearing.

The size of the minimum oil film thickness and change in micro-geometry are of the

same order of magnitude. The size of solid contaminants varies and many particles

are of the same order of magnitude as minimum oil thickness or micro-geometry

parameters such as: out-of-roundness, roughness. The effect of solid contaminants of

the size close to minimum oil film thickness is very harmful on bearing’s wear and

lubrication.

2.5.1 Roughness effects in hydrodynamic bearings

A theoretical consideration of effect of roughness in hydrodynamic bearings was first

studied by Tzeng and Saibel (1967) and subsequently by Christensen (1970). The

motive was to understand the effect of straighted roughness on film thickness, load

carrying capacity and friction in bearings. Roughness on the bearing surfaces was

considered one dimensional and modified film thickness (HT) in the Reynolds’

equation was substituted as:

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δ+= nT hH (2.8)

Where hn is the nominal film thickness and δ is the excursion of the profile from the

centre line which is a random variable and for new surfaces, the probability density

function was considered to be a Gaussian distribution. Tzeng and Saibel (1967)

predicted that the load carrying capacity of such bearings is high and frictional force

in an infinitely long bearing is low. They compared smooth and rough bearings with

film thickness defined as h and hn respectively and presented their theoretical

solution for transverse roughness case. Later Christensen (1970) extended Tzeng’s

model for the longitudinal roughness case. The conclusions from their studies are

given in Table 2.3.

Table 2.3 Results for infinitely wide bearing (Christensen 1969-70)

The modifications of Reynolds’ equation did not yield a simple equation applicable

for rough surface. This renders these theories impracticable and difficult to apply in

engineering design and practice. Patir and Cheng (1978) have proposed a general

theory for an arbitrary surface pattern.

A number of researchers developed algorithms and numerical methods to either

simplify the solution or to predict the film thickness more precisely than previous

workers for different roughness orientations (longitudinal, transverse or random).

The concept of a moving and stationary roughness Christensen (1970), Tzeng and

Saibel (1967) and Tonder (1986) was also introduced by researchers but the

predictions did not fully agree with experimental results produced by them.

However, theoretical models of Patir and Cheng (1978) proved to be more practical

than the others. The salient features of this model are:

Any roughness pattern on the lubricated surface reduces the lubricant film thickness,

halla
This table is not available online. Please consult the hardcopy thesis available from the QUT Library
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the film thickness decreases with an increase in load but the effect of the roughness is

independent of the load, the position of the roughness does not influence the bearing

performance (stationary or moving roughness), longitudinal and transverse roughness

pattern have the same effect on the bearing performance for a given size, and the

influence of roughness on the lubricant film did not depend on bearing internal

clearance or speeds.

In late 80’s some researchers Mitsuya et al. (1989); Mitsuya and Ota (1991) gave a

different concept of film thickness measurement by determining a different datum

line for measuring the film thickness and showed that they had better agreement in

their

experimental and theoretical results. Their studies were related to gas bearings; hence

their research did not gain recognition for conventional bearings.

Zielinski (1997) agreed to film thickness measurement method in rough bearings

approved by Mitsuya et al. (1989) and Mitsuya and Ota (1991) Furthermore, he

developed a new model based on the concept of material removal from the rough

surfaces.

2.5.1.1 Concept of Film Thickness and Material Removed from the Original

Surface

The approach used by Zielinski (1997) differs from other researchers due to the

selection of a datum line from which film thickness in rough lubricated contact is

measured. Existing surface parameters such as Ra and γ cause an ambiguity as two

surfaces having the same Ra values can be significantly different. Therefore these

parameters cannot be reliably used. Asperities above the centre line or mean line

cause restriction to flow whereas valleys below the line enhance the flow (provided

there is a pressure gradient).

2.5.1.2 Modified Bearing Surfaces

In a new concept in design to protect bearings from solid contaminants a two-

component surface layer was manufactured. Applying this concept to a journal

bearing, a soft layer of metal was applied as a corrugated coating on the surface of a

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journal. This geometry helped in excluding the contaminants from the bearing

contact. In a recent attempt Sep and Kucaba-Pietal (2001) and Sep (2004)

demonstrated that having a layer on the journal with soft metal with microgrooves

bearings can be made up to five times more wear resistant. The component surface

layer design of bearings is based on a concept of preferential path suggested by

Hirstch et al. (1980).

2.5.2 Worn journal bearing analysis

Journal bearings ideally operate in hydrodynamic lubrication regime and so they do

not wear. However, at the start when speed is close to zero, theoretically the film

thickness in the contact zone is zero and hence metal-to-metal contact occurs and

causes wear in the bearing. Normally the wear rate in such bearings is low and the

extent where the bearing is considered to have failed takes a long time. Under ideal

conditions it may last for more than ten years. Problems related to misalignment,

improper lubricant selection, abusive operating conditions and hostile environment

may cause the bearing to fail much earlier than expected. Duckworth (1957)

analysed wear in journal bearings. Forrester (1960) derived similar conclusions.

The change in micro-geometry of a bearing due to wear affects its performance and

causes a reduction in the load carrying capacity and the minimum oil film thickness.

The literature review revealed that very limited work has been done to study the

effect of change in geometry such as wear groove and change in radial clearance.

Previous studies have been performed on the transition from hydrodynamic to

boundary lubrication as speed of a six-inch bearing were reduced in the laboratory,

Elwell (1977) They recommended that the film thickness in the bearing needs to be

ten times the composite roughness of the bearing and the shaft.

Radial clearance determines the bearing performance characteristics.

In their work Chu and Kay (1974) on journal bearings found that the optimum

clearance has a direct link with the bearing diameter. A theoretical trend of minimum

oil film thickness to a radial clearance ratio plotted by them is shown in Figure 2.4.

Film thickness vs bearing radial clearance graphs can be plotted for various values of

bearing parameter (ηU/W). These graphs tend to have the shape depicted in Figure

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45

2.4. Safe operation of a bearing is expected only when the minimum oil film

thickness in the bearing is above 95% of the highest value obtained from this graph

can be expected when the operating minimum oil thickness is 95% to 100% of the

optimum minimum oil film thickness. Higher or lower values of radial clearance than

the optimum values may cause a reduction in film thickness.

The metrology associated with the roundness of a bearing affects the effective inside

diameter (ID) and outside diameter (OD) of the bearing and journal respectively.

The bearing or shaft may appear to be round – it may have a constant diameter, when

measured with the micrometer, but when the shape is greatly enlarged, scale it could

be as shown in Figure 2.5, Bagnel (1978). It is hard to achieve a perfectly circular

bearing or shaft. Depending upon the roundness a reference centre can be achieved

with the radii in all the directions varying and thus the radial clearance is different at

each point along the periphery. It is important to know the accuracy of the

measurements and its influence on performance. Since bearings operate on a film

that is a few microns thick the out of roundness needs to be within tight limits.

Figure 2.4 Clearance ratio and film thickness relationship Chu (1974)

halla
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Bearing failures due to various reasons have been studied by Katzenmeier (1972)

who found that improper lubrication is the major factor responsible for bearing

failures. Greenwood (1970) reviewed the research work of Tallian (1964), and

suggested that the minimum oil film thickness in a contact needs to be at least three

times higher than the value predicted by Tallian’s model. The reason given was the

electrical and thermal contacts which could lead to wear at the film thickness

obtained from the design process. Gradner (1978) also studied the effect of bearings

operating on low Sommerfeld number. In a similar study, Mokhtar (1978) presented

the effect of start and stop speeds on journal bearing wear.

Figure 2.5 Out of roundness magnified part of the edge, Bagnel (1978)

The effect of wear geometry was studied by Dufrane and Kannel (1989); Dufrane

(1983).They showed that, in a steam engine bearing, wear takes place under the load

point and suggested a geometrical model taking into account the worn region of the

bearing for calculations of pressure and film profile based on Reynolds’ equation.

They stated that an optimum amount of wear exists beyond which the altered

geometry would accelerate the wear. They suggested that the wear groove size and

shape depend upon the maximum wear depth δ0. They suggested two models for

simulation of the shape of the worn bearing region as follows:

halla
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47

⎥⎦

⎤⎢⎣

⎡⎟⎠⎞

⎜⎝⎛+−= θδδ cos1 0

CC (2.9)

( )θδδ cos10 −−=CC

(2.10)

Where δ0 is the wear depth at an angular coordinate θ and ‘C’ is the radial clearance

and δ is the non-dimensional wear depth. They also considered the effect of pressure

on viscosity of the oil. Both the models can be used with minor change in precision

value. However, the shape of the wear pattern may be the guiding factor for selecting

the model to achieve precision.

Hashimoto et. al.(1986), and Dufrane et. al.(1983) analysed the influence of the wear

defect on the pressure field and also on the eccentricity ratio. They showed that wear

defect damages bearing stability and that low L/D ratio bearings were less sensitive

to a defect. Vaidyanathan (1991) studied four bearings with different geometries for

their influence on parameters such as friction, pressure and Sommerfeld number.

Scharrer (1991) demonstrated that small wear defects have only slight influence on

dynamic coefficient of a hydrostatic bearing. The stability of a bearing was also

studied by Tanaka (1994) and Kumar and Misra (1996). They studied the

hydrostatic bearing stability and extended the work of Suzuki to show that the wear

defect decreases the stability even at light loads. In another study in the same year

Kumar and Misra (1996 b) analysed noncircular journal bearings operating in

turbulent flow and showed that the wear defect increases the flow rate and friction

and reduces the load capacity of such bearings.

In subsequent studies Mizuhara et al. (2000) extended the research by showing that

the friction increases in the bearing lubricated with oil containing solid particles

however the effect disappears as speed increases.

In a recent study Fillon (2002) has considered wear grooves of different radial

clearance and maximum wear depth ratios and determined pressure distribution, film

profile, temperature rise, oil flow rate, power loss and film thickness profile. He

concluded that worn bearings do not always present disadvantages but may have

some advantages such as reduced temperature rise as the geometry of such bearings

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may come close to a lobed bearings. His solution is purely theoretical without any

experimental support.

2.6 Knowledge gaps

Thorough literature review was carried out to contextualise the aims and objectives

of this research project within the current state of art in this area. This ensured that

the research carried out in this project adds to the existing body of knowledge. The

following knowledge gaps were identified through literature review:

• Lack of detailed study on the effect of solid contaminants treated with

antiwear additives on journal bearing wear

• Need for characterisation of antiwear additives based on their efficacy for

dusty applications under hydrodynamic lubrication

• In-depth knowledge of the effect of solid contaminants on the bearing micro-

geometry, and its effect on the bearing’s tribological performance

• Lack of any standard numerical parameter for classifying the performance of

antiwear additives operating in dusty hydrodynamic lubrication conditions

2.7 Conclusion

The literature review included areas of research such as: wear mechanism,

contaminants types, sources and their impact on wear, journal bearing design,

lubrication and wear, bi-polar lubricants, bearing micro-geometry, antiwear

additives, and the effect of roughness on bearing lubrication.

The main focus of the literature review was on the performance of journal bearings

lubricated with oil containing solid contaminants treated with antiwear additives. The

reviewed literature covered knowledge on issues such as types of contaminants, their

morphology, concentration and hardness. Furthermore, it covered their impact on

journal bearing wear.

Literature on bi-polar lubricants explained the current hydrodynamic theory and its

application to contaminated bearings. Significance of oil film thickness and latest

measurement techniques were also reviewed in for oils containing solid contaminants

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treated with antiwear additives.

However, researchers have not studied thoroughly the effect of additives on bearings

lubricated with oil containing solid contaminants. The effects of change in micro-

geometry parameters such as out-of-roundness and radial clearance due to

contaminants treated with antiwear additives have also not been studied extensively.

Thus the literature review was useful in refining the research problem by making use

of existing knowledge base and finally in preparing a strategy to meet the aims and

objectives of this research.

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BLANK PAGE

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CHAPTER-3

3. EXPERIMENT DESIGN AND DEVELOPMENT

3.1 Overview

Experiment design comprised the road map for the experiment setup and procedures

used in this project, and this led to the development of new practical and theoretical

methodologies for improving bearing design and metrology.

This chapter comprises of two parts, in the first part all the experimental

requirements were identified; including identification of performance parameters,

procurement of materials, instruments, instrumentation and their setting up, and also

some preliminary test results. In the second part, a preliminary study on micro-

geometry of bearings and issues related to them were investigated. This resulted in

identifying some problems and finding their solutions.

Journal bearings are one of the most commonly used tribological components that

are not sealed or shielded. This results in solid contaminant ingress in the lubricated

contacts of the bearing. These contaminants cause wear and as a result micro-

geometry of the bearing changes, which results in poor tribological performance and

reduced bearing life. These problems are more severe when a machine works in a

dusty environment. The use of antiwear additives is common in the industry to

enhance the performance and the life of such bearings. Although, antiwear additive

manufacturers claim superiority of their product, no established method exists by

which their claims can be verified.

After reviewing the literature and analysing the problem, it was concluded that there

is a need to study the effect of solid contaminants treated with antiwear additives on

journal bearings, and specifically, on their micro-geometry – i.e. surface roughness,

roundness and radial clearance. Furthermore, there is a need to develop a systematic

methodology for determining the efficacy of antiwear additives.

To achieve these objectives, the following factors had to be considered (i) bearing

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design (ii) types of antiwear additives (iii) amount and types of contaminants, (iv)

antiwear additives, (v) operating parameters, (vi) wear measurement techniques, and

vi) available resources such as test rig, time, money, expertise, and measuring

equipment.

There are no standard criteria to select methods and techniques for measuring wear

performance of journal bearings, hence a suitable criterion for defining the

performance of a journal bearing was developed. Parameters were identified to

represent the wear performance of the journal bearing. These parameters included:

weight loss, change in micro-geometry, and change in particle count.

Bearing micro-geometry has been used in this research for tribological performance

testing. The main micro-geometry parameters used include: out-of-roundness, radial

clearance and wear depth; the effect of these parameters on oil film thickness has

been used as the tribological performance measure.

This chapter presents the experimental details including bearing design, selection of

input and output parameters, test rig modifications and instrumentation, selection of

additives, metrology of micro-geometry, wear measurement techniques and

measurement of minimum oil film thickness, to examine the combined effect of

contaminants, additives and micro-geometry. Strategy for collecting and analysing

data was also prepared as a part of experimental design.

3.2 Identification of Performance Parameters

There is no single parameter by which the performance of a bearing can be

measured. The tribological performance of a journal bearing ultimately relates to its

capacity to conserve energy and materials. These can be measured by the friction

forces and the wear in the bearing under the stated operating conditions. The

tribological performance of a machine component can be compared with other

components under the same operating conditions rather than measured in absolute

terms. A machine may comprise of several bearings so that it is difficult to accurately

measure the frictional loss in an individual bearing. Similarly the amount of wear in a

bearing is usually so small that it is difficult to predict the life of a bearing. Moreover

there are several methods by which wear in a bearing can be measured but there is no

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surety that the results obtained from different methods will produce the same

magnitude of wear. Another difficulty is that the repeatability of test results is poor.

Thus a multi-wear parameter approach where several wear measurement parameters

have been recorded and compared has been adopted to address this problem. Due to

the reasons stated it is also not possible to measure the friction and wear directly but

some parameters have been identified that represent the tribological performance of

the journal bearings subjected to test in this study.

3.2.1 Parameters as measure of energy conservation

The direct method of assessing the energy losses in an operating bearing is to

measure the friction force in the bearing. Attempts were made to measure the friction

force in an operating bearing but it was concluded that unless a sophisticated system

with air bearing support is used to measure the small change in friction the

distinction between the friction forces in the bearing under the influence of different

antiwear additives cannot be made.

Since friction force measurement in a bearing is a complex procedure, common

practice is to measure and compare parameters such as temperature rise, oil pressure

drop, vibration and noise. The temperature rise in a bearing indicates that the friction

in a bearing is high. However, the rise in temperature may be due to viscous shearing

or due to metal to metal contact and it is hard to ascertain the contribution of each

factor individually. Reduction in inlet pressure indicates that the load carrying

capacity of a bearing has reduced if all other operating conditions are kept the same.

This may be due to increase in radial clearance or wear in the bearing which in turn

influences the bearing performance in two ways; a reduction in bearing pressure and

an increase in lubricant viscosity due to cooling of bearing as a result of excessive

side leakage. Vibration and noise measurement are commonly used condition

monitoring tools. Change in vibration mode or level in journal bearings is mainly due

to misalignment, severe wear marks on the bearing surface, entrapment of a large

solid particle or transfer of fluctuating forces from the surrounding area. It is difficult

to identify the contribution of each of the influencing parameters.

Performance testing of bearings requires exactly the same operating conditions for all

additive cases including inlet oil temperature (40 0C) and oil feed pressure 100 kPa.

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Therefore neither of these two parameters could be used as performance measures.

Since contribution to vibration and noise may be from sources within or without the

bearing components these may prove to be a very complex method for investigating

the minor changes due to additives.

With cognisance of above limitations and those of the test rig used for the

experimental study, other fundamental aspects of journal bearing lubrication were

examined and this helped to identify the parameters used to represent the bearing

performance.

A bearing operating in the hydrodynamic lubrication regime, where specific film

thickness (lambda ratio) is between four and ten, an optimum oil film thickness is the

key to the desired performance of a bearing. A change in friction force, rise in

temperature or drop in bearing inlet pressure are directly linked to the oil film

thickness in the bearing contact zone. Change in performance parameters occur

when there is a change in oil film thickness at the contact. A bearing will run

satisfactorily as long as an optimum specific film thickness at the contact exists.

Although a temporary change in operating conditions such as inclusion of solid

contaminants, change in viscosity or temperature may compensate the effect of one

parameter over another, the final impact on bearing performance is the oil film

thickness in the contact. Hence the change in minimum oil film thickness in a

bearing can represent the influence of an individual antiwear additive or of

contaminants on the performance. The minimum oil film thickness is a small

quantity but with current techniques it can be reliably measured in a bearing with an

accuracy of a few microns. Though the measurement of oil film thickness in a

bearing of an operating machine may not be practical, it can be easily achieved in a

laboratory setup.

3.2.2 Parameters as a measure of bearing life

A tribological component is said to have failed when it is unable to perform its duty

to the accepted level of performance. The geometry of a journal bearing is the key to

achieve desired oil film thickness. When the geometry changes due to wear are

beyond an acceptable limit the bearing cannot carry the rated load and is considered

to have failed. A critical geometrical parameter of a bearing is the radial clearance. A

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larger clearance than the design requirements results in a thinner oil film at the

contact thus increasing the friction and temperature rise with a subsequent further

reduction in film thickness. When the film thickness reduces to an extent where

metal to metal contact occurs, significant wear takes place and the radial clearance

increases further. This causes the film thickness to keep reducing with hydrodynamic

lubrication being replaced with the mixed then boundary regimes until seizure due to

scuffing takes place. A bearing may be able to form hydrodynamic film at low loads

but if it cannot sustain the rated load it is said to have failed. Thus the rate of wear in

a bearing correlates directly to the bearing life.

There are several methods for measuring wear and the most appropriate ones have to

be chosen. It is a well known fact that the wear tests have poor repeatability and

reproducibility and hence the results differ from one test to another, depending on the

test equipment. It may be difficult to establish which method gives the most reliable

results. A difficulty is that the amount of wear is very small in comparison to the

specimen size in which case the resolution of the measuring instrument becomes of

paramount importance. In such cases it is helpful to utilize more than one

measurement method and by comparing the results of one with another the reliability

of the measurement technique be established. It was decided therefore to explore

several wear measurement techniques for the bearing components. In this case the

selection of wear measuring techniques depended on the availability of resources

also. The wear measurements were categorised in the following three groups:

1. Weight loss: weight loss in both bearing elements

2. Change in micro-geometry: such as; out-of-roundness, roughness and

radial clearance, maximum wear depth

3. Particle counts: including wear debris weight

3.3 Journal Bearing Design

A requirement was that the bearing had to fit the existing test rig. A bronze bearing

with a steel shaft sleeve 40 mm nominal internal diameter (ID) and 40 mm nominal

shaft outer diameter (OD) with L/D ratio 1 was designed using the ESDU method

ESDU84031 (1996).

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Figure 3.1 Bearing and journal drawing

BE

AR

ING

M

ATE

RIA

L LG

2 B

S 1

400

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The dimensions of the bearing with tolerances are shown in Figure 3.1. A sample of

bearing design parameters is shown in Table 3.1 and hardness measurements on

bearing and shaft sleeve samples are shown in Table 3.2.

Table 3.1 Sample of test parameters

No. Parameter Value

1 Oil viscosity 0.042 Pa s (40 oC)

2 Inlet temperature 40 oC

3 Oil feed pressure 1 bar

4 Required min. oil film thickness 16 μm

5 Contaminant (Al2O3) size 16μm (nominal)

6 Required K value Close to 1

7 Sliding distance (l) 7536m

8 Contaminant concentration 4 g/l

9 Speed (varies) 400-550 rpm

10 Load (Fixed) 500N

11 Bearing weight 330 g approx.

12 Shaft sleeve weight (nominal) 178 g approx.

13 Out of roundness 2-10 μm

14 Surface finish required <1.0μm Ra

15 Particle counts Results vary

16 Additive type 5 different types

17 Radial clearance 80-90 μm

18 Probe scale factor 25 micron/V

19 ID bearing (tolerance) 016.0040+

− (mm)

20 OD shaft sleeve (tolerance) 0016.08.39 +

− (mm)

21 L/D ratio 1

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Table 3.2 Hardness measurements on bearing and shaft sleeves

Bearing Part

Location 1 Hardness

Location 2 Hardness

Location 3 Hardness

Average Hardness

Steel Bush No.1 ASI 4143

27.5 HRC 27.5HRC 29.0HRC 28.0HRC

Steel Bush No.2 ASI 4143

27.0 HRC 28.5 HRC 28.5 HRC 28.0HRC

Steel Bush No.3 ASI 4131

29.5 HRC 27.0 HRC 27.0 HRC 28.15HRC

Bearing No.1 Bronze LG2 BS 1400

75 HB 78 HB 78 HB 75HRB

Bearing No.2 Bronze LG2 BS1400

81 HRB 74 HRB 74 HRB 76.3 HRB

Bearing No.3 Bronze LG2 BS1400

74 HRB 74 HRB 78 HRB 75.3 HRB

The bronze bearing and shaft sleeve materials were chosen as LG2 BS1400 and EN

ASI 4143 steel respectively. The hardness of the bronze varied from 74 to 81 Brinell

hardness (Rockwell 'C' scale). The shaft sleeve material chosen was low carbon steel

its hardness varied from 27 to 29.5 HRC. The hardness measurements for 3 bearings

randomly picked are shown in Table.3.2.

Initially the bearing was designed with 100 micron diametral clearance. When

preliminary tests were carried out, the wear marks due to misalignment occurred on

two opposite ends of the bearing and a larger clearance was chosen. It was decided

that the bearing would operate on low speeds and loads. A bearing with 180 micron

diametral clearance was found to be satisfactory. The bearing design called for a

lubricating oil of viscosity 0.042 Pa.s at 40 oC inlet temperature. Standard bearing

tolerances were maintained as desired for a bearing with chosen design parameters.

The calculations were also checked analytically. A sample of test conditions used in

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this experimental study is given in Table 3.1. Similar analysis for different operating

conditions has been obtained using ESDU 84031 software program available on-line

and the results are included in the (Appendix-B).

3.4 Contaminant Selection and Characterization

Aluminium Oxide (Al2O3), which was used as the test contaminant, is one of the

most versatile refractory ceramic oxides and finds use in a wide range of

applications.

It is found in nature as corundum which exists as rhombohedral crystals with

hexagonal structure. The unit cell is an acute rhombohedron of side length 5.2Å and

plane angle ~55°. It is the close packing of the aluminium and oxygen atoms within

this structure that leads to its good mechanical and thermal properties.

This has very high melting point of 2015±15 °C and refractive index 1.765. The

product supplied by the manufacturer (Australian Norton Abrasive Pty Ltd) is

reported as 99.75% pure. An optical analysis on Scanning Electron Microscope is

shown in Figure 3.2. The grading of the powdered product is also given in Appendix-

A Table A3.2. The reported size of the particles is F 400 (17.3±1 microns mean

diameter). The bottle of sample used for the experimental study was labelled grade

F400 Micro-grit and 16 microns overall size.

The nominal size of the aluminium oxide powder was verified by Mastersizer 2000

supplied by Malvern Instruments. The powder was mixed with water to form slurry

for the analysis of size distribution. It can be seen that the actual particle size was

slightly larger than the 16 microns specified by the supplier. Since variation in the

measured and specified value was not greater the latter was accepted as the true

value for experimental work.. The reason for accepting the specified value was due

to doubts that powder may not have been well mixed before taking the sample and

the measurements could not be repeated. An Energy Dispersive X-ray Analysis

(EDAX) image of the Al2O3 shown in Figure 3.3 confirms the purity of the product.

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Figure 3.2 SEM micrograph of Aluminium Oxide particles

3.5 Lubricant and Additive Selection

Selection of base oil is a part of hydrodynamic bearing design. As a first step of

bearing design, base oil viscosity and radial clearance are chosen for given operating

conditions by a rule of thumb. Then chosen oil viscosity is verified for design

criteria. If design criteria are not satisfied, either oil with different viscosity is chosen

or radial clearance is varied using iterative process till the design criteria are

satisfied. Viscosity is the most important lubricant characteristic directly responsible

for forming an optimum film thickness in the bearing for given operating conditions

However, a lubricant has to discharge many other duties apart from forming an

optimum oil film thickness in the bearing. Depending upon the application and

requirements oils are treated with additives. These additives are identified either by

their chemical names such as sulphur-phosphorous, MoS2, graphite etc. or by the

duty they discharge such as antiwear, friction modifiers, viscosity improvers, etc. In

this particular case, the base oil and antiwear additives were chosen by Fuchs

Lubricants Australia based on their long experience and they supplied the products

for the research.

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3.5.1 Base oil

Fuchs supplied the base oil manufactured by Caltex Oil Company and the additives

by different additive manufacturers. The base oil belonged to paraffinic group,

ALOR 300 Solvent Neutral with a viscosity of 55.0 cSt at 40 oC, density 0.876 kg/L

at 15 oC and Viscosity Index 96. The lubricant contained 4g/L, powdered Al2O3 of

16-micron size as solid contaminants. Some experiments were also performed with

contaminant concentration 0.1 to 0.2 g/L concentration. The amount of wear was too

small and could not be measured reliably. Fuchs have found from experience that

solid contaminants in mining industry reaches more than 5 g/L. and hence 4g/L was

the chosen concentration.

3.5.2 Additives selection

There were a total of five additives supplied by the industrial research partner and

these were chosen from range which is widely used in the field. The reported

information is limited due to confidentiality policy of the manufacturers. Additive

details obtained from the supplier are given in Table 3.5. These antiwear additives

are commonly used in mining industry for lubricating sliding bearings.

Figure 3.3 EDAX elemental analysis of Al2 O3

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Additive Treatment

The additives listed in Table 3.5 were mixed with base oil in recommended dosages

by following the safety instructions and procedures advised by the suppliers. The

standard procedure was as follows:

• Calculate the quantity of additive required for 4 litres of base oil either by

volume or by weight.

• Weigh the required quantity of contaminants

• Soak the contaminants in a petty dish with 10ml additive overnight.

• Take 4 litres of base oil and pour 3 litres of it in the sump of the test rig and

heat it to 60 0C and circulate it for 30 minutes in the test rig.

• Mix the quantity of additive with the sump oil.

• Mix the additive soaked contaminants in the sump of the test rig

• Rinse the additive container (beaker) and the contaminant container with the

remaining 1 litre oil to top up the sump to 4 litres.

• Let the oil circulate in the hot oil system for one hour before starting the test.

Figure 3.4 Test rig assembly

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3.6 Test Rig and Instrumentation

An existing test rig (Figure 3.4) was used for this study. It required several

modifications to the loading and oil supply systems motor drive, housing and

proximity probe mounting system.

