Proposed Redevelopment 90-02 168 Street Jamaica, Queens ......Dec 13, 2019 · Soil borings...

Phase II Environmental Site Assessment Report

FOR

Proposed Redevelopment 90-02 168th Street

Jamaica, Queens, New York

Prepared For:

90Ninety LLC

767 3rd Avenue, 33rd Floor

New York, New York 10017

Prepared By:

SESI CONSULTING ENGINEERS, DPC 12A Maple Avenue

Pine Brook, NJ 07058

DATE:

December 13, 2019

____________________

Fuad Dahan, P.E.

NY Lic. No. 10394

Table of Contents

1.0 INTRODUCTION ................................................................................................................................. 1

1.1 Recognized Environmental Concerns ..................................................................................... 1

1.2 Site Settings ................................................................................................................................ 1

1.3 Proposed Site Development ..................................................................................................... 2

2.0 SUBSURFACE INVESTIGATION .................................................................................................... 3

2.1 Utility Clearance and Geophysical Survey ............................................................................. 3

2.2 Borings ......................................................................................................................................... 3

3.0 ANALYTICAL RESULTS ................................................................................................................... 5

3.1 Soil Investigation Results .......................................................................................................... 5

3.2 Groundwater Investigation Results .......................................................................................... 7

3.3 Soil Vapor Results ...................................................................................................................... 7

4.0 CONCLUSIONS AND RECOMMENDATIONS .............................................................................. 9

Appendices

Appendix A: GPR Report

Appendix B: Boring Logs

Appendix C: Analytical Results (Electronic)

Figures

Figure 1: Site Location Map

Figure 2: Site Plan

Figure 3: Soil Boring Location Plan

Figure 4: Soil Vapor Sample Location Plan

Figure 5: Groundwater Results Plan

Tables

Table 1: Soil Sample Results – Pesticides and PCBs

Table 2: Soil Sample Results – Semivolatile Organic Compounds

Table 3: Soil Sample Results - Metals

Table 4: Soil Sample Results – Volatile Organic Compounds

Table 5: Soil Vapor Sample Results

Phase II Environmental Site Assessment Report 90-02 168th Street Jamaica, New York December 13, 2019 Page 1 of 9

1.0 INTRODUCTION SESI Consulting Engineers, DPC (SESI) has conducted this Phase II Environmental Site

Assessment (Phase II ESA) on behalf of the Requestor, 90Ninety LLC, for a 99,500 ft2 (2.28

Acres) property located at 90-02 168th Street in Jamaica, Queens County, New York (the “Site”).

The Subject Property is bound to the north by 90th Avenue, to the east by 168th Street, to the west

by a church complex, a religious bookstore, and residential buildings, and to the south by

commercial retail buildings. Figure 1 presents a Site Location Map.

SESI reviewed Sanborn maps of the Site and a previous Phase I ESA by AKRF, Inc. from October

2018 to determine potential areas of concern. Historical uses of the Site of potential environmental

concern include an automotive repair shop (circa 1942), a plumber’s shop, and paint storage area

(circa 1925). The Site has been used as a parking lot since the early 1960s.

SESI collected soil, sub-slab soil vapor, and groundwater samples, to further investigate the

identified Recognized Environmental Concerns (RECs) at the Site and determine the Site’s

eligibility for entry into the New York State Brownfields Cleanup Program (BCP). Figure 2

presents a site plan.

1.1 Recognized Environmental Concerns

One (1) onsite REC was identified in the Phase I ESA performed by AKRF in 2018, which is

covered under REC-1 identified during SESI’s review of historic Sanborn maps, as detailed below.

- REC 1 – Historic Site Use: As noted above, historical uses of the Site of potential

environmental concern include an automotive repair shop (circa 1942), a plumber’s shop,

and paint storage area (circa 1925).

1.2 Site Settings

The Site consists of a 99,500 square-foot (2.28-acre) property located at 90-02 168th Street,

Jamaica, Queens County, New York. The Site is located in a commercial and residential area

with commercial properties to the south of the Site, a public library and religious structures to the

north across 90th Avenue, a police precinct and parking lot to the east across 168th Street, and a

church complex, religious bookstore, and residential properties to the west. The closest surface


water body is Baisley Pond, located approximately 1.9 miles southeast of the Site. The Site

topography is generally flat and regionally slopes gently downward to the south.

1.3 Proposed Site Development

The planned new construction for the Site will be a multi-story residential apartment building with

ground-floor retail and subgrade parking.


2.0 SUBSURFACE INVESTIGATION The field work was conducted under the site-specific Health and Safety Plan (HASP) between

August 29th and September 3rd, 2019.

2.1 Utility Clearance and Geophysical Survey

Prior to conducting any subsurface drilling, SESI’s drilling contractor contacted New York’s utility

mark-out system. In addition, SESI retained the services of Ground Penetrating Radar Systems

(GPRS), a private utility locator, to locate underground utilities not included in the one-call and to

conduct a geophysical survey to investigate the potential for historical USTs. GPRS performed

the survey on August 29, 2019 and located several underground utilities throughout the Site but

no anomalies consistent with an UST. The GPRS report is provided in Appendix A.

2.2 Borings

Twenty (20) soil borings, and five (5) soil vapor points were advanced using a direct push

Geoprobe® rig. Four (4) soil borings were converted to temporary wells to obtain groundwater

samples. The boring and soil vapor point locations are shown in Figure 3 and Figure 4,

respectively. Soil boring logs are presented in Appendix B. A total of twenty-two (22) soil

samples, four (4) groundwater samples, and five (5) soil vapor samples were collected and

analyzed for various parameters at Alpha Analytical Laboratories (Alpha), which is a NYSDEC

ELAP-certified laboratory. The soil samples were collected from varying depths based on field

screening, which included screening with a Photo Iodization Detector (PID), visual and olfactory

observations and generally biased towards fill materials. All soil samples were named based on

their respective soil boring number and specified depth. A summary table of all samples collected

is presented below.


Sample Location

Depth Interval

(ft bg) Matrix Analysis

SESI-SB-1 2-3 Soil TCL+30/TAL

SESI-SB-2/TW-3 3-4 Soil/GW TCL+30/TAL




















SV-1 35 Soil Vapor TO-15 (VOCs)






3.0 ANALYTICAL RESULTS

3.1 Soil Investigation Results

In total, twenty-two (22) soil samples were collected. The soil sample locations were distributed

based on the RECs identified in investigation of historic documents as well as to cover all areas

of the Site. The soil sample depths were selected based on the field screening and visual

observations. The soil samples were sent to Alpha with a chain-of-custody (COC) and analyzed

for TCL/TAL+30. The laboratory analytical reports are included in Appendix C. Soil boring

locations and a summary of results exceeding applicable standards are shown on Figure 3.

Summary tables of all analytical results compared to New York State Department of

Environmental Conservation (NYSDEC) Unrestricted Use Soil Cleanup Objectives (USCO),

Residential Soil Clean-up Objectives (RSCOs), and Restricted Residential Soil Clean-up

Objectives (RRSCOs) are presented in Tables 1-4.

Soil borings SESI-SB-4, and SESI-SB-6 targeted the former auto repair area, borings SESI-SB-

1 and SESI-SB-2 targeted the former plumber store, and boring SESI-SB-3 targeted the former

paint storage area. The remaining borings were spread throughout the Site for spatial coverage.

Table 3.1 below presents a summary of the soil exceedances to the RSCOs. The soil data

indicates the presence of several SVOCs exceeding NYSDEC USCOs, RSCOs, and RRSCOs

including indeno(1,2,3-cd)pyrene in seven samples, benzo(a)anthracene, benzo(a)pyrene, and

benzo(b)fluoranthene in five samples, dibenz(a,h)anthracene in two samples, and chrysene in

one sample as shown in the table below. SVOCs exceeding UUSCOs only were also reported

in several samples as illustrated on Figure 3. Metals including mercury exceeded USCOs,

RSCOs, and RRSCOs in three samples, and lead in two samples, with zinc exceeding only

USCOs in nine samples as shown in table 3.1. Select pesticides were detected exceeding USCOs

in four soil samples. PCBs were not detected exceeding UUSCOs in any samples. No volatile

organic compounds (VOCs) were identified in any sample collected exceeding the USCOs other

than acetone, which is a common laboratory contaminant and is not considered to be site-related.

Complete soil sample analytical results are summarized in Tables 1-4.


Table 3.1: Summary of Soil Exceedances of Applicable SCOs

PESTICIDES

Aldrin 0.097 0.005 U U U U U

Dieldrin 0.2 0.005 U U U U U

Endosulfan I 8.9 0.0033 U U U U U

4,4'-DDE 7.9 0.0033 U U U 0.00603 0.00156

4,4'-DDD 13 0.0033 U U 0.00168 U U

4,4'-DDT 7.9 0.0033 U U U U U

Heptachlor 2.1 0.042 U U U 0.00342 U

cis-Chlordane 4.2 0.094 0.00169 U U U U

SEMIVOLATILES

Benzo(a)anthracene 1 1 3.2 1.3 1.6 4 4.4

Benzo(a)pyrene 1 1 2.8 1.1 1.1 3.2 4.2

Benzo(b)fluoranthene 1 1 3.6 1.2 1.5 4.2 5.3

Benzo(k)fluoranthene 3.9 0.8 1.5 0.5 0.6 1.6 2.1

Chrysene 3.9 1 2.8 1.1 1.4 3.3 4.2

Dibenzo(a,h)anthracene 0.33 0.33 0.38 0.21 0.17 0.48 0.56

Indeno(1,2,3-cd)pyrene 0.5 0.5 2.2 0.85 0.78 2.1 2.4

TOTAL METALS

Lead 400 63 127 113 576 127 185

Mercury 0.81 0.18 0.168 0.263 0.712 0.228 0.253

Zinc 10000 109 85.4 60.6 91.5 171 157

PESTICIDES

Aldrin 0.097 0.005 U U U U U

Dieldrin 0.2 0.005 U U U U U

Endosulfan I 8.9 0.0033 U U U U U

4,4'-DDE 7.9 0.0033 0.00902 U 0.0259 U 0.0022

4,4'-DDD 13 0.0033 0.00646 U U U 0.0018

4,4'-DDT 7.9 0.0033 0.0354 U 0.00711 U U

Heptachlor 2.1 0.042 U U U U U

cis-Chlordane 4.2 0.094 0.00645 U U U U

SEMIVOLATILES

Benzo(a)anthracene 1 1 0.95 U 2.6 0.34 0.89

Benzo(a)pyrene 1 1 0.93 U 2.5 0.34 0.91

Benzo(b)fluoranthene 1 1 1.2 U 3.2 0.44 1.2

Benzo(k)fluoranthene 3.9 0.8 0.51 U 1.3 0.17 0.4

Chrysene 3.9 1 0.92 U 2.5 0.34 0.92

Dibenzo(a,h)anthracene 0.33 0.33 0.12 U 0.34 0.048 0.12

Indeno(1,2,3-cd)pyrene 0.5 0.5 0.55 U 1.6 0.18 0.53

TOTAL METALS

Lead 400 63 386 522 279 329 268

Mercury 0.81 0.18 0.343 0.761 0.848 2.67 2.84

Zinc 10000 109 190 116 215 207 160

Note: U - Not detected at the reported detection limit for the sample.

All Concentrations in milligrams per kilogram (mg/kg)

AnalyteRestricted

Residential

Unrestricted

Use

AnalyteRestricted

Residential

Unrestricted

Use

SESI-SB-13

(3-4')

SESI-SB-14

(4-5')

SESI-SB-16

(1-2')

SESI-SB-18

(2-3')

SESI-SB-1

(2-3')

SESI-SB-4

(2-3')

SESI-SB-10

(2-3')

SESI-SB-11

(3-4')

SESI-SB-8

(2-3')

SESI-SB-12

(6-7')


3.2 Groundwater Investigation Results

Four (4) groundwater samples were collected during the investigation. The samples were sent to

Alpha on a chain of custody (COC) and analyzed for TCL/TAL+30 including filtered and unfiltered

samples for metals. The laboratory analytical reports are included in Appendix C. A groundwater

sample location and a summary of the results is shown in Figure 5. Complete summary tables of

the analytical results compared to NYSDEC Technical and Administrative Guidance Series 1.1.1

Ambient Groundwater Quality Criteria (TOGS AWQS) are presented in Tables 5-8.

Table 3.2 presents a summary of the groundwater exceedances to the AWQS. SVOCs were

identified at concentrations exceeding the TOGS AWQS in the sample collected from temporary

well TW-1 as shown in Table 3.2. These SVOCs were also detected Site soils at concentrations

exceeding the RSCOs. Numerous metals were detected in the unfiltered samples from all

temporary wells exceeding TOGS AWQS, but only manganese and sodium were detected in the

filtered samples in excess of TOGS AWQS.

Table 3.2 Summary of Groundwater Exceedances of TOGS AWQS

3.3 Soil Vapor Results

Five (5) soil vapor samples were collected during the investigation. The samples were sent to

Alpha, an ELAP-Certified laboratory, on a chain of custody (COC) for TO-15 analysis. All the soil

vapor samples were collected approximately 35 feet below grade surface in order to target a

depth between 2-5 feet above the observed groundwater table. The laboratory analytical reports

are included in Appendix C. Soil vapor sample locations and a summary of the results are shown

Analyte

NYSDEC Ambient

Groundwater

Quality Standards

Units TW-1 TW-2 TW-3 TW-4

Manganese, Dissolved 300 ug/l 5307 7655 5950 5856

Sodium, Dissolved 20000 ug/l 217000 424000 210000 202000

Benzo(a)anthracene 0.002 ug/l 0.04 ND ND ND

Benzo(a)pyrene 0 ug/l 0.02 ND ND ND

Benzo(b)fluoranthene 0.002 ug/l 0.02 ND ND ND

Benzo(k)fluoranthene 0.002 ug/l 0.02 ND ND ND

Chrysene 0.002 ug/l 0.01 ND ND ND

Indeno(1,2,3-cd)pyrene 0.002 ug/l 0.1 ND ND ND


on Figure 4. The attached Table 5 presents all soil vapor results compared to their United States

Environmental Protection Agency (USEPA) Vapor Intrusion Screening Level (VISL) Target Sub-

Slab Soil Gas Concentrations dated May 2018 and the New York State Department of Health

(NYSDOH) Sub-Slab Vapor Concentration Criteria for Evaluating Soil Vapor Intrusion dated May

2017.

As shown in table 3.3 below, trichloroethene was identified exceeding the NYSDOH criteria in two

samples, and tetrachloroethene was identified exceeding the NYSDOH Criteria in one sample.

The NYSDOH guidance indicates that these concentrations may require monitoring and/or

mitigation in the future, depending on the corresponding indoor air concentration. In addition, 1,3-

Butadiene and chloroform were identified at concentrations exceeding the USEPA-VISLs in all

samples, and benzene was identified exceeding the USEPA-VISL in two samples,.

Table 3.3 Summary of soil gas exceedances of the EPA and NYSDOH levels

Analyte USEPA

VISL

NYSDOH

Criteria SV-1 SV-2 SV-3 SV-4 SV-5

ug/m3 ug/m3 ug/m3 ug/m3 ug/m3 ug/m3 ug/m3

1,3-Butadiene 3.12 40 10.1 40.7 19.7 13

Chloroform 4.07 21.2 48.8 80.1 4.13 18.3

Benzene 12 17.5 6.8 16.7 7.54 5.43

Trichloroethene 15.9 6 4.53 2.83 71.5 20.8 3.78

Tetrachloroethene 360 100 ND 71.2 16.7 26.8 110

Notes:

ug/m3 = micrograms per cubic meter of air

SV = Soil Vapor Sample

Yellow Highlight = Concentration exceeds USEPA VISL and/or NYSDOH Criteria


4.0 CONCLUSIONS AND RECOMMENDATIONS

Semi-volatile organic compounds (SVOCs) and metals were identified in soils at concentrations

exceeding their respective RRSCOs in various samples. The SVOC exceedances are higher

than typical historic fill levels and are most likely a result of the Site historic activities that included

an auto repair shop.

Metal exceedances (mercury and lead) were also detected at levels that exceed the typical

historic fill concentrations. The source of the metals specifically mercury is most likely the result

of the historic plumbing activities and paint storage.

SVOCs were identified at concentrations exceeding the TOGS AWQS in the groundwater sample

collected from temporary well TW-1. The same SVOCs were detected in the soils at

concentrations that exceed the RRSCO. Numerous metals were detected in the unfiltered

samples from all temporary wells exceeding TOGS AWQS, but only manganese and sodium were

detected in the filtered samples in excess of TOGS AWQS.

Soil vapor samples indicated that trichloroethene was identified exceeding the NYSDOH criteria

in two samples, and tetrachloroethene was identified exceeding the NYSDOH Criteria in one

sample. The NYSDOH guidance indicates that these concentrations may require monitoring

and/or mitigation in the future, depending on the corresponding indoor air concentration. In

addition, 1,3-Butadiene and chloroform were identified at concentrations exceeding the USEPA-

VISLs in all samples, and benzene was identified exceeding the USEPA-VISL in two samples.

Further investigation is required to determine the extent of and identify the sources of the

contaminants that exceed their respective standards. Remediation will be required to mitigate

the soil and soil vapor exceedances to render the property suitable for development.

TABLES

Table 1

Metals in Soil

90-02 168th Street, Queens, New York

LOCATION NY 375-6.8(c) NY 375-6.8(a) NY 375-6.8(b)

SAMPLING DATE Residential Restricted Unrestricted

LAB SAMPLE ID Use Residential Use

SAMPLE TYPE

Units Results Qual Results Qual Results Qual Results Qual Results Qual Results Qual

Total Metals

Aluminum, Total mg/kg 3140 2550 8080 11600 10100 9330

Antimony, Total mg/kg 0.892 J 4.03 U 4.76 U 4.6 U 4.35 U 4.98 U

Arsenic, Total 16 16 13 mg/kg 3.97 2.49 3.44 3.52 1.49 3.86

Barium, Total 350 400 350 mg/kg 63.4 22.4 93 98.1 35.6 132

Beryllium, Total 14 72 7.2 mg/kg 0.168 J 0.193 J 0.466 J 0.396 J 0.148 J 0.518

Cadmium, Total 2.5 4.3 2.5 mg/kg 0.875 0.379 J 0.181 J 0.221 J 0.174 J 0.469 J

Calcium, Total mg/kg 2180 106000 1150 3350 689 2110

Chromium, Total mg/kg 8.44 9.35 11.5 19 20.4 15.5

Cobalt, Total mg/kg 3.84 5.34 4.9 6.71 8.31 4.38

Copper, Total 270 270 50 mg/kg 20.9 10.3 15.2 13.9 14.4 18.3

Iron, Total mg/kg 8940 10900 11900 15700 17900 11500

Lead, Total 400 400 63 mg/kg 127 17.3 248 113 5.15 231

Magnesium, Total mg/kg 923 46600 999 2500 2120 1310

Manganese, Total 2000 2000 1600 mg/kg 207 478 396 443 224 230

Mercury, Total 0.81 0.81 0.18 mg/kg 0.168 0.581 0.116 0.263 0.071 U 0.286

Nickel, Total 140 310 30 mg/kg 9.94 9.54 6.44 9.93 15.6 8.38

Potassium, Total mg/kg 300 256 258 465 908 405

Selenium, Total 36 180 3.9 mg/kg 0.395 J 0.298 J 0.762 J 0.405 J 1.74 U 1.99 U

Silver, Total 36 180 2 mg/kg 0.841 U 0.806 U 0.952 U 0.92 U 0.87 U 0.997 U

Sodium, Total mg/kg 134 J 131 J 304 220 232 246

Thallium, Total mg/kg 1.68 U 1.61 U 1.9 U 1.84 U 1.74 U 1.99 U

Vanadium, Total mg/kg 17.6 20.2 18.4 31.5 32 21

Zinc, Total 2200 10000 109 mg/kg 85.4 49.2 61.5 60.6 23.5 114

J : Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

U : Indicates the analyte was analyzed for but not detected.

Exceeds Unrestricted Standard

Exceeds Restricted Residential Standard

SESI-SB-6 (1-2)SESI-SB-5 (4-5)SESI-SB-3 (2-3)

8/29/2019

L1939567-05

SOIL

8/29/2019

L1939567-06

SOIL

L1939567-03

8/29/2019

SOIL SOIL

SESI-SB-4 (2-3)

8/29/2019

L1939567-04

SOIL

SESI-SB-1 (2-3)

8/29/2019

L1939567-01

SOIL

SESI-SB-2 (3-4)

8/29/2019

L1939567-02

Table 1

Metals in Soil





SAMPLE TYPE

Units

Total Metals

Aluminum, Total mg/kg

Antimony, Total mg/kg

Arsenic, Total 16 16 13 mg/kg

Barium, Total 350 400 350 mg/kg

Beryllium, Total 14 72 7.2 mg/kg

Cadmium, Total 2.5 4.3 2.5 mg/kg

Calcium, Total mg/kg

Chromium, Total mg/kg

Cobalt, Total mg/kg

Copper, Total 270 270 50 mg/kg

Iron, Total mg/kg

Lead, Total 400 400 63 mg/kg

Magnesium, Total mg/kg

Manganese, Total 2000 2000 1600 mg/kg

Mercury, Total 0.81 0.81 0.18 mg/kg

Nickel, Total 140 310 30 mg/kg

Potassium, Total mg/kg

Selenium, Total 36 180 3.9 mg/kg

Silver, Total 36 180 2 mg/kg

Sodium, Total mg/kg

Thallium, Total mg/kg

Vanadium, Total mg/kg

Zinc, Total 2200 10000 109 mg/kg





Results Qual Results Qual Results Qual Results Qual Results Qual Results Qual

7310 8930 9350 3380 5020 5530

0.761 J 0.39 J 1.11 J 1.12 J 0.811 J 1.26 J

8.32 4.92 3.47 2.4 3.02 3.94

238 144 48.7 289 73.8 109

0.318 J 0.486 0.358 J 0.105 J 0.239 J 0.276 J

1.04 J 0.209 J 0.447 J 0.631 J 0.384 J 0.528 J

4820 2060 1030 48800 1860 2610

18.5 16.4 15.7 11.2 11.3 13.3

6.53 5.31 6.32 3.23 4.7 4.72

60.3 19.8 45.9 22.2 17.6 22.5

12700 13300 15000 7350 9730 11100

717 576 25.1 405 185 386

1380 1230 1210 18600 1300 1580

158 416 182 159 196 146

0.745 0.712 0.073 U 0.228 0.253 0.343

13.4 9.12 7.81 5.88 8.86 8.64

403 376 331 276 468 256

1.65 J 0.504 J 0.232 J 1.62 U 1.71 U 1.57 U

1.14 U 0.952 U 0.894 U 0.809 U 0.854 U 0.787 U

372 277 154 J 238 308 239

2.27 U 1.9 U 1.79 U 1.62 U 1.71 U 1.57 U

28 24.7 24 20 19 21

221 91.5 118 171 157 190

SESI-SB-10 (2-3) SESI-SB-11 (3-4)

8/30/2019

L1939733-03

SOIL

SESI-SB-12 (6-7)

8/30/2019

L1939733-04

SOIL

SESI-SB-9 (1-2)SESI-SB-8 (2-3)SESI-SB-7 (3-4)

8/30/2019

L1939733-01

SOIL

8/30/2019

L1939733-02

SOIL

8/29/2019

L1939567-07

SOIL

8/29/2019

SOIL

L1939567-08

Table 1

Metals in Soil





SAMPLE TYPE

Units

Total Metals









Cobalt, Total mg/kg


Iron, Total mg/kg









Sodium, Total mg/kg









7820 7560 5230 3380 1800 5740

1.64 J 3.89 J 0.633 J 4 J 0.428 J 1.9 J

4.73 9.15 1.98 6.12 2.06 5.58

212 132 54.2 120 44 97.6

0.453 0.371 J 0.167 J 0.137 J 0.411 U 0.344 J

0.408 J 0.782 J 0.408 J 0.911 J 0.23 J 0.762 J

2580 4980 11000 117000 79800 2600

13.4 16.7 8.31 8.93 6.74 14.4

5.59 5.68 6 3.84 1.93 4.24

22 40.2 51.9 45.8 9.63 29.7

12700 18000 13300 25100 5250 12300

522 279 134 329 107 268

1130 1520 2010 38600 28800 1470

918 249 164 237 165 164

0.761 0.848 0.171 2.67 0.067 U 2.84

9.17 10.8 6.84 7.79 4.09 10

502 381 715 322 198 J 474

0.417 J 1.95 U 1.67 U 0.637 J 0.288 J 0.576 J

0.907 U 0.977 U 0.833 U 0.98 U 0.823 U 0.929 U

843 538 353 173 J 220 337

1.81 U 1.95 U 1.67 U 1.96 U 1.64 U 1.86 U

20.4 23.3 24.4 15.3 8.45 21.4

116 215 62.4 207 64.2 160

SESI-SB-14 (4-5) SESI-SB-18 (2-3)

8/30/2019

L1939733-10

SOIL

SESI-SB-16 (1-2)

8/30/2019

L1939733-08

SOIL

SESI-SB-17 (2-3)

8/30/2019

L1939733-09

SOIL

8/30/2019

L1939733-06

SOIL

SESI-SB-15 (2-3)

8/30/2019

L1939733-07

SOIL

SESI-SB-13 (3-4)

8/30/2019

L1939733-05

SOIL

Table 1

Metals in Soil





SAMPLE TYPE

Units

Total Metals









Cobalt, Total mg/kg


Iron, Total mg/kg









Sodium, Total mg/kg








SESI-SB-16 (14-15)

Results Qual Results Qual Results Qual Results Qual

13700 2620 1370 2610

1.56 J 4 U 4.76 U 4.09 U

4.85 0.536 J 3.1 0.565 J

74.2 17.7 31.3 22.2

0.531 0.112 J 0.476 U 0.106 J

0.43 J 0.152 J 0.257 J 0.172 J

933 372 176000 478

20.7 6.03 6.09 9.54

7.44 2.89 2.07 2.99

7.85 7.24 12.5 9.49

18800 6010 7940 6070

15.3 2.14 J 109 1.93 J

1780 864 91300 928

274 202 224 207

0.074 U 0.065 U 0.076 U 0.065 U

10 6.36 5.08 7.4

469 274 200 J 273

1.83 U 1.6 U 1.9 U 1.64 U

0.915 U 0.8 U 0.952 U 0.819 U

650 71.1 J 65.4 J 59.6 J

1.83 U 1.6 U 1.9 U 1.64 U

32.6 8.13 7.51 10.2

28.4 10.1 30.2 10.2

SESI-SB-20 (14-15)

9/3/2019

L1940104-02

SOIL

8/30/2019

L1939733-12

SOIL

SESI-SB-20 (2-3)

9/3/2019

L1940104-01

SOIL

SESI-SB-19 (4-5)

8/30/2019

L1939733-11

SOIL

Table 2

Volatile Organic Compounds in Soil


LOCATION NY 375-6.8(c) NY 375-6.8(a)NY 375-6.8(b)



SAMPLE TYPE

Units Results Qual Results Qual Results Qual Results Qual Results Qual Results Qual Results Qual Results Qual Results Qual Results Qual

Volatile Organics by EPA 5035

Methylene chloride 51 100 0.05 mg/kg 0.0051 U 0.0046 U 0.0052 U 0.0049 U 0.0046 U 0.0061 U 0.0064 U 0.0056 U 0.0045 U 0.0046 U

1,1-Dichloroethane 19 26 0.27 mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

Chloroform 10 49 0.37 mg/kg 0.0015 U 0.0014 U 0.0016 U 0.0015 U 0.0014 U 0.0018 U 0.0019 U 0.0017 U 0.0013 U 0.0014 U

Carbon tetrachloride 1.4 2.4 0.76 mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

1,2-Dichloropropane mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

Dibromochloromethane mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

1,1,2-Trichloroethane mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

Tetrachloroethene 5.5 19 1.3 mg/kg 0.00051 U 0.00046 U 0.00052 U 0.00049 U 0.00046 U 0.00061 U 0.00064 U 0.00056 U 0.00045 U 0.00046 U

Chlorobenzene 100 100 1.1 mg/kg 0.00051 U 0.00046 U 0.00052 U 0.00049 U 0.00046 U 0.00061 U 0.00064 U 0.00056 U 0.00045 U 0.00046 U

Trichlorofluoromethane mg/kg 0.0041 U 0.0037 U 0.0042 U 0.0039 U 0.0037 U 0.0048 U 0.0052 U 0.0044 U 0.0036 U 0.0037 U

1,2-Dichloroethane 2.3 3.1 0.02 mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

1,1,1-Trichloroethane 100 100 0.68 mg/kg 0.00051 U 0.00046 U 0.00052 U 0.00049 U 0.00046 U 0.00061 U 0.00064 U 0.00056 U 0.00045 U 0.00046 U

Bromodichloromethane mg/kg 0.00051 U 0.00046 U 0.00052 U 0.00049 U 0.00046 U 0.00061 U 0.00064 U 0.00056 U 0.00045 U 0.00046 U

trans-1,3-Dichloropropene mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

cis-1,3-Dichloropropene mg/kg 0.00051 U 0.00046 U 0.00052 U 0.00049 U 0.00046 U 0.00061 U 0.00064 U 0.00056 U 0.00045 U 0.00046 U

1,3-Dichloropropene, Total mg/kg 0.00051 U 0.00046 U 0.00052 U 0.00049 U 0.00046 U 0.00061 U 0.00064 U 0.00056 U 0.00045 U 0.00046 U

1,1-Dichloropropene mg/kg 0.00051 U 0.00046 U 0.00052 U 0.00049 U 0.00046 U 0.00061 U 0.00064 U 0.00056 U 0.00045 U 0.00046 U

Bromoform mg/kg 0.0041 U 0.0037 U 0.0042 U 0.0039 U 0.0037 U 0.0048 U 0.0052 U 0.0044 U 0.0036 U 0.0037 U

1,1,2,2-Tetrachloroethane mg/kg 0.00051 U 0.00046 U 0.00052 U 0.00049 U 0.00046 U 0.00061 U 0.00064 U 0.00056 U 0.00045 U 0.00046 U

Benzene 2.9 4.8 0.06 mg/kg 0.00051 U 0.00046 U 0.00052 U 0.00049 U 0.00046 U 0.00061 U 0.00064 U 0.00056 U 0.00045 U 0.00046 U

Toluene 100 100 0.7 mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

Ethylbenzene 30 41 1 mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

Chloromethane mg/kg 0.0041 U 0.0037 U 0.0042 U 0.0039 U 0.0037 U 0.0048 U 0.0052 U 0.0044 U 0.0036 U 0.0037 U

Bromomethane mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

Vinyl chloride 0.21 0.9 0.02 mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

Chloroethane mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

1,1-Dichloroethene 100 100 0.33 mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

trans-1,2-Dichloroethene 100 100 0.19 mg/kg 0.00041 J 0.00065 J 0.00056 J 0.00036 J 0.00053 J 0.00064 J 0.00038 J 0.00047 J 0.0013 U 0.0014 U

Trichloroethene 10 21 0.47 mg/kg 0.00051 U 0.00046 U 0.00052 U 0.00049 U 0.00046 U 0.00061 U 0.00064 U 0.00056 U 0.00045 U 0.00046 U

1,2-Dichlorobenzene 100 100 1.1 mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

1,3-Dichlorobenzene 17 49 2.4 mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

1,4-Dichlorobenzene 9.8 13 1.8 mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

Methyl tert butyl ether 62 100 0.93 mg/kg 0.0011 J 0.001 J 0.001 J 0.00077 J 0.00081 J 0.0011 J 0.0012 J 0.001 J 0.00074 J 0.00093 J

p/m-Xylene mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

o-Xylene mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

Xylenes, Total 100 100 0.26 mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

cis-1,2-Dichloroethene 59 100 0.25 mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

1,2-Dichloroethene, Total mg/kg 0.00041 J 0.00065 J 0.00056 J 0.00036 J 0.00053 J 0.00064 J 0.00038 J 0.00047 J 0.00089 U 0.00093 U

Dibromomethane mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

Styrene mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

Dichlorodifluoromethane mg/kg 0.01 U 0.0093 U 0.01 U 0.0098 U 0.0092 U 0.012 U 0.013 U 0.011 U 0.0089 U 0.0093 U

Acetone 100 100 0.05 mg/kg 0.14 0.18 0.076 0.098 0.15 0.014 0.22 0.23 0.7 E 0.2

Carbon disulfide mg/kg 0.01 U 0.0093 U 0.01 U 0.0098 U 0.0092 U 0.012 U 0.013 U 0.011 U 0.0089 U 0.0093 U

2-Butanone 100 100 0.12 mg/kg 0.01 U 0.0093 U 0.01 U 0.0098 U 0.0092 U 0.012 U 0.027 0.011 U 0.015 0.005 J

Vinyl acetate mg/kg 0.01 U 0.0093 U 0.01 U 0.0098 U 0.0092 U 0.012 U 0.013 U 0.011 U 0.0089 U 0.0093 U

4-Methyl-2-pentanone mg/kg 0.01 U 0.0093 U 0.01 U 0.0098 U 0.0092 U 0.012 U 0.013 U 0.011 U 0.0089 U 0.0093 U

1,2,3-Trichloropropane mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

2-Hexanone mg/kg 0.01 U 0.0093 U 0.01 U 0.0098 U 0.0092 U 0.012 U 0.013 U 0.011 U 0.0089 U 0.0093 U

Bromochloromethane mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U


1,2-Dibromoethane mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U


1,1,1,2-Tetrachloroethane mg/kg 0.00051 U 0.00046 U 0.00052 U 0.00049 U 0.00046 U 0.00061 U 0.00064 U 0.00056 U 0.00045 U 0.00046 U

Bromobenzene mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

n-Butylbenzene 100 100 12 mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

sec-Butylbenzene 100 100 11 mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

tert-Butylbenzene 100 100 5.9 mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

o-Chlorotoluene mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

p-Chlorotoluene mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

1,2-Dibromo-3-chloropropane mg/kg 0.0031 U 0.0028 U 0.0031 U 0.0029 U 0.0028 U 0.0036 U 0.0039 U 0.0033 U 0.0027 U 0.0028 U

Hexachlorobutadiene mg/kg 0.0041 U 0.0037 U 0.0042 U 0.0039 U 0.0037 U 0.0048 U 0.0052 U 0.0044 U 0.0036 U 0.0037 U

Isopropylbenzene mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

p-Isopropyltoluene mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

Naphthalene 100 100 12 mg/kg 0.0041 U 0.0037 U 0.0042 U 0.0039 U 0.0037 U 0.0048 U 0.0052 U 0.0044 U 0.0036 U 0.0037 U

Acrylonitrile mg/kg 0.0041 U 0.0037 U 0.0042 U 0.0039 U 0.0037 U 0.0048 U 0.0052 U 0.0044 U 0.0036 U 0.0037 U

n-Propylbenzene 100 100 3.9 mg/kg 0.001 U 0.00093 U 0.001 U 0.00098 U 0.00092 U 0.0012 U 0.0013 U 0.0011 U 0.00089 U 0.00093 U

1,2,3-Trichlorobenzene mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

1,2,4-Trichlorobenzene mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

1,3,5-Trimethylbenzene 47 52 8.4 mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

1,2,4-Trimethylbenzene 47 52 3.6 mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

1,4-Dioxane 9.8 13 0.1 mg/kg 0.082 U 0.074 U 0.084 U 0.078 U 0.074 U 0.097 U 0.1 U 0.089 U 0.071 U 0.074 U

p-Diethylbenzene mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

p-Ethyltoluene mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

1,2,4,5-Tetramethylbenzene mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

Ethyl ether mg/kg 0.002 U 0.0019 U 0.0021 U 0.002 U 0.0018 U 0.0024 U 0.0026 U 0.0022 U 0.0018 U 0.0018 U

trans-1,4-Dichloro-2-butene mg/kg 0.0051 U 0.0046 U 0.0052 U 0.0049 U 0.0046 U 0.0061 U 0.0064 U 0.0056 U 0.0045 U 0.0046 U





SOIL SOIL SOIL SOILSOIL SOIL SOIL SOIL SOIL SOIL

L1939567-08 L1939733-01 L1939733-02L1939567-01 L1939567-02 L1939567-03 L1939567-04 L1939567-05 L1939567-06 L1939567-07

8/30/2019 8/30/20198/29/2019 8/29/2019 8/29/2019 8/29/2019 8/29/2019 8/29/2019 8/29/2019 8/29/2019

SESI-SB-7 (3-4) SESI-SB-8 (2-3) SESI-SB-9 (1-2) SESI-SB-10 (2-3)SESI-SB-1 (2-3) SESI-SB-2 (3-4) SESI-SB-3 (2-3) SESI-SB-4 (2-3) SESI-SB-5 (4-5) SESI-SB-6 (1-2)

Table 2

Volatile Organic Compounds in Soil


LOCATION NY 375-6.8(c) NY 375-6.8(a)NY 375-6.8(b)



SAMPLE TYPE

Units

Volatile Organics by EPA 5035

Methylene chloride 51 100 0.05 mg/kg

1,1-Dichloroethane 19 26 0.27 mg/kg

Chloroform 10 49 0.37 mg/kg

Carbon tetrachloride 1.4 2.4 0.76 mg/kg

1,2-Dichloropropane mg/kg

Dibromochloromethane mg/kg

1,1,2-Trichloroethane mg/kg

Tetrachloroethene 5.5 19 1.3 mg/kg

Chlorobenzene 100 100 1.1 mg/kg

Trichlorofluoromethane mg/kg

1,2-Dichloroethane 2.3 3.1 0.02 mg/kg

1,1,1-Trichloroethane 100 100 0.68 mg/kg

Bromodichloromethane mg/kg

trans-1,3-Dichloropropene mg/kg

cis-1,3-Dichloropropene mg/kg

1,3-Dichloropropene, Total mg/kg

1,1-Dichloropropene mg/kg

Bromoform mg/kg

1,1,2,2-Tetrachloroethane mg/kg

Benzene 2.9 4.8 0.06 mg/kg

Toluene 100 100 0.7 mg/kg

Ethylbenzene 30 41 1 mg/kg

Chloromethane mg/kg

Bromomethane mg/kg

Vinyl chloride 0.21 0.9 0.02 mg/kg

Chloroethane mg/kg

1,1-Dichloroethene 100 100 0.33 mg/kg

trans-1,2-Dichloroethene 100 100 0.19 mg/kg

Trichloroethene 10 21 0.47 mg/kg

1,2-Dichlorobenzene 100 100 1.1 mg/kg


1,4-Dichlorobenzene 9.8 13 1.8 mg/kg

Methyl tert butyl ether 62 100 0.93 mg/kg

p/m-Xylene mg/kg

o-Xylene mg/kg

Xylenes, Total 100 100 0.26 mg/kg

cis-1,2-Dichloroethene 59 100 0.25 mg/kg

1,2-Dichloroethene, Total mg/kg

Dibromomethane mg/kg

Styrene mg/kg

Dichlorodifluoromethane mg/kg

Acetone 100 100 0.05 mg/kg

Carbon disulfide mg/kg

2-Butanone 100 100 0.12 mg/kg

Vinyl acetate mg/kg

4-Methyl-2-pentanone mg/kg

1,2,3-Trichloropropane mg/kg

2-Hexanone mg/kg

Bromochloromethane mg/kg


1,2-Dibromoethane mg/kg


1,1,1,2-Tetrachloroethane mg/kg

Bromobenzene mg/kg

n-Butylbenzene 100 100 12 mg/kg

sec-Butylbenzene 100 100 11 mg/kg

tert-Butylbenzene 100 100 5.9 mg/kg

o-Chlorotoluene mg/kg

p-Chlorotoluene mg/kg

1,2-Dibromo-3-chloropropane mg/kg

Hexachlorobutadiene mg/kg

Isopropylbenzene mg/kg

p-Isopropyltoluene mg/kg

Naphthalene 100 100 12 mg/kg

Acrylonitrile mg/kg

n-Propylbenzene 100 100 3.9 mg/kg

1,2,3-Trichlorobenzene mg/kg


1,3,5-Trimethylbenzene 47 52 8.4 mg/kg

1,2,4-Trimethylbenzene 47 52 3.6 mg/kg

1,4-Dioxane 9.8 13 0.1 mg/kg

p-Diethylbenzene mg/kg

p-Ethyltoluene mg/kg

1,2,4,5-Tetramethylbenzene mg/kg

Ethyl ether mg/kg

trans-1,4-Dichloro-2-butene mg/kg





SESI-SB-14 (4-5) SESI-SB-16 (14-15) SESI-SB-20 (14-15)

Results Qual Results Qual Results Qual Results Qual Results Qual Results Qual Results Qual Results Qual Results Qual Results Qual Results Qual Results Qual

0.0047 U 0.0044 U 0.006 U 0.0052 U 0.0049 U 0.005 U 0.0042 U 0.0056 U 0.0052 U 0.0048 U 0.0052 U 0.0053 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.0014 U 0.00013 J 0.00018 J 0.00017 J 0.0015 U 0.0015 U 0.0013 U 0.0017 U 0.00015 J 0.0014 U 0.0015 U 0.0016 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.00047 U 0.00046 0.00028 J 0.00045 J 0.00049 U 0.0005 U 0.00042 U 0.00056 U 0.00052 U 0.00048 U 0.00052 U 0.00053 U

0.00047 U 0.00044 U 0.0006 U 0.00052 U 0.00049 U 0.0005 U 0.00042 U 0.00056 U 0.00052 U 0.00048 U 0.00052 U 0.00053 U

0.0037 U 0.0035 U 0.0048 U 0.0042 U 0.0039 U 0.004 U 0.0034 U 0.0045 U 0.0041 U 0.0038 U 0.0041 U 0.0042 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.00047 U 0.00044 U 0.0006 U 0.00052 U 0.00049 U 0.0005 U 0.00042 U 0.00056 U 0.00052 U 0.00048 U 0.00052 U 0.00053 U

0.00047 U 0.00044 U 0.0006 U 0.00052 U 0.00049 U 0.0005 U 0.00042 U 0.00056 U 0.00052 U 0.00048 U 0.00052 U 0.00053 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.00047 U 0.00044 U 0.0006 U 0.00052 U 0.00049 U 0.0005 U 0.00042 U 0.00056 U 0.00052 U 0.00048 U 0.00052 U 0.00053 U

0.00047 U 0.00044 U 0.0006 U 0.00052 U 0.00049 U 0.0005 U 0.00042 U 0.00056 U 0.00052 U 0.00048 U 0.00052 U 0.00053 U

0.00047 U 0.00044 U 0.0006 U 0.00052 U 0.00049 U 0.0005 U 0.00042 U 0.00056 U 0.00052 U 0.00048 U 0.00052 U 0.00053 U

0.0037 U 0.0035 U 0.0048 U 0.0042 U 0.0039 U 0.004 U 0.0034 U 0.0045 U 0.0041 U 0.0038 U 0.0041 U 0.0042 U

0.00047 U 0.00044 U 0.0006 U 0.00052 U 0.00049 U 0.0005 U 0.00042 U 0.00056 U 0.00052 U 0.00048 U 0.00052 U 0.00053 U

0.00047 U 0.00044 U 0.0006 U 0.00052 U 0.00049 U 0.0005 U 0.00042 U 0.00056 U 0.00052 U 0.00048 U 0.00052 U 0.00053 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00057 J 0.001 U 0.001 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.0037 U 0.0035 U 0.0048 U 0.0042 U 0.0039 U 0.004 U 0.0034 U 0.0045 U 0.0041 U 0.0038 U 0.0041 U 0.0042 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.0014 U 0.0013 U 0.0018 U 0.0016 U 0.0015 U 0.0015 U 0.0013 U 0.0017 U 0.0016 U 0.0014 U 0.0015 U 0.0016 U

0.00047 U 0.00044 U 0.0006 U 0.00052 U 0.00049 U 0.0005 U 0.00042 U 0.00056 U 0.00052 U 0.00048 U 0.00052 U 0.00053 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.00091 J 0.00095 J 0.001 J 0.0011 J 0.001 J 0.001 J 0.00093 J 0.00066 J 0.001 J 0.0012 J 0.0017 J 0.0022

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.0093 U 0.0088 U 0.012 U 0.01 U 0.0098 U 0.01 U 0.0085 U 0.011 U 0.01 U 0.0095 U 0.01 U 0.01 U

0.48 E 0.49 E 0.18 0.54 E 0.2 0.21 0.24 0.11 0.29 0.51 E 0.015 0.19

0.0093 U 0.0088 U 0.012 U 0.01 U 0.0098 U 0.01 U 0.0085 U 0.011 U 0.01 U 0.0095 U 0.01 U 0.01 U

0.011 0.012 0.0051 J 0.013 0.0061 J 0.0055 J 0.0061 J 0.011 U 0.008 J 0.014 0.01 U 0.0027 J

0.0093 U 0.0088 U 0.012 U 0.01 U 0.0098 U 0.01 U 0.0085 U 0.011 U 0.01 U 0.0095 U 0.01 U 0.01 U

0.0093 U 0.0088 U 0.012 U 0.01 U 0.0098 U 0.01 U 0.0085 U 0.011 U 0.01 U 0.0095 U 0.01 U 0.01 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.0093 U 0.0088 U 0.012 U 0.01 U 0.0098 U 0.01 U 0.0085 U 0.011 U 0.01 U 0.0095 U 0.01 U 0.01 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.00047 U 0.00044 U 0.0006 U 0.00052 U 0.00049 U 0.0005 U 0.00042 U 0.00056 U 0.00052 U 0.00048 U 0.00052 U 0.00053 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.0028 U 0.0026 U 0.0036 U 0.0031 U 0.0029 U 0.003 U 0.0026 U 0.0034 U 0.0031 U 0.0028 U 0.0031 U 0.0032 U

0.0037 U 0.0035 U 0.0048 U 0.0042 U 0.0039 U 0.004 U 0.0034 U 0.0045 U 0.0041 U 0.0038 U 0.0041 U 0.0042 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.0037 U 0.0035 U 0.0048 U 0.0042 U 0.0039 U 0.004 U 0.0034 U 0.0045 U 0.0041 U 0.0038 U 0.0041 U 0.0042 U

0.0037 U 0.0035 U 0.0048 U 0.0042 U 0.0039 U 0.004 U 0.0034 U 0.0045 U 0.0041 U 0.0038 U 0.0041 U 0.0042 U

0.00093 U 0.00088 U 0.0012 U 0.001 U 0.00098 U 0.001 U 0.00085 U 0.0011 U 0.001 U 0.00095 U 0.001 U 0.001 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.074 U 0.07 U 0.096 U 0.084 U 0.078 U 0.08 U 0.068 U 0.09 U 0.083 U 0.076 U 0.082 U 0.084 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.0019 U 0.0018 U 0.0024 U 0.0021 U 0.002 U 0.002 U 0.0017 U 0.0023 U 0.0021 U 0.0019 U 0.0021 U 0.0021 U

0.0047 U 0.0044 U 0.006 U 0.0052 U 0.0049 U 0.005 U 0.0042 U 0.0056 U 0.0052 U 0.0048 U 0.0052 U 0.0053 U

SOIL SOIL SOIL SOIL SOILSOIL SOIL SOIL SOIL SOILSOIL SOIL

L1939733-11 L1939733-12 L1940104-01 L1940104-02L1939733-06 L1939733-07 L1939733-08 L1939733-09 L1939733-10L1939733-03 L1939733-04 L1939733-05

8/30/2019 9/3/2019 9/3/20198/30/2019 8/30/2019 8/30/2019 8/30/2019 8/30/2019 8/30/20198/30/2019 8/30/2019 8/30/2019

SESI-SB-19 (4-5) SESI-SB-20 (2-3)SESI-SB-13 (3-4) SESI-SB-15 (2-3) SESI-SB-16 (1-2) SESI-SB-17 (2-3) SESI-SB-18 (2-3)SESI-SB-11 (3-4) SESI-SB-12 (6-7)

Table 3

Pesticides and PCB's in Soil





SAMPLE TYPE


General Chemistry

Solids, Total % 93.4 96.4 83.5 85 88.6 78.9

Cyanide, Total 27 27 27 mg/kg 1 U 0.96 U 1.2 U 1.2 U 1 U 1.2 U

Organochlorine Pesticides by GC

Delta-BHC 100 100 0.04 mg/kg 0.00162 U 0.00161 U 0.00189 U 0.0018 U 0.00174 U 0.00193 U

