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PROGRESS REPORT ON THE GEOKINETICS HORIZONTAL IN SITU RETORTING PROCESS M. A. Lekas Geokinetics Inc. 280 Buchanan Field Road Concord, CA 94520 Geokinetics Inc., in cooperation with the U. S. Department of Energy, is engaged in developing an in situ process for the extraction of shale oil. The process is designed specifically for areas where the oil shale beds are relatively thin and close to the surface. We call this technique the LOFRECO process. Geokinetics is a very small company, and does not have the resources for massive capital expendi tures ahead of production. Therefore, we set out to develop a process with low front end costs. The result was the LOFRECO process - LOFRECO being an acronym for Low Front End Cost. LOFRECO truly lives up to its name. Front end costs are minimal, as most of the expenditures are in the form of operating costs. In the process, a pattern of blastholes is drilled from the surface, through the overburden, and into the oil shale bed. The holes are loaded with explosives and fired, using a carefully planned blast system. The blast results in a well fragmented mass of oil shale, with a high permeability. The void space in the fragmented zone comes from lifting the overburden, and producing a small uplift of the surface. The fragmented zone constitutes an in situ retort. (Figure 3) The bottom of the retort is sloped to provide drain age for the oil to a sump where it is lifted by a number of oil production wells. Air injection holes are drilled at one end of the retort, and off gas holes are drilled at the other end. The oil shale is ignited at the air injection wells, and air is injected to establish and maintain a burning front that occupies the full thickness of the fragmented zone . The front is moved in a horizontal direction through the fractured shale towards the off gas wells at the far end of the retort. The burning front heats the oil shale ahead of the front, driving out the shale oil, which drains to the bottom of the retort , where it flows along the sloping bottom to the oil pro duction wells. As the burn front moves from the air-in to the air-out wells, it burns the residual coke in the retorted shale as fuel. The combustion gases are recovered at the air-out wells. This gas is combustible, and could be used for power generation. Progress of the burn front is monitored by thermocouples set in thermocouple wells. Although the process was designed to retort relatively thin oil shale beds under shallow overburden, the basic horizontal burn that is being developed can be applied to a number of other situations, such as a modified in situ process in thinner oil shale beds, or as a secondary recovery process to follow after a room and pillar mining operation to recover oil from the mine pillars and from oil shales above and below the mined zone. Laboratory and pilot work was carried out at the Geokinetics facilities at Concord, California, during 1974 and early 1975, to demonstrate the technical feasibility of establishing and maintaining a horizontally moving burning front through a random sized mass of rubblized oil shale. In March of 1975, leases on oil shale lands suitable for the LOFRECO process were acquired in the Book Cliffs area, south of Vernal, Utah, on lands 228
Transcript
Page 1: developing · PROGRESSREPORTON THEGEOKINETICSHORIZONTAL INSITURETORTINGPROCESS M. A. Lekas GeokineticsInc. 280BuchananFieldRoad Concord,CA 94520 GeokineticsInc.,incooperationwith

PROGRESS REPORT ON THE GEOKINETICS HORIZONTAL

IN SITU RETORTING PROCESS

M. A. Lekas

Geokinetics Inc.

280 Buchanan Field Road

Concord, CA 94520

Geokinetics Inc., in cooperation with

the U. S. Department of Energy, is engaged

in developing an in situ process for the

extraction of shale oil. The process is

designed specifically for areas where the

oil shale beds are relatively thin and

close to the surface. We call this

technique the LOFRECO process. Geokinetics

is a very small company, and does not have

the resources for massive capital expendi

tures ahead of production. Therefore, we

set out to develop a process with low

front end costs. The result was the

LOFRECO process - LOFRECO being an acronym

for Low Front End Cost.

LOFRECO truly lives up to its name.

Front end costs are minimal, as most of the

expenditures are in the form of operating

costs. In the process, a pattern of

blastholes is drilled from the surface,

through the overburden, and into the oil

shale bed. The holes are loaded with

explosives and fired, using a carefully

planned blast system. The blast results

in a well fragmented mass of oil shale,

with a high permeability. The void space

in the fragmented zone comes from lifting

the overburden, and producing a small

uplift of the surface.

The fragmented zone constitutes an

in situ retort. (Figure 3) The bottom

of the retort is sloped to provide drain

age for the oil to a sump where it is

lifted by a number of oil production wells.

Air injection holes are drilled at one

end of the retort, and off gas holes are

drilled at the other end.