The rig has a provision to hold a stationary bearing of 40 mm diameter in a housing

floating at one end of a shaft supported on two rolling element bearings. The

designed test bearings were fixed in a 30-mm wall thick steel housing. The outer

surface of the bearing is slightly tapered with a bush in the housing. The bearing at

the non drive end of the shaft is guided through a pin so that its position aligns with

the housing holes for the proximity probes and the oil supply. This end of the shaft

forms a cantilever over which a test shaft sleeve is keyed. This sleeve fits inside the

test bearing which is mounted in the housing. Movement in the horizontal direction

is constrained by a check nut. The ID of the bearing was chosen in correspondence

with the shaft sleeve diameter to achieve the desired radial clearance. Test bearings

and shaft sleeves are replaceable.

Table 3.3 Antiwear additive properties

Additive** Lube Category Chemical Family Concentration*

A3 Hydraulic Oil additive Confidential 0.7% by volume @ sp.gr. 1.0

A4 Hydraulic fluid Aryl phosphate esters

1% by weight @ 0.89

A5 Hydraulic fluid ash less antiwear additive

proprietary blend, confidential

5% by Volume @ sp. Gr 0.95-1.055

A6 Gear and hydraulic oil antiwear, anti corrosion and friction modifier additive

Sulphur/ phosphorous based

2% by weight @ sp.gr. 1.69 (at 15.6 oC)

A7 Lubricant Additive Isopropyl Oleate; fatty acid, isopropyl ester

1% by weight @sp gr. 0.86

*Specific gravity measured at 15C. ** Product names were suppressed to maintain the manufacturer’s confidentiality.

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The shaft is supported on two self-aligning rolling element bearings. Originally the

drive was via a constant speed a 1420 rpm constant speed 1200 Watt electric AC

motor, the speed of which could be changed with the help of three step pulleys. This

was changed to a continuous variable speed 3 phase AC speed control system giving

0 to 1420 rpm with an accuracy of ± 5 rpm. Further details of the test rig and some

preliminary results have been reported by Sharma and Hargreaves (2001) in

Appendix - A.

Loading system

The load was directly attached to a hanger attached to the bearing through an eye bolt

as shown in Figure 3.5.

Figure 3.5 Loading System

Loads

Journal

Hanger

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Oil supply

The oil supply system consisted of a reservoir supplying oil to a peristaltic pump

below by a flexible tube. Flow rate and therefore oil pressure were controlled by pass

throttle valve in parallel with the main oil supply line. A constant temperature

heating system with a thermostat capable of ± 1 0C accuracy was fitted in the oil

reservoir. It was observed that the temperature recorded by the dial gauge of the

thermostat varied with the ambient temperature and so it was adjusted and set to give

40 0C at the closest possible location to the bearing oil inlet. The temperature at the

entry was monitored by a thermocouple connected to a handheld electronic

measuring unit. The oil entered through a flexible pipe connected to a nipple on the

bearing housing and the out coming oil was collected in a perspex container which

was connected to the main oil reservoir. The oil pressure was maintained at 100kPa

to assure full fluid film lubrication during the test. A type K chromel-alumel sensed

the temperature which was controlled by type PN-4BIC device. The controlled

temperature bath ensured oil supply to the bearing at 40 ± 1 0C. The oil circuit is

shown in Figure 3.6.

Figure 3.6 Oil Circuit

Journal bearing Main valve

Pump

Bypass valve Oil sump

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Proximity probes for film thickness measurement

The bearing housing had a provision to mount two REBAM-3300 proximity probes

at right angles to each other for measuring the oil film thickness. The probes were

screwed into the housing and through the holes in the bearing at a minimum distance

from the target (shaft sleeve) in order to give a linear output. .This distance was 3

mm or 10volt output. The bearing also had a provision for mounting a thermocouple

at the bearing surface.

3.7 Multi-Wear Parameter Approach (MWPA)

Wear tests under lubricated conditions are very time consuming and the wear

measurements have very poor repeatability. During preliminary testing it was

observed that after running long duration tests the wear in bearing was small and

while repeating the test bearing failed without prior warning. There were two

potential strategies to improve the accuracy and saving time, first, to conduct long

duration tests and to repeat them till reliable results are obtained and second, to

conduct short duration tests and measure wear using different measurement methods.

Keeping in view the time factor and the resources available, the second strategy was

adopted. This required a methodology for selecting the wear measurement

parameters, which in this thesis is referred to as multi wear parameter approach

(MWPA). Using this approach the measurements were categorised in three main

groups, i.e.

a) weight loss

b) change in micro-geometry

c) change in particle count.

All performance parameters that could be measured confidently in the laboratory

were identified as discussed in section 3.2. In this research wear was measured by

different methods and test results were compared for their reliability and precision.

On the basis of consistency of results and principle merits, the best method was

chosen for characterisation of anti-wear additives. The MPWA is shown in Figure

3.7 and the various methods are discussed below.

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3.7.1 Weight loss

Weight loss in the bearings and shaft sleeves was recorded by weighing the bearing

and shaft sleeve before and after the tests. The accuracy of the weighing scale was to

three decimal places in grams. All the bearing and shaft sleeve test specimens were

degreased by dipping them in hexane for five minutes and subsequently cleaning by

ultrasonics for ten minutes before weighing. It was difficult to repeat the results to

third decimal place accuracy. However after extending the test duration, accuracy to

two decimal places was obtained. The results obtained were useful for observing

metal transfer and determining the mode of wear of the components.

3.7.2 Out-of-roundness

Out of roundness was successfully used by Zeilinski (Zeilinski, 1997) and Martin

[Martin 1991] as a wear measuring parameter. The change in the out of roundness of

a bearing after the test correlated well with the amount of wear. The out of

roundness measurement process is time consuming and so it was decided to measure

it only for the test bearings since this was stationary part. Under loaded conditions,

wear occurs at the contact zone of the test bearing whereas; wear of the shaft sleeve

is virtually uniform around its circumference. Although the shaft sleeve out of

roundness may also change it is not as distinct as that of the bearing.

The Taylor Hobson Talyrond 100 was used for out-of-roundness measurements

Figure 3.8. These were taken at three positions along the bearing length, i.e., top,

middle and end. The measurement of out of roundness at the middle position was

difficult due to the oil feed groove and the holes for the proximity probes.

The standard probe of the Talyrond was modified to avoid the sudden jerk due to

holes in the bearing. These jerks caused displacement of the specimen and hence an

aluminium plate with a shallow groove of the size of the bearing OD was fabricated.

This plate could hold the bearing firmly in position. A closer study of the out of

roundness method revealed the superiority of this technique for measuring wear of

the bearings. It also raised several serious issues with regard to current metrological

practices in tribology. In fact, it raises the fundamental issue of accurately measuring

radial clearance.

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Wear measures

Change in weight

Bearing wt. loss

Sleeve weight

loss

Wear debris Change in geometry

Debris weight

Particle count

Out of roundness Radial

clearance

Surface roughness

Max. wear depth

Sleeve Bearing

Circumferential Transverse

Transverse Circumferential

3.7.3 Radial clearance measurements

Radial clearance constitutes the micro-geometry of a bearing and is a key design

parameter for determining the load carrying capability. As a guide the radial

clearance for a bearing is taken as one thousandth of its radius. Smaller, clearances

generate greater load carrying capacity of a bearing for the same operating

conditions.

For studying the effect of change in micro-geometry on bearing minimum oil film

thickness, it is important that radial clearance in a bearing is measured with a fair

degree of accuracy especially when the anticipated minimum oil film thickness in the

bearing is small as every one micron change in radial clearance reduces the film

thickness by approximately 1%. The measurement of radial clearance for the test

bearings varied from one method to another and from one position in the bearing to

another by up to 50%, thus emphasising the importance of metrology for successful

bearing performance.

Figure 3.7 Multi-Wear Parameter Approach (MWPA)

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The measurements of radial clearance were obtained by measuring the ID and OD of

the bearing and shaft sleeve respectively. The specimen was fabricated in the

workshop according to the drawing shown in Figure 3.1.

To confirm the dimensions the ID and OD of each test bearing was measured

separately to cross check the actual radial clearance. The design guidelines indicate

that the nominal ID and OD were 40.00 mm and 39.82 mm respectively, giving

minimal radial clearance 90 microns. However with tolerances the maximum ID

could be 40.00 + 0.016 mm and minimum OD 39.82-0.016 mm and hence the radial

clearance can fall any where between 90 microns and 106 microns. Thus

theoretically the radial clearance could vary more than 16 microns. If each micron

radial clearance added to nominal radial clearance of 90 microns will reduce the film

thickness by 1% (Chiu and Kay, 1974), it may compound the problem. Thus the

maximum variation in minimum oil film thickness can be reduced by 16% (2.5

microns) of the required minimum oil film thickness (16 microns) to 13.5 microns

which is approximately 84% of the required value.

Figure 3.8 Talyrond 100

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When ID and OD of the test specimen were measured the measurements were taken

at 10 locations along the bearing circumference (5 at one end and 5 on the other) at

an interval of 36 degrees on either side covering the whole circumference. The main

focus was on the bearing ID measurements using four different instruments i.e.

vernier calliper, Sigmascope, Hole-test-gauge and Metroscope. OD of the shaft

sleeve was measured with the help of HP Laser system only.

The variations in ID measurements at different locations were observed more than

the tolerance limits. Even though the precision of each measuring device is known

the accuracy in measurement is not assured due to human errors in handling or

observing the readings. When diameters were measured on the same bearing sample

at different locations the variations in a bearing’s radial clearance were found to be

780, 760 and 25 microns respectively for these methods. These measurements

recorded at different locations along the bearing circumference of both ends are

shown in the Table 3.4. The highest and lowest values for each method have been

highlighted and an average value has been calculated for each measuring device. A

statistical analysis shown in Table 3.5 clearly states the superiority of ID

measurement with Metroscope (Figure 3.9) which works on the optical comparator

principle.

Figure 3.9 Metroscope for bearing ID measurements

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The results show that the vernier measurements are the poorest in terms of accuracy

and Sigmascope results are the poorest for repeatability. With the latter there is

significant subjectivity involved in focusing the lamp and positioning the cursor.

The gauge test proved to be a better instrument but the Metroscope gave the best

results with an accuracy of up to 5 microns. The results of bearing ID measurements

have been discussed as an example but a similar situation occurred with the

measurements of shaft sleeve OD also. The use of all the above devices was

unsatisfactory in measuring the OD of the shaft sleeve and the best results were

obtained with the HP Laser System. The errors and problems associated with the

metrology of radial clearance measurements have been discussed in a separate

publication (Sharma , 2004).

Exaggerated end-view of these measurements has been plotted in the form of radar

graphs (Figure 3.10a-3.10e). The graphs 3.10e is the exaggerated radar plot of ID and

OD of concentric bearing and shaft sleeve together and highlight the metrological

problem associated with the radial clearance measurements.

Table 3.4 Bearing ID measurements

Observation No.

Vernier calliper

Sigmascope Hole-test- gauge

Metroscope

1 39.90 39.948 40.015 40.005 2 40.01 39.974 40.000 40.000 3 40.00 39.951 40.005 40.002 4 39.95 39.956 40.005 40.005 5 39.96 40.000 39.990 40.000 6 40.02 39.985 39.990 40.005 7 40.03 40.005 40.010 40.002 8 40.02 40.008 40.010 40.002 9 40.66 39.282 39.966 40.004 10 39.88 39.246 39.962 40.000 Average 39.986 39.9783 40.0031 40.0026

Figure 3.10e shows that there may be instances during the complete rotation of the

shaft when there is almost zero radial clearance in the bearing. As the film thickness

is the distance between the average lines of the roughness of the two mating surfaces,

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the actual film thickness may frequently result in mixed lubrication, or boundary

lubrication regimes during each revolution of the shaft sleeve.

Table 3.5 Bearing ID measurements: statistical analysis

Instrument Standard Deviation

Median Mean

Vernier 0.222962 40.005 40.043 Sigmascope 0.302116 39.965 39.8355 Hole-test-guage 0.018421 40.0025 39.9953 Metroscope 0.002121 40.002 40.0025

3.7.3.1 Metrological issues

This study raises some serious issues pertaining to the radial clearance of the bearing.

It can be concluded from this study that the accuracy in radial clearance

measurement can be achieved by choosing the right instrument and precision

manufacturing process. No matter how accurate the measuring device is the diameter

of the bearing and shaft sleeve varies from one location to the other along the

circumference as well as along the bearing length. The out-of -roundness and

roughness varies from one location to the other and so too the diameters. This is

mainly due to limited control over the manufacturing process. The poor measuring

practice can cause a serious deficiency, if the error in measurement is of the same

order as operating minimum oil film thickness.

The current standard practice of choosing the average value for the diameter does not

guarantee that a desired oil film thickness is obtained at every instant through out the

bearing length. Designers should allow for these problems and researchers should be

pedantic in ensuring that they are dealing with actual dimensions (not specifications)

and thereby producing reliable research results.

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Figure 3.10a Bearing ID profile by Vernier measurements

Figure 3.10b Bearing ID profile by Sigmascope

End view Vernier profile

39.739.839.9

40

12

34

5

6

7

89

1011

1213

14

15

16

17

18 19

20

End view Sigmascope profile

38.5

39

39.5

40

40.51

23

4

5

6

7

8

910

1112

13 14

15

16

17

18 19

20

Series1

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End view profile hole test guage

39.9239.9439.9639.98

40

12

3

4

5

6

7

8

910

1112

13

14

15

16

17

18

1920

Series1

Figure 3.10c Bearing ID profile by Hole-test-gauge

End view Metroscope

39.99639.998

4040.00240.004

12

3

4

5

6

7

8

910

1112

13

14

15

16

17

18

1920

Series1

Figure 3.10d Bearing ID profile by Metroscope

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Sleeve OD and bearing ID plot

3838.5

3939.5

4040.5

1

2

3

4

5

6

7

8

9

10

HP-laser data

metroscope data

Figure 3.10e Concentric bearing and shaft sleeve diameter graphs

Given the foregoing discussions it was difficult to select a single value for diameter.

The diameters were measured with Metroscope for the bearing ID and the HP laser

system for the shaft sleeve OD. Diameter was measured at different positions along

the bearing and shaft sleeve length and at equally spaced angular positions. Average

values were taken as the mean diameter. Both methods gave precision up to five

microns. A combined plot of Bearing ID data obtained from Metroscope and shaft

sleeve OD data obtained from HP laser system has been plotted and is shown in

Figure 3.10e. The plot indicates that under normal circumstances there are instances

where bearing radial clearance is almost zero.

The purpose of plotting these exaggerated profiles is to highlight the metrological

problems associated with bearings and the resulting impact on oil film thickness at

the contact.

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3.7.3.2 Some observations about radial clearance measurements

Measurement of radial clearance is a key factor in this research, therefore, it is

imperative to measure the bearing ID and shaft sleeve OD with confidence.

However, the following aspects of radial clearance measurement need further

attention:

• The radius of the bearing varies along the circumference of the bearing,

leading to variations in the radial clearance.

• Accuracy in measuring the radial clearance depends upon the metrological

procedure and the precision of the measuring instrument.

• Specifying the radial clearance as the average of various measurements taken

along the circumference is not adequate.

• Due to out of roundness, the radial clearance of a bearing varies along the

circumference, as well as along the bearing length.

• Just as cut-off length is specified in measuring surface roughness, similarly,

out-of-roundness must be specified when radial clearance is reported.

• The rule of thumb that specific film thickness or lambda ratio 10 is adequate

for designing hydrodynamic journal bearings, needs to be reviewed in view

of change in bearing ID along its circumference

3.7.4 Gamma ratio for film thickness measurement

The out-of-roundness values recorded before the wear tests show that these are

higher as compared to surface roughness values. This indicates the bearing design

parameter called film parameter or lambda ratio need to be reviewed to ensure

adequate separation of the bearing surfaces during lubrication. Pursuing this matter

further a new parameter has been proposed.

3.7.4.1 Significance of film parameter

The film parameter popularly known as lambda ratio or specific film thickness is the

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ratio between the oil film thickness and composite roughness of the two lubricated

surfaces, as shown in figures 3.11a and 3.11 b.

Where h is the oil film thickness and σ1 and σ2 are the rms values of roughness of

surfaces 1 and 2 respectively. It is important to note here that the film thickness ‘h’ is

the distance between the mean lines. Figure 311a shows an exaggerated view of this

concept. Alternatively, Figure 13.11b shows a simple sketch of rms values.

Figure 3.11a Oil film thickness between the surfaces

Figure 3.11b Oil film thickness based on composite roughness

The ratio of film thickness h, and the composite roughness of the two surfaces is

known as the film parameter, lambda ratio or specific film thickness. It can be

represented through Equation 3.1, where σ1 and σ2 are the rms roughness values of

surfaces 1 and 2 respectively.

h

σ1

σ2

h

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⎟⎠⎞⎜

⎝⎛ +

=22

21 σσ

λ h (3.1)

Where: composite roughness ( )22

21 σσσ +=comp

The lambda ratio is a direct indicator of lubrication regime in which a bearing is

operating. The lowest value of lambda occurs in boundary lubrication (λ<1) and

maximum value occurs in hydrodynamic lubrication (λ >10). Bearing designers aim

to achieve lambda ratio close to 10 for hydrodynamic bearings. This ensures

adequate separation of the two surfaces, and thus, minimum frictional losses.

In this experimental study a dichotomy has arisen in specifying the micro-geometry

tolerance values. The variation in bearing ID along the circumference raised doubts,

if the surfaces in a lubricated contact will be adequately separated. While a

roughness based lambda ratio is commonly used, it seems that an out-of-roundness

based ratio would be more appropriate.

3.7.4.2 Film Shape Factor (FSF)

If out-of-roundness value of the bearing element is higher than the roughness values,

the chosen value of lambda ratio does not ensure the separation of the surfaces as

assumed. Therefore, a new parameter –called Film Shape Factor (FSF), or gamma (γ)

ratio– has been proposed, to make the bearing micro-geometry measurements more

robust.

Before elaborating on the FSF, it is important to understand the reason for choosing

the lambda ratio equal to or greater than 10, for hydrodynamic bearings. This is done

to ensure that the surfaces are separated by at least 10 times the composite roughness

value. However, this fails to ensure adequate separation if the out-of-roundness value

is higher than the roughness value.

This study shows that the ‘localised radius’ changes along the circumference of a

bearing. The change in localised radius may be due to two reasons: firstly, due to the

local roughness excursions, and secondly due to the local out-of roundness –called

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localised roughness (σi) and localised out-of-roundness (Ori) respectively.

The current method of defining out-of-roundness is based on the ASME Y14.5 M-

1994 standard (Cho and Tu, 2001). This method specifies circularity tolerance based

on two extreme circle boundaries to confine the highest peak and lowest valley of a

roundness profile, as shown in Figure 3.12.

Figure 3.12 Film thickness based on composite out-of-roundness concept

Cho and Tu (2001) also analysed the profile variations within these two boundaries,

which are otherwise not being accounted far. In this research, these profile variations

have been called ‘localised out-of-roundness (Ori)’, which result in change of radius

from one location to another, as explained earlier.

In Figure 3.12 bearing and shaft sleeve have been referred by surfaces 1 and 2

respectively. The geometry of these two surfaces has been shown by two types of

circles i.e. outer extreme circles and inner extreme circles; where the mean circles

represent mean radii, similar to the mean lines for surface roughness. The

exaggerated out-of-roundness shape is drawn in between these two circles for both

the bearing elements with subscripts 1 and 2 respectively.

Figure 3.12 shows that areas where roughness values are higher than the out-of-

Extreme outer

/inner circle 1

σ2<Or2

Out-of-roundness profile 1

Out-of-roundness profile 1

Extreme inner/ outer circle 2

σ1>Or1

Mean circle 2

Mean circle 1

Film thickness

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roundness values (i.e. σ2> Or2), keeping lambda ratio = 10 ensures adequate

separation of the two surfaces. However, when out-of-roundness dominates the

surface roughness value (i.e. σ2<Or2), even though the lambda ratio is 10 the

separation of two surfaces is not adequate. The figure shows, if out-of-roundness

value is too high, then metal to metal contact can occur even with lambda = 10.

The gamma ratio (γ), or the FSF, based on the out-of-roundness values is defined as

in Equation 3.2.

( )22

21 OrOr

h

+=γ (3.2)

Where γ is the film shape factor (FSF), Or1 and Or2 the out-of-roundness of

two surfaces, and h is the film thickness.

Figure 3.13 shows simplified diagram for defining γ ratio, where film thickness h is

the radial distance between the mean radius of bearing and mean radius of the shaft

sleeve.

Figure 3.13 Film thickness based on out-of-roundness concept

Inner circle extreme surface 1

Mean circle, 1

Outer extreme circle,1

Outer extreme circle 2

mean circle 2

Film thickness

Inner extreme circle 2

Inner extreme circle 1

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Table 3.6 Roughness and out-of-roundness data of test bearings

Tests σb σs σcomp

hhdl = λ (10) x σcomp

Orb Hhdl = γ (10)

x Orb Hhdl / hhdl

A1 1.62 0.525 1.70 17.0 3 30 1.76A2 1.29 0.525 1.39 13.9 4.7 47 3.38A3 0.91 1.1375 1.46 14.6 4.6 46 3.15A4 0.39 0.725 0.82 8.2 14.3 143 17.43A5 1.19 0.625 1.34 13.4 6.8 68 5.07A6 1.36 0.4875 1.44 14.4 3.6 36 2.5A7 1.43 0.4375 1.50 15.0 10.06 100.6 6.7

Notes 1: All film thickness and rms roughness measurement are in microns 2: Shaft sleeve is presumed to be perfectly round (σs=0)

Table 3.6 shows the roughness and out-of-roundness data for the test bearings. In this

table, the values of bearing roughness as well as shaft sleeve roughness have been

converted to rms values (σb) and (σs), and from these values, the composite

roughness (σcomp) was calculated. Multiplying composite roughness by 10 gave the

required oil film thickness (hhdl) value, which is based on lambda ratio = 10.

The measured out-of-roundness values (Orb) for all the bearing elements are higher

than those for the respective composite roughness values (σcomp ). The Hhdl film

thickness values are calculated as 10 times the out-of-roundness values (Orb),

ensuring that the surfaces are adequately separated. To make the process simple the

shaft sleeves are presumed to be perfectly circular i.e. σs = 0.

The last column shows that Hhdl (the film thickness calculated from the out-of-

roundness) is a significant multiple of hhdl (the film thickness calculated from

roughness). Thus, if a bearing was designed for lambda ratio (λ) = 10, then the

resultant film thickness could be 17 times smaller than that required, as shown for

Test A4. Thus, a bearing designed with gamma (γ) = 10 is much safer than that

designed for lambda (λ) =10. This effect is exaggerated in dusty environments, and

therefore, the need for considering this newly proposed gamma ratio is even more

important for such applications.

The application of Film Shape Factor (or gamma ratio) can also be applied to flat

surface hydrodynamic thrust bearings, where surface waviness is higher than the

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roughness values. In these bearings, waviness of the flat surfaces at a cross section

can be treated as out-of-roundness.

3.7.5 Bearing Component Roughness

Surface roughness is not a direct measurement of wear but is good indicator of the

mode of wear. The pattern of wear and surface topography can reveal useful

information when the effect of surface finish on lubrication is considered. The

surface roughness of bearing elements changes with operation. The roughness and

their orientation have a direct influence on bearing performance, because it affects

the oil film thickness in the contact zone. Studies by Tonder [1986], Patir and Cheng

[1978], revealed that roughness in the transverse or axial direction helps to increase

the minimum oil film thickness. Since thicker oil film indicates the higher load

carrying capacity, increase in the roughness value in transverse direction is useful in

carrying the higher loads for the same bearing design parameters. Similarly there is

evidence to show that circumferential roughness promotes the flow of fluid, thus

reducing the film thickness. However, it has been found that the frictional losses in

such bearings are lower compared to the transverse roughness case. Thus the average

roughness values of the bearing and shaft sleeve surfaces were measured in the

circumferential and transverse directions before and after the tests. The

measurements were taken on a Taylor Hobson’s Surtronic 3+ profilometer. The

equipment recorded several other roughness related parameters. The results obtained

will be discussed in the following chapter. The major problem associated with these

measurements was that the roughness varied drastically from one location to the

other within the contact zone. The areas of interest for roughness measurements were

identified either visually or through a microscope. The reported surface roughness

values are an average of three or more measurements within the wear zone.

3.7.6 Maximum Wear Depth

Every test performed in the presence of solid contaminants demonstrated that there is

discernable wear in the bearing and there was a shaft imprint on the bearing at the

contact zone. This wear area was visible with the naked eye. The maximum depth of

wear varied from one test condition to another depending upon the antiwear additive.

Direct measurement of the depth of these worn patterns was not possible and so

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the out of roundness profiles for each bearing were obtained. Wear depth was

determined by recording the change in geometry. Although this is not a standard

method used by researchers for wear measurements, a comparison with other

measured wear parameters showed that the method is as reliable as many others.

3.7.7 Particle Counts in Oil Sample

Wear debris analysis and particle counting are well known condition monitoring

techniques. The solid contaminants ingress in the lubricating oils is unavoidable.

Starting from the stage of manufacturing, packaging and handling and usage in the

machines the particles from the environment or generated within the bearing harm

the bearing. The size of these particles may vary depending upon the sources and

this may change due to entrapment within the bearing surfaces and by further

crushing action. A Quant-Alert system shown in Figure 3.14 was used to measure the

number of particles of different size ranges present in the oil sample

The Quant Alert measures the number of particles present in the oil sample of 10 ml.

It works on pressure drop/flow principle. The equipment categorises particles in

eight different groups. The size groups selected for this study were: particles >5, >10,

>15, >20, >40, > 50, >75 and >100 micron. The change in particle number was

recorded by counting the particles at these sizes in the sample of pure base oil, oil

containing 4g/l Al2O3 before the test and then after the test. The number of particles

generated within the bearing depends upon the influence of the respective additives,

the change in motion of the particles within the contact and crushing of the particles

under the influence of each antiwear additive.

3.7.8 Minimum Oil Film Thickness Measurement

An optimum oil film thickness in the bearing contact is the key to successful bearing

performance. Film thickness is a very sensitive parameter especially when the

bearing is operating with small minimum oil film thickness and the accuracy in

measurements is of prime importance. An error of a few microns in calculations or

measurements can cause the bearing to run in boundary or mixed lubrication regime.

There are several conventional methods for measurement of oil film thickness such

as; sensors/transducers based on capacitance or eddy current, X-Ray, shock pulse,

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optical and voltage discharge methods. The influence of wear due to contaminants

treated with antiwear additives resulted in change of micro-geometry of the bearing

which reduced the minimum oil film thickness in conjunction with the physical

obstruction of the oil flow at the bearing inlet. This was examined by recording the

change in minimum oil film thickness in the bearing contact at three stages during

the test i.e. at the beginning at the middle and at the end of the test with the help of

eddy current type proximity probes.

Figure 3.14 Quant Alert

3.7.8.1 Film thickness Measurement by proximity probes

Proximity probes were chosen for measuring the film thickness. They work on eddy

current principle where intensity of the current between the tip of the probe and the

target material relates to the distance between them. These are recommended to be

used in pairs at a time mounted at right angle to each other on the bearing housing.

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85

These probes are said to be capable of measuring film thickness with an accuracy of

half a micron.