Lindane 0.28 1.3 0.1 mg/kg 0.000676 U 0.00067 U 0.000787 U 0.000752 U 0.000726 U 0.000805 U

Alpha-BHC 0.097 0.48 0.02 mg/kg 0.000676 U 0.00067 U 0.000787 U 0.000752 U 0.000726 U 0.000805 U

Beta-BHC 0.072 0.36 0.036 mg/kg 0.00162 U 0.00161 U 0.00189 U 0.0018 U 0.00174 U 0.00193 U

Heptachlor 0.42 2.1 0.042 mg/kg 0.000812 U 0.000804 U 0.000945 U 0.000903 U 0.000872 U 0.000966 U

Aldrin 0.019 0.097 0.005 mg/kg 0.00162 U 0.00161 U 0.00189 U 0.0018 U 0.00174 U 0.00193 U

Heptachlor epoxide mg/kg 0.00304 U 0.00301 U 0.00354 U 0.00338 U 0.00327 U 0.00362 U

Endrin 2.2 11 0.014 mg/kg 0.000676 U 0.00067 U 0.000787 U 0.000752 U 0.000726 U 0.000805 U

Endrin aldehyde mg/kg 0.00203 U 0.00201 U 0.00236 U 0.00226 U 0.00218 U 0.00241 U

Endrin ketone mg/kg 0.00162 U 0.00161 U 0.00189 U 0.0018 U 0.00174 U 0.00193 U

Dieldrin 0.039 0.2 0.005 mg/kg 0.00101 U 0.001 U 0.00118 U 0.00113 U 0.00109 U 0.00121 U

4,4'-DDE 1.8 8.9 0.0033 mg/kg 0.00162 U 0.00161 U 0.00189 U 0.0018 U 0.00174 U 0.00193 U

4,4'-DDD 2.6 13 0.0033 mg/kg 0.00162 U 0.00161 U 0.00189 U 0.0018 U 0.00174 U 0.00193 U

4,4'-DDT 1.7 7.9 0.0033 mg/kg 0.00304 U 0.00301 U 0.00354 U 0.00338 U 0.00327 U 0.00362 U

Endosulfan I 4.8 24 2.4 mg/kg 0.00162 U 0.00161 U 0.00189 U 0.0018 U 0.00174 U 0.00193 U

Endosulfan II 4.8 24 2.4 mg/kg 0.00162 U 0.00161 U 0.00189 U 0.0018 U 0.00174 U 0.00193 U

Endosulfan sulfate 4.8 24 2.4 mg/kg 0.000676 U 0.00067 U 0.000787 U 0.000752 U 0.000726 U 0.000805 U

Methoxychlor mg/kg 0.00304 U 0.00301 U 0.00354 U 0.00338 U 0.00327 U 0.00362 U

Toxaphene mg/kg 0.0304 U 0.0301 U 0.0354 U 0.0338 U 0.0327 U 0.0362 U

cis-Chlordane 0.91 4.2 0.094 mg/kg 0.00169 J 0.00201 U 0.00236 U 0.00226 U 0.00218 U 0.00241 U

trans-Chlordane mg/kg 0.00134 JIP 0.00201 U 0.00236 U 0.00226 U 0.00218 U 0.00241 U

Chlordane mg/kg 0.0132 U 0.013 U 0.0154 U 0.0147 U 0.0142 U 0.0157 U

Polychlorinated Biphenyls by GC

Aroclor 1016 1 1 0.1 mg/kg 0.0354 U 0.0326 U 0.0382 U 0.037 U 0.0362 U 0.0413 U





Aroclor 1254 1 1 0.1 mg/kg 0.0354 U 0.0326 U 0.0382 U 0.0094 J 0.0362 U 0.0413 U

Aroclor 1260 1 1 0.1 mg/kg 0.00922 J 0.0326 U 0.0382 U 0.037 U 0.0362 U 0.0413 U



PCBs, Total 1 1 0.1 mg/kg 0.00922 J 0.0326 U 0.0382 U 0.0094 J 0.0362 U 0.0413 U





SOIL SOIL SOIL SOIL SOIL SOIL

L1939567-01 L1939567-02 L1939567-03 L1939567-04 L1939567-05 L1939567-06

8/29/2019 8/29/2019 8/29/2019 8/29/2019 8/29/2019 8/29/2019

SESI-SB-1 (2-3) SESI-SB-2 (3-4) SESI-SB-3 (2-3) SESI-SB-4 (2-3) SESI-SB-5 (4-5) SESI-SB-6 (1-2)

Table 3






SAMPLE TYPE

Units

General Chemistry

Solids, Total %

Cyanide, Total 27 27 27 mg/kg


Delta-BHC 100 100 0.04 mg/kg

Lindane 0.28 1.3 0.1 mg/kg

Alpha-BHC 0.097 0.48 0.02 mg/kg

Beta-BHC 0.072 0.36 0.036 mg/kg

Heptachlor 0.42 2.1 0.042 mg/kg

Aldrin 0.019 0.097 0.005 mg/kg

Heptachlor epoxide mg/kg

Endrin 2.2 11 0.014 mg/kg

Endrin aldehyde mg/kg

Endrin ketone mg/kg

Dieldrin 0.039 0.2 0.005 mg/kg

4,4'-DDE 1.8 8.9 0.0033 mg/kg

4,4'-DDD 2.6 13 0.0033 mg/kg

4,4'-DDT 1.7 7.9 0.0033 mg/kg

Endosulfan I 4.8 24 2.4 mg/kg

Endosulfan II 4.8 24 2.4 mg/kg

Endosulfan sulfate 4.8 24 2.4 mg/kg

Methoxychlor mg/kg

Toxaphene mg/kg

cis-Chlordane 0.91 4.2 0.094 mg/kg

trans-Chlordane mg/kg

Chlordane mg/kg


Aroclor 1016 1 1 0.1 mg/kg









PCBs, Total 1 1 0.1 mg/kg






69.3 80.8 86.9 96.3 89.1 95.7

1.4 U 1.2 U 1.1 U 0.95 U 0.24 J 0.96 U

0.00226 U 0.00195 U 0.00181 U 0.0016 U 0.00177 U 0.00159 U

0.000942 U 0.000811 U 0.000756 U 0.000666 U 0.000738 U 0.000663 U

0.000942 U 0.000811 U 0.000756 U 0.000666 U 0.000738 U 0.000663 U

0.00226 U 0.00195 U 0.00181 U 0.0016 U 0.00177 U 0.00159 U

0.00113 U 0.000973 U 0.000907 U 0.000799 U 0.000886 U 0.000796 U

0.00226 U 0.00195 U 0.00181 U 0.0016 U 0.00177 U 0.00159 U

0.00424 U 0.00365 U 0.0034 U 0.003 U 0.00332 U 0.00298 U

0.000942 U 0.000811 U 0.000756 U 0.000666 U 0.000738 U 0.000663 U

0.00282 U 0.00243 U 0.00227 U 0.002 U 0.00222 U 0.00199 U

0.00226 U 0.00195 U 0.00181 U 0.0016 U 0.00177 U 0.00159 U

0.00141 U 0.00122 U 0.00113 U 0.000998 U 0.00111 U 0.000994 U

0.00226 U 0.00195 U 0.000987 JIP 0.00603 0.00156 JIP 0.00902 IP

0.00271 IP 0.00168 J 0.00181 U 0.00342 0.00177 U 0.00646

0.00424 U 0.00365 U 0.0034 U 0.003 U 0.00332 U 0.0354

0.00226 U 0.00195 U 0.00181 U 0.0016 U 0.00177 U 0.00159 U

0.00226 U 0.00195 U 0.00181 U 0.0016 U 0.00177 U 0.00159 U

0.000942 U 0.000811 U 0.000756 U 0.000666 U 0.000738 U 0.000663 U

0.00424 U 0.00365 U 0.0034 U 0.003 U 0.00332 U 0.00298 U

0.0424 U 0.0365 U 0.034 U 0.03 U 0.0332 U 0.0298 U

0.00282 U 0.00243 U 0.00227 U 0.002 U 0.00222 U 0.00645 IP

0.00282 U 0.000796 JIP 0.00227 U 0.002 U 0.00222 U 0.0098 IP

0.0184 U 0.0158 U 0.0147 U 0.013 U 0.0144 U 0.0129 U

0.0461 U 0.0388 U 0.0368 U 0.0331 U 0.0355 U 0.0331 U

0.0461 U 0.0388 U 0.0368 U 0.0331 U 0.0355 U 0.0331 U

0.0461 U 0.0388 U 0.0368 U 0.0331 U 0.0355 U 0.0331 U

0.0461 U 0.0388 U 0.0368 U 0.0331 U 0.0355 U 0.0331 U

0.0461 U 0.0388 U 0.0368 U 0.0331 U 0.0355 U 0.0331 U

0.0461 U 0.0388 U 0.0368 U 0.0331 U 0.0355 U 0.0331 U

0.0284 J 0.0388 U 0.0368 U 0.015 J 0.0134 J 0.0331 U

0.0461 U 0.0388 U 0.0368 U 0.0331 U 0.0355 U 0.0331 U

0.0136 J 0.0388 U 0.0368 U 0.0331 U 0.0355 U 0.0331 U

0.042 J 0.0388 U 0.0368 U 0.015 J 0.0134 J 0.0331 U


L1939567-08 L1939733-01 L1939733-02 L1939733-03 L1939733-04L1939567-07

8/30/2019 8/30/2019 8/30/2019 8/30/20198/29/2019 8/29/2019


Table 3






SAMPLE TYPE

Units

General Chemistry

Solids, Total %





Alpha-BHC 0.097 0.48 0.02 mg/kg

Beta-BHC 0.072 0.36 0.036 mg/kg


Aldrin 0.019 0.097 0.005 mg/kg




Endrin ketone mg/kg


4,4'-DDE 1.8 8.9 0.0033 mg/kg

4,4'-DDD 2.6 13 0.0033 mg/kg

4,4'-DDT 1.7 7.9 0.0033 mg/kg




Methoxychlor mg/kg

Toxaphene mg/kg



Chlordane mg/kg

















85.3 78.3 92.3 81 95.4 85.5

0.41 J 1.2 U 1 U 1.2 U 0.96 U 1.1 U

0.00182 U 0.00195 U 0.00168 U 0.00187 U 0.00158 U 0.00181 U

0.000758 U 0.000812 U 0.000699 U 0.000781 U 0.000659 U 0.000756 U

0.000758 U 0.000812 U 0.000699 U 0.000781 U 0.000659 U 0.000756 U

0.00182 U 0.00195 U 0.00168 U 0.00187 U 0.00158 U 0.00181 U

0.00091 U 0.000974 U 0.000839 U 0.000937 U 0.000791 U 0.000907 U

0.00182 U 0.00195 U 0.00168 U 0.00187 U 0.00158 U 0.00181 U

0.00341 U 0.00365 U 0.00314 U 0.00351 U 0.00297 U 0.0034 U

0.000758 U 0.000812 U 0.000699 U 0.000781 U 0.000659 U 0.000756 U

0.00227 U 0.00244 U 0.0021 U 0.00234 U 0.00198 U 0.00227 U

0.00182 U 0.00195 U 0.00168 U 0.00187 U 0.00158 U 0.00181 U

0.00114 U 0.00122 U 0.00105 U 0.00117 U 0.000989 U 0.00113 U

0.00182 U 0.0259 0.00142 JIP 0.00187 U 0.0038 IP 0.0022 IP

0.00182 U 0.00257 0.00168 U 0.00187 U 0.00158 U 0.0018 JIP

0.00341 U 0.00711 IP 0.00269 J 0.00351 U 0.00718 0.0034 U

0.00182 U 0.00195 U 0.00168 U 0.00187 U 0.00158 U 0.00181 U

0.00182 U 0.00195 U 0.00168 U 0.00187 U 0.00158 U 0.00181 U

0.000758 U 0.000812 U 0.000699 U 0.000781 U 0.000659 U 0.000756 U

0.00341 U 0.00365 U 0.00314 U 0.00351 U 0.00297 U 0.0034 U

0.0341 U 0.0365 U 0.0314 U 0.0351 U 0.0297 U 0.034 U

0.00227 U 0.00244 U 0.00408 IP 0.00234 U 0.000768 JIP 0.00227 U

0.00227 U 0.00244 U 0.00379 IP 0.00234 U 0.000892 JIP 0.00227 U

0.0148 U 0.0158 U 0.0136 U 0.0152 U 0.0128 U 0.0147 U

0.0372 U 0.0401 U 0.0351 U 0.0394 U 0.034 U 0.0372 U

0.0372 U 0.0401 U 0.0351 U 0.0394 U 0.034 U 0.0372 U

0.0372 U 0.0401 U 0.0351 U 0.0394 U 0.034 U 0.0372 U

0.0372 U 0.0401 U 0.0351 U 0.0394 U 0.034 U 0.0372 U

0.0372 U 0.0401 U 0.0351 U 0.0394 U 0.034 U 0.0372 U

0.0372 U 0.0401 U 0.0351 U 0.0394 U 0.034 U 0.0372 U

0.0372 U 0.0401 U 0.0351 U 0.00798 J 0.034 U 0.00837 J

0.0372 U 0.0401 U 0.0351 U 0.0394 U 0.034 U 0.0372 U

0.0372 U 0.0401 U 0.0351 U 0.0394 U 0.034 U 0.0372 U

0.0372 U 0.0401 U 0.0351 U 0.00798 J 0.034 U 0.00837 J

SOILSOIL SOIL SOIL SOIL SOIL

L1939733-06 L1939733-07 L1939733-08 L1939733-09 L1939733-10L1939733-05

8/30/2019 8/30/2019 8/30/2019 8/30/2019 8/30/20198/30/2019


Table 3






SAMPLE TYPE

Units

General Chemistry

Solids, Total %





Alpha-BHC 0.097 0.48 0.02 mg/kg

Beta-BHC 0.072 0.36 0.036 mg/kg


Aldrin 0.019 0.097 0.005 mg/kg




Endrin ketone mg/kg


4,4'-DDE 1.8 8.9 0.0033 mg/kg

4,4'-DDD 2.6 13 0.0033 mg/kg

4,4'-DDT 1.7 7.9 0.0033 mg/kg




Methoxychlor mg/kg

Toxaphene mg/kg



Chlordane mg/kg
















Results Qual Results Qual Results Qual Results Qual

84.6 96.2 83 96

1.1 U 1 U 1.2 U 1 U

0.00179 U 0.00156 U 0.00186 U 0.00159 U

0.000748 U 0.000651 U 0.000777 U 0.000661 U

0.000748 U 0.000651 U 0.000777 U 0.000661 U

0.00179 U 0.00156 U 0.00186 U 0.00159 U

0.000897 U 0.000781 U 0.000932 U 0.000794 U

0.00179 U 0.00156 U 0.00186 U 0.00159 U

0.00336 U 0.00293 U 0.0035 U 0.00298 U

0.000748 U 0.000651 U 0.000777 U 0.000661 U

0.00224 U 0.00195 U 0.00233 U 0.00198 U

0.00179 U 0.00156 U 0.00186 U 0.00159 U

0.00112 U 0.000976 U 0.00116 U 0.000992 U

0.00179 U 0.00156 U 0.00298 0.00159 U

0.00179 U 0.00156 U 0.0026 0.00159 U

0.00336 U 0.00293 U 0.00166 JIP 0.00298 U

0.00179 U 0.00156 U 0.00186 U 0.00159 U

0.00179 U 0.00156 U 0.00186 U 0.00159 U

0.000748 U 0.000651 U 0.000777 U 0.000661 U

0.00336 U 0.00293 U 0.0035 U 0.00298 U

0.0336 U 0.0293 U 0.035 U 0.0298 U

0.00224 U 0.00195 U 0.000946 JIP 0.00198 U

0.00224 U 0.00195 U 0.00233 U 0.00198 U

0.0146 U 0.0127 U 0.0151 U 0.0129 U

0.0387 U 0.0333 U 0.0389 U 0.0335 U

0.0387 U 0.0333 U 0.0389 U 0.0335 U

0.0387 U 0.0333 U 0.0389 U 0.0335 U

0.0387 U 0.0333 U 0.0389 U 0.0335 U

0.0387 U 0.0333 U 0.0389 U 0.0335 U

0.0387 U 0.0333 U 0.0389 U 0.0335 U

0.0387 U 0.0333 U 0.0389 U 0.0335 U

0.0387 U 0.0333 U 0.0389 U 0.0335 U

0.0387 U 0.0333 U 0.0389 U 0.0335 U

0.0387 U 0.0333 U 0.0389 U 0.0335 U

SESI-SB-20 (14-15)SESI-SB-16 (14-15)

SOIL SOIL SOIL SOIL

L1939733-11 L1939733-12 L1940104-01 L1940104-02

8/30/2019 9/3/2019 9/3/20198/30/2019

SESI-SB-19 (4-5) SESI-SB-20 (2-3)

Table 4

Semivolatile Organic Compounds in Soil





SAMPLE TYPE


Semivolatile Organics by GC/MS

Acenaphthene 100 100 20 mg/kg 0.34 J 0.047 J 0.16 U 0.095 J 0.15 U 0.16 U

1,2,4-Trichlorobenzene mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

Hexachlorobenzene 0.33 1.2 0.33 mg/kg 0.53 U 0.1 U 0.12 U 0.12 U 0.11 U 0.12 U

Bis(2-chloroethyl)ether mg/kg 0.79 U 0.15 U 0.18 U 0.17 U 0.17 U 0.18 U

2-Chloronaphthalene mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

1,2-Dichlorobenzene 100 100 1.1 mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

1,3-Dichlorobenzene 17 49 2.4 mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

1,4-Dichlorobenzene 9.8 13 1.8 mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

3,3'-Dichlorobenzidine mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

2,4-Dinitrotoluene mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

2,6-Dinitrotoluene mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

Fluoranthene 100 100 100 mg/kg 6.1 1.1 1 2.4 0.11 U 0.06 J

4-Chlorophenyl phenyl ether mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

4-Bromophenyl phenyl ether mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

Bis(2-chloroisopropyl)ether mg/kg 1 U 0.2 U 0.24 U 0.23 U 0.22 U 0.25 U

Bis(2-chloroethoxy)methane mg/kg 0.95 U 0.18 U 0.21 U 0.21 U 0.2 U 0.22 U

Hexachlorobutadiene mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

Hexachlorocyclopentadiene mg/kg 2.5 U 0.48 U 0.57 U 0.55 U 0.54 U 0.59 U

Hexachloroethane mg/kg 0.71 U 0.14 U 0.16 U 0.15 U 0.15 U 0.16 U

Isophorone mg/kg 0.79 U 0.15 U 0.18 U 0.17 U 0.17 U 0.18 U

Naphthalene 100 100 12 mg/kg 0.16 J 0.039 J 0.2 U 0.06 J 0.19 U 0.21 U

Nitrobenzene mg/kg 0.79 U 0.15 U 0.18 U 0.17 U 0.17 U 0.18 U

NDPA/DPA mg/kg 0.71 U 0.14 U 0.16 U 0.15 U 0.15 U 0.16 U

n-Nitrosodi-n-propylamine mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

Bis(2-ethylhexyl)phthalate mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

Butyl benzyl phthalate mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

Di-n-butylphthalate mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

Di-n-octylphthalate mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

Diethyl phthalate mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

Dimethyl phthalate mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

Benzo(a)anthracene 1 1 1 mg/kg 3.2 0.63 0.52 1.3 0.11 U 0.039 J

Benzo(a)pyrene 1 1 1 mg/kg 2.8 0.55 0.56 1.1 0.15 U 0.16 U

Benzo(b)fluoranthene 1 1 1 mg/kg 3.6 0.69 0.7 1.2 0.11 U 0.047 J

Benzo(k)fluoranthene 1 3.9 0.8 mg/kg 1.5 0.28 0.28 0.5 0.11 U 0.12 U

Chrysene 1 3.9 1 mg/kg 2.8 0.58 0.43 1.1 0.11 U 0.034 J

Acenaphthylene 100 100 100 mg/kg 0.51 J 0.027 J 0.1 J 0.27 0.15 U 0.16 U

Anthracene 100 100 100 mg/kg 1.4 0.19 0.068 J 0.59 0.11 U 0.12 U

Benzo(ghi)perylene 100 100 100 mg/kg 1.9 0.33 0.36 0.8 0.15 U 0.027 J

Fluorene 100 100 30 mg/kg 0.44 J 0.053 J 0.2 U 0.16 J 0.19 U 0.21 U

Phenanthrene 100 100 100 mg/kg 4.6 0.71 0.13 1.9 0.11 U 0.029 J

Dibenzo(a,h)anthracene 0.33 0.33 0.33 mg/kg 0.38 J 0.1 0.091 J 0.21 0.11 U 0.12 U

Indeno(1,2,3-cd)pyrene 0.5 0.5 0.5 mg/kg 2.2 0.37 0.4 0.85 0.15 U 0.16 U

Pyrene 100 100 100 mg/kg 4.7 0.96 0.94 2.2 0.11 U 0.048 J

Biphenyl mg/kg 2 U 0.38 U 0.45 U 0.44 U 0.43 U 0.47 U

4-Chloroaniline mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

2-Nitroaniline mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U



Dibenzofuran 14 59 7 mg/kg 0.25 J 0.033 J 0.2 U 0.084 J 0.19 U 0.21 U

2-Methylnaphthalene mg/kg 1 U 0.2 U 0.24 U 0.038 J 0.22 U 0.25 U

1,2,4,5-Tetrachlorobenzene mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

Acetophenone mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

2,4,6-Trichlorophenol mg/kg 0.53 U 0.1 U 0.12 U 0.12 U 0.11 U 0.12 U

p-Chloro-m-cresol mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

2-Chlorophenol mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

2,4-Dichlorophenol mg/kg 0.79 U 0.15 U 0.18 U 0.17 U 0.17 U 0.18 U

2,4-Dimethylphenol mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

2-Nitrophenol mg/kg 1.9 U 0.36 U 0.43 U 0.41 U 0.4 U 0.44 U

4-Nitrophenol mg/kg 1.2 U 0.24 U 0.28 U 0.27 U 0.26 U 0.29 U

2,4-Dinitrophenol mg/kg 4.2 U 0.81 U 0.95 U 0.92 U 0.9 U 0.99 U

4,6-Dinitro-o-cresol mg/kg 2.3 U 0.44 U 0.52 U 0.5 U 0.49 U 0.54 U

Pentachlorophenol 2.4 6.7 0.8 mg/kg 0.71 U 0.14 U 0.16 U 0.15 U 0.15 U 0.16 U

Phenol 100 100 0.33 mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

2-Methylphenol 100 100 0.33 mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

3-Methylphenol/4-Methylphenol 34 100 0.33 mg/kg 1.3 U 0.24 U 0.28 U 0.28 U 0.27 U 0.3 U

2,4,5-Trichlorophenol mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

Benzoic Acid mg/kg 2.9 U 0.55 U 0.64 U 0.62 U 0.61 U 0.67 U

Benzyl Alcohol mg/kg 0.88 U 0.17 U 0.2 U 0.19 U 0.19 U 0.21 U

Carbazole mg/kg 0.69 J 0.074 J 0.2 U 0.23 0.19 U 0.21 U

1,4-Dioxane 9.8 13 0.1 mg/kg 0.13 U 0.025 U 0.03 U 0.029 U 0.028 U 0.031 U



Exceeds Residential Use Standard




L1939567-01 L1939567-02 L1939567-03 L1939567-04 L1939567-05 L1939567-06

8/29/2019 8/29/2019 8/29/2019 8/29/2019 8/29/2019 8/29/2019


Table 4






SAMPLE TYPE

Units


Acenaphthene 100 100 20 mg/kg


Hexachlorobenzene 0.33 1.2 0.33 mg/kg

Bis(2-chloroethyl)ether mg/kg

2-Chloronaphthalene mg/kg




3,3'-Dichlorobenzidine mg/kg

2,4-Dinitrotoluene mg/kg


Fluoranthene 100 100 100 mg/kg

4-Chlorophenyl phenyl ether mg/kg

4-Bromophenyl phenyl ether mg/kg

Bis(2-chloroisopropyl)ether mg/kg

Bis(2-chloroethoxy)methane mg/kg


Hexachlorocyclopentadiene mg/kg

Hexachloroethane mg/kg

Isophorone mg/kg


Nitrobenzene mg/kg

NDPA/DPA mg/kg

n-Nitrosodi-n-propylamine mg/kg

Bis(2-ethylhexyl)phthalate mg/kg

Butyl benzyl phthalate mg/kg

Di-n-butylphthalate mg/kg

Di-n-octylphthalate mg/kg

Diethyl phthalate mg/kg

Dimethyl phthalate mg/kg

Benzo(a)anthracene 1 1 1 mg/kg

Benzo(a)pyrene 1 1 1 mg/kg

Benzo(b)fluoranthene 1 1 1 mg/kg

Benzo(k)fluoranthene 1 3.9 0.8 mg/kg

Chrysene 1 3.9 1 mg/kg

Acenaphthylene 100 100 100 mg/kg

Anthracene 100 100 100 mg/kg

Benzo(ghi)perylene 100 100 100 mg/kg

Fluorene 100 100 30 mg/kg

Phenanthrene 100 100 100 mg/kg

Dibenzo(a,h)anthracene 0.33 0.33 0.33 mg/kg

Indeno(1,2,3-cd)pyrene 0.5 0.5 0.5 mg/kg

Pyrene 100 100 100 mg/kg

Biphenyl mg/kg

4-Chloroaniline mg/kg

2-Nitroaniline mg/kg



Dibenzofuran 14 59 7 mg/kg

2-Methylnaphthalene mg/kg

1,2,4,5-Tetrachlorobenzene mg/kg

Acetophenone mg/kg

2,4,6-Trichlorophenol mg/kg

p-Chloro-m-cresol mg/kg

2-Chlorophenol mg/kg

2,4-Dichlorophenol mg/kg

2,4-Dimethylphenol mg/kg

2-Nitrophenol mg/kg

4-Nitrophenol mg/kg

2,4-Dinitrophenol mg/kg

4,6-Dinitro-o-cresol mg/kg

Pentachlorophenol 2.4 6.7 0.8 mg/kg

Phenol 100 100 0.33 mg/kg

2-Methylphenol 100 100 0.33 mg/kg

3-Methylphenol/4-Methylphenol 34 100 0.33 mg/kg


Benzoic Acid mg/kg

Benzyl Alcohol mg/kg

Carbazole mg/kg

1,4-Dioxane 9.8 13 0.1 mg/kg







0.097 J 0.13 J 0.15 U 0.094 J 0.23 J 0.11 J

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.14 U 0.61 U 0.11 U 0.2 U 0.44 U 0.1 U

0.22 U 0.91 U 0.17 U 0.3 U 0.66 U 0.16 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.77 3.2 0.37 6.6 8.2 2

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.29 U 1.2 U 0.22 U 0.4 U 0.88 U 0.21 U

0.26 U 1.1 U 0.2 U 0.36 U 0.8 U 0.19 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.68 U 2.9 U 0.53 U 0.96 U 2.1 U 0.5 U

0.19 U 0.81 U 0.15 U 0.27 U 0.59 U 0.14 U

0.22 U 0.91 U 0.17 U 0.3 U 0.66 U 0.16 U

0.21 J 1 U 0.19 U 0.12 J 0.33 J 0.17 U

0.22 U 0.91 U 0.17 U 0.3 U 0.66 U 0.16 U

0.19 U 0.81 U 0.15 U 0.27 U 0.59 U 0.14 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.12 J 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.4 1.6 0.18 4 4.4 0.95

0.34 1.1 0.19 3.2 4.2 0.93

0.43 1.5 0.24 4.2 5.3 1.2

0.16 0.6 J 0.1 J 1.6 2.1 0.51

0.35 1.4 0.18 3.3 4.2 0.92

0.081 J 0.28 J 0.15 U 0.083 J 0.16 J 0.068 J

0.18 0.64 0.056 J 1 1.7 0.27

0.24 0.69 J 0.12 J 1.9 2.3 0.52

0.1 J 0.24 J 0.19 U 0.12 J 0.29 J 0.094 J

0.7 2.5 0.21 2.7 4.6 1.1

0.065 J 0.17 J 0.023 J 0.48 0.56 0.12

0.26 0.78 J 0.11 J 2.1 2.4 0.55

0.7 2.3 0.31 5.7 6.8 1.7

0.54 U 2.3 U 0.43 U 0.77 U 1.7 U 0.39 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.05 J 0.11 J 0.19 U 0.07 J 0.2 J 0.038 J

0.12 J 1.2 U 0.22 U 0.041 J 0.095 J 0.21 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.059 J 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.14 U 0.61 U 0.11 U 0.2 U 0.44 U 0.1 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.22 U 0.91 U 0.17 U 0.3 U 0.66 U 0.16 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.52 U 2.2 U 0.4 U 0.73 U 1.6 U 0.37 U

0.33 U 1.4 U 0.26 U 0.47 U 1 U 0.24 U

1.1 U 4.8 U 0.9 U 1.6 U 3.5 U 0.83 U

0.62 U 2.6 U 0.49 U 0.88 U 1.9 U 0.45 U

0.19 U 0.81 U 0.15 U 0.27 U 0.59 U 0.14 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.053 J 1.4 U 0.27 U 0.49 U 1.1 U 0.25 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.77 U 3.3 U 0.6 U 1.1 U 2.4 U 0.56 U

0.24 U 1 U 0.19 U 0.34 U 0.74 U 0.17 U

0.079 J 0.47 J 0.02 J 0.11 J 0.23 J 0.11 J

0.036 U 0.15 U 0.028 U 0.051 U 0.11 U 0.026 U


L1939567-08 L1939733-01 L1939733-02 L1939733-03 L1939733-04L1939567-07

8/30/2019 8/30/2019 8/30/2019 8/30/20198/29/2019 8/29/2019


Table 4






SAMPLE TYPE

Units





















Isophorone mg/kg


Nitrobenzene mg/kg

NDPA/DPA mg/kg





















Biphenyl mg/kg








Acetophenone mg/kg






2-Nitrophenol mg/kg

4-Nitrophenol mg/kg








Benzoic Acid mg/kg


Carbazole mg/kg

1,4-Dioxane 9.8 13 0.1 mg/kg






SESI-SB-14 (4-5)


0.15 U 0.45 U 0.27 J 0.026 J 0.03 J 0.029 J

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.12 U 0.34 U 0.25 U 0.11 U 0.12 U 0.1 U

0.17 U 0.51 U 0.37 U 0.16 U 0.18 U 0.16 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.12 U 0.34 U 5.2 1.1 0.69 0.74

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.23 U 0.68 U 0.5 U 0.21 U 0.24 U 0.21 U

0.21 U 0.61 U 0.45 U 0.19 U 0.22 U 0.19 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.55 U 1.6 U 1.2 U 0.51 U 0.58 U 0.5 U

0.15 U 0.45 U 0.33 U 0.14 U 0.16 U 0.14 U

0.17 U 0.51 U 0.37 U 0.16 U 0.18 U 0.16 U

0.19 U 0.57 U 0.2 J 0.18 U 0.2 U 0.17 U

0.17 U 0.51 U 0.37 U 0.16 U 0.18 U 0.16 U

0.15 U 0.45 U 0.33 U 0.14 U 0.16 U 0.14 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.12 U 0.34 U 2.6 0.39 0.34 0.32

0.15 U 0.45 U 2.5 0.36 0.34 0.34

0.12 U 0.34 U 3.2 0.5 0.44 0.43

0.12 U 0.34 U 1.3 0.2 0.17 0.23

0.12 U 0.34 U 2.5 0.36 0.34 0.34

0.15 U 0.45 U 0.55 0.058 J 0.16 U 0.14 U

0.12 U 0.34 U 0.91 0.13 0.084 J 0.087 J

0.15 U 0.45 U 1.5 0.21 0.2 0.24

0.19 U 0.57 U 0.27 J 0.042 J 0.04 J 0.022 J

0.12 U 0.34 U 3.1 0.55 0.33 0.35

0.12 U 0.34 U 0.34 0.046 J 0.048 J 0.052 J

0.15 U 0.45 U 1.6 0.21 0.18 0.24

0.12 U 0.34 U 4.4 0.89 0.57 0.6

0.44 U 1.3 U 0.94 U 0.41 U 0.46 U 0.4 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.16 J 0.18 U 0.2 U 0.17 U

0.23 U 0.68 U 0.066 J 0.21 U 0.24 U 0.21 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.12 U 0.34 U 0.25 U 0.11 U 0.12 U 0.1 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.17 U 0.51 U 0.37 U 0.16 U 0.18 U 0.16 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.42 U 1.2 U 0.89 U 0.38 U 0.44 U 0.38 U

0.27 U 0.8 U 0.58 U 0.25 U 0.28 U 0.24 U

0.93 U 2.7 U 2 U 0.86 U 0.97 U 0.84 U

0.5 U 1.5 U 1.1 U 0.46 U 0.52 U 0.45 U

0.15 U 0.45 U 0.33 U 0.14 U 0.16 U 0.14 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.28 U 0.82 U 0.6 U 0.26 U 0.29 U 0.25 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.63 U 1.8 U 1.3 U 0.58 U 0.65 U 0.56 U

0.19 U 0.57 U 0.41 U 0.18 U 0.2 U 0.17 U

0.19 U 0.57 U 0.38 J 0.085 J 0.036 J 0.04 J

0.029 U 0.085 U 0.062 U 0.027 U 0.03 U 0.026 U


L1939733-05 R1 L1939733-06 L1939733-07 L1939733-08 L1939733-09L1939733-05

8/30/2019 8/30/2019 8/30/2019 8/30/20198/30/2019 8/30/2019

SESI-SB-13 (3-4) SESI-SB-13 (3-4) SESI-SB-15 (2-3) SESI-SB-16 (1-2) SESI-SB-17 (2-3)

Table 4






SAMPLE TYPE

Units





















Isophorone mg/kg


Nitrobenzene mg/kg

NDPA/DPA mg/kg





















Biphenyl mg/kg








Acetophenone mg/kg






2-Nitrophenol mg/kg

4-Nitrophenol mg/kg








Benzoic Acid mg/kg


Carbazole mg/kg

1,4-Dioxane 9.8 13 0.1 mg/kg






SESI-SB-16 (14-15) SESI-SB-20 (14-15)

Results Qual Results Qual Results Qual Results Qual Results Qual

0.071 J 0.15 U 0.14 U 0.16 U 0.13 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.12 U 0.12 U 0.1 U 0.12 U 0.1 U

0.17 U 0.17 U 0.16 U 0.18 U 0.15 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

1.6 0.12 U 0.1 U 0.18 0.1 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.23 U 0.23 U 0.21 U 0.24 U 0.2 U

0.21 U 0.21 U 0.19 U 0.21 U 0.18 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.55 U 0.55 U 0.49 U 0.56 U 0.48 U

0.15 U 0.15 U 0.14 U 0.16 U 0.13 U

0.17 U 0.17 U 0.16 U 0.18 U 0.15 U

0.072 J 0.19 U 0.17 U 0.071 J 0.17 U

0.17 U 0.17 U 0.16 U 0.18 U 0.15 U

0.15 U 0.15 U 0.14 U 0.16 U 0.13 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.89 0.12 U 0.1 U 0.091 J 0.1 U

0.91 0.15 U 0.14 U 0.11 J 0.13 U

1.2 0.12 U 0.1 U 0.15 0.1 U

0.4 0.12 U 0.1 U 0.062 J 0.1 U

0.92 0.12 U 0.1 U 0.1 J 0.1 U

0.13 J 0.15 U 0.14 U 0.16 U 0.13 U

0.21 0.12 U 0.1 U 0.12 U 0.1 U

0.5 0.15 U 0.14 U 0.08 J 0.13 U

0.054 J 0.19 U 0.17 U 0.2 U 0.17 U

0.89 0.12 U 0.1 U 0.068 J 0.1 U

0.12 0.12 U 0.1 U 0.12 U 0.1 U

0.53 0.15 U 0.14 U 0.092 J 0.13 U

1.5 0.12 U 0.1 U 0.16 0.1 U

0.44 U 0.44 U 0.39 U 0.45 U 0.38 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.03 J 0.19 U 0.17 U 0.2 U 0.17 U

0.032 J 0.23 U 0.21 U 0.24 U 0.2 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.12 U 0.12 U 0.1 U 0.12 U 0.1 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.17 U 0.17 U 0.16 U 0.18 U 0.15 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.42 U 0.41 U 0.37 U 0.42 U 0.36 U

0.27 U 0.27 U 0.24 U 0.27 U 0.24 U

0.93 U 0.92 U 0.83 U 0.94 U 0.81 U

0.5 U 0.5 U 0.45 U 0.51 U 0.44 U

0.15 U 0.15 U 0.14 U 0.16 U 0.13 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.28 U 0.28 U 0.25 U 0.28 U 0.24 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.63 U 0.62 U 0.56 U 0.64 U 0.54 U

0.19 U 0.19 U 0.17 U 0.2 U 0.17 U

0.09 J 0.19 U 0.17 U 0.2 U 0.17 U

0.029 U 0.029 U 0.026 U 0.029 U 0.025 U

SOIL SOIL SOIL SOIL SOIL

L1939733-11 L1939733-12 L1940104-01 L1940104-02L1939733-10

8/30/2019 9/3/2019 9/3/20198/30/2019 8/30/2019

SESI-SB-19 (4-5) SESI-SB-20 (2-3)SESI-SB-18 (2-3)

Table 5

Dissolved and Total Metals in Groundwater


LOCATION

SAMPLING DATE

LAB SAMPLE ID

SAMPLE TYPE

SAMPLE DEPTH (ft.)

CasNum NY-AWQS Units Results Qual Results Qual Results Qual Results Qual

Total Metals

Aluminum, Total 7429-90-5 ug/l 61500 78900 57000 60500

Antimony, Total 7440-36-0 3 ug/l 0.56 J 0.43 J 4 U 4 U

Arsenic, Total 7440-38-2 25 ug/l 12.94 16.68 11.44 11.19

Barium, Total 7440-39-3 1000 ug/l 902.1 1627 932.2 1152

Beryllium, Total 7440-41-7 3 ug/l 3.41 4.33 3.23 3.08

Cadmium, Total 7440-43-9 5 ug/l 1.2 1.88 1.3 1.2

Calcium, Total 7440-70-2 ug/l 54600 213000 66800 76000

Chromium, Total 7440-47-3 50 ug/l 642.6 847.3 360.3 471.9

Cobalt, Total 7440-48-4 ug/l 202.9 272.8 218 213.5

Copper, Total 7440-50-8 200 ug/l 276.4 354 204.6 257.5

Iron, Total 7439-89-6 300 ug/l 216000 269000 183000 194000

Lead, Total 7439-92-1 25 ug/l 90.66 385.1 118.5 98.4

Magnesium, Total 7439-95-4 35000 ug/l 30300 54200 34400 34700

Manganese, Total 7439-96-5 300 ug/l 13570 20250 15940 19000

Mercury, Total 7439-97-6 0.7 ug/l 0.2 U 0.2 U 0.2 U 0.2 U

Nickel, Total 7440-02-0 100 ug/l 550.4 777.7 560.9 907.8

Potassium, Total 7440-09-7 ug/l 26200 24800 23900 21800

Selenium, Total 7782-49-2 10 ug/l 21 28.4 21.5 19

Silver, Total 7440-22-4 50 ug/l 0.21 J 0.36 J 0.19 J 0.18 J

Sodium, Total 7440-23-5 20000 ug/l 201000 420000 214000 193000

Thallium, Total 7440-28-0 0.5 ug/l 1.35 2.12 1.52 2.11

Vanadium, Total 7440-62-2 ug/l 128.1 114.9 108 114.4

Zinc, Total 7440-66-6 2000 ug/l 267.2 367.8 273.2 258.7

Dissolved Metals

Aluminum, Dissolved 7429-90-5 ug/l 10 U 4.9 J 6.98 J 3.88 J

Antimony, Dissolved 7440-36-0 3 ug/l 4 U 4 U 4 U 4 U

Arsenic, Dissolved 7440-38-2 25 ug/l 0.22 J 0.25 J 0.3 J 0.22 J

Barium, Dissolved 7440-39-3 1000 ug/l 62.07 232.3 90.91 87.94

Beryllium, Dissolved 7440-41-7 3 ug/l 0.5 U 0.5 U 0.5 U 0.5 U

Cadmium, Dissolved 7440-43-9 5 ug/l 0.15 J 0.19 J 0.16 J 0.14 J

Calcium, Dissolved 7440-70-2 ug/l 46200 173000 61400 67200

Chromium, Dissolved 7440-47-3 50 ug/l 1 U 1 U 1 U 1 U

Cobalt, Dissolved 7440-48-4 ug/l 24.47 28.93 22.65 17.95

Copper, Dissolved 7440-50-8 200 ug/l 0.8 J 1.3 0.58 J 2.77

Iron, Dissolved 7439-89-6 300 ug/l 50 U 29 J 28.2 J 50 U

Lead, Dissolved 7439-92-1 25 ug/l 1 U 1 U 1 U 1 U

Magnesium, Dissolved 7439-95-4 35000 ug/l 9070 23800 11200 12900

Manganese, Dissolved 7439-96-5 300 ug/l 5307 7655 5950 5856

Mercury, Dissolved 7439-97-6 0.7 ug/l 0.2 U 0.2 U 0.2 U 0.2 U

Nickel, Dissolved 7440-02-0 100 ug/l 48.67 67.38 54.22 58.48

Potassium, Dissolved 7440-09-7 ug/l 12000 8630 6450 6710

Selenium, Dissolved 7782-49-2 10 ug/l 2.37 J 5 U 2.09 J 3.24 J

Silver, Dissolved 7440-22-4 50 ug/l 0.4 U 0.4 U 0.4 U 0.4 U

Sodium, Dissolved 7440-23-5 20000 ug/l 217000 424000 210000 202000

Thallium, Dissolved 7440-28-0 0.5 ug/l 0.16 J 0.27 J 0.25 J 0.16 J

Vanadium, Dissolved 7440-62-2 ug/l 5 U 5 U 5 U 5 U

Zinc, Dissolved 7440-66-6 2000 ug/l 10 U 10 U 10 U 10 U

NY-AWQS: New York TOGS 111 Ambient Water Quality Standards criteria reflects all addendum to criteria through June

Exceeds NY-AWQS

L1940104-03 L1940104-04 L1940104-05 L1940104-06

WATER WATER WATER WATER

TW-1 TW-2 TW-3 TW-4

9/3/2019 9/3/2019 9/3/2019 9/3/2019

Table 6

Volatile Organic Compounds in Groundwater


LOCATION

SAMPLING DATE

LAB SAMPLE ID

SAMPLE TYPE

SAMPLE DEPTH (ft.)

CasNum NY-AWQS Units Results Qual Results Qual Results Qual Results Qual Results Qual

Volatile Organics by GC/MS

Methylene chloride 75-09-2 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

1,1-Dichloroethane 75-34-3 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Chloroform 67-66-3 7 ug/l 4.2 3.9 5.9 1.4 J 2.5 U

Carbon tetrachloride 56-23-5 5 ug/l 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U

1,2-Dichloropropane 78-87-5 1 ug/l 1 U 1 U 1 U 1 U 1 U

Dibromochloromethane 124-48-1 50 ug/l 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U

1,1,2-Trichloroethane 79-00-5 1 ug/l 1.5 U 1.5 U 1.5 U 1.5 U 1.5 U

Tetrachloroethene 127-18-4 5 ug/l 0.41 J 0.85 0.25 J 0.68 0.5 U

Chlorobenzene 108-90-7 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Trichlorofluoromethane 75-69-4 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

1,2-Dichloroethane 107-06-2 0.6 ug/l 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U

1,1,1-Trichloroethane 71-55-6 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Bromodichloromethane 75-27-4 50 ug/l 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U

trans-1,3-Dichloropropene 10061-02-6 0.4 ug/l 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U

cis-1,3-Dichloropropene 10061-01-5 0.4 ug/l 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U

1,3-Dichloropropene, Total 542-75-6 ug/l 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U

1,1-Dichloropropene 563-58-6 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Bromoform 75-25-2 50 ug/l 2 U 2 U 2 U 2 U 2 U

1,1,2,2-Tetrachloroethane 79-34-5 5 ug/l 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U

Benzene 71-43-2 1 ug/l 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U

Toluene 108-88-3 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Ethylbenzene 100-41-4 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Chloromethane 74-87-3 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Bromomethane 74-83-9 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Vinyl chloride 75-01-4 2 ug/l 1 U 1 U 1 U 1 U 1 U

Chloroethane 75-00-3 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

1,1-Dichloroethene 75-35-4 5 ug/l 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U

trans-1,2-Dichloroethene 156-60-5 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Trichloroethene 79-01-6 5 ug/l 0.44 J 0.5 U 0.49 J 0.5 U 0.5 U

1,2-Dichlorobenzene 95-50-1 3 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U



Methyl tert butyl ether 1634-04-4 10 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

p/m-Xylene 179601-23-1 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

o-Xylene 95-47-6 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Xylenes, Total 1330-20-7 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

cis-1,2-Dichloroethene 156-59-2 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

1,2-Dichloroethene, Total 540-59-0 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Dibromomethane 74-95-3 5 ug/l 5 U 5 U 5 U 5 U 5 U

1,2,3-Trichloropropane 96-18-4 0.04 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Acrylonitrile 107-13-1 5 ug/l 5 U 5 U 5 U 5 U 5 U

Styrene 100-42-5 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Dichlorodifluoromethane 75-71-8 5 ug/l 5 U 5 U 5 U 5 U 5 U

Acetone 67-64-1 50 ug/l 4.5 J 4.1 J 3.7 J 4.9 J 2.3 J

Carbon disulfide 75-15-0 60 ug/l 5 U 5 U 5 U 5 U 5 U

2-Butanone 78-93-3 50 ug/l 5 U 5 U 5 U 5 U 5 U

Vinyl acetate 108-05-4 ug/l 5 U 5 U 5 U 5 U 5 U

4-Methyl-2-pentanone 108-10-1 ug/l 5 U 5 U 5 U 5 U 5 U

2-Hexanone 591-78-6 50 ug/l 5 U 5 U 5 U 5 U 5 U

Bromochloromethane 74-97-5 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

2,2-Dichloropropane 594-20-7 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

1,2-Dibromoethane 106-93-4 0.0006 ug/l 2 U 2 U 2 U 2 U 2 U

1,3-Dichloropropane 142-28-9 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

1,1,1,2-Tetrachloroethane 630-20-6 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Bromobenzene 108-86-1 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

n-Butylbenzene 104-51-8 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

sec-Butylbenzene 135-98-8 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

tert-Butylbenzene 98-06-6 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

o-Chlorotoluene 95-49-8 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

p-Chlorotoluene 106-43-4 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

1,2-Dibromo-3-chloropropane 96-12-8 0.04 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Hexachlorobutadiene 87-68-3 0.5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Isopropylbenzene 98-82-8 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

p-Isopropyltoluene 99-87-6 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

Naphthalene 91-20-3 10 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

n-Propylbenzene 103-65-1 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

1,2,3-Trichlorobenzene 87-61-6 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

1,2,4-Trichlorobenzene 120-82-1 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

1,3,5-Trimethylbenzene 108-67-8 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

1,2,4-Trimethylbenzene 95-63-6 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

1,4-Dioxane 123-91-1 ug/l 250 U 250 U 250 U 250 U 250 U

p-Diethylbenzene 105-05-5 ug/l 2 U 2 U 2 U 2 U 2 U

p-Ethyltoluene 622-96-8 ug/l 2 U 2 U 2 U 2 U 2 U

1,2,4,5-Tetramethylbenzene 95-93-2 5 ug/l 2 U 2 U 2 U 2 U 2 U

Ethyl ether 60-29-7 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

trans-1,4-Dichloro-2-butene 110-57-6 5 ug/l 2.5 U 2.5 U 2.5 U 2.5 U 2.5 U

NY-AWQS: New York TOGS 111 Ambient Water Quality Standards criteria reflects all addendum to criteria

Exceeds NY-AWQS

TW-4

9/3/2019

L1940104-06

WATER

TW-1 TW-2 TW-3

9/3/2019

L1940104-03 L1940104-04 L1940104-05

WATER WATER WATER

9/3/2019 9/3/2019

TB

8/28/2019

L1940104-07

WATER

Table 7

Pesticides and PCB's in Groundwater


LOCATION

SAMPLING DATE

LAB SAMPLE ID

SAMPLE TYPE

SAMPLE DEPTH (ft.)