The oil shale is ignited at the air

injection wells, and air is injected to

establish and maintain a burning front

that occupies the full thickness of the

fragmented zone . The front is moved in a

horizontal direction through the fractured

shale towards the off gas wells at the far

end of the retort. The burning front

heats the oil shale ahead of the front,

driving out the shale oil, which drains to

the bottom of the retort,where it flows

along the sloping bottom to the oil pro

duction wells. As the burn front moves

from the air-in to the air-out wells, it

burns the residual coke in the retorted

shale as fuel. The combustion gases are

recovered at the air-out wells. This gas

is combustible, and could be used for

power generation. Progress of the burn

front is monitored by thermocouples set

in thermocouple wells.

Although the process was designed to

retort relatively thin oil shale beds

under shallow overburden, the basic

horizontal burn that is being developed

can be applied to a number of other

situations, such as a modified in situ

process in thinner oil shale beds, or as

a secondary recovery process to follow

after a room and pillar mining operation

to recover oil from the mine pillars and

from oil shales above and below the mined

zone.

Laboratory and pilot work was carried

out at the Geokinetics facilities at

Concord, California, during 1974 and early

1975, to demonstrate the technical

feasibility of establishing and maintaining

a horizontally moving burning front

through a random sized mass of rubblized

oil shale.

In March of 1975, leases on oil

shale lands suitable for the LOFRECO

process were acquired in the Book Cliffs

area, south of Vernal, Utah, on lands

228

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owned by the State of Utah. The oil shale

bed is approximately 30 feet thick, and has

an average grade of about 23 gallons per

ton. The beds strike in an east-west

direction and dip to the north at about

120 feet per mile. Overburden over the

shale ranges from zero to 150 feet.

(Figure 1)

The leases are located in a very

remote area, 70 miles from the nearest

settlement. Communication is by a poorly

maintained, unpaved road. There are no

power lines or telephone lines in the area.

Immediately upon acquiring the property,

field operations began. Because of the

remote location and poor communications, it

was necessary to establish a fully equipped,

self-contained living and operating

facility at the test site. In order to

move the project ahead with the minimum

delay, the experimental work began concur

rently with the construction of the camp

facilities, and the camp has grown as the

project progressed and increased in size.

The initial camp was established in April

of 1975, and was promptly christened

"KampKerogen."

Kamp Kerogen consisted

initially of three tents and outdoor cooking

and eating facilities. The field work

progressed rapidly. Two small retorts

were blasted in July of 1975, and the first

small retort was ignited on March of 1976.

Work has proceeded seven days a week, and

continued throughout the winters despite

heavy snowfall and difficult living

conditions .

Our field program has made steady

progress since its inception in the spring

of 1975. After four years of field work,

we have blasted 18 retorts, and burned

11 retorts. In the course of carrying out

our experimental work, we have produced

over 5,000 barrels of shale oil. Kamp

Kerogen has grown from three tents in the

sagebrush to a small village, with a

permanent population of 30 persons,includ

ing wives and children.

It has been demonstrated that:

1) It is possible to drill a pattern

of blastholes from the surface into the

oil shale, and fracture the shale in a

manner to establish a zone of high perme

ability in the shale, with a relatively

impermeable zone between the fragmented

shale and the surface.

2) It is possible to drill through

the rubblized material, and construct the

various wells necessary for the operation,

including air-in holes, off gas holes,

oil recovery wells and instrument wells.

3) A point ignition can be made in

the rubblized shale and expanded into a

burn front that covers the cross section

of the retort.

4) The burn front can be moved down

the length of the retort as a cohesive

temperature front, with satisfactory sweep

efficiency.

5) Produced oil can be recovered

from a well drilled to the bottom of the

rubblized zone.

We feel that the technical feasibility

of the LOFRECO process is established. We

are now engaged in optimizing the process

to make it economically feasible. This

involves :

1) Reducing the cost of rock frag

mentation. This is the single most

significant cost item in the process.

2) Improving the recovery of in-place

oil. This involves improved blasting

techniques to prepare the shale bed for

retorting, optimized burning techniques

to minimize burn-up and coking of oil in

the retort, and better oil lifting

techniques . Our target is a recovery of

50% or more of the in-place oil. Out of

11 retorts burned to date we have achieved

50% recovery on two retorts, including

the #16, which is our latest and largest.

3) Making effective use of the

combustible retort off gas to generate

electrical power.

4) Meeting all of the environmental

requirements .