At no load the shaft and bearing are theoretically concentric. The probes measure the

distance between their tip and the nearest surface of the shaft in two perpendicular

directions. The eccentricity in the bearing was measured in two steps. First the

distances between the tip of the probe and the shaft sleeve were measured when

operating and theoretical concentricity. Later the bearing was run with a known load

and speed, and the distances between the tip and the shaft sleeve surface were

measured again. The distances measured by these two probes were treated as

coordinates of an imaginary point in space and measurements at no load and full load

conditions were treated as the change in coordinates of the point in space. The

displacement of the points in space can be calculated by knowing the change in

coordinates of these points. In a bearing, whose shaft is fixed and the bearing is

floating, if (X1, Y1) are the coordinates of the centre measured from the origin of a

fixed reference frame at no load and (X2,Y2 ) are the coordinates of the centre of the

bearing after the load is applied, the bearing eccentricity ‘e’ can be expressed as:

( )212

221 )()( YYXXe −+−= (3.3)

The minimum oil film thickness is the difference between the radial clearance and

the eccentricity, and can be expressed as:

eCh −=min (3.4)

It should be noted that in this experimental set-up the proximity probes were fixed on

the bearing, which is floating with respect to shaft, and hence the reference frame is

not fixed. Thus, the eccentricity cannot be measured directly by using Equation 3.3.

Ideally, at no load the gap between the shaft and bearing surface is supposed to be

equal to radial clearance ‘C’. But in reality the bearing was not concentric due to its

own weight (25 N).

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Calculate, program constants

Set P(i,j) = 0

Calculate h(i,j) add WD(i)

Solve Reynolds Equation (finite difference form)

Set boundary conditions

Calculate P (i,j)’s & SPN

Set SPO = SPN

Assume ε and Φ

2

Calculate in finite difference

Is SPN -SPO .LT. 0.001

YES

1

3

Continued on next page

Input data

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87

Figure 3.15 Flow chart

Calculate WX, ,WY & Φ

Is Wcal < W app.

YES

Print P(i,j), h(i,j), Φ,ψ

2

Calculate ψ

END

Is ψ < φ

YES NO

3

Continued from the previous page

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88

Efforts were made to estimate this eccentricity ‘eo’ at no load and corresponding H0

using ESDU charts, but due to small bearing load it could not be determined with

sufficient accuracy. To improve the accuracy, value of eo was determined by

developing a program for this research, based on algorithm used by Pai and

Mazumdar (1992). In this case an error in measuring the eccentricity eo due to

change in viscosity was ignored, because the load is too small (25N). The flow chart

of the program developed in Fortran language is shown in Figure 3.15, and the

Fortran code in Appendix B. The film thickness predicted by this program and the

experimental results were also compared with the standard ESDU software. This

software package is developed by the ESDU, and is used for predicting journal

bearing performance for known input parameters for normal lubricated conditions.

The results of this program, for selected test cases are shown in Appendix C.

The actual load in bearings at so called “no load” condition is not zero because

bearings have their own weight, and hence the minimum oil film thickness hmin at no

load is also not equal to the radial clearance 'C'. The value of the film thickness at no

load condition reduces by an amount 'eo' which is the eccentricity created by the self

weight of the bearing. Thus amount 'eo' needs to be subtracted from all hmin values

measured experimentally. The steps followed for the measurements of film thickness

by proximity probes are given as below:

• Calibrate the probes

• Measure the radial clearance as accurately as possible.

• Calculate theoretically the value of hmin using the Fortran Program (will be

discussed later) for given operating parameters at self-weight of bearing (25

N) and speed 1420rpm (the reference experimental hmin for no load

condition).

• Measure the displacement from both the probes for no load conditions and

treat them like coordinates of an imaginary point in space. Since hmin is the

difference between radial clearance and eccentricity eo, the value needs to be

subtracted from each hmin value measured for operating conditions other than

no load conditions.

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• Measure the coordinates for operating load and speed condition and calculate

the displacement between the imaginary points and calculate the film

thickness. The actual oil film thickness is smaller by an amount ‘eo’ as

determined in the previous step.

After completing the experiments using the above methodology, it was realised that

the calculations of film thickness were not straight forward. The proximity probes

were mounted on the floating bearing housing. Thus, the reference coordinates at no

load cannot be used as the reference point for measuring the shaft sleeve

displacement. Though the measurement error was not large and would have been

acceptable if measuring thick oil films; further improvement was considered

desirable, as film thickness under study is small. Investigations revealed that a key

phaser device could have been used to accurately map the change in coordinates of

the bearing with change in operating conditions, but that was too late. In order to

avoid repetition of the experiments a trigonometric solution was developed to solve

this problem which is explained in the following sections.

3.7.8.2 Calibration of Proximity Probes

Proximity probes REBAM 300 were chosen for film thickness measurements. These

probes with scale factor 40V/mm were found to be suitable for measuring thin films.

The probes were recalibrated to confirm their efficacy in the actual environment.

Change in output was measured by moving the target material (shaft sleeve) against

the probe tip with controlled displacements in micron steps. The change in mV

output was recorded against the displacement. In experimental set-up the probes

were mounted in a steel housing and tip passing through a hole in the bronze bearing

and there was oil in the gap between the probe tip and shaft sleeve. This required a

fixture where probe passed through a hole in the bronze bearing and the space

between the tip of the probe and shaft sleeve surface was filled with oil.

The mV out put was recorded for 180 micron gap equivalent to diametral clearance

of the bearing which could not be achieved successfully because the shaft sleeve

inside the bearing could not be held perfectly square. In Figure 3.16a the calibration

fixture of a half cut bearing is shown which was used for calibration to achieve

perfect squareness. A full calibration set-up is shown for the proximity probes in

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90

Figure 3.16b; the probes were mounted on a stationary frame and a half piece of

bronze bearing was mounted on another stationary plate such that the probe passes

freely through the hole in the bearing.

The shaft sleeve was mounted on a micro-displacement table and was moved in steps

with the micro displacement controller against the probe tip. As shown in the Figure

3.16b the probes are connected to a proximeter with an extension lead of two metre

lengths which gives eddy current output in mV. It requires input power voltage 18-24

V. In this experimental study 24 V input was used throughout to get a stronger output

signal. The probes were calibrated under conditions as close as possible to the actual

experiments. To simulate the performance of the probe in the oil medium, an oil drop

was placed in between the probe tip and the shaft sleeve surface to simulate the probe

tip and the shaft sleeve surface covered with the oil film.

It was noticed that the calibration did not change due to the presence of lubricant.

However the bearing surrounding material affects the output depending upon

whether the bearing material is bronze or steel. It was also observed that the

calibration is linear only when the output voltage is more than 10V as recommended

by the manufacture.

Figure 3.16a Probe calibration fixture

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91

Figure 3.16b Calibration setup

Figure 3.17a Calibration chart of probe 1

This output can be achieved with the minimum 3mm gap between the probe tip and

the target. Hence before mounting the probes on the bearing housing for actual

measurements, it was kept in mind that the minimum gap between them is more

Calibration of REBAM 300 Proximity Probe1

0

20

40

60

80

100

120

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15

Output (mV)

disp

alce

men

t (m

icro

ns)

Series1

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92

than 3 mm or the output is more than 10V. The calibration graphs are shown in the

Figures 3.17 (a) and (b).

Figure 3.17b Calibration chart of probe -2

3.8 Trigonometric Solution of Film Thickness Measurement

The journal bearing test rig accommodates a fixed bearing and a rotating shaft

sleeve. The probes are mounted on the bearing housing, which floats with respect to

the shaft. Thus, the probes do not measure the displacements from a fixed reference

and hence, either an electronic device called key phaser be used else the Equation 3.3

requires geometrical corrections. A geometrical solution has been developed for

measuring the eccentricity of the bearing from the displacements recorded by two

proximity probes, as explained in the following paragraphs.

In Figure 3.18 two circles with centres S and B represent the shaft sleeve and bearing

with Rs and RB radii respectively – for a bearing operating at full speed and load.

The positions of the proximity probe tips mounted on the bearing housing are 90o

apart; these are represented by arrows ‘X’ and ‘Y’ in the figure. The probe ‘X’ is

located at 900 from the load direction of the bearing. Line of centre (LC) makes an

attitude angle ψ from load direction ‘W’. Bearing eccentricity is the distance between

Calibration graph REBAM 300 probe2

0

20

40

60

80

100

120

1 2 3 4 5 6 7 8 9 10 11 12 13 14

Output (mV)

disp

lace

men

t (m

icro

ns)

Series1

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93

the two centres, i.e S and B, and is represented by ‘e’.

The distance measured by probe X is XM, and that measured by probe Y is YN,

denoted as PX and PY respectively. The relationship between ‘e’ and displacements

measured by probes X and Y can be derived as follows:

RB = Bearing radius

Rs = Shaft sleeve radius

PX = Displacement measured with probe X

PY = Displacement measured with probe Y

Thus:

yb PRBN −=

xb PRMB −=

sRSMSN ==

Since probes are at right angle, Δ MNB is a right angle triangle and hence;

22 BNMBMN +=

Or

( ) 22 )( ybxb PRPRMN −+−=

Consider Δ MNB, Δ SMN, and Δ SNB where:

β=∠SNB , θ=∠MNB , φ=∠MNS

Thus: φθβ ∠−∠=∠

and: φθφθφθβ SinSinCosCosCosCos ..)( −=−=

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94

Figure 3.18 Geometrical representation of film thickness measurement

In Δ SNB, SN and BN are known. Thus:

MNPR

MNNBCos yb )( −

==θ

MNPR

MNMBSin xb )( −

==θ

Similarly considering Δ SMN;

sRMNCos.2

and

SNSPSin =φ or

s

s

R

MNRSin

22

2⎟⎠⎞

⎜⎝⎛−

C

S

X

PY

Px

β

Load

ψ

ø

θ

L

eB

M

N

Y

P

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95

By substituting the values of MN and cos β in the following equation the value of ‘e’

can be calculated as follows:

βCosBNSNBNSNe ...222 −+= (3.5)

After substituting all the values:

(3.6)

For calculating the value of hmin , Value of eccentricity ‘e’ can be substituted in

Equation 3.4, which was:

eCh −=min

Thus eccentricity can be calculated (in microns) by substituting the values of shaft

sleeve radius, bearing radius, and displacement recorded by probes X and Y in

equation 3.6. The displacement measured by probes is recorded in mV output which

can be converted to Px and Py respectively in microns by multiplying it by scale

factor of the probe, where 1 mV corresponds to a 25 micron displacement.

3.9 Test Procedure and Experiment Design

The purpose of the test was to run the bearing at a ‘K’ ratio ≤ 1 for a fixed sliding

distance. A total of seven tests were performed. The first test was performed with

base oil alone. After running the test for fixed sliding distance, the change in wear

parameters as well as oil film thickness was recorded. The second test was

performed with the base oil containing 4g/l contaminants. The changes in wear

parameters were recorded for the base oil and base oil mixed with contaminants tests,

and results were compared to find out the amount of wear caused due to

contaminants. The remaining tests were performed with five different antiwear

additives. The film thickness and wear parameters were recorded for each test

condition. Thus the influence of contaminants over the base oil was studied from the

first two sets of experiments and the performance results obtained from the

remaining five tests were used to determine the effect of an individual antiwear

( )( ) ⎥

⎢⎢

⎡ −+−−

⎪⎭

⎪⎬⎫

⎪⎩

⎪⎨⎧

−+−

−−

⎭⎬⎫

⎩⎨⎧ −

−−−+=s

ybxbs

ybxb

xb

s

ybybsYbS R

PRPRR

PRPRPR

RPR

PRRPRRe.4

)()((.

)()(2).(

).(.222

22

22

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96

additive. The wear results were compared to determine the efficacy of each antiwear

additive used in the tests.

Table 3.7 Operating parameters and experiment design

Lubricant/ Additive*

Radial Clearance C (μm)

eo(H0) (μm) No load1

Speed N (rpm)

Load W(N)

Duration t (s)

hmin (μm)

‘K’ Ratio

A1 (pure base oil)

80 2.8(77.2) 400

500 150 15.84 0.99

A2 (Al2O3) 82 3.0(79) 420 500 143 16.08 1.005

A3 89 3.8(85.2) 500 500 120 17.09 1.09

A4 80 2.8(77.2) 400 500 150 15.84 0.99

A5 89 3.8(85.2) 500 500 120 17.09 1.09

A6 89 3.8(85.2) 500 500 120 17.09 1.09

A7 80 2.8(77.2) 400 500 150 15.84 0.99

*The product names have been suppressed by randomised double blind trial testing to maintain the manufacturer’s confidentiality. 1. H0 is the film thickness measured at no load, but including the housing weight

Film thickness was recorded during the above seven test conditions. In most of the

cases the film thickness was recorded in the beginning, middle, and at the end of the

test. Minimum oil film thickness represented the tribological performance of the

bearing and revealed the lubrication status as well as its impact on the bearing life.

Table 3.7 gives an over view of the experiment design, it shows all important

operating and design parameters, such as radial clearance, actual ‘K’ ratio, load,

speed and duration of the tests.

3.10 Conclusion

An extensive literature search provided the required background for designing

experiments to meet the research aims and objectives. The experimental design and

micro-geometry metrological investigations reported in this chapter led to the

following conclusions:

• It was decided that the effect of 5 antiwear additives will be studied

on the wear of journal bearings lubricated with oil containing solid

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97

contaminants.

• It was also decided that the effect of change in micro-geometry on the

tribological performance of the bearing will be studied by measuring

the change in minimum oil film thickness as a combined effect of a)

change in micro-geometry due to wear, b) antiwear additives and c)

presence of contaminants in and around the bearing contact.

• Modifications to the exiting test rig were required to conduct the

required experiments.

• It was necessary to design and produce a bronze bearing with shaft

sleeve using the ESDU 84031 method.

• A Fortarn program was required for predicting the minimum oil film

thickness and bearing performance, to validate the experimental

results.

• The need to minimise the test duration and selecting most suitable

method for measuring wear in test bearings resulted in development

of a multi-wear parameter approach (MWPA). Whereby, wear

measurements methods or techniques were categorised in three main

groups: 1) weight loss, 2) change in micro-geometry and 3) change in

particle counts.

• Experimental design comprised of testing seven sets of bearings for

three lubricating conditions: 1) with pure base oil; 2) with oil

containing Al 2O3 contaminants; and 3) with contaminated oil treated

with five different antiwear additives. All test conditions were kept

the same ensuring that the ‘K’ ratio ≈ 1, and the sliding distance =

7536 m.

• The graphical representation of ID and OD data of the bearing and

shaft sleeve respectively indicated that the radial clearance in the

bearing was not constant when measured at different locations on the

circumference. Therefore, it is recommended that the out-of-

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98

roundness should always be specified along with the radial clearance

of a bearing.

• It was necessary to develop a geometrical method for measuring the

minimum oil film thickness with higher precision. Proximity probes

mounted on a floating bearing housing required the proposed

geometric correction.

• Designing hydrodynamic bearings with lambda ratio 10 was found to

be inadequate for bearings operating in hydrodynamic lubrication

regime, specially with out-of-roundness value more than the

roughness value, the proposed Film Shape Factor, (FSF or gamma

ratio) can be used as a more reliable design parameter.

• The concept of defining the Film Shape Factor (FSF) can also be

applied to flat surface hydrodynamic bearings, especially when the

waviness values are higher than the surface roughness values; this is

analogous to treating surface waviness similar to out-of-roundness.

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CHAPTER-4

4. EXPERIMENTAL RESULTS AND ANALYSIS

4.1 Overview

The purpose of the experimental analysis was three fold, 1) to find out the effect of

antiwear additives on the wear of the test bearings, 2) to compare the wear

measurement technique for their accuracy leading to selection of the best technique

to be used for characterisation of anti-wear additives and 3) to examine the effect of

change in micro-geometry on the tribological performance of the test bearings.

The experiments were conducted on seven bronze bearing and shaft sleeve sets. All

tests were performed for a fixed sliding distance 7536 m and fixed “K” ratio of 1. As

stated in the previous chapter, the bearings varied in radial clearance hence for the

same operating conditions the thickness of the oil film formed in the contact zone

would be different. A combination of load and speed was determined such that the

bearings operated at a minimum oil film thickness close to the size of the

contaminants these giving a ‘K’ ratio close to 1. Since all bearings had operated with

a small oil film thickness, the influence of self weight (including housing) of the

bearing had to be taken into account. To cite one of the test examples, a bearing

having radial clearance 80 microns, self weight of 50N and speed 1420 rpm, at no

load, gives eccentricity (eo) of 2.8 micron or correspondingly 77.2 microns minimum

oil film thickness. For a required minimum oil film thickness of 16 microns a hit and

miss method was used to choose a speed that gives desired ‘K’ ratio.

A combination of fixed 500N load and a speed 400 rpm gave a minimum oil film

thickness of 15.89 microns and hence a ‘K’ value equal to 0.99. It was decided to run

the test for a duration that would cause a measurable amount of wear in the bearing.

150 minute duration (equivalent to 7536 m sliding distance) gave adequate wear in

the bearing. The ‘K’ ratio and the sliding distance were kept the same for all seven

tests. The tests were labelled A1 to A7; A1: pure base oil and A2: base oil mixed

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100

with 4% (16-micron) Al2O3. The remaining five tests (A3 to A7) were performed

with contaminated oil (4% Al2O3), treated with five different antiwear additives.

Details of different tests (Test A1 to A7) are as follows:

A1- Base oil only

A2- Base oil mixed with contaminants (Al2O3 particles)

A3- Contaminants treated with commercial antiwear additive mixed with oil

A4- Contaminants treated with aryl phosphate group of additive mixed with oil

A5- Contaminants treated with Fuch’s proprietary additive mixed with oil

A6- Contaminants treated with sulphur/phosphorous group of additive mixed with oil

A7- Contaminants treated with isopropyl oleate, fatty acid and isopropyl ester group additive mixed with oil

The other conditions such as; base oil Solvent Neutral 300 with dynamic viscosity

0.042 Pa.s at 40 0C, solid contaminant; Al2O3 of size of 16-μm with concentration

4g/l, inlet temperature 40 0C and oil feed pressure of one bar were maintained the

same for all the test conditions. The sliding distance (7536 m) was also kept the

same for all the seven tests. However, to maintain the “K” ratio equal to one for

bearings with varied radial clearance the shaft speed requirements were different for

different sets of test bearings and hence the duration of the test to achieve the same

sliding distance changed from one test to another.

There were three main categories of wear tests in this experimental research viz.

weight loss, change in micro-geometry and change in particle count. Different wear

parameters and minimum oil film thickness in the bearing contact zone were

measured before and after the tests to examine the effect of the above additives on

the bearing performance. The need for measurements of different wear parameters

has been explained in the previous chapter through MWPA. These parameters were

recorded at the beginning and end of each test and change in their value gave a

measure of wear. Total 14 wear parameters were recorded for each set of test bearing

using MWPA, and these are listed as grouped below:

1. Weight loss in bearing (ΔWb)

2. Weight loss in shaft sleeve shaft (ΔWs )

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3. Change in bearing out-of-roundness (ΔORb)

4. Change in bearing radial geometry (ΔODs, ΔIDs, ΔC )

5. Change in bearing and shaft sleeve roughness in transverse as well as in

circumferential directions (Δ Rb, ΔRbt, ΔRs, ΔRst )

6. Change in wear particle counts and change in weight of wear debris

generated (ΔPC, ΔPcg)

7. Maximum wear depth in bearing contact (ΔWD)

8. Change in minimum oil film thickness (Δhmin)

The above parameters were recorded before and after the tests and the change in their

values gave the wear in the test bearings. The initial values or values before the tests

of relevant MWPA parameters are given in Table 4.1.

Table 4.1 Initial measurements before the tests

Tests Contaminants treated with additives

Wear Parameters

Base oil only A1

Al2O3 in Oil A2

A3 A4 A5 A6 A7

Wb (gm) 333.72 333.71 330.14 333.25 341.01 340.22 340.41Ws (gm) 178.52 178.51 178.60 178.80 179.71 181.43 181.30ORb (μm) 3.0 4.7 4.6 14.3 6.8 3.6 10.6 ODs (μm) 39.799 39.801 39.796 39.792 39.847 39.842 39.842IDb (μm) 39.959 39.965 39.969 39.953 40.025 40.020 40.001C (μm) 80.0 82.0 86.0 80.0 89.0 89.0 80.0 Rb (μm) 1.22 0.965 0.69 0.30 0.90 1.03 1.08 Rbt (μm) 1.25 0.94 0.53 0.27 1.03 0.99 0.64 Rs (μm) 0.42 0.42 0.91 0.58 0.50 0.39 0.35 Rst (μm) 0.36 0.3 0.525 0.38 0.47 0.28 0.40 PC*(count/ml) 9 340 227 226 305 255 287 Pcg (g/l) 0.036 5.513 5.38 5.59 5.22 5.8 5.4 Hxps (μm) 17.86 17.24 18.28 14.76 15.62 15.60 14.90 WD (μm) 0.0 0.0 0.0 0.0 0.0 0.0 0.0

*After mixing Al2 O3 powder of 15 micron size in all the oil samples except A1

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Amongst these parameters the minimum oil film thickness was considered to be the

key bearing performance parameter and was recorded at three intervals during the

test; at the start, midway and at the end of each test. The oil film thickness was

measured using proximity probes and compared for three test conditions i.e. before

adding any contaminants or additives, after adding contaminants and after treatment

with different antiwear additives. The oil film thickness measured before adding the

contaminants represents the performance under standard operating conditions;

measurements after adding the contaminants indicate the adverse effect of

contaminants; measurements after adding an antiwear additive represents the

influence of individual additives on performance. Thus an additive was evaluated in

terms of longevity of the bearing and performance as related to oil film forming

capacity. Changes in oil film thickness were observed during the test by recording

measurements at the start of the test (Hxps), in the middle (Hxpm) and at the end of the

test (Hxpe).

Surface micrographs of some worn bearings and shaft sleeves were also prepared.

These micrographs helped in analysing the wear mode, wear severity and metal

transfer between bearing and shaft sleeve surfaces.

Particle counts were obtained using QuantAlert apparatus to examine the changes in

the number of particles present in the oil. The source of these particles could be

different such as; generated wear debris, added contaminants or broken particles

during the test. The results were obtained by subtracting initial values from the final

values (after the tests values) of different wear parameters obtained from various

measurement techniques. These results, as a change in wear parameters are reported

Table 4.2 and discussed further for their relevance to this research.

The multi-wear parameter method (MWPA) was useful in saving considerable amount of

testing time, and also in comparing the wear measuring methods for their precision as well as

the reliability of results.

The MWPA methodology will be expounded in the following sections.

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103

Table 4.2 Experimental results

Test Wear Parameters

A1 (Base oil)

A2 (Al2O3)

A3 A4 A5 A6 A7

ΔWb (g) 0.01 0.25 0.15 0.17 0.15 0.08 -0.09 ΔWs (g) 0.01 0.125 0.03 0.07 0.07 -0.02 0.05 ΔORb (μm) 1.7 31.3 14.3 25.00 16.4 6.6 11.8 ΔODs (μm) -1 15 7 3 4 1 -1 ΔIDb (μm) 2 37 28 39 32 10 16 ΔC (μm) 1 26 17.5 21 18 5.5 7.5 Δ Rb (μm) -0.25 0.2 0 0.63 -0.15 -0.42 -0.48 ΔRbt (μm) -0.290 0.005 0.16 0.41 -0.37 -0.21 -0.26 ΔRs (μm) -0.09 0.11 -0.11 0.13 -0.09 0.05 -0.01 ΔRst (μm) -0.06 0.05 0.08 -0.03 -0.05 0.1 -0.04 ΔPC*

(count/ml) 21 1008 181 318 337 174 257 ΔPcg (g/l) 0.3 1.35 0.72 1.2 0.95 0.3 0.6 ΔWDmax (μm) 1.66 42 29 42 36 12.5 20 Δhmin (μm) 0.0 10.9 4.1 5.8 5.15 3.8 3.8

*Change in 15 micron particle size counts only

4.2 Weight Loss

Weight loss is the directly measured wear parameter. The bearing and sleeve both

were worn during the tests and hence, the weight loss in bearing (ΔWb) and shaft

sleeve (ΔWs) were measured with an electronic balance, which gave an accuracy of

up to three decimal places of a gram. The weight loss results shown in Table 4.2 are

illustrated graphically in Figures 4.1.

Bearing weight loss

-0.2-0.1

00.10.20.3

A1 A2 A3 A4 A5 A6 A7

Tests

Wt.

loss

(mg)

w eight loss

Figure 4.1 Weight loss in bearings

Figure 4.1 shows that, the weight loss in the bearing lubricated with base oil only

(Test A1) was very low and almost insignificant in comparison to others. It would

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104

be expected that a bearing operating under full fluid film conditions would not incur

wear except during the starting and stopping. The bearing weight loss was a

maximum at 0.25g for Test A2 which was expected due to presence of solid

contaminants and no antiwear additive.

Figure 4.2a a shows a micrograph of test bearing used in Test A2 after the test. In

this micrograph embedding of particles is clearly visible. The weight loss and

embedding occurring simultaneously in the bearing indicate that the rate of wear in

the bearing might have been changed after the embedding.

Figure 4.2a After Test A2 bearing surface (X50)

The effect of additive used in test A7 showed a weight gain of 0.09g. This weight

gain may be attributed to embedded particles in the bearing surface, as evident from

micrographs of the test bearing A7 shown in Figure 4.2a and 4.2b. Figure 4.2b shows

Al2O3, and steel particles embedded in the bearing surface. As evident from the bar

chart, this is the only test where weight gain was recorded. Minimum weight loss of

0.08 g was observed in Test A6. The weight loss results of Test A6 show that the

additive with Sulphur and Phosphorus (S and P) technology was more effective than

others.

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Figure 4.2b Micrograph of bearing surface after Test A7 (X100)

Sleeve weight loss

-0.050

0.050.1

0.15

A1 A2 A3 A4 A5 A6 A7

Tests

wei

ght l

oss

(mg)

w eight loss

Figure 4.3 Weight loss in shaft sleeves

The weight loss in shaft sleeves is shown in Figure 4.3. The loss varied from 0.01 g

in the case of pure base oil (A1) without any contaminant to maximum 0.12 g in the

case of Al2O3 (A2). In Test A7 the ester based additive caused weight loss of the

shaft sleeve of 0.05g. Minimum shaft sleeve wear of 0.03g was observed in Test

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A3. Additive A4 and A5 showed similar antiwear performance with weight loss of

0.07g and proved to be less effective in the case of shaft sleeve wear. Shaft sleeve

wear loss in Test A1 is too small and seems to be an observational error, whereas in

case of Test A6 the trend shows the weight gain of 0.02g which is very close to

experimental error. It concludes that the wear in this case was minimal and S-P

technology based additive proved to be the best performer. It may also be possible

that the shaft sleeve in Test A7 was worn more compared to other tests because the

particles embedded in the bearing acted as cutting tools for the matching shaft sleeve.

Micrographs (figures 4.2a and 4.2b) clearly show an evidence of embedding of small

wear particles on the bearing surface which excludes the possibility of cutting action.

Similar micrographs have also been obtained (Appendix D) for selected test

bearings. Micrographs of other tests bearings indicate that there was a severe

abrasive wear and some signs of cutting wear in case of Test A2 and Test A6.

Cutting action can also be seen in sleeves of Test A5 and A6 and bearings of Test A5

and A6.

The weight gain in Test A7 needs more support to prove the claim and hence the

surface micrographs of these baring surfaces were examined as shown in Figures

4.2a and 4.2b and were compared with the micrographs of other test bearings. The

Other micrographs clearly show the marks of abrasive wear –indicating weight loss,

and also the signs of metal transfer due to embedding of particles –leading to weight

gain. However, none of these micrographs give any evidence that weight gain due to

embedding of particles (weight gain) is more than the weight loss due to wear. Hence

there is a need for further support to claim the weight gain in the test bearing.

4.3. Out-of-roundness

Out-of-roundness (OR) was considered to be a sensitive micro-geometry parameter

and a superior wear indicator than any other wear parameter. To save the time, it was

decided that the out-of-roundness will be measured for test bearings only. The shaft

sleeves are rotating elements of the test bearings, and hence the change in their out-

of-roundness due to wear is not significant as compared to bearings.