General Chemistry

Cyanide, Total 57-12-5 200 ug/l 5 U 2 J 1 J 1 J


Delta-BHC 319-86-8 0.04 ug/l 0.014 U 0.014 U 0.014 U 0.014 U

Lindane 58-89-9 0.05 ug/l 0.014 U 0.014 U 0.014 U 0.014 U

Alpha-BHC 319-84-6 0.01 ug/l 0.014 U 0.014 U 0.014 U 0.014 U

Beta-BHC 319-85-7 0.04 ug/l 0.014 U 0.014 U 0.014 U 0.014 U

Heptachlor 76-44-8 0.04 ug/l 0.014 U 0.014 U 0.014 U 0.014 U

Aldrin 309-00-2 0 ug/l 0.014 U 0.014 U 0.014 U 0.014 U

Heptachlor epoxide 1024-57-3 0.03 ug/l 0.014 U 0.014 U 0.014 U 0.014 U

Endrin 72-20-8 0 ug/l 0.029 U 0.029 U 0.029 U 0.029 U

Endrin aldehyde 7421-93-4 5 ug/l 0.029 U 0.029 U 0.029 U 0.029 U

Endrin ketone 53494-70-5 5 ug/l 0.029 U 0.029 U 0.029 U 0.029 U

Dieldrin 60-57-1 0.004 ug/l 0.029 U 0.029 U 0.029 U 0.029 U

4,4'-DDE 72-55-9 0.2 ug/l 0.029 U 0.029 U 0.029 U 0.029 U

4,4'-DDD 72-54-8 0.3 ug/l 0.029 U 0.029 U 0.029 U 0.029 U

4,4'-DDT 50-29-3 0.2 ug/l 0.029 U 0.029 U 0.029 U 0.029 U

Endosulfan I 959-98-8 ug/l 0.014 U 0.014 U 0.014 U 0.014 U

Endosulfan II 33213-65-9 ug/l 0.029 U 0.029 U 0.029 U 0.029 U

Endosulfan sulfate 1031-07-8 ug/l 0.029 U 0.029 U 0.029 U 0.029 U

Methoxychlor 72-43-5 35 ug/l 0.143 U 0.143 U 0.143 U 0.143 U

Toxaphene 8001-35-2 0.06 ug/l 0.143 U 0.143 U 0.143 U 0.143 U

cis-Chlordane 5103-71-9 ug/l 0.014 U 0.014 U 0.014 U 0.014 U

trans-Chlordane 5103-74-2 ug/l 0.014 U 0.014 U 0.014 U 0.014 U

Chlordane 57-74-9 0.05 ug/l 0.143 U 0.143 U 0.143 U 0.143 U


Aroclor 1016 12674-11-2 0.09 ug/l 0.083 U 0.083 U 0.083 U 0.083 U

Aroclor 1221 11104-28-2 0.09 ug/l 0.083 U 0.083 U 0.083 U 0.083 U

Aroclor 1232 11141-16-5 0.09 ug/l 0.083 U 0.083 U 0.083 U 0.083 U

Aroclor 1242 53469-21-9 0.09 ug/l 0.083 U 0.083 U 0.083 U 0.083 U

Aroclor 1248 12672-29-6 0.09 ug/l 0.083 U 0.083 U 0.083 U 0.083 U

Aroclor 1254 11097-69-1 0.09 ug/l 0.083 U 0.083 U 0.083 U 0.083 U

Aroclor 1260 11096-82-5 0.09 ug/l 0.083 U 0.083 U 0.083 U 0.083 U

Aroclor 1262 37324-23-5 0.09 ug/l 0.083 U 0.083 U 0.083 U 0.083 U

Aroclor 1268 11100-14-4 0.09 ug/l 0.083 U 0.083 U 0.083 U 0.083 U

PCBs, Total 1336-36-3 ug/l 0.083 U 0.083 U 0.083 U 0.083 U

NY-AWQS: New York TOGS 111 Ambient Water Quality Standards criteria reflects all addendum to criteria through June 2004.

Exceeds NY-AWQS

L1940104-03 L1940104-04 L1940104-05 L1940104-06


TW-1 TW-2 TW-3 TW-4

9/3/2019 9/3/2019 9/3/2019 9/3/2019

Table 8

Semivolatile Organic Compounds in Groundwater


LOCATION

SAMPLING DATE

LAB SAMPLE ID

SAMPLE TYPE

SAMPLE DEPTH (ft.)



1,2,4-Trichlorobenzene 120-82-1 5 ug/l 5 U 5 U 5 U 5 U

Bis(2-chloroethyl)ether 111-44-4 1 ug/l 2 U 2 U 2 U 2 U

1,2-Dichlorobenzene 95-50-1 3 ug/l 2 U 2 U 2 U 2 U



3,3'-Dichlorobenzidine 91-94-1 5 ug/l 5 U 5 U 5 U 5 U

2,4-Dinitrotoluene 121-14-2 5 ug/l 5 U 5 U 5 U 5 U

2,6-Dinitrotoluene 606-20-2 5 ug/l 5 U 5 U 5 U 5 U

4-Chlorophenyl phenyl ether 7005-72-3 ug/l 2 U 2 U 2 U 2 U

4-Bromophenyl phenyl ether 101-55-3 ug/l 2 U 2 U 2 U 2 U

Bis(2-chloroisopropyl)ether 108-60-1 5 ug/l 2 U 2 U 2 U 2 U

Bis(2-chloroethoxy)methane 111-91-1 5 ug/l 5 U 5 U 5 U 5 U

Hexachlorocyclopentadiene 77-47-4 5 ug/l 20 U 20 U 20 U 20 U

Isophorone 78-59-1 50 ug/l 5 U 5 U 5 U 5 U

Nitrobenzene 98-95-3 0.4 ug/l 2 U 2 U 2 U 2 U

NDPA/DPA 86-30-6 50 ug/l 2 U 2 U 2 U 2 U

n-Nitrosodi-n-propylamine 621-64-7 ug/l 5 U 5 U 5 U 5 U

Bis(2-ethylhexyl)phthalate 117-81-7 5 ug/l 2.1 J 2.1 J 2.3 J 2.6 J

Butyl benzyl phthalate 85-68-7 50 ug/l 5 U 5 U 5 U 5 U

Di-n-butylphthalate 84-74-2 50 ug/l 5 U 5 U 5 U 5 U

Di-n-octylphthalate 117-84-0 50 ug/l 5 U 5 U 5 U 5 U

Diethyl phthalate 84-66-2 50 ug/l 5 U 5 U 5 U 5 U

Dimethyl phthalate 131-11-3 50 ug/l 5 U 5 U 5 U 5 U

Biphenyl 92-52-4 ug/l 2 U 2 U 2 U 2 U

4-Chloroaniline 106-47-8 5 ug/l 5 U 5 U 5 U 5 U

2-Nitroaniline 88-74-4 5 ug/l 5 U 5 U 5 U 5 U



Dibenzofuran 132-64-9 ug/l 2 U 2 U 2 U 2 U

1,2,4,5-Tetrachlorobenzene 95-94-3 5 ug/l 10 U 10 U 10 U 10 U

Acetophenone 98-86-2 ug/l 5 U 5 U 5 U 5 U

2,4,6-Trichlorophenol 88-06-2 ug/l 5 U 5 U 5 U 5 U

p-Chloro-m-cresol 59-50-7 ug/l 2 U 2 U 2 U 2 U

2-Chlorophenol 95-57-8 ug/l 2 U 2 U 2 U 2 U

2,4-Dichlorophenol 120-83-2 1 ug/l 5 U 5 U 5 U 5 U

2,4-Dimethylphenol 105-67-9 50 ug/l 5 U 5 U 5 U 5 U

2-Nitrophenol 88-75-5 ug/l 10 U 10 U 10 U 10 U

4-Nitrophenol 100-02-7 ug/l 10 U 10 U 10 U 10 U

2,4-Dinitrophenol 51-28-5 10 ug/l 20 U 20 U 20 U 20 U

4,6-Dinitro-o-cresol 534-52-1 ug/l 10 U 10 U 10 U 10 U

Phenol 108-95-2 1 ug/l 5 U 5 U 5 U 5 U

2-Methylphenol 95-48-7 ug/l 5 U 5 U 5 U 5 U

3-Methylphenol/4-Methylphenol 108-39-4/106-44-5 ug/l 5 U 5 U 5 U 5 U

2,4,5-Trichlorophenol 95-95-4 ug/l 5 U 5 U 5 U 5 U

Benzoic Acid 65-85-0 ug/l 50 U 50 U 50 U 50 U

Benzyl Alcohol 100-51-6 ug/l 2.9 2 U 2 U 2 U

Carbazole 86-74-8 ug/l 2 U 2 U 2 U 2 U

Semivolatile Organics by GC/MS-SIM

Acenaphthene 83-32-9 20 ug/l 0.04 J 0.02 J 0.1 U 0.1 U

2-Chloronaphthalene 91-58-7 10 ug/l 0.2 U 0.2 U 0.2 U 0.2 U

Fluoranthene 206-44-0 50 ug/l 0.04 J 0.1 U 0.04 J 0.1 U

Hexachlorobutadiene 87-68-3 0.5 ug/l 0.5 U 0.5 U 0.5 U 0.5 U

Naphthalene 91-20-3 10 ug/l 0.07 JB 0.06 JB 0.1 U 0.1 U

Benzo(a)anthracene 56-55-3 0.002 ug/l 0.04 J 0.1 U 0.1 U 0.1 U

Benzo(a)pyrene 50-32-8 0 ug/l 0.02 J 0.1 U 0.1 U 0.1 U

Benzo(b)fluoranthene 205-99-2 0.002 ug/l 0.02 J 0.1 U 0.1 U 0.1 U

Benzo(k)fluoranthene 207-08-9 0.002 ug/l 0.02 J 0.1 U 0.1 U 0.1 U

Chrysene 218-01-9 0.002 ug/l 0.01 J 0.1 U 0.1 U 0.1 U

Acenaphthylene 208-96-8 ug/l 0.03 J 0.1 U 0.1 U 0.1 U

Anthracene 120-12-7 50 ug/l 0.04 J 0.1 U 0.02 J 0.1 U

Benzo(ghi)perylene 191-24-2 ug/l 0.02 J 0.1 U 0.1 U 0.1 U

Fluorene 86-73-7 50 ug/l 0.05 J 0.02 J 0.03 J 0.1 U

Phenanthrene 85-01-8 50 ug/l 0.07 J 0.05 J 0.09 J 0.1 U

Dibenzo(a,h)anthracene 53-70-3 ug/l 0.02 J 0.1 U 0.1 U 0.1 U

Indeno(1,2,3-cd)pyrene 193-39-5 0.002 ug/l 0.1 0.1 U 0.1 U 0.1 U

Pyrene 129-00-0 50 ug/l 0.04 J 0.1 U 0.03 J 0.1 U

2-Methylnaphthalene 91-57-6 ug/l 0.08 J 0.1 U 0.1 U 0.1 U

Pentachlorophenol 87-86-5 1 ug/l 0.8 U 0.8 U 0.8 U 0.8 U

Hexachlorobenzene 118-74-1 0.04 ug/l 0.8 U 0.8 U 0.8 U 0.8 U

Hexachloroethane 67-72-1 5 ug/l 0.8 U 0.8 U 0.8 U 0.8 U

NY-AWQS: New York TOGS 111 Ambient Water Quality Standards criteria reflects all addendum to criteria through June 2004.

Exceeds NY-AWQS

L1940104-03 L1940104-04 L1940104-05 L1940104-06


TW-1 TW-2 TW-3 TW-4

9/3/2019 9/3/2019 9/3/2019 9/3/2019

FIGURES

SITE LOCATION MAP12A MAPLE AVE. PINE BROOK, N.J. 07058 PH: 973-808-9050

C O N S U L T I N G

SITE DESIGN

ENVIRONMENTAL

SOILS / FOUNDATIONS

JOB NO.:

DATE:

SCALE:

CHECKED BY:

DRAWN BY:

E N G I N E E R S D.P.C.

10831

yy

FL

N.T.S.

12/13/19

FIG-1

PROJECT

SITE

90-02 168TH STREET

QUEENS, NY

9

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6

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90

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68

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REFERENCE

1. IMAGE TAKEN FROM BING MAPS ON 9/10/19.

12

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AP

LE

A

VE

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© SESI CONSULTING ENGINEERS D.P.C. 2019

This drawing and all information contained here on is proprietary

information of SESI CONSULTING ENGINEERS D.P.C. and may not

be copied or reproduced, either in whole or in part, by any method,

without written permission of SESI CONSULTING ENGINEERS D.P.C.

NYS Education Law

Unauthorized alterations or additions to this plan are a violation of

section 7209 (2) of the New York State Education Law. Copies of this

map not having the seal of the engineer shall not be valid.

10831

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NYS Education Law




10831

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FIG 3

1 of 1

NOTE:

1. THIS PLAN IS FOR LOCATING BORINGS ONLY. OTHER SITE

WORK SHOWN HERE IS NOT INTENDED FOR CONSTRUCTION.

2. ALL CONCENTRATIONS ARE IN PARTS PER MILLION (PPM)

SESI-SB-10

- SOIL BORING NUMBER & APPROX. LOCATION

LEGEND:

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SCALE: 1"=60'

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SESI-SB-8

SESI-SB-9

SESI-SB-10

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NYS Education Law




10831

JL

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FIG 5

NOTE:

ALL CONCENTRATIONS ARE IN PARTS PER MILLION (PPM)

SESI-SB-10

TW-1

- SOIL BORING NUMBER & APPROX. LOCATION

LEGEND:

60 120

SCALE: 1"=60'

0

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- EXCEEDS NYSDEC AMBIENT GROUNDWATER QUALITY STANDARDS

- TEMPORARY MONITORING WELL NUMBER & APPROX. LOCATION

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NYS Education Law




10831

JL

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3/1

9

FIG 4

NOTE:

THIS PLAN IS FOR LOCATING SOIL VAPOR SAMPLES ONLY.

OTHER SITE WORK SHOWN HERE IS NOT INTENDED FOR CONSTRUCTION.

SV-1

- SOIL VAPOR SAMPLE NUMBER & APPROX. LOCATION

LEGEND:

0

Scale 1"=80'

80 160

MA

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- EXCEEDS RESTRICTED RESIDENTIAL ScO

APPENDIX A Ground Penetrating Radar Report

SESI CONSULTING ENGINEERSCustomer Phone Number (973) 600-7630

12A MAPLE AVE

Job Details

City

PINE BROOK

State

NJ

Zip

07058

City JamaicaState NY

Jobsite Location 90-02 168th street

146958

Job Num

PO Num

WA Number

Lead Technician BERTHOLD, DENNIS Phone 929-418-0069 Email [email protected]

Thank you for using Ground Penetrating Radar Systems on your project. We appreciate the opportunity to workwith you. If you have questions regarding the results of this scanning, please contact the lead GPRS technician on this project.

Billing Address

EQUIPMENT USED

The following equipment was used on this project:

400 MHz GPR antenna. Typically capable of detecting objects several feet deep. Maximum effective depth depends on site and soil conditions.

RD 7000/8000 Radio Frequency detector. Detects electromagnetic fields. Used to actively trace metallic pipes and tracer wires, or passively detect electric,communications and other lines.

Work Performed

Ground Penetrating Radar Systems performed the following work on this project:

Underground Utility

Scanning the specified area to locate underground utilities and other significant anomalies. A tracer signal was sent along any accessible metallic utility or tracer wire, and the area was scanned with GPR to locate any additional targets. The locations of any detected utilities and anomalies were marked directly at the site with paint, flags, stakes, or other appropriate means, and results were reviewed with onsite personnel.

The total area scanned was approximately 700 square feet.

Scanning the areas around proposed soil borings. Typically a 10' radius around each proposed soil boring will be scanned. A total of 25+ boring locations were scanned.

Clearing for 7 soil boring locations

The effective depth of GPR will vary throughout a site depending on surface and soil conditions. In this area, the maximum effective GPR depth was approximately 4 feet.

Page 1 of 2

Job Date : 8/29/2019

Job Summary

Actual scope of work 25 boring locations to be cleared. Informed client the scans would take significantly longer then one hour to complete. Locations marked by client with white spray paint and each location scanned 10‘ x 10‘ area bracketed out in pink paint. All detections marked on surface: Electric in red, storm in green, and any other unknown labeled as such. Max gpr depth approximately 4’ on asphalt lot. Attempted to trace storm drains visually and with gpr due to flooding and other site limitations (vehicles, etc.). Cannot work or mark surface within 2’ of any vehicle and cannot scan within 2’ of any other obstruction. Please avoid all marks by at least 2’.

Report rejected

Pictures

Utility Limitations

TERMS & CONDITIONS

http://www.gprsinc.com/termsandconditions.html

SIGNATURE

Contact NameJohn Stewart (973) 600-7630 [email protected]

Page 2 of 2

Job Date : 8/29/2019

Job Summary

http://m.gprsinc.com/terms-conditions

APPENDIX B Boring Logs

be35-0037-fb71-23d6

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

30 1 0

0

5 5 0

5 0

0

32 2 0

0

10 0

0

0

36 3 0

0

15 0

0

0

40 4 0

0

20 0

0

0

30 5 0

0

25 0

0

0

32 6 0

0

30 0

0

0

40 7 0

0

35 35 0

40

in.

1⅜ in

Soil descriptions represent a field identification after D. M. Burmister unless otherwise noted.

GEOPROBE BY: Allstar (Joe)

INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.

Approximate Change in Strata: ____________ Inferred Change in Strata: _ _ _ _ _ _ _ _ _ _ _ _ _

Pp: Pocket Penetrometer; DP: Direct Push

The subsurface information shown hereon was obtained for the design and estimating purposes for our client.

It is made available to authorized users only that they may have access to the same information available

to our client. It is presented in good faith, but it is not intended as a substitute for investigations, interpretations

or judgment of such authorized users. Information on the logs should not be relied upon without the geotechnical

engineers recommendations contained in the report from which these logs were extracted.

Nominal I.D. of Hole

Nominal I.D. of Barrel Sampler

FIGURE Page 1 of 1

(moist/wet)

Light brown coarse to fine SAND, some coarse to fine Gravel

Boring Complete at ±35' BGS

DEPTH

sesi-SB-1(2-3)

ENVIRONMENTAL

SOIL SAMPLE NAME

NA

8/29/19 GROUNDWATER TABLE DEPTH: NE

Dual Tube

DATE STARTED:

SOIL DESCRIPTION AND STRATIFICATION

DATE COMPLETED:

GEOPROBE NO. sesi-SB-1

JOB NO. 10831

PROJECT NAME: 90-02 168th Street

LOCATION:

METHOD:

Jamaica, Queens, NY

Date8/29/19

PID

(FILL) Dark brown coarse to fine SAND, little Silt, trace Clay

c3e8-3c73-d465-f943

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

28 1 0

0

5 5 0

5 0

0

36 2 0

0

10 0

0

0

30 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in



INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.










FIGURE Page 1 of 1


DEPTH

sesi-SB-2(3-4)

ENVIRONMENTAL

SOIL SAMPLE NAME

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

Date8/29/19

PID

(FILL) Dark brown coarse to fine SAND, little Silt, trace Clay.

fd11-eb10-f0bf-41bd

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

28 1 3 0

3 0

5 5 0

5 0

0

36 2 0

0

10 0

0

0

42 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in



INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.










FIGURE Page 1 of 1


Boring Complete at ±15 Feet BGS

(FILL) Gray brown coarse to fine SAND, some Silt, trace Clay

DEPTH

sesi-SB-3(2-3)

ENVIRONMENTAL

SOIL SAMPLE NAME

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

Date8/29/19

PID

(FILL) Brown coarse to fine SAND, some Silt, little Clay

f05f-5932-328b-3850

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

40 1 0

0

5 5 0

5 0

0

20 2 0

0

10 0

0

0

38 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in



INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.










FIGURE Page 1 of 1

Light brown coarse to fine SAND, little coarse to fine Gravel.


DEPTH

sesi-SB-4(2-3)

ENVIRONMENTAL

SOIL SAMPLE NAME

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

Date8/29/19

PID

(FILL) Brown coarse to fine SAND, some Silt, trace Clay

54b7-0936-4da7-8d25

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

38 1 0

0

5 5 0

5 0

0

32 2 0

0

10 0

0

0

42 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in



INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.










FIGURE Page 1 of 1

Light brown coarse to fine SAND, some coarse to fine Gravel.


DEPTH ENVIRONMENTAL

SOIL SAMPLE NAME

sesi-SB-5(4-5)

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

Date8/29/19

PID

(FILL) Brown coarse to fine SAND, some Silt, little Clay

3c56-612e-d28d-4448

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

36 1 0

0

5 5 0

5 0

0

40 2 0

0

10 0

0

0

42 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in



INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.










FIGURE Page 1 of 1

Light brown coarse to fine SAND, little coarse to fine Gravel.


DEPTH ENVIRONMENTAL

SOIL SAMPLE NAME

sesi-SB-6(1-2)

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

Date8/29/19

PID

(FILL) Brown coarse to fine SAND and Silt

94b1-3777-499c-7d1a

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

46 1 0

4 0

5 4 5 0

5 0

0

42 2 0

0

10 0

0

0

20 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in



INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.










FIGURE Page 1 of 1



(FILL) Brown-black coarse to fine SAND, little Silt, trace Clay

DEPTH

sesi-SB-7(3-4)

ENVIRONMENTAL

SOIL SAMPLE NAME

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:

GEOPROBE NO. sesi-SB-

JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

Date8/29/19

PID

(FILL) Brown coarse to fine SAND, little Silt, trace Clay

1179-affe-0f11-6e8c

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

32 1 3 0

3 0

5 5 0

5 0

0

36 2 0

0

10 0

0

0

44 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in



INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.










FIGURE Page 1 of 1

Light brown coarse to fine SAND, little coarse to fine Gravel


(FILL) Dark brown coarse to fine SAND, some Silt, trace Clay

DEPTH

sesi-SB-8(2-3)

ENVIRONMENTAL

SOIL SAMPLE NAME

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

Date8/29/19

PID

(FILL) brown coarse to fine SAND, some Silt, trace Clay

0b4c-db0c-f830-d62c

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

28 1 0

4 0

5 5 0

0

0

36 2 0

0

10 0

0

0

42 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in



INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.










FIGURE Page 1 of 1


Boring Complete at ±15 Fet BGS


DEPTH ENVIRONMENTAL

SOIL SAMPLE NAME

sesi-SB-9(1-2)

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

Date8/30/19

PID

3088-5dc6-40ce-8655

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

30 1 0.3

0

5 5 0

5 0

0

38 2 0

0

10 0

0

0

42 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in



INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.










FIGURE Page 1 of 1

Light brown coase to fine SAND, little coarse to fine Gravel


DEPTH

sesi-SB-10(2-3)

ENVIRONMENTAL

SOIL SAMPLE NAME

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

(FILL) Dark brown coarse to fine SAND, little coarse to fine Gravel

trace Silt with some brick

Date8/30/19

PID

48cd-11c5-ae29-f469

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

36 1 0

0

5 5 0

5 0

0

50 2 0

0

10 0

0

0

48 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in


Date8/30/19

PID


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:

DEPTH

sesi-SB-11(3-4)

ENVIRONMENTAL

SOIL SAMPLE NAME



FIGURE Page 1 of 1











INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.

(FILL) Dark brown coarse to fine SAND, little Silt, trace coarse to

fine Gravel, band of black soil at 3-4 - no odor

58d7-fef0-ba05-d126

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

28 1 0

0

5 0

0

0

32 2 8 0

8 0

10 0

0

0

55 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in


Date8/30/19

PID


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:

DEPTH ENVIRONMENTAL

SOIL SAMPLE NAME



FIGURE Page 1 of 1











INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.

sesi-SB-12(6-7) (FILL) Brown coarse to fine SAND, little Silt, trace Clay with Brick,

Concrete

ff0a-056a-0a9c-11ad

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

48 1 0

0

5 5 0

5 0

0

50 2 0

0

10 0

0

0

52 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in


Date8/30/19

PID


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:

DEPTH

sesi-SB-13(3-4)

ENVIRONMENTAL

SOIL SAMPLE NAME



FIGURE Page 1 of 1











INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.

(FILL) Black-brown coarse to fine SAND, little Silt, trace coarse to

fine Gravel with Brick

db99-f747-74fa-16a8

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

36 1 0

0

5 5 0

5 0

0

40 2 0

0

10 0

0

0

52 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in


Date8/30/19

PID


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:

DEPTH ENVIRONMENTAL

SOIL SAMPLE NAME

sesi-SB14(4-5)



FIGURE Page 1 of 1











INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.

(FILL) Dark brown coarse to fine SAND, little Silt, trace coarse to

fine Gravel with Brick

0b87-7157-0718-e0a8

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0

0

30 1 3 0

3 0

5 0

0

0

56 2 0

0

10 0

0

0

48 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in


Date8/30/19

PID


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:

DEPTH

sesi-SB-15(2-3)

ENVIRONMENTAL

SOIL SAMPLE NAME



FIGURE Page 1 of 1











INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.

(FILL) Dark brown coarse to fine SAND, little coarse to fine Gravel,

trace Silt, with Brick

10d3-bbae-d2ec-1a35

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

34 1 0

0

5 5 0

5 0

0

50 2 0

0

10 0

0

0

54 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in


Date8/30/19

PID

Brown coarse to fine SAND, little coarse to fine Gravel, trace Clay


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:

DEPTH ENVIRONMENTAL

SOIL SAMPLE NAME

sesi-SB-16(1-2)



FIGURE Page 1 of 1











INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.

sesi-SB-16(14-15)

2b05-47e4-23f8-3cf8

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

30 1 0

0

5 5 0

5 0

0

44 2 0

0

10 0

0

0

18 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in


Date8/30/19

PID



JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:

DEPTH

sesi-SB-17(2-3)

ENVIRONMENTAL

SOIL SAMPLE NAME



FIGURE Page 1 of 1











INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.

5190-4b46-42a7-b14f

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

36 1 0

0

5 5 0

5 0

0

40 2 0

0

10 0

0

0

46 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in


Date8/30/19

PID



JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:

DEPTH

sesi-SB-18(2-3)

ENVIRONMENTAL

SOIL SAMPLE NAME



FIGURE Page 1 of 1











INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.

d352-46cb-726d-a9b0

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 (ft) (ft)

0 0

0

48 1 0

0

5 5 0

5 0

0

50 2 0

0

10 0

0

0

50 3 0

0

15 15 0

20

25

30

35

40

in.

1⅜ in


Date8/30/19

PID

(FILL) Brown coarse to fine SAND and Silt.


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:

DEPTH ENVIRONMENTAL

SOIL SAMPLE NAME

sesi-SB-19(4-5)



FIGURE Page 1 of 1











INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.

4fde-79e9-dc15-bd76

GROUND ELEVATION:

0 Hr. 24 Hr.

DEPTH

(ft) FROM TO

0 0 (ft)

0 0

0

38 1 0

4 0

5 4 0

0

0

44 2 0

0

10 0

0

0

42 3 0

15 0

15

20

25

30

35

40

in.

1⅜ in


Date9/3/19

PID


JOB NO. 10831


LOCATION:

METHOD:

Jamaica, Queens, NY

NA


Dual Tube

DATE STARTED:


DATE COMPLETED:


DEPTH

sesi-SB-20(2-3)

ENVIRONMENTAL

SOIL SAMPLE NAME


Light brown coarse to fine SAND, come coarse to fine Gravel

FIGURE Page 1 of 1











INSPECTOR: JCS

RECOVERY

(in)

SAMPLE

TUBE

No.

sesi-SB-20(14-15)

APPENDIX C Laboratory Results

(Electronic)

L1939733

Soils Engineering Services, Inc.

10831

90-02 168TH ST., JAMAICA, NY

Client:

Project Name:

Project Number:

09/09/19

Eight Walkup Drive, Westborough, MA 01581-1019

Lab Number:

Report Date:

508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com

12A Maple Avenue


Jesse MausnerATTN:

ANALYTICAL REPORT

Certifications & Approvals: MA (M-MA086), NH NELAP (2064), CT (PH-0574), IL (200077), ME (MA00086), MD (348), NJ (MA935), NY (11148), NC (25700/666), PA (68-03671), RI (LAO00065), TX (T104704476), VT (VT-0935), VA (460195), USDA (Permit #P330-17-00196).

(973) 808-9050Phone:

The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in itsentirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.

Serial_No:09091918:03

Page 1 of 222

L1939733-01

L1939733-02

L1939733-03

L1939733-04

L1939733-05

L1939733-06

L1939733-07

L1939733-08

L1939733-09

L1939733-10

L1939733-11

L1939733-12

Alpha Sample ID

SESI-SB-9 (1-2)

SESI-SB-10 (2-3)

SESI-SB-11 (3-4)

SESI-SB-12 (6-7)

SESI-SB-13 (3-4)

SESI-SB-14 (4-5)

SESI-SB-15 (2-3)

SESI-SB-16 (1-2)

SESI-SB-17 (2-3)

SESI-SB-18 (2-3)

SESI-SB-19 (4-5)

SESI-SB-16 (14-15)

Client ID

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

Sample Location


10831

Project Name:Project Number:

Lab Number: Report Date:

L193973309/09/19

08/30/19 07:50

08/30/19 08:25

08/30/19 08:55

08/30/19 09:25

08/30/19 10:00

08/30/19 10:35

08/30/19 11:05

08/30/19 11:30

08/30/19 12:10

08/30/19 13:35

08/30/19 14:00

08/30/19 11:35

Collection Date/TimeMatrix Receive Date

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

08/30/19

08/30/19

08/30/19

08/30/19

08/30/19

08/30/19

08/30/19

08/30/19

08/30/19

08/30/19

08/30/19

08/30/19

Serial_No:09091918:03

Page 2 of 222


10831

Project Name:

Project Number:

Lab Number:

Report Date:L1939733

09/09/19

Case Narrative

The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation

or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.

Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all

NELAP accredited parameters unless otherwise noted in the following narrative. The data presented in this report is organized by parameter

(i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list

for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. Tentatively Identified

Compounds (TICs), if requested, are reported for compounds identified to be present and are not part of the method/program Target

Compound List, even if only a subset of the TCL are being reported. If a sample was re-analyzed or re-extracted due to a required quality

control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R"

or "RE", respectively.

When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in

the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed

Acceptance Criteria is bolded in the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria

for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances, the

specific failure is not narrated but noted in the associated QC Outlier Summary Report, located directly after the Case Narrative. QC

information is also incorporated in the Data Usability Assessment table (Format 11) of our Data Merger tool, where it can be reviewed in

conjunction with the sample result, associated regulatory criteria and any associated data usability implications.

Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms

used in this report are provided in the Glossary located at the back of the report.

HOLD POLICY - For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21

calendar days from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put

on hold unless you have contacted your Alpha Project Manager and made arrangements for Alpha to continue to hold the samples. Air

canisters will be disposed after 3 business days from the date the project is completed.

Please contact Project Management at 800-624-9220 with any questions.

Serial_No:09091918:03

Page 3 of 222

Case Narrative (continued)


10831

Project Name:

Project Number:

Lab Number:


09/09/19

Report Submission

All non-detect (ND) or estimated concentrations (J-qualified) have been quantitated to the limit noted in the

MDL column.

Volatile Organics

L1939733-01, -03, -04, -06, and -12: The sample was analyzed as a High Level Methanol in order to

quantitate the sample within the calibration range. The result should be considered estimated, and is qualified

with an E flag, for any compound that exceeded the calibration on the initial Low Level analysis. The results of

both analyses are reported. Differences were noted between the results of the analyses which have been

attributed to vial discrepancies.

Semivolatile Organics

L1939733-02, -03, and -06: The sample has elevated detection limits due to the dilution required by the

sample matrix.

L1939733-05: The surrogate recoveries were outside the acceptance criteria for 2-fluorophenol (5%) and

2,4,6-tribromophenol (0%); however, re-extraction achieved similar results: 2-fluorophenol (11%) and 2,4,6-

tribromophenol (2%). The results of both extractions are reported.

Total Metals

L1939733-01 through -12: The sample has elevated detection limits for all elements, with the exception of

mercury, due to the dilution required by matrix interferences encountered during analysis.

The WG1280281-3 MS recoveries for aluminum (1620%), iron (3060%) and manganese (481%), performed on

L1939733-01, do not apply because the sample concentrations are greater than four times the spike amounts

added.

The WG1280281-3 MS recovery, performed on L1939733-01, is outside the acceptance criteria for copper

(4%). A post digestion spike was performed and was within acceptance criteria.

The WG1280504-3 MS recovery, performed on L1939733-01, is outside the acceptance criteria for mercury

Serial_No:09091918:03

Page 4 of 222



10831

Project Name:

Project Number:

Lab Number:


09/09/19

(127%). A post digestion spike was performed and was within acceptance criteria.

The WG1280281-4 Laboratory Duplicate RPDs for aluminum (23%), barium (26%), calcium (90%), copper

(47%), iron (24%), lead (27%), magnesium (22%), manganese (83%), and vanadium (21%), performed on

L1939733-01, are outside the acceptance criteria. The elevated RPDs have been attributed to the non-

homogeneous nature of the native sample.

Cyanide, Total

The WG1279408-2/-3 LCS/LCSD recoveries (64%/69%), associated with L1939733-01 through -05, are

outside our in-house acceptance criteria, but within the vendor-certified acceptance limits. The results of the

original analyses are reported.



original analyses are reported. In addition, the LCS/LCSD RPD (48%) is above the acceptance criteria.

Solids, Total

L1939733: A Laboratory Duplicate was prepared with the sample batch; however, analysis of the native sample

was cancelled; therefore, the QC result could not be reported.

I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report.

Authorized Signature:

Title: Technical Director/Representative Date: 09/09/19

Serial_No:09091918:03

Page 5 of 222

ORGANICS

Serial_No:09091918:03

Page 6 of 222

VOLATILES

Serial_No:09091918:03

Page 7 of 222

FF

Methylene chloride

1,1-Dichloroethane

Chloroform

Carbon tetrachloride

1,2-Dichloropropane

Dibromochloromethane

1,1,2-Trichloroethane

Tetrachloroethene

Chlorobenzene

Trichlorofluoromethane

1,2-Dichloroethane


Bromodichloromethane

trans-1,3-Dichloropropene

cis-1,3-Dichloropropene

1,3-Dichloropropene, Total

1,1-Dichloropropene

Bromoform

1,1,2,2-Tetrachloroethane

Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene

trans-1,2-Dichloroethene

Parameter Result Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Volatile Organics by EPA 5035 Low - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

4.5

0.89

1.3

0.89

0.89

0.89

0.89

0.45

0.45

3.6

0.89

0.45

0.45

0.89

0.45

0.45

0.45

3.6

0.45

0.45

0.89

0.89

3.6

1.8

0.89

1.8

0.89

1.3

09/09/19

SESI-SB-9 (1-2)Client ID:08/30/19 07:50Date Collected:08/30/19Date Received:

JAMAICA, QUEENS, NYSample Location:

L1939733-01Lab ID:

Field Prep: Not Specified

Matrix: SoilAnalytical Method:Analytical Date:Analyst:

1,8260C09/07/19 10:16AD 87%Percent Solids:

MDL

2.0

0.13

0.12

0.20

0.11

0.12

0.24

0.17

0.11

0.62

0.23

0.15

0.10

0.24

0.14

0.14

0.14

0.22

0.15

0.15

0.48

0.12

0.83

0.52

0.30

0.40

0.21

0.12

Sample Depth:

Serial_No:09091918:03

Page 8 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Methyl tert butyl ether

p/m-Xylene

o-Xylene

Xylenes, Total

cis-1,2-Dichloroethene

1,2-Dichloroethene, Total

Dibromomethane

Styrene

Dichlorodifluoromethane

Acetone

Carbon disulfide

2-Butanone

Vinyl acetate

4-Methyl-2-pentanone

1,2,3-Trichloropropane

2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene

1,2-Dibromo-3-chloropropane

Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

E

Dilution Factor

ND

ND

ND

ND

0.74

ND

ND

ND

ND

ND

ND

ND

ND

700

ND

15

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.45

1.8

1.8

1.8

1.8

1.8

0.89

0.89

0.89

0.89

1.8

0.89

8.9

8.9

8.9

8.9

8.9

8.9

1.8

8.9

1.8

1.8

0.89

1.8

0.45

1.8

0.89

0.89

1.8

1.8

1.8

2.7

3.6

0.89

0.89

3.6

3.6

09/09/19



L1939733-01Lab ID:


MDL

0.12

0.13

0.13

0.15

0.18

0.50

0.26

0.26

0.16

0.12

0.21

0.17

0.82

4.3

4.0

2.0

1.9

1.1

0.11

1.0

0.18

0.18

0.25

0.15

0.12

0.13

0.15

0.13

0.10

0.17

0.10

0.89

0.15

0.10

0.10

0.58

1.0

Sample Depth:

Serial_No:09091918:03

Page 9 of 222

n-Propylbenzene

1,2,3-Trichlorobenzene


1,3,5-Trimethylbenzene


1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene

1,2,4,5-Tetramethylbenzene

Ethyl ether

trans-1,4-Dichloro-2-butene


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.89

1.8

1.8

1.8

1.8

71

1.8

1.8

1.8

1.8

4.5

1,2-Dichloroethane-d4

Toluene-d8

4-Bromofluorobenzene

Dibromofluoromethane

107

98

106

102

70-130

70-130

70-130

70-130

Acceptance CriteriaSurrogate % Recovery Qualifier

09/09/19



L1939733-01Lab ID:


Total TIC Compounds

Unknown

Unknown

Ethyl Acetate

Unknown

J

J

J

NJ

J

283

21.4

27.6

227

6.96

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Tentatively Identified Compounds

MDL

0.15

0.29

0.24

0.17

0.30

31.

0.16

0.34

0.17

0.30

1.3

Sample Depth:

Serial_No:09091918:03

Page 10 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

60

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Volatile Organics by EPA 5035 High - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

260

52

78

52

52

52

52

26

26

210

52

26

26

52

26

26

26

210

26

26

52

52

210

100

52

100

52

78

09/09/19



L1939733-01Lab ID:



1,8260C09/08/19 10:21JC 87%Percent Solids:

MDL

120

7.5

7.3

12.

6.5

7.3

14.

10.

6.6

36.

13.

8.7

5.7

14.

8.2

8.2

8.2

13.

8.6

8.6

28.

7.3

48.

30.

17.

23.

12.

7.1

Sample Depth:

Serial_No:09091918:03

Page 11 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

26

100

100

100

100

100

52

52

52

52

100

52

520

520

520

520

520

520

100

520

100

100

52

100

26

100

52

52

100

100

100

160

210

52

52

210

210

09/09/19



L1939733-01Lab ID:


MDL

7.1

7.5

7.7

8.9

10.

29.

15.

15.

9.1

7.1

12.

10.

48.

250

240

120

110

66.

6.6

61.

11.

10.

14.

8.7

6.8

7.5

8.7

7.6

6.1

9.9

5.6

52.

8.8

5.7

5.7

34.

60.

Sample Depth:

Serial_No:09091918:03

Page 12 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

52

100

100

100

100

4200

100

100

100

100

260


Toluene-d8



108

95

95

98

70-130

70-130

70-130

70-130


09/09/19



L1939733-01Lab ID:


Total TIC Compounds

Cyclotrisiloxane, Hexamethyl-

J

NJ

129

129

ug/kg

ug/kg

1

1


MDL

8.9

17.

14.

10.

17.

1800

9.2

20.

9.9

18.

74.

Sample Depth:

Serial_No:09091918:03

Page 13 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

4.6

0.93

1.4

0.93

0.93

0.93

0.93

0.46

0.46

3.7

0.93

0.46

0.46

0.93

0.46

0.46

0.46

3.7

0.46

0.46

0.93

0.93

3.7

1.8

0.93

1.8

0.93

1.4

09/09/19



L1939733-02Lab ID:




MDL

2.1

0.13

0.13

0.21

0.12

0.13

0.25

0.18

0.12

0.64

0.24

0.15

0.10

0.25

0.15

0.15

0.15

0.23

0.15

0.15

0.50

0.13

0.86

0.54

0.31

0.42

0.22

0.13

Sample Depth:

Serial_No:09091918:03

Page 14 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

0.93

ND

ND

ND

ND

ND

ND

ND

ND

200

ND

5.0

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.46

1.8

1.8

1.8

1.8

1.8

0.93

0.93

0.93

0.93

1.8

0.93

9.3

9.3

9.3

9.3

9.3

9.3

1.8

9.3

1.8

1.8

0.93

1.8

0.46

1.8

0.93

0.93

1.8

1.8

1.8

2.8

3.7

0.93

0.93

3.7

3.7

09/09/19



L1939733-02Lab ID:


MDL

0.13

0.13

0.14

0.16

0.19

0.52

0.27

0.27

0.16

0.13

0.22

0.18

0.85

4.5

4.2

2.0

2.0

1.2

0.12

1.1

0.19

0.19

0.26

0.15

0.12

0.13

0.15

0.14

0.11

0.18

0.10

0.92

0.16

0.10

0.10

0.60

1.1

Sample Depth:

Serial_No:09091918:03

Page 15 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.93

1.8

1.8

1.8

1.8

74

1.8

1.8

1.8

1.8

4.6


Toluene-d8



109

99

111

104

70-130

70-130

70-130

70-130


09/09/19



L1939733-02Lab ID:


Total TIC Compounds

Acetic acid, methyl ester

Ethyl Acetate

J

NJ

NJ

117

9.08

108

ug/kg

ug/kg

ug/kg

1

1

1


MDL

0.16

0.30

0.25

0.18

0.31

32.

0.16

0.36

0.18

0.32

1.3

Sample Depth:

Serial_No:09091918:03

Page 16 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

4.7

0.93

1.4

0.93

0.93

0.93

0.93

0.47

0.47

3.7

0.93

0.47

0.47

0.93

0.47

0.47

0.47

3.7

0.47

0.47

0.93

0.93

3.7

1.9

0.93

1.9

0.93

1.4

09/09/19



L1939733-03Lab ID:




MDL

2.1

0.14

0.13

0.21

0.12

0.13

0.25

0.18

0.12

0.65

0.24

0.16

0.10

0.25

0.15

0.15

0.15

0.23

0.15

0.15

0.51

0.13

0.87

0.54

0.31

0.42

0.22

0.13

Sample Depth:

Serial_No:09091918:03

Page 17 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

E

Dilution Factor

ND

ND

ND

ND

0.91

ND

ND

ND

ND

ND

ND

ND

ND

480

ND

11

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.47

1.9

1.9

1.9

1.9

1.9

0.93

0.93

0.93

0.93

1.9

0.93

9.3

9.3

9.3

9.3

9.3

9.3

1.9

9.3

1.9

1.9

0.93

1.9

0.47

1.9

0.93

0.93

1.9

1.9

1.9

2.8

3.7

0.93

0.93

3.7

3.7

09/09/19



L1939733-03Lab ID:


MDL

0.13

0.13

0.14

0.16

0.19

0.52

0.27

0.27

0.16

0.13

0.22

0.18

0.85

4.5

4.2

2.1

2.0

1.2

0.12

1.1

0.19

0.19

0.26

0.16

0.12

0.14

0.16

0.14

0.11

0.18

0.10

0.93

0.16

0.10

0.10

0.60

1.1

Sample Depth:

Serial_No:09091918:03

Page 18 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.93

1.9

1.9

1.9

1.9

74

1.9

1.9

1.9

1.9

4.7


Toluene-d8



107

100

109

103

70-130

70-130

70-130

70-130


09/09/19



L1939733-03Lab ID:


Total TIC Compounds

Unknown

Ethyl Acetate

J

J

NJ

175

12.8

162

ug/kg

ug/kg

ug/kg

1

1

1


MDL

0.16

0.30

0.25

0.18

0.31

33.

0.16

0.36

0.18

0.32

1.3

Sample Depth:

Serial_No:09091918:03

Page 19 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

20

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

280

57

85

57

57

57

57

28

28

230

57

28

28

57

28

28

28

230

28

28

57

57

230

110

57

110

57

85

09/09/19



L1939733-03Lab ID:




MDL

130

8.2

8.0

13.

7.1

8.0

15.

11.

7.2

40.

15.

9.5

6.2

16.

9.0

9.0

9.0

14.

9.4

9.4

31.

8.0

53.

33.

19.

26.

14.

7.8

Sample Depth:

Serial_No:09091918:03

Page 20 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

Dilution Factor

43

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

270

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

360

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

28

110

110

110

110

110

57

57

57

57

110

57

570

570

570

570

570

570

110

570

110

110

57

110

28

110

57

57

110

110

110

170

230

57

57

230

230

09/09/19



L1939733-03Lab ID:


MDL

7.8

8.2

8.4

9.7

11.

32.

16.

16.

10.

7.8

14.

11.

52.

270

260

130

120

73.

7.2

67.

12.

12.

16.

9.5

7.5

8.2

9.5

8.3

6.7

11.

6.2

57.

9.6

6.2

6.2

37.

65.

Sample Depth:

Serial_No:09091918:03

Page 21 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

57

110

110

110

110

4600

110

110

110

110

280


Toluene-d8



107

96

94

98

70-130

70-130

70-130

70-130


09/09/19



L1939733-03Lab ID:


No Tentatively Identified Compounds ND ug/kg 1


MDL

9.7

18.

15.

11.

19.

2000

10.

22.

11.

19.

81.

Sample Depth:

Serial_No:09091918:03

Page 22 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

0.13

ND

ND

ND

ND

0.46

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

4.4

0.88

1.3

0.88

0.88

0.88

0.88

0.44

0.44

3.5

0.88

0.44

0.44

0.88

0.44

0.44

0.44

3.5

0.44

0.44

0.88

0.88

3.5

1.8

0.88

1.8

0.88

1.3

09/09/19



L1939733-04Lab ID:




MDL

2.0

0.13

0.12

0.20

0.11

0.12

0.23

0.17

0.11

0.61

0.23

0.15

0.10

0.24

0.14

0.14

0.14

0.22

0.15

0.15

0.48

0.12

0.82

0.51

0.29

0.40

0.21

0.12

Sample Depth:

Serial_No:09091918:03

Page 23 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

E

Dilution Factor

ND

ND

ND

ND

0.95

ND

ND

ND

ND

ND

ND

ND

ND

490

ND

12

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.44

1.8

1.8

1.8

1.8

1.8

0.88

0.88

0.88

0.88

1.8

0.88

8.8

8.8

8.8

8.8

8.8

8.8

1.8

8.8

1.8

1.8

0.88

1.8

0.44

1.8

0.88

0.88

1.8

1.8

1.8

2.6

3.5

0.88

0.88

3.5

3.5

09/09/19



L1939733-04Lab ID:


MDL

0.12

0.13

0.13

0.15

0.18

0.49

0.26

0.26

0.15

0.12

0.21

0.17

0.80

4.2

4.0

2.0

1.9

1.1

0.11

1.0

0.18

0.18

0.24

0.15

0.12

0.13

0.15

0.13

0.10

0.17

0.10

0.88

0.15

0.10

0.10

0.57

1.0

Sample Depth:

Serial_No:09091918:03

Page 24 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.88

1.8

1.8

1.8

1.8

70

1.8

1.8

1.8

1.8

4.4


Toluene-d8



107

101

114

102

70-130

70-130

70-130

70-130


09/09/19



L1939733-04Lab ID:


Total TIC Compounds

Unknown

Unknown

Unknown

Unknown

Ethyl Acetate

J

J

J

J

J

NJ

53.0

2.77

3.08

9.30

3.02

34.8

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1


MDL

0.15

0.28

0.24

0.17

0.29

31.

0.16

0.34

0.17

0.30

1.2

Sample Depth:

Serial_No:09091918:03

Page 25 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene



ND

ND

ND

ND

ND

ND

ND

30

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

230

46

69

46

46

46

46

23

23

180

46

23

23

46

23

23

23

180

23

23

46

46

180

92

46

92

46

69

09/09/19



L1939733-04Lab ID:




MDL

100

6.7

6.5

11.