229

Page 3: developing · PROGRESSREPORTON THEGEOKINETICSHORIZONTAL INSITURETORTINGPROCESS M. A. Lekas GeokineticsInc. 280BuchananFieldRoad Concord,CA 94520 GeokineticsInc.,incooperationwith

5) Establishing a market for crude

shale oil at the refineries in Salt Lake

City; Roosevelt, Utah; or at Fruita,

Colorado. In order to make our shale oil

acceptable to these refineries, we are

investigating the feasibility of controlled

blending of shale oil with the normal

refinery feedstock, and upgrading our shale

oil by a hydrotreating process.

Our primary objectives for 1979 are

to:

1) test a number of retorting pro

cedures to optimize oil recovery,

2) burn a retort with full thickness

of the oil shale bed (30 feet) , and

3) blast a full-sized retort (200

feet wide by 200 feet long by 30 feet

thick) .

In 1980, we plan to blast a cluster

of three full-sized retorts. During 1981,we will burn this cluster, and blast a

second three-retort cluster. This second

cluster will be burned during 1981 and the

first half of 1982.

By mid-1982, we expect to have

achieved our overall program objective of

developing and testing the Geokinetics

Horizontal In Situ Retorting Process. Bythis date we should have sufficient data

on hand to evaluate the technical,

environmental, and economic feasibility of

the process. If the results are favorable,we will be in a position to construct a

full scale operating unit producing a

minimum of 2,000 barrels of shale oil

each day.

230

Page 4: developing · PROGRESSREPORTON THEGEOKINETICSHORIZONTAL INSITURETORTINGPROCESS M. A. Lekas GeokineticsInc. 280BuchananFieldRoad Concord,CA 94520 GeokineticsInc.,incooperationwith

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Page 6: developing · PROGRESSREPORTON THEGEOKINETICSHORIZONTAL INSITURETORTINGPROCESS M. A. Lekas GeokineticsInc. 280BuchananFieldRoad Concord,CA 94520 GeokineticsInc.,incooperationwith

Retort

Number

Date

Blasted

Thickness

of Shale

Blasted

Overburden

Thickness Width Length

Cross -

Sectional

Area ft2

Tons of

Broken

Shale

Date

Ignited

Barrels

of Oil

Recovered

1 7/75 10 ft. 0 ft. 10 ft. 50 ft. 100 330 9/76 56

2 7/75 3 10 10 30 30 60 3/76 28

3 1/76 10 17 20 40 200 530 7/76 82

4 2/76 10 16 20 40 200 530 2/77 146

S 2/76 11 19 20 81 220 1200 5/77 354

6 Drilled - Not Blasted

7 11/76 10 15 20 50 200 670 -

8 11/76 23 22 20 83 460 2600 - -

9 12/76 22 22 40 83 880 4900 9/77 1007

10 12/76 11 14 20 50 220 730 - -

11 3/77 12 14 20 45 240 720 4/77 272

12 3/7/ 11 31 30 50 330 1100 - -

13 6/77 11 31 30 50 330 1100 - -

14 6/77 12 29 40 70 480 2200 2/78 384

15 7/77 20 31 50 75 1000 5000 5/78 1003

16 8/77 20 41 62 87 1200 7200 8/78 2067

17 5/78 17 26 72 156 1200 13000 - -

18 7/78 17 27 108 156 1800 19000 - -

19 12/78 30 50 126 182 3800 46000 - -

FIGURE 4. SUMMARY OF DATA ON re:"ORTS 1 THROUGH 19 (to 12/31/78)

Days API

Gravity

Pour Nitro-

Point gen

oF%

Sulfur

7.

Engler Distillation D-86

IBP 57. 107. 207. 307. 407. 507. 607. 707. 807.

Residue

907. 7.

1-6 24.4 55 1.88

7-10 25.0 60 1.83

11-15 25.6 66 1.67

16-20 25.8 65 1.55

21-25 26.2 64 1.66

26-30 25.8 69 1.46

31-35 26.4 60'

1.45

36-40 26.7 63 1.42

41-45 26.7 65 1.19

46-51 26.5 64 1.28

0.91 210

0.92 j 302

0.84 212

0.81 I 230

0.78

0.77

0.83

0.80

0.77

0.91

232

223

205

214

238

223

398 436 501 548 594 630 670

384 431 496 552 605 644 689

382 438 490 550 599 640 672

416 452 501 548 589 630 680

407 444 498 546 589 634 685

416 449 502 547 592 641 672

408 444 503 555 598 643 692

406 441 493 543 588 627 670

383 436 486 529 571 616 657

439 466 510 548 589 627 670

732

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737

734

752

750

753

755

755

755

754

748

6

14

13

9

3

6

5

6

6

6

Avg. 25.9 63 1.54 0.83 229 404 444 498 547 591 633 676 715 738 754

FIGURE 5. ANALYSIS OF OIL PRODUCED FROM RETORT #14, SHOWING CHANGE IN CHARACTERISTICS

OF THE OIL DURING RETORTING.