The results of change in out-of-roundness (ΔORb) as recorded in Table 4.2 have been

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represented graphically in Figure 4.4. To illustrate the process of determining the

change in out-of-roundness (ΔORb) various graphs obtained from the Talyrond for

Test A2 and A6 are shown in Figures 4.5a to 4.5f. The out-of-roundness of the test

bearings was recorded at three fixed locations: at the top end, middle and bottom end

of the test bearing. The out-of-roundness of a bearing is the average of these three

readings.

Change in out-of-roundness of bearing

010203040

A1 A2 A3 A4 A5 A6 A7

Tests

Cha

nge

in o

ut o

f ro

undn

ess

(mic

rons

)

out-of-roundness

Figure 4.4 Change in out-of-roundness of bearings

It should be noted that the shape of the out-of-roundness graph is not the true

representation of the bearing geometry. The graph represents the amplified

excursions from the nominal circumference. In other words two points diagonally

opposite to each other on the out-of-roundness trace do not represent the diameter of

the circle. It depends upon choosing the position of the trace point on the graph paper

from the centre of the chart. The shape of out-of-roundness graph at one cross-

section may look entirely different by choosing different tracer positions and

magnifications. Magnification of the graph can be adjusted and it also depends upon

the type of transducer arm length.

The actual out-of–roundness is calculated with the help of a monograph. One should

not conclude from these traces that their out-of-roundness has changed with change

in magnification or tracer position. However, the foot print of the wear area in the

bearing can be clearly identified from the graph as the excursions in the region of the

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108

wear. These excursions are in general much larger than the normal out-of-roundness

trace of the rest of the periphery. Similarly position of a transducer can also alter the

shape of the out-of-roundness graph. Normally wear in a bearing appears concave in

the trace. A convex or inverted out-of roundness graph of a bearing was also

obtained (Figure 4.5h).

The reverse trace can be obtained by mounting the transducer in the reverse

direction. To demonstrate the procedure adopted for measuring the out-of-roundness

and the results obtained for the best and the worst case of wear have been discussed

through Talyrond graphs shown in Figures 4.5a to Figure 4.5h. The worst case of

wear is Test A2 where contaminants were used without any additive and the value of

out-of-roundness was 31 microns. The best results were obtained with S-P additive

used in Test A6, where out-of-roundness changed by 6.6 microns only. The change

in out-of-roundness of the bearing used in Test A4 was close to Test A2 with a

change of 25 microns and hence the additive performance was of the lowest order in

comparison to other additives.

Minimum wear occurred in Test A1, where base oil was used and no contaminant or

additive was present in the oil. As expected, there was hardly any change in

roundness of the test bearing lubricated with base oil only. Additives, A3 and A5

results were comparable at 14.3 microns and 16.54 microns respectively.

Performance of ester based additive used in A7 resulted in a change of 11.8 microns,

which is almost two times higher than the Test A6 bearing –10.2 microns.

The micrographs showed that embedding as well as normal wear took place

simultaneously in almost all the test bearings and hence the weight gain in Test A7

cannot be justified with the higher value of change in out-of–roundness. Thus the

out-of-roundness test results do not support the weight gain in Test A7, and hence the

weight gain appears to be an experimental error.

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Figure 4.5a Bottom end out-of-roundness before Test A2

Figure 4.5b Bottom end out-of-roundness (convex graph) after Test A2

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Figure 4.5c Top end out-of-roundness before Test A3

Figure 4.5d Middle position out-of-roundness before Test A6

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Figure 4.5e Bottom end out-of-roundness before Test A6

Figure 4.5f Top end out-of-roundness of bearing after Test A6

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Figure 4.5g Middle position out-of-roundness of bearing after Test A6

Figure 4.5h Bottom end out-of-roundness Test A6

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4.4 Radial Clearance

In the existing journal bearing test rig a 40 mm nominal bore journal bearing with

radial clearance of 90 microns was used. As discussed in the previous chapter, to

avoid the misalignment of the shaft the radial clearance (C) was chosen in the higher

range. However due to manufacturing limitations the bearings with exact dimensions

cannot be produced and hence the radial clearance varied from one test bearing to

another. Keeping in view this fact as well as the constraints associated with the

metrology of measurements, the problem was further investigated.

Figure 4.6 Shaft sleeve trace inside the bearing out-of-roundness trace

Shown in Figure 4.6 the out-of-roundness trace of shaft sleeve and bearing were

recorded on the same graph paper with the same magnification but tracer position

slightly shifted from one another. It should be noted that individually the out-of-

roundness of these elements is less than 2 microns which is well within the

acceptable limits. However, the graph clearly shows that the clearance between the

two surfaces is not uniform through their periphery when the bearing is stationery,

and it varies from one location to another. If this bearing is in motion the transient

values of radial clearance within the bearing may vary with time. This also highlights

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114

the problem of assigning a single value of radial clearance apart from the metrology

issues discussed in the previous chapter. The problem exaggerates when out-of-

roundness is larger. Traces in the figure clearly indicate that no matter how precise

the bearing and sleeve samples are, they are never perfect and assigning a single

value of radial clearance in a bearing with a high precision is not as simple as

thought to be.

Radial clearance has a direct influence on the load carrying capacity of bearings; i.e.

the film thickness in the bearing changes significantly with minor change in radial

clearance (Chu and Kay, 19740). The common practice of finding the radial

clearance is to measure the difference in nominal ID of the bearing and the nominal

OD of the shaft. It is presumed that this value of radial clearance holds well in a

running bearing along the line of centres which forms certain attitude angle from the

load line. However, the actual radial clearance which is the transient clearance is

time dependent and may depend upon the out-of-roundness at an instance at a fixed

location. The change in radial clearance (ΔC) was found by recording the radial

clearance before and after the test. The initial values were calculated from the

nominal ID and OD of the bearing and shaft sleeve respectively. The final values

were calculated from the maximum bearing ID measured in the worn surface area

(with hole-test-gauge) and shaft sleeve OD – measured with the HP laser system.

The results of change in radial clearance are shown in Figure 4.7. The figure shows

that the change in Test A6 was minimal with a value of 5.5 microns and was close to

the performance of additive used in Test A7 which had a an increase of 7.5 microns.

The performances of additives used in tests A3, A4 and A5 were of the same order of

magnitude with change in values 17.5 microns, 21microns and 18 microns

respectively. As anticipated with pure base oil in Test A1 a negligible change of 1

micron was recorded. In case of Test A2 with contaminants in absence of additive

treatment was recorded to the highest value of 26 microns. It may be noticed that in

Test A2 the change in radial clearance was not too high in comparison to Test A4

which performed poorly, and the change is only 21 microns. This may be due to

embedding of wear particles in the bearing surface of Test A2, which might have

reduced the successive rate of wear in the bearing.

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Change in radial clearance

0

10

20

30

A1 A2 A3 A4 A5 A6 A7

Tests

Cha

nge

in ra

dial

cl

eran

ce (m

icro

ns)

radial clerance

Figure 4.7 Change in radial clearance of bearings

The results also show that the change in radial clearance varied from one test bearing

to another depending upon the oil condition and the influence of their respective

antiwear additives. The change in radial clearance may occur due to dimensional

change in either bearing ID or shaft sleeve OD or both. In case of Test A5 the

increase in bearing ID was recorded 32 microns and a reduction of 4 microns in the

shaft sleeve ID, resulting in 18 micron change in radial clearance. Whereas, in Test

A2 bearing ID increased by 37 microns and the shaft sleeve OD reduced by 15

microns, correspondingly the change in radial clearance was 26 microns. Thus, in

this test, the contribution of change in bearing ID is significant in comparison to

other tests. It is also important to note that an additive influences the micro-geometry

of the bearing as well as of the shaft sleeve and its degree of influence differs from

one another.

Though, it is hard to determine the effect of an additive individually on both the

bearing elements, the data collected is represented graphically in Figure 4.8. It shows

the changes in ID and OD of test bearings and the shaft sleeve respectively. The

graph shows the absolute change in diameter of the bearing and the shaft sleeve,

where change in bearing ID means increase in its diameter and change in shaft sleeve

diameter corresponds to reduction in OD.

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116

Figure 4.8 shows that the bearings were worn more than the shaft sleeves. It also

shows that in Test A2 the shaft sleeve and the bearing both were worn significantly

and even in the absence of an antiwear additive the bearing was not worn as severely

as in case of Test A4, where antiwear additive was supposed to be effective. This

indicates that the metal transfer in the Test A2 bearing could have been effective at

the early stage, which retarded the wear rate after embedding of the wear particles in

the bearing surface. Phosphorus based additive used in Test A4 shows an increase in

bearing ID (39 microns) higher than Test A2, where no additive was used. The

reason for higher bearing wear in Test A4 could be opposite to Test A2, where

cutting action from the particles embedded on the shaft sleeve resulted in gauging of

the bearing.

Change in bearing geometry

-100

1020304050

A1 A2 A3 A4 A5 A6 A7

Tets

Cha

nge

in d

iam

eter

(m

icro

ns)

reduction in sleeve OD increase in bearing ID

Figure 4.8 Changes in bearing element geometry

This can be supported with the weight loss results of the shaft sleeve in Test A2,

which was higher (0.125 g) as compared to 0.07 g in Test A4. Unlike bearing, the

change in shaft sleeve OD of Test A4 was lower (by 4 microns) in comparison to 15

microns in Test A2. In Test A3, wear in bearing as well as in the shaft was higher in

comparison to Test A6 and A7 which is unexplained. In case of Test A6, the

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additive was most effective with the least change in ID and OD of the respective

bearing elements i.e. 1 micron and 10 microns respectively. A change of 1 micron in

shaft sleeve OD of Test A7 is so small that it can be treated as a variation in

measurement. Moreover, negative change or no change in shaft sleeve OD proves

that the weight gain in Test A7 bearing is not possible.

4.5 Change in Roughness

The literature survey revealed that the roughness of bearing elements affects the

formation of minimum oil film thickness at the contact zone. Minimum oil film

thickness in the bearing contact is the best indicator of its load carrying capacity. It is

common to think that ‘smooth is best’ but the orientation of roughness in a preferred

direction can help to develop thicker films. Transverse roughness helps to increase

the oil film thickness at the contact whereas rougher surfaces in the circumferential

direction increase the fluid flow through the contact and hence give thinner films, but

an easy passage for contaminants flow. Keeping in view this phenomenon,

roughness of bearings and shaft sleeves were recorded in both orientations. The

roughness was measured in both directions before and after the tests and respective

changes were recorded. The change was determined by subtracting the initial

roughness value from the final value (after the test). The negative change in surface

roughness means smoothening effect after the test and positive change shows the

opposite.

A number of surface topography parameters were used including Ra (arithmetic mean

height) Rq, (root mean square roughness) Rt, (maximum valley to peak excursion),

Bearing ratio (i.e. the percentage of the assessment at a level below the highest peak)

was also measured. The cut-off length of 0.8 mm was chosen for all the surface

roughness measurements and the surface roughness were measured as average

roughness or Ra values. The roughness of the bearing and sleeve surface varied from

one location to another and so the average values were recorded. Surtronic-3

instrument was used for the measurements, which averaged 5 scanned cut-off lengths

of 0.8 mm each (total 4 mm linear stroke) and gave Ra values in microns.

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Roughness measurements were taken at different locations on the bearing’s inner

surface and on the shaft sleeve’s outer surface –before the tests by choosing locations

randomly. It was often found difficult to select the location as a true representative of

the worn surface. Because, in test samples, some times the roughness within the

worn area varied drastically from one location to another. It is common to find a burr

or scuff mark in the worn area which is lot rougher than the normal worn area. Thus

abnormal roughness values did not make sense, and hence discarded to make a useful

analysis of the results. The measurement locations were chosen by visual judgment,

some times using a magnifying glass and the average of minimum three

measurements was considered to be the representative roughness of the bearing

elements in the worn area. It was not possible to record traces for all the

measurements, these were recorded randomly and hence Ra values of the traces

included in figures do not match with the reported average Ra values in the tables 4.1

and 4.2 and so in the bar charts. The roughness values recorded in the roughness

traces are as close to the reported average values as possible any value matching with

the average value is a coincidence.

4.5.1 Bearing roughness

Although the bearings were produced in lots by using the same manufacturing

process, their roughness varied from one test specimen to another. Table 4.1 shows

the initial roughness values of the entire lot of test specimen before the test. The

change in roughness value (Ra) was recorded by subtracting the before test

roughness value from the after test value. The negative values indicate that the

surface has smoothened. The changes in surface roughness of all the test bearings in

circumferential and transverse direction are presented in Table 4.2 and shown

graphically in Figure 4.9 (a) and (b).

Figure 4.9a shows that the bearing surface becomes smoother after operating with

base oil only (Test A1). This indicates that the start and stop conditions were helpful

for the running-in process in the bearings.

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Change in bearing roughness

-1

-0.5

0

0.5

A1 A2 A3 A4 A5 A6 A7

Tests

Cha

nge

in R

a va

lue

(mic

rons

)roughness

Figure 4.9a Change in bearing circumferential roughness

The change in the bearing Ra value -0.25 microns states that the surface has

smoothened from 1.22 microns to 0.97 microns. However in Test A2 with oil

containing 4g/litre of Al2O3, the roughness increased by 0.2 micron i.e. from 0.97

microns to 1.17 microns. In Test A4, the phosphate ester based additive gave the

worst results, where Ra value increased maximum from 0.27 to 0.4 microns in

comparison to all other cases including Test A2 where no additive was used. The

reason for increase in roughness is not well understood, however, it is anticipated

that the initial roughness of this bearing was very low (0.3 microns) and results in

Table 4.1 and 4.2 show that there is a trend that the bearings with lower initial

roughness were worn more. It is obvious that Test A4 additive had shown even

worse performance than the Test A2. The increase in roughness of test bearing A4 is

three times (0.63) higher than the Test A2 (0.2 microns Ra value). Test A7 showed

the best performance as the smoothening effect is maximum (-0.48 microns). Thus

Test A7 showed better smoothening than Test A6 which gave -0.42 micron Ra value.

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.

Change in bearing transverse roughness

-0.4-0.2

00.20.4

A1 A2 A3 A4 A5 A6 A7

Tests

Cha

nge

in b

earin

g tr

ansv

erse

Ra

(mic

rons

)

roughness

Figure 4.9b Change in bearing transverse roughness

Change in transverse roughness of the bearings is shown in Figure 4.9(b). In this case

also the results are some what similar to that of circumferential roughness. In this

case Test A2 bearing surface was even smoother in transverse direction than

circumferential direction that is from 0.2 to 0.005 micron Ra value. Test A4 results

again showed that the additive was not effective in reducing the roughness in either

direction. The influence of phosphate ester additive in Test A4 was adverse,

transverse surface roughness of the bearing changed from 0.27 to 0.68 micron Ra

value which is 150% higher than the initial Ra value, and these values are very high

as compared to Test A2. Test A6 did not show the best smoothening effect as

compare to other antiwear additives, but the additive was effective in reducing the

roughness in both the directions. Another surprising roughness result was obtained

for Test A3 where roughness has increased from 0.53 to 0.16. This shows that the

additive was more effective in reducing the roughness in circumferential direction

than the transverse direction and this additive was also not as effective in reducing

the roughness as pure contaminants in absence of any additive (Test A2). Test A1

results were consistent and showed slightly better smoothening effect. The

commercial additive used in Test A5 has maximum smoothening effect, reducing Ra

value by 36% from 1.03 to 0.66 microns. In case of transverse roughness

performance of additives used in Tests A6 and A7, their performance was close to

each other with change in Ra values to -0.21 and -0.26 respectively –approximately

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121

40% smoothening effect.

4.5.2 Shaft sleeve roughness

Changes in shaft sleeve circumferential and transverse roughness values are shown in

Figures 4.10a and 4.10b respectively.

Change in sleeve roughness

-0.15-0.1

-0.050

0.050.1

0.15

A1 A2 A3 A4 A5 A6 A7T est s

Cha

nge

in

roug

hnes

s (m

icro

ns)

roughness

Figure 4.10a Change in shaft sleeve circumferential roughness

In Test A1 (for base oil only) the circumferential roughness (Ra) of the shaft sleeve

changed from 0.42 to 0.33 microns, which is smoother by 0.09 microns. The

smoothening effect can also be seen in Tests A3, A5 and A7, with reduction in Ra

values to 0.11, 0.09 and 0.01 microns respectively. In case of Test A3 the bearing

was rougher than sleeves after the test. The shaft sleeve was smoother in transverse

direction; the effect was very prominent in comparison to other tests as change was -

0.0.11 micron Ra value. In Tests A5 again the shaft sleeve was highly smooth by -0.9

micron Ra value which of the same order as Test A5. In Test A7 the effect on the

shaft sleeve was smoothening but lowers than the bearing roughness this was close to

.0.01 micron which is with the measurement error limit. Results of Test A6 were

unexpected when compared with bearing roughness because roughness has increased

by 0.05 microns Ra value.

The shaft sleeve used in Tests A2, with contaminants without additive showed an

increase in roughness by 26% from its initial value of 0.42 microns Ra value. Test A4

showed poor results in this case also; where roughness of the shaft sleeve

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122

increased by 0.13 microns Ra value (22% increase). The most smoothening effect of

about 9% was observed with the commercial additive used in Test A3. In Test A2;

with the base oil contaminants but no additives, increased the shaft sleeve roughness

by the same order of magnitude as for the Test A4 i.e. 0.13 and 0.11 microns

respectively.

Change in sleeve transverse roughness

-0.1-0.05

00.050.1

A1 A2 A3 A4 A5 A6 A7

Tests

Cha

nge

in

tran

seve

rse

Ra

(mic

rons

)

roughness

Figure 4.10 b Change in shaft sleeve transverse roughness

Additives influenced transverse roughness of the shaft sleeve in a random fashion as

shown in Figure 4.10b. Test A1, where only base oil was used showed that the

surfaces were smoother after the test by 0.06 microns Ra value. The shaft sleeve was

rougher in transverse direction by 17% to 0.35 micron Ra value in Test A2. Thus

Test A2 showed that the surfaces were rough in both the elements in either direction.

This effect in transverse direction was an increase of only 0.05 microns Ra value.

The shaft sleeve surface was rougher in transverse direction for Test A3 by 0.08

microns Ra value (15%) contrary to the smoothening effect in the circumferential

direction of about 12%. Though the smoothening effect was very mild, unlike

previous increases in roughness of both the bearing and the sleeve, the shaft sleeve

were smoother in transverse direction was smoother in Test A4 by -0.03 microns Ra

value. Similar to Test A4 the effect of S-P based additive in Test A6 was also

unexpected where roughness of the sleeve increased in the transverse direction by 0.1

micron Ra value (from 0.28 to 0.38 microns Ra value). This effect of phosphate ester

additive is unexplained.

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The smoothening effect in Test A5 was significant, where shaft sleeve surface was

smoother by approximately 10% and Ra values changed from 0.47 to 0.42 microns.

Smoothening effect in the Test A7 was not as strong as in the case of Test A5, where

Ra value changed from 0.4 to 0.38 microns – a 5% change only.

4.5.3 Individual additive effects

Effects of individual additives were also analysed on each bearing element’s

roughness in both the directions and are represented graphically in Figure 4.11a to

Figure 4.11g. Pure base oil in Test A1 had smoothening effect in all the bearing

elements on both type of roughness (circumferential and transverse). The effect was

more prominent on bearings than shaft sleeves. The maximum smoothening effect

occurred on the bearing in transverse direction. A minimal smoothening effect was

observed on the shaft sleeve in transverse direction.

In Test A2 with oil containing contaminants Al2O3 but no additive, both the elements

were rougher and the influence was more prominent on the transverse roughness in

comparison to circumferential direction. The difference in increase in their values

was not in the same proportion because very small rise in roughness took place in the

transverse direction of the bearing when compared with all other elements. Similarly

the maximum rise in roughness was recorded in the bearing circumferential

roughness. The rise in roughness between the shaft sleeve directions was more

prominent in the circumferential direction than the transverse direction.

Roughness changes in Test A1

-0.4

-0.3

-0.2

-0.1

0RB RBT RS RST

Bearing and sleeve roughness patterns

Cha

nge

in R

a va

lue

(mic

rons

)

roughness

Figure 4.11a Roughness effects after Test A1

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Contaminants in the absence of antiwear additives are likely to cause more wear than

the cases where antiwear additives are used or no contaminants are used. As shown

in Figure 4.11(b) the maximum effect of about 20% occurred with circumferential

roughness of bearing whereas the effect on transverse roughness of bearing is

negligible.

R o ughness changes in T est A 2

0

0.1

0.2

0.3

RB RBT RS RST

B earing and sleeve roughness pat t erns

roughness

Figure 4.11b Roughness effects after Test A2

The influence on circumferential roughness of the shaft sleeve is almost half the

bearings circumferential roughness whereas in comparison to transverse roughness of

the shaft sleeve about 100% higher. However the overall influence is less than some

of the additives. This may be due to running-in effect or lapping effects during the

test.

Figure 4.11c shows the effect of commercial additive used in Test A3. The pattern of

influence was irregular. Though effect on the bearing was more prominent than the

shaft sleeve, no regular pattern could be established.

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Roughness changes in Test A3

-0.2-0.1

00.10.2

RB RBT RS RST

Bearing and sleeve roughness patterns

Cha

nge

in R

a va

lue

(mic

rons

)roughness

Figure 4.11c Roughness effects after Test A3

The influence of the additive was more favourable in case of circumferential

direction when compared with the transverse roughness and as in previous cases

increase in roughness was more in case of bearings than the shaft sleeves. The rise in

transverse roughness was higher for both the elements as compared to

circumferential roughness.

In Figure 4.11d influence of additive use in Test A4 shows that the rise in roughness

was higher in the bearing as compared to shaft sleeves. Similarly in both the

elements effect on the circumferential direction was more prominent as compared to

transverse direction. Though negligible, the only smoothening effect was observed

on the shaft sleeve in transverse direction which was about 7%.

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Roughness change in Test A4

-0.20

0.20.40.60.8

RB RBT RS RST

Bearning and sleeve roughness patterns

Cha

nge

in R

a va

lue

(mic

rons

)

roughness

Figure 4.11d Roughness effects after Test A4

Shown in Figure 4.11 (e) the commercial additive used in Test A5 improved the

roughness in both the elements in either direction. Bearing transverse roughness was

maximum smoothened maximum by 35%, whereas the influence on the shaft sleeve

transverse roughness in the transverse direction was approximately 10%.

Roughness changes in Test A5

-0.4-0.3-0.2-0.1

0RB RBT RS RST

Bearing and sleeve roughness patternsCha

nge

in R

a va

lue

(mic

rons

)

roughness

Figure 4.11e Roughness effects after Test A5

As shown in figure 4.11f the influence of the phosphorous-sulphur based additive in

Test A6 was quite significant in all cases except transverse roughness of the shaft

sleeve where surface rougher by 3.5%. The influence on circumferential roughness

of the bearing was most dominant with a reduction of roughness by approximately

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127

40%. Similarly its effect on shaft sleeve smoothening was observed in

circumferential direction whereas there was arise in roughness value in the transverse

direction. The effect was almost 100% when compared between circumferential and

transverse direction.

Roughness changes in Test A6

-0.6-0.4-0.2

00.2

RB RBT RS RST

Bearing and sleeve roughness pattern

Cha

nge

in R

a va

lue(

mic

rons

0

roughness

Figure 4.11f Roughness effects after Test A6

The isopropyl oleate additive used in Test A7 proved to be the dominant antiwear

additive influencing the circumferential roughness of the bearing (maximum 44%).

Figure 4.11g shows the minimum smoothening effect observed was the

circumferential roughness of the shaft sleeve (a negligible by 2.8%).

Roughness changes in Test A7

-0.6

-0.4

-0.2

0RB RBT RS RST

Bearing and sleeve roughness pattern

Cha

nge

in R

a va

lue

(mic

rons

)

roughness

Figure 4.11g Roughness effects after Test A7

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4.5.4 Roughness traces of bearing elements

To cite a few examples, the traces of roughness measurements for Test A5 have been

shown in Figure 4.12(a) to (h).

Figure 4.12a Bearing circumferential roughness before Test A5

Figure 4.12b Bearing circumferential roughness after Test A5

Shown in Figure 4.12a and Figure 4.12b the traces of surface roughness where Ra

values shown are 0.9 micron before the test and 0.71 microns after the test. As

explained earlier, these are the traces acquired randomly, and hence different but

close to the reported average values (0.9and 0.75 microns respectively) as shown in

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129

the Table 4.1 and 4.2. In this case the roughness has improved from 0.9 to 0.75

microns Ra value, which is a smoothening effect of -0.15 microns Ra value. These

traces show that the Ra values are very close to the average of several values

measured in the worn area. It could be observed from the test that the peaks have

been knocked off after the test.

Figure 4.12c Bearing transverse roughness before Test A5

The peak to valley height Rt has increased after the test from 5.5 to 9.8 microns. The

only cause of rise in Rt value can be attributed to the cutting action by the edge of the

solid contaminants.

Figure 4.12d Bearing transverse roughness after Test A5

The change in transverse roughness of the bearing is evident from Figures 4.12c and

4.12d, where the Ra value has decreased from 1.03 microns to 0.66 microns. For

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130

example, Ra = 0.68 microns in the sample trace shown in figure 4.12d, but the Rt

value remained unchanged at 6.3 microns. Nonetheless, the smoothening of the

surface is obvious due to the additive used in this test.

Figure 4.12e and Figure 4.12f show that the Ra value of the shaft sleeve in the

circumferential direction has improved from 0.52 to 0.44 microns, but the maximum

peak to valley height (Rt) has only insignificant increase i.e. from 6.7 to 6.9 microns

only.

Figure 4.12e Shaft sleeve roughness before Test A5

There is no standard explanation for cutting action by the edge of the solid

contaminants; however the Ra values vary, being statistical numbers that are close to

each other, making it difficult to highlight the effect of one parameter over the other

with existing equipment. Moreover, the roughness parameters vary drastically within

the wear zone where measurement cut-off lengths were chosen at different locations

randomly. In case of transverse roughness of the shaft sleeve the Ra value appears to

decreased from 0.47 to 0.42 (0.40 in the trace) as shown in Figure 4.12g and Figure

4.12h. The change in Rt value has occurred from 4.5 to 3.4 microns Ra value, which

indicates that the cutting action does not dominate the surface roughness change.

Similar traces can be referred in Appendix-F for selective test conditions. These

traces show that the roughness often varies significantly within the wear zone. It is

difficult to represent the surface finish by a single trace or a single roughness

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value. Therefore, the average of a significant number of readings must be used for

characterising the surface. The results analysis shows that it is hard to explain the

phenomenon behind the change in Rt value after the tests.

Figure 4.12f Shaft sleeve roughness after Test A5

Figure 4.12 g Shaft sleeve transverse roughness before TestA5

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Figure 4.12 h Shaft sleeve transverse roughness after Test A5

4. 6 Particle Counts (PC)

Particle counts technique for used oils is a well known tool for monitoring the wear

in machines. Lubricating oils contain solid particles even when they are fresh

supplied. The sources of these particles in fresh oil could be several, starting from the

environment in which they are manufactured, handled or stored. Whereas in used oil

the main source is the wear debris generated during the operation in addition to

particles that oil inherit from different sources prior to actual use.

The morphology of wear debris changes with time as particles may break into

smaller sizes and new particles are generated due to wear and so the actual particle

counts change with the usage of oil. Particle counts were measured with the

QuantAlert system for the fresh oil and after mixing the contaminants (Al2O3).

The samples were collected following the standard collection method –directly

tapped from the oil line. The oil was thoroughly mixed before and soon after the

tests. The counts were measured using eight different channels of different particle

sizes. These sensors gave the counts of particles greater than 5, 10, 15, 20, 25, 40, 75

and 100 microns respectively.

The counts of different sizes recorded by QuantAlert from different channels as well

as the change in the weight of total particles present in the oil are given in Table 4.3.