5.8

6.5

12.

9.0

5.9

32.

12.

7.7

5.0

12.

7.3

7.3

7.3

11.

7.7

7.7

25.

6.5

43.

27.

15.

21.

11.

6.3

Sample Depth:

Serial_No:09091918:03

Page 26 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

23

92

92

92

92

92

46

46

46

46

92

46

460

460

460

460

460

460

92

460

92

92

46

92

23

92

46

46

92

92

92

140

180

46

46

180

180

09/09/19



L1939733-04Lab ID:


MDL

6.3

6.6

6.8

7.9

9.3

26.

13.

13.

8.1

6.3

11.

9.0

42.

220

210

100

99.

59.

5.9

54.

9.5

9.3

13.

7.7

6.1

6.7

7.7

6.7

5.4

8.8

5.0

46.

7.8

5.0

5.0

30.

53.

Sample Depth:

Serial_No:09091918:03

Page 27 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

46

92

92

92

92

3700

92

92

92

92

230


Toluene-d8



110

97

95

100

70-130

70-130

70-130

70-130


09/09/19



L1939733-04Lab ID:




MDL

7.9

15.

12.

8.9

15.

1600

8.2

18.

8.8

16.

66.

Sample Depth:

Serial_No:09091918:03

Page 28 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

J

Dilution Factor

ND

ND

0.18

ND

ND

ND

ND

0.28

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

6.0

1.2

1.8

1.2

1.2

1.2

1.2

0.60

0.60

4.8

1.2

0.60

0.60

1.2

0.60

0.60

0.60

4.8

0.60

0.60

1.2

1.2

4.8

2.4

1.2

2.4

1.2

1.8

09/09/19



L1939733-05Lab ID:




MDL

2.7

0.17

0.17

0.27

0.15

0.17

0.32

0.23

0.15

0.83

0.31

0.20

0.13

0.32

0.19

0.19

0.19

0.29

0.20

0.20

0.65

0.17

1.1

0.69

0.40

0.54

0.28

0.16

Sample Depth:

Serial_No:09091918:03

Page 29 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

1.0

ND

ND

ND

ND

ND

ND

ND

ND

180

ND

5.1

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.60

2.4

2.4

2.4

2.4

2.4

1.2

1.2

1.2

1.2

2.4

1.2

12

12

12

12

12

12

2.4

12

2.4

2.4

1.2

2.4

0.60

2.4

1.2

1.2

2.4

2.4

2.4

3.6

4.8

1.2

1.2

4.8

4.8

09/09/19



L1939733-05Lab ID:


MDL

0.16

0.17

0.18

0.20

0.24

0.67

0.35

0.35

0.21

0.16

0.28

0.23

1.1

5.7

5.4

2.6

2.6

1.5

0.15

1.4

0.24

0.24

0.33

0.20

0.16

0.17

0.20

0.17

0.14

0.23

0.13

1.2

0.20

0.13

0.13

0.78

1.4

Sample Depth:

Serial_No:09091918:03

Page 30 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.2

2.4

2.4

2.4

2.4

96

2.4

2.4

2.4

2.4

6.0


Toluene-d8



107

100

110

103

70-130

70-130

70-130

70-130


09/09/19



L1939733-05Lab ID:


Total TIC Compounds

Ethyl Acetate


J

NJ

NJ

179

172

7.15

ug/kg

ug/kg

ug/kg

1

1

1


MDL

0.20

0.38

0.32

0.23

0.40

42.

0.21

0.46

0.23

0.41

1.7

Sample Depth:

Serial_No:09091918:03

Page 31 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

J

Dilution Factor

ND

ND

0.17

ND

ND

ND

ND

0.45

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

5.2

1.0

1.6

1.0

1.0

1.0

1.0

0.52

0.52

4.2

1.0

0.52

0.52

1.0

0.52

0.52

0.52

4.2

0.52

0.52

1.0

1.0

4.2

2.1

1.0

2.1

1.0

1.6

09/09/19



L1939733-06Lab ID:




MDL

2.4

0.15

0.15

0.24

0.13

0.15

0.28

0.20

0.13

0.73

0.27

0.17

0.11

0.28

0.16

0.16

0.17

0.26

0.17

0.17

0.57

0.15

0.98

0.61

0.35

0.47

0.25

0.14

Sample Depth:

Serial_No:09091918:03

Page 32 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

E

Dilution Factor

ND

ND

ND

ND

1.1

ND

ND

ND

ND

ND

ND

ND

ND

540

ND

13

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.52

2.1

2.1

2.1

2.1

2.1

1.0

1.0

1.0

1.0

2.1

1.0

10

10

10

10

10

10

2.1

10

2.1

2.1

1.0

2.1

0.52

2.1

1.0

1.0

2.1

2.1

2.1

3.1

4.2

1.0

1.0

4.2

4.2

09/09/19



L1939733-06Lab ID:


MDL

0.14

0.15

0.15

0.18

0.21

0.59

0.30

0.30

0.18

0.14

0.25

0.20

0.96

5.0

4.8

2.3

2.2

1.3

0.13

1.2

0.21

0.21

0.29

0.17

0.14

0.15

0.17

0.15

0.12

0.20

0.11

1.0

0.18

0.11

0.11

0.68

1.2

Sample Depth:

Serial_No:09091918:03

Page 33 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.0

2.1

2.1

2.1

2.1

84

2.1

2.1

2.1

2.1

5.2


Toluene-d8



111

99

109

102

70-130

70-130

70-130

70-130


09/09/19



L1939733-06Lab ID:


Total TIC Compounds

Ethyl Acetate

Unknown

J

NJ

J

145

136

9.37

ug/kg

ug/kg

ug/kg

1

1

1


MDL

0.18

0.34

0.28

0.20

0.35

37.

0.18

0.40

0.20

0.36

1.5

Sample Depth:

Serial_No:09091918:03

Page 34 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

14

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

300

60

90

60

60

60

60

30

30

240

60

30

30

60

30

30

30

240

30

30

60

60

240

120

60

120

60

90

09/09/19



L1939733-06Lab ID:




MDL

140

8.7

8.4

14.

7.5

8.4

16.

12.

7.7

42.

16.

10.

6.6

16.

9.5

9.5

9.6

15.

10.

10.

33.

8.5

56.

35.

20.

27.

14.

8.3

Sample Depth:

Serial_No:09091918:03

Page 35 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

30

120

120

120

120

120

60

60

60

60

120

60

600

600

600

600

600

600

120

600

120

120

60

120

30

120

60

60

120

120

120

180

240

60

60

240

240

09/09/19



L1939733-06Lab ID:


MDL

8.3

8.7

8.9

10.

12.

34.

18.

18.

10.

8.3

14.

12.

55.

290

270

130

130

77.

7.7

71.

12.

12.

17.

10.

8.0

8.7

10.

8.8

7.1

12.

6.5

60.

10.

6.6

6.6

39.

69.

Sample Depth:

Serial_No:09091918:03

Page 36 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

60

120

120

120

120

4800

120

120

120

120

300


Toluene-d8



107

96

94

100

70-130

70-130

70-130

70-130


09/09/19



L1939733-06Lab ID:




MDL

10.

19.

16.

12.

20.

2100

11.

23.

12.

20.

86.

Sample Depth:

Serial_No:09091918:03

Page 37 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

4.9

0.98

1.5

0.98

0.98

0.98

0.98

0.49

0.49

3.9

0.98

0.49

0.49

0.98

0.49

0.49

0.49

3.9

0.49

0.49

0.98

0.98

3.9

2.0

0.98

2.0

0.98

1.5

09/09/19



L1939733-07Lab ID:




MDL

2.2

0.14

0.14

0.22

0.12

0.14

0.26

0.19

0.12

0.68

0.25

0.16

0.11

0.27

0.16

0.16

0.16

0.24

0.16

0.16

0.53

0.14

0.91

0.57

0.33

0.44

0.23

0.13

Sample Depth:

Serial_No:09091918:03

Page 38 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

1.0

ND

ND

ND

ND

ND

ND

ND

ND

200

ND

6.1

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.49

2.0

2.0

2.0

2.0

2.0

0.98

0.98

0.98

0.98

2.0

0.98

9.8

9.8

9.8

9.8

9.8

9.8

2.0

9.8

2.0

2.0

0.98

2.0

0.49

2.0

0.98

0.98

2.0

2.0

2.0

2.9

3.9

0.98

0.98

3.9

3.9

09/09/19



L1939733-07Lab ID:


MDL

0.13

0.14

0.14

0.17

0.20

0.55

0.28

0.28

0.17

0.13

0.23

0.19

0.90

4.7

4.5

2.2

2.1

1.2

0.12

1.2

0.20

0.20

0.27

0.16

0.13

0.14

0.16

0.14

0.12

0.19

0.10

0.98

0.16

0.11

0.11

0.64

1.1

Sample Depth:

Serial_No:09091918:03

Page 39 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.98

2.0

2.0

2.0

2.0

78

2.0

2.0

2.0

2.0

4.9


Toluene-d8



108

99

110

102

70-130

70-130

70-130

70-130


09/09/19



L1939733-07Lab ID:


Total TIC Compounds

Ethyl Acetate

J

NJ

169

169

ug/kg

ug/kg

1

1


MDL

0.17

0.32

0.27

0.19

0.33

34.

0.17

0.38

0.19

0.33

1.4

Sample Depth:

Serial_No:09091918:03

Page 40 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

5.0

1.0

1.5

1.0

1.0

1.0

1.0

0.50

0.50

4.0

1.0

0.50

0.50

1.0

0.50

0.50

0.50

4.0

0.50

0.50

1.0

1.0

4.0

2.0

1.0

2.0

1.0

1.5

09/09/19



L1939733-08Lab ID:




MDL

2.3

0.14

0.14

0.23

0.12

0.14

0.27

0.20

0.13

0.70

0.26

0.17

0.11

0.27

0.16

0.16

0.16

0.25

0.17

0.17

0.54

0.14

0.94

0.58

0.34

0.45

0.24

0.14

Sample Depth:

Serial_No:09091918:03

Page 41 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

1.0

ND

ND

ND

ND

ND

ND

ND

ND

210

ND

5.5

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.50

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

1.0

2.0

1.0

10

10

10

10

10

10

2.0

10

2.0

2.0

1.0

2.0

0.50

2.0

1.0

1.0

2.0

2.0

2.0

3.0

4.0

1.0

1.0

4.0

4.0

09/09/19



L1939733-08Lab ID:


MDL

0.14

0.14

0.15

0.17

0.20

0.56

0.29

0.29

0.18

0.14

0.24

0.20

0.92

4.8

4.6

2.2

2.2

1.3

0.13

1.2

0.20

0.20

0.28

0.17

0.13

0.14

0.17

0.15

0.12

0.19

0.11

1.0

0.17

0.11

0.11

0.65

1.2

Sample Depth:

Serial_No:09091918:03

Page 42 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.0

2.0

2.0

2.0

2.0

80

2.0

2.0

2.0

2.0

5.0


Toluene-d8



111

99

110

104

70-130

70-130

70-130

70-130


09/09/19



L1939733-08Lab ID:


Total TIC Compounds

Ethyl Acetate


J

NJ

NJ

170

163

7.00

ug/kg

ug/kg

ug/kg

1

1

1


MDL

0.17

0.32

0.27

0.19

0.34

35.

0.18

0.38

0.19

0.34

1.4

Sample Depth:

Serial_No:09091918:03

Page 43 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

4.2

0.85

1.3

0.85

0.85

0.85

0.85

0.42

0.42

3.4

0.85

0.42

0.42

0.85

0.42

0.42

0.42

3.4

0.42

0.42

0.85

0.85

3.4

1.7

0.85

1.7

0.85

1.3

09/09/19



L1939733-09Lab ID:




MDL

1.9

0.12

0.12

0.20

0.11

0.12

0.23

0.17

0.11

0.59

0.22

0.14

0.09

0.23

0.13

0.13

0.14

0.21

0.14

0.14

0.46

0.12

0.79

0.49

0.28

0.38

0.20

0.12

Sample Depth:

Serial_No:09091918:03

Page 44 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

0.93

ND

ND

ND

ND

ND

ND

ND

ND

240

ND

6.1

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.42

1.7

1.7

1.7

1.7

1.7

0.85

0.85

0.85

0.85

1.7

0.85

8.5

8.5

8.5

8.5

8.5

8.5

1.7

8.5

1.7

1.7

0.85

1.7

0.42

1.7

0.85

0.85

1.7

1.7

1.7

2.6

3.4

0.85

0.85

3.4

3.4

09/09/19



L1939733-09Lab ID:


MDL

0.12

0.12

0.12

0.14

0.17

0.48

0.25

0.25

0.15

0.12

0.20

0.17

0.78

4.1

3.9

1.9

1.8

1.1

0.11

1.0

0.17

0.17

0.24

0.14

0.11

0.12

0.14

0.12

0.10

0.16

0.09

0.85

0.14

0.09

0.09

0.55

0.98

Sample Depth:

Serial_No:09091918:03

Page 45 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.85

1.7

1.7

1.7

1.7

68

1.7

1.7

1.7

1.7

4.2


Toluene-d8



109

101

113

103

70-130

70-130

70-130

70-130


09/09/19



L1939733-09Lab ID:


Total TIC Compounds


Ethyl Acetate

J

NJ

NJ

138

11.8

126

ug/kg

ug/kg

ug/kg

1

1

1


MDL

0.14

0.27

0.23

0.16

0.28

30.

0.15

0.33

0.16

0.29

1.2

Sample Depth:

Serial_No:09091918:03

Page 46 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

5.6

1.1

1.7

1.1

1.1

1.1

1.1

0.56

0.56

4.5

1.1

0.56

0.56

1.1

0.56

0.56

0.56

4.5

0.56

0.56

1.1

1.1

4.5

2.3

1.1

2.3

1.1

1.7

09/09/19



L1939733-10Lab ID:




MDL

2.6

0.16

0.16

0.26

0.14

0.16

0.30

0.22

0.14

0.79

0.29

0.19

0.12

0.31

0.18

0.18

0.18

0.28

0.19

0.19

0.61

0.16

1.0

0.66

0.38

0.51

0.27

0.15

Sample Depth:

Serial_No:09091918:03

Page 47 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

0.66

ND

ND

ND

ND

ND

ND

ND

ND

110

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.56

2.3

2.3

2.3

2.3

2.3

1.1

1.1

1.1

1.1

2.3

1.1

11

11

11

11

11

11

2.3

11

2.3

2.3

1.1

2.3

0.56

2.3

1.1

1.1

2.3

2.3

2.3

3.4

4.5

1.1

1.1

4.5

4.5

09/09/19



L1939733-10Lab ID:


MDL

0.15

0.16

0.17

0.19

0.23

0.63

0.33

0.33

0.20

0.15

0.27

0.22

1.0

5.4

5.1

2.5

2.4

1.4

0.14

1.3

0.23

0.23

0.32

0.19

0.15

0.16

0.19

0.16

0.13

0.22

0.12

1.1

0.19

0.12

0.12

0.74

1.3

Sample Depth:

Serial_No:09091918:03

Page 48 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.1

2.3

2.3

2.3

2.3

90

2.3

2.3

2.3

2.3

5.6


Toluene-d8



108

102

117

103

70-130

70-130

70-130

70-130


09/09/19



L1939733-10Lab ID:


Total TIC Compounds

Ethyl Acetate

J

NJ

15.7

15.7

ug/kg

ug/kg

1

1


MDL

0.19

0.36

0.31

0.22

0.38

40.

0.20

0.43

0.22

0.38

1.6

Sample Depth:

Serial_No:09091918:03

Page 49 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

0.15

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

5.2

1.0

1.6

1.0

1.0

1.0

1.0

0.52

0.52

4.1

1.0

0.52

0.52

1.0

0.52

0.52

0.52

4.1

0.52

0.52

1.0

1.0

4.1

2.1

1.0

2.1

1.0

1.6

09/09/19



L1939733-11Lab ID:




MDL

2.4

0.15

0.14

0.24

0.13

0.14

0.28

0.20

0.13

0.72

0.27

0.17

0.11

0.28

0.16

0.16

0.16

0.26

0.17

0.17

0.56

0.15

0.97

0.60

0.35

0.47

0.25

0.14

Sample Depth:

Serial_No:09091918:03

Page 50 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

1.0

ND

ND

ND

ND

ND

ND

ND

ND

290

ND

8.0

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.52

2.1

2.1

2.1

2.1

2.1

1.0

1.0

1.0

1.0

2.1

1.0

10

10

10

10

10

10

2.1

10

2.1

2.1

1.0

2.1

0.52

2.1

1.0

1.0

2.1

2.1

2.1

3.1

4.1

1.0

1.0

4.1

4.1

09/09/19



L1939733-11Lab ID:


MDL

0.14

0.15

0.15

0.18

0.21

0.58

0.30

0.30

0.18

0.14

0.25

0.20

0.95

5.0

4.7

2.3

2.2

1.3

0.13

1.2

0.21

0.21

0.29

0.17

0.14

0.15

0.17

0.15

0.12

0.20

0.11

1.0

0.18

0.11

0.11

0.67

1.2

Sample Depth:

Serial_No:09091918:03

Page 51 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.0

2.1

2.1

2.1

2.1

83

2.1

2.1

2.1

2.1

5.2


Toluene-d8



109

98

108

103

70-130

70-130

70-130

70-130


09/09/19



L1939733-11Lab ID:


Total TIC Compounds

Ethyl Acetate

J

NJ

259

259

ug/kg

ug/kg

1

1


MDL

0.18

0.33

0.28

0.20

0.35

36.

0.18

0.40

0.20

0.35

1.5

Sample Depth:

Serial_No:09091918:03

Page 52 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.57

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

4.8

0.95

1.4

0.95

0.95

0.95

0.95

0.48

0.48

3.8

0.95

0.48

0.48

0.95

0.48

0.48

0.48

3.8

0.48

0.48

0.95

0.95

3.8

1.9

0.95

1.9

0.95

1.4

09/09/19



L1939733-12Lab ID:




MDL

2.2

0.14

0.13

0.22

0.12

0.13

0.25

0.19

0.12

0.66

0.24

0.16

0.10

0.26

0.15

0.15

0.15

0.23

0.16

0.16

0.52

0.13

0.89

0.55

0.32

0.43

0.23

0.13

Sample Depth:

Serial_No:09091918:03

Page 53 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

E

Dilution Factor

ND

ND

ND

ND

1.2

ND

ND

ND

ND

ND

ND

ND

ND

510

ND

14

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.48

1.9

1.9

1.9

1.9

1.9

0.95

0.95

0.95

0.95

1.9

0.95

9.5

9.5

9.5

9.5

9.5

9.5

1.9

9.5

1.9

1.9

0.95

1.9

0.48

1.9

0.95

0.95

1.9

1.9

1.9

2.8

3.8

0.95

0.95

3.8

3.8

09/09/19



L1939733-12Lab ID:


MDL

0.13

0.14

0.14

0.16

0.19

0.53

0.28

0.28

0.17

0.13

0.23

0.19

0.87

4.6

4.3

2.1

2.0

1.2

0.12

1.1

0.20

0.19

0.26

0.16

0.12

0.14

0.16

0.14

0.11

0.18

0.10

0.95

0.16

0.10

0.10

0.62

1.1

Sample Depth:

Serial_No:09091918:03

Page 54 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

0.95

1.9

1.9

1.9

1.9

76

1.9

1.9

1.9

1.9

4.8


Toluene-d8



108

99

106

102

70-130

70-130

70-130

70-130


09/09/19



L1939733-12Lab ID:


Total TIC Compounds

Ethyl Acetate

J

NJ

451

451

ug/kg

ug/kg

1

1


MDL

0.16

0.31

0.26

0.18

0.32

33.

0.17

0.36

0.18

0.32

1.4

Sample Depth:

Serial_No:09091918:03

Page 55 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

280

56

84

56

56

56

56

28

28

220

56

28

28

56

28

28

28

220

28

28

56

56

220

110

56

110

56

84

09/09/19



L1939733-12Lab ID:




MDL

130

8.2

7.9

13.

7.0

7.9

15.

11.

7.1

39.

14.

9.4

6.1

15.

8.9

8.9

8.9

14.

9.3

9.3

30.

7.9

52.

33.

19.

25.

13.

7.7

Sample Depth:

Serial_No:09091918:03

Page 56 of 222

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

28

110

110

110

110

110

56

56

56

56

110

56

560

560

560

560

560

560

110

560

110

110

56

110

28

110

56

56

110

110

110

170

220

56

56

220

220

09/09/19



L1939733-12Lab ID:


MDL

7.7

8.1

8.3

9.6

11.

31.

16.

16.

9.8

7.7

13.

11.

51.

270

260

120

120

72.

7.1

66.

12.

11.

16.

9.4

7.4

8.2

9.4

8.2

6.6

11.

6.1

56.

9.5

6.1

6.1

36.

65.

Sample Depth:

Serial_No:09091918:03

Page 57 of 222

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

56

110

110

110

110

4500

110

110

110

110

280


Toluene-d8



108

95

94

100

70-130

70-130

70-130

70-130


09/09/19



L1939733-12Lab ID:




MDL

9.6

18.

15.

11.

19.

2000

10.

22.

11.

19.

80.

Sample Depth:

Serial_No:09091918:03

Page 58 of 222

Method Blank AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/07/19 09:371,8260CAnalytical Method:

Analytical Date:

09/09/19

Analyst: MKS

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

5.0

1.0

1.5

1.0

1.0

1.0

1.0

0.50

0.50

4.0

1.0

0.50

0.50

1.0

0.50

0.50

0.50

4.0

0.50

0.50

1.0

1.0

4.0

2.0

1.0

2.0

1.0

1.5

0.50

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Volatile Organics by EPA 5035 Low - Westborough Lab for sample(s): 01-12 Batch: WG1281594-5

MDL

2.3

0.14

0.14

0.23

0.12

0.14

0.27

0.20

0.13

0.70

0.26

0.17

0.11

0.27

0.16

0.16

0.16

0.25

0.17

0.17

0.54

0.14

0.93

0.58

0.34

0.45

0.24

0.14

0.14

Serial_No:09091918:03

Page 59 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Analytical Date:

09/09/19

Analyst: MKS

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

1.0

2.0

1.0

10

10

10

10

10

10

2.0

10

2.0

2.0

1.0

2.0

0.50

2.0

1.0

1.0

2.0

2.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

0.14

0.15

0.17

0.20

0.56

0.29

0.29

0.18

0.14

0.24

0.20

0.92

4.8

4.6

2.2

2.2

1.3

0.13

1.2

0.20

0.20

0.28

0.17

0.13

0.14

0.17

0.15

0.12

0.19

Serial_No:09091918:03

Page 60 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Analytical Date:

09/09/19

Analyst: MKS

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.0

3.0

4.0

1.0

1.0

4.0

4.0

1.0

2.0

2.0

2.0

2.0

80

2.0

2.0

2.0

2.0

5.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


No Tentatively Identified Compounds ND ug/kg


MDL

0.11

1.0

0.17

0.11

0.11

0.65

1.2

0.17

0.32

0.27

0.19

0.33

35.

0.18

0.38

0.19

0.34

1.4

Serial_No:09091918:03

Page 61 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Analytical Date:

09/09/19

Analyst: MKS

Parameter Result RLUnitsQualifier



Toluene-d8



103

98

106

100

70-130

70-130

70-130

70-130

Surrogate %Recovery QualifierAcceptance

Criteria

MDL

Serial_No:09091918:03

Page 62 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Analytical Date:

09/09/19

Analyst: AD

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

Parameter Result

160

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

250

50

75

50

50

50

50

25

25

200

50

25

25

50

25

25

25

200

25

25

50

50

200

100

50

100

50

75

25

J ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Volatile Organics by EPA 5035 High - Westborough Lab for sample(s): 01,03-04,06,12 Batch: WG1281807-5

MDL

110

7.2

7.0

12.

6.2

7.0

13.

9.8

6.4

35.

13.

8.4

5.4

14.

7.9

7.9

8.0

12.

8.3

8.3

27.

7.0

47.

29.

17.

23.

12.

6.8

6.8

Serial_No:09091918:03

Page 63 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Analytical Date:

09/09/19

Analyst: AD

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

Parameter Result

ND

ND

ND

10

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

100

100

100

100

100

50

50

50

50

100

50

500

500

500

500

500

500

100

500

100

100

50

100

25

100

50

50

100

100

J

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

7.2

7.4

8.6

10.

28.

14.

14.

8.8

6.8

12.

9.8

46.

240

230

110

110

64.

6.4

59.

10.

10.

14.

8.4

6.6

7.2

8.4

7.3

5.9

9.6

Serial_No:09091918:03

Page 64 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Analytical Date:

09/09/19

Analyst: AD

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

100

150

200

50

50

200

200

50

100

100

100

100

4000

100

100

100

100

250

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier




MDL

5.4

50.

8.4

5.4

5.4

32.

58.

8.6

16.

14.

9.6

17.

1800

8.8

19.

9.6

17.

71.

Serial_No:09091918:03

Page 65 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Analytical Date:

09/09/19

Analyst: AD




Toluene-d8



107

96

93

99

70-130

70-130

70-130

70-130


Criteria

MDL

Serial_No:09091918:03

Page 66 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

100

110

101

106

108

92

98

91

92

120

105

105

100

100

104

112

86

99

105

98

100

143

110

102

112

104

108

111

93

100

92

94

122

108

107

104

102

107

113

89

101

107

100

102

143

114

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-139

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

52-130

57-147

2

2

3

2

3

1

2

1

2

2

3

2

4

2

3

1

3

2

2

2

2

0

4

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Volatile Organics by EPA 5035 Low - Westborough Lab Associated sample(s): 01-12 Batch: WG1281594-3 WG1281594-4

Lab Control Sample AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual

Q Q

Qual

Serial_No:09091918:03

Page 67 of 222

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

141

130

112

106

103

92

94

94

102

98

95

101

102

98

203

122

117

119

115

104

99

108

97

140

130

115

109

105

93

95

94

106

99

97

105

105

100

205

123

119

119

119

104

100

110

100

67-130

50-151

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

70-130

70-130

30-146

54-140

59-130

70-130

70-130

70-130

68-130

70-130

70-130

1

0

3

3

2

1

1

0

4

1

2

4

3

2

1

1

2

0

3

0

1

2

3

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual

Q

Q

Q

Q

Qual

Serial_No:09091918:03

Page 68 of 222

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

108

95

98

92

90

100

101

98

98

100

89

88

99

99

100

114

103

92

94

99

100

105

94

110

96

100

93

92

101

102

99

100

101

90

88

100

99

100

117

104

95

97

100

100

105

94

70-130

70-130

69-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

68-130

67-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

65-136

70-130

2

1

2

1

2

1

1

1

2

1

1

0

1

0

0

3

1

3

3

1

0

0

0

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual Qual

Serial_No:09091918:03

Page 69 of 222

p-Ethyltoluene


Ethyl ether


94

93

106

106

96

93

109

106

70-130

70-130

67-130

70-130

2

0

3

0

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1,2-Dichloroethane-d4Toluene-d84-BromofluorobenzeneDibromofluoromethane

1049910598

70-13070-13070-13070-130

1039810499

Surrogate Qual%Recovery Qual%RecoveryLCS LCSD

09/09/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09091918:03

Page 70 of 222

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

136

102

103

100

98

95

97

92

91

128

107

99

96

98

94

96

97

94

91

92

94

102

116

141

102

101

99

95

95

96

89

90

127

107

98

94

97

94

94

95

93

90

91

93

101

114

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-139

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

52-130

57-147

4

0

2

1

3

0

1

3

1

1

0

1

2

1

0

2

2

1

1

1

1

1

2

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Volatile Organics by EPA 5035 High - Westborough Lab Associated sample(s): 01,03-04,06,12 Batch: WG1281807-3 WG1281807-4


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual

Q Q

Qual

Serial_No:09091918:03

Page 71 of 222

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

114

125

99

97

93

93

94

93

100

92

90

94

100

90

88

135

98

108

100

91

102

86

96

112

123

97

95

92

91

93

92

99

90

90

93

99

89

87

119

96

100

100

92

101

82

94

67-130

50-151

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

70-130

70-130

30-146

54-140

59-130

70-130

70-130

70-130

68-130

70-130

70-130

2

2

2

2

1

2

1

1

1

2

0

1

1

1

1

13

2

8

0

1

1

5

2

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual Qual

Serial_No:09091918:03

Page 72 of 222

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

99

95

97

91

93

98

92

91

96

94

92

88

91

92

86

104

96

91

91

93

93

110

92

96

96

97

90

91

96

91

90

93

93

87

86

90

90

87

102

94

90

91

92

92

105

90

70-130

70-130

69-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

68-130

67-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

65-136

70-130

3

1

0

1

2

2

1

1

3

1

6

2

1

2

1

2

2

1

0

1

1

5

2

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual Qual

Serial_No:09091918:03

Page 73 of 222

p-Ethyltoluene


Ethyl ether


94

90

116

104

92

89

116

102

70-130

70-130

67-130

70-130

2

1

0

2

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


1089693101

70-13070-13070-13070-130

1099692100


09/09/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09091918:03

Page 74 of 222

SEMIVOLATILES

Serial_No:09091918:03

Page 75 of 222

FF

Acenaphthene


Hexachlorobenzene

Bis(2-chloroethyl)ether

2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

3,3'-Dichlorobenzidine

2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene

4-Chlorophenyl phenyl ether

4-Bromophenyl phenyl ether

Bis(2-chloroisopropyl)ether

Bis(2-chloroethoxy)methane

Hexachlorobutadiene

Hexachlorocyclopentadiene

Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA

n-Nitrosodi-n-propylamine

Bis(2-ethylhexyl)phthalate

Butyl benzyl phthalate

Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

370

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

120

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Semivolatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

150

190

110

170

190

190

190

190

190

190

190

110

190

190

220

200

190

530

150

170

190

170

150

190

190

190

190

190

09/09/19



L1939733-01Lab ID:


Matrix: Soil Extraction Method:

Analytical Method:Analytical Date:Analyst:

1,8270D09/06/19 02:20KR

EPA 3546Extraction Date: 09/04/19 04:27

87%Percent Solids:

MDL

19.

21.

21.

25.

18.

34.

32.

33.

50.

37.

32.

21.

20.

28.

32.

19.

27.

170

30.

24.

23.

28.

21.

29.

65.

47.

35.

64.

Sample Depth:

Serial_No:09091918:03

Page 76 of 222

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene

Dibenzo(a,h)anthracene

Indeno(1,2,3-cd)pyrene

Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene

1,2,4,5-Tetrachlorobenzene

Acetophenone

2,4,6-Trichlorophenol

p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol

4,6-Dinitro-o-cresol

Pentachlorophenol

Phenol

2-Methylphenol

3-Methylphenol/4-Methylphenol

Parameter Result

J

J

J

J

J

Dilution Factor

ND

ND

180

190

240

100

180

ND

56

120

ND

210

23

110

310

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

190

190

110

150

110

110

110

150

110

150

190

110

110

150

110

430

190

190

190

190

190

220

190

190

110

190

190

170

190

400

260

900

490

150

190

190

270

09/09/19



L1939733-01Lab ID:


MDL

17.

39.

21.

46.

31.

30.

19.

29.

36.

22.

18.

23.

22.

26.

18.

43.

34.

36.

35.

77.

18.

22.

20.

23.

35.

28.

22.

30.

62.

70.

76.

87.

90.

41.

28.

29.

29.

Sample Depth:

Serial_No:09091918:03

Page 77 of 222


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

J

Dilution Factor

ND

ND

ND

20

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

190

600

190

190

28

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl

2,4,6-Tribromophenol

4-Terphenyl-d14

78

80

65

54

135

59

25-120

10-120

23-120

30-120

10-136

18-120


09/09/19



L1939733-01Lab ID:


Total TIC Compounds

Unknown

Unknown

J

J

J

1320

702

617

ug/kg

ug/kg

ug/kg

1

1

1


MDL

36.

190

57.

18.

8.6

Sample Depth:

Serial_No:09091918:03

Page 78 of 222

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

J

Dilution Factor

94

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

6600

ND

ND

ND

ND

ND

ND

ND

ND

120

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

270

340

200

300

340

340

340

340

340

340

340

200

340

340

400

360

340

960

270

300

340

300

270

340

340

340

340

340

09/09/19



L1939733-02Lab ID:


D



1,8270D09/09/19 14:31KR


96%Percent Solids:

MDL

35.

39.

38.

46.

33.

61.

58.

59.

90.

68.

58.

39.

36.

52.

58.

34.

49.

300

55.

44.

41.

50.

38.

52.

120

85.

64.

110

Sample Depth:

Serial_No:09091918:03

Page 79 of 222

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

Dilution Factor

ND

ND

4000

3200

4200

1600

3300

83

1000

1900

120

2700

480

2100

5700

ND

ND

ND

ND

ND

70

41

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

340

340

200

270

200

200

200

270

200

270

340

200

200

270

200

770

340

340

340

340

340

400

340

340

200

340

340

300

340

730

470

1600

880

270

340

340

490

09/09/19



L1939733-02Lab ID:


D

MDL

31.

71.

38.

82.

57.

54.

35.

52.

66.

40.

33.

41.

39.

47.

34.

78.

61.

65.

64.

140

32.

41.

35.

42.

64.

50.

40.

54.

110

130

140

160

160

74.

51.

52.

53.

Sample Depth:

Serial_No:09091918:03

Page 80 of 222


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

J

Dilution Factor

ND

ND

ND

110

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

2

2

2

2

2

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

340

1100

340

340

51

09/09/19



L1939733-02Lab ID:


D

Total TIC Compounds

Unknown PAH

Unknown

Unknown PAH

Unknown PAH

Dibenzothiophene

Unknown PAH

Unknown PAH

Unknown PAH

Unknown PAH

Unknown PAH

Unknown Ketone

Unknown PAH

Unknown PAH

Unknown Ketone

Unknown Thiophene

Unknown PAH

Unknown

Unknown

Unknown PAH

J

J

J

J

J

NJ

J

J

J

J

J

J

J

J

J

J

J

J

J

J

12600

523

811

563

919

294

440

460

604

2210

1020

404

304

570

802

319

725

407

363

885

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2


MDL

65.

340

100

33.

16.

Sample Depth:

Serial_No:09091918:03

Page 81 of 222

Parameter Result Dilution FactorQualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

31

37

31

35

28

31

25-120

10-120

23-120

30-120

10-136

18-120


09/09/19



L1939733-02Lab ID:


D

MDL

Sample Depth:

Serial_No:09091918:03

Page 82 of 222

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

J

Dilution Factor

230

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

8200

ND

ND

ND

ND

ND

ND

ND

ND

330

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

590

740

440

660

740

740

740

740

740

740

740

440

740

740

880

800

740

2100

590

660

740

660

590

740

740

740

740

740

09/09/19



L1939733-03Lab ID:


D



1,8270D09/09/19 15:50KR


89%Percent Solids:

MDL

76.

84.

82.

100

73.

130

130

130

200

150

130

85.

79.

110

120

74.

110

670

120

96.

90.

110

84.

110

260

180

140

250

Sample Depth:

Serial_No:09091918:03

Page 83 of 222

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

Dilution Factor

ND

ND

4400

4200

5300

2100

4200

160

1700

2300

290

4600

560

2400

6800

ND

ND

ND

ND

ND

200

95

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

740

740

440

590

440

440

440

590

440

590

740

440

440

590

440

1700

740

740

740

740

740

880

740

740

440

740

740

660

740

1600

1000

3500

1900

590

740

740

1100

09/09/19



L1939733-03Lab ID:


D

MDL

68.

150

83.

180

120

120

77.

110

140

87.

72.

90.

85.

100

73.

170

130

140

140

300

70.

89.

77.

91.

140

110

87.

120

240

280

300

340

350

160

110

110

120

Sample Depth:

Serial_No:09091918:03

Page 84 of 222


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

J

Dilution Factor

ND

ND

ND

230

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

4

4

4

4

4

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

740

2400

740

740

110

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

36

35

37

45

57

36

25-120

10-120

23-120

30-120

10-136

18-120


09/09/19



L1939733-03Lab ID:


D

Total TIC Compounds

Unknown

Unknown PAH

Unknown

Unknown

Unknown Dibenzopyrene

Unknown

Unknown PAH


Unknown PAH

Unknown PAH

Unknown PAH

Unknown


J

J

J

J

J

J

J

J

J

J

J

J

J

J

12500

1010

2290

671

865

967

626

724

1040

772

861

1180

637

884

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

4

4

4

4

4

4

4

4

4

4

4

4

4

4


MDL

140

750

220

72.

34.

Sample Depth:

Serial_No:09091918:03

Page 85 of 222

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

Dilution Factor

110

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

2000

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

140

170

100

160

170

170

170

170

170

170

170

100

170

170

210

190

170

500

140

160

170

160

140

170

170

170

170

170

09/09/19



L1939733-04Lab ID:




1,8270D09/06/19 03:39KR


96%Percent Solids:

MDL

18.

20.

19.

23.

17.

31.

30.

30.

46.

35.

30.

20.

18.

26.

30.

17.

25.

160

28.

22.

21.

26.

20.

27.

60.

44.

33.

59.

Sample Depth:

Serial_No:09091918:03

Page 86 of 222

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

Dilution Factor

ND

ND

950

930

1200

510

920

68

270

520

94

1100

120

550

1700

ND

ND

ND

ND

ND

38

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

170

170

100

140

100

100

100

140

100

140

170

100

100

140

100

390

170

170

170

170

170

210

170

170

100

170

170

160

170

370

240

830

450

140

170

170

250

09/09/19



L1939733-04Lab ID:


MDL

16.

36.

20.

42.

29.

28.

18.

27.

34.

20.

17.

21.

20.

24.

17.

40.

32.

33.

33.

72.

16.

21.

18.

21.

33.

26.

20.

28.

57.

65.

71.

81.

83.

38.

26.

27.

27.

Sample Depth:

Serial_No:09091918:03

Page 87 of 222


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

J

Dilution Factor

ND

ND

ND

110

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

170

560

170

170

26

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

83

83

88

76

146

60

25-120

10-120

23-120

30-120

10-136

18-120

Acceptance Criteria

Q

Surrogate % Recovery Qualifier

09/09/19



L1939733-04Lab ID:


Total TIC Compounds

Unknown

Unknown PAH

Unknown

Unknown PAH

Unknown PAH

Unknown

Unknown PAH

Unknown

Unknown PAH

Unknown PAH

Unknown PAH

Unknown PAH

J

J

J

J

J

J

J

J

J

J

J

J

J

3050

173

196

462

140

226

153

150

316

510

223

273

229

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1


MDL

33.

180

53.

17.

8.0

Sample Depth:

Serial_No:09091918:03

Page 88 of 222

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

150

190

120

170

190

190

190

190

190

190

190

120

190

190

230

210

190

550

150

170

190

170

150

190

190

190

190

190

09/09/19



L1939733-05Lab ID:




1,8270D09/06/19 00:36KR


85%Percent Solids:

MDL

20.

22.

22.

26.

19.

35.

33.

34.

52.

39.

33.

22.

21.

30.

33.

19.

28.

180

31.

25.

24.

29.

22.

30.

67.

49.

37.

66.

Sample Depth:

Serial_No:09091918:03

Page 89 of 222

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

190

190

120

150

120

120

120

150

120

150

190

120

120

150

120

440

190

190

190

190

190

230

190

190

120

190

190

170

190

420

270

930

500

150

190

190

280

09/09/19



L1939733-05Lab ID:


MDL

18.

41.

22.

47.

33.

31.

20.

30.

38.

23.

19.

24.

22.

27.

19.

45.

35.

37.

36.

80.

18.

23.

20.

24.

37.

29.

23.

31.

64.

73.

79.

90.

93.

43.

29.

30.

30.

Sample Depth:

Serial_No:09091918:03

Page 90 of 222


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane


ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

190

630

190

190

29

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

5

33

59

60

0

71

25-120

10-120

23-120

30-120

10-136

18-120

Acceptance Criteria

Q

Q


09/09/19



L1939733-05Lab ID:


Total TIC Compounds

Unknown

Unknown Aldehyde

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown Organic Acid

Unknown

Aldol Condensates (A)

Unknown

J

J

J

J

J

J

J

J

J

J

J

J

J

23300

1130

156

5440

198

400

1400

155

267

266

6640

6500

781

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1


MDL

37.

200

59.

19.

8.9

Sample Depth:

Serial_No:09091918:03

Page 91 of 222

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

450

570

340

510

570

570

570

570

570

570

570

340

570

570

680

610

570

1600

450

510

570

510

450

570

570

570

570

570

09/09/19



L1939733-05Lab ID:


RE



1,8270D09/09/19 15:23KR


85%Percent Solids:

MDL

59.

65.

64.

77.

56.

100

98.

99.

150

110

97.

65.

61.

87.

97.

57.

83.

510

92.

74.

69.

84.

65.

88.

200

140

110

190

Sample Depth:

Serial_No:09091918:03

Page 92 of 222

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

570

570

340

450

340

340

340

450

340

450

570

340

340

450

340

1300

570

570

570

570

570

680

570

570

340

570

570

510

570

1200

800

2700

1500

450

570

570

820

09/09/19



L1939733-05Lab ID:


RE

MDL

52.

120

64.

140

96.

91.

59.

88.

110

67.

55.

69.

66.

79.

56.

130

100

110

110

240

54.

69.

59.

70.

110

85.

67.

91.

190

210

230

260

270

120

86.

88.

89.

Sample Depth:

Serial_No:09091918:03

Page 93 of 222


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane


ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

570

1800

570

570

85

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

11

40

42

47

2

38

25-120

10-120

23-120

30-120

10-136

18-120

Acceptance Criteria

Q

Q


09/09/19



L1939733-05Lab ID:


RE

Total TIC Compounds


Unknown

J

J

J

2260

1270

986

ug/kg

ug/kg

ug/kg

1

1

1


MDL

110

570

170

55.

26.

Sample Depth:

Serial_No:09091918:03

Page 94 of 222

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

J

Dilution Factor

270

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

5200

ND

ND

ND

ND

ND

ND

ND

ND

200

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

330

410

250

370

410

410

410

410

410

410

410

250

410

410

500

450

410

1200

330

370

410

370

330

410

410

410

410

410

09/09/19



L1939733-06Lab ID:


D



1,8270D09/09/19 14:57KR


78%Percent Solids:

MDL

43.

47.

46.

56.

41.

74.

71.

72.

110

83.

71.

48.

44.

63.

71.

41.

60.

370

67.

54.

50.

61.

47.

64.

140

100

78.

140

Sample Depth:

Serial_No:09091918:03

Page 95 of 222

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

Dilution Factor

ND

ND

2600

2500

3200

1300

2500

550

910

1500

270

3100

340

1600

4400

ND

ND

ND

ND

ND

160

66

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

410

410

250

330

250

250

250

330

250

330

410

250

250

330

250

940

410

410

410

410

410

500

410

410

250

410

410

370

410

890

580

2000

1100

330

410

410

600

09/09/19



L1939733-06Lab ID:


D

MDL

38.

87.

46.

100

70.

66.

43.

64.

81.

49.

40.

50.

48.

58.

41.

96.

75.

80.

78.

170

39.

50.

43.

51.

78.

62.

49.

66.

140

160

170

190

200

91.

62.

64.

65.

Sample Depth:

Serial_No:09091918:03

Page 96 of 222


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

J

Dilution Factor

ND

ND

ND

380

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

2

2

2

2

2

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

410

1300

410

410

62

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

63

60

50

58

84

46

25-120

10-120

23-120

30-120

10-136

18-120


09/09/19



L1939733-06Lab ID:


D

Total TIC Compounds

Unknown

Unknown PAH

Unknown PAH

Unknown PAH

Unknown Ketone

Unknown


Unknown PAH

Unknown PAH

Unknown

Unknown PAH

Unknown PAH

Unknown

J

J

J

J

J

J

J

J

J

J

J

J

J

J

7130

351

513

1280

545

368

530

584

682

515

415

530

466

352

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2


MDL

79.

420

130

40.

19.

Sample Depth:

Serial_No:09091918:03

Page 97 of 222

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

Dilution Factor

26

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

1100

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

140

180

110

160

180

180

180

180

180

180

180

110

180

180

210

190

180

510

140

160

180

160

140

180

180

180

180

180

09/09/19



L1939733-07Lab ID:




1,8270D09/06/19 04:31KR


92%Percent Solids:

MDL

18.

20.

20.

24.

18.

32.

31.

31.

47.

36.

31.

20.

19.

27.

30.

18.

26.

160

29.

23.

22.

26.

20.

28.

62.

45.

34.

61.

Sample Depth:

Serial_No:09091918:03

Page 98 of 222

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

Dilution Factor

ND

ND

390

360

500

200

360

58

130

210

42

550

46

210

890

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

180

180

110

140

110

110

110

140

110

140

180

110

110

140

110

410

180

180

180

180

180

210

180

180

110

180

180

160

180

380

250

860

460

140

180

180

260

09/09/19



L1939733-07Lab ID:


MDL

16.

37.

20.

44.

30.

28.

18.

28.

35.

21.

17.

22.

21.

25.

18.

41.

32.

34.

34.

74.

17.

22.

19.

22.

34.

26.

21.

29.

59.

67.

73.

83.

86.

39.

27.

28.

28.

Sample Depth:

Serial_No:09091918:03

Page 99 of 222


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

J

Dilution Factor

ND

ND

ND

85

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

180

580

180

180

27

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

67

66

51

62

102

60

25-120

10-120

23-120

30-120

10-136

18-120


09/09/19



L1939733-07Lab ID:


Total TIC Compounds

Unknown PAH

Unknown

Unknown Ketone

Unknown PAH

Unknown

Unknown PAH

J

J

J

J

J

J

J

1460

183

272

148

149

542

163

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1


MDL

34.

180

54.

17.

8.2

Sample Depth:

Serial_No:09091918:03

Page 100 of 222

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

Dilution Factor

30

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

690

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

160

200

120

180

200

200

200

200

200

200

200

120

200

200

240

220

200

580

160

180

200

180

160

200

200

200

200

200

09/09/19



L1939733-08Lab ID:




1,8270D09/06/19 04:57KR


81%Percent Solids:

MDL

21.

23.

23.

27.

20.

36.

35.

35.

54.

40.

35.

23.

22.

31.

34.

20.

30.

180

33.

26.

25.

30.

23.

31.

70.

51.

38.

69.

Sample Depth:

Serial_No:09091918:03

Page 101 of 222

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

Dilution Factor

ND

ND

340

340

440

170

340

ND

84

200

40

330

48

180

570

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

200

200

120

160

120

120

120

160

120

160

200

120

120

160

120

460

200

200

200

200

200

240

200

200

120

200

200

180

200

440

280

970

520

160

200

200

290

09/09/19



L1939733-08Lab ID:


MDL

19.

42.

23.

49.

34.

32.

21.

31.

39.

24.

20.

24.

23.

28.

20.

47.

37.

39.

38.

84.

19.

24.

21.

25.

38.

30.

24.

32.

67.

76.

82.

94.

97.

44.

30.

31.

32.

Sample Depth:

Serial_No:09091918:03

Page 102 of 222


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

J

Dilution Factor

ND

ND

ND

36

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

200

650

200

200

30

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

64

62

47

59

105

46

25-120

10-120

23-120

30-120

10-136

18-120


09/09/19



L1939733-08Lab ID:


Total TIC Compounds

Unknown

Unknown Alkane

Unknown Alkane

J

J

J

J

616

247

188

181

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1


MDL

39.

200

62.

20.

9.3

Sample Depth:

Serial_No:09091918:03

Page 103 of 222

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

Dilution Factor

29

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

740

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

140

170

100

160

170

170

170

170

170

170

170

100

170

170

210

190

170

500

140

160

170

160

140

170

170

170

170

170

09/09/19



L1939733-09Lab ID:




1,8270D09/06/19 01:54KR


95%Percent Solids:

MDL

18.

20.

20.

24.

17.

31.

30.

30.

46.

35.

30.

20.

19.

26.

30.

17.

25.

160

28.

23.

21.

26.

20.

27.

60.

44.

33.