FIVE DAY COMPOSITE SAMPLES

233

Page 7: developing · PROGRESSREPORTON THEGEOKINETICSHORIZONTAL INSITURETORTINGPROCESS M. A. Lekas GeokineticsInc. 280BuchananFieldRoad Concord,CA 94520 GeokineticsInc.,incooperationwith

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1-10 71.1 6.3 15.5 2.2 1.1 2.5 .109 .119 .009 .029 .046 .007 .005 .009..017

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11-20 67.4 4.8 18.2 3.5 1.5 3.6 .078 .069 .019 .030 .034 .009 .003 .003 .005.013 .006 .27 .31

21-30 67.9 4.3 17.7 3.6 1.3 4.2 .082 .061 .012 .030 .030 .006 .003 .003 .006 .016 .006 .30 .35

31-40 67.2 3.7 18.1 4.6 1.2 4.3 .068 .048 .012 .032 .028 .006 .004 .002 .013 .019 .008 .30 .38

41-50 67.7 3.7 17.6 4.3 1.1 4.3 .092 .062 .013 .037 .030 .007 .003 .001 .008 .024 .008 .28 .46

51-60 65.2 2.0 18.6 4.9 1.8 5.9 .113 .074 .017 .051 .034 .010 .006 .003 .013 .207 .206 .24 .44

61-70 - - - - - - - - - - - - - - - - - - -

71-80 60.3 4.1 13.3 9.9 1.3 10.5 .084 .071 .017 .054 .042 .010 .005

-.006 .031 .008 .03 .19

81-90 59.1 2.3 17.6 8.5 0.8 10.7 .140 .139 .030 .072 .052 .012 .006 .005 .015 .052 .015 .12 .31

91-100 62.5 1.9 19.3 5.0 1.1 9.2 .250 .189 .033 .084 .065 .015 .010 .003 .017 .067 .020 .05 .24

101-110 62.0 1.5 22.0 3.9 1.3 8.1 .238 .184 .046 .070 .058 .027 .011 .017 .015 .058 .085 .13 .28

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Avg. 64.5 3.4 18.8 4.6 1.3 6.4 .144 .112 .024 .053 .045 .012 .007 .009 .013 .054 .050 .21 .33

FIGURE 6. ANALYSIS OF RETORT #16 OFF GAS, SHOWING CHANGE IN CHARACTERISTICS DURING RETORTING

TEN DAY COMPOSITE SAMPLES

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ELAPSED DAYS

'FIGURE 7. RETORT #14, SHOWING CHANGE IN NITROGEN AND SULFUR IN OIL DURING RETORTING

234

Page 8: developing · PROGRESSREPORTON THEGEOKINETICSHORIZONTAL INSITURETORTINGPROCESS M. A. Lekas GeokineticsInc. 280BuchananFieldRoad Concord,CA 94520 GeokineticsInc.,incooperationwith

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Page 9: developing · PROGRESSREPORTON THEGEOKINETICSHORIZONTAL INSITURETORTINGPROCESS M. A. Lekas GeokineticsInc. 280BuchananFieldRoad Concord,CA 94520 GeokineticsInc.,incooperationwith

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Page 10: developing · PROGRESSREPORTON THEGEOKINETICSHORIZONTAL INSITURETORTINGPROCESS M. A. Lekas GeokineticsInc. 280BuchananFieldRoad Concord,CA 94520 GeokineticsInc.,incooperationwith

PRODUCT YIELDS

R. N. Heistand

Development Engineering, Inc.

Box A, Anvil Points

Rifle, Colorado 81650

ABSTRACT

The Fischer Assay (FA) , termed "the

standard for the oil shale industry", is

designed to assay the oil potential of geo

logical deposits. It is not designed for

process control nor process evaluation. Yet

traditionally, the calculation "oil yield,

volume percent FischerAssay"

is used.

The product split between oil and gas

in the Fischer Assay does not relate to any

known oil shale retorting process. The

Fischer Assay is a laboratory test; heat is

transferred through the reactor wall; it is

a batch process in which the energy products

are separated by cooling to 0C.