Initial counts and change in counts of particles larger than 15 micron but smaller

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133

than 20 microns were the main focus of this study and are listed in Table 4.1 and 4.2

respectively. Table 4.3 presents the change in particle counts of other sizes for

different tests, and in addition the change in weight of total solid contaminants.

Combining particle count and their weight gives a more reliable comparison for the

overall change in wear particles.

Table 4.3 Rise in particle counts of different sizes

Particle Size (μm) Test

>5 >10 >15 >20 >2 >40 >75 <100 Gravimetric change (mg/l)

A1 141 39 21 7 3 0 1 0 0.3

A2 9430 2627 1008 465 24 53 5 10 1.35 A3 1684 469 181 83 43 10 0 0 0.72

A4 1609 449 318 79 42 9 1 10 1.2

A5 3315 926 337 154 80 17 1 5 0.95

A6 1628 453 174 80 41 9 1 0 0.3

A7 4822 1343 257 238 12 28 25 7 0.6

Initially, particles of different sizes as mentioned in the Table 4.3 were measured

from the fresh oil sample. Subsequently the total weight of all types of solid particles

suspended in this oil sample was measured.

The particle count results showed that the supplied oil was well within the acceptable

cleanliness limits of ISO4406 (1987) standards 16/14/11. Some of the used oil

samples were very dark and opaque and required dilution with hexane up to 8 times.

However the dilution varied with oil condition. Efforts were made to keep the

sampling and testing procedures the same during the measurements. However the

variations in counts were large with poor repeatability in many cases.

To make the analysis meaningful only relevant data was considered. Main emphasis

was given to the counts of particles larger than 15 microns, keeping in view the ‘K’

ratio of the operating bearing which makes it mandatory that the minimum oil film

thickness is of the size of the averaged size of the contaminant particles (16 microns).

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Change in particle count >15 microns

0

500

1000

1500

A1 A2 A3 A4 A5 A6 A7

Tests

Part

icle

cou

nt

total counts

Figure 4.13 Comparison of change in counts for different tests

The analysis of particle counts of each size for different oil samples could have been

more time consuming but less useful keeping the objectives in view, data from all the

channels was collected to observe the pattern of change in counts. Initial values of

particle counts per millilitre of oil sample have been recorded in Table 4.1 and

change in number of particles of 15 microns or larger but smaller than 20 microns in

one millilitre of oil sample has been recorded in Table 4.2. Table 4.2 also shows the

change in weight of total solid particles suspended in the oil sample in g/l. The

results of particles larger than 15 microns are the main concern in this study and have

been presented graphically in Figure 4.13. The performance of individual additives

in generating particles of different sizes has also been illustrated by their respective

graphs in Figures 4.13 (a) to (g).

Figure 4.13 shows that the change in the count of particles larger than 15 microns in

Test A1 was low and increased by 15 counts (from 9 to 30 per ml). Ideally there

should have been no change but experimental errors and ingestion of contaminants

from the surroundings or generation of wear debris during the starting and stopping

could be the contributing factors. The high count rise of 1008 after Test A2 was

expected due to contamination of oil without any additive. The oil sample initially

contained 340 particles per millilitre (after mixing 4g/l Al2O3) before the test and it

increased to 1348 after the test. The counts after the Test A4 commensurate with the

other wear measure parameters with an increase of 318. However the additive used

in Test A5 resulted in an increase in particle counts of 337 which is high in

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135

comparison to Test A4. Performance of additive A3 and A6 was also of the same

order with a rise of 181 and 174 respectively. But the effect of additive A7 was

moderate with a rise of 257. Additive A6 proved to be the best performer. However

the performance of the remaining additives did not give a clear indication of

superiority of one over the other. As discussed the repeatability of the QuantAlert

was poor and after repeating the tests only the data deemed relevant was considered

for the analysis.

Test A1 results for sizes of particles chosen from the QuantAlert are given in Table

4.3 and shown in Figure 4.13(a). It shows the change in different sizes of particles

after the test graphically. Results for 100 microns and 40 microns are absent.

However, >75 micron particles were detected in the sample which may be an

experimental error or an inclusion of particles from some external source. Normally

the number of larger particles present in the sample is small compared with the

smaller size particles but there can be exceptions. The largest change for the 5

microns size was 141 which is too small and indicates that the oil was clean. Ideally

there should be no change in counts under hydrodynamic lubrication condition; this

small rise in counts was expected mainly due to small wear during start and stop

conditions or ingestion from surroundings. The rise in count for other sizes of

particles such as >10,>15, >20 and >25 were small and with in acceptable limits.

Change in particle count Test A1

020406080

100120140160

>5 >10 >15 >20 >25 >40 >75 <100

Particle size

Cha

nge

in p

artic

le c

ount

/ m

g

particle counts

Figure 4.13a Change in counts after Test A1

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In Test A2 the contaminants in the absence of additive caused a large change in

particle counts which indicates severe wear in the bearing. The change in the number

of particles larger than 15 microns rose to 1008 counts. The particles larger than 40

microns were very few in this case but the number of particles larger than 15 microns

was very large in comparison to other test conditions. The results were anticipated in

presence of solid Al2O3 particles without any kind of antiwear additive treatment.

Change in particle count Test A2

0

20004000

60008000

10000

>5 >10 >15 >20 >25 >40 >75 <100

Particle size

Cha

nge

in p

artic

le

coun

t/ m

g

particle counts

Figure 4.13b Changes in counts after Test A2

Results of other tests shown in Figures 4.13c to 4.13g follow the same trend as test

A1 and A2. The results obtained for all the tests for eight different sizes have been

plotted for a comparison and shown in Figure 4.14. The graph shows the dominance

of one additive over another with superiority of additive A6 and poorest performance

of additive A5. The repeatability of the results is poor because generation of particle

of a particular size is not fixed and also the grinding and crushing of bigger particles

results into smaller particles cannot be predicted. To improve the reliability of the

results the total count of all the eight different sizes of particles were recorded for

each test case and presented in Figure 4.13h.

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Change in particle count Test A3

0

500

1000

1500

2000

>5 >10 >15 >20 >25 >40 >75 <100

Particle size

Cha

nge

in p

artic

le

coun

t/ m

g

particle counts

Figure 4.13c Changes in counts after Test A3

Change in particle count Test A4

0

500

1000

1500

2000

>5 >10 >15 >20 >25 >40 >75 <100

Particle size

Cha

nge

in p

artic

le

coun

t/ m

g

particle counts

Figure 4.13d Changes in Counts After Test A4

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Change in particle count Test A5

0

1000

2000

3000

4000

>5 >10 >15 >20 >25 >40 >75 <100

Particle size

Cha

nge

in p

artic

le

coun

t/ m

g

particle counts

Figure 4.13e Changes in counts after Test A5

Change in particle count Test A6

0

500

1000

1500

2000

>5 >10 >15 >20 >25 >40 >75 <100

Particle size

Cha

nge

in p

artic

le

coun

t/ m

g

particle counts

Figure 4.13f Change in counts after Test A6

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Change in particle count Test A7

0

2000

4000

6000

>5 >10 >15 >20 >25 >40 >75 <100

Particle size

Cha

nge

in p

artic

le

coun

t/ m

l

particle counts

Figure 4.13g Changes in counts after Test A7

The figure shows that the trend in change is similar to change of >15 micron

particles shown in Figure 4.13. However, keeping the poor repeatability of the

equipment in mind the similarity in the trend of results makes analysis worth

considering. The only limitation of the results shown in Figure 4.13(h) is that the

total number of particles counted for only eight different sizes and there may be

many more other sizes smaller than 5 microns or bigger than 100 microns may be

unaccounted.

Change in total counts

02000400060008000

10000120001400016000

A1 A2 A3 A4 A5 A6 A7

Tests

Cha

ngei

n co

unts

/ml

Series1

Figure 4.13h Change in total particle count

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comparison of particle generation

0

5000

10000

15000

20000

25000

30000

35000

>5 >10 >15 >20 >40 >50 >75 >100

particle sizes

Cou

nts/

ml

A1A2A3A4A5A6A7Gravimetric

Figure 4.14 Comparison of wear particles changes

The generation of particles in a bearing is a complex phenomenon. As particles

during the motion break and their number may change drastically. The particle size

less than 5 microns are very large in number because they are formed by breaking

and rubbing of large particles. Hence, this analysis is merely a guideline and not a

guarantee that particles of any other size were not generated during the wear process.

Keeping in view the problem, the results of weight of total particles present in the oil

sample gives better trend of wear than the total number from different channels of

Quant Alert which is discussed further in the next section.

4.6.1 Gravimetric change (PCg)

The morphology of particles and so their sizes change as the wear progresses in the

bearing. This makes it difficult to analyse the effect of the contaminant particle size

on lubrication and further wear in the system. It is even more difficult to assess the

accurate number of particles generated in the system below five microns. However,

the weight of the total particles generated can be assessed by recording the change in

the total weight of the solid particles present in the oil. This can prove to be a good

technique but errors due to inclusions from the environment, accuracy in

measurements could be the limitations of this technique. The gravimetric

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141

measurements taken by Quantalert are presented graphically in Figure 4.15. The

initial values and the corresponding change in their counts are presented in Table 4.1

and 4.2 respectively.

The weight of total particles was measured with the QuantAlert in 10ml sample

which was later converted to g/l as shown in Figure 4.15. The initial weight of the

contaminants in Test A1 could not be detected before the test; however the weight

change of 0.3 mg was recorded after the test. In ideal conditions there was no wear

and hence there should not be wear debris generation but the change may be due to

environment or there may be errors in accuracy.

The change in weight of total debris generated after Test 2 was maximum and

commensurate with the change in particle counts. However, Table 4.2 shows that in

the case of Test A4 even though the particle counts is lower as compared to Test A5,

the change in total weight of the solid particles is higher due to the presence of

particles >100 microns. The particles of >100 microns are lot heavier than the

smaller size particles hence the influence of the number of smaller size particles is

not so severe on the total weight. Change in weight after Test 6 is the lowest, and

similar to the change in particle count. Change in weight after the Test A7 is

comparable to Test A3. These results show that the gravimetric change is also

significant in case of Test A1 compared with Test A6.

There is no good explanation as to why the change in particle count is not similar to

the change in total weight of the particles. The only explanation could be that the

particle morphology changes with time and there is no guarantee that particles larger

than 15 micron changes in the same order as other particle. Hence a comparison of

total weight change, with the change in particle count of size larger than 15 microns,

is not a valid comparison. Though gravimetric results are expected to give more

reliable results, the source of particles or the material being weighed is not

necessarily the wear particles or suspended solid contaminants. There is likelihood

that polymer material which is not solid may also be agglomerated and weighed

during the gravimetric measurements. Overall the particle count technique did not

prove to be a reliable method as claimed by the equipment manufacturers.

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Particle weight change

0

5

10

15

20

A1 A2 A3 A4 A5 A6 A7

Tests

Cha

nge

in w

eigh

t (g/

l)

total w t.

Figure 4.15 Changes in total weight of contaminants

4.7 Maximum Wear Depth (WDmax)

The worn area in the bearing varies from one test to another. The maximum wear

depth is independent of the projected area and that decides the wear profile for each

worn bearing. Wear profile of each bearing is unique for different bearings worn

under the same operating conditions and hence they create their own signatures.

Wear depth is the maximum departure of the worn surface from the original surface

in the radial direction within the wear zone.

There were a number of options to record the maximum wear depth (WDmax). In fact

the maximum change in bearing ID is the maximum wear depth. Data shown in

Table 4.1 and Table 4.2 are the average value of changes in ID and OD of the

bearings and shafts respectively. These measurements were taken with sophisticated

measuring apparatus such as Metroscope and HP Laser system. Identifying

maximum wear depth as an easy tool for wear measurements, another method was

developed where magnified out-of-roundness trace was used to achieve higher

accuracy. This method will be discussed further in the following chapter. However,

using sophisticated measuring devices was found to be time consuming and using

out-of-roundness trace involved subjectivity. Hence a simple method was used where

bearing ID was measured with a bore gauge at several locations in the wear zone of

the bearing and the highest value of change in ID was recorded as maximum wear

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143

depth (WDmax).

The results showed that the WDmax parameter can be used successfully as a wear

measurement parameter similar to that of wear scar diameter in four ball test

machine. The results have been presented in Table 4.2 and were compared with the

maximum change in bearing ID measured with a Metroscope and hole-gauge-test.

Figure 4.16 shows that the trend of measured WDmax values are similar to change in

maximum ID though the values are slightly lower than the change in maximum

bearing ID measured with a Metroscope. The maximum variation is close to 25% for

Test A7, where change in IDmax is 16 microns and change in WDmax is 20 microns.

Minimum variation was recorded for Test A3 where the measured WDmax is 29

microns whereas the change in maximum ID is of the same order i.e. 28 microns.

Figure 4.16 shows the results graphically where maximum wear depth in case of Test

A1 could be ignored as it is too low and could be due to human error in

measurements. The results of Test A2 and A4 are the same with WDmax values 42

microns. These results are susceptive as Test A4 results indicate that the phosphate

ester additive was ineffective. The sources of variations may be several such as;

human error and lack of user controlled environment. However the trend is same as

change in IDmax.

Comparison of maximum wear depth and change in bearing ID

01020304050

A1 A2 A3 A4 A5 A6 A7

Tests

WD

max

/ ID

ch

ange

(mic

rons

)

WD max ID max change

Figure 4.16 Changes in maximum wear depth

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4.8 Changes in Minimum Oil Film Thickness (Hmin)

The change in micro-geometry of the bearing due to successive wear influences the

tribological performance of a bearing. This influence is reflected through the change

in minimum oil film thickness in the bearing contact. The change in minimum oil

film thickness is a compound effect of various factors; the main ones are: change in

radial clearance, out-of roundness, roughness, and wear depth. The other most

important factors are the presence of solid contaminants in and around the bearing

contact which creates restriction to the free flow of the lubricant and lastly the

antiwear additives, which influences the motion of the solid contaminants.

As wear progresses in the bearing the radial clearance increases and the minimum oil

film thickness decreases. Reduction in minimum oil film thickness during the test

causes a rise in oil temperature and/or progression of wear. Though, this parameter is

not directly related to the wear, however, as a result of wear, film thickness reduces

and decreases the load capacity of the bearing. If this phenomenon continues, a

situation arises when film thickness reduces to an extent that metal to metal contact

takes place, which brings hydrodynamic regime to mixed and boundary lubrication

regime, and finally scuffing takes place in the bearing contact.

The operating parameters were chosen in such a way that the oil film thickness and

sliding distance remained the same for all the test conditions. Since radial clearance

of each test bearing was different the speed required to achieve 16 micron minimum

oil thickness was also different. Thus test duration for each case varied such that the

total sliding distance remains the same. Minimum oil film thickness was recorded at

three intervals of time during the tests i.e. at the start (Hxps), middle (Hxpm) and end

(Hxpe). While recording the film thickness measurements it was observed that the

readings were fluctuating in a random manner. Several probe output readings were

recorded out of which only relevant data was considered. The output of the proximity

probes could not be directly converted to film thickness as they were giving the

relationship with the minimum distances between the tip of the proximity probe and

the shaft sleeve surface. Using a geometrical method developed for this study

(explained in Chapter 3) the minimum oil film thickness was calculated from the

output recorded in millivolts. Minimum oil film thickness at the start of the each of

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test to achieve ‘K’ ratio close to one have been recorded in Table 4.1

The changes in minimum oil film thickness values calculated with the help of the

proposed geometrical method are presented in Table 4.2. The table shows that the

film thickness reduced with time as contaminants caused wear in the bearing. In a

worn bearing the minimum oil film thickness was based on the eccentricity of the

shaft sleeve centre which occurs in the direction of line of centres.

In case of a worn bearing the minimum oil film thickness does not necessarily occur

along the line of centres because the wear depth along the line is normally a deep

trough. However, in this analysis minimum oil film thickness was calculated based

on the eccentricity in the bearing and wear depth was not considered.

Minimum oil film thickness was recorded for each test bearing of known radial

clearance ‘C’ and operating speed ‘N’ for a constant load of 500N. The values of

film thickness recorded at the start (Hxps), in the middle (Hxpm) and at the end (Hxpe)

of the experiments are shown in Table 4.4. Figure 4.17 shows the change in

minimum oil film thickness results graphically. The change in minimum oil film

thickness was calculated by subtracting Hxpe readings from Hxps readings. The values

show that as wear progresses the value of film thickness gets reduced.

Table 4.4 Changes in measured minimum oil film thickness

Tests C (μm)

N (rpm)

Hxps (μm)

Hxpm (μm)

Hxpe (μm)

ΔHmin (μm)

% change

A1 82 400 17.86 17.82 17.82 0.04 0.2

A2 82 420 17.24 11.01 6.43 10.9 63.2

A3 86 470 18.28 15.107 14.18 4.1 22.4

A4 80 400 17.46 14.41 8.96 5.8 33.2

A5 89 500 15.62 8.0 10.47 5.15 32.9

A6 89 500 15.6 13.06 11.80 3.8 24.4

A7 80 400 14.9 11.13 11.10 3.8 25.5

The following equation derived by geometrical method in Chapter 3 (Equation 3.3)

was used to calculate the eccentricity in the bearing and subsequently by substituting

the value in Equation 3.6 the minimum oil film thickness was calculated for different

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operating conditions:

Change in minimum oil film thickness

0

2

4

6

8

10

12

A1 A2 A3 A4 A5 A6 A7

Tests

Cha

nge

in m

in. o

il fil

m

htic

knes

s (m

icro

ns)

Figure 4.17 Reduction in minimum oil film thickness

Figure 4.17 shows that the reduction in minimum oil film thickness was negligible

in Test A1. This was mainly because the bearing was operating on a full

hydrodynamic oil film throughout the test. In the absence of solid contaminants,

wear occurred only during starting and stopping of the tests. In Test A2, where 4g/l

Al2O3 was used as a solid contaminant, the wear resulted in reducing the minimum

oil film thickness drastically i.e. from 17.24 microns to 6.43 microns; almost 63%.

Reduction in minimum oil film thickness was also recorded in other test conditions.

For Test A3 the value changed from 18.28 microns to 14.18 microns, a 22%

reduction. For Test A4, with phosphate ester additive present, the minimum oil film

thickness reduced from 14.76 to 8.96 microns, a 40% reduction. Wear results

obtained from other methods confirm the poor performance of the phosphorous

based additive used in Test. Test A5 shows that the change was greater than

expected. In Test A3 the reduction in minimum oil film thickness was 5.15 microns,

33% lower than the initial value. Changes in Test A7, A6 and A3 are of similar

magnitude: 25%, 24% and 22.4% respectively. The measurements recorded for Test

A5 show that there is an error in recording Hxpe (10.47 microns) value, which is

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higher than the Hxpm value of 8 microns, and it cannot be so. Like other wear test

methods, this method also proved to be reliable only for cases where changes due to

performance of the additive are discernable.

The overall results do not show a clarity and high confidence level for predicting

wear in the bearing contact. Though the required minimum oil film thickness was 16

microns but measured values vary from 14.9 microns to 18.28 microns. This may be

due to error in measurement or human error in maintaining constant test conditions

such as temperature, pressure and speed. The tests were noisy after adding the

contaminants in the oil. Vibrations in the bearing also caused difficulty in recording

the measurements fluctuations in reading were excessive hence data was analysed

thoroughly and redundant or irrelevant data was discarded.

The rate of film thickness reduction was more pronounced in some tests; for

example, in Test A2 the rate of film thickness reduction up until middle of the test

was comparable that in the other tests, except Test A5. However, in Test A2 the loss

in film thickness from middle to end of the test was rapid, followed by that in Test

A4. The film thickness reduction rate was minimal in Test A3. In tests A5, A6 and

A7 these were rather similar. In case of Test A5 the minimum oil film thickness

reading is unexpected and there seems to be some error as the value observed in the

middle of the test was 8.0 microns, whereas at the end of the test it was 10.47

microns. The rate at which the film thickness reduced and its mechanism may be

linked to the additive chemistry which is beyond the scope of this study.

The above results show that a bearing operating at ‘K ≈ 1’ gives rise to more wear

and low oil film thickness, which leads to higher friction. Even though the minimum

oil film thickness of half a micron can be recorded with the proximity probes,

excessive vibrations caused unacceptable fluctuations in readings. Thus the norm of

operating a hydrodynamic bearing at a lambda ratio 10 is not universally applicable.

4.9 Comparative Analysis of Techniques and Results

This section compares the methodologies adopted in this study as a part of the multi-

wear parameter approach (MWPA). The outcome of this comparative study helped in

choosing the most suitable wear measurement technique that helped in developing a

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tool for characterising antiwear additives. Furthermore, based on the selected wear

measuring technique, the performance of various antiwear additives was evaluated.

4.9.1 Methodologies

Weight loss is one of the most commonly used parameter to quantify wear, however

it can give false results if the wear is too small, which can be further exacerbated due

to human or equipment error. For example, Test A7 showed a weight gain of 0.09 g

contrary to what is expected; while all other tests showed a weight loss. The above

analysis showed that it is difficult to conclude as to which parameter was dominating

i.e. wear or metal transfer due to embedding. Since, micrographs show that the trend

of wear and metal transfer in Test A7 is similar to that in the other tests (Appendix-

D), the reason for this contradiction (i.e. weight gain in Test 7) can be an error in

measurement.

Out-of-roundness results show the wear reducing behaviour of additives clearly,

because the graphs are highly magnified. These traces give a unique signature of

wear reducing behaviour of the additives, and bearing wear can be measured with

higher precision. The special feature of this method is that it gives highly magnified

view of the departure of circumference from the ideal shape, without magnifying the

overall size of the test piece. Also, a small geometrical change which may not be

possible to detect from other techniques, can often be observed visually by

comparing the out-of-roundness traces taken before and after the tests. Thus the

possibility of error in measurements is lower as compared to that in the other

methods.

The methodology based on change in radial clearance gives results with poor

repeatability. More over the results show that the radial clearance varies along the

circumference of the bearing. However, this methodology can give better design

guidelines if its metrology can be improved as discussed in chapter 3. The method

highlights the need of the correct metrological practices. The method itself needs

more improvements for predicting results with desired confidence.

Roughness measurements raised several issues, such as, selection of the

measurement points within the wear zone, as roughness varied significantly from one

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point to another; hence, it is hard to choose a representative sample area. The same is

true with the shaft sleeve as well. Averaging the readings taken at several locations

does not give a true picture, and there was no repeatable pattern in the wear reducing

behaviour. These problems were encountered with both bearing elements, i.e.

bearing and shaft sleeve, in transverse as well as circumferential directions. Though,

efforts were made to consider the most representative readings, these did not depict

any relationship of preferential path, as proposed by Martin (1991). However, the

measurement of surface roughness helped in identifying the severity of abrasive

wear. As stated earlier the roughness values are statistically calculated numbers, in

this case these are not controlled roughness, hence random pattern of roughness

cannot be compared with a controlled roughness case.

The methodology based on measured maximum wear depth gives reasonably reliable

results. Experimental data demonstrated that the pattern of wear reducing behaviour

of additives predicted by this method is commensurate with the other accepted

techniques. However, locating the point of maximum wear depth within the wear

zone remains a challenge and hence the method may not be highly reliable.

In the particle counting methodology, even a 4 % concentration of Al2O3 in oil

caused opacity; consequently, the oil was diluted several times to minimise this

effect. However, the repeatability of the results was still poor. The results showed

that the variations could be as much as 50% to 100%. In some cases where results

were repeated after few days the repeatability was even poorer and hence an error

analysis was not thought to be a useful exercise. The total weight of the suspended

particles (in the oil samples) was recorded using the QuantAlert particle counter.

This methodology showed similar wear reducing trend as other techniques. However,

keeping in view of the poor repeatability of the results obtained from this equipment,

this technique cannot be relied upon.

Minimum oil film thickness measurements showed that proximity probe method is

reliable and gives results with desired accuracy when there are no contaminants

suspended in the oil. Minimum oil film thickness was recorded at the start, in the

middle, and at the end of the test. However, for high concentration of solid

contaminants the results were less reliable, due to rapid drop in oil film thickness

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leading to excessive vibrations.

4.9.2 Additive performance

Analysis of the results showed that it is difficult to predict the performance of an

individual antiwear additive based on just one of the wear measurement techniques,

due to very little difference between the performance results and the precision of the

existing wear measuring methodologies. Ranking of antiwear additives based on

their wear measurements is shown in shown in Table 4.5.

Table 4.5 Comparison of performance of antiwear additives

No Technique Test A3 Test A4 Test A5 Test A6 Test A7 1 ΔWb (gm) 3 5 4 1 2*

2 ΔORb (μm) 3 5 4 1 2 3 ΔC (μm) 3 5 4 1 2 4 ΔID (μm) 3 5 4 1 2 5 Δhmin 3 5 4 1 2 6 ΔWD max 3 5 4 1 2 7 ΔPCg 3 5 4 1 2 8 ΔWs (gm) 2 5 4 1 3 9 ΔOD (μm) 5 3 4 2 1 10 ΔPC (count/ml) 2 4 5 1 3 11 Rb (microns) 4 5 3 2 1 12 Rbt (microns) 4 5 1 3 2 13 Rs (microns) 1 5 2 4 3 14 Rst (microns) 4 3 1 5 2

(* Presumed weight gain was an experimental error)

As shown in the table, techniques 1 to 7 depict same results, whereas, the remaining

techniques show much variance in additive performance. Table 4.5 shows that the

additive used in Test A6 proved to be the best and that of the additive used in Test

A4 was the worst. However, technique number 2 (out-of-roundness method) gave the

most distinct results for the various additives, and techniques 1 and 3-7 confirm these

results. Therefore, the out-of-roundness method has been selected for the

characterisation of the additives.

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4.10 Conclusion

The analysis of results helped in understanding the behaviour of different antiwear

additives on the bearing element’s wear. It helped in selecting the most appropriate

wear measurement method for characterising the antiwear additives and also in

determining the effect of change in micro-geometry on the tribological performance

of the bearing. The following conclusions were drawn from the analysis:

• This chapter compared six methods including fourteen wear measurement

parameters that comprise the MWPA (multi-wear parameter approach) suite.

The aim was to identify the most efficacious testing methodology for

measuring wear under dusty environments.

• The analysis of data showed that the antiwear additive used in Test A6

performed the best and additive used in Test A4 had almost no antiwear

properties. This finding was supported consistently by seven measured wear

parameters. There is a clear distinction between the wear caused by pure base

oil, and that by oils containing solid contaminants. However, there is only a

marginal difference in the performances of some additives, which is rather

difficult to quantify.

• Weight loss is the parameter which quantifies wear loss in a tribological

component most directly; however, significant errors are likely if the amount

of wear is too low. The out-of-roundness emerged as the most reliable and

suitable methodology for quantifying wear.

• This research revealed a high concentration of solid contaminants in and

around the bearing contact. Accumulation of solid contaminants at the contact

entry and within the contact zone restricts the lubricant flow, and hence,

increasing level of mixed or boundary lubrication conditions occur as the test

progresses.

• The reduction in minimum oil film thickness was considered as the

cumulative effect of all the micro-geometry parameters, as well as that of the

concentration of the contaminants in the contact zone. This led to rapid

reduction in minimum oil film thickness, and excessive wear;

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consequently, the film thickness measurements did not produce repeatable

results. However, it clearly depicts the adverse effect of changed micro-

geometry and contaminants on the bearing’s tribological performance. In

other methodologies, either due to lack of precision in measurements, or

variation in measurement location resulted in poor data repeatability.

• Surface roughness measurements were random and inconsistent within the

wear zone, hence could not be used for further analysis. The concept of

preferential path could also not be established because actual surface

roughness patterns were random.

• Particle count method did not prove to be reliable because of heavy

concentration of solid particles, which could not be counted reliably.

Furthermore, break up of polymeric additives into particle-like structures

caused interference with particle count.

• In conclusion, the out-of-roundness technique gave the most reliable results

and has been chosen for the characterisation of the additives.