59.

Sample Depth:

Serial_No:09091918:03

Page 104 of 222

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

Dilution Factor

ND

ND

320

340

430

230

340

ND

87

240

22

350

52

240

600

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

170

170

100

140

100

100

100

140

100

140

170

100

100

140

100

400

170

170

170

170

170

210

170

170

100

170

170

160

170

380

240

840

450

140

170

170

250

09/09/19



L1939733-09Lab ID:


MDL

16.

36.

20.

42.

29.

28.

18.

27.

34.

20.

17.

21.

20.

24.

17.

40.

32.

34.

33.

72.

16.

21.

18.

22.

33.

26.

20.

28.

57.

65.

71.

81.

84.

38.

26.

27.

27.

Sample Depth:

Serial_No:09091918:03

Page 105 of 222


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

J

Dilution Factor

ND

ND

ND

40

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

170

560

170

170

26

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

89

88

64

64

143

71

25-120

10-120

23-120

30-120

10-136

18-120

Acceptance Criteria

Q


09/09/19



L1939733-09Lab ID:


Total TIC Compounds

Unknown PAH

Unknown

Unknown

J

J

J

J

1350

187

548

612

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1


MDL

33.

180

53.

17.

8.0

Sample Depth:

Serial_No:09091918:03

Page 106 of 222

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

J

Dilution Factor

71

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

1600

ND

ND

ND

ND

ND

ND

ND

ND

72

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

150

190

120

170

190

190

190

190

190

190

190

120

190

190

230

210

190

550

150

170

190

170

150

190

190

190

190

190

09/09/19



L1939733-10Lab ID:




1,8270D09/06/19 05:24KR


86%Percent Solids:

MDL

20.

22.

22.

26.

19.

35.

33.

34.

51.

39.

33.

22.

21.

30.

33.

19.

28.

180

31.

25.

24.

29.

22.

30.

67.

49.

37.

66.

Sample Depth:

Serial_No:09091918:03

Page 107 of 222

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

Dilution Factor

ND

ND

890

910

1200

400

920

130

210

500

54

890

120

530

1500

ND

ND

ND

ND

ND

30

32

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

190

190

120

150

120

120

120

150

120

150

190

120

120

150

120

440

190

190

190

190

190

230

190

190

120

190

190

170

190

420

270

930

500

150

190

190

280

09/09/19



L1939733-10Lab ID:


MDL

18.

41.

22.

47.

32.

31.

20.

30.

38.

23.

19.

24.

22.

27.

19.

45.

35.

37.

36.

80.

18.

23.

20.

24.

37.

29.

23.

31.

64.

73.

79.

90.

93.

42.

29.

30.

30.

Sample Depth:

Serial_No:09091918:03

Page 108 of 222


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

J

Dilution Factor

ND

ND

ND

90

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

190

630

190

190

29

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

66

63

56

68

124

48

25-120

10-120

23-120

30-120

10-136

18-120


09/09/19



L1939733-10Lab ID:


Total TIC Compounds

Unknown

Unknown

Unknown PAH

Unknown

Unknown PAH

Unknown

Unknown PAH

Unknown PAH

Unknown

Unknown PAH

Unknown

J

J

J

J

J

J

J

J

J

J

J

J

3590

346

324

183

204

205

199

501

228

180

255

969

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1


MDL

37.

200

59.

19.

8.9

Sample Depth:

Serial_No:09091918:03

Page 109 of 222

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

150

190

120

170

190

190

190

190

190

190

190

120

190

190

230

210

190

550

150

170

190

170

150

190

190

190

190

190

09/09/19



L1939733-11Lab ID:




1,8270D09/06/19 01:02KR


85%Percent Solids:

MDL

20.

22.

22.

26.

19.

34.

33.

34.

51.

38.

33.

22.

20.

29.

33.

19.

28.

170

31.

25.

23.

28.

22.

30.

66.

48.

36.

65.

Sample Depth:

Serial_No:09091918:03

Page 110 of 222

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

190

190

120

150

120

120

120

150

120

150

190

120

120

150

120

440

190

190

190

190

190

230

190

190

120

190

190

170

190

410

270

920

500

150

190

190

280

09/09/19



L1939733-11Lab ID:


MDL

18.

40.

22.

47.

32.

31.

20.

30.

37.

22.

19.

23.

22.

27.

19.

44.

35.

37.

36.

79.

18.

23.

20.

24.

36.

29.

23.

31.

63.

72.

78.

89.

92.

42.

29.

30.

30.

Sample Depth:

Serial_No:09091918:03

Page 111 of 222


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane


ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

190

620

190

190

29

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

111

79

56

98

101

48

25-120

10-120

23-120

30-120

10-136

18-120


09/09/19



L1939733-11Lab ID:




MDL

37.

190

59.

19.

8.8

Sample Depth:

Serial_No:09091918:03

Page 112 of 222

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

140

170

100

160

170

170

170

170

170

170

170

100

170

170

210

190

170

490

140

160

170

160

140

170

170

170

170

170

09/09/19



L1939733-12Lab ID:




1,8270D09/06/19 00:10KR


96%Percent Solids:

MDL

18.

20.

19.

23.

17.

31.

30.

30.

46.

34.

30.

20.

18.

26.

29.

17.

25.

160

28.

22.

21.

26.

20.

27.

60.

43.

33.

59.

Sample Depth:

Serial_No:09091918:03

Page 113 of 222

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

170

170

100

140

100

100

100

140

100

140

170

100

100

140

100

390

170

170

170

170

170

210

170

170

100

170

170

160

170

370

240

830

450

140

170

170

250

09/09/19



L1939733-12Lab ID:


MDL

16.

36.

19.

42.

29.

28.

18.

27.

34.

20.

17.

21.

20.

24.

17.

40.

31.

33.

32.

71.

16.

21.

18.

21.

33.

26.

20.

28.

57.

65.

70.

80.

83.

38.

26.

27.

27.

Sample Depth:

Serial_No:09091918:03

Page 114 of 222


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane


ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

170

560

170

170

26

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

96

96

67

80

110

60

25-120

10-120

23-120

30-120

10-136

18-120


09/09/19



L1939733-12Lab ID:




MDL

33.

170

53.

17.

7.9

Sample Depth:

Serial_No:09091918:03

Page 115 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/05/19 22:261,8270DAnalytical Method:

Analytical Date:Extraction Method: EPA 3546Extraction Date: 09/04/19 04:27

09/09/19

Analyst: KR

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

130

160

98

150

160

160

160

160

160

160

160

98

160

160

200

180

160

470

130

150

160

150

130

160

160

160

160

160

160

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Semivolatile Organics by GC/MS - Westborough Lab for sample(s): 01-12 Batch: WG1279893-1

MDL

17.

19.

18.

22.

16.

29.

28.

28.

43.

33.

28.

19.

17.

25.

28.

16.

24.

150

26.

21.

20.

24.

18.

25.

56.

41.

31.

55.

15.

Serial_No:09091918:03

Page 116 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733



09/09/19

Analyst: KR

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

160

98

130

98

98

98

130

98

130

160

98

98

130

98

370

160

160

160

160

160

200

160

160

98

160

160

150

160

350

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

34.

18.

40.

27.

26.

17.

25.

32.

19.

16.

20.

19.

23.

16.

38.

30.

31.

31.

68.

15.

20.

17.

20.

31.

24.

19.

26.

54.

61.

Serial_No:09091918:03

Page 117 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733



09/09/19

Analyst: KR

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

230

780

420

130

160

160

230

160

530

160

160

24

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

93

90

63

79

100

75

25-120

10-120

23-120

30-120

10-136

18-120


Criteria



MDL

66.

76.

78.

36.

25.

25.

26.

31.

160

50.

16.

7.5

Serial_No:09091918:03

Page 118 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733



09/09/19

Analyst: KR

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

130

160

98

150

160

160

160

160

160

160

160

98

160

160

200

180

160

470

130

150

160

150

130

160

160

160

160

160

160

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Semivolatile Organics by GC/MS - Westborough Lab for sample(s): 05 Batch: WG1281682-1

MDL

17.

19.

18.

22.

16.

29.

28.

28.

43.

33.

28.

19.

17.

25.

28.

16.

24.

150

26.

21.

20.

24.

18.

25.

56.

41.

31.

55.

15.

Serial_No:09091918:03

Page 119 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733



09/09/19

Analyst: KR

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

160

98

130

98

98

98

130

98

130

160

98

98

130

98

370

160

160

160

160

160

200

160

160

98

160

160

150

160

350

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

34.

18.

40.

27.

26.

17.

25.

32.

19.

16.

20.

19.

23.

16.

38.

30.

31.

31.

68.

15.

20.

17.

20.

31.

24.

19.

26.

54.

61.

Serial_No:09091918:03

Page 120 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733



09/09/19

Analyst: KR

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

230

780

420

130

160

160

230

160

530

160

160

24

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

64

66

72

69

71

67

25-120

10-120

23-120

30-120

10-136

18-120


Criteria

Total TIC Compounds

Unknown

J

J

142

142

ug/kg

ug/kg


MDL

66.

76.

78.

36.

25.

25.

26.

31.

160

50.

16.

7.5

Serial_No:09091918:03

Page 121 of 222

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA

82

84

82

74

88

77

77

76

68

86

91

83

88

71

64

75

85

74

75

75

81

73

84

89

93

97

116

144

89

84

85

76

96

144

91

93

95

52

77

107

98

81

77

92

76

90

31-137

38-107

40-140

40-140

40-140

40-140

40-140

28-104

40-140

40-132

40-140

40-140

40-140

40-140

40-140

40-117

40-140

40-140

40-140

40-140

40-140

40-140

36-157

8

10

17

44

48

14

9

11

11

11

45

9

6

29

21

3

23

28

8

3

13

4

7

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Semivolatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-12 Batch: WG1279893-2 WG1279893-3


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual

Q

Q

Qual

Serial_No:09091918:03

Page 122 of 222




Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

77

76

75

78

106

83

84

78

102

104

115

88

86

83

73

86

78

71

70

80

90

73

91

76

83

66

90

84

92

135

85

95

93

104

94

137

94

105

94

89

92

88

67

146

86

148

32-121

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

35-142

37-127

40-140

47-134

1

9

13

14

23

10

47

9

7

11

10

7

46

12

36

9

13

26

23

18

47

16

48

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual

Q

Q

Qual

Serial_No:09091918:03

Page 123 of 222

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



Benzoic Acid

Benzyl Alcohol

Carbazole

67

72

85

84

96

78

92

90

84

92

89

82

62

72

82

68

85

84

93

92

22

80

81

75

82

93

95

113

84

108

100

128

100

98

91

72

83

92

87

131

89

97

146

29

85

92

26-129

41-125

40-140

40-140

40-117

14-144

30-130

26-103

25-102

30-130

30-130

30-130

11-114

4-130

10-130

17-109

26-90

30-130.

30-130

30-130

10-110

40-140

54-128

11

13

9

12

16

7

16

11

42

8

10

10

15

14

11

25

43

6

4

45

27

6

13

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual

Q

Q

Q

Qual

Serial_No:09091918:03

Page 124 of 222

1,4-Dioxane 50 70 40-140 33 50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

2-FluorophenolPhenol-d6Nitrobenzene-d52-Fluorobiphenyl2,4,6-Tribromophenol4-Terphenyl-d14

8383627310675

25-12010-12023-12030-12010-13618-120

1331306511611362

QQ


09/09/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09091918:03

Page 125 of 222

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA

68

62

66

58

71

61

59

59

62

87

83

74

70

70

48

62

66

41

59

65

64

75

72

69

67

68

59

74

64

63

62

63

91

88

77

71

72

50

62

68

43

61

65

69

75

76

31-137

38-107

40-140

40-140

40-140

40-140

40-140

28-104

40-140

40-132

40-140

40-140

40-140

40-140

40-140

40-117

40-140

40-140

40-140

40-140

40-140

40-140

36-157

1

8

3

2

4

5

7

5

2

4

6

4

1

3

4

0

3

5

3

0

8

0

5

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Semivolatile Organics by GC/MS - Westborough Lab Associated sample(s): 05 Batch: WG1281682-2 WG1281682-3


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual Qual

Serial_No:09091918:03

Page 126 of 222




Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

65

79

80

71

79

74

73

70

68

76

67

68

73

71

70

73

68

68

71

72

73

50

90

67

81

86

76

84

76

75

75

70

79

69

71

75

72

72

74

71

71

74

77

76

60

97

32-121

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

35-142

37-127

40-140

47-134

3

3

7

7

6

3

3

7

3

4

3

4

3

1

3

1

4

4

4

7

4

18

7

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual Qual

Serial_No:09091918:03

Page 127 of 222

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



Benzoic Acid

Benzyl Alcohol

Carbazole

70

82

73

70

68

67

80

80

69

77

80

90

102

68

80

84

67

69

72

78

31

78

71

74

84

74

74

72

70

82

84

68

76

81

88

98

55

82

89

67

70

72

81

24

79

75

26-129

41-125

40-140

40-140

40-117

14-144

30-130

26-103

25-102

30-130

30-130

30-130

11-114

4-130

10-130

17-109

26-90

30-130.

30-130

30-130

10-110

40-140

54-128

6

2

1

6

6

4

2

5

1

1

1

2

4

21

2

6

0

1

0

4

25

1

5

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual Qual

Serial_No:09091918:03

Page 128 of 222

1,4-Dioxane 48 43 40-140 11 50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


667075707668

25-12010-12023-12030-12010-13618-120

646669707570


09/09/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09091918:03

Page 129 of 222

PCBS

Serial_No:09091918:03

Page 130 of 222

FF

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Polychlorinated Biphenyls by GC - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

36.8

36.8

36.8

36.8

36.8

36.8

36.8

36.8

36.8

36.8

2,4,5,6-Tetrachloro-m-xylene

Decachlorobiphenyl


Decachlorobiphenyl

65

63

65

61

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B

Surrogate % Recovery Qualifier Column

09/09/19



L1939733-01Lab ID:



Cleanup Method:Analytical Method:Analytical Date:Analyst:

1,8082A09/06/19 05:57AD

EPA 3546

EPA 3665AExtraction Date: 09/04/19 02:51

Cleanup Date: 09/04/19Cleanup Method: EPA 3660BCleanup Date: 09/04/19

87%Percent Solids:

MDL

3.27

3.69

7.80

4.96

5.52

4.03

6.80

4.68

3.81

3.27

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 131 of 222

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

15.0

ND

ND

15.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

33.1

33.1

33.1

33.1

33.1

33.1

33.1

33.1

33.1

33.1


Decachlorobiphenyl


Decachlorobiphenyl

45

55

43

59

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/09/19



L1939733-02Lab ID:




1,8082A09/06/19 06:08AD

EPA 3546



96%Percent Solids:

MDL

2.94

3.32

7.02

4.46

4.96

3.62

6.12

4.20

3.43

2.94

A

A

A

A

A

A

B

A

A

B

Column

Sample Depth:

Serial_No:09091918:03

Page 132 of 222

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

13.4

ND

ND

13.4

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

35.5

35.5

35.5

35.5

35.5

35.5

35.5

35.5

35.5

35.5


Decachlorobiphenyl


Decachlorobiphenyl

56

64

54

69

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/09/19



L1939733-03Lab ID:




1,8082A09/06/19 06:20AD

EPA 3546



89%Percent Solids:

MDL

3.15

3.55

7.52

4.78

5.32

3.88

6.56

4.50

3.67

3.15

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 133 of 222

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

33.1

33.1

33.1

33.1

33.1

33.1

33.1

33.1

33.1

33.1


Decachlorobiphenyl


Decachlorobiphenyl

48

52

47

58

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/09/19



L1939733-04Lab ID:




1,8082A09/06/19 06:32AD

EPA 3546



96%Percent Solids:

MDL

2.94

3.31

7.01

4.46

4.96

3.62

6.11

4.20

3.42

2.94

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 134 of 222

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

37.2

37.2

37.2

37.2

37.2

37.2

37.2

37.2

37.2

37.2


Decachlorobiphenyl


Decachlorobiphenyl

55

49

54

51

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/09/19



L1939733-05Lab ID:




1,8082A09/06/19 06:44AD

EPA 3546



85%Percent Solids:

MDL

3.31

3.73

7.89

5.02

5.59

4.07

6.88

4.73

3.86

3.31

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 135 of 222

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

40.1

40.1

40.1

40.1

40.1

40.1

40.1

40.1

40.1

40.1


Decachlorobiphenyl


Decachlorobiphenyl

46

42

47

49

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/09/19



L1939733-06Lab ID:




1,8082A09/06/19 06:55AD

EPA 3546



78%Percent Solids:

MDL

3.56

4.01

8.49

5.40

6.01

4.38

7.40

5.09

4.15

3.56

A

A

A

A

A

A

B

A

A

B

Column

Sample Depth:

Serial_No:09091918:03

Page 136 of 222

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

35.1

35.1

35.1

35.1

35.1

35.1

35.1

35.1

35.1

35.1


Decachlorobiphenyl


Decachlorobiphenyl

51

50

51

54

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/09/19



L1939733-07Lab ID:




1,8082A09/06/19 07:07AD

EPA 3546



92%Percent Solids:

MDL

3.11

3.51

7.43

4.73

5.26

3.84

6.48

4.45

3.63

3.11

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 137 of 222

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

7.98

ND

ND

7.98

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

39.4

39.4

39.4

39.4

39.4

39.4

39.4

39.4

39.4

39.4


Decachlorobiphenyl


Decachlorobiphenyl

51

56

49

61

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/09/19



L1939733-08Lab ID:




1,8082A09/06/19 07:19AD

EPA 3546



81%Percent Solids:

MDL

3.50

3.95

8.35

5.31

5.91

4.31

7.28

5.00

4.08

3.50

A

A

A

A

A

A

B

A

A

B

Column

Sample Depth:

Serial_No:09091918:03

Page 138 of 222

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

34.0

34.0

34.0

34.0

34.0

34.0

34.0

34.0

34.0

34.0


Decachlorobiphenyl


Decachlorobiphenyl

58

59

56

63

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/09/19



L1939733-09Lab ID:




1,8082A09/06/19 07:31AD

EPA 3546



95%Percent Solids:

MDL

3.02

3.41

7.22

4.59

5.10

3.72

6.29

4.32

3.52

3.02

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 139 of 222

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

8.37

ND

ND

8.37

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

37.2

37.2

37.2

37.2

37.2

37.2

37.2

37.2

37.2

37.2


Decachlorobiphenyl


Decachlorobiphenyl

59

57

59

61

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/09/19



L1939733-10Lab ID:




1,8082A09/06/19 07:43AD

EPA 3546



86%Percent Solids:

MDL

3.31

3.73

7.90

5.02

5.59

4.07

6.88

4.73

3.86

3.31

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 140 of 222

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

38.7

38.7

38.7

38.7

38.7

38.7

38.7

38.7

38.7

38.7


Decachlorobiphenyl


Decachlorobiphenyl

55

46

57

52

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/09/19



L1939733-11Lab ID:




1,8082A09/06/19 07:54AD

EPA 3546



85%Percent Solids:

MDL

3.44

3.88

8.20

5.22

5.80

4.23

7.15

4.92

4.01

3.44

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 141 of 222

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

33.3

33.3

33.3

33.3

33.3

33.3

33.3

33.3

33.3

33.3


Decachlorobiphenyl


Decachlorobiphenyl

64

55

67

58

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/09/19



L1939733-12Lab ID:




1,8082A09/06/19 08:06AD

EPA 3546



96%Percent Solids:

MDL

2.96

3.34

7.06

4.49

4.99

3.64

6.15

4.23

3.45

2.96

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 142 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/04/19 12:101,8082AAnalytical Method:

Analytical Date:Extraction Method:

Cleanup Method:

EPA 3546


09/09/19

Cleanup Method: EPA 3660B

Analyst: AWS

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

32.7

32.7

32.7

32.7

32.7

32.7

32.7

32.7

32.7

32.7

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Polychlorinated Biphenyls by GC - Westborough Lab for sample(s): 01-12 Batch: WG1279871-1


Decachlorobiphenyl


Decachlorobiphenyl

73

60

73

62

30-150

30-150

30-150

30-150

Surrogate %Recovery Qualifier ColumnAcceptance

Criteria

Cleanup Date: 09/04/19


MDL

2.91

3.28

6.94

4.41

4.91

3.58

6.05

4.16

3.39

2.91

Column

A

A

A

A

A

A

A

A

A

A

A

A

B

B

Serial_No:09091918:03

Page 143 of 222

Aroclor 1016

Aroclor 1260

74

60

77

64

40-140

40-140

4

6

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Polychlorinated Biphenyls by GC - Westborough Lab Associated sample(s): 01-12 Batch: WG1279871-2 WG1279871-3


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

2,4,5,6-Tetrachloro-m-xyleneDecachlorobiphenyl2,4,5,6-Tetrachloro-m-xyleneDecachlorobiphenyl

79598172

30-15030-15030-15030-150

AABB

78647977

Surrogate Qual Column%Recovery Qual%RecoveryLCS LCSD

09/09/19

AcceptanceCriteria

Qual Qual Qual Column

A

A

Serial_No:09091918:03

Page 144 of 222

PESTICIDES

Serial_No:09091918:03

Page 145 of 222

FF

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

JIP

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.987

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Organochlorine Pesticides by GC - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.81

0.756

0.756

1.81

0.907

1.81

3.40

0.756

2.27

1.81

1.13

1.81

1.81

3.40

1.81

1.81

0.756

3.40

34.0

2.27

2.27

14.7

09/09/19



L1939733-01Lab ID:




1,8081B09/05/19 23:47BM

EPA 3546

EPA 3620BExtraction Date: 09/04/19 02:54

Cleanup Date: 09/05/19 87%Percent Solids:

MDL

0.355

0.338

0.215

0.688

0.407

0.639

1.02

0.310

0.794

0.467

0.567

0.420

0.647

1.46

0.429

0.606

0.360

1.06

9.53

0.632

0.599

6.01

A

A

A

A

A

A

A

A

A

A

A

B

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 146 of 222



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Decachlorobiphenyl


Decachlorobiphenyl

87

78

108

107

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/09/19



L1939733-01Lab ID:


MDL Column

Sample Depth:

Serial_No:09091918:03

Page 147 of 222

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

6.03

3.42

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.60

0.666

0.666

1.60

0.799

1.60

3.00

0.666

2.00

1.60

0.998

1.60

1.60

3.00

1.60

1.60

0.666

3.00

30.0

2.00

2.00

13.0

09/09/19



L1939733-02Lab ID:




1,8081B09/06/19 02:10BM

EPA 3546



MDL

0.313

0.298

0.189

0.606

0.358

0.562

0.899

0.273

0.699

0.411

0.499

0.369

0.570

1.28

0.377

0.534

0.317

0.932

8.39

0.556

0.527

5.29

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 148 of 222



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Decachlorobiphenyl


Decachlorobiphenyl

46

44

66

166

30-150

30-150

30-150

30-150

Acceptance Criteria

Q

B

B

A

A


09/09/19



L1939733-02Lab ID:


MDL Column

Sample Depth:

Serial_No:09091918:03

Page 149 of 222

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

JIP

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

1.56

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.77

0.738

0.738

1.77

0.886

1.77

3.32

0.738

2.22

1.77

1.11

1.77

1.77

3.32

1.77

1.77

0.738

3.32

33.2

2.22

2.22

14.4

09/09/19



L1939733-03Lab ID:




1,8081B09/06/19 02:23BM

EPA 3546



MDL

0.347

0.330

0.210

0.672

0.397

0.624

0.997

0.303

0.775

0.456

0.554

0.410

0.632

1.42

0.419

0.592

0.351

1.03

9.30

0.617

0.585

5.87

A

A

A

A

A

A

A

A

A

A

A

B

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 150 of 222



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Decachlorobiphenyl


Decachlorobiphenyl

69

43

88

121

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/09/19



L1939733-03Lab ID:


MDL Column

Sample Depth:

Serial_No:09091918:03

Page 151 of 222

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

IP

IP

IP

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

9.02

6.46

35.4

ND

ND

ND

ND

ND

6.45

9.80

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.59

0.663

0.663

1.59

0.796

1.59

2.98

0.663

1.99

1.59

0.994

1.59

1.59

2.98

1.59

1.59

0.663

2.98

29.8

1.99

1.99

12.9

09/09/19



L1939733-04Lab ID:




1,8081B09/06/19 00:00BM

EPA 3546



MDL

0.312

0.296

0.188

0.603

0.357

0.560

0.895

0.272

0.696

0.410

0.497

0.368

0.568

1.28

0.376

0.532

0.316

0.928

8.35

0.554

0.525

5.27

A

A

A

A

A

A

A

A

A

A

A

B

B

A

A

A

A

A

A

B

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 152 of 222



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Decachlorobiphenyl


Decachlorobiphenyl

74

64

97

140

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/09/19



L1939733-04Lab ID:


MDL Column

Sample Depth:

Serial_No:09091918:03

Page 153 of 222

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.82

0.758

0.758

1.82

0.910

1.82

3.41

0.758

2.27

1.82

1.14

1.82

1.82

3.41

1.82

1.82

0.758

3.41

34.1

2.27

2.27

14.8

09/09/19



L1939733-05Lab ID:




1,8081B09/05/19 22:55BM

EPA 3546



MDL

0.356

0.339

0.215

0.690

0.408

0.641

1.02

0.311

0.796

0.469

0.569

0.421

0.649

1.46

0.430

0.608

0.361

1.06

9.55

0.634

0.600

6.03

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 154 of 222



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Decachlorobiphenyl


Decachlorobiphenyl

96

83

81

79

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/09/19



L1939733-05Lab ID:


MDL Column

Sample Depth:

Serial_No:09091918:03

Page 155 of 222

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

IP

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

25.9

2.57

7.11

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.95

0.812

0.812

1.95

0.974

1.95

3.65

0.812

2.44

1.95

1.22

1.95

1.95

3.65

1.95

1.95

0.812

3.65

36.5

2.44

2.44

15.8

09/09/19



L1939733-06Lab ID:




1,8081B09/06/19 00:13BM

EPA 3546



MDL

0.382

0.363

0.230

0.739

0.437

0.686

1.10

0.333

0.852

0.502

0.609

0.451

0.695

1.57

0.460

0.651

0.386

1.14

10.2

0.679

0.643

6.45

A

A

A

A

A

A

A

A

A

A

A

A

B

B

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 156 of 222



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Decachlorobiphenyl


Decachlorobiphenyl

90

69

166

141

30-150

30-150

30-150

30-150

Acceptance Criteria

Q

B

B

A

A


09/09/19



L1939733-06Lab ID:


MDL Column

Sample Depth:

Serial_No:09091918:03

Page 157 of 222

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

JIP

J

IP

IP

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

1.42

ND

2.69

ND

ND

ND

ND

ND

4.08

3.79

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.68

0.699

0.699

1.68

0.839

1.68

3.14

0.699

2.10

1.68

1.05

1.68

1.68

3.14

1.68

1.68

0.699

3.14

31.4

2.10

2.10

13.6

09/09/19



L1939733-07Lab ID:




1,8081B09/06/19 02:36BM

EPA 3546



MDL

0.328

0.312

0.198

0.636

0.376

0.591

0.944

0.286

0.734

0.432

0.524

0.388

0.598

1.35

0.396

0.560

0.333

0.978

8.81

0.584

0.554

5.56

A

A

A

A

A

A

A

A

A

A

A

B

A

A

A

A

A

A

A

B

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 158 of 222



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Decachlorobiphenyl


Decachlorobiphenyl

71

52

85

127

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/09/19



L1939733-07Lab ID:


MDL Column

Sample Depth:

Serial_No:09091918:03

Page 159 of 222

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

IP

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.87

0.781

0.781

1.87

0.937

1.87

3.51

0.781

2.34

1.87

1.17

1.87

1.87

3.51

1.87

1.87

0.781

3.51

35.1

2.34

2.34

15.2

09/09/19



L1939733-08Lab ID:




1,8081B09/06/19 00:26BM

EPA 3546



MDL

0.367

0.349

0.222

0.710

0.420

0.660

1.05

0.320

0.820

0.482

0.586

0.433

0.668

1.51

0.443

0.626

0.372

1.09

9.84

0.653

0.618

6.21

A

A

A

A

A

A

A

A

A

A

A

B

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 160 of 222



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Decachlorobiphenyl


Decachlorobiphenyl

84

60

99

123

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/09/19



L1939733-08Lab ID:


MDL Column

Sample Depth:

Serial_No:09091918:03

Page 161 of 222

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

IP

JIP

JIP

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

3.80

ND

7.18

ND

ND

ND

ND

ND

0.768

0.892

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.58

0.659

0.659

1.58

0.791

1.58

2.97

0.659

1.98

1.58

0.989

1.58

1.58

2.97

1.58

1.58

0.659

2.97

29.7

1.98

1.98

12.8

09/09/19



L1939733-09Lab ID:




1,8081B09/05/19 23:08BM

EPA 3546



MDL

0.310

0.295

0.187

0.600

0.355

0.557

0.890

0.270

0.692

0.407

0.494

0.366

0.564

1.27

0.374

0.529

0.314

0.923

8.31

0.551

0.522

5.24

A

A

A

A

A

A

A

A

A

A

A

B

A

A

A

A

A

A

A

B

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 162 of 222



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Decachlorobiphenyl


Decachlorobiphenyl

94

79

106

97

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/09/19



L1939733-09Lab ID:


MDL Column

Sample Depth:

Serial_No:09091918:03

Page 163 of 222

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

IP

JIP

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

2.20

1.80

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.81

0.756

0.756

1.81

0.907

1.81

3.40

0.756

2.27

1.81

1.13

1.81

1.81

3.40

1.81

1.81

0.756

3.40

34.0

2.27

2.27

14.7

09/09/19



L1939733-10Lab ID:




1,8081B09/06/19 00:39BM

EPA 3546



MDL

0.355

0.338

0.214

0.688

0.406

0.638

1.02

0.310

0.793

0.467

0.567

0.419

0.647

1.46

0.428

0.606

0.360

1.06

9.52

0.632

0.598

6.01

A

A

A

A

A

A

A

A

A

A

A

B

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 164 of 222



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Decachlorobiphenyl


Decachlorobiphenyl

90

91

103

93

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/09/19



L1939733-10Lab ID:


MDL Column

Sample Depth:

Serial_No:09091918:03

Page 165 of 222

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.79

0.748

0.748

1.79

0.897

1.79

3.36

0.748

2.24

1.79

1.12

1.79

1.79

3.36

1.79

1.79

0.748

3.36

33.6

2.24

2.24

14.6

09/09/19



L1939733-11Lab ID:




1,8081B09/05/19 23:21BM

EPA 3546



MDL

0.351

0.334

0.212

0.680

0.402

0.632

1.01

0.306

0.785

0.462

0.561

0.415

0.640

1.44

0.424

0.600

0.356

1.05

9.42

0.625

0.592

5.94

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 166 of 222



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Decachlorobiphenyl


Decachlorobiphenyl

91

73

102

92

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/09/19



L1939733-11Lab ID:


MDL Column

Sample Depth:

Serial_No:09091918:03

Page 167 of 222

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

1.56

0.651

0.651

1.56

0.781

1.56

2.93

0.651

1.95

1.56

0.976

1.56

1.56

2.93

1.56

1.56

0.651

2.93

29.3

1.95

1.95

12.7

09/09/19



L1939733-12Lab ID:




1,8081B09/05/19 23:34BM

EPA 3546



MDL

0.306

0.291

0.185

0.592

0.350

0.550

0.879

0.267

0.683

0.402

0.488

0.361

0.557

1.26

0.369

0.522

0.310

0.911

8.20

0.544

0.516

5.17

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09091918:03

Page 168 of 222



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


Decachlorobiphenyl


Decachlorobiphenyl

94

79

105

102

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/09/19



L1939733-12Lab ID:


MDL Column

Sample Depth:

Serial_No:09091918:03

Page 169 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/06/19 01:421,8081BAnalytical Method:


Cleanup Method:

EPA 3546


09/09/19

Analyst: BM

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.56

0.651

0.651

1.56

0.781

1.56

2.93

0.651

1.95

1.56

0.976

1.56

1.56

2.93

1.56

1.56

0.651

2.93

29.3

1.95

1.95

12.7

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Organochlorine Pesticides by GC - Westborough Lab for sample(s): 01-12 Batch: WG1279874-1


MDL

0.306

0.291

0.185

0.592

0.350

0.550

0.878

0.267

0.683

0.402

0.488

0.361

0.557

1.26

0.369

0.522

0.310

0.911

8.20

0.544

0.515

5.17

Column

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:09091918:03

Page 170 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733



Cleanup Method:

EPA 3546


09/09/19

Analyst: BM




Decachlorobiphenyl


Decachlorobiphenyl

111

176

92

94

Q

30-150

30-150

30-150

30-150


Criteria


MDL Column

B

B

A

A

Serial_No:09091918:03

Page 171 of 222

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

cis-Chlordane

trans-Chlordane

98

98

97

94

84

87

95

102

69

99

100

88

104

107

87

97

77

97

87

93

102

102

102

100

85

88

102

106

88

108

104

93

106

111

93

103

90

98

91

97

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

4

4

5

6

1

1

7

4

24

9

4

6

2

4

7

6

16

1

4

4

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Organochlorine Pesticides by GC - Westborough Lab Associated sample(s): 01-12 Batch: WG1279874-2 WG1279874-3


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19


A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:09091918:03

Page 172 of 222

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733


1101349180

30-15030-15030-15030-150

BBAA

1091349360


09/09/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09091918:03

Page 173 of 222

METALS

Serial_No:09091918:03

Page 174 of 222

FF

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

SAMPLE RESULTS


Matrix: Soil


L1939733-01Lab ID:


Parameter ResultDilution FactorQualifier Units RL

DateAnalyzed

AnalyticalMethod Analyst

Date Prepared

Total Metals - Mansfield Lab

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

J

J

9350

1.11

3.47

48.7

0.358

0.447

1030

15.7

6.32

45.9

15000

25.1

1210

182

ND

7.81

331

0.232

ND

154

ND

24.0

118

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

8.94

4.47

0.894

0.894

0.447

0.894

8.94

0.894

1.79

0.894

4.47

4.47

8.94

0.894

0.073

2.24

224

1.79

0.894

179

1.79

0.894

4.47

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 18:42

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

09/05/19 19:06

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

GD

MC

MC

MC

MC

MC

MC

MC

MC

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/05/19 09:30

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 87%

MDL

2.41

0.340

0.186

0.156

0.030

0.088

3.13

0.086

0.148

0.231

0.807

0.240

1.38

0.142

0.048

0.216

12.9

0.231

0.253

2.82

0.282

0.182

0.262

Sample Depth:

Serial_No:09091918:03

Page 175 of 222

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

SAMPLE RESULTS


Matrix: Soil


L1939733-02Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

3380

1.12

2.40

289

0.105

0.631

48800

11.2

3.23

22.2

7350

405

18600

159

0.228

5.88

276

ND

ND

238

ND

20.0

171

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

20

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

8.09

4.05

0.809

0.809

0.405

0.809

80.9

0.809

1.62

0.809

4.05

4.05

8.09

0.809

0.065

2.02

202

1.62

0.809

162

1.62

0.809

4.05

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

09/06/19 01:57

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

09/05/19 19:05

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

09/05/19 19:52

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

GD

MC

MC

MC

MC

MC

MC

MC

MC

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/05/19 09:30

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 96%

MDL

2.18

0.308

0.168

0.141

0.027

0.079

28.3

0.078

0.134

0.209

0.731

0.217

1.25

0.129

0.043

0.196

11.6

0.209

0.229

2.55

0.255

0.164

0.237

Sample Depth:

Serial_No:09091918:03

Page 176 of 222

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

SAMPLE RESULTS


Matrix: Soil


L1939733-03Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

5020

0.811

3.02

73.8

0.239

0.384

1860

11.3

4.70

17.6

9730

185

1300

196

0.253

8.86

468

ND

ND

308

ND

19.0

157

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

8.54

4.27

0.854

0.854

0.427

0.854

8.54

0.854

1.71

0.854

4.27

4.27

8.54

0.854

0.070

2.14

214

1.71

0.854

171

1.71

0.854

4.27

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:15

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

09/05/19 19:56

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

GD

MC

MC

MC

MC

MC

MC

MC

MC

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/05/19 09:30

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 89%

MDL

2.31

0.324

0.178

0.149

0.028

0.084

2.99

0.082

0.142

0.220

0.771

0.229

1.32

0.136

0.046

0.207

12.3

0.220

0.242

2.69

0.269

0.173

0.250

Sample Depth:

Serial_No:09091918:03

Page 177 of 222

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

SAMPLE RESULTS


Matrix: Soil


L1939733-04Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

5530

1.26

3.94

109

0.276

0.528

2610

13.3

4.72

22.5

11100

386

1580

146

0.343

8.64

256

ND

ND

239

ND

21.0

190

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

7.87

3.94

0.787

0.787

0.394

0.787

7.87

0.787

1.57

0.787

3.94

3.94

7.87

0.787

0.066

1.97

197

1.57

0.787

157

1.57

0.787

3.94

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 19:18

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

09/05/19 20:01

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

GD

MC

MC

MC

MC

MC

MC

MC

MC

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/05/19 09:30

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 96%

MDL

2.13

0.299

0.164

0.137

0.026

0.077

2.76

0.076

0.131

0.203

0.711

0.211

1.21

0.125

0.043

0.190

11.3

0.203

0.223

2.48

0.248

0.160

0.231

Sample Depth:

Serial_No:09091918:03

Page 178 of 222

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

SAMPLE RESULTS


Matrix: Soil


L1939733-05Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

7820

1.64

4.73

212

0.453

0.408

2580

13.4

5.59

22.0

12700

522

1130

918

0.761

9.17

502

0.417

ND

843

ND

20.4

116

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

9.07

4.53

0.907

0.907

0.453

0.907

9.07

0.907

1.81

0.907

4.53

4.53

9.07

0.907

0.075

2.27

227

1.81

0.907

181

1.81

0.907

4.53

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 19:21

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

09/05/19 20:05

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

GD

MC

MC

MC

MC

MC

MC

MC

MC

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/05/19 09:30

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 85%

MDL

2.45

0.344

0.188

0.158

0.030

0.089

3.17

0.087

0.150

0.234

0.819

0.243

1.40

0.144

0.049

0.219

13.0

0.234

0.256

2.86

0.286

0.184

0.266

Sample Depth:

Serial_No:09091918:03

Page 179 of 222

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

SAMPLE RESULTS


Matrix: Soil


L1939733-06Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

7560

3.89

9.15

132

0.371

0.782

4980

16.7

5.68

40.2

18000

279

1520

249

0.848

10.8

381

ND

ND

538

ND

23.3

215

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

9.77

4.88

0.977

0.977

0.488

0.977

9.77

0.977

1.95

0.977

4.88

4.88

9.77

0.977

0.081

2.44

244

1.95

0.977

195

1.95

0.977

4.88

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 19:25

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

09/05/19 20:09

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

GD

MC

MC

MC

MC

MC

MC

MC

MC

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/05/19 09:30

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 78%

MDL

2.64

0.371

0.203

0.170

0.032

0.096

3.42

0.094

0.162

0.252

0.882

0.262

1.50

0.155

0.053

0.236

14.1

0.252

0.276

3.08

0.308

0.198

0.286

Sample Depth:

Serial_No:09091918:03

Page 180 of 222

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

SAMPLE RESULTS


Matrix: Soil


L1939733-07Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

5230

0.633

1.98

54.2

0.167

0.408

11000

8.31

6.00

51.9

13300

134

2010

164

0.171

6.84

715

ND

ND

353

ND

24.4

62.4

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

8.33

4.17

0.833

0.833

0.417

0.833

8.33

0.833

1.67

0.833

4.17

4.17

8.33

0.833

0.068

2.08

208

1.67

0.833

167

1.67

0.833

4.17

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 19:28

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

09/05/19 20:13

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

GD

MC

MC

MC

MC

MC

MC

MC

MC

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/05/19 09:30

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 92%

MDL

2.25

0.317

0.173

0.145

0.028

0.082

2.92

0.080

0.138

0.215

0.752

0.223

1.28

0.132

0.044

0.202

12.0

0.215

0.236

2.62

0.262

0.169

0.244

Sample Depth:

Serial_No:09091918:03

Page 181 of 222

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

SAMPLE RESULTS


Matrix: Soil


L1939733-08Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

J

J

3380

4.00

6.12

120

0.137

0.911

117000

8.93

3.84

45.8

25100

329

38600

237

2.67

7.79

322

0.637

ND

173

ND

15.3

207

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

20

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

9.80

4.90

0.980

0.980

0.490

0.980

98.0

0.980

1.96

0.980

4.90

4.90

9.80

0.980

0.078

2.45

245

1.96

0.980

196

1.96

0.980

4.90

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

09/06/19 02:01

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

09/05/19 19:31

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

09/05/19 20:38

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

GD

MC

MC

MC

MC

MC

MC

MC

MC

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/05/19 09:30

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 81%

MDL

2.64

0.372

0.204

0.170

0.032

0.096

34.3

0.094

0.163

0.253

0.885

0.262

1.51

0.156

0.051

0.237

14.1

0.253

0.277

3.09

0.309

0.199

0.287

Sample Depth:

Serial_No:09091918:03

Page 182 of 222

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

SAMPLE RESULTS


Matrix: Soil


L1939733-09Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

J

1800

0.428

2.06

44.0

ND

0.230

79800

6.74

1.93

9.63

5250

107

28800

165

ND

4.09

198

0.288

ND

220

ND

8.45

64.2

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

20

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

8.23

4.11

0.823

0.823

0.411

0.823

82.3

0.823

1.64

0.823

4.11

4.11

8.23

0.823

0.067

2.06

206

1.64

0.823

164

1.64

0.823

4.11

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

09/06/19 02:05

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

09/05/19 19:35

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

09/05/19 20:43

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

GD

MC

MC

MC

MC

MC

MC

MC

MC

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/05/19 09:30

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 95%

MDL

2.22

0.313

0.171

0.143

0.027

0.081

28.8

0.079

0.136

0.212

0.743

0.220

1.27

0.131

0.044

0.199

11.8

0.212

0.233

2.59

0.259

0.167

0.241

Sample Depth:

Serial_No:09091918:03

Page 183 of 222

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

SAMPLE RESULTS


Matrix: Soil


L1939733-10Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

J

5740

1.90

5.58

97.6

0.344

0.762

2600

14.4

4.24

29.7

12300

268

1470

164

2.84

10.0

474

0.576

ND

337

ND

21.4

160

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

9.29

4.64

0.929

0.929

0.464

0.929

9.29

0.929

1.86

0.929

4.64

4.64

9.29

0.929

0.074

2.32

232

1.86

0.929

186

1.86

0.929

4.64

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 19:38

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

09/05/19 20:47

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

GD

MC

MC

MC

MC

MC

MC

MC

MC

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/05/19 09:30

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 86%

MDL

2.51

0.353

0.193

0.162

0.031

0.091

3.25

0.089

0.154

0.240

0.839

0.249

1.43

0.148

0.048

0.225

13.4

0.240

0.263

2.93

0.293

0.188

0.272

Sample Depth:

Serial_No:09091918:03

Page 184 of 222

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

SAMPLE RESULTS


Matrix: Soil


L1939733-11Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

13700

1.56

4.85

74.2

0.531

0.430

933

20.7

7.44

7.85

18800

15.3

1780

274

ND

10.0

469

ND

ND

650

ND

32.6

28.4

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

9.15

4.57

0.915

0.915

0.457

0.915

9.15

0.915

1.83

0.915

4.57

4.57

9.15

0.915

0.074

2.29

229

1.83

0.915

183

1.83

0.915

4.57

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 19:41

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

09/05/19 20:51

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

GD

MC

MC

MC

MC

MC

MC

MC

MC

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/05/19 09:30

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 85%

MDL

2.47

0.348

0.190

0.159

0.030

0.090

3.20

0.088

0.152

0.236

0.826

0.245

1.41

0.145

0.048

0.221

13.2

0.236

0.259

2.88

0.288

0.186

0.268

Sample Depth:

Serial_No:09091918:03

Page 185 of 222

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

SAMPLE RESULTS


Matrix: Soil


L1939733-12Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

J

J

2620

ND

0.536

17.7

0.112

0.152

372

6.03

2.89

7.24

6010

2.14

864

202

ND

6.36

274

ND

ND

71.1

ND

8.13

10.1

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

8.00

4.00

0.800

0.800

0.400

0.800

8.00

0.800

1.60

0.800

4.00

4.00

8.00

0.800

0.065

2.00

200

1.60

0.800

160

1.60

0.800

4.00

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 19:45

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

09/05/19 20:55

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

GD

MC

MC

MC

MC

MC

MC

MC

MC

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/05/19 09:30

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 96%

MDL

2.16

0.304

0.166

0.139

0.026

0.078

2.80

0.077

0.133

0.206

0.723

0.214

1.23

0.127

0.043

0.194

11.5

0.206

0.226

2.52

0.252

0.162

0.234

Sample Depth:

Serial_No:09091918:03

Page 186 of 222

FF

Parameter

Parameter

Result

Result

Dilution Factor

Dilution Factor

Qualifier

Qualifier

Units

Units

RL

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

DateAnalyzed

DateAnalyzed

AnalyticalMethod

AnalyticalMethod

Analyst

Analyst

Date Prepared

Date Prepared

09/09/19

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

Mercury, Total

J

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

7.19

ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

4.00

2.00

0.400

0.400

0.200

0.400

4.00

0.400

0.800

0.400

2.00

2.00

4.00

0.400

1.00

100

0.800

0.400

80.0

0.800

0.400

2.00

0.083

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:49

09/05/19 18:35

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

MC

GD

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/04/19 22:22

09/05/19 09:30

Total Metals - Mansfield Lab for sample(s): 01-12 Batch: WG1280281-1


EPA 3050BDigestion Method:

Prep Information

MDL

MDL

1.08

0.152

0.083

0.070

0.013

0.039

1.40

0.038

0.066

0.103

0.361

0.107

0.616

0.064

0.097

5.76

0.103

0.113

1.26

0.126

0.081

0.117

0.054

Serial_No:09091918:03

Page 187 of 222


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19


Prep Information

Serial_No:09091918:03

Page 188 of 222

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

55

158

100

84

92

102

77

84

95

90

70

92

72

78

98

69

98

84

87

97

84

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

51-149

19-249

70-130

75-125

75-125

75-125

73-127

70-130

75-125

75-125

38-162

71-128

63-137

76-124

70-131

60-140

63-137

69-131

37-162

68-132

65-135

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPD RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 01-12 Batch: WG1280281-2 SRM Lot Number: D105-540


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual Qual

Serial_No:09091918:03

Page 189 of 222

Zinc, Total

Mercury, Total

96

103

-

-

70-130

60-141

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery





Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Serial_No:09091918:03

Page 190 of 222

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

9350

1.11J

3.47

48.7

0.358J

0.447J

1030

15.7

6.32

45.9

15000

25.1

1210

182

7.81

331

0.232J

ND

154J

ND

24.0

12200

42.4

14.8

220

4.48

4.94

1820

34.5

48.4

46.8

17700

59.9

2200

394

49.9

1180

10.2

23.9

940

9.35

70.0

1620

96

107

97

102

110

90

107

96

4

3060

77

112

481

96

96

96

90

107

88

104

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterNative Sample

MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 01-12 QC Batch ID: WG1280281-3 QC Sample: L1939733-01 Client ID: SESI-SB-9 (1-2)

176

44

10.6

176

4.4

4.49

881

17.6

44

22

88.1

44.9

881

44

44

881

10.6

26.4

881

10.6

44

MS Added

Matrix Spike AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual

Q

Q

Q

Q

Qual Qual

Serial_No:09091918:03

Page 191 of 222

Zinc, Total

Mercury, Total

118

ND

164

0.187

104

127

-

-

-

-

75-125

80-120

-

-

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits



44

0.147

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Q

Serial_No:09091918:03

Page 192 of 222

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

9350

1.11J

3.47

48.7

0.358J

0.447J

1030

15.7

6.32

45.9

15000

25.1

1210

182

7.81

331

0.232J

ND

154J

11800

1.28J

3.87

63.5

0.414J

0.517J

2720

19.2

7.28

28.3

19000

19.2

1510

439

8.44

396

ND

ND

179

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

23

NC

11

26

NC

NC

90

20

14

47

24

27

22

83

8

18

NC

NC

NC

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

Units RPDParameter Native Sample Duplicate Sample RPD Limits



10831

Project Name:

Project Number:

L1939733Lab Number:

Report Date:

Lab Duplicate AnalysisBatch Quality Control

09/09/19

Qual

Q

Q

Q

Q

Q

Q

Q

Q

Serial_No:09091918:03

Page 193 of 222

Thallium, Total

Vanadium, Total

Zinc, Total

Mercury, Total

ND

24.0

118

ND

ND

29.6

119

ND

mg/kg

mg/kg

mg/kg

mg/kg

NC

21

1

NC

20

20

20

20





10831

Project Name:

Project Number:

L1939733Lab Number:

Report Date:


09/09/19

Q

Serial_No:09091918:03

Page 194 of 222

INORGANICS&

MISCELLANEOUS

Serial_No:09091918:03

Page 195 of 222

FF


Parameter ResultDilution Factor

Matrix: Soil


L1939733-01Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

Field Prep:

DateAnalyzed


Not Specified

General Chemistry - Westborough LabSolids, Total

Cyanide, Total

86.9

ND

%

mg/kg

1

1

0.100

1.1

08/31/19 12:46

09/03/19 12:35

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 22:55

09/09/19

MDL

NA

0.24

Sample Depth:

Serial_No:09091918:03

Page 196 of 222

FF



Matrix: Soil


L1939733-02Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

96.3

ND

%

mg/kg

1

1

0.100

0.95

08/31/19 12:46

09/03/19 12:36

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 22:55

09/09/19

MDL

NA

0.20

Sample Depth:

Serial_No:09091918:03

Page 197 of 222

FF



Matrix: Soil


L1939733-03Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total J

89.1

0.24

%

mg/kg

1

1

0.100

1.0

08/31/19 12:46

09/03/19 12:39

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 22:55

09/09/19

MDL

NA

0.22

Sample Depth:

Serial_No:09091918:03

Page 198 of 222

FF



Matrix: Soil


L1939733-04Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

95.7

ND

%

mg/kg

1

1

0.100

0.96

08/31/19 12:46

09/03/19 12:40

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 22:55

09/09/19

MDL

NA

0.20

Sample Depth:

Serial_No:09091918:03

Page 199 of 222

FF



Matrix: Soil


L1939733-05Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total J

85.3

0.41

%

mg/kg

1

1

0.100

1.1

08/31/19 12:46

09/03/19 12:41

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 22:55

09/09/19

MDL

NA

0.24

Sample Depth:

Serial_No:09091918:03

Page 200 of 222

FF



Matrix: Soil


L1939733-06Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

78.3

ND

%

mg/kg

1

1

0.100

1.2

08/31/19 12:46

09/04/19 12:17

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 16:05

09/09/19

MDL

NA

0.25

Sample Depth:

Serial_No:09091918:03

Page 201 of 222

FF



Matrix: Soil


L1939733-07Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

92.3

ND

%

mg/kg

1

1

0.100

1.0

08/31/19 12:46

09/04/19 12:18

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 16:05

09/09/19

MDL

NA

0.22

Sample Depth:

Serial_No:09091918:03

Page 202 of 222

FF



Matrix: Soil


L1939733-08Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

81.0

ND

%

mg/kg

1

1

0.100

1.2

08/31/19 12:46

09/04/19 12:19

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 16:05

09/09/19

MDL

NA

0.25

Sample Depth:

Serial_No:09091918:03

Page 203 of 222

FF



Matrix: Soil


L1939733-09Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

95.4

ND

%

mg/kg

1

1

0.100

0.96

08/31/19 12:46

09/04/19 12:20

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 16:05

09/09/19

MDL

NA

0.20

Sample Depth:

Serial_No:09091918:03

Page 204 of 222

FF



Matrix: Soil


L1939733-10Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

85.5

ND

%

mg/kg

1

1

0.100

1.1

08/31/19 12:46

09/04/19 12:23

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 16:05

09/09/19

MDL

NA

0.24

Sample Depth:

Serial_No:09091918:03

Page 205 of 222

FF



Matrix: Soil


L1939733-11Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

84.6

ND

%

mg/kg

1

1

0.100

1.1

08/31/19 12:46

09/04/19 12:24

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 16:05

09/09/19

MDL

NA

0.23

Sample Depth:

Serial_No:09091918:03

Page 206 of 222

FF



Matrix: Soil


L1939733-12Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

96.2

ND

%

mg/kg

1

1

0.100

1.0

08/31/19 12:46

09/04/19 12:25

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 16:05

09/09/19

MDL

NA

0.22

Sample Depth:

Serial_No:09091918:03

Page 207 of 222

FF



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

DateAnalyzed


Date Prepared

09/09/19

Cyanide, Total

Cyanide, Total

ND

ND

mg/kg

mg/kg

1

1

0.84

0.94

09/03/19 12:19

09/04/19 12:02

1,9010C/9012B

1,9010C/9012B

ML

ML

09/02/19 22:55

09/02/19 16:05

General Chemistry - Westborough Lab for sample(s): 01-05 Batch: WG1279408-1


MDL

0.18

0.20

Serial_No:09091918:03

Page 208 of 222

Cyanide, Total

Cyanide, Total

64

77

69

56

80-120

80-120

35

48

35

35

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


General Chemistry - Westborough Lab Associated sample(s): 01-05 Batch: WG1279408-2 WG1279408-3



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual

Q

Q

Q

Q

Qual

Q

Serial_No:09091918:03

Page 209 of 222

Cyanide, Total

Cyanide, Total

1.2

0.39J

11

11

88

97

12

11

96

98

75-125

75-125

9

0

35

35


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

General Chemistry - Westborough Lab Associated sample(s): 01-05 QC Batch ID: WG1279408-4 WG1279408-5 QC Sample: L1939221-07 Client ID: MS Sample


11

11

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939733

09/09/19

Qual Qual Qual

Serial_No:09091918:03

Page 210 of 222

*Values in parentheses indicate holding time in days

L1939733-01A

L1939733-01B

L1939733-01C

L1939733-01D

L1939733-01E

L1939733-01F

L1939733-01X

L1939733-01Y

L1939733-01Z

L1939733-02A

L1939733-02B

L1939733-02C

L1939733-02D

L1939733-02E

L1939733-02F

L1939733-02X

L1939733-02Y

5 gram Encore Sampler



Plastic 2oz unpreserved for TS

Metals Only-Glass 60mL/2oz unpreserved

Glass 250ml/8oz unpreserved

Vial MeOH preserved split

Vial Water preserved split










A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

A AbsentCooler Custody SealCooler Information


10831

NYTCL-8260H(14),NYTCL-8260HLW(14)



TS(7)

BE-TI(180),AS-TI(180),BA-TI(180),AG-TI(180),AL-TI(180),CR-TI(180),NI-TI(180),TL-TI(180),CU-TI(180),PB-TI(180),SB-TI(180),SE-TI(180),ZN-TI(180),CO-TI(180),V-TI(180),FE-TI(180),HG-T(28),MG-TI(180),MN-TI(180),CA-TI(180),CD-TI(180),K-TI(180),NA-TI(180)

NYTCL-8270(14),TCN-9010(14),NYTCL-8081(14),NYTCL-8082(14)




NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)



NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

Project Name:

Project Number:

L1939733Lab Number:

Report Date:

Sample Receipt and Container Information

Container ID Container Type CoolerTempdeg C Pres Seal

Container Information

Analysis(*)

09/09/19

Were project specific reporting limits specified? YES

31-AUG-19 12:38

31-AUG-19 12:38

31-AUG-19 12:38

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09091918:03

Page 211 of 222


L1939733-02Z

L1939733-03A

L1939733-03B

L1939733-03C

L1939733-03D

L1939733-03E

L1939733-03F

L1939733-03X

L1939733-03Y

L1939733-03Z

L1939733-04A

L1939733-04B

L1939733-04C

L1939733-04D

L1939733-04E

L1939733-04F

L1939733-04X

L1939733-04Y

L1939733-04Z

L1939733-05A

L1939733-05B

L1939733-05C

L1939733-05D
























A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent


10831

NYTCL-8260HLW(14)




TS(7)









TS(7)






NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

Project Name:

Project Number:

L1939733Lab Number:

Report Date:



Analysis(*)

09/09/19

31-AUG-19 12:38

31-AUG-19 12:38

31-AUG-19 12:38

31-AUG-19 12:38

31-AUG-19 12:38

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09091918:03

Page 212 of 222


L1939733-05E

L1939733-05F

L1939733-05X

L1939733-05Y

L1939733-05Z

L1939733-06A

L1939733-06B

L1939733-06C

L1939733-06D

L1939733-06E

L1939733-06F

L1939733-06X

L1939733-06Y

L1939733-06Z

L1939733-07A

L1939733-07B

L1939733-07C

L1939733-07D

L1939733-07E

L1939733-07F





















A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent


10831



NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)




TS(7)






NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)



Project Name:

Project Number:

L1939733Lab Number:

Report Date:



Analysis(*)

09/09/19

31-AUG-19 12:38

31-AUG-19 12:38

31-AUG-19 12:38

31-AUG-19 12:38

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09091918:03

Page 213 of 222


L1939733-07X

L1939733-07Y

L1939733-07Z

L1939733-08A

L1939733-08B

L1939733-08C

L1939733-08D

L1939733-08E

L1939733-08F

L1939733-08X

L1939733-08Y

L1939733-08Z

L1939733-09A

L1939733-09B

L1939733-09C

L1939733-09D

L1939733-09E

L1939733-09F

L1939733-09X

L1939733-09Y

L1939733-09Z

L1939733-10A

L1939733-10B
























A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent


10831

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)



NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)



NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

Project Name:

Project Number:

L1939733Lab Number:

Report Date:



Analysis(*)

09/09/19

31-AUG-19 12:38

31-AUG-19 12:38

31-AUG-19 12:38

31-AUG-19 12:38

31-AUG-19 12:38

31-AUG-19 12:38

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09091918:03

Page 214 of 222


L1939733-10C

L1939733-10D

L1939733-10E

L1939733-10F

L1939733-10X

L1939733-10Y

L1939733-10Z

L1939733-11A

L1939733-11B

L1939733-11C

L1939733-11D

L1939733-11E

L1939733-11F

L1939733-11X

L1939733-11Y

L1939733-11Z

L1939733-12A

L1939733-12B

L1939733-12C

L1939733-12D




















Glass 60ml unpreserved split

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

2.9

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent


10831

NYTCL-8260HLW(14)

TS(7)



NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)



NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)




BE-TI(180),AS-TI(180),BA-TI(180),AG-TI(180),AL-TI(180),CR-TI(180),NI-TI(180),TL-TI(180),CU-TI(180),PB-TI(180),SB-TI(180),SE-TI(180),ZN-TI(180),CO-TI(180),FE-TI(180),HG-T(28),MG-TI(180),MN-TI(180),CA-TI(180),CD-TI(180),K-TI(180),NA-TI(180)

Project Name:

Project Number:

L1939733Lab Number:

Report Date:



Analysis(*)

09/09/19

31-AUG-19 12:38

31-AUG-19 12:38

31-AUG-19 12:38

31-AUG-19 12:38

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09091918:03

Page 215 of 222


L1939733-12E

L1939733-12X

L1939733-12Y

L1939733-12Z





A

A

A

A

NA

NA

NA

NA

2.9

2.9

2.9

2.9

Y

Y

Y

Y

Absent

Absent

Absent

Absent


10831

NYTCL-8270(14),TCN-9010(14),TS(7),NYTCL-8081(14),NYTCL-8082(14)




Project Name:

Project Number:

L1939733Lab Number:

Report Date:



Analysis(*)

09/09/19

31-AUG-19 12:38

31-AUG-19 12:38

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09091918:03

Page 216 of 222

Report Format: DU Report with 'J' Qualifiers

GLOSSARY

Project Name:

Project Number:

Lab Number:

Report Date:

L193973390-02 168TH ST., JAMAICA, NY

10831 09/09/19

Acronyms

DL

EDL

EMPC

EPA

LCS

LCSD

LFB

LOD

LOQ

MDL

MS

MSD

NA

NC

NDPA/DPA

NI

NP

RL

RPD

SRM

STLP

TEF

TEQ

TIC

Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the limit of quantitation (LOQ). The DL includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats only.)Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction (SPME).Estimated Maximum Possible Concentration: The concentration that results from the signal present at the retention time of an analyte when the ions meet all of the identification criteria except the ion abundance ratio criteria. An EMPC is a worst-case estimate of the concentration.Environmental Protection Agency.

Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Laboratory Control Sample Duplicate: Refer to LCS.

Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Limit of Detection: This value represents the level to which a target analyte can reliably be detected for a specific analyte in a specific matrix by a specific method. The LOD includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats only.) Limit of Quantitation: The value at which an instrument can accurately measure an analyte at a specific concentration. The LOQ includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats only.)

Limit of Quantitation: The value at which an instrument can accurately measure an analyte at a specific concentration. The LOQ includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats only.)

Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample forwhich an independent estimate of target analyte concentration is available. For Method 332.0, the spike recovery is calculated using the native concentration, including estimated values.Matrix Spike Sample Duplicate: Refer to MS.

Not Applicable.

Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit.N-Nitrosodiphenylamine/Diphenylamine.

Not Ignitable.

Non-Plastic: Term is utilized for the analysis of Atterberg Limits in soil.

Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report.Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples.Semi-dynamic Tank Leaching Procedure per EPA Method 1315.

Toxic Equivalency Factors: The values assigned to each dioxin and furan to evaluate their toxicity relative to 2,3,7,8-TCDD.

Toxic Equivalent: The measure of a sample's toxicity derived by multiplying each dioxin and furan by its corresponding TEF and then summing the resulting values.Tentatively Identified Compound: A compound that has been identified to be present and is not part of the target compound list (TCL) for the method and/or program. All TICs are qualitatively identified and reported as estimated concentrations.

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

Footnotes

Serial_No:09091918:03

Page 217 of 222


Project Name:

Project Number:

Lab Number:

Report Date:

L193973390-02 168TH ST., JAMAICA, NY

10831 09/09/19

Terms

Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.Difference: With respect to Total Oxidizable Precursor (TOP) Assay analysis, the difference is defined as the Post-Treatment value minus thePre-Treatment value. Final pH: As it pertains to Sample Receipt & Container Information section of the report, Final pH reflects pH of container determined after adjustment at the laboratory, if applicable. If no adjustment required, value reflects Initial pH.Frozen Date/Time: With respect to Volatile Organics in soil, Frozen Date/Time reflects the date/time at which associated Reagent Water-preserved vials were initially frozen. Note: If frozen date/time is beyond 48 hours from sample collection, value will be reflected in 'bold'.Initial pH: As it pertains to Sample Receipt & Container Information section of the report, Initial pH reflects pH of container determined uponreceipt, if applicable.PFAS Total: With respect to PFAS analyses, the 'PFAS, Total (5)' result is defined as the summation of results for: PFHpA, PFHxS, PFOA, PFNA and PFOS. If a 'Total' result is requested, the results of its individual components will also be reported.Total: With respect to Organic analyses, a 'Total' result is defined as the summation of results for individual isomers or Aroclors. If a 'Total' result is requested, the results of its individual components will also be reported. This is applicable to 'Total' results for methods 8260, 8081 and 8082.

Data Qualifiers

A

B

C

D

E

G

H

I

J

M

ND

NJ

P

Q

R

RE

S

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

Spectra identified as "Aldol Condensates" are byproducts of the extraction/concentration procedures when acetone is introduced in the process.The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit. For NJ-related projects (excluding Air), flag only applies to associated field samples that have detectable concentrations of the analyte, which was detected above the reporting limit in the associated method blank or above five times the reporting limit for common lab contaminants (Phthalates, Acetone, Methylene Chloride, 2-Butanone). Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses.Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte.Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.

The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated.The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.

The lower value for the two columns has been reported due to obvious interference.

Estimated value. The Target analyte concentration is below the quantitation limit (RL), but above the Method Detection Limit (MDL) or Estimated Detection Limit (EDL) for SPME-related analyses. This represents an estimated concentration for Tentatively Identified Compounds (TICs).Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.

Not detected at the method detection limit (MDL) for the sample, or estimated detection limit (EDL) for SPME-related analyses.

Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search.The RPD between the results for the two columns exceeds the method-specified criteria.

The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing CalibrationStandard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoverieswhen the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are lessthan 5x the RL. (Metals only.)Analytical results are from sample re-analysis.

Analytical results are from sample re-extraction.

Analytical results are from modified screening analysis.

1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original method.

-

Serial_No:09091918:03

Page 218 of 222

Alpha Analytical performs services with reasonable care and diligence normal to the analytical testinglaboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analyticalshall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liablefor any incidental, consequential or special damages, including but not limited to, damages in any wayconnected with the use of, interpretation of, information or analysis provided by Alpha Analytical.

We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,containers, sampling procedures, holding time and splitting of samples in the field.

LIMITATION OF LIABILITIES

1

121

Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IV, 2007.

Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WEF. Standard Methods Online.

Project Name:

Project Number:

Lab Number:

Report Date:

L193973390-02 168TH ST., JAMAICA, NY

10831

REFERENCES

09/09/19

Serial_No:09091918:03

Page 219 of 222

Alpha Analytical, Inc. ID No.:17873 Facility: Company-wide Revision 15Department: Quality Assurance Published Date: 8/15/2019 9:53:42 AMTitle: Certificate/Approval Program Summary Page 1 of 1

Document Type: Form Pre-Qualtrax Document ID: 08-113

Certification Information

The following analytes are not included in our Primary NELAP Scope of Accreditation:

Westborough FacilityEPA 624/624.1: m/p-xylene, o-xyleneEPA 8260C: NPW: 1,2,4,5-Tetramethylbenzene; 4-Ethyltoluene, Azobenzene; SCM: Iodomethane (methyl iodide), 1,2,4,5-Tetramethylbenzene; 4-Ethyltoluene.EPA 8270D: NPW: Dimethylnaphthalene,1,4-Diphenylhydrazine; SCM: Dimethylnaphthalene,1,4-Diphenylhydrazine.SM4500: NPW: Amenable Cyanide; SCM: Total Phosphorus, TKN, NO2, NO3.

Mansfield FacilitySM 2540D: TSSEPA 8082A: NPW: PCB: 1, 5, 31, 87,101, 110, 141, 151, 153, 180, 183, 187.EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene, 3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene. Biological Tissue Matrix: EPA 3050B

The following analytes are included in our Massachusetts DEP Scope of Accreditation

Westborough Facility:

Drinking WaterEPA 300.0: Chloride, Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500F-C, SM4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, SM2320B, SM2540C, SM4500H-B, SM4500NO2-BEPA 332: Perchlorate; EPA 524.2: THMs and VOCs; EPA 504.1: EDB, DBCP.Microbiology: SM9215B; SM9223-P/A, SM9223B-Colilert-QT,SM9222D.

Non-Potable WaterSM4500H,B, EPA 120.1, SM2510B, SM2540C, SM2320B, SM4500CL-E, SM4500F-BC, SM4500NH3-BH: Ammonia-N and Kjeldahl-N, EPA 350.1: Ammonia-N, LACHAT 10-107-06-1-B: Ammonia-N, EPA 351.1, SM4500NO3-F, EPA 353.2: Nitrate-N, SM4500P-E, SM4500P-B, E, SM4500SO4-E, SM5220D, EPA 410.4, SM5210B, SM5310C, SM4500CL-D, EPA 1664, EPA 420.1, SM4500-CN-CE, SM2540D, EPA 300: Chloride, Sulfate, Nitrate. EPA 624.1: Volatile Halocarbons & Aromatics, EPA 608.3: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBsEPA 625.1: SVOC (Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil. Microbiology: SM9223B-Colilert-QT; Enterolert-QT, SM9221E, EPA 1600, EPA 1603.

Mansfield Facility:

Drinking WaterEPA 200.7: Al, Ba, Cd, Cr, Cu, Fe, Mn, Ni, Na, Ag, Ca, Zn. EPA 200.8: Al, Sb, As, Ba, Be, Cd, Cr, Cu, Pb, Mn, Ni, Se, Ag, TL, Zn. EPA 245.1 Hg.EPA 522.

Non-Potable WaterEPA 200.7: Al, Sb, As, Be, Cd, Ca, Cr, Co, Cu, Fe, Pb, Mg, Mn, Mo, Ni, K, Se, Ag, Na, Sr, TL, Ti, V, Zn. EPA 200.8: Al, Sb, As, Be, Cd, Cr, Cu, Fe, Pb, Mn, Ni, K, Se, Ag, Na, TL, Zn.EPA 245.1 Hg. SM2340B

For a complete listing of analytes and methods, please contact your Alpha Project Manager.

Serial_No:09091918:03

Page 220 of 222

Serial_No:09091918:03

Page 221 of 222

Serial_No:09091918:03

Page 222 of 222

L1940104


10831


Client:

Project Name:

Project Number:

09/11/19


Lab Number:

Report Date:


12A Maple Avenue


Jesse MausnerATTN:

ANALYTICAL REPORT

Certifications & Approvals: MA (M-MA030), NH NELAP (2062), CT (PH-0141), DoD (L2474), FL (E87814), IL (200081), LA (85084),ME (MA00030), MD (350), NJ (MA015), NY (11627), NC (685), OH (CL106), PA (68-02089), RI (LAO00299), TX (T104704419), VT (VT-0015), VA (460194), WA (C954), US Army Corps of Engineers, USDA (Permit #P330-17-00150), USFWS (Permit #206964).

(973) 808-9050Phone:


Serial_No:09111913:42

Page 1 of 177

L1940104-01

L1940104-02

L1940104-03

L1940104-04

L1940104-05

L1940104-06

L1940104-07

Alpha Sample ID

SESI-SB-20 (2-3)

SESI-SB-20 (14-15)

TW-1

TW-2

TW-3

TW-4

TB

Client ID

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

Sample Location


10831



L194010409/11/19

09/03/19 10:25

09/03/19 10:30

09/03/19 09:10

09/03/19 11:10

09/03/19 13:00

09/03/19 15:30

08/28/19 00:00


SOIL

SOIL

WATER

WATER

WATER

WATER

WATER

09/04/19

09/04/19

09/04/19

09/04/19

09/04/19

09/04/19

09/04/19

Serial_No:09111913:42

Page 2 of 177


10831

Project Name:

Project Number:

Lab Number:


09/11/19

Case Narrative

























Serial_No:09111913:42

Page 3 of 177



10831

Project Name:

Project Number:

Lab Number:


09/11/19

Report Submission


MDL column.

Semivolatile Organics by SIM

The WG1280001-1 Method Blank, associated with L1940104-03 through -06, has a concentration above the

reporting limit for naphthalene. The results of the original analysis are reported and are qualified with a "B" for

any associated sample concentrations that are less than 10x the blank concentration for this analyte.


The WG1279999-2/-3 LCS/LCSD recoveries, associated with L1940104-03 through -06, are below the

acceptance criteria for benzoic acid (0%/0%); however, it has been identified as a "difficult" analyte. The results

of the associated samples are reported.

PCBs

The WG1280288-1 Method Blank, associated with L1940104-03 through -06, has a concentration above the

reporting limit for Aroclor 1260. Since the samples were non-detect to the RL for this target analyte, no further

actions were taken. The results of the original analysis are reported.

Total Metals

L1940104-01 and -02: The sample has elevated detection limits for all elements, with the exception of


Dissolved Metals

The WG1282377-3 MS recoveries for calcium (260%), manganese (51%), and sodium (140%), performed on

L1940104-04, do not apply because the sample concentrations are greater than four times the spike amounts

added.

Serial_No:09111913:42

Page 4 of 177



10831

Project Name:

Project Number:

Lab Number:


09/11/19

Cyanide, Total

The WG1280650-2/-3 LCS/LCSD recoveries (71%/57%), associated with L1940104-01 and -02, are outside

our in-house acceptance criteria, but within the vendor-certified acceptance limits. The results of the original

analyses are reported. The LCS/LCSD RPD (39%) is above the acceptance criteria.




Serial_No:09111913:42

Page 5 of 177

ORGANICS

Serial_No:09111913:42

Page 6 of 177

VOLATILES

Serial_No:09111913:42

Page 7 of 177

FF

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

5.2

1.0

1.5

1.0

1.0

1.0

1.0

0.52

0.52

4.1

1.0

0.52

0.52

1.0

0.52

0.52

0.52

4.1

0.52

0.52

1.0

1.0

4.1

2.1

1.0

2.1

1.0

1.5

09/11/19



L1940104-01Lab ID:



1,8260C09/06/19 13:59MKS 83%Percent Solids:

MDL

2.4

0.15

0.14

0.24

0.13

0.14

0.28

0.20

0.13

0.72

0.26

0.17

0.11

0.28

0.16

0.16

0.16

0.25

0.17

0.17

0.56

0.14

0.96

0.60

0.34

0.47

0.24

0.14

Sample Depth:

Serial_No:09111913:42

Page 8 of 177

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

1.7

ND

ND

ND

ND

ND

ND

ND

ND

15

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.52

2.1

2.1

2.1

2.1

2.1

1.0

1.0

1.0

1.0

2.1

1.0

10

10

10

10

10

10

2.1

10

2.1

2.1

1.0

2.1

0.52

2.1

1.0

1.0

2.1

2.1

2.1

3.1

4.1

1.0

1.0

4.1

4.1

09/11/19



L1940104-01Lab ID:


MDL

0.14

0.15

0.15

0.18

0.21

0.58

0.30

0.30

0.18

0.14

0.24

0.20

0.94

5.0

4.7

2.3

2.2

1.3

0.13

1.2

0.21

0.21

0.29

0.17

0.14

0.15

0.17

0.15

0.12

0.20

0.11

1.0

0.17

0.11

0.11

0.67

1.2

Sample Depth:

Serial_No:09111913:42

Page 9 of 177

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

1.0

2.1

2.1

2.1

2.1

82

2.1

2.1

2.1

2.1

5.2


Toluene-d8



106

99

107

102

70-130

70-130

70-130

70-130


09/11/19



L1940104-01Lab ID:




MDL

0.18

0.33

0.28

0.20

0.34

36.

0.18

0.40

0.20

0.35

1.5

Sample Depth:

Serial_No:09111913:42

Page 10 of 177

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

5.3

1.0

1.6

1.0

1.0

1.0

1.0

0.53

0.53

4.2

1.0

0.53

0.53

1.0

0.53

0.53

0.53

4.2

0.53

0.53

1.0

1.0

4.2

2.1

1.0

2.1

1.0

1.6

09/11/19



L1940104-02Lab ID:



1,8260C09/06/19 14:39MKS 96%Percent Solids:

MDL

2.4

0.15

0.15

0.24

0.13

0.15

0.28

0.21

0.13

0.73

0.27

0.18

0.11

0.29

0.17

0.17

0.17

0.26

0.18

0.18

0.57

0.15

0.98

0.61

0.35

0.48

0.25

0.14

Sample Depth:

Serial_No:09111913:42

Page 11 of 177

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

2.2

ND

ND

ND

ND

ND

ND

ND

ND

190

ND

2.7

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.53

2.1

2.1

2.1

2.1

2.1

1.0

1.0

1.0

1.0

2.1

1.0

10

10

10

10

10

10

2.1

10

2.1

2.1

1.0

2.1

0.53

2.1

1.0

1.0

2.1

2.1

2.1

3.2

4.2

1.0

1.0

4.2

4.2

09/11/19



L1940104-02Lab ID:


MDL

0.14

0.15

0.16

0.18

0.21

0.59

0.31

0.31

0.18

0.14

0.25

0.21

0.96

5.1

4.8

2.3

2.3

1.3

0.13

1.2

0.22

0.21

0.29

0.18

0.14

0.15

0.18

0.15

0.12

0.20

0.11

1.0

0.18

0.11

0.11

0.68

1.2

Sample Depth:

Serial_No:09111913:42

Page 12 of 177

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

1.0

2.1

2.1

2.1

2.1

84

2.1

2.1

2.1

2.1

5.3


Toluene-d8



107

99

107

101

70-130

70-130

70-130

70-130


09/11/19



L1940104-02Lab ID:




MDL

0.18

0.34

0.29

0.20

0.35

37.

0.19

0.40

0.20

0.36

1.5

Sample Depth:

Serial_No:09111913:42

Page 13 of 177

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

4.2

ND

ND

ND

ND

0.41

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Volatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2.5

2.5

2.5

0.50

1.0

0.50

1.5

0.50

2.5

2.5

0.50

2.5

0.50

0.50

0.50

0.50

2.5

2.0

0.50

0.50

2.5

2.5

2.5

2.5

1.0

2.5

0.50

2.5

09/11/19

TW-1Client ID:09/03/19 09:10Date Collected:09/04/19Date Received:


L1940104-03Lab ID:


Matrix: WaterAnalytical Method:Analytical Date:Analyst:

1,8260C09/09/19 13:08AD

MDL

0.70

0.70

0.70

0.13

0.14

0.15

0.50

0.18

0.70

0.70

0.13

0.70

0.19

0.16

0.14

0.14

0.70

0.65

0.17

0.16

0.70

0.70

0.70

0.70

0.07

0.70

0.17

0.70

Sample Depth:

Serial_No:09111913:42

Page 14 of 177

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane


Acrylonitrile

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Parameter Result

J

J

Dilution Factor

0.44

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

4.5

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.50

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

5.0

2.5

5.0

2.5

5.0

5.0

5.0

5.0

5.0

5.0

5.0

2.5

2.5

2.0

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

09/11/19



L1940104-03Lab ID:


MDL

0.18

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

1.0

0.70

1.5

0.70

1.0

1.5

1.0

1.9

1.0

1.0

1.0

0.70

0.70

0.65

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

Sample Depth:

Serial_No:09111913:42

Page 15 of 177

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2.5

2.5

2.5

2.5

2.5

250

2.0

2.0

2.0

2.5

2.5


Toluene-d8



90

107

84

92

70-130

70-130

70-130

70-130


09/11/19



L1940104-03Lab ID:


Total TIC Compounds

Silanol, Trimethyl-

Propene

Unknown

J

NJ

NJ

J

4.01

1.11

1.36

1.54

ug/l

ug/l

ug/l

ug/l

1

1

1

1


MDL

0.70

0.70

0.70

0.70

0.70

61.

0.70

0.70

0.54

0.70

0.70

Sample Depth:

Serial_No:09111913:42

Page 16 of 177

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene



ND

ND

3.9

ND

ND

ND

ND

0.85

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2.5

2.5

2.5

0.50

1.0

0.50

1.5

0.50

2.5

2.5

0.50

2.5

0.50

0.50

0.50

0.50

2.5

2.0

0.50

0.50

2.5

2.5

2.5

2.5

1.0

2.5

0.50

2.5

09/11/19



L1940104-04Lab ID:



1,8260C09/09/19 13:33AD

MDL

0.70

0.70

0.70

0.13

0.14

0.15

0.50

0.18

0.70

0.70

0.13

0.70

0.19

0.16

0.14

0.14

0.70

0.65

0.17

0.16

0.70

0.70

0.70

0.70

0.07

0.70

0.17

0.70

Sample Depth:

Serial_No:09111913:42

Page 17 of 177

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane


Acrylonitrile

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

4.1

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.50

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

5.0

2.5

5.0

2.5

5.0

5.0

5.0

5.0

5.0

5.0

5.0

2.5

2.5

2.0

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

09/11/19



L1940104-04Lab ID:


MDL

0.18

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

1.0

0.70

1.5

0.70

1.0

1.5

1.0

1.9

1.0

1.0

1.0

0.70

0.70

0.65

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

Sample Depth:

Serial_No:09111913:42

Page 18 of 177

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2.5

2.5

2.5

2.5

2.5

250

2.0

2.0

2.0

2.5

2.5


Toluene-d8



92

90

94

92

70-130

70-130

70-130

70-130


09/11/19



L1940104-04Lab ID:


Total TIC Compounds

Unknown

Unknown

J

J

J

3.60

1.80

1.80

ug/l

ug/l

ug/l

1

1

1


MDL

0.70

0.70

0.70

0.70

0.70

61.

0.70

0.70

0.54

0.70

0.70

Sample Depth:

Serial_No:09111913:42

Page 19 of 177

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

5.9

ND

ND

ND

ND

0.25

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2.5

2.5

2.5

0.50

1.0

0.50

1.5

0.50

2.5

2.5

0.50

2.5

0.50

0.50

0.50

0.50

2.5

2.0

0.50

0.50

2.5

2.5

2.5

2.5

1.0

2.5

0.50

2.5

09/11/19



L1940104-05Lab ID:



1,8260C09/09/19 13:59AD

MDL

0.70

0.70

0.70

0.13

0.14

0.15

0.50

0.18

0.70

0.70

0.13

0.70

0.19

0.16

0.14

0.14

0.70

0.65

0.17

0.16

0.70

0.70

0.70

0.70

0.07

0.70

0.17

0.70

Sample Depth:

Serial_No:09111913:42

Page 20 of 177

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane


Acrylonitrile

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Parameter Result

J

J

Dilution Factor

0.49

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

3.7

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.50

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

5.0

2.5

5.0

2.5

5.0

5.0

5.0

5.0

5.0

5.0

5.0

2.5

2.5

2.0

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

09/11/19



L1940104-05Lab ID:


MDL

0.18

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

1.0

0.70

1.5

0.70

1.0

1.5

1.0

1.9

1.0

1.0

1.0

0.70

0.70

0.65

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

Sample Depth:

Serial_No:09111913:42

Page 21 of 177

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2.5

2.5

2.5

2.5

2.5

250

2.0

2.0

2.0

2.5

2.5


Toluene-d8



91

92

94

93

70-130

70-130

70-130

70-130


09/11/19



L1940104-05Lab ID:


Total TIC Compounds

Unknown

1-Propene, 2-methyl-

J

J

NJ

2.77

1.19

1.58

ug/l

ug/l

ug/l

1

1

1


MDL

0.70

0.70

0.70

0.70

0.70

61.

0.70

0.70

0.54

0.70

0.70

Sample Depth:

Serial_No:09111913:42

Page 22 of 177

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

1.4

ND

ND

ND

ND

0.68

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2.5

2.5

2.5

0.50

1.0

0.50

1.5

0.50

2.5

2.5

0.50

2.5

0.50

0.50

0.50

0.50

2.5

2.0

0.50

0.50

2.5

2.5

2.5

2.5

1.0

2.5

0.50

2.5

09/11/19



L1940104-06Lab ID:



1,8260C09/09/19 14:24AD

MDL

0.70

0.70

0.70

0.13

0.14

0.15

0.50

0.18

0.70

0.70

0.13

0.70

0.19

0.16

0.14

0.14

0.70

0.65

0.17

0.16

0.70

0.70

0.70

0.70

0.07

0.70

0.17

0.70

Sample Depth:

Serial_No:09111913:42

Page 23 of 177

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane


Acrylonitrile

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

4.9

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.50

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

5.0

2.5

5.0

2.5

5.0

5.0

5.0

5.0

5.0

5.0

5.0

2.5

2.5

2.0

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

09/11/19



L1940104-06Lab ID:


MDL

0.18

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

1.0

0.70

1.5

0.70

1.0

1.5

1.0

1.9

1.0

1.0

1.0

0.70

0.70

0.65

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

Sample Depth:

Serial_No:09111913:42

Page 24 of 177

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2.5

2.5

2.5

2.5

2.5

250

2.0

2.0

2.0

2.5

2.5


Toluene-d8



92

77

93

93

70-130

70-130

70-130

70-130


09/11/19



L1940104-06Lab ID:


Total TIC Compounds

Propene

Unknown

Unknown

J

NJ

J

J

12.7

6.54

4.35

1.79

ug/l

ug/l

ug/l

ug/l

1

1

1

1


MDL

0.70

0.70

0.70

0.70

0.70

61.

0.70

0.70

0.54

0.70

0.70

Sample Depth:

Serial_No:09111913:42

Page 25 of 177

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2.5

2.5

2.5

0.50

1.0

0.50

1.5

0.50

2.5

2.5

0.50

2.5

0.50

0.50

0.50

0.50

2.5

2.0

0.50

0.50

2.5

2.5

2.5

2.5

1.0

2.5

0.50

2.5

09/11/19

TBClient ID:08/28/19 00:00Date Collected:09/04/19Date Received:


L1940104-07Lab ID:



1,8260C09/09/19 14:49AD

MDL

0.70

0.70

0.70

0.13

0.14

0.15

0.50

0.18

0.70

0.70

0.13

0.70

0.19

0.16

0.14

0.14

0.70

0.65

0.17

0.16

0.70

0.70

0.70

0.70

0.07

0.70

0.17

0.70

Sample Depth:

Serial_No:09111913:42

Page 26 of 177

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane


Acrylonitrile

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

2.3

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.50

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

5.0

2.5

5.0

2.5

5.0

5.0

5.0

5.0

5.0

5.0

5.0

2.5

2.5

2.0

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

09/11/19



L1940104-07Lab ID:


MDL

0.18

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

1.0

0.70

1.5

0.70

1.0

1.5

1.0

1.9

1.0

1.0

1.0

0.70

0.70

0.65

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

Sample Depth:

Serial_No:09111913:42

Page 27 of 177

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2.5

2.5

2.5

2.5

2.5

250

2.0

2.0

2.0

2.5

2.5


Toluene-d8



91

99

94

94

70-130

70-130

70-130

70-130


09/11/19



L1940104-07Lab ID:


Total TIC Compounds

Unknown


J

J

NJ

3.32

2.30

1.02

ug/l

ug/l

ug/l

1

1

1


MDL

0.70

0.70

0.70

0.70

0.70

61.

0.70

0.70

0.54

0.70

0.70

Sample Depth:

Serial_No:09111913:42

Page 28 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Analytical Date:

09/11/19

Analyst: MV

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

Parameter Result

ND

ND

0.16

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

5.0

1.0

1.5

1.0

1.0

1.0

1.0

0.50

0.50

4.0

1.0

0.50

0.50

1.0

0.50

0.50

0.50

4.0

0.50

0.50

1.0

1.0

4.0

2.0

1.0

2.0

1.0

1.5

0.50

J

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

2.3

0.14

0.14

0.23

0.12

0.14

0.27

0.20

0.13

0.70

0.26

0.17

0.11

0.27

0.16

0.16

0.16

0.25

0.17

0.17

0.54

0.14

0.93

0.58

0.34

0.45

0.24

0.14

0.14

Serial_No:09111913:42

Page 29 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Analytical Date:

09/11/19

Analyst: MV

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

1.0

2.0

1.0

10

10

10

10

10

10

2.0

10

2.0

2.0

1.0

2.0

0.50

2.0

1.0

1.0

2.0

2.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

0.14

0.15

0.17

0.20

0.56

0.29

0.29

0.18

0.14

0.24

0.20

0.92

4.8

4.6

2.2

2.2

1.3

0.13

1.2

0.20

0.20

0.28

0.17

0.13

0.14

0.17

0.15

0.12

0.19

Serial_No:09111913:42

Page 30 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Analytical Date:

09/11/19

Analyst: MV

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.0

3.0

4.0

1.0

1.0

4.0

4.0

1.0

2.0

2.0

2.0

2.0

80

2.0

2.0

2.0

2.0

5.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier




MDL

0.11

1.0

0.17

0.11

0.11

0.65

1.2

0.17

0.32

0.27

0.19

0.33

35.

0.18

0.38

0.19

0.34

1.4

Serial_No:09111913:42

Page 31 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Analytical Date:

09/11/19

Analyst: MV




Toluene-d8



104

98

104

100

70-130

70-130

70-130

70-130


Criteria

MDL

Serial_No:09111913:42

Page 32 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Analytical Date:

09/11/19

Analyst: PD

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.98

ND

ND

ND

ND

ND

RL

2.5

2.5

2.5

0.50

1.0

0.50

1.5

0.50

2.5

2.5

0.50

2.5

0.50

0.50

0.50

0.50

2.5

2.0

0.50

0.50

2.5

2.5

2.5

2.5

1.0

2.5

0.50

2.5

0.50

J

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

Volatile Organics by GC/MS - Westborough Lab for sample(s): 03-07 Batch: WG1281895-5

MDL

0.70

0.70

0.70

0.13

0.14

0.15

0.50

0.18

0.70

0.70

0.13

0.70

0.19

0.16

0.14

0.14

0.70

0.65

0.17

0.16

0.70

0.70

0.70

0.70

0.07

0.70

0.17

0.70

0.18

Serial_No:09111913:42

Page 33 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Analytical Date:

09/11/19

Analyst: PD

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane


Acrylonitrile

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

5.0

2.5

5.0

2.5

5.0

5.0

5.0

5.0

5.0

5.0

5.0

2.5

2.5

2.0

2.5

2.5

2.5

2.5

2.5

2.5

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier


MDL

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

1.0

0.70

1.5

0.70

1.0

1.5

1.0

1.9

1.0

1.0

1.0

0.70

0.70

0.65

0.70

0.70

0.70

0.70

0.70

0.70

Serial_No:09111913:42

Page 34 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Analytical Date:

09/11/19

Analyst: PD

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

250

2.0

2.0

2.0

2.5

2.5

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier


No Tentatively Identified Compounds ND ug/l


MDL

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

0.70

61.

0.70

0.70

0.54

0.70

0.70

Serial_No:09111913:42

Page 35 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Analytical Date:

09/11/19

Analyst: PD




Toluene-d8



94

95

105

92

70-130

70-130

70-130

70-130


Criteria

MDL

Serial_No:09111913:42

Page 36 of 177

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

105

116

105

111

111

93

101

96

96

128

108

110

103

100

106

118

89

99

109

102

105

147

110

105

114

106

110

112

95

101

95

96

125

108

110

104

103

108

116

90

100

108

101

104

149

114

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-139

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

52-130

57-147

0

2

1

1

1

2

0

1

0

2

0

0

1

3

2

2

1

1

1

1

1

1

4

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual

Q Q

Qual

Serial_No:09111913:42

Page 37 of 177

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

150

132

119

111

109

95

98

97

105

102

100

105

104

101

217

122

123

114

116

107

102

108

100

147

132

118

111

108

95

98

97

106

102

99

105

105

102

215

117

121

117

118

107

101

109

102

67-130

50-151

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

70-130

70-130

30-146

54-140

59-130

70-130

70-130

70-130

68-130

70-130

70-130

2

0

1

0

1

0

0

0

1

0

1

0

1

1

1

4

2

3

2

0

1

1

2

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual

Q

Q

Q

Q

Qual

Serial_No:09111913:42

Page 38 of 177

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

114

96

100

94

94

105

107

103

103

105

88

91

105

104

102

118

108

96

99

104

104

107

98

113

97

101

95

94

103

104

101

102

103

89

90

103

101

101

114

106

94

98

102

103

107

96

70-130

70-130

69-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

68-130

67-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

65-136

70-130

1

1

1

1

0

2

3

2

1

2

1

1

2

3

1

3

2

2

1

2

1

0

2

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual Qual

Serial_No:09111913:42

Page 39 of 177

p-Ethyltoluene


Ethyl ether


100

96

107

106

98

95

110

106

70-130

70-130

67-130

70-130

2

1

3

0

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


1039910599

70-13070-13070-13070-130

1029810499


09/11/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09111913:42

Page 40 of 177

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

90

94

88

89

93

89

97

89

89

89

90

87

89

91

90

93

89

95

94

91

90

86

99

92

93

93

89

95

89

96

90

90

89

93

87

90

92

91

91

94

97

94

91

89

85

95

70-130

70-130

70-130

63-132

70-130

63-130

70-130

70-130

75-130

62-150

70-130

67-130

67-130

70-130

70-130

70-130

54-136

67-130

70-130

70-130

70-130

64-130

39-139

2

1

6

0

2

0

1

1

1

0

3

0

1

1

1

2

5

2

0

0

1

1

4

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 03-07 Batch: WG1281895-3 WG1281895-4


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual Qual

Serial_No:09111913:42

Page 41 of 177

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Dibromomethane


Acrylonitrile

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

88

93

89

92

90

92

91

90

92

90

90

90

92

94

110

90

82

110

91

120

97

100

100

87

92

91

93

91

92

90

90

94

85

90

90

94

92

110

90

82

110

87

120

98

100

100

55-140

55-138

61-145

70-130

70-130

70-130

70-130

70-130

63-130

70-130

70-130

70-130

70-130

64-130

70-130

70-130

36-147

58-148

51-130

63-138

70-130

59-130

57-130

1

1

2

1

1

0

1

0

2

6

0

0

2

2

0

0

0

0

4

0

1

0

0

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual Qual

Serial_No:09111913:42

Page 42 of 177

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

95

94

94

97

87

90

92

94

92

90

92

96

85

93

92

96

93

94

92

92

94

120

90

96

96

95

96

88

91

92

93

92

92

92

92

82

92

92

99

91

95

94

92

93

114

90

70-130

63-133

70-130

70-130

64-130

70-130

53-136

70-130

70-130

70-130

70-130

41-144

63-130

70-130

70-130

70-130

69-130

70-130

70-130

64-130

70-130

56-162

70-130

1

2

1

1

1

1

0

1

0

2

0

4

4

1

0

3

2

1

2

0

1

5

0

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual Qual

Serial_No:09111913:42

Page 43 of 177

p-Ethyltoluene


Ethyl ether


92

94

93

90

92

94

97

89

70-130

70-130

59-134

70-130

0

0

4

1

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


94969991

70-13070-13070-13070-130

969610091


09/11/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09111913:42

Page 44 of 177

SEMIVOLATILES

Serial_No:09111913:42

Page 45 of 177

FF

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

180

ND

ND

ND

ND

ND

ND

ND

ND

71

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

160

200

120

180

200

200

200

200

200

200

200

120

200

200

240

210

200

560

160

180

200

180

160

200

200

200

200

200

09/11/19



L1940104-01Lab ID:




1,8270D09/11/19 02:06JG


83%Percent Solids:

MDL

20.

22.

22.

27.

19.

35.

34.

34.

52.

39.

34.

22.

21.

30.

34.

20.

29.

180

32.

25.

24.

29.

22.

30.

68.

49.

37.

67.

Sample Depth:

Serial_No:09111913:42

Page 46 of 177

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

J

J

J

Dilution Factor

ND

ND

91

110

150

62

100

ND

ND

80

ND

68

ND

92

160

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

200

200

120

160

120

120

120

160

120

160

200

120

120

160

120

450

200

200

200

200

200

240

200

200

120

200

200

180

200

420

270

940

510

160

200

200

280

09/11/19



L1940104-01Lab ID:


MDL

18.

41.

22.

48.

33.

31.

20.

30.

38.

23.

19.

24.

23.

27.

20.

46.

36.

38.

37.

81.

18.

24.

20.

24.

37.

29.

23.

32.

65.

74.

80.

91.

94.

43.

30.

30.

31.

Sample Depth:

Serial_No:09111913:42

Page 47 of 177


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane


ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

200

640

200

200

29

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

92

101

112

72

100

70

25-120

10-120

23-120

30-120

10-136

18-120


09/11/19



L1940104-01Lab ID:


Total TIC Compounds

Unknown

Unknown

J

J

J

1280

686

597

ug/kg

ug/kg

ug/kg

1

1

1


MDL

38.

200

60.

19.

9.0

Sample Depth:

Serial_No:09111913:42

Page 48 of 177

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

130

170

100

150

170

170

170

170

170

170

170

100

170

170

200

180

170

480

130

150

170

150

130

170

170

170

170

170

09/11/19



L1940104-02Lab ID:




1,8270D09/11/19 00:14JG


96%Percent Solids:

MDL

17.

19.

19.

23.

17.

30.

29.

29.

45.

34.

29.

19.

18.

26.

29.

17.

25.

150

27.

22.

20.

25.

19.

26.

58.

42.

32.

57.

Sample Depth:

Serial_No:09111913:42

Page 49 of 177

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

170

170

100

130

100

100

100

130

100

130

170

100

100

130

100

380

170

170

170

170

170

200

170

170

100

170

170

150

170

360

240

810

440

130

170

170

240

09/11/19



L1940104-02Lab ID:


MDL

16.

35.

19.

41.

28.

27.

18.

26.

33.

20.

16.

20.

19.

23.

17.

39.

31.

32.

32.

70.

16.

20.

18.

21.

32.