Sincf? both the crude shale oil and

product gas are valuable energy products, a

calculated Product Yield presents a truer

picture of retort production. This Product

Yield compares the retort products (oil and

gas) with the Fischer Assay products (oil

and gas) .

The Product Yield is based on the

products produced from the retorting opera

tions before any allowance for energy

consumed. No credit is given for any

process heat supplied from the raw shale

feed. When this energy (expressed as

MBtu/T) is included, Retort Yield can be

calculated using products plus any heat

supplied by the carbon residue on the shale.

For the Paraho Direct Mode process, the

Retort Yields are generally 110% of assay.

Increases in this number are anticipated as

more of the carbon residue is utilized.

OIL YIELD

The classical approach toward assessing

a given retorting process is to calculate

the oil yield as based on Fischer Assay.

The oil yield, as a volume percent of

Fischer Assay, is simply the oil produced

by the retort divided by the oil produced

by the assay, as shown by the following

equation :

R(1) Oil Yield, % Assay

= 100% x

Where 0 = Oil Produced

R = Retort

A = Assay

This simple expression has several draw

backs. The first is the Fischer Assay

itself (Heistand, 1976) . It is meant to

assay geological deposits, not assess

retorting processes. The American

Society for Testing and Materials (ASTM)

cautions the user that:

"The method neither yields quantities

that necessarily duplicate yields

in experimental or commercial oil

shale processes nor does it yield

products that necessarily duplicate

in physical or chemical nature the

products that may be obtained in

such experimental or commerical

processes."

(ASTM, 1978)

Also, the oil, determined by Fischer

Assay, is obtained by cooling the off

gas to 0C. This cooling cannot be

achieved economically nor practically in

a commercial process. The most important

drawback of the simple expression is that

only the liquid oil is considered. In

the Green River oil shale, oil comprises

only two-thirds of the total organics,

or kerogen, in the raw shale. For many

other shales, this oil fraction is less

yet since they yield larger assaygas-to-

oil ratios.

237

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PRODUCT YIELD

A better approach would be to expand

Equation (1) to consider both the oil and

gas yields as shown in the following

equation:

(2) Product Yield, % Assay = 100% x fc + )Oa

gA'

Where g=

energy value of the gas produced.

This expression, Equation (2), has the

advantage that both commercial products of

oil shale retorting, oil and gas, are taken

into consideration. However, this complex

expression has several drawbacks. First,

this expression results in a mixed number -

percent oil plus percent gas, as determined

by Fischer Assay-

since oil produced is

measured in liter/tonne and the gas produced

in kcal/tonne. Secondly, the energy value

of the Fischer Assay gas, kcal/tonne, is not

normally determined.

The energy value of the gas produced

from the retorting process, kcal/tonne, can

be calculated from the gross heating value,

3 3kcal/m , and the quantity, m /tonne. This

can be converted to equivalent oil using

the following equation:

(3) 1.0 Liter of Oil = 9500 kcal.

Although the heating value of the gas

produced by Fischer Assay is normally not

determined in the standard Fischer Assay

procedure, the value can be determined using

the Material Balance Assay. (Goodfellow and

Atwood, 1974)

The heating value of the assay gas has

been determined for Green River shales

having different assay oil contents. (USBM,

1951) The relationship between assay oil,

liter/tonne and gas, kcal/tonne, can be

expressed by a straight line formula using

least squares (see Figure 1) . Combining

this straight line relationship between

assay oil and gas with Equation (3), it is

possible to calculate the assay gas, equiva

lent oil (EO) , from the measured assay oil.

This produces the following expression:

(4) Gas (EO) Liter/Tonne = 0.11 x 0A,Liter/Tonne - 3.3

The good agreement between the calculated

and measured gas data, as indicated by

the r2 term = 0.982, tends to validate

the straight line equation. Thus, with

this straight line equation, one can cal

culate the equivalent oil of the assay

gas from the measured assay oil yield.

.300

GAS

4

-200 kcal/Tonne

-100

OIL

Liter/Tonne

'100 200

i

300

Assay Oil vs. Gas (USBM RI4825)

Figure 1

Using the relationships developed

in Equations (3) and (4) , the product

(oil plus gas) for both the retort and

the Fischer Assay can be expressed as

liquid volumes per unit weight of raw

shale (liter/tonne). Thus, the Product

Yield, expressed in Equation (2) , can be

simplified as follows:

R Gr(5) Product Yield, % Assay = 100% x ^ + ^

9a gA

Where G = equivalent oil of gas produced

(liter/tonne) .