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CHAPTER 5

5. CHARACTERISATION OF ANTIWEAR ADDITIVES

5.1 Overview

Use of antiwear additives is common in situations where machines are prone to

excessive wear. Machinery working in mining industry, highway construction or any

dusty environment is subject to substantial solid contamination. Antiwear additives

enhance the life of tribological components under worn conditions, and, to some

extent, reduce energy consumption due to reduction in frictional forces between the

mating surfaces.

The question has often been asked if the added cost of the additives is justified under

such conditions. Several additive manufacturers claim their product is better than the

others. In general, industry needs some universally agreed guidelines to judge the

efficacy of a product. But, there is no reliable measure by which two products can be

compared, except by evaluating their performance in the machine. It may be possible

to prove that one product is better than another under certain laboratory conditions;

however this may not be replicated in real machine operation.

The life expectancy of a machine depends on several factors, and improvement in a

component’s life may be so marginal that it is hard to isolate that factor which has

maximum influence. Similarly, the difference in the performance of antiwear

additives is so small that it may be hard to distinguish between the effect of antiwear

additives and the other factors influencing the performance of a bearing.

Journal bearings normally operate in the hydrodynamic regime, where the two

mating surfaces are separated by more than 10 times the composite roughness.

However, very small amount of wear is expected in such bearings, especially when

bearing starts or stops. The amount of wear is so small that it may be hard to record.

However, a small change in coefficient of friction, and consequential reduction in

wear can result in significant savings when considering industry-wide application,

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where thousands of bearings are used. Reduced downtime costs due to lower failure

rates and energy saving are the key factors for targeting an efficiently operating

machine.

The interaction between solid contaminant particles and the bearing surfaces, as well

as the interaction amongst the solid contaminant particles causes additional wear and

friction. The tribology of such bearings is not well understood. There is a need to

develop a standard methodology by which the wear reducing performance of an

additive can be judged. This will help in selecting the proper lubricant for a specific

machine and its operating environment.

In this research different additives have been compared for journal bearing wear

performance. Test bearings were lubricated with oil containing Al2O3 as a solid

contaminant. Various tests were performed after mixing different types of antiwear

additives in prescribed dosage. Tests were run for the same operating conditions and

the same sliding distance. The effect of these additives on journal bearing wear was

observed using Multi-Wear Parameter Approach (MWPA), using various wear

measurement techniques. Analysis of the data obtained from different measurement

techniques used under MWPA showed that weight loss and out-of–roundness are

more reliable wear measure techniques. Using these two techniques, a methodology

has been developed to characterise the antiwear additives for their wear reducing

behaviour.

5.2 Wear Measurement by Weight Loss

Weight loss is one of the quantitative measures of wear in bearings and gives direct

evidence of wear quantity. However, human or equipment errors in measuring the

minuscule weight loss can reduce the reliability of the results. Therefore our aim is

to develop a method that does not rely solely on the measurement of weight loss. It

was shown in Chapter-4 that the out-of-roundness trace of a worn test bearing can

provide a magnified view of wear in the bearing. By measuring the change in the

shape of a trace, wear in a bearing can be quantified reliably and easily. It is also

important to note that the shape of the out-of-roundness trace for each additive is

different and hence each additive gives a unique signature of its anti-wear

performance. Literature review revealed that the out-of-roundness measurement has

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not been used effectively, thus far. We postulated that out-of-roundness measurement

can be an efficacious method for wear characterisation. Its features such as: unique

wear signatures and high magnification lead to better accuracy and consistency in

calculating weight loss. In this research a methodology has been developed to

calculate weight loss in worn bearings from their out-of-roundness traces for known

bearing length and material density.

Out-of-roundness trace magnifies the deviation of the circumference from the true

circular shape at a fixed bearing cross section without magnifying the overall

diameter of the circular work piece. The region of the trace, where worn surface

departs from the original is identified as the wear zone. By comparing the traces of a

bearing before and after the test, the zone can be identified by visual inspection, in

the form of a wear crescent, as shown in Figure 5.1. A process has been developed,

by which the area of this wear crescent can be measured with desired precision, and

subsequently wear volume and weight loss can be computed for known bearing

length and material density.

Figure 5.1 Wear profile of a worn bearing

5.2.1 Wear Computation from Out-of-roundness Trace

The out-of-roundness trace of a bearing gives more precise distance between the

centre about which the work piece is rotated and the circumference at any angular

Unworn surface

Maximum wear depth

Wear zone width

Wear zone

Worn surface

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location. The trace of a worn bearing is similar to the end view of the bearing shown

in Figure 5.1. The departure from normal of the bearing surface in the wear zone is

characterised by the wear depth, which varies along the wear crescent. The area of

the wear crescent is the wear area at a fixed cross section of the bearing and is termed

as cross sectional wear area (CSWA). In order to find the weight loss, the CSWA

value needs to be determined with high precision, subsequently wear volume and

weight loss can be computed, for known bearing length and material density.

Figure 5.2 Roundness measurements locations

The out-of roundness traces were recorded at three fixed locations along the bearing

length, i.e. at H1= 5mm, H2 =15mm and H3 = 35 mm as shown in Figure 5.2. Ideally

the CSWA should be the same all along the bearing length. However, it changes

from point to point along the length due to two reasons: firstly, the changes in out-of-

roundness from one cross section to another, and secondly, wear due to misalignment

of the shaft when bearing is loaded. Figure 5.3 shows the effect of misalignment

where shape of the worn area along the bearing length changes with the degree of

misalignment. Under ideal conditions the worn area should look like a rectangle, as

shown in this (Figure 5.3) by solid lines. Similarly, under extreme misalignment

conditions the wear surface may look like a triangle, as shown by dotted lines.

However, the size of the triangle will depend upon the radial clearance as well as the

load applied. If the amount of misalignment is small, as is the case in this study, the

worn area may look like the shaded area shown in Figure 5.3.

H3 =35mm L =40mm

H1 = 5 mm

H2 =15 mm

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Figure 5.3 Wear zone shape

The width of the worn area at any point along the bearing length is termed as wear

zone width (WZW) at that point. In other words WZW varies along the bearing

length depending upon the degree of misalignment. The WZW may vary from point

to point all along the bearing length, either due to change in out-of-roundness, due to

misalignment, or both. Thus the CSWA may vary from one cross section to another.

Initially, three out-of-roundness traces were acquired to find the average value of the

CSWA. The CSWA computed on the two ends varied around 5% only; hence the

variation can be ignored. Under such circumstances, only one trace that gave largest

WZW was considered and it was presumed that the CSWA is the same for all

bearing cross sections. As stated the CSWA needs to be estimated with high

precision, therefore a systematic procedure has been developed to minimise errors in

measurements.

5.2.2 Computation of Cross Sectional Wear Area (CSWA)

Computation of weight loss from the out-of-roundness method requires calculation

of area of the wear crescent with high precision. The technique for measuring this

Cross Sectional Wear Area (CSWA)

Bearing length

wear zone width WZW

Extreme misalignment wear shape

Ideal rectangular wear shape

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area is based on the measurement of out-of-roundness of the circular work pieces,

using Talyrond equipment.

Ideally, an out-of-roundness trace of a perfectly circular bearing should be a perfect

circle. An enlarged view of a trace obtained for a bearing before the test is shown

Figure 5.4. This trace shows that the shape is not a perfect circle, implying that it has

some degree of out-of-roundness. In order to understand the method of computing

the CSWA, it is necessary to understand the principle used by the Talyrond

equipment. An out-of-roundness trace of a circular work piece is acquired by

rotating it against a transducer which records the circumference, showing the

departure of the periphery from the true circle.

The out-of-roundness from this trace is measured with the help of a monograph. This

monograph is a transparent plastic sheet on which concentric circles of different

diameters are marked. The monograph is placed on the trace in such a way that one

of the concentric circles sits inside the trace and touches the trace at minimum two

points. The farthest point of the trace touching the largest diameter concentric circle

gives the maximum departure of the traced circumference from the touching circle.

This maximum departure can be measured in terms of the number of radially

graduated divisions marked on the trace graph paper (Figure 5.4).

Each division marked on the graph paper corresponds to a calibrated value in

microns, depending upon the magnification chosen to acquire the trace. Multiplying

the divisions of departure with the magnification factor (in microns per division)

gives the out-of-roundness of the bearing in microns.

Measurement of the CSWA with precision is the most important step for the weight

loss computation process. The following step-by-step process has been developed

for the computation of CSWA with precision.

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Graduations marked

Figure 5.4 Out-of-roundness ‘before test trace’

Step1: Prepare out-of-roundness traces

Select a high magnification (say few hundred times) on a photocopier depending

upon the paper size available and the accuracy required. Photocopy the ‘before test

trace,’ on an overhead transparency (Figure 5.4). Using the same magnification

photocopy the ‘after test trace’ for the same bearing location – preferably on an

overhead transparency (Figure 5.5).

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Figure 5.5 Out-of-roundness ‘after test trace’

Step2: Identify Wear Crescent

Place the ‘before test trace’ transparency over the ‘after test trace’ and try to match

the shape, identifying the wear zone. By topography complete the wear zone part of

the circumference of the after test trace by drawing the crescent arc with dotted line.

Thus, the wear crescent can be identified by locating the inner crescent arc and the

outer crescent arc (Figure 5.6). These crescent arcs are also shown in Figure 5.7

where an inner crescent arc has been drawn on an actual out-of-roundness graph

paper. Thus on the ‘after test trace’, the worn part of the ‘before test trace’ can be

identified clearly.

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Figure 5.6 Computed out-of-roundness shape of a worn bearing

Step3: Mark computed maximum wear depth (WD)

Figure 5.8 shows the process used for finding the computed wear depth (WD).

According to this process the centre of the ‘before test trace’ component called trace

centre ‘O’ can be marked by visual inspection; else by inscribing a concentric circle

marked on the monograph touching the ‘before test trace’ part at minimum three

points.

Mark mid-point D on the outer crescent arc in the wear zone in such a way that ‘OD‘

is the largest distance between the trace centre (O) and the outer crescent arc. Now

draw the line OD intersecting the inner crescent arc at W (Figure 5.8). Distance WD

in this figure is the computed maximum wear depth.

Step4: Mark wear depths (wn dn)

It is observed that the angular extent of WZW is less than 1200. Keeping in view this

assumption, mark nodes w1d1 and w17 d17 on 60o angle either sides of the mid-point D

respectively. These are the two extreme ends of the wear crescent. Divide the outer

crescent arc in ‘n’ number of parts. In this study the inner crescent arc has been

Wear zone start

Wear zone ends

Crescent Arc (inner)

Crescent Arc (outer)

Trace centre ‘O’

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divided in 16 equal parts. There is no specific reason for choosing this number except

that it may be helpful in developing a simple theoretical model in future. Mark

nodes from w1 to w17 total n+1 nodes (from w1 to wn+1). Now draw lines Od1 Od2

Od3 etc. up to Od17, intersecting inner crescent arc at w1, w2, w3 etc corresponding to

d1, d2, d3, etc up to d17. Thus giving w1d1,.w2d2,. w3d3,. w4d4,.up to w17d17,.as wear

depths at 17 equally spaced nodes within the wear zone (Figure 5.8). Wear depths

can also be identified by generic term wndn where ‘n’ represents the ‘nth’ node. It

should be noted that on some extreme end nodes the wear depth can be even zero

depending upon the angular extent of the WZW.

Step5: Measure nodal distance

Measure the distance between the two nodes called nodal distances in millimetres for

a 120 0 angle arc.

Figure 5.7 Actual trace of a test bearing with redrawn shape

Computed shape before test

Graduations

Maximum wear depth

CSWA

Inner Crescent Arc

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Step 6: Find out Scale Factor (SF)

Measure the distance between the two grid points of the graduations marked radially

on the enlarged (photocopied) trace. Compare this value with the equipment

manufacturer’s calibrated value for each division (microns/division) for the chosen

magnification and convert the distance between the two grids into scale factor (SF) in

microns/mm.

Figure 5.8 Wear depth measurement at different nodes (wndn)

Inner Crescent Arc

Nodes

w1d1

w17 d17

WD

Out-of-roundness trace

d2

d6

O

d3

D

W d 16

Trace Centre

Outer Crescent Arc

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Table 5.1 Computed maximum wear depth data

Nodes/ wear depth (wndn)

Grid distance mm

(wndn) (µm) A2

(wndn) (µm) A3

(wndn) (µm) A4

(wndn) (µm) A5

(wndn) (µm) A6

(wndn) (µm) A7

1 2.616 0 0 0 0 0 0 2 5.233 2.4 0 2 0 1.5 1 3 7.85 8.8 2 5 3 2.5 5 4 10.466 15.2 6 13 11 5 10 5 13.083 22.4 14 16 16 8 14 6 15.7 30.4 18 21 21 9 16 7 18.316 42.4 23 28 27 10 20 8 20.933 43.2 24 34 29 10 21 9 23.55 41.6 29 35 31 9 22 10 26.166 38.4 28 33 31 7.5 21 11 28.783 30.4 24 36 30 5.5 18 12 31.4 24.8 21 34 29 4 12 13 34.016 18.4 15 29 24 2 5 14 36.633 11.2 7 26 20 1 0 15 39.25 7.2 2 16 11 0 0 16 41.866 3.2 0 10 0 0 0 17 44.483 0 0 0 0 0 0

Step7: Calculate wear depths (wn dn)

Measure wear depths wndn for all ‘n’ number of nodes from the enlarged trace and

multiply them with the scale factor (SF) to convert them into microns. These values

have been recorded in Table 5.1 for all the tests. The values highlighted with bold are

the computed maximum wear depths (WD) recorded from this method.

Step 8: Develop graphs and equations

The distance between the nodes and the corresponding wear depths (wndn) can now

be used for plotting wear profile using Microsoft Excel program. This profile looks

different from the actual out-of-roundness profile because in this case the X-axis is a

straight line representing the inner crescent arc. Furthermore, equations can also be

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developed to represent the outer crescent arc. These equations are discussed in

Section 5.2.3.

Step 9: Calculate CSWA

Develop a suitable numerical method for calculating the area of the wear crescent or

use equations of these curves and find the area between the two curves. Equations

derived for this purpose are discussed in the following section.

5.2.3 Wear Characteristic Equation

The wear depth data obtained from the out-of-roundness traces was used for

representing the outer crescent arc as polynomial equations. The angular

displacement on the inner crescent arc was converted to linear distance in millimetres

as explained in step-8 of the previous subsection.

These wear depths were treated as independent variable and a graph between the

linear distance and the wear depths were plotted with the help of Microsoft Excel

program. Add Trend Line Function of the Excel program gave the best fit curve as

well as the equation of the curve. The equations developed for these best fit curves

are called “Wear Characteristic Equations (WCE)” and were developed for all the six

test conditions using wear depth data shown in Table 5.1.

Best fit curves and their corresponding WCE for Test A2 and A3 are given in Figure

5.9 and 5.10 respectively. In developing these equations and best fit curve the

distance between the nodes is taken in millimetres whereas wear depth is microns.

Polynomial equations of higher order derived to represent the curves the error in

wear depth calculations is minimised.

The magnification of the trace is also very high; the combination of these two factors

minimises the errors in CSWA calculations. These equations also serve as unique

characterisation of an individual antiwear additive, and can be used for deriving the

area under the curve: i.e. CSWA.

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The WCE’s developed for the tests A2 to A7 are given as Equation 5.1 to 5.6

respectively, where y represents the wear depth in microns and X represents the

angular displacement along the bearing circumference, in millimetres.

3774.1178.2499.134.3015.00088.00002.0 23456 ++−+−+−= XXXXXXy (5.1)

64.414.776.2226.00044.0.106.106 2345566 +−+−+−= −− XXXXXxXxy (5.2)

212.013.1123.4822.3627.8903.429.5 23456 +−++−−−= XXXXXXy (5.3)

55.091.628.127.8692.12139.5403.8 23456 +−++−−−= XXXXXXy (5.4)

04.091.1009.7037.4808.1180.1513.3 23456 +−+−−++−= XXXXXXy (5.5)

94.145.32174.4364.285637.9627.13 23456 ++−+−= XXXXXy (5.6)

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Test A2- Wear profiley = -0.0002x6 + 0.0088x5 - 0.1501x4 +

0.9686x3 - 1.4993x2 + 2.1718x - 1.3774

-10

0

10

20

30

40

50

G1 G3 G5 G7 G9G11 G13 G15 G17

Node no

wea

r dep

th m

icro

ns

WDmaxPoly. (WDmax)

Figure 5.9 Wear Characteristic Equation for Test A2

Wear Profile Test A3y = 6E-06x6 - 6E-05x5 + 0.0044x4 -

0.2266x3 + 2.7687x2 - 7.1473x + 4.6425

-505

101520253035

1 3 5 7 9 11 13 15 17Node number

wea

r de

pth

(mic

rons

)

wear profilePoly. (wear profile)

Figure 5.10 Wear Characteristic Equation for Test A3

5.2.4 Area measurement by Newton Cotes method

Several methods can be used to find out the area of an irregular shape. Area of the

wear crescent CSWA can be calculated by any numerical method such as: Simpson’s

Rule, Trapezoidal Rule, etc. for known equally space ordinates. The CSWA can also

be calculated as area between the two curves, i.e the ‘inner crescent trace’ and the

‘outer crescent trace’. The equation of the outer crescent is the WCE derived in the

previous section, and the inner trace arc can be treated as a straight line due its very

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low curvature.

A planimeter can be used to measure the area of an irregular shape; therefore it could

have been used to measure CSWA directly. However, CSWA was calculated by

using a numerical method for known node spacing and wear depths (wndn).

The Newton-Cotes Weisstein (2004) numerical method (an enhanced algorithm of

Simpson’s rule) was used due to simplicity and accuracy. The CSWA was computed

by approximating the integral of a function f(x) using quadratic polynomials (i.e.,

parabolic arcs instead of the straight line segments in the trapezoidal rule). Simpson’s

rule can be derived by integrating the third-order Lagrange interpolating polynomial

fit, Trott (2004), Weisstein (2004) and was used by Allen and Kline (1971) for

micro-fluid analysis. The procedure for deriving the function is explained as below:

Let the function f (x) be tabulated at X0, X1, and X2 equally spaced by distance h.

Then Simpson’s Allen (1971) Rule states that :

∫ ∫+

=2 2

)()(X

Xo

hXo

Xo

dXXfdxxf (5.7)

Τ ( )21431 fffh o ++≈ (5.8)

Since it is derived using quadratic polynomials to approximate functions, Simpson’s

rule actually gives exact results when approximating integrals of polynomials up to

cubic order.

In Equation 5.8

Τ = Cross Sectional Wear Area (CSWA) (mm2)

Δh = Δx or distance between the two nodes (mm)

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f0 = wear depth at the first node (microns)

f1= sum of all the wd’s at odd nodes (i.e. 3,5, 7,……..17)

f2 = sum of all the wd’s at even nodes (i.e. 2, 4, 6…….16)

Thus the wear depth data was substituted in the Equation (5.8) and CSWA values for

all the test cases were calculated. The results of CSWA are reported in Table 5.2.

5.3 Wear Assessment from Out-of-roundness Traces

The wear depth data has been used for computing various wear parameters, such as:

the CSWA, wear depth, wear characteristics equations (WCE), wear volume, and

finally, the weight loss.

Though, each of the above parameters can be used as a wear measure in its own

right, their reliability and practicability need to be adjudged before choosing the best

one for characterising the antiwear additives. Thus each method was compared with

the MWPA technique. However, only two parameters derived from the out-of-

roundness method are comparable to the measured values: computed maximum wear

depth (WD) and computed weight loss (W). Though wear volume is widely used, in

this study it could not be relied upon due to the small dimensional changes caused by

wear. The measured value of maximum wear depth (WDmax) is, similarly less than

ideal, as the wear depth changes abruptly at some points. Thus, computed weight loss

was considered to be the best wear measure parameter, to characterise additives.

Further discussion on these high potential wear parameters is necessary to understand

their utility as well as their limitations.

5.3.1 Maximum wear depth

The ‘measured maximum wear depth’ (WDmax) was determined by using hole-test

gauge as explained in Chapter 3. The ‘calculated maximum wear depth’ (WD) has

been computed from the out-of-roundness traces, which are nothing but the

maximum departure of the surface arch from the original surface arch. In Chapter-4

the maximum change in radial clearance (ΔC) was derived from the change in ID and

OD of the bearing and shaft sleeve respectively, this is theoretically nothing but the

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maximum wear depth (WDmax).

The values of measured maximum wear depth WDmax, maximum wear depth

computed ‘(WD)’ and maximum change in radial clearance (ΔC) for various tests are

given in Table 5.2. These values have also been compared graphically in the bar

chart shown in Figure 5.11.

Figure 5.11 shows that the trend of wear reducing behaviour of different additives is,

by-and-large, similar to that indicated by most of the other techniques. The computed

values are comparable to the change in radial clearance (ΔC) in most of the cases,

though they are lower by as much as 50% in case of Test A6. By and large the

measured maximum wear depth (WDmax) values are higher than 16% the computed

wear depth (WD) values, e.g. Test A4.

For Test A4, the computed and the measured values are quite comparable, as the

maximum variation in case of Test A4 is only 6 microns (Figure 5.11). All the

techniques used for measuring the maximum wear depth (WD) show that the wear

reducing behaviour of antiwear additives is rather similar, the worst performing case

is when there is no additive present in the oil i.e. Test A2 and the best case is Test

A6.

Measurements of the change in radial clearance (ΔC) parameter are not highly

reliable; however, the measurements of the maximum wear depth parameters

(WDmax, and WD) can be relied upon but for some errors if there is high roughness in

the wear zone.

Table 5.2 Comparison of maximum wear depth*

Tests Change in radial clearance (ΔC)

Max. Wear depth measured(WDmax)

Max. Wear Depth computed (WD)

A2 26 42 43.2 A3 17.5 29 29 A4 21 42 36 A5 18 36 31 A6 5.5 12.5 10 A7 7.5 20 22 *All dimensions in microns

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Figure 5.11 Comparison of maximum wear depth

5.3.2 Computed wear volume (V)

The change in wear area is not a widely used wear parameter and hence the CSWA was not

chosen as the wear measure parameter in this research. Wear volume is a very commonly

used wear parameter which can be derived from the CSWA.

Measured values of CSWA are the values of the wear crescent at a given point along

the bearing length (L). If test bearings are perfectly circular and the shaft is perfectly

aligned, the value of CSWA will be the same at all points along the bearing length,

and hence the wear volume can be calculated by multiplying CSWA by the bearing

length. For greater precision the volume should be calculated by taking the aveaged

of the various CSWA values measured along the bearing length (see Section 5.2.1).

However, the wear volume (V) was calculated using Equation 5.9.

LTV .= (5.9)

Where L is the bearing length and T is the higher CSWA value computed at one of

the bearing ends. This gives a more conservative valus for the wear volume, and is

desirable for more robust bearing design.

Though it may be complex to measure the wear volume of the wear crescent form

Maximum wear depth comparison

0 10 20 30 40 50

A1 A2 A3 A4 A5 A6 A7Tests

Wea

r de

pth

(mic

rons

)

WDmax measured WD IDmax

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through out the bearing length, It can be possible to develop a measurement

technique similar to Plint and Partner’s pin-on-disc machine used by Sharma (1994)

for wear measurements where a change in diameter of a taper groove formed on the

test bearing can give the wear volume loss in the bearing. However, in current

situation this parameter cannot be compared with any other MWPA technique.

5.3.3 Computed weight loss (W)

Weight loss is considered to be the most straight forward approach of quantifying the

wear in tribological components. However, its measurement with precision is

difficult when wear in the component is too small. The out-of-roundness trace

method is an alternate method of computing the weight loss with minimal errors and

higher precision. Weight loss in a test bearing can be calculated from CSWA by

multiplying it by bearing length and material density or from wear volume by simply

multiplying it by material density.

The out-of-roundness is another wear measure parameter that can be used for

comparing the wear in machine components; however, it cannot quantify wear in

absolute terms and hence cannot be compared with other methods. The wear volume

measured by out-of-roundness method gives better quantification of wear in

bearings. However, the amount of wear cannot be compared with any other MWPA

technique used in this study. Therefore, computation of weight loss from out-of-

roundness trace can be more useful and reliable in comparing or characterising

different antiwear additives.

Weight loss in the bearing can be calculated for the known wear volume and material

density. The density of the bearing material reported in standard handbooks/

literature for bearing material BS LG2500 is 8g/cm3 (Tzeng and Saibel (1967))

(0.008g/mm3). Thus, weight loss (W) is calculated using Equation 5.10.:

ρ..LTW = (5.10)

Where:

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W = computed wear

ρ = material density

L = bearing length

Τ = CSWA

The computed weight loss (W), wear volume (V) and CSWA (Τ) is compared with

the measured weight loss (ΔW) in Table 5.3. The computed weight loss and

measured weight loss results are shown graphically in Figure 5.12, where,

discrepancy in results can be seen for Test A7. This discrepancy clearly indicates the

error in weight loss measurement. The result analysis in Chapter-4 showed that

except roughness, particle count and film thickness all other wear parameters showed

the similar trends of additive wear performing behaviour. However, the only other

parameter that showed discrepancy in results was the Test A7 where only weight loss

was the odd reading and it was suspected that the weight gain may be due to metal

transfer. However, the out-of-roundness method verifies and proves that there was an

error in weight loss measurement.

Table 5.3 Wear Volume

Tests (Additives)

CSWA (T) mm2

Computed Wear Volume ‘V’ (mm3)

Computed weight loss (W), (g)

Measured weight loss Δ Wb , (g)

% change

Test-A2 0.738 29.52 0.236 0.25 -0.06 Test-A3 0.542 21.68 0.173 0.15 o.13 Test-A4 0.747 29.88 0.238 0.17 0.28 Test –A5 0.671 26.84 0.214 0.15 0.3 Test-A6 0.164 6.56 0.052 0.08 -.53 Test-A7 0.471 18.84 0.150 -0.09 1.6

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Figure 5.12 Comparison of computed weight loss and measured weight loss

Results plotted in Figure 5.12 show that the computed values are either higher than

the measured values, or are close to each other, except for Test A7. The behaviour is

similar to that shown by other techniques, where best performing additive is A6 and

the worst one is A4. In case of Test A2 and A6 the computed test results are slightly

higher than the measured results.

Since weight loss is one of the universally accepted wear measure parameters, and

furthermore, using out-of-roundness for calculating the weight loss is the most

reliable method, the calculated weight loss is the most suitable parameter for

characterising the antiwear additives.

5.4 Characterisation of Additives

The results obtained from different wear measuring techniques showed that in some

cases the results for different additives are very close to each other. Thus, it is

difficult to distinguish the wear behaviour of one additive from another. Hence, there

is a need to develop a method by which an additive can be identified for its wear

reducing performance with confidence. This goal can be achieved by using a reliable

wear measure parameter correlating it with other operating conditions. After a

Weight loss estimated vs measured

-0.15 -0.1

-0.05 0

0.05 0.1

0.15 0.2

0.25 0.3

A2 A3 A4 A5 A6 A7

Tests

wei

ght l

oss

(mg)

estimated

measured

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thorough review, so far the computed weight loss (W) has been identified as one of

the most reliable wear parameter and was thus used for deriving a number called

wear characteristic number (WCN). This number can be used for identifying an

antiwear additive for its wear reducing performance. The method for deriving WCN

is explained in the following section.

5.4.1 Wear Characteristic Number (N)

Wear coefficient is a well known parameter as explained by Rowe (1986) for

expressing the wear characteristics of a material under lubricated conditions. The

standard relationship amongst material parameters is expressed as:

HWK

lV

= (5.11)

Where:

V =Wear Volume (mm3)

I = sliding distance (m)

W = Normal load (N) or W

H = hardness (N/m2)

K = wear coefficient

A similar approach has been used in this research for characterising the antiwear

additives. For this purpose data has been generated using test conditions by adding

Al2O3 as solid contaminant. Though the tests were run for short duration, the

authenticity of the data has been verified using MWPA, and the out-of-roundness

method. Of the various MWPA techniques, investigated, out-of–roundness method,

prove to be most reliable and precise technique. Though, weight loss is used widely,

the out-of-roundness method for computing the weight loss gave higher precision.