25.

20.

27.

56.

63.

69.

78.

81.

37.

25.

26.

26.

Sample Depth:

Serial_No:09111913:42

Page 50 of 177


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane


ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

170

540

170

170

25

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

103

115

105

81

109

87

25-120

10-120

23-120

30-120

10-136

18-120


09/11/19



L1940104-02Lab ID:




MDL

32.

170

52.

16.

7.7

Sample Depth:

Serial_No:09111913:42

Page 51 of 177



1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene






Isophorone

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Dimethyl phthalate

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

2.1

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

5.0

2.0

2.0

2.0

2.0

5.0

5.0

5.0

2.0

2.0

2.0

5.0

20

5.0

2.0

2.0

5.0

3.0

5.0

5.0

5.0

5.0

5.0

2.0

5.0

5.0

5.0

5.0

09/11/19



L1940104-03Lab ID:


Matrix: Water Extraction Method:


1,8270D09/11/19 03:43RC

EPA 3510CExtraction Date: 09/05/19 07:53

MDL

0.50

0.50

0.45

0.40

0.43

1.6

1.2

0.93

0.49

0.38

0.53

0.50

0.69

1.2

0.77

0.42

0.64

1.5

1.2

0.39

1.3

0.38

1.8

0.46

1.1

0.50

0.81

0.80

Sample Depth:

Serial_No:09111913:42

Page 52 of 177

Dibenzofuran


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Phenol

2-Methylphenol



Benzoic Acid

Benzyl Alcohol

Carbazole


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

2.9

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2.0

10

5.0

5.0

2.0

2.0

5.0

5.0

10

10

20

10

5.0

5.0

5.0

5.0

50

2.0

2.0

09/11/19



L1940104-03Lab ID:


MDL

0.50

0.44

0.53

0.61

0.35

0.48

0.41

1.8

0.85

0.67

6.6

1.8

0.57

0.49

0.48

0.77

2.6

0.59

0.49

Sample Depth:

Serial_No:09111913:42

Page 53 of 177



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

48

47

70

66

37

70

21-120

10-120

23-120

15-120

10-120

41-149


09/11/19



L1940104-03Lab ID:


Total TIC Compounds

Unknown

Unknown

Unknown



Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

J

J

J

J

J

J

J

J

J

J

J

J

45.4

1.49

2.29

1.56

2.62

26.4

1.60

2.00

2.54

1.60

1.49

1.78

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1


MDL

Sample Depth:

Serial_No:09111913:42

Page 54 of 177

Acenaphthene

2-Chloronaphthalene

Fluoranthene

Hexachlorobutadiene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

2-Methylnaphthalene

Pentachlorophenol

Hexachlorobenzene

Hexachloroethane

Parameter Result

J

J

JB

J

J

J

J

J

J

J

J

J

J

J

J

J

Dilution Factor

0.04

ND

0.04

ND

0.07

0.04

0.02

0.02

0.02

0.01

0.03

0.04

0.02

0.05

0.07

0.02

0.10

0.04

0.08

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Semivolatile Organics by GC/MS-SIM - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.10

0.20

0.10

0.50

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.80

0.80

0.80

09/11/19



L1940104-03Lab ID:




1,8270D-SIM09/08/19 19:59DV


MDL

0.01

0.02

0.02

0.05

0.05

0.02

0.02

0.01

0.01

0.01

0.01

0.01

0.01

0.01

0.02

0.01

0.01

0.02

0.02

0.01

0.01

0.06

Sample Depth:

Serial_No:09111913:42

Page 55 of 177



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

61

61

92

93

56

103

21-120

10-120

23-120

15-120

10-120

41-149


09/11/19



L1940104-03Lab ID:


MDL

Sample Depth:

Serial_No:09111913:42

Page 56 of 177



1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene






Isophorone

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Dimethyl phthalate

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

2.1

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

5.0

2.0

2.0

2.0

2.0

5.0

5.0

5.0

2.0

2.0

2.0

5.0

20

5.0

2.0

2.0

5.0

3.0

5.0

5.0

5.0

5.0

5.0

2.0

5.0

5.0

5.0

5.0

09/11/19



L1940104-04Lab ID:




1,8270D09/11/19 04:07RC


MDL

0.50

0.50

0.45

0.40

0.43

1.6

1.2

0.93

0.49

0.38

0.53

0.50

0.69

1.2

0.77

0.42

0.64

1.5

1.2

0.39

1.3

0.38

1.8

0.46

1.1

0.50

0.81

0.80

Sample Depth:

Serial_No:09111913:42

Page 57 of 177

Dibenzofuran


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Phenol

2-Methylphenol



Benzoic Acid

Benzyl Alcohol

Carbazole


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2.0

10

5.0

5.0

2.0

2.0

5.0

5.0

10

10

20

10

5.0

5.0

5.0

5.0

50

2.0

2.0

09/11/19



L1940104-04Lab ID:


MDL

0.50

0.44

0.53

0.61

0.35

0.48

0.41

1.8

0.85

0.67

6.6

1.8

0.57

0.49

0.48

0.77

2.6

0.59

0.49

Sample Depth:

Serial_No:09111913:42

Page 58 of 177



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

30

34

61

60

27

65

21-120

10-120

23-120

15-120

10-120

41-149


09/11/19



L1940104-04Lab ID:


Total TIC Compounds

Unknown

Unknown

Unknown


Unknown

Unknown

Unknown

Unknown

Unknown

Unknown


Unknown

J

J

J

J

J

J

J

J

J

J

J

J

J

79.4

6.76

1.93

2.51

19.6

1.60

1.60

3.45

28.3

2.33

3.09

1.67

6.58

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1


MDL

Sample Depth:

Serial_No:09111913:42

Page 59 of 177

Acenaphthene

2-Chloronaphthalene

Fluoranthene

Hexachlorobutadiene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

2-Methylnaphthalene

Pentachlorophenol

Hexachlorobenzene

Hexachloroethane

Parameter Result

J

JB

J

J

Dilution Factor

0.02

ND

ND

ND

0.06

ND

ND

ND

ND

ND

ND

ND

ND

0.02

0.05

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.10

0.20

0.10

0.50

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.80

0.80

0.80

09/11/19



L1940104-04Lab ID:




1,8270D-SIM09/08/19 20:16DV


MDL

0.01

0.02

0.02

0.05

0.05

0.02

0.02

0.01

0.01

0.01

0.01

0.01

0.01

0.01

0.02

0.01

0.01

0.02

0.02

0.01

0.01

0.06

Sample Depth:

Serial_No:09111913:42

Page 60 of 177



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

30

38

73

74

37

90

21-120

10-120

23-120

15-120

10-120

41-149


09/11/19



L1940104-04Lab ID:


MDL

Sample Depth:

Serial_No:09111913:42

Page 61 of 177



1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene






Isophorone

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Dimethyl phthalate

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

2.3

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

5.0

2.0

2.0

2.0

2.0

5.0

5.0

5.0

2.0

2.0

2.0

5.0

20

5.0

2.0

2.0

5.0

3.0

5.0

5.0

5.0

5.0

5.0

2.0

5.0

5.0

5.0

5.0

09/11/19



L1940104-05Lab ID:




1,8270D09/11/19 04:31RC


MDL

0.50

0.50

0.45

0.40

0.43

1.6

1.2

0.93

0.49

0.38

0.53

0.50

0.69

1.2

0.77

0.42

0.64

1.5

1.2

0.39

1.3

0.38

1.8

0.46

1.1

0.50

0.81

0.80

Sample Depth:

Serial_No:09111913:42

Page 62 of 177

Dibenzofuran


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Phenol

2-Methylphenol



Benzoic Acid

Benzyl Alcohol

Carbazole


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2.0

10

5.0

5.0

2.0

2.0

5.0

5.0

10

10

20

10

5.0

5.0

5.0

5.0

50

2.0

2.0

09/11/19



L1940104-05Lab ID:


MDL

0.50

0.44

0.53

0.61

0.35

0.48

0.41

1.8

0.85

0.67

6.6

1.8

0.57

0.49

0.48

0.77

2.6

0.59

0.49

Sample Depth:

Serial_No:09111913:42

Page 63 of 177



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

34

42

65

74

32

89

21-120

10-120

23-120

15-120

10-120

41-149


09/11/19



L1940104-05Lab ID:


Total TIC Compounds

Unknown

Unknown

Unknown


Unknown

Unknown

Unknown Siloxane

Unknown

Unknown

Unknown

Unknown

Unknown

J

J

J

J

J

J

J

J

J

J

J

J

J

78.2

2.33

8.33

1.82

32.5

2.18

2.04

6.40

2.76

14.6

1.49

2.22

1.49

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1


MDL

Sample Depth:

Serial_No:09111913:42

Page 64 of 177

Acenaphthene

2-Chloronaphthalene

Fluoranthene

Hexachlorobutadiene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

2-Methylnaphthalene

Pentachlorophenol

Hexachlorobenzene

Hexachloroethane

Parameter Result

J

J

J

J

J

Dilution Factor

ND

ND

0.04

ND

ND

ND

ND

ND

ND

ND

ND

0.02

ND

0.03

0.09

ND

ND

0.03

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.10

0.20

0.10

0.50

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.80

0.80

0.80

09/11/19



L1940104-05Lab ID:




1,8270D-SIM09/08/19 20:32DV


MDL

0.01

0.02

0.02

0.05

0.05

0.02

0.02

0.01

0.01

0.01

0.01

0.01

0.01

0.01

0.02

0.01

0.01

0.02

0.02

0.01

0.01

0.06

Sample Depth:

Serial_No:09111913:42

Page 65 of 177



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

56

58

82

88

74

106

21-120

10-120

23-120

15-120

10-120

41-149


09/11/19



L1940104-05Lab ID:


MDL

Sample Depth:

Serial_No:09111913:42

Page 66 of 177



1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene






Isophorone

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Dimethyl phthalate

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

2.6

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

5.0

2.0

2.0

2.0

2.0

5.0

5.0

5.0

2.0

2.0

2.0

5.0

20

5.0

2.0

2.0

5.0

3.0

5.0

5.0

5.0

5.0

5.0

2.0

5.0

5.0

5.0

5.0

09/11/19



L1940104-06Lab ID:




1,8270D09/11/19 05:43RC


MDL

0.50

0.50

0.45

0.40

0.43

1.6

1.2

0.93

0.49

0.38

0.53

0.50

0.69

1.2

0.77

0.42

0.64

1.5

1.2

0.39

1.3

0.38

1.8

0.46

1.1

0.50

0.81

0.80

Sample Depth:

Serial_No:09111913:42

Page 67 of 177

Dibenzofuran


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Phenol

2-Methylphenol



Benzoic Acid

Benzyl Alcohol

Carbazole


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2.0

10

5.0

5.0

2.0

2.0

5.0

5.0

10

10

20

10

5.0

5.0

5.0

5.0

50

2.0

2.0

09/11/19



L1940104-06Lab ID:


MDL

0.50

0.44

0.53

0.61

0.35

0.48

0.41

1.8

0.85

0.67

6.6

1.8

0.57

0.49

0.48

0.77

2.6

0.59

0.49

Sample Depth:

Serial_No:09111913:42

Page 68 of 177



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

60

54

73

74

58

89

21-120

10-120

23-120

15-120

10-120

41-149


09/11/19



L1940104-06Lab ID:


Total TIC Compounds

Unknown

Unknown

Unknown

Unknown


Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown


Unknown


J

J

J

J

J

J

J

J

J

J

J

J

J

J

J

J

281

3.56

2.33

2.62

180

3.93

2.87

3.38

6.04

24.9

2.65

3.67

3.89

4.76

8.36

27.8

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1


MDL

Sample Depth:

Serial_No:09111913:42

Page 69 of 177

Acenaphthene

2-Chloronaphthalene

Fluoranthene

Hexachlorobutadiene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

2-Methylnaphthalene

Pentachlorophenol

Hexachlorobenzene

Hexachloroethane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.10

0.20

0.10

0.50

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.80

0.80

0.80

09/11/19



L1940104-06Lab ID:




1,8270D-SIM09/08/19 20:48DV


MDL

0.01

0.02

0.02

0.05

0.05

0.02

0.02

0.01

0.01

0.01

0.01

0.01

0.01

0.01

0.02

0.01

0.01

0.02

0.02

0.01

0.01

0.06

Sample Depth:

Serial_No:09111913:42

Page 70 of 177



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

76

75

99

101

91

121

21-120

10-120

23-120

15-120

10-120

41-149


09/11/19



L1940104-06Lab ID:


MDL

Sample Depth:

Serial_No:09111913:42

Page 71 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Analytical Date:Extraction Method: EPA 3510CExtraction Date: 09/04/19 08:58

09/11/19

Analyst: EK

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.0

5.0

2.0

2.0

2.0

2.0

2.0

2.0

5.0

5.0

5.0

2.0

2.0

2.0

2.0

5.0

2.0

20

2.0

5.0

2.0

2.0

2.0

5.0

3.0

5.0

5.0

5.0

5.0

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier


MDL

0.44

0.50

0.46

0.50

0.44

0.45

0.40

0.43

1.6

1.2

0.93

0.26

0.49

0.38

0.53

0.50

0.66

0.69

0.58

1.2

0.46

0.77

0.42

0.64

1.5

1.2

0.39

1.3

0.38

Serial_No:09111913:42

Page 72 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104



09/11/19

Analyst: EK

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

5.0

2.0

2.0

2.0

2.0

2.0

2.0

2.0

2.0

2.0

2.0

2.0

2.0

2.0

2.0

5.0

5.0

5.0

5.0

2.0

2.0

10

5.0

5.0

2.0

2.0

5.0

5.0

10

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier


MDL

1.8

0.32

0.41

0.35

0.37

0.34

0.46

0.33

0.30

0.41

0.33

0.32

0.40

0.28

0.46

1.1

0.50

0.81

0.80

0.50

0.45

0.44

0.53

0.61

0.35

0.48

0.41

1.8

0.85

Serial_No:09111913:42

Page 73 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104



09/11/19

Analyst: EK

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



Benzoic Acid

Benzyl Alcohol

Carbazole

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

10

20

10

10

5.0

5.0

5.0

5.0

50

2.0

2.0

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier


Total TIC Compounds

Aldol Condensates(A)

Unknown

Unknown

J

J

J

J

72.4

68.7

1.96

1.74

ug/l

ug/l

ug/l

ug/l


MDL

0.67

6.6

1.8

1.8

0.57

0.49

0.48

0.77

2.6

0.59

0.49

Serial_No:09111913:42

Page 74 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104



09/11/19

Analyst: EK



2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

58

45

68

81

70

83

21-120

10-120

23-120

15-120

10-120

41-149


Criteria

MDL

Serial_No:09111913:42

Page 75 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/05/19 10:301,8270D-SIMAnalytical Method:


09/11/19

Analyst: DV

Acenaphthene

2-Chloronaphthalene

Fluoranthene

Hexachlorobutadiene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

2-Methylnaphthalene

Pentachlorophenol

Hexachlorobenzene

Hexachloroethane

Parameter Result

ND

ND

0.03

ND

0.23

ND

ND

ND

ND

ND

ND

0.02

ND

ND

0.04

ND

ND

0.02

0.09

ND

ND

ND

RL

0.10

0.20

0.10

0.50

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.80

0.80

0.80

J

J

J

J

J

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

Semivolatile Organics by GC/MS-SIM - Westborough Lab for sample(s): 03-06 Batch: WG1280001-1

MDL

0.01

0.02

0.02

0.05

0.05

0.02

0.02

0.01

0.01

0.01

0.01

0.01

0.01

0.01

0.02

0.01

0.01

0.02

0.02

0.01

0.01

0.06

Serial_No:09111913:42

Page 76 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/05/19 10:301,8270D-SIMAnalytical Method:


09/11/19

Analyst: DV


Semivolatile Organics by GC/MS-SIM - Westborough Lab for sample(s): 03-06 Batch: WG1280001-1

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

76

60

94

89

97

98

21-120

10-120

23-120

15-120

10-120

41-149


Criteria

MDL

Serial_No:09111913:42

Page 77 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104



09/11/19

Analyst: RC

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

130

160

98

150

160

160

160

160

160

160

160

98

160

160

200

180

160

470

130

150

160

150

130

160

160

160

160

160

160

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

17.

19.

18.

22.

16.

30.

28.

29.

44.

33.

28.

19.

18.

25.

28.

16.

24.

150

26.

21.

20.

24.

19.

25.

57.

41.

31.

56.

15.

Serial_No:09111913:42

Page 78 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104



09/11/19

Analyst: RC

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

160

98

130

98

98

98

130

98

130

160

98

98

130

98

370

160

160

160

160

160

200

160

160

98

160

160

150

160

350

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

34.

18.

40.

28.

26.

17.

25.

32.

19.

16.

20.

19.

23.

16.

38.

30.

32.

31.

68.

16.

20.

17.

20.

31.

24.

19.

26.

54.

62.

Serial_No:09111913:42

Page 79 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104



09/11/19

Analyst: RC

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

230

790

430

130

160

160

240

160

530

160

160

25

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

88

90

97

94

96

94

25-120

10-120

23-120

30-120

10-136

18-120


Criteria

Total TIC Compounds

Unknown

J

J

221

221

ug/kg

ug/kg


MDL

67.

76.

79.

36.

25.

25.

26.

31.

170

50.

16.

7.6

Serial_No:09111913:42

Page 80 of 177

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA

79

85

91

84

93

79

78

78

73

81

98

91

89

92

92

88

93

86

82

88

87

84

88

71

74

82

72

83

68

67

68

65

73

89

79

79

85

78

78

80

79

70

80

80

76

79

37-111

39-98

40-140

40-140

40-140

40-140

40-140

36-97

40-140

48-143

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

11

14

10

15

11

15

15

14

12

10

10

14

12

8

16

12

15

8

16

10

8

10

11

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual Qual

Serial_No:09111913:42

Page 81 of 177




Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

94

85

88

88

90

90

99

90

89

90

90

88

97

92

88

85

90

91

92

88

86

84

92

82

82

82

79

86

81

88

81

74

78

76

77

84

82

74

75

79

78

79

78

75

70

83

29-132

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

45-123

40-140

40-140

40-140

40-140

40-140

40-140

26-127

40-140

40-140

52-143

14

4

7

11

5

11

12

11

18

14

17

13

14

11

17

13

13

15

15

12

14

18

10

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual Qual

Serial_No:09111913:42

Page 82 of 177

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



Benzoic Acid

Benzyl Alcohol

Carbazole

68

70

81

88

88

76

99

98

86

88

82

93

76

89

97

87

67

83

89

99

0

81

90

58

64

73

78

77

69

90

86

75

80

75

85

66

63

88

76

60

74

79

89

0

73

78

25-145

51-143

40-140

40-140

2-134

39-129

30-130

23-97

27-123

30-130

30-130

30-130

10-80

20-130

20-164

9-103

12-110

30-130

30-130

30-130

10-164

26-116

55-144

16

9

10

12

13

10

10

13

14

10

9

9

14

34

10

13

11

11

12

11

NC

10

14

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual

Q

Q Q

Qual

Q

Serial_No:09111913:42

Page 83 of 177

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


726487958990

21-12010-12023-12015-12010-12041-149

635777838080


09/11/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09111913:42

Page 84 of 177

Acenaphthene

2-Chloronaphthalene

Fluoranthene

Hexachlorobutadiene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

2-Methylnaphthalene

Pentachlorophenol

Hexachlorobenzene

Hexachloroethane

87

90

86

78

86

89

88

93

88

89

89

89

103

88

84

103

87

85

89

89

85

76

90

91

85

81

89

88

88

92

88

90

90

88

104

88

85

104

88

84

91

77

87

82

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

3

1

1

4

3

1

0

1

0

1

1

1

1

0

1

1

1

1

2

14

2

8

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Semivolatile Organics by GC/MS-SIM - Westborough Lab Associated sample(s): 03-06 Batch: WG1280001-2 WG1280001-3


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual Qual

Serial_No:09111913:42

Page 85 of 177

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Semivolatile Organics by GC/MS-SIM - Westborough Lab Associated sample(s): 03-06 Batch: WG1280001-2 WG1280001-3


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


786692848482

21-12010-12023-12015-12010-12041-149

796593858381


09/11/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09111913:42

Page 86 of 177

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA

68

63

67

56

70

65

67

66

62

88

84

70

70

70

45

59

63

63

64

63

65

71

70

68

73

67

66

71

80

80

80

64

89

85

72

70

71

52

62

71

70

78

69

69

78

73

31-137

38-107

40-140

40-140

40-140

40-140

40-140

28-104

40-140

40-132

40-140

40-140

40-140

40-140

40-140

40-117

40-140

40-140

40-140

40-140

40-140

40-140

36-157

0

15

0

16

1

21

18

19

3

1

1

3

0

1

14

5

12

11

20

9

6

9

4

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual Qual

Serial_No:09111913:42

Page 87 of 177




Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

67

76

78

69

77

75

75

70

68

76

70

69

72

66

70

72

65

66

70

68

73

58

91

71

75

80

71

77

76

76

70

69

74

69

68

71

68

69

73

65

68

70

70

73

56

91

32-121

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

35-142

37-127

40-140

47-134

6

1

3

3

0

1

1

0

1

3

1

1

1

3

1

1

0

3

0

3

0

4

0

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual Qual

Serial_No:09111913:42

Page 88 of 177

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



Benzoic Acid

Benzyl Alcohol

Carbazole

72

83

72

70

68

66

76

83

63

72

76

81

89

91

98

78

66

65

69

76

58

71

68

75

84

72

71

69

77

75

81

70

74

76

89

96

94

101

78

69

66

70

74

58

78

69

26-129

41-125

40-140

40-140

40-117

14-144

30-130

26-103

25-102

30-130

30-130

30-130

11-114

4-130

10-130

17-109

26-90

30-130.

30-130

30-130

10-110

40-140

54-128

4

1

0

1

1

15

1

2

11

3

0

9

8

3

3

0

4

2

1

3

0

9

1

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual Qual

Serial_No:09111913:42

Page 89 of 177

1,4-Dioxane 54 61 40-140 12 50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


656975757670

25-12010-12023-12030-12010-13618-120

787188747970


09/11/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09111913:42

Page 90 of 177

PCBS

Serial_No:09111913:42

Page 91 of 177

FF

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

38.9

38.9

38.9

38.9

38.9

38.9

38.9

38.9

38.9

38.9


Decachlorobiphenyl


Decachlorobiphenyl

63

35

58

30

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/11/19



L1940104-01Lab ID:




1,8082A09/07/19 17:23HT

EPA 3546



83%Percent Solids:

MDL

3.45

3.89

8.24

5.24

5.83

4.25

7.18

4.94

4.03

3.45

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09111913:42

Page 92 of 177

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

33.5

33.5

33.5

33.5

33.5

33.5

33.5

33.5

33.5

33.5


Decachlorobiphenyl


Decachlorobiphenyl

81

55

77

47

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/11/19



L1940104-02Lab ID:




1,8082A09/07/19 17:35HT

EPA 3546



96%Percent Solids:

MDL

2.97

3.36

7.10

4.52

5.02

3.66

6.19

4.25

3.47

2.97

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09111913:42

Page 93 of 177

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083


Decachlorobiphenyl


Decachlorobiphenyl

64

40

62

38

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/11/19



L1940104-03Lab ID:




1,8082A09/06/19 20:09HT

EPA 3510C



MDL

0.034

0.067

0.046

0.039

0.049

0.039

0.032

0.035

0.034

0.032

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09111913:42

Page 94 of 177

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083


Decachlorobiphenyl


Decachlorobiphenyl

73

51

70

50

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/11/19



L1940104-04Lab ID:




1,8082A09/06/19 20:22HT

EPA 3510C



MDL

0.034

0.067

0.046

0.039

0.049

0.039

0.032

0.035

0.034

0.032

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09111913:42

Page 95 of 177

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083


Decachlorobiphenyl


Decachlorobiphenyl

75

44

72

45

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/11/19



L1940104-05Lab ID:




1,8082A09/06/19 20:36HT

EPA 3510C



MDL

0.034

0.067

0.046

0.039

0.049

0.039

0.032

0.035

0.034

0.032

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09111913:42

Page 96 of 177

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083


Decachlorobiphenyl


Decachlorobiphenyl

82

53

78

52

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/11/19



L1940104-06Lab ID:




1,8082A09/06/19 20:49HT

EPA 3510C



MDL

0.034

0.067

0.046

0.039

0.049

0.039

0.032

0.035

0.034

0.032

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09111913:42

Page 97 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104



Cleanup Method:

EPA 3510C


09/11/19


Analyst: HT

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total

Parameter Result

ND

ND

ND

ND

ND

ND

0.326

ND

ND

0.326

RL

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083

0.083

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier



Decachlorobiphenyl


Decachlorobiphenyl

80

87

76

87

30-150

30-150

30-150

30-150


Criteria



MDL

0.034

0.067

0.046

0.039

0.049

0.039

0.032

0.035

0.034

0.032

Column

A

A

A

A

A

A

A

A

A

A

A

A

B

B

Serial_No:09111913:42

Page 98 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104



Cleanup Method:

EPA 3546


09/11/19


Analyst: WR

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

32.2

32.2

32.2

32.2

32.2

32.2

32.2

32.2

32.2

32.2

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier



Decachlorobiphenyl


Decachlorobiphenyl

85

75

75

59

30-150

30-150

30-150

30-150


Criteria



MDL

2.86

3.22

6.82

4.34

4.83

3.52

5.94

4.09

3.33

2.86

Column

A

A

A

A

A

A

A

A

A

A

A

A

B

B

Serial_No:09111913:42

Page 99 of 177

Aroclor 1016

Aroclor 1260

77

86

88

89

40-140

40-140

13

3

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


70957198

30-15030-15030-15030-150

AABB

9310287101


09/11/19

AcceptanceCriteria


A

A

Serial_No:09111913:42

Page 100 of 177

Aroclor 1016

Aroclor 1260

81

83

82

87

40-140

40-140

1

5

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


84728168

30-15030-15030-15030-150

AABB

83768269


09/11/19

AcceptanceCriteria


A

A

Serial_No:09111913:42

Page 101 of 177

PESTICIDES

Serial_No:09111913:42

Page 102 of 177

FF

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

JIP

JIP

IP

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

2.98

2.60

1.66

ND

ND

ND

ND

ND

0.946

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

1.86

0.777

0.777

1.86

0.932

1.86

3.50

0.777

2.33

1.86

1.16

1.86

1.86

3.50

1.86

1.86

0.777

3.50

35.0

2.33

2.33

15.1

09/11/19



L1940104-01Lab ID:




1,8081B09/09/19 13:25BM

EPA 3546



MDL

0.365

0.347

0.221

0.707

0.418

0.656

1.05

0.318

0.816

0.480

0.583

0.431

0.665

1.50

0.440

0.623

0.370

1.09

9.79

0.649

0.615

6.18

A

A

A

A

A

A

A

A

A

A

A

B

B

A

A

A

A

A

A

B

B

A

Column

Sample Depth:

Serial_No:09111913:42

Page 103 of 177



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Decachlorobiphenyl


Decachlorobiphenyl

98

93

89

67

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/11/19



L1940104-01Lab ID:


MDL Column

Sample Depth:

Serial_No:09111913:42

Page 104 of 177

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

1.59

0.661

0.661

1.59

0.794

1.59

2.98

0.661

1.98

1.59

0.992

1.59

1.59

2.98

1.59

1.59

0.661

2.98

29.8

1.98

1.98

12.9

09/11/19



L1940104-02Lab ID:




1,8081B09/09/19 13:37BM

EPA 3546



MDL

0.311

0.296

0.188

0.602

0.356

0.559

0.893

0.271

0.694

0.409

0.496

0.367

0.566

1.28

0.375

0.530

0.315

0.926

8.33

0.553

0.524

5.26

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09111913:42

Page 105 of 177



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Decachlorobiphenyl


Decachlorobiphenyl

113

127

98

64

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/11/19



L1940104-02Lab ID:


MDL Column

Sample Depth:

Serial_No:09111913:42

Page 106 of 177

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.014

0.014

0.014

0.014

0.014

0.014

0.014

0.029

0.029

0.029

0.029

0.029

0.029

0.029

0.014

0.029

0.029

0.143

0.143

0.014

0.014

0.143

09/11/19



L1940104-03Lab ID:




1,8081B09/09/19 01:42BM


MDL

0.003

0.003

0.003

0.004

0.002

0.002

0.003

0.003

0.006

0.003

0.003

0.003

0.003

0.003

0.002

0.004

0.003

0.005

0.045

0.005

0.004

0.033

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09111913:42

Page 107 of 177



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Decachlorobiphenyl


Decachlorobiphenyl

87

25

77

55

30-150

30-150

30-150

30-150

Acceptance Criteria

Q

A

A

B

B


09/11/19



L1940104-03Lab ID:


MDL Column

Sample Depth:

Serial_No:09111913:42

Page 108 of 177

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.014

0.014

0.014

0.014

0.014

0.014

0.014

0.029

0.029

0.029

0.029

0.029

0.029

0.029

0.014

0.029

0.029

0.143

0.143

0.014

0.014

0.143

09/11/19



L1940104-04Lab ID:




1,8081B09/09/19 01:55BM


MDL

0.003

0.003

0.003

0.004

0.002

0.002

0.003

0.003

0.006

0.003

0.003

0.003

0.003

0.003

0.002

0.004

0.003

0.005

0.045

0.005

0.004

0.033

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09111913:42

Page 109 of 177



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Decachlorobiphenyl


Decachlorobiphenyl

80

23

81

74

30-150

30-150

30-150

30-150

Acceptance Criteria

Q

A

A

B

B


09/11/19



L1940104-04Lab ID:


MDL Column

Sample Depth:

Serial_No:09111913:42

Page 110 of 177

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.014

0.014

0.014

0.014

0.014

0.014

0.014

0.029

0.029

0.029

0.029

0.029

0.029

0.029

0.014

0.029

0.029

0.143

0.143

0.014

0.014

0.143

09/11/19



L1940104-05Lab ID:




1,8081B09/09/19 02:07BM


MDL

0.003

0.003

0.003

0.004

0.002

0.002

0.003

0.003

0.006

0.003

0.003

0.003

0.003

0.003

0.002

0.004

0.003

0.005

0.045

0.005

0.004

0.033

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09111913:42

Page 111 of 177



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Decachlorobiphenyl


Decachlorobiphenyl

75

21

77

54

30-150

30-150

30-150

30-150

Acceptance Criteria

Q

A

A

B

B


09/11/19



L1940104-05Lab ID:


MDL Column

Sample Depth:

Serial_No:09111913:42

Page 112 of 177

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

0.014

0.014

0.014

0.014

0.014

0.014

0.014

0.029

0.029

0.029

0.029

0.029

0.029

0.029

0.014

0.029

0.029

0.143

0.143

0.014

0.014

0.143

09/11/19



L1940104-06Lab ID:




1,8081B09/09/19 02:20BM


MDL

0.003

0.003

0.003

0.004

0.002

0.002

0.003

0.003

0.006

0.003

0.003

0.003

0.003

0.003

0.002

0.004

0.003

0.005

0.045

0.005

0.004

0.033

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09111913:42

Page 113 of 177



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


Decachlorobiphenyl


Decachlorobiphenyl

65

26

69

59

30-150

30-150

30-150

30-150

Acceptance Criteria

Q

A

A

B

B


09/11/19



L1940104-06Lab ID:


MDL Column

Sample Depth:

Serial_No:09111913:42

Page 114 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104



09/11/19

Analyst: SL

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

0.014

0.014

0.014

0.014

0.014

0.014

0.014

0.029

0.029

0.029

0.029

0.029

0.029

0.029

0.014

0.029

0.029

0.143

0.143

0.014

0.014

0.143

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier


MDL

0.003

0.003

0.003

0.004

0.002

0.002

0.003

0.003

0.006

0.003

0.003

0.003

0.003

0.003

0.002

0.004

0.003

0.005

0.045

0.005

0.004

0.033

Column

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:09111913:42

Page 115 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104



09/11/19

Analyst: SL




Decachlorobiphenyl


Decachlorobiphenyl

76

79

79

116

30-150

30-150

30-150

30-150


Criteria

MDL Column

A

A

B

B

Serial_No:09111913:42

Page 116 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104



Cleanup Method:

EPA 3546


09/11/19

Analyst: BM

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.59

0.662

0.662

1.59

0.794

1.59

2.98

0.662

1.98

1.59

0.993

1.59

1.59

2.98

1.59

1.59

0.662

2.98

29.8

1.98

1.98

12.9

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier



MDL

0.311

0.296

0.188

0.602

0.356

0.559

0.893

0.271

0.695

0.409

0.496

0.367

0.566

1.28

0.375

0.531

0.315

0.926

8.34

0.553

0.524

5.26

Column

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:09111913:42

Page 117 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104



Cleanup Method:

EPA 3546


09/11/19

Analyst: BM




Decachlorobiphenyl


Decachlorobiphenyl

105

135

91

70

30-150

30-150

30-150

30-150


Criteria


MDL Column

B

B

A

A

Serial_No:09111913:42

Page 118 of 177

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

cis-Chlordane

trans-Chlordane

52

70

69

75

69

67

74

78

62

81

76

68

75

76

75

72

66

86

73

70

66

89

88

91

87

83

92

97

76

101

93

85

97

96

90

90

82

95

93

87

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

24

23

24

20

22

21

21

22

19

22

21

22

25

24

18

22

21

10

24

21

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual Qual

Q

Q

Q

Q

Q

Q

Q

Q

Q

Q

Q

Q

Q

Q

Q

Q

Column

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:09111913:42

Page 119 of 177

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


65726897

30-15030-15030-15030-150

AABB

829088129


09/11/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09111913:42

Page 120 of 177

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

cis-Chlordane

trans-Chlordane

88

88

88

86

73

75

84

88

61

89

86

77

88

92

73

87

84

76

69

82

82

83

82

83

67

72

80

84

59

86

82

75

83

86

70

82

79

73

67

79

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

7

6

7

4

9

4

5

5

3

3

5

3

6

7

4

6

6

4

3

4

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19


A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:09111913:42

Page 121 of 177

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104


981098250

30-15030-15030-15030-150

BBAA

90917743


09/11/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09111913:42

Page 122 of 177

METALS

Serial_No:09111913:42

Page 123 of 177

FF

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

SAMPLE RESULTS


Matrix: Soil


L1940104-01Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

1370

ND

3.10

31.3

ND

0.257

176000

6.09

2.07

12.5

7940

109

91300

224

ND

5.08

200

ND

ND

65.4

ND

7.51

30.2

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

20

2

2

2

2

2

20

2

1

2

2

2

2

2

2

2

2

9.52

4.76

0.952

0.952

0.476

0.952

95.2

0.952

1.90

0.952

4.76

4.76

95.2

0.952

0.076

2.38

238

1.90

0.952

190

1.90

0.952

4.76

09/09/19 15:07

09/09/19 15:07

09/09/19 15:07

09/09/19 15:07

09/09/19 15:07

09/09/19 15:07

09/09/19 16:03

09/09/19 15:07

09/09/19 15:07

09/09/19 15:07

09/09/19 15:07

09/09/19 15:07

09/09/19 16:03

09/09/19 15:07

09/09/19 20:39

09/09/19 15:07

09/09/19 15:07

09/09/19 15:07

09/09/19 15:07

09/09/19 15:07

09/09/19 15:07

09/09/19 15:07

09/09/19 15:07

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

GD

LC

LC

LC

LC

LC

LC

LC

LC

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 18:00

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 83%

MDL

2.57

0.362

0.198

0.166

0.031

0.093

33.3

0.091

0.158

0.246

0.860

0.255

14.7

0.151

0.050

0.230

13.7

0.246

0.270

3.00

0.300

0.193

0.279

Sample Depth:

Serial_No:09111913:42

Page 124 of 177

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

SAMPLE RESULTS


Matrix: Soil


L1940104-02Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

J

J

2610

ND

0.565

22.2

0.106

0.172

478

9.54

2.99

9.49

6070

1.93

928

207

ND

7.40

273

ND

ND

59.6

ND

10.2

10.2

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

8.19

4.09

0.819

0.819

0.409

0.819

8.19

0.819

1.64

0.819

4.09

4.09

8.19

0.819

0.065

2.05

205

1.64

0.819

164

1.64

0.819

4.09

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 20:41

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

09/09/19 15:11

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

GD

LC

LC

LC

LC

LC

LC

LC

LC

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 18:00

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 96%

MDL

2.21

0.311

0.170

0.142

0.027

0.080

2.87

0.079

0.136

0.211

0.739

0.219

1.26

0.130

0.043

0.198

11.8

0.211

0.232

2.58

0.258

0.166

0.240

Sample Depth:

Serial_No:09111913:42

Page 125 of 177

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

SAMPLE RESULTS


Matrix: Water


L1940104-03Lab ID:



DateAnalyzed


Date Prepared


Dissolved Metals - Mansfield Lab

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

Aluminum, Dissolved

Antimony, Dissolved

Arsenic, Dissolved

Barium, Dissolved

Beryllium, Dissolved

J

J

J

61.5

0.00056

0.01294

0.9021

0.00341

0.00120

54.6

0.6426

0.2029

0.2764

216.

0.09066

30.3

13.57

ND

0.5504

26.2

0.0210

0.00021

201.

0.00135

0.1281

0.2672

ND

ND

0.00022

0.06207

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.0100

0.00400

0.00050

0.00050

0.00050

0.00020

0.100

0.00100

0.00050

0.00100

0.0500

0.00100

0.0700

0.00100

0.00020

0.00200

0.100

0.00500

0.00040

0.100

0.00050

0.00500

0.01000

0.0100

0.00400

0.00050

0.00050

0.00050

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 18:44

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 10:26

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,7470A

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AL

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/10/19 11:47

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 7470A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

PrepMethodMDL

0.00327

0.00042

0.00016

0.00017

0.00010

0.00005

0.0394

0.00017

0.00016

0.00038

0.0191

0.00034

0.0242

0.00044

0.00009

0.00055

0.0309

0.00173

0.00016

0.0293

0.00014

0.00157

0.00341

0.00327

0.00042

0.00016

0.00017

0.00010

Sample Depth:

Serial_No:09111913:42

Page 126 of 177

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

SAMPLE RESULTS


Matrix: Water


L1940104-03Lab ID:



DateAnalyzed


Date Prepared

Cadmium, Dissolved

Calcium, Dissolved

Chromium, Dissolved

Cobalt, Dissolved

Copper, Dissolved

Iron, Dissolved

Lead, Dissolved

Magnesium, Dissolved

Manganese, Dissolved

Mercury, Dissolved

Nickel, Dissolved

Potassium, Dissolved

Selenium, Dissolved

Silver, Dissolved

Sodium, Dissolved

Thallium, Dissolved

Vanadium, Dissolved

Zinc, Dissolved

J

J

J

J

0.00015

46.2

ND

0.02447

0.00080

ND

ND

9.07

5.307

ND

0.04867

12.0

0.00237

ND

217.

0.00016

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.00020

0.100

0.00100

0.00050

0.00100

0.0500

0.00100

0.0700

0.00100

0.00020

0.00200

0.100

0.00500

0.00040

0.100

0.00100

0.00500

0.01000

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

09/10/19 20:43

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

09/10/19 19:55

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,7470A

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

AM

AM

AM

AM

AM

AM

AM

AM

AM

AL

AM

AM

AM

AM

AM

AM

AM

AM

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 15:11

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 7470A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

PrepMethodMDL

0.00005

0.0394

0.00017

0.00016

0.00038

0.0191

0.00034

0.0242

0.00044

0.00009

0.00055

0.0309

0.00173

0.00016

0.0293

0.00014

0.00157

0.00341

Sample Depth:

Serial_No:09111913:42

Page 127 of 177

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

SAMPLE RESULTS


Matrix: Water


L1940104-04Lab ID:



DateAnalyzed


Date Prepared



Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

Aluminum, Dissolved

Antimony, Dissolved

Arsenic, Dissolved

Barium, Dissolved


J

J

J

J

78.9

0.00043

0.01668

1.627

0.00433

0.00188

213.

0.8473

0.2728

0.3540

269.

0.3851

54.2

20.25

ND

0.7777

24.8

0.0284

0.00036

420.

0.00212

0.1149

0.3678

0.00490

ND

0.00025

0.2323

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.0100

0.00400

0.00050

0.00050

0.00050

0.00020

0.100

0.00100

0.00050

0.00100

0.0500

0.00100

0.0700

0.00100

0.00020

0.00200

0.100

0.00500

0.00040

0.100

0.00050

0.00500

0.01000

0.0100

0.00400

0.00050

0.00050

0.00050

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 18:46

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 10:30

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,7470A

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AL

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/10/19 11:47

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 7470A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

PrepMethodMDL

0.00327

0.00042

0.00016

0.00017

0.00010

0.00005

0.0394

0.00017

0.00016

0.00038

0.0191

0.00034

0.0242

0.00044

0.00009

0.00055

0.0309

0.00173

0.00016

0.0293

0.00014

0.00157

0.00341

0.00327

0.00042

0.00016

0.00017

0.00010

Sample Depth:

Serial_No:09111913:42

Page 128 of 177

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

SAMPLE RESULTS


Matrix: Water


L1940104-04Lab ID:



DateAnalyzed


Date Prepared

Cadmium, Dissolved

Calcium, Dissolved

Chromium, Dissolved

Cobalt, Dissolved

Copper, Dissolved

Iron, Dissolved

Lead, Dissolved



Mercury, Dissolved

Nickel, Dissolved


Selenium, Dissolved

Silver, Dissolved

Sodium, Dissolved

Thallium, Dissolved

Vanadium, Dissolved

Zinc, Dissolved

J

J

J

0.00019

173.

ND

0.02893

0.00130

0.0290

ND

23.8

7.655

ND

0.06738

8.63

ND

ND

424.

0.00027

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.00020

0.100

0.00100

0.00050

0.00100

0.0500

0.00100

0.0700

0.00100

0.00020

0.00200

0.100

0.00500

0.00040

0.100

0.00100

0.00500

0.01000

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

09/10/19 20:49

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

09/10/19 19:50

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,7470A

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

AM

AM

AM

AM

AM

AM

AM

AM

AM

AL

AM

AM

AM

AM

AM

AM

AM

AM

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 15:11

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 7470A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

PrepMethodMDL

0.00005

0.0394

0.00017

0.00016

0.00038

0.0191

0.00034

0.0242

0.00044

0.00009

0.00055

0.0309

0.00173

0.00016

0.0293

0.00014

0.00157

0.00341

Sample Depth:

Serial_No:09111913:42

Page 129 of 177

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

SAMPLE RESULTS


Matrix: Water


L1940104-05Lab ID:



DateAnalyzed


Date Prepared



Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

Aluminum, Dissolved

Antimony, Dissolved

Arsenic, Dissolved

Barium, Dissolved


J

J

J

57.0

ND

0.01144

0.9322

0.00323

0.00130

66.8

0.3603

0.2180

0.2046

183.

0.1185

34.4

15.94

ND

0.5609

23.9

0.0215

0.00019

214.

0.00152

0.1080

0.2732

0.00698

ND

0.00030

0.09091

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.0100

0.00400

0.00050

0.00050

0.00050

0.00020

0.100

0.00100

0.00050

0.00100

0.0500

0.00100

0.0700

0.00100

0.00020

0.00200

0.100

0.00500

0.00040

0.100

0.00050

0.00500

0.01000

0.0100

0.00400

0.00050

0.00050

0.00050

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 18:48

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 10:35

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,7470A

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AL

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/10/19 11:47

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 7470A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

PrepMethodMDL

0.00327

0.00042

0.00016

0.00017

0.00010

0.00005

0.0394

0.00017

0.00016

0.00038

0.0191

0.00034

0.0242

0.00044

0.00009

0.00055

0.0309

0.00173

0.00016

0.0293

0.00014

0.00157

0.00341

0.00327

0.00042

0.00016

0.00017

0.00010

Sample Depth:

Serial_No:09111913:42

Page 130 of 177

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

SAMPLE RESULTS


Matrix: Water


L1940104-05Lab ID:



DateAnalyzed


Date Prepared

Cadmium, Dissolved

Calcium, Dissolved

Chromium, Dissolved

Cobalt, Dissolved

Copper, Dissolved

Iron, Dissolved

Lead, Dissolved



Mercury, Dissolved

Nickel, Dissolved


Selenium, Dissolved

Silver, Dissolved

Sodium, Dissolved

Thallium, Dissolved

Vanadium, Dissolved

Zinc, Dissolved

J

J

J

J

J

0.00016

61.4

ND

0.02265

0.00058

0.0282

ND

11.2

5.950

ND

0.05422

6.45

0.00209

ND

210.

0.00025

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.00020

0.100

0.00100

0.00050

0.00100

0.0500

0.00100

0.0700

0.00100

0.00020

0.00200

0.100

0.00500

0.00040

0.100

0.00100

0.00500

0.01000

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

09/10/19 20:51

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

09/10/19 19:46

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,7470A

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

AM

AM

AM

AM

AM

AM

AM

AM

AM

AL

AM

AM

AM

AM

AM

AM

AM

AM

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 15:11

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 7470A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

PrepMethodMDL

0.00005

0.0394

0.00017

0.00016

0.00038

0.0191

0.00034

0.0242

0.00044

0.00009

0.00055

0.0309

0.00173

0.00016

0.0293

0.00014

0.00157

0.00341

Sample Depth:

Serial_No:09111913:42

Page 131 of 177

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

SAMPLE RESULTS


Matrix: Water


L1940104-06Lab ID:



DateAnalyzed


Date Prepared



Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

Aluminum, Dissolved

Antimony, Dissolved

Arsenic, Dissolved

Barium, Dissolved


J

J

J

60.5

ND

0.01119

1.152

0.00308

0.00120

76.0

0.4719

0.2135

0.2575

194.

0.09840

34.7

19.00

ND

0.9078

21.8

0.0190

0.00018

193.

0.00211

0.1144

0.2587

0.00388

ND

0.00022

0.08794

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.0100

0.00400

0.00050

0.00050

0.00050

0.00020

0.100

0.00100

0.00050

0.00100

0.0500

0.00100

0.0700

0.00100

0.00020

0.00200

0.100

0.00500

0.00040

0.100

0.00050

0.00500

0.01000

0.0100

0.00400

0.00050

0.00050

0.00050

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 18:49

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 10:55

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,7470A

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AL

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/10/19 11:47

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 7470A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

PrepMethodMDL

0.00327

0.00042

0.00016

0.00017

0.00010

0.00005

0.0394

0.00017

0.00016

0.00038

0.0191

0.00034

0.0242

0.00044

0.00009

0.00055

0.0309

0.00173

0.00016

0.0293

0.00014

0.00157

0.00341

0.00327

0.00042

0.00016

0.00017

0.00010

Sample Depth:

Serial_No:09111913:42

Page 132 of 177

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

SAMPLE RESULTS


Matrix: Water


L1940104-06Lab ID:



DateAnalyzed


Date Prepared

Cadmium, Dissolved

Calcium, Dissolved

Chromium, Dissolved

Cobalt, Dissolved

Copper, Dissolved

Iron, Dissolved

Lead, Dissolved



Mercury, Dissolved

Nickel, Dissolved


Selenium, Dissolved

Silver, Dissolved

Sodium, Dissolved

Thallium, Dissolved

Vanadium, Dissolved

Zinc, Dissolved

J

J

J

0.00014

67.2

ND

0.01795

0.00277

ND

ND

12.9

5.856

ND

0.05848

6.71

0.00324

ND

202.