RETORT YIELD

The Product Yield, as shown in Equa

tion (5), compares the retort and Fischer

Assay products. The numerator is the sum

of products out of the retort and the

denominator is the sum of products

measured in the raw shale feed using

Fischer Assay. This concept still does

not give the complete picture of

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retorting. It needs to be expanded to

include the thermal energy supplied from the

raw shale feed for retorting. When thermal

energy is included, the expression becomes

Retort Yield. The thermal energy (E) is

added to the retort products when it origi

nates from the kerogen in the raw shale in

the same manner as the product gas and oil.

It is subtracted from the retort products

when it is obtained from burning part of the

oil or gas produced in the retort. Thus,

the Retort Yield becomes:

(6) Retort Yield, % of Assay=

100* x0r +

g;+ Er

A + A

Where E = thermal energy to fuel process.

CONCLUSIONS

For the Paraho Direct Mode, a typical

Retort Net Yield is 114 Vol% assay (see

Table 1) . This reflects the 14 liter/tonne

TABLE 1

YIELDS

Indirect Direct

Liter/Tonne Liter/Tonne

Raw Shale Feed

Assay Oil + Gas (EO) 115 123

Paraho Retort

Oil + Gas (EO) 115 126

Thermal Energy (EO)- 14 + 14

Total 101 140

Yields, Volume % Assay

Product 100 102

Retort 88 114

B0 is the equivalent oil, in liter/tonne.

(equivalent oil) of thermal energy supplied

as heat by the raw shale feed to operate the

retorting process. For the Paraho Indirect

Mode, a typical Retort Yield is 88 Vol%

assay (see Table 1) . This reflects the heat

supplied by the external combustion of

product oil or gas. Product yields for both

Direct Mode and Indirect Mode are 100-102

Vol% assay.

Further expansion of the Retort Yield

equation would provide the means for

including other terms such as resource

recovery, materials handling, and energy

conversion. This expanded equation could

then compare in-situ to above-ground

retorting, take into account the convey

ing or transport of shale, include the

energy consumption of other operations

such as mining and crushing, and the

losses caused by energy conversion and

environmental controls. However, for

many processes, these detailed energy

requirements for commercial operations

are not available at this time.

There are both disadvantages and

advantages in using the concepts of

Retort Yield and the more expanded equa

tions. Some additional work is needed.

Some of the disadvantages are:

1) Fischer Assay remains the

benchmark .

2) Additional laboratory work is

needed to quantify the assay

gas.

3) Energy premiums for oil and

gas products are not the same.

However, the advantages far outweigh the

disadvantages. Some of the advantages

are:

1) Both products (oil and gas)

are considered.

2) A numerical assessment of a

particular oil shale retorting

process is possible.

3) The technique can be expanded

to various energy (or economic)

parameters.

4) Results are based on a common

point- the Fischer Assay of

the raw shale feed.

Some additional work which should

be done to assure that the concepts of

Retort Yield are used in valid fashion

include:

1) The equation relating assay

gas quantity to the assay oil

yield should be confirmed.

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2) The heating value of crude shale

oil should be measured for each

retort tested.

3) The heat and power required for

retorting should be confirmed.

4) The energy requirements for

various aspects of oil shale

operations should be determined.

What has been presented is a basis for

more fully evaluating oil shale retorting

processes. At this time, the concept of

Retort Yield, which takes into account both

products of oil shale retorting (oil plus

gas) , and the energy required to fuel the

retort, best describes the retorting

process.

ACKNOWLEDGEMENT

This work was carried out at the

Department of Energy's Anvil Points Oil

Shale Research Facility located on the

Naval Oil Shale Reserves near Rifle,

Colorado.

REFERENCES

American Society for Testing and

Materials, "Oil and Water from Oil

Shale (Resource Evaluation by the

USBM Fischer Assay Procedure)",D 78T, ASTM, Phila, PA, 1978.

Bureau of Mines, Report of Investiga

tion 4825, III-4b(2), (3), 1951.

Goodfellow, L and M. T. Atwood,

"Fischer Assay of the Oil Shale

Procedures of The Oil Shale Corpor

ation", 7th Oil Shale Symposium,

Colorado School of Mines, Golden,

CO, 1974.

Heistand, R.N. , "The Fischer Assay: A

Standard Method?", Div. of Fuel

Chemistry (ACS) Preprints, 21~(6) ,

40-43 (1976).

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