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Wear volume has also been derived from the wear crescent (CSWA). Thus, making

use of these parameters, the Equation 5.11 can be rewritten as:

WlHVN

..

= (5.12)

Where N has been defined as wear characteristic number (WCN or N), V is the

computed volume in mm3, hardness H=1500-1650 kgf/mm2 for Al2O3 and hardness

of bronze is 75 using Rockwell scale B, l is sliding distance in meters and W is the

computed weight loss in mg.

Rowe (1986) attempted to find wear coefficients under lubricated conditions for

some lubricating oils with different viscosities. But these coefficients were calculated

only for clean oils, and no further work has been reported on their implementation.

Following Rowe’s guidelines the additives used in test A2 to A7 were characterised

by their wear coefficients for bronze bearing and steel shaft sleeve pair. The wear

characteristic number (N) obtained from Equation 5.12 for different additives are

given in Table 5.14. Their values vary from 1.1X10 -11 to 9.7X10-12. A higher value

for wear coefficient indicates poor antiwear behaviour of the additive. Additive A6

was found to be the best, with WCN (N) = 3.4XE-12. The highest value of ‘N’ was

obtained with no additive in Test A2, where ‘N’ = 1.5XE-11. The worst performing

additive is A4 with ‘N’ = 1.5XE-11, the same as with no additive. WCN (N) is a

unique number derived from the most reliable wear parameter i.e. CSWA. This

number highlights the wear reducing performance of antiwear additives.

Thus wear characteristic number can be used successfully in identifying the wear

reducing performance of an antiwear additive. The range of this number varies

between from E-11 and E-12; thus the performance can be characterised with

confidence.

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Table 5.4 Wear Coefficients of antiwear additives

Test Rpm (N)

Sliding/distance (l)

Wear volume m3(V)

Wear Characteristic Number (N)

A1 400 7536 0 0 A2 420 7536 1.48E-08 1.52E-11 A3 470 7536 1.08E-08 1.1E-11 A4 400 7536 1.49E-08 1.5E-11 A5 500 7536 1.34E-08 1.4E-11 A6 500 7536 3.30E-09 3.4E-12 A7 500 7536 9.42E-09 9.7E-12

5.5 Discussion on Results

The results obtained for CSWA show that the trend of wear reducing behaviour of

different additives is similar to that shown by other methods except in case of Test

A7. In this test, weight loss (ΔW) measurement results indicate a weight gain of 0.09

mg; whereas; the results obtained from computed weight loss (W) show a weight loss

of 0.15 mg. The weight loss results also highlight the errors in measurements, which

vary from one test to another: -6% in case of test A2, and +28% for Test A4,. -53%

for Test A5. The results confirm the trend of wear reducing behaviour of additives

revealed by most of MWPA techniques such as: measured weight loss, maximum

wear depth measured and computed (WDmax and WD), change in radial clearance

(ΔC), out-of-roundness and particle weight (PCg). This proves that even though the

weight loss measurement methods is considered to be one of the most reliable and

authentic wear measure parameter, it is not suitable for measuring low wear volumes.

The results of computed weight loss (W) indicate that the computed values are in

general higher than the measured values. This is mainly due to reasons that the

CSWA value considered is not the average value which could be achieved by taking

an average of several CSWA values measured on different points along the bearing

length. However, it could be safely concluded that the measured weight loss results

for Test A7 incur an error. Because no other test method supports this phenomenon

including weigh loss computation. Thus reliability of out-of-roundness method is

proved. Similarly a discrepancy in weight loss for Test A5 also shows that this

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may be due to error in measuring weight loss rather than computing weight loss. The

possibility of error in computation is low as discussed earlier, because the wear

reducing trend is similar to most of the MWPA techniques used in this research.

The WCN may still have scope for refinement but this has no bearing on comparing

additives performance, because this is the quantity derived from CSWA and bearing

length which is constant.

Methodology developed for characterising the antiwear additives gives a unique

number (N) as wear coefficient which can help distinguishing the wear reducing

performances of any two antiwear additives. The methodology can be further

modified by better average value of CSWA.

Measured maximum wear depth (WDmax) may have some discrepancies because in

case of maximum change in radial clearance method the measured values also take

into account the wear of shaft sleeve and it is expected that the over all change in

radial clearance is greater than expected. Similarly measurement of wear depth can

also be subjective because within the wear zone, some times the contact is rough in

the tested bearing and it is hard to locate a single location with maximum wear depth.

Which is similar to roughness measurement as discussed in the previous chapter. The

change in radial clearance results indicate that the measurements of ID and OD using

hole-test-gauge may not give desired accuracy because wear depth may be too small

as compared to the radius of the hole-test-gauge stylus.

5.6 Conclusion

Out-of-roundness technique was found to be the most suitable technique for

measuring the wear in test bearings. A methodology was developed where out-of-

roundness traces were used to estimate weight loss, which helped in deriving the

Wear Characteristic Number (N). The best antiwear performance was obtained for

Test A6 where N = 1.4 X 10-12; and the worst case was obtained for Test A2 (without

antiwar additive) where N = 1.52 X 10-11.

The results demonstrated that even though the weight loss measurement is

inherently one of the most reliable wear measure parameters, it may not be suitable

for low wear volumes. The out-of-roundness method for computing the wear

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volume, and weight loss – using the CSWA (cross-sectional wear area) from the

trace – proved to be the most reliable technique.

Precision in computing weight loss (W) can be further improved by measuring the

density of the material as well as bearing length with higher accuracy. Wear

characteristic equations were developed, which can be used to calculate the wear

volume and maximum wear depth, and consequently, derive wear signatures for

individual additives.

Finally, a wear characteristic number (N) was derived; this number is useful for

comparing the efficacy of various antiwear additives. Users as well as manufacturers

of antiwear additives can successfully characterise additives by using the proposed

method. This wear characteristic number (N) can be derived at any independent test

laboratory, and thus, national or international standards organisations can assign

ratings to various antiwear additives to characterise their performance for dusty

applications.

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CHAPTER 6

6. CONCLUSIONS

The main conclusions of this research are presented in this chapter. These

conclusions cover the rational for this research project, knowledge gaps identified

from the literature review, experimental design approach, new knowledge derived

from experimental results and the main contributions of this research to the existing

body of knowledge.

6.1 Problem Statement

This research aimed to investigate the effect of antiwear additives on journal

bearings operating in hydrodynamic conditions. In this research the following three

main aspects have been studied:

a) The effect of contaminants –treated with antiwear additives– on journal bearing

wear.

b) The effect of change in micro-geometry on bearing’s tribological performance.

c) Characterisation of additives using the most suitable wear measuring technique.

The research methodology adopted for this research can be broken into the following

five phases, with matching deliverables:

1. Compare the tribological performance of: a) journal bearings lubricated with

pure base oil, b) base oil containing solid contaminants, and c) oils containing

solid contaminants treated with different antiwear additives.

2. Determine the effect of antiwear additives on wear and micro-geometry of a

journal bearing, operating with lubricants containing solid contaminants.

3. Evaluate different wear measurement techniques for their suitability to

identifying a methodology for characterising the antiwear additives.

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4. Study the effect of micro-geometry on the tribological performance, by

measuring the change in minimum oil film thickness.

5. Characterise antiwear additives using a unique number, and rank them for

their efficacy.

6.2 Literature Review

This research required an in-depth knowledge and literature search in the following

main areas:

• Contaminants’ effect on wear

• Effect of solid contaminants on journal bearings

• Tribological performance and criteria for its measurement

• Micro-geometry parameters and their effect on bearing lubrication

• Antiwear additives and their characterisation

The literature review revealed the following information on different aspects of the

problem that was important for this research project:

Contaminants:

The literature revealed the information about various aspects of contaminants such

as: sources of contaminants, latest ISO 4406 cleanliness requirements, different

multi-body wear mechanisms and modes, advances in micro-polar effects in

lubrication, and information related failures due to contaminants.

‘K’ Ratio:

The literature highlighted the detrimental effects of ‘K’ ratio and its relationship with

wear, friction and embedding of the particles on the journal bearing surfaces.

Maximum wear occurs for K=1, and hence, the effect of antiwear additives has been

studied for this condition.

Hardness Ratio:

Literature on interaction of contaminants with the bearing surfaces gave the insight

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that if the ratio of contaminant hardness to bearing surface hardness is close to three,

it leads to high wear.

Micro-geometry:

The literature research in the area of micro-geometry showed substantial amount of

existing research on roughness effects in both transverse and circumferential

directions; however, this research does not appear to be conclusive, consequently,

‘smooth-is-best’ concept is still widely accepted.

Only limited amount of research has been carried out to study the effect of out-of-

roundness and radial clearance of journal bearings. Out-of-roundness has been

accepted by some researchers as a valid wear measure parameter, however, it has not

been widely used for bearing specification. This research demonstrates that out-of-

roundness measurements are as important as roughness measurements.

Radial clearance has direct impact on the load bearing capacity of a journal bearing;

therefore, this research investigated its impact on oil film thickness.

Measurement techniques:

Meta-research exposed the state-of-art in measurement of oil film thickness and wear

measurement techniques. However, no study highlighted the preference of one

measurement method over the others. Therefore, this research has compared the

suitability of various wear measurement techniques, to select the most suitable one

for characterising antiwear additives.

Antiwear additives:

Literature on antiwear additives discussed mainly their chemistry and applications.

Little information is available on the performance of antiwear additives when used in

bearings containing solid contaminants. This research is thus focused on filling this

knowledge gap.

Characterisation:

Literature search on characterisation of antiwear additives revealed the limited

amount of past research on this topic. The literature found on this topic focused on

characterisation of additives with clean oils in Elastohydrodynamic or concentrated

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contact regimes. A study on the journal bearing wear with oil containing antiwear

additive was also found; however, this study discussed the effect of antiwear

additives on the wear modes and mechanisms only. Therefore, this research included

the development of a model to characterise antiwear additives, particularly for dusty

journal bearings.

Other important areas:

Literature search in allied areas revealed useful information on topics such as:

theoretical modelling of wear performance in worn journal bearings, vibration

monitoring of contaminated bearings, ISO cleanliness and filtration requirements,

and micro-grooved two-component surface layers. Literature review in these areas

helped in identifying appropriate methodologies and techniques used in this research,

and ensuring that this project builds on existing knowledge.

Knowledge Gaps

The literature review revealed the following knowledge gaps in areas relevant to this

research project:

• The effect of solid contaminants treated with antiwear additives on journal

bearing wear has not been fully studied.

• Characterisation of antiwear additives based on their efficacy for dusty

applications under hydrodynamic lubrication has not been carried out.

• The effect of solid contaminants on the bearing micro-geometry and its effect on

the bearing’s tribological performance are not well understood.

• There is no standard numerical parameter for classifying the performance of

antiwear additives operating in dusty hydrodynamic lubrication conditions.

6.3 Experiment Design and Development

Experiment design comprised the road map for the experiment setup and procedures

used in this project, and this led to the development of new practical and theoretical

methodologies for improving bearing design and metrology.

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Test procedures

The experiments were designed for best utilisation of the available resources, which

led to the flowing strategic decisions:

• Conduct short duration test without repeating them.

• Compare the wear measurements obtained from different methods to compare

their accuracy, and select the most reliable method to obtain reliable results.

• Keep testing environment and procedures consistent, because the tests are not

to be repeated.

• Keep K=1, sliding distance = 7536m, and all other operating and

environmental parameters the same.

• Develop a performance parameter selection process based on weight loss,

micro-geometry and particle counts. This process was called Multi Wear

Parameter Approach (MWPA).

Preliminary problems and solutions:

The aims and objectives of this study demanded that micro-geometry parameters are

carefully monitored. This required preliminary measurements of radial clearance,

roughness and roundness measurements prior to wear tests. Further analysis of these

measurements lead to the identification of the following problems, and their

solutions:

• Radial clearance varied from one location to another all along the

circumference of the bearing, mainly due to out-of-roundness; as a result, a

new heuristic was developed: that out-of-roundness must be specified along

with the radial clearance, just as cut-off length is specified with the surface

roughness.

• In this preliminary study, it was observed that roughness values are lower

than the out-of-roundness values, this predicated that the film parameter (λ=

10) does not ensure adequate separation of lubricated surfaces and need

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another design parameter. A new design parameter called Film Shape Factor

(FSF, or gamma ratio) has been defined.

• Film thickness measurement technique using proximity probes require

verification based on theoretical models. This led to the development of a

FORTRAN based program for predicting the bearing performance.

6.4 Results and Analysis

The analysis of results was aimed to determine the effect of each antiwear additive

on the journal bearing. A set of 14 wear measure parameters were used as a part of

the MWPA methodology to identify the most suitable method for characterising the

additives. The following conclusions were drawn from this analysis:

Efficacy of antiwear additives:

The antiwear additive based on sulphur / phosphorous chemistry used in Test A6 has

maximum wear-reducing effect. Whereas, the additive used in Test A4 has almost no

antiwear effect. This fact was supported by seven wear measure parameters.

Weight loss:

Even though weight loss is a direct method for wear measurement, with microscopic

wear, it did not prove to be reliable.

Radial clearance:

There were two reasons for not accepting radial clearance as the best candidate for

measuring wear. First, the radial clearance may change due to change in bearing ID

as well as shaft sleeve OD, and it is difficult to isolate the contribution of each

bearing element. Second, the radial clearance changes within a single rotation from

one location to another. Hence, it is not accurate to assign a single value to this

parameter.

Surface roughness:

There were two problems with roughness measurements, and hence, these could not

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be used for characterising the additives:

• The roughness on both the bearing elements varies randomly (in either

direction), hence, neither the theory of preferential path nor the theoretical

predictions made by other researchers could be confirmed.

• Roughness values vary drastically from one location to another within the

wear zone, hence there is a subjectivity involved in recording the data.

Out-of- roundness:

Out-of-roundness proved to the best micro-geometry parameter; it gave the most

reliable results, and hence was chosen for the characterisation of antiwear additives.

This methodology magnified the departure of circumference from the perfect circle

several thousand times, without magnifying the overall diameter of the bearing,

leading to highly accurate results.

Particle counts and debris weight:

Particle count is a widely used condition monitoring technique; however, due to

heavy contamination, repeatability of test results was poor, and hence was not

suitable. Change in total wear debris weight was not used as a wear measurement

parameter because of inconsistencies in results obtained for the same.

Minimum oil film thickness:

Minimum oil film thickness measurements were reliable when pure base oil results

were compared with the predicted values obtained from the FORTRAN program, or

the on-line ESDU program. However, as the tests proceeded, the contaminant

congestion caused severe fluctuations in readings, thus the results were not reliable.

However, observations demonstrated that K = 1 condition (i.e. contaminate size =

film thickness) causes sever congestion in the bearing contacts.

6.5 Characterisation of Antiwear Additives

The salient features of the method developed for characterising the antiwear

additives, using the out-of-roundness traces, are as follows:

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• The out-of-roundness trace methodology provides a systematic and step-by-

step process for characterising antiwar additives.

• It calculates the area of wear on the out-of-roundness trace at a chosen

bearing cross-section (CSWA). The weight loss calculated from CSWA is

less error prone than physical measurement of these very small quantities.

• The wear depths measured at different angular location along the bearing

circumference give the true geometry of the worn area, and so is the case with

the maximum wear depth.

• Wear characteristic equations developed from the wear depth data give

unique wear performance signature for the antiwear additives. However,

these equations cannot quantify the wear.

• Estimated wear loss from the out-of-roundness traces was used for deriving a

wear characteristic number (N). This number can be used for selecting the

most appropriate antiwear additive for a given dusty application.

6.6 Research Contributions

This research has made the following main contributions to the existing body of

knowledge in this domain:

• This study is first of its own kind where effect of solid contaminates treated

with antiwear additives have been experimentally studied on a journal

bearing.

• A unique method has been developed for computing the microscopic weight

loss in bearings with high precision and reliability using the out-of-roundness

traces.

• A geometrical method has been developed by which oil film thickness can be

measured with higher precision in a bearing where proximity probes are

mounted on a floating bearing housing.

• It is demonstrated that the radius of the bearing changes with the location

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along the circumference, which is mainly due to out-of-roundness, and hence

out-of-roundness should be specified along with the radial clearance –just as

the cut-of length is specified along with surface roughness.

• A seminal concept have been proposed in which the Film Shape Factor (FSF

or gamma ratio) is used for calculating minimum oil film thickness in journal

bearings whose out-of-roundness values are higher than roughness values.

• Wear characteristics equations have been developed with the help of out-of-

roundness traces. These act as signatures of antiwear additive’s wear

behaviour.

• A method for finding Wear Characteristic Number (WCN, or N) has been

developed, and different additives can be ranked for their efficacy based on

this number. Therefore, the users can select the most suitable additive for

their dusty applications by using this number.

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CHAPTER 7

7. SCOPE FOR FUTURE WORK

This research has investigated the effect of antiwear additives on bearings lubricated

with oils containing solid contaminants. Though the main objectives of this project

have been achieved, this research can be advanced in the following directions:

Metrology of the bearings: This research revealed that there is need to study the

effect of the metrology of the bearing under dusty environments. Effects of changes

in oil film thickness due to change in instantaneous radial clearance of a running

bearing need to be studied in more detail, so that its influence on bearing

performance can be better understood.

Film Shape Factor: The proposed Film Shape Factor (γ ratio) is a seminal model,

and needs further research to regiourously test its validity and apply it more widely.

Furthermore, this model can be extended to derived a similar factor for

hydrodynamic thrust bearings – by treating the surface waviness as out-of-

roundness.

Method for finding CSWA: A method for finding CSWA with higher precision

needs to be developed, such as, considering more traces along the bearing length.

Theoretical modelling of worn bearings: A theoretical model should be developed

for predicting minimum oil film thickness in a dynamic system with radial clearance

as a time variant. Such a model would be helpful in developing an expert system for

condition monitoring of machines operating in dusty environments.

Testing of more antiwear additives: A wider variety of antiwear additives should

be tested to characterise these for the benefit of industrial users.

A wider variety of antiwear additives should be tested to characterise them for the

benefit of industrial users.

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Influence of some other parameters: The bearing operating parameters such as ‘K’

ratios, bearing clearances, temperature rise, types of contaminants and their

concentration need to be varied and their effect on bearing wear and tribological

performance be studied in more detail.

A study of reduction in friction due to antiwear additives needs to be pursued, with

regards to energy saving in dusty applications.

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APPENDICES

SUMMARY OF APPENDICES

APPENDIX A- Publications

1. Sharma, S., C. and Hargreaves, D (2001), “Effect of Solid Contaminants on Journal Bearing Performance”, World Tribology Conference, Vienna, pp.1-4

2. Sharma, S. C., Hargreaves, D. and Scott, W., (2004), Influence of Errors in Measuring the Radial Clearance of Journal Bearing Performance. 1st International Conference on Advanced Tribology, Singapore. pp.1

3. Sharma, S., Hargreaves, D., Scott, W., (2008), “Journal bearing metrology and manufacturing issues”, 9th Global Congress on Manufacturing and management (GCMM 2008), 12-14 November 2008, pp (paper accepted).

4. Sharma, S., Hargreaves, D., Scott, W., (2008), “Characterisation of antiwear additives”, 9th Global Congress on Manufacturing and management (GCMM 2008), 12-14 November 2008, pp. (abstract accepted- paper to be published in The Journal of Computational materials and Surface Engineering).

5. Sharma, S., Hargreaves, D., Scott, W. (2008), “Characterisation of additives using out-of roundness traces”, 2nd International Conference on Advance Tribology 2008 (ICAT 2008), 3-5 December 2008, Singapore (paper accepted)

APPENDIX B-Fortran Program

A Fortran program was developed for minimum oil film thickness calculations.

These calculations were used to find out eccentricity at no load condition, and also to

calculate the minimum oil film thickness for ideal conditions when there is no

contaminant mixed with the oil.

APPENDIX C- ESDU output

ESDU OUTPUT: Some examples of theoretical calculations for different test

conditions have been presented. These were acquired using ESDU program 84031

(version 1996). The output gives bearing performance parameters such as: minimum

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oil film thickness, attitude angle, lubricant flow rate etc.

APPENDIX D- Micro-graphs Selected micrographs have been shown for

examining the embedding effect of particles. These micrographs are prepared for

both shaft sleeve as well as journal bearing.

APPENDIX E- Out-of-roundness traces

Selected out-of-roundness traces have been included for demonstrating the effect of

wear and change in roundness of the test bearings. Shaft sleeves have not been

included.

APPENDIX F- Surface roughness traces

Selected surface roughness traces after the tests are presented in the appendix. These

were obtained from Taylor Hobson’s Surtronic 3+ and Talysurf for bearings and

shaft sleeve, in circumferential as well as transverse directions have been shown in

this Appendix. These traces are examples of the roughness in the wear zones of test

bearing elements, and are as close to the average values as possible.

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APPENDIX A- PUBLICATIONS

halla
These articles are not available here.Please consult the hardcopy thesis available from QUT Library
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Abstract accepted: 9th Global Congress on Manufacturing and management (GCMM 2008), 12-14

November 2008

Journal bearing metrology and manufacturing issues

Subhash Sharma*, Doug Hargreaves and Will Scott

School of Systems Engineering, Queensland University of Technology, 2 George St , Brisbane, Australia School of *Aerospace, Mechanical and Manufacturing Engineering, RMIT University, Melbourne3001, email: [email protected]

Abstract:

Journal bearings lubricated with oils containing solid contaminants are subjected to

malfunctioning and can cause premature failures. The malfunctioning of machines

results in poor quality output and premature failures, leading to increased downtime.

In an experimental study of journal bearing lubrication, the radial clearance in a

bearing was measured. The investigation revealed that the radial clearance varies

along the periphery of the bearing. This clearance varies so much so that the small

solid particles of the size of the minimum oil film thickness in the bearing contact

can trap and hamper the performance of a machine and reduce the bearing life. Thus

the metrology of bearing clearance measurement, manufacturing process and the

procedures for bearing design need to be reviewed, if a bearing is subjected to

contaminated environment. A simply statement that the hydrodynamic bearings

should operate on lambda ratio 10 is not enough.

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Abstract accepted: 9th Global Congress on Manufacturing and management (GCMM 2008), 12-14

November 2008

Characterisation of additives using out-of-roundness traces

Subhash Sharma*, Doug Hargreaves and Will Scott

School of Systems Engineering, Queensland University of Technology, 2 George St , Brisbane, Australia School of *Aerospace, Mechanical and Manufacturing Engineering, RMIT University, Melbourne3001, email: [email protected]

ABSTRACT:

In a tribological study, out-of-roundness traces have been used for characterising the

antiwear additives. Wear tests have been conducted on a journal bearing and wear in

bearings was estimated using out-of-roundness traces. The study showed that the

Talyrond instrument can be successfully used for studying the wear performance of a

bearing. This study has been further extended, and antiwear additives used for

treating the solid contaminants contained in the lubricating oils were characterised

for their wear performance. Wear characteristic numbers have been derived for some

additives using out-of-roundness traces. At present, there are various types of

antiwear additives available in the market and their manufacturers claim high about

their efficacy without any substantial proof. The proposed wear characteristic

numbers can be useful in selecting the most appropriate additive for applications

where bearings are exposed to solid contaminants.

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Characterisation of antiwear additives

Subhash Sharma*, Doug Hargreaves and Will Scott School of Systems Engineering, Queensland University of Technology, 2 George St , Brisbane, Australia School of *School of Aerospace, Mechanical and Manufacturing Engineering, RMIT University, Melbourne3001, email: [email protected] KEY WORDS: Journal bearing, antiwear additives, out-of-roundness, contaminants, wear ABSTRACT In this tribological study, out-of-roundness traces have been used for characterising antiwear additives. Wear tests have been conducted on a journal bearing and wear depth has been computed from the out-of-roundness traces obtained before and after the wear tests on a bronze journal bearing. The traces give wear depth at different locations and also the maximum wear depth in the bearing. The wear depth results computed from this method have been compared with the measured values and were found a good comparison. Wear characteristic Equations have been derived from this data which gives unique wear signature of wear reducing behaviour of an additive. INTRODUCTION: Use of Antiwear additives is very common in machines operating in dusty environments. There are several products available in the market and manufacturers make unsubstantiated claims about efficacy of their products. There is a need for a tool by which a user can rank these products for their efficacy and choose one that suits his requirements. Journal bearings are worst affected bearing component There are very few studies carried out on the bearings operating with oils containing solid contaminants treated with antiwear additives. Some studies have been carried in this area without using antiwear additives (Mckee, 1927, Roach and Mich, 1950, Elwell, 1977, Duchowski, 1998, Maru 2006). The objectives of their studies were different such as: to study the wear modes, embedding of particles, friction. In a recent study on journal bearing wear with contaminants treated with antiwear additives was carried by Maru et.al. (2006) but his main concern was to study the wear modes and mechanisms. Rowe (1986) determined the coefficient of wear for some antiwear additives using a four-ball test machine and clean oils. Thus there is a need to conduct experiments aimed to study the effect of antiwear additives on bearings operating with oils containing solid contaminants and find a method by which efficacy of these additives could be adjudged. It is difficult to measure small quantities of wear in journal bearings directly, with precision especially when lubricated bearings are dust laden. This study deals with wear tests under the said conditions, where a method has been developed to characterise the antiwear additives using out-of roundness traces of the journal bearings. Using this method Method: Wear tests were conducted on a journal bearing test rig keeping the same operating conditions and specifically the sliding distance 7536 m and ‘K’ ratio (minimum film thickness to particle size ratio) close to 1. Aluminium oxide Al2O3 of 16 microns size was chosen for this study. The wear tests were run on a journal bearing tests rig where a bronze bearing of 40 mm diameter and L/D ratio equal to one was used. The bearing shaft was made of steel sleeve. The out-of-roundness traces were prepared before and after the tests as shown in Figure 1a and b. Wear depths in the wear zone were computed from these traces and their values were compared with the measured values. The process has been shown graphically in Figure 2a and 2b and has been described step-by-step as below: Steps1) Prepare two out-of-roundness traces of a journal bearing i.e. before and after the wear tests (Figure 1 a and b) respectively). Step2) Enlarge both the traces to a suitable magnification (same magnification) and superimpose them. Step 3) Mark the wear zone, by labelling inner crescent and outer crescent, Step 4) mark the probable Trace centre (O) and mark the longest distance point on outer crescent D Step 5) Draw a line from the trace centre ‘O’ to the outer crescent such that it is the longest distance point at the outer crescent mark this point D and mark point W where it intersects the inner crescent, giving WD as maximum wear depth WD. Step 6) Locate point D1 and w17 on either side of D at 60 degree angular displacement either sides respectively, and so the w 1 to w 17 on the inner

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Graduations marked

magnified traces convert the marked division in microns per millimetre called Scale Factor (SF). Thus record the wear depth at each node. As reported in Table 1.

a) b) Figure 5.4 Out-of-roundness traces a) before wear test b) after wear test

Figure 2a Actual trace of a test bearing with redrawn shape

Discussion: The results show that there is a variation up to 20 %. The measurements with hole-test-gauge showed that it is difficult to locate the location of wear depth manually. This becomes even harder when wear quantity is too small. Traces clearly indicate the wear zone even when the wear depth is too small. This is mainly due to the property of out-of-roundness measurement equipment which amplifies the departure of bearing circumference without amplifying the overall dimensions of the work piece. Though the magnification on Talyrond equipment is limited it was further enhanced while photocopying the traces. Thus the computed values of wear depths are more precise than the measured values from conventional devices.

Inner Crescent Arc

Nodes

w1d1

w17 d17

WD

Out-of-roundness trace

d2

d6

O

d3

D

W

w 2

d 16

Trace Centre

Outer Crescent Arc

Computed shape before test

Graduations

Max. wear depth

CSWA

Inner Crescent Arc

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Figure 2b Graphical representation of out-of-roundness trace method

Results:The wear depth data is recoded in Table 1.

Table 1. Computed maximum wear depth data Nodes/ wear depth (wndn)

Grid distance mm

(wndn) (µm) A2

(wndn) (µm) A3

(wndn) (µm) A4

(wndn) (µm) A5

(wndn) (µm) A6

(wndn) (µm) A7

1 2.616 0 0 0 0 0 0 2 5.233 2.4 0 2 0 1.5 1 3 7.85 8.8 2 5 3 2.5 5 4 10.466 15.2 6 13 11 5 10 5 13.083 22.4 14 16 16 8 14 6 15.7 30.4 18 21 21 9 16 7 18.316 42.4 23 28 27 10 20 8 20.933 43.2 24 34 29 10 21 9 23.55 41.6 29 35 31 9 22 10 26.166 38.4 28 33 31 7.5 21 11 28.783 30.4 24 36 30 5.5 18 12 31.4 24.8 21 34 29 4 12 13 34.016 18.4 15 29 24 2 5 14 36.633 11.2 7 26 20 1 0 15 39.25 7.2 2 16 11 0 0 16 41.866 3.2 0 10 0 0 0 17 44.483 0 0 0 0 0 0

These wear depths were also measured (WDmax) using hole-test-gauge the results have been reported and compared graphically in Figure 2.

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APPENDIX –B BEARING FORTRAN PROGRAM

C PROGRAM WORN BEARING PERFORMANCE (HRWD1)

C ****************************************************************

C *MODIFIED WEAR DEPTH ADDED AT EACH GRID

C * THIS PROGRAM IS FOR AXIAL BEARING IT CALCULATES FILM THICK *

C * BY PRESUMING EE=0.01 AND COMPARES LOAD CALCULATED AND APPLIED*

C *BY INCRESING EE VALUE IN STEPS. FILM THICKNESS IS MODIFIED BY *

C * INCORPORATING WEAR PROFILE EQUATION DEVELOPED IMERICALLY *

C ****************************************************************

REAL C,ETA,WR,EE,AR,AL,WB,WW,ORF

INTEGER N,M,WA,AN

DIMENSION P(50,20), H(50),C1(50),C2(50),C3(50),F1(20),F2(20)

C DIMENSION WD(50), THW(50)

C INPUT: N= 46 THETA & M=9 IN Z DIRECTION'

C NORMALLY C=0.000080 METERS, WA=500N,AN=500RPM

C READ (5,*)N,M,C,WA,AN

WRITE(6,*)'INPUT DATA: N,M,C,WA,AN,ETA'

READ (5,*)N,M,C,WA,AN,ETA

C OVERRELAXATION FACTOR,ORF=1.3 IN GENERAL WR=0 STATIC BRG

C R IS L/D RATIO = 1

R=1.0

C CHANGE ETA IF FILON CASE

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C ETA=0.042

ORF=1.3

EE=0.01

WR=1.0

C CALCULATE NON DIM. LOAD

c LENGTH OF BEARING IS L=40MM, AR IS THE RADIUS =20MM=AL/2

AL=0.040

AR=AL/2.

C NON DIEMSIONAL BEARING CHARACTERISTIC NUMBER HAMROCK

PI=4.*ATAN(1.)

C WW=(1.6*WA*C**2)*6/(ETA*AL*AN*AR**3)

C BEARING SPEED WB IN RADIANS PER SECOND

WB=2.*PI*AN/60.

WRITE (6,*)'WB=',WB

WRITE (6,*)'AN=',AN

WW=WA/(ETA*WB*AL*AR*(AR/C)**2)

WRITE (6,*)'WW=',WW

DEE=0.0

DPHII=0.0

RR=(1./R)**2

C GRID NUMBERING

I5=N

I6=I5+1

I4=I5-1

I3=I4-1

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AI3=I3

PI=4.*ATAN(1.)

C GRID SPACING DEL= 2*PI/46-2 IN RADIANS, DELZ=M/9-2

C SINCE ONE GRID WILL BE OVERLAPPED

DEL=2.*PI/AI3

DELZ=1./AJ3

DEL2=DEL**2

DELZ2=DELZ**2

C WRITE(6,*)'AI3=',AI3,'AJ3=',AJ3,'DEL=',DEL,'DELZ=',DELZ

C INITIALIZATION OF PRESSURE

100 DO I=1,I6

DO J=1,J6

P(I,J)=0.0

ENDDO

ENDDO

ITER=1

SPO=0.0

DO I=1,I5

DO J=1,J5

SPO=SPO+P(I,J)

ENDDO

ENDDO

CO=RR*(DEL2/DELZ2)

DO I=1,I5

AI=I-2

THETA=AI*DEL

H(I)=1.+EE*COS(THETA)

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C1(I)=(3.*EE*SIN(THETA)*DEL)/(2.*H(I))

C2(I)=(6.*EE*SIN(THETA)*DEL2)*(1.-2.*WR*DPHII)/(H(I)**3)

C3(I)=(12.*WR*DEE*COS(THETA)*DEL2)/(H(I)**3)

ENDDO

C++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++

C WRITE(6,*)C1(I),C2(I)

C WEAR DEPTH CALCULATIONS

C DO I=IWS,IWF

C THETA=(I-2)*DEL

C THW=(I-IWS)*DEL

C X=THW

C ESTEROL WEAR DEPTH EQUATION

C 20 GRID SECOND SIXTH ORDER WEAR EQUATION FOR TEST A7

C WD=((-11.458*X*X+26.095*X-4.3477)*0.000001)/C

C 20 GRID SIXTH ORDER WEAR EQUATION FOR TEST A7

C WD=(13.276*X**6-96.637*X**5+285.4*X**4-436.74*X**3

C /+321.45*X**2-52.569*X+1.9385)*1000000/C

C H(I)=1.+EE*COS(THETA)-WD

C +++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++

C " FILM THICKNESS WITH WD ADDED AT EACH NODE"

C ADDITIVE /TEST NUMBER

IF (H(I).GE. H(16))THEN

H(16)=H(16)+0.0

H(17)=H(17)+0.0

H(18)=H(18)+2*1.0E-06/C

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H(19)=H(19)+4*1.0E-06/C

h(20)=H(19)+6*1.0E-06/C

H(21)=H(19)+8*1.0E-06/C

H(22)=H(19)+10*1.0E-06/C

H(23)=H(19)+12*1.0E-06/C

H(24)=H(19)+14*1.0E-06/C

H(25)=H(19)+12*1.0E-06/C

H(26)=H(19)+10*1.0E-06/C

H(27)=H(19)+8*1.0E-06/C

H(28)=H(19)+6*1.0E-06/C

H(29)=H(19)+4*1.0E-06/C

H(30)=H(19)+2*1.0E-06/C

H(31)=H(19)+0.0

H(32)=H(19)+0.0

ENDIF

C1(I)=(3.*EE*SIN(THETA)*DEL)/(2.*H(I))

C2(I)=(6.*EE*SIN(THETA)*DEL2)*(1.-2.*WR*DPHII)/(H(I)**3)

C3(I)=(12.*WR*DEE*COS(THETA)*DEL2)/(H(I)**3)

IF (H(I) .GE. H(33)) THEN

H(I)=1.+EE*COS(THETA)

ENDIF

C1(I)=(3.*EE*SIN(THETA)*DEL)/(2.*H(I))

C2(I)=(6.*EE*SIN(THETA)*DEL2)*(1.-2.*WR*DPHII)/(H(I)**3)

C3(I)=(12.*WR*DEE*COS(THETA)*DEL2)/(H(I)**3)

C WRITE (6,*)H(15),H(16),H(24),H(26),H(32),H(33),H(36)C

C WRITE(6,*)C1(18),C2(18)

C OPEN(55,FILE='HWEAR AREA.DAT')

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C WRITE(55,555)(H(I),I=1,47)

C555 FORMAT(2X,8F8.2)

500 DO I=1,I6

P(I,1)=P(I,3)

ENDDO

DO J=2,J4

DO I=2,I4

TERM=(P(I+1,J)+P(I-1,J)+CO*(P(I,J+1)+P(I,J-1))

/-C1(I)*(P(I+1,J)-P(I-1,J))+C2(I)-C3(I))/(2.*(1.+CO))

ERR=TERM-P(I,J)

P(I,J)=P(I,J)+ORF*ERR

IF (P(I,J) .LT. 0.0)P(I,J)=0.0

IF (I.EQ.2) GO TO 101

IF (I .EQ.I4) Go TO 102

GO TO 50

101 P(I5,J)=P(2,J)

GO TO 50

102 P(I,J)=P(I4,J)

50 ENDDO

ENDDO

C ++++++++++ AXIAL GRROVE CONDITION++++++++++

C DO I=26,29

C DO J=2,7

C P(I,J)=101.3*c**2*60.0/(ETA*AR**2*31.4*AN)

C WRITE (6,*)'XP(I,J)=', P(26,2),P(29,7)

C P(I,J)=0.123

c P(I,J)=1.0

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c ENDDO

c ENDDO

c WRITE (*,*)P(26,2),P(28,3),P(29,7)

C +++++++ UPTO THIS POINT MODIFICATIONS+++++++++

C TEST FOR CONVERGENCE

SPN=0.0

DO I=1,I5

DO J=1,J5

SPN=SPN+P(I,J)

ENDDO

ENDDO

ERR=1.-SPO/SPN

IF(ABS(ERR) .LE. 0.01) GO TO 400

SPO=SPN

ITER=ITER+1

GO TO 500

400 SPO=SPN

C WRITE(6,7) ((P(I,J),I=1,I5),J=1,J5)

C7 FORMAT(1X,8F10.3/)

C OPEN(51,FILE='PRESSURE1.DAT')

C DO I=2,I5

C WRITE(51,52)I,P(I,2)

C52 FORMAT(I3,1X,E10.3)

C ENDDO

C EVALUATION OF LOAD BEARING CAPACITY

DO J=2,J6

F1(J)=0.0

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F2(J)=0.0

DO I=2,I3,2

AI=I-2

TH1=AI*DEL

TH2=(AI+1.)*DEL

TH3=(AI+2.)*DEL

TERM1=P(I,J)*COS(TH1)+4.*P(I+1,J)*COS(TH2)+P(I+2,J)*COS(TH3)

TERM2=P(I,J)*SIN(TH1)+4.*P(I+1,J)*SIN(TH2)+P(I+2,J)*SIN(TH3)

F1(J)=F1(J)+TERM1*DEL/3.

F2(J)=F2(J)+TERM2*DEL/3.

ENDDO

ENDDO

WX=0.0

WY=0.0

DO J=2,J4,2

TERM1=F1(J)+4.*F1(J+1)+F1(J+2)

TERM2=F2(J)+4.*F2(J+1)+F2(J+2)

WX=WX+TERM1*DELZ/3.

WY=WY+TERM2*DELZ/3.

ENDDO

W=SQRT(WX*WX+WY*WY)

IF (W.GE.WW) THEN

GO TO 200

ELSE

EE=EE+0.01

GO TO 100

ENDIF

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200 ATT=-ATAN(WY/WX)*180/PI

DO I=1,I5

AI=I-2

THETA=AI*DEL

H(I)=(1.+EE*COS(THETA))*C*1000000.0

ENDDO

C OPEN(52,FILE='OPERATING DATA.DAT')

C WRITE(52,4)

C 4 FORMAT(10X,'l/D',5X,'E',7X,'W',8X,'PHI'/)

C WRITE(52,3)R,EE,WW,ATT

C WRITE (52,3)R,EE,WW,ATT,WA

C 3 FORMAT(2X,F7.2,1X,F8.5,F9.5,F10.5,F5.2/)

OPEN(51,FILE='FILMTHICKNESS.DAT')

WRITE(51,111)

111 FORMAT(2X,'NAME OF THE ADDITIVE.....')

WRITE(51,112)

112 FORMAT(2X,'WA',7X,'AN',6X,'EE',6X,'WW',6X,'PHI'

/,5X,'ETA',5X,'L/D',5X,'C'/)

WRITE(51,113)WA,AN,EE,WW,ATT,ETA,R,C

113 FORMAT(1X,F6.1,4X,F6.1,3X,F6.4,2X,F6.2,2X,F6.2,

/2X,F6.2,4X,F3.1,4X,F7.6)

WRITE(51,7)(H(I),I=1,47)

C7 FORMAT(1X,8E12.3)

WRITE(51,8)(P(I,2),I=1,46)

7 FORMAT(1X,F8.2)

8 FORMAT(2X,F14.6)

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C OPEN(52,FILE='INPUT DATA.DAT')

C WRITE(52,8)

C 8 FORMAT(4X,'LOAD',5X,'SPEED',5X,'VISCOSITY',5X,'NDLOAD'/)

C WRITE(52,9)WA,AN,ETA,WW

C 9 FORMAT(4X,F6.2,1X,F8.2,1X,F10.4,1X,F10.3//)

WRITE(6,*) 'WW=',WW

STOP

END

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APPENDIX –C EXAMPLES OF ESDU BEARING OUTPUT

ESDU A9305

* Example 1 of Item 84031 * ~~~~~~~~~~~~~~~~~~~~~~~ * Two bearings are required to support the weight of the rotor of an * electric motor. The load on each bearing is 38 kN under both start- * up and running conditions. It is anticipated that the rotor would * be started and stopped once each day. The rotor has a steel journal * 0.25 m diameter and rotates unidirectional at 6.67 rev/s (400 rev/min). * The shaft angular deflection is calculated to be 2.0E-4 rad at the * bearing. Space limitations restrict the maximum width of the bearing * to 0.25 m. It is assumed that the feed temperature will be 40 deg C * and the feed pressure 1.0E5 N/m^2 (1 bar). lubDat name of lubricant database = MIN.DAT lubID lubricant identifier = VG46 Tf lubricant feed temperature = 40.0 deg C Pf lubricant feed pressure = 1.0E5 N/m^2 d diameter of journal = 0.04 m b axial length of bearing = 0.04 m a groove axial length = 0.036 m wg circumferential width of lubricant groove = 0.01 m Cd diametral clearance (minimum case) = 160E-6 m

N frequency of rotation of journal = 6.66

rev/s

W running load on bearing = 500 N Ws start-up load on bearing = 500 N beta angular misalignment = ? rad � Plain Text Attachment [ Download File | Save to my Yahoo! Briefcase ] ---------------------------------------------------------------------- ESDU International plc. PROGRAM A9305 ESDUpac Number: A9305

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ESDUpac Title: Calculation methods for steadily loaded,

axial groove hydrodynamic journal bearings Data Item Number: 93005 Data Item Title: Calculation methods for steadily loaded, axial groove hydrodynamic journal bearings (Guide to use of computer program A9305). ESDUpac Version: 1.1, June 1996. (See Data Item for full input/output specification and interpretation) ---------------------------------------------------------------------- Name of input data file EXP1_SHARMA.IN INPUT DATA ~~~~~~~~~~ * Example 1 of Item 84031 * ~~~~~~~~~~~~~~~~~~~~~~~ * Two bearings are required to support the weight of the rotor of an * electric motor. The load on each bearing is 38 kN under both start- * up and running conditions. It is anticipated that the rotor would * be started and stopped once each day. The rotor has a steel journal * 0.25 m diameter and rotates unidirectionally at 6.67 rev/s (400 rev/min). * The shaft angular deflection is calculated to be 2.0E-4 rad at the * bearing. Space limitations restrict the maximum width of the bearing * to 0.25 m. It is assumed that the feed temperature will be 40 deg C * and the feed pressure 1.0E5 N/m^2 (1 bar). lubDat name of lubricant database = MIN.DAT lubID lubricant identifier = VG46 Tf lubricant feed temperature = 40.0 deg C Pf lubricant feed pressure = 1.0E5 N/m^2 d diameter of journal = 0.04 m b axial length of bearing = 0.04 m a groove axial length = 0.036 m wg circumferential width of lubricant groove = 0.01 m Cd diametral clearance (minimum case) = 160E-6 m N frequency of rotation of journal = 6.66 rev/s W running load on bearing = 500 N

Ws start-up load on bearing = 500 N

beta angular misalignment = ?

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rad OUTPUT DATA ~~~~~~~~~~~ LUBRICATION SYSTEM ~~~~~~~~~~~~~~~~~~ Lubricant database : MIN.DAT Lubricant description: ISO VG 46 mineral oil rho density of lubricant = 0.850 E+03 kg/m^3 rhoC volumetric heat capacity = 1.70 E+06 J/m^3 K kappa thermal diffusivity of lubricant = 80.0 E-09 m^2/s Pf lubricant supply pressure = 0.100 E+06 N/m^2 Tf lubricant supply temperature = 40.0 deg C BEARING DIMENSIONS ~~~~~~~~~~~~~~~~~~ d diameter of journal = 40.0 E-03 m b axial length of bearing = 40.0 E-03 m Cd diametral clearance = 0.160 E-03 m a axial length of lubricant groove = 36.0 E-03 m wg circumferential width of groove = 10.0 E-03 m dg recommended minimum groove depth = 3.20 E-03 m bdRat bearing length to diameter ratio = 1.00 CdRat diametral clearance ratio = 4.00 E-03 abRat groove length to bearing length ratio = 0.900 theta angular extent of lubricant groove = 28.6 deg OPERATIONAL PARAMETERS ~~~~~~~~~~~~~~~~~~~~~~ Default values have been assigned to the unspecified operational parameters. N frequency of shaft rotation = 6.66 rev/s W applied load = 0.500 E+03 N Ws load at start-up = 0.500 E+03 N Prun specific loading for running load = 0.313 E+06 N/m^2 Pstart specific loading for start-up load = 0.313 E+06 N/m^2 beta angular misalignment = 0.00 rad RESULTS OF ANALYSIS ~~~~~~~~~~~~~~~~~~~ Re bearing Reynolds number = 1.49

ReCrit critical Reynolds number = 0.809 E+03

NOTE: Bearing lubricant flows are laminar.

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Results of laminar flow analysis ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ Q lubricant flow rate into bearing = 3.02 E-06 m^3/s H power loss = 2.61 W Tmax bearing maximum temperature = 40.6 deg C Tout lubricant outlet temperature = 40.2 deg C eccRat eccentricity ratio (for aligned bearing) = 0.794 psi attitude angle = 30.6 deg hmin minimum film thickness (at edge of bearing) = 16.5 E-06 m hs safe allowable minimum film thickness = 4.28 E-06 m Ra recommended maximum surface roughness value = 0.55 E-06 m ---------------------------------------------------------------------- ***Normal end Plain Text Attachment [ Download File | Save to my Yahoo! Briefcase ] ESDU A9305 * Example 1 of Item 84031 * ~~~~~~~~~~~~~~~~~~~~~~~ * Two bearings are required to support the weight of the rotor of an * electric motor. The load on each bearing is 38 kN under both start- * up and running conditions. It is anticipated that the rotor would * be started and stopped once each day. The rotor has a steel journal * 0.25 m diameter and rotates unidirectionally at 6.67 rev/s (400 rev/min). * The shaft angular deflection is calculated to be 2.0E-4 rad at the * bearing. Space limitations restrict the maximum width of the bearing * to 0.25 m. It is assumed that the feed temperature will be 40 deg C * and the feed pressure 1.0E5 N/m^2 (1 bar). lubDat name of lubricant database = MIN.DAT lubID lubricant identifier = VG46 Tf lubricant feed temperature = 40.0 deg C Pf lubricant feed pressure = 1.0E5 N/m^2

d diameter of journal = 0.04 m b axial length of bearing = 0.04 m a groove axial length = 0.036 m wg circumferential width of lubricant groove = 0.01 m Cd diametral clearance (minimum case) = 178E-6 m N frequency of rotation of journal = 8.33 rev/s W running load on bearing = 500 N Ws start-up load on bearing = 500 N beta angular misalignment = ? rad

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Plain Text Attachment [ Download File | Save to my Yahoo! Briefcase ] ---------------------------------------------------------------------- ESDU International plc. PROGRAM A9305 ESDUpac Number: A9305 ESDUpac Title: Calculation methods for steadily loaded, axial groove hydrodynamic journal bearings Data Item Number: 93005 Data Item Title: Calculation methods for steadily loaded, axial groove hydrodynamic journal bearings (Guide to use of computer program A9305). ESDUpac Version: 1.1, June 1996. (See Data Item for full input/output specification and interpretation) ---------------------------------------------------------------------- Name of input data file EXP1_HT_SHARMA89.IN INPUT DATA ~~~~~~~~~~ * Example 1 of Item 84031 * ~~~~~~~~~~~~~~~~~~~~~~~ * Two bearings are required to support the weight of the rotor of an * electric motor. The load on each bearing is 38 kN under both start- * up and running conditions. It is anticipated that the rotor would * be started and stopped once each day. The rotor has a steel journal * 0.25 m diameter and rotates unidirectionally at 6.67 rev/s (400 rev/min). * The shaft angular deflection is calculated to be 2.0E-4 rad at the * bearing. Space limitations restrict the maximum width of the bearing * to 0.25 m. It is assumed that the feed temperature will be 40 deg C * and the feed pressure 1.0E5 N/m^2 (1 bar). lubDat name of lubricant database = MIN.DAT lubID lubricant identifier = VG46 Tf lubricant feed temperature = 40.0 deg C Pf lubricant feed pressure = 1.0E5 N/m^2 d diameter of journal = 0.04 m b axial length of bearing = 0.04 m a groove axial length = 0.036 m wg circumferential width of lubricant groove = 0.01 m Cd diametral clearance (minimum case) = 178E-6 m

N frequency of rotation of journal = 8.33

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rev/s

W running load on bearing = 500 N Ws start-up load on bearing = 500 N beta angular misalignment = ? rad OUTPUT DATA ~~~~~~~~~~~ LUBRICATION SYSTEM ~~~~~~~~~~~~~~~~~~ Lubricant database : MIN.DAT Lubricant description: ISO VG 46 mineral oil rho density of lubricant = 0.850 E+03 kg/m^3 rhoC volumetric heat capacity = 1.70 E+06 J/m^3 K kappa thermal diffusivity of lubricant = 80.0 E-09 m^2/s Pf lubricant supply pressure = 0.100 E+06 N/m^2 Tf lubricant supply temperature = 40.0 deg C BEARING DIMENSIONS ~~~~~~~~~~~~~~~~~~ d diameter of journal = 40.0 E-03 m b axial length of bearing = 40.0 E-03 m Cd diametral clearance = 0.178 E-03 m a axial length of lubricant groove = 36.0 E-03 m wg circumferential width of groove = 10.0 E-03 m dg recommended minimum groove depth = 3.56 E-03 m bdRat bearing length to diameter ratio = 1.00 CdRat diametral clearance ratio = 4.45 E-03 abRat groove length to bearing length ratio = 0.900 theta angular extent of lubricant groove = 28.6 deg OPERATIONAL PARAMETERS ~~~~~~~~~~~~~~~~~~~~~~ Default values have been assigned to the unspecified operational parameters. N frequency of shaft rotation = 8.33 rev/s W applied load = 0.500 E+03 N Ws load at start-up = 0.500 E+03 N

Prun specific loading for running load = 0.313 E+06

N/m^2

Pstart specific loading for start-up load = 0.313 E+06 N/m^2 beta angular misalignment = 0.00

rad

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RESULTS OF ANALYSIS ~~~~~~~~~~~~~~~~~~~ Re bearing Reynolds number = 2.09 ReCrit critical Reynolds number = 0.766 E+03 NOTE: Bearing lubricant flows are laminar. Results of laminar flow analysis ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ Q lubricant flow rate into bearing = 4.19 E-06 m^3/s H power loss = 3.63 W Tmax bearing maximum temperature = 40.9 deg C Tout lubricant outlet temperature = 40.2 deg C eccRat eccentricity ratio (for aligned bearing) = 0.793

psi attitude angle = 30.6

deg hmin minimum film thickness (at edge of bearing) = 18.4 E-06

m

hs safe allowable minimum film thickness = 4.28 E-06 m

Ra recommended maximum surface roughness value = 0.55 E-06 m

---------------------------------------------------------------------- ***Normal end

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APPENDIX-D MICROGRAPHS (SURFACE IMAGES)

Figure D-A1.1Bearing before Test A1 Figure D-A1.2 Bearing after Test A2X20

Figure D-A1.3 Bearing after Test A2 X50 Figure D- A1.4 Sleeve after test A2 X20

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Figure D A1.5 Sleeve before test A1 Figure D A1.6Sleeve after Test A1

Figure D- A17 Sleeve Before Test A2 X10 Figure D-A1.8 Sleeve after Test A2 X50

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FigureD- A3 Bearing before Test Figure D-A3.3 Bearing after Test A3 X20

Figure D A3.3 Bearing after Test A3 X50 Figure D A3.4 Sleeve after Test A3 (edge unworn)

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Figure D A4.1 bearing after Test A4 X10 Figure D A4.2 earing after Tets A3X50

Figure D A4.3 Sleeve after wear X10 Figure D A4.4 Sleeve afre Test A4 X50

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Figure D A5.1. bearing after wear X20 Figure D A5.2Bearing after test A5 X 50

Figure D A5.3. Sleeve before Test A5 Figure D A5.4 Sleeve after Test A5 X 40

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Figure D A6.1 bearing after Test A6X10 Figure D A6.2 Bearing after Test A6X40

Figure D-A6.3 sleeve after Test A6 Figure D A5.1Sleeve after Test A6 X40

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Figure D A7.1 Bearing after Test A7 X20 Figure D A7.2 Bearing after Test 7X100

Figure D7 A7.3 Sleeve after Test A7 Figure D 7.4 Sleeve after Test A7 X 40

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APPENDIX-E OUT–OF–ROUNDNESS TRACES

Figure E- A1.1 OR before Test A1

Figure E –A2.1 OR before Test A2/ after Test A1

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Figure E. A2.2 OR After Test A2

Figure E. A3.1 OR before Test A3

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Figure E. A3.2 OR after Test A3

Figure E. A4.1 OR before Test A4

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Figure E. A4.2 OR after Test A4

Figure E A5.1 OR before Test A5

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Figure E A5.2 OR after Test A5

Figure E.A6.1 Before Test A6

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Figure E. A6.2 OR after Test A6

Figure E. A6.3 Shaft sleeve OR before Test A6

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Figure E. A6.4 Shaft sleeve Or After Test A6

Figure E-A7.1Trace before Test A7

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Figure E-A7.2 Trace after Test A7

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Figure E A7.3 Process of wear depth measurement from the trace

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APPENDIX F –ROUGHNESS TRACES OF BEARINGS AND SHAFT SLEEVE

Figure F-A2.1 Bearing roughness after Test A2

Figure F –A2.2 Bearing transverse roughness after Test A2

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Figure F- A2.3 Shaft sleeve roughness after Test A2

Figure F- A2.4 Shaft sleeve transverse roughness after test A2

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Figure F- A3.1 Bearing roughness after Test A3

Figure F- A3.2 Bearing transverse roughness after Test A3

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Figure F –A3.3 Shaft sleeve roughness after Test A3

Figure F- A3.4 Shaft sleeve transverse roughness after Test A3

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Figure F–A4.1 Bearing roughness after Test A2

Figure F- A4.2 Bearing transverse roughness after Test A4

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Figure F- A4.3 Shaft sleeve roughness after Test A4

Figure F- A4.4 Shaft sleeve transverse roughness after Test A4

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Figure F- A6.1 Bearing roughness after Test A6

Figure F- A6.2 Bearing transverse roughness after Test A6

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Figure F – A6.3 Shaft sleeve roughness after Test A6

Figure F- A6.4 Shaft sleeve transverse roughness after Test A6

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Figure F- A7.1 Bearing roughness after Test A7

Figure F- A7.2 Bearing transverse roughness after Test A7

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Figure F- A7.3 Shaft sleeve roughness after Test A7

Figure F- A7.4 Shaft sleeve transverse roughness after Test A7

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