0.00016

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.00020

0.100

0.00100

0.00050

0.00100

0.0500

0.00100

0.0700

0.00100

0.00020

0.00200

0.100

0.00500

0.00040

0.100

0.00100

0.00500

0.01000

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

09/10/19 20:53

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

09/10/19 20:00

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,7470A

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

AM

AM

AM

AM

AM

AM

AM

AM

AM

AL

AM

AM

AM

AM

AM

AM

AM

AM

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 15:11

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 7470A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

PrepMethodMDL

0.00005

0.0394

0.00017

0.00016

0.00038

0.0191

0.00034

0.0242

0.00044

0.00009

0.00055

0.0309

0.00173

0.00016

0.0293

0.00014

0.00157

0.00341

Sample Depth:

Serial_No:09111913:42

Page 133 of 177

FF

Parameter

Parameter

Result

Result

Dilution Factor

Dilution Factor

Qualifier

Qualifier

Units

Units

RL

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

DateAnalyzed

DateAnalyzed

AnalyticalMethod

AnalyticalMethod

Analyst

Analyst

Date Prepared

Date Prepared

09/11/19

Mercury, Total

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

ND

ND

ND

0.092

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.083

4.00

2.00

0.400

0.400

0.200

0.400

4.00

0.400

0.800

0.400

2.00

2.00

4.00

0.400

1.00

100

0.800

0.400

80.0

0.800

0.400

2.00

09/09/19 19:56

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

09/09/19 13:39

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

GD

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

09/06/19 18:00

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15

09/06/19 21:15




Prep Information

MDL

MDL

0.054

1.08

0.152

0.083

0.070

0.013

0.039

1.40

0.038

0.066

0.103

0.361

0.107

0.616

0.064

0.097

5.76

0.103

0.113

1.26

0.126

0.081

0.117

Serial_No:09111913:42

Page 134 of 177



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

DateAnalyzed


Date Prepared

09/11/19

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.00019

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.0100

0.00400

0.00050

0.00050

0.00050

0.00020

0.100

0.00100

0.00050

0.00100

0.0500

0.00100

0.0700

0.00100

0.00200

0.100

0.00500

0.00040

0.100

0.00050

0.00500

0.01000

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

09/10/19 09:58

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40

09/09/19 19:40


EPA 3050B

EPA 3005A

Digestion Method:

Digestion Method:

Prep Information

Prep Information

MDL

0.00327

0.00042

0.00016

0.00017

0.00010

0.00005

0.0394

0.00017

0.00016

0.00038

0.0191

0.00034

0.0242

0.00044

0.00055

0.0309

0.00173

0.00016

0.0293

0.00014

0.00157

0.00341

Serial_No:09111913:42

Page 135 of 177

Parameter

Parameter

Parameter

Result

Result

Result

Dilution Factor

Dilution Factor

Dilution Factor

Qualifier

Qualifier

Qualifier

Units

Units

Units

RL

RL

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

DateAnalyzed

DateAnalyzed

DateAnalyzed

AnalyticalMethod

AnalyticalMethod

AnalyticalMethod

Analyst

Analyst

Analyst

Date Prepared

Date Prepared

Date Prepared

09/11/19

Mercury, Total

Mercury, Dissolved

Aluminum, Dissolved

Antimony, Dissolved

Arsenic, Dissolved

Barium, Dissolved


Cadmium, Dissolved

Calcium, Dissolved

Chromium, Dissolved

Cobalt, Dissolved

Copper, Dissolved

Iron, Dissolved

Lead, Dissolved



Nickel, Dissolved

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.00020

0.00020

0.0100

0.00400

0.00050

0.00050

0.00050

0.00020

0.100

0.00100

0.00050

0.00100

0.0500

0.00100

0.0700

0.00100

0.00200

09/10/19 18:25

09/10/19 20:35

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

1,7470A

1,7470A

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

AL

AL

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

09/10/19 11:47

09/10/19 15:11

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20


Dissolved Metals - Mansfield Lab for sample(s): 03-06 Batch: WG1282346-1

Dissolved Metals - Mansfield Lab for sample(s): 03-06 Batch: WG1282377-1

EPA 7470A

EPA 7470A

Digestion Method:

Digestion Method:

Prep Information

Prep Information

MDL

MDL

MDL

0.00009

0.00009

0.00327

0.00042

0.00016

0.00017

0.00010

0.00005

0.0394

0.00017

0.00016

0.00038

0.0191

0.00034

0.0242

0.00044

0.00055

Serial_No:09111913:42

Page 136 of 177


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19


Selenium, Dissolved

Silver, Dissolved

Sodium, Dissolved

Thallium, Dissolved

Vanadium, Dissolved

Zinc, Dissolved

J

ND

ND

ND

ND

0.00028

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

0.100

0.00500

0.00040

0.100

0.00100

0.00500

0.01000

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

09/10/19 20:18

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

1,6020B

AM

AM

AM

AM

AM

AM

AM

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

09/10/19 16:20

EPA 3005ADigestion Method:

Prep Information

0.0309

0.00173

0.00016

0.0293

0.00014

0.00157

0.00341

Serial_No:09111913:42

Page 137 of 177

Mercury, Total 76 - 60-141 -

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual Qual

Serial_No:09111913:42

Page 138 of 177

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

56

136

99

89

96

96

82

89

91

94

76

90

76

99

92

72

95

92

96

94

88

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

51-149

19-249

70-130

75-125

75-125

75-125

73-127

70-130

75-125

75-125

38-162

71-128

63-137

76-124

70-131

60-140

63-137

69-131

37-162

68-132

65-135

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Serial_No:09111913:42

Page 139 of 177

Zinc, Total 93 - 70-130 -

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Serial_No:09111913:42

Page 140 of 177

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

98

88

109

104

98

105

104

101

103

99

116

108

97

99

103

96

105

99

98

108

102

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Total Metals - Mansfield Lab Associated sample(s): 03-06 Batch: WG1281987-2


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Serial_No:09111913:42

Page 141 of 177

Zinc, Total

Mercury, Total

Mercury, Dissolved

105

88

94

-

-

-

80-120

80-120

80-120

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Dissolved Metals - Mansfield Lab Associated sample(s): 03-06 Batch: WG1282346-2


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Serial_No:09111913:42

Page 142 of 177

Aluminum, Dissolved

Antimony, Dissolved

Arsenic, Dissolved

Barium, Dissolved


Cadmium, Dissolved

Calcium, Dissolved

Chromium, Dissolved

Cobalt, Dissolved

Copper, Dissolved

Iron, Dissolved

Lead, Dissolved



Nickel, Dissolved


Selenium, Dissolved

Silver, Dissolved

Sodium, Dissolved

Thallium, Dissolved

Vanadium, Dissolved

101

83

100

104

103

108

107

100

100

97

112

105

100

98

99

101

104

101

101

105

102

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Serial_No:09111913:42

Page 143 of 177

Zinc, Dissolved 104 - 80-120 -

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Serial_No:09111913:42

Page 144 of 177

Mercury, Total ND ND 0 - - 80-120 - 20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 01-02 QC Batch ID: WG1281257-3 QC Sample: L1900009-64 Client ID: MS Sample

0.147

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual

Q

Qual Qual

Serial_No:09111913:42

Page 145 of 177

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

4660

1.51J

6.04

149

0.189J

0.890

38500

12.7

4.92

23.6

16600

583

2200

258

9.53

755

ND

ND

331

ND

19.3

5400

41.5

16.6

358

4.15

4.70

37200

29.7

41.1

45.1

13600

450

9320

263

46.1

1580

10.0

25.5

1190

7.99

63.0

412

92

98

116

92

83

0

95

80

96

0

0

793

11

81

92

93

95

96

74

97

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits


180

44.9

10.8

180

4.49

4.58

898

18

44.9

22.4

89.8

45.8

898

44.9

44.9

898

10.8

26.9

898

10.8

44.9

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Q

Q

Q

Q

Q

Q

Q

Serial_No:09111913:42

Page 146 of 177

Zinc, Total 249 273 53 - - 75-125 - 20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits


44.9

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Q

Serial_No:09111913:42

Page 147 of 177

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

0.081

0.0006J

0.0006

0.0106

ND

0.00008J

267

0.0002J

ND

0.0008J

0.230

ND

272

0.04144

0.0014J

2.90

ND

ND

641.

0.0003J

ND

2.04

0.5402

0.1326

2.100

0.05203

0.05658

316

0.2029

0.5302

0.2598

1.40

0.5532

288

0.5402

0.5252

13.0

0.135

0.05058

671

0.1324

0.5230

98

108

110

104

104

111

490

101

106

104

117

108

160

100

105

101

112

101

300

110

105

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits


2

0.5

0.12

2

0.05

0.051

10

0.2

0.5

0.25

1

0.51

10

0.5

0.5

10

0.12

0.05

10

0.12

0.5

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Q

Q

Q

Serial_No:09111913:42

Page 148 of 177

Zinc, Total

Mercury, Total

Mercury, Dissolved

0.0082J

ND

ND

0.5550

0.00467

0.00447

111

93

89

-

-

-

-

-

-

75-125

75-125

75-125

-

-

-

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits



Dissolved Metals - Mansfield Lab Associated sample(s): 03-06 QC Batch ID: WG1282346-3 QC Sample: L1940104-03 Client ID: TW-1

0.5

0.005

0.005

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Serial_No:09111913:42

Page 149 of 177

Aluminum, Dissolved

Antimony, Dissolved

Arsenic, Dissolved

Barium, Dissolved


Cadmium, Dissolved

Calcium, Dissolved

Chromium, Dissolved

Cobalt, Dissolved

Copper, Dissolved

Iron, Dissolved

Lead, Dissolved



Nickel, Dissolved


Selenium, Dissolved

Silver, Dissolved

Sodium, Dissolved

Thallium, Dissolved

Vanadium, Dissolved

0.00490J

ND

0.00025J

0.2323

ND

0.00019J

173.

ND

0.02893

0.00130

0.0290J

ND

23.8

7.655

0.06738

8.63

ND

ND

424.

0.00027J

ND

1.97

0.4988

0.1311

2.294

0.05137

0.05534

199

0.1955

0.5326

0.2431

1.16

0.5305

32.9

7.912

0.5646

18.8

0.138

0.04944

438

0.1239

0.5038

98

100

109

103

103

108

260

98

101

97

116

104

91

51

99

102

115

99

140

103

101

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits


2

0.5

0.12

2

0.05

0.051

10

0.2

0.5

0.25

1

0.51

10

0.5

0.5

10

0.12

0.05

10

0.12

0.5

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Q

Q

Q

Serial_No:09111913:42

Page 150 of 177

Zinc, Dissolved ND 0.5363 107 - - 75-125 - 20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits


0.5

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Serial_No:09111913:42

Page 151 of 177

Mercury, Total ND ND mg/kg NC 20


Total Metals - Mansfield Lab Associated sample(s): 01-02 QC Batch ID: WG1281257-4 QC Sample: L1900009-64 Client ID: DUP Sample


10831

Project Name:

Project Number:

L1940104Lab Number:

Report Date:


09/11/19

Qual

Serial_No:09111913:42

Page 152 of 177

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Silver, Total

Thallium, Total

Vanadium, Total

Zinc, Total

4660

1.51J

6.04

149

0.189J

0.890

12.7

4.92

23.6

16600

583

258

9.53

ND

ND

ND

19.3

249

5410

1.31J

5.51

202

0.246

0.799

13.7

4.69

25.4

12100

386

255

10.2

ND

ND

ND

21.5

233

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

15

NC

9

30

NC

11

8

5

7

31

41

1

7

NC

NC

NC

11

7

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20




10831

Project Name:

Project Number:

L1940104Lab Number:

Report Date:


09/11/19

Q

Q

Q

Serial_No:09111913:42

Page 153 of 177

Cadmium, Total

Iron, Total

Lead, Total

Manganese, Total

Potassium, Total

Sodium, Total

Mercury, Total

Mercury, Dissolved

0.00008J

0.230

ND

0.04144

2.90

641.

ND

ND

0.00007J

0.240

ND

0.04213

2.76

625

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

NC

4

NC

2

5

3

NC

NC

20

20

20

20

20

20

20

20






10831

Project Name:

Project Number:

L1940104Lab Number:

Report Date:


09/11/19

Serial_No:09111913:42

Page 154 of 177

Aluminum, Dissolved

Antimony, Dissolved

Arsenic, Dissolved

Barium, Dissolved


Cadmium, Dissolved

Calcium, Dissolved

Chromium, Dissolved

Cobalt, Dissolved

Copper, Dissolved

Iron, Dissolved

Lead, Dissolved



Nickel, Dissolved


Selenium, Dissolved

Silver, Dissolved

Sodium, Dissolved

0.00698J

ND

0.00030J

0.09091

ND

0.00016J

61.4

ND

0.02265

0.00058J

0.0282J

ND

11.2

5.950

0.05422

6.45

0.00209J

ND

210.

0.00724J

0.00062J

0.00032J

0.08997

ND

0.00018J

62.4

ND

0.02236

0.00051J

0.0359J

ND

11.2

5.914

0.05157

6.50

0.00205J

ND

209

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

NC

NC

NC

1

NC

NC

2

NC

1

NC

NC

NC

0

1

5

1

NC

NC

0

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20




10831

Project Name:

Project Number:

L1940104Lab Number:

Report Date:


09/11/19

Serial_No:09111913:42

Page 155 of 177

Thallium, Dissolved

Vanadium, Dissolved

Zinc, Dissolved

0.00025J

ND

ND

0.00066J

ND

ND

mg/l

mg/l

mg/l

NC

NC

NC

20

20

20




10831

Project Name:

Project Number:

L1940104Lab Number:

Report Date:


09/11/19

Serial_No:09111913:42

Page 156 of 177

INORGANICS&

MISCELLANEOUS

Serial_No:09111913:42

Page 157 of 177

FF



Matrix: Soil


L1940104-01Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

83.0

ND

%

mg/kg

1

1

0.100

1.2

09/05/19 03:30

09/06/19 12:39

121,2540G

1,9010C/9012B

YA

ML

Date Prepared

-

09/05/19 15:15

09/11/19

MDL

NA

0.25

Sample Depth:

Serial_No:09111913:42

Page 158 of 177

FF



Matrix: Soil


L1940104-02Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

96.0

ND

%

mg/kg

1

1

0.100

1.0

09/05/19 03:30

09/06/19 12:40

121,2540G

1,9010C/9012B

YA

ML

Date Prepared

-

09/05/19 15:15

09/11/19

MDL

NA

0.22

Sample Depth:

Serial_No:09111913:42

Page 159 of 177

FF



Matrix: Water


L1940104-03Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

Field Prep:

DateAnalyzed


Not Specified

General Chemistry - Westborough LabCyanide, Total ND mg/l 10.005 09/09/19 11:34 1,9010C/9012B LH

Date Prepared

09/07/19 09:10

09/11/19

MDL

0.001

Sample Depth:

Serial_No:09111913:42

Page 160 of 177

FF



Matrix: Water


L1940104-04Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

Field Prep:

DateAnalyzed


Not Specified

General Chemistry - Westborough LabCyanide, Total J0.002 mg/l 10.005 09/09/19 11:37 1,9010C/9012B LH

Date Prepared

09/07/19 09:10

09/11/19

MDL

0.001

Sample Depth:

Serial_No:09111913:42

Page 161 of 177

FF



Matrix: Water


L1940104-05Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

09/07/19 09:10

09/11/19

MDL

0.001

Sample Depth:

Serial_No:09111913:42

Page 162 of 177

FF



Matrix: Water


L1940104-06Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

09/07/19 09:10

09/11/19

MDL

0.001

Sample Depth:

Serial_No:09111913:42

Page 163 of 177

FF



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

DateAnalyzed


Date Prepared

09/11/19

Cyanide, Total

Cyanide, Total

ND

ND

mg/kg

mg/l

1

1

0.84

0.005

09/06/19 12:24

09/09/19 11:09

1,9010C/9012B

1,9010C/9012B

ML

LH

09/05/19 15:15

09/07/19 09:10



MDL

0.18

0.001

Serial_No:09111913:42

Page 164 of 177

Cyanide, Total

Cyanide, Total

71

95

57

94

80-120

85-115

39

1

35

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery





Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual

Q Q

Qual

Q

Serial_No:09111913:42

Page 165 of 177

Cyanide, Total

Cyanide, Total

ND

ND

8.8

0.192

90

96

9.2

0.187

92

94

75-125

80-120

4

3

35

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits


General Chemistry - Westborough Lab Associated sample(s): 03-06 QC Batch ID: WG1281441-4 WG1281441-5 QC Sample: L1940104-03 Client ID: TW-1

9.7

0.2

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940104

09/11/19

Qual Qual Qual

Serial_No:09111913:42

Page 166 of 177

Solids, Total 96.0 96.3 % 0 20


General Chemistry - Westborough Lab Associated sample(s): 01-02 QC Batch ID: WG1280389-1 QC Sample: L1940104-02 Client ID: SESI-SB-20 (14-15)


10831

Project Name:

Project Number:

L1940104Lab Number:

Report Date:


09/11/19

Qual

Serial_No:09111913:42

Page 167 of 177


L1940104-01A

L1940104-01B

L1940104-01C

L1940104-01D

L1940104-01E

L1940104-01F

L1940104-01X

L1940104-01Y

L1940104-01Z

L1940104-02A

L1940104-02B

L1940104-02C

L1940104-02D

L1940104-02E

L1940104-02X

L1940104-02Y

L1940104-02Z













Glass 60ml unpreserved split





A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent



10831

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)


TS(7)


NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)


NYTCL-8270(14),TCN-9010(14),TS(7),NYTCL-8081(14),NYTCL-8082(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

Project Name:

Project Number:

L1940104Lab Number:

Report Date:




Analysis(*)

09/11/19


05-SEP-19 02:25

05-SEP-19 02:25

05-SEP-19 02:25

05-SEP-19 02:25

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09111913:42

Page 168 of 177


L1940104-03A

L1940104-03B

L1940104-03C

L1940104-03D

L1940104-03E

L1940104-03F

L1940104-03G

L1940104-03H

L1940104-03J

L1940104-03K

L1940104-03L

L1940104-03M

L1940104-03X

L1940104-04A

L1940104-04B

L1940104-04C

Vial HCl preserved

Vial HCl preserved

Vial HCl preserved

Plastic 250ml HNO3 preserved

Plastic 250ml NaOH preserved

Plastic 250ml unpreserved

Amber 120ml unpreserved






Plastic 120ml HNO3 preserved Filtrates

Vial HCl preserved

Vial HCl preserved

Vial HCl preserved

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

<2

>12

7

7

7

7

7

7

7

NA

NA

NA

NA

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent


10831

NYTCL-8260(14)

NYTCL-8260(14)

NYTCL-8260(14)

BA-6020T(180),FE-6020T(180),SE-6020T(180),TL-6020T(180),CA-6020T(180),CR-6020T(180),K-6020T(180),NI-6020T(180),CU-6020T(180),NA-6020T(180),ZN-6020T(180),PB-6020T(180),BE-6020T(180),MN-6020T(180),AS-6020T(180),SB-6020T(180),V-6020T(180),AG-6020T(180),AL-6020T(180),CD-6020T(180),HG-T(28),MG-6020T(180),CO-6020T(180)

TCN-9010(14)

-

NYTCL-8082-LVI(7)

NYTCL-8082-LVI(7)

NYTCL-8081(7)

NYTCL-8081(7)

NYTCL-8270-SIM-LVI(7),NYTCL-8270-LVI(7)


CU-6020S(180),K-6020S(180),SE-6020S(180),V-6020S(180),MN-6020S(180),BE-6020S(180),CO-6020S(180),MG-6020S(180),ZN-6020S(180),CA-6020S(180),CR-6020S(180),FE-6020S(180),BA-6020S(180),NA-6020S(180),NI-6020S(180),PB-6020S(180),TL-6020S(180),AG-6020S(180),AS-6020S(180),SB-6020S(180),AL-6020S(180),CD-6020S(180),HG-S(28)

NYTCL-8260(14)

NYTCL-8260(14)

NYTCL-8260(14)

Project Name:

Project Number:

L1940104Lab Number:

Report Date:



Analysis(*)

09/11/19

<2

>12

7

7

7

7

7

7

7

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09111913:42

Page 169 of 177


L1940104-04D

L1940104-04E

L1940104-04F

L1940104-04G

L1940104-04H

L1940104-04J

L1940104-04K

L1940104-04L

L1940104-04M

L1940104-04X

L1940104-05A

L1940104-05B

L1940104-05C

L1940104-05D

L1940104-05E

L1940104-05F











Vial HCl preserved

Vial HCl preserved

Vial HCl preserved




A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

<2

>12

7

7

7

7

7

7

7

NA

NA

NA

NA

<2

>12

7

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent


10831


TCN-9010(14)

-

NYTCL-8082-LVI(7)

NYTCL-8082-LVI(7)

NYTCL-8081(7)

NYTCL-8081(7)




NYTCL-8260(14)

NYTCL-8260(14)

NYTCL-8260(14)


TCN-9010(14)

-

Project Name:

Project Number:

L1940104Lab Number:

Report Date:



Analysis(*)

09/11/19

<2

>12

7

7

7

7

7

7

7

<2

>12

7

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09111913:42

Page 170 of 177


L1940104-05G

L1940104-05H

L1940104-05J

L1940104-05K

L1940104-05L

L1940104-05M

L1940104-05X

L1940104-06A

L1940104-06B

L1940104-06C

L1940104-06D

L1940104-06E

L1940104-06F

L1940104-06G

L1940104-06H

L1940104-06J

L1940104-06K

L1940104-06L

L1940104-06M








Vial HCl preserved

Vial HCl preserved

Vial HCl preserved










A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

7

7

7

7

7

7

NA

NA

NA

NA

<2

>12

7

7

7

7

7

7

7

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent


10831

NYTCL-8082-LVI(7)

NYTCL-8082-LVI(7)

NYTCL-8081(7)

NYTCL-8081(7)




NYTCL-8260(14)

NYTCL-8260(14)

NYTCL-8260(14)


TCN-9010(14)

-

NYTCL-8082-LVI(7)

NYTCL-8082-LVI(7)

NYTCL-8081(7)

NYTCL-8081(7)



Project Name:

Project Number:

L1940104Lab Number:

Report Date:



Analysis(*)

09/11/19

7

7

7

7

7

7

<2

>12

7

7

7

7

7

7

7

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09111913:42

Page 171 of 177


L1940104-06X

L1940104-07A

L1940104-07B


Vial HCl preserved

Vial HCl preserved

A

A

A

NA

NA

NA

2.5

2.5

2.5

Y

Y

Y

Absent

Absent

Absent


10831


NYTCL-8260(14)

NYTCL-8260(14)

Project Name:

Project Number:

L1940104Lab Number:

Report Date:



Analysis(*)

09/11/19

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09111913:42

Page 172 of 177


GLOSSARY

Project Name:

Project Number:

Lab Number:

Report Date:

L194010490-02 118TH ST., JAMAICA, NY

10831 09/11/19

Acronyms

DL

EDL

EMPC

EPA

LCS

LCSD

LFB

LOD

LOQ

MDL

MS

MSD

NA

NC

NDPA/DPA

NI

NP

RL

RPD

SRM

STLP

TEF

TEQ

TIC






Not Applicable.


Not Ignitable.





-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

Footnotes

Serial_No:09111913:42

Page 173 of 177


Project Name:

Project Number:

Lab Number:

Report Date:

L194010490-02 118TH ST., JAMAICA, NY

10831 09/11/19

Terms


Data Qualifiers

A

B

C

D

E

G

H

I

J

M

ND

NJ

P

Q

R

RE

S

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-











-

Serial_No:09111913:42

Page 174 of 177




1

121



Project Name:

Project Number:

Lab Number:

Report Date:

L194010490-02 118TH ST., JAMAICA, NY

10831

REFERENCES

09/11/19

Serial_No:09111913:42

Page 175 of 177











Mansfield Facility:




Serial_No:09111913:42

Page 176 of 177

Serial_No:09111913:42

Page 177 of 177

L1940152


10831

90-02 168TH ST, JAMAICA, NY

Client:

Project Name:

Project Number:

09/11/19

320 Forbes Boulevard, Mansfield, MA 02048-1806

Lab Number:

Report Date:


12A Maple Avenue


Jesse MausnerATTN:

ANALYTICAL REPORT

Certifications & Approvals: MA (M-MA030), NH NELAP (2062), CT (PH-0141), DoD (L2474), FL (E87814), IL (200081), LA (85084),ME (MA00030), MD (350), NJ (MA015), NY (11627), NC (685), OH (CL106), PA (68-02089), RI (LAO00299), TX (T104704419), VT (VT-0015), VA (460194), WA (C954), US Army Corps of Engineers, USDA (Permit #P330-17-00150), USFWS (Permit #206964).

(973) 808-9050Phone:


Serial_No:09111919:41

Page 1 of 45

L1940152-01

L1940152-02

L1940152-03

L1940152-04

L1940152-05

Alpha Sample ID

SV-1

SV-2

SV-3

SV-4

SV-5

Client ID

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

JAMAICA, QUEENS, NY

Sample Location


10831



L194015209/11/19

09/03/19 12:00

09/03/19 14:05

09/03/19 15:20

09/03/19 16:18

09/03/19 17:00


SOIL_VAPOR

SOIL_VAPOR

SOIL_VAPOR

SOIL_VAPOR

SOIL_VAPOR

09/04/19

09/04/19

09/04/19

09/04/19

09/04/19

Serial_No:09111919:41

Page 2 of 45


10831

Project Name:

Project Number:

Lab Number:


09/11/19

Case Narrative

























Serial_No:09111919:41

Page 3 of 45



10831

Project Name:

Project Number:

Lab Number:


09/11/19

Volatile Organics in Air

Canisters were released from the laboratory on August 28, 2019. The canister certification results are provided

as an addendum.

L1940152-01: The sample has elevated detection limits due to the dilution required by the elevated

concentrations of non-target compounds in the sample.




Serial_No:09111919:41

Page 4 of 45

AIR

Serial_No:09111919:41

Page 5 of 45

FF


Chloromethane

1,2-Dichloro-1,1,2,2-tetrafluoroethane

Vinyl chloride

1,3-Butadiene

Bromomethane

Chloroethane

Ethyl Alcohol

Vinyl bromide

Acetone


iso-Propyl Alcohol

1,1-Dichloroethene

tert-Butyl Alcohol

Methylene chloride

3-Chloropropene

Carbon disulfide

1,1,2-Trichloro-1,2,2-Trifluoroethane


1,1-Dichloroethane


2-Butanone


Parameter Results

0.492

2.67

ND

ND

18.1

ND

ND

52.3

ND

217

ND

3.45

ND

ND

ND

ND

1.71

ND

ND

ND

ND

19.8

ND

RL

Volatile Organics in Air - Mansfield Lab

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.400

0.400

0.400

0.400

0.400

0.400

0.400

10.0

0.400

2.00

0.400

1.00

0.400

1.00

1.00

0.400

0.400

0.400

0.400

0.400

0.400

1.00

0.400

Results

Dilution Factor

2.43

5.51

ND

ND

40.0

ND

ND

98.5

ND

515

ND

8.48

ND

ND

ND

ND

5.33

ND

ND

ND

ND

58.4

ND

QualifierRL

1.98

0.826

2.80

1.02

0.885

1.55

1.06

18.8

1.75

4.75

2.25

2.46

1.59

3.03

3.47

1.25

1.25

3.07

1.59

1.62

1.44

2.95

1.59

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

ppbV ug/m3

09/11/19

SV-1Client ID:09/03/19 12:00Date Collected:09/04/19Date Received:

Matrix: Soil_Vapor


L1940152-01Lab ID:

SAMPLE RESULTS

Field Prep:

Anaytical Method:Analytical Date:Analyst:

48,TO-1509/11/19 00:56EW

Not Specified

D

MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Sample Depth:

Serial_No:09111919:41

Page 6 of 45

Ethyl Acetate

Chloroform

Tetrahydrofuran

1,2-Dichloroethane

n-Hexane


Benzene


Cyclohexane

1,2-Dichloropropane


Xylene (Total)

1,4-Dioxane

Trichloroethene

2,2,4-Trimethylpentane

Heptane





Toluene

1,2-Dichloroethene (total)

2-Hexanone



1,2-Dibromoethane

Parameter Results

ND

4.34

ND

ND

9.25

ND

5.47

ND

0.806

ND

ND

1.44

ND

0.842

ND

3.89

ND

1.64

ND

ND

3.08

ND

ND

ND

ND

ND

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

1.00

0.400

1.00

0.400

0.400

0.400

0.400

0.400

0.400

0.400

0.400

0.400

0.400

0.400

0.400

0.400

0.400

1.00

0.400

0.400

0.400

0.400

0.400

0.400

0.400

0.400

Results

Dilution Factor

ND

21.2

ND

ND

32.6

ND

17.5

ND

2.77

ND

ND

6.25

ND

4.53

ND

15.9

ND

6.72

ND

ND

11.6

ND

ND

ND

ND

ND

QualifierRL

3.60

1.95

2.95

1.62

1.41

2.18

1.28

2.52

1.38

1.85

2.68

1.74

1.44

2.15

1.87

1.64

1.82

4.10

1.82

2.18

1.51

1.59

1.64

3.41

1.82

3.07

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

ppbV ug/m3

09/11/19



L1940152-01Lab ID:

SAMPLE RESULTS


D

MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Sample Depth:

Serial_No:09111919:41

Page 7 of 45

Tetrachloroethene

Chlorobenzene

Ethylbenzene

p/m-Xylene

Bromoform

Styrene


o-Xylene

4-Ethyltoluene



Benzyl chloride

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene


Hexachlorobutadiene

Parameter Results

ND

ND

0.436

1.01

ND

ND

ND

0.432

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.400

0.400

0.400

0.800

0.400

0.400

0.400

0.400

0.400

0.400

0.400

0.400

0.400

0.400

0.400

0.400

0.400

Results

Dilution Factor

ND

ND

1.89

4.39

ND

ND

ND

1.88

ND

ND

ND

ND

ND

ND

ND

ND

ND

QualifierRL

2.71

1.84

1.74

3.47

4.14

1.70

2.75

1.74

1.97

1.97

1.97

2.07

2.40

2.40

2.40

2.97

4.27

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

ppbV ug/m3

09/11/19



L1940152-01Lab ID:

SAMPLE RESULTS


D

MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

1,4-Difluorobenzene

Bromochloromethane

chlorobenzene-d5

102

97

96

Internal Standard % Recovery QualifierAcceptance

Criteria

60-140

60-140

60-140

Sample Depth:

Serial_No:09111919:41

Page 8 of 45


Chloromethane


Vinyl chloride

1,3-Butadiene

Bromomethane

Chloroethane

Ethyl Alcohol

Vinyl bromide

Acetone


iso-Propyl Alcohol

1,1-Dichloroethene

tert-Butyl Alcohol

Methylene chloride

3-Chloropropene

Carbon disulfide



1,1-Dichloroethane


2-Butanone


Parameter Results

0.710

1.92

ND

ND

4.57

ND

ND

28.7

ND

108

0.308

1.76

ND

6.45

ND

ND

1.31

ND

ND

ND

ND

9.20

ND

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.200

0.200

0.200

0.200

0.200

0.200

0.200

5.00

0.200

1.00

0.200

0.500

0.200

0.500

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.500

0.200

Results

Dilution Factor

3.51

3.96

ND

ND

10.1

ND

ND

54.1

ND

257

1.73

4.33

ND

19.6

ND

ND

4.08

ND

ND

ND

ND

27.1

ND

QualifierRL

0.989

0.413

1.40

0.511

0.442

0.777

0.528

9.42

0.874

2.38

1.12

1.23

0.793

1.52

1.74

0.626

0.623

1.53

0.793

0.809

0.721

1.47

0.793

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19


Matrix: Soil_Vapor


L1940152-02Lab ID:

SAMPLE RESULTS

Field Prep:


48,TO-1509/11/19 01:35EW

Not Specified

MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Sample Depth:

Serial_No:09111919:41

Page 9 of 45

Ethyl Acetate

Chloroform

Tetrahydrofuran

1,2-Dichloroethane

n-Hexane


Benzene


Cyclohexane

1,2-Dichloropropane

Xylene (Total)


1,4-Dioxane

Trichloroethene


Heptane





Toluene


2-Hexanone



1,2-Dibromoethane

Parameter Results

ND

9.99

ND

ND

2.48

2.53

2.13

ND

0.273

ND

1.36

ND

ND

0.526

ND

1.88

ND

1.96

ND

ND

1.87

ND

ND

ND

ND

ND

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.500

0.200

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

Results

Dilution Factor

ND

48.8

ND

ND

8.74

13.8

6.80

ND

0.940

ND

5.91

ND

ND

2.83

ND

7.70

ND

8.03

ND

ND

7.05

ND

ND

ND

ND

ND

QualifierRL

1.80

0.977

1.47

0.809

0.705

1.09

0.639

1.26

0.688

0.924

0.869

1.34

0.721

1.07

0.934

0.820

0.908

2.05

0.908

1.09

0.754

0.793

0.820

1.70

0.908

1.54

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19



L1940152-02Lab ID:

SAMPLE RESULTS


MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Sample Depth:

Serial_No:09111919:41

Page 10 of 45

Tetrachloroethene

Chlorobenzene

Ethylbenzene

p/m-Xylene

Bromoform

Styrene


o-Xylene

4-Ethyltoluene



Benzyl chloride

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene


Hexachlorobutadiene

Parameter Results

10.5

ND

0.377

0.878

ND

ND

ND

0.477

ND

ND

ND

ND

0.391

ND

ND

ND

ND

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.200

0.200

0.200

0.400

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

Results

Dilution Factor

71.2

ND

1.64

3.81

ND

ND

ND

2.07

ND

ND

ND

ND

2.35

ND

ND

ND

ND

QualifierRL

1.36

0.921

0.869

1.74

2.07

0.852

1.37

0.869

0.983

0.983

0.983

1.04

1.20

1.20

1.20

1.48

2.13

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19



L1940152-02Lab ID:

SAMPLE RESULTS


MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

1,4-Difluorobenzene

Bromochloromethane

chlorobenzene-d5

103

98

100


Criteria

60-140

60-140

60-140

Sample Depth:

Serial_No:09111919:41

Page 11 of 45


Chloromethane


Vinyl chloride

1,3-Butadiene

Bromomethane

Chloroethane

Ethyl Alcohol

Vinyl bromide

Acetone


iso-Propyl Alcohol

1,1-Dichloroethene

tert-Butyl Alcohol

Methylene chloride

3-Chloropropene

Carbon disulfide



1,1-Dichloroethane


2-Butanone


Parameter Results

0.486

1.04

ND

ND

18.4

ND

ND

ND

ND

108

0.426

0.770

ND

ND

ND

ND

2.34

ND

ND

ND

ND

15.4

ND

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.200

0.200

0.200

0.200

0.200

0.200

0.200

5.00

0.200

1.00

0.200

0.500

0.200

0.500

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.500

0.200

Results

Dilution Factor

2.40

2.15

ND

ND

40.7

ND

ND

ND

ND

257

2.39

1.89

ND

ND

ND

ND

7.29

ND

ND

ND

ND

45.4

ND

QualifierRL

0.989

0.413

1.40

0.511

0.442

0.777

0.528

9.42

0.874

2.38

1.12

1.23

0.793

1.52

1.74

0.626

0.623

1.53

0.793

0.809

0.721

1.47

0.793

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19


Matrix: Soil_Vapor


L1940152-03Lab ID:

SAMPLE RESULTS

Field Prep:


48,TO-1509/11/19 02:15EW

Not Specified

MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Sample Depth:

Serial_No:09111919:41

Page 12 of 45

Ethyl Acetate

Chloroform

Tetrahydrofuran

1,2-Dichloroethane

n-Hexane


Benzene


Cyclohexane

1,2-Dichloropropane

Xylene (Total)


1,4-Dioxane

Trichloroethene


Heptane





Toluene


2-Hexanone



1,2-Dibromoethane

Parameter Results

ND

16.4

ND

ND

5.12

ND

5.24

ND

0.566

ND

5.63

ND

ND

13.3

ND

3.51

ND

2.14

ND

ND

4.58

ND

ND

ND

ND

ND

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.500

0.200

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

Results

Dilution Factor

ND

80.1

ND

ND

18.0

ND

16.7

ND

1.95

ND

24.5

ND

ND

71.5

ND

14.4

ND

8.77

ND

ND

17.3

ND

ND

ND

ND

ND

QualifierRL

1.80

0.977

1.47

0.809

0.705

1.09

0.639

1.26

0.688

0.924

0.869

1.34

0.721

1.07

0.934

0.820

0.908

2.05

0.908

1.09

0.754

0.793

0.820

0.908

1.70

1.54

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19



L1940152-03Lab ID:

SAMPLE RESULTS


MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Sample Depth:

Serial_No:09111919:41

Page 13 of 45

Tetrachloroethene

Chlorobenzene

Ethylbenzene

p/m-Xylene

Bromoform

Styrene


o-Xylene

4-Ethyltoluene



Benzyl chloride

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene


Hexachlorobutadiene

Parameter Results

2.47

ND

1.22

3.43

ND

0.443

ND

2.20

0.258

0.235

1.13

ND

ND

ND

ND

ND

ND

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.200

0.200

0.200

0.400

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

Results

Dilution Factor

16.7

ND

5.30

14.9

ND

1.89

ND

9.56

1.27

1.16

5.56

ND

ND

ND

ND

ND

ND

QualifierRL

1.36

0.921

0.869

1.74

2.07

0.852

1.37

0.869

0.983

0.983

0.983

1.04

1.20

1.20

1.20

1.48

2.13

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19



L1940152-03Lab ID:

SAMPLE RESULTS


MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

1,4-Difluorobenzene

Bromochloromethane

chlorobenzene-d5

104

100

105


Criteria

60-140

60-140

60-140

Sample Depth:

Serial_No:09111919:41

Page 14 of 45


Chloromethane


Vinyl chloride

1,3-Butadiene

Bromomethane

Chloroethane

Ethyl Alcohol

Vinyl bromide

Acetone


iso-Propyl Alcohol

1,1-Dichloroethene

tert-Butyl Alcohol

Methylene chloride

3-Chloropropene

Carbon disulfide



1,1-Dichloroethane


2-Butanone


Parameter Results

0.589

0.855

ND

ND

8.91

ND

ND

ND

ND

107

0.395

0.760

ND

3.36

ND

ND

0.914

ND

ND

ND

ND

9.07

ND

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.200

0.200

0.200

0.200

0.200

0.200

0.200

5.00

0.200

1.00

0.200

0.500

0.200

0.500

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.500

0.200

Results

Dilution Factor

2.91

1.77

ND

ND

19.7

ND

ND

ND

ND

254

2.22

1.87

ND

10.2

ND

ND

2.85

ND

ND

ND

ND

26.8

ND

QualifierRL

0.989

0.413

1.40

0.511

0.442

0.777

0.528

9.42

0.874

2.38

1.12

1.23

0.793

1.52

1.74

0.626

0.623

1.53

0.793

0.809

0.721

1.47

0.793

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19


Matrix: Soil_Vapor


L1940152-04Lab ID:

SAMPLE RESULTS

Field Prep:


48,TO-1509/11/19 02:54EW

Not Specified

MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Sample Depth:

Serial_No:09111919:41

Page 15 of 45

Ethyl Acetate

Chloroform

Tetrahydrofuran

1,2-Dichloroethane

n-Hexane


Benzene


Cyclohexane

1,2-Dichloropropane

Xylene (Total)


1,4-Dioxane

Trichloroethene


Heptane





Toluene


2-Hexanone



1,2-Dibromoethane

Parameter Results

ND

0.846

ND

ND

2.59

0.790

2.36

ND

ND

ND

3.00

ND

ND

3.87

ND

1.63

ND

0.879

ND

ND

2.26

ND

ND

ND

ND

ND

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.500

0.200

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

Results

Dilution Factor

ND

4.13

ND

ND

9.13

4.31

7.54

ND

ND

ND

13.0

ND

ND

20.8

ND

6.68

ND

3.60

ND

ND

8.52

ND

ND

ND

ND

ND

QualifierRL

1.80

0.977

1.47

0.809

0.705

1.09

0.639

1.26

0.688

0.924

0.869

1.34

0.721

1.07

0.934

0.820

0.908

2.05

0.908

1.09

0.754

0.793

0.820

1.70

0.908

1.54

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19



L1940152-04Lab ID:

SAMPLE RESULTS


MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Sample Depth:

Serial_No:09111919:41

Page 16 of 45

Tetrachloroethene

Chlorobenzene

Ethylbenzene

p/m-Xylene

Bromoform

Styrene


o-Xylene

4-Ethyltoluene



Benzyl chloride

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene


Hexachlorobutadiene

Parameter Results

3.95

ND

0.661

1.75

ND

0.223

ND

1.25

ND

ND

0.487

ND

ND

ND

ND

ND

ND

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.200

0.200

0.200

0.400

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

Results

Dilution Factor

26.8

ND

2.87

7.60

ND

0.949

ND

5.43

ND

ND

2.39

ND

ND

ND

ND

ND

ND

QualifierRL

1.36

0.921

0.869

1.74

2.07

0.852

1.37

0.869

0.983

0.983

0.983

1.04

1.20

1.20

1.20

1.48

2.13

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19



L1940152-04Lab ID:

SAMPLE RESULTS


MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

1,4-Difluorobenzene

Bromochloromethane

chlorobenzene-d5

109

103

108


Criteria

60-140

60-140

60-140

Sample Depth:

Serial_No:09111919:41

Page 17 of 45


Chloromethane


Vinyl chloride

1,3-Butadiene

Bromomethane

Chloroethane

Ethyl Alcohol

Vinyl bromide

Acetone


iso-Propyl Alcohol

1,1-Dichloroethene

tert-Butyl Alcohol

Methylene chloride

3-Chloropropene

Carbon disulfide



1,1-Dichloroethane


2-Butanone


Parameter Results

0.497

0.868

ND

ND

5.88

ND

ND

ND

ND

92.3

0.804

0.538

ND

2.57

ND

ND

0.610

ND

ND

ND

ND

6.67

ND

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.200

0.200

0.200

0.200

0.200

0.200

0.200

5.00

0.200

1.00

0.200

0.500

0.200

0.500

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.500

0.200

Results

Dilution Factor

2.46

1.79

ND

ND

13.0

ND

ND

ND

ND

219

4.52

1.32

ND

7.79

ND

ND

1.90

ND

ND

ND

ND

19.7

ND

QualifierRL

0.989

0.413

1.40

0.511

0.442

0.777

0.528

9.42

0.874

2.38

1.12

1.23

0.793

1.52

1.74

0.626

0.623

1.53

0.793

0.809

0.721

1.47

0.793

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19


Matrix: Soil_Vapor


L1940152-05Lab ID:

SAMPLE RESULTS

Field Prep:


48,TO-1509/11/19 03:34EW

Not Specified

MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Sample Depth:

Serial_No:09111919:41

Page 18 of 45

Ethyl Acetate

Chloroform

Tetrahydrofuran

1,2-Dichloroethane

n-Hexane


Benzene


Cyclohexane

1,2-Dichloropropane


Xylene (Total)

1,4-Dioxane

Trichloroethene


Heptane





Toluene


2-Hexanone



1,2-Dibromoethane

Parameter Results

ND

3.74

ND

ND

1.44

0.605

1.70

ND

ND

ND

ND

4.42

ND

0.704

ND

1.12

ND

0.864

ND

ND

1.92

ND

ND

ND

ND

ND

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.500

0.200

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

Results

Dilution Factor

ND

18.3

ND

ND

5.08

3.30

5.43

ND

ND

ND

ND

19.2

ND

3.78

ND

4.59

ND

3.54

ND

ND

7.24

ND

ND

ND

ND

ND

QualifierRL

1.80

0.977

1.47

0.809

0.705

1.09

0.639

1.26

0.688

0.924

1.34

0.869

0.721

1.07

0.934

0.820

0.908

2.05

0.908

1.09

0.754

0.793

0.820

1.70

0.908

1.54

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19



L1940152-05Lab ID:

SAMPLE RESULTS


MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Sample Depth:

Serial_No:09111919:41

Page 19 of 45

Tetrachloroethene

Chlorobenzene

Ethylbenzene

p/m-Xylene

Bromoform

Styrene


o-Xylene

4-Ethyltoluene



Benzyl chloride

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene


Hexachlorobutadiene

Parameter Results

16.2

ND

0.832

2.32

ND

0.202

ND

2.09

0.488

1.26

3.49

ND

ND

ND

ND

ND

ND

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.200

0.200

0.200

0.400

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

Results

Dilution Factor

110

ND

3.61

10.1

ND

0.860

ND

9.08

2.40

6.19

17.2

ND

ND

ND

ND

ND

ND

QualifierRL

1.36

0.921

0.869

1.74

2.07

0.852

1.37

0.869

0.983

0.983

0.983

1.04

1.20

1.20

1.20

1.48

2.13

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19



L1940152-05Lab ID:

SAMPLE RESULTS


MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

1,4-Difluorobenzene

Bromochloromethane

chlorobenzene-d5

107

102

107


Criteria

60-140

60-140

60-140

Sample Depth:

Serial_No:09111919:41

Page 20 of 45

FF

Chlorodifluoromethane

Propylene

Propane


Chloromethane


Methanol

Vinyl chloride

1,3-Butadiene

Butane

Bromomethane

Chloroethane

Ethyl Alcohol

Dichlorofluoromethane

Vinyl bromide

Acrolein

Acetone

Acetonitrile


iso-Propyl Alcohol

Acrylonitrile

Pentane

Ethyl ether

1,1-Dichloroethene

tert-Butyl Alcohol

Parameter Results

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

Analytical Date: 09/10/19 16:0648,TO-15Analytical Method:

RL

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.200

0.500

0.500

0.200

0.200

0.200

5.00

0.200

0.200

0.200

0.200

0.200

5.00

0.200

0.200

0.500

1.00

0.200

0.200

0.500

0.500

0.200

0.200

0.200

0.500

Results

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

QualifierRL

0.707

0.861

0.902

0.989

0.413

1.40

6.55

0.511

0.442

0.475

0.777

0.528

9.42

0.842

0.874

1.15

2.38

0.336

1.12

1.23

1.09

0.590

0.606

0.793

1.52

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3


09/11/19

Volatile Organics in Air - Mansfield Lab for sample(s): 01-05 Batch: WG1282448-4

MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Serial_No:09111919:41

Page 21 of 45

Methylene chloride

3-Chloropropene

Carbon disulfide



1,1-Dichloroethane


Vinyl acetate

2-Butanone

Xylene (Total)


Ethyl Acetate

Chloroform

Tetrahydrofuran

2,2-Dichloropropane

1,2-Dichloroethane

n-Hexane

Isopropyl Ether

Ethyl-Tert-Butyl-Ether




1,1-Dichloropropene

Benzene


Parameter Results

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND


RL

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.500

0.200

0.200

0.200

0.200

0.200

0.200

1.00

0.500

0.200

0.200

0.500

0.200

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

Results

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

QualifierRL

1.74

0.626

0.623

1.53

0.793

0.809

0.721

3.52

1.47

0.869

0.793

1.80

0.977

1.47

0.924

0.809

0.705

0.836

0.836

0.793

1.09

0.908

0.908

0.639

1.26

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3


09/11/19


MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Serial_No:09111919:41

Page 22 of 45

Cyclohexane

Tertiary-Amyl Methyl Ether

Dibromomethane

1,2-Dichloropropane


1,4-Dioxane

Trichloroethene


Methyl Methacrylate

Heptane





Toluene

1,3-Dichloropropane

2-Hexanone


1,2-Dibromoethane

Butyl Acetate

Octane

Tetrachloroethene


Chlorobenzene

Ethylbenzene

Parameter Results

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND


RL

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.500

0.200

0.200

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.500

0.200

0.200

0.200

0.200

0.200

Results

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

QualifierRL

0.688

0.836

1.42

0.924

1.34

0.721

1.07

0.934

2.05

0.820

0.908

2.05

0.908

1.09

0.754

0.924

0.820

1.70

1.54

2.38

0.934

1.36

1.37

0.921

0.869

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3


09/11/19


MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Serial_No:09111919:41

Page 23 of 45

p/m-Xylene

Bromoform

Styrene


o-Xylene


Nonane (C9)

Isopropylbenzene

Bromobenzene

o-Chlorotoluene

n-Propylbenzene

p-Chlorotoluene

4-Ethyltoluene


tert-Butylbenzene


Decane (C10)

Benzyl chloride

1,3-Dichlorobenzene

1,4-Dichlorobenzene

sec-Butylbenzene

p-Isopropyltoluene

1,2-Dichlorobenzene

n-Butylbenzene


Parameter Results

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND


RL

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.400

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

Results

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

QualifierRL

1.74

2.07

0.852

1.37

0.869

1.21

1.05

0.983

0.793

1.04

0.983

1.04

0.983

0.983

1.10

0.983

1.16

1.04

1.20

1.20

1.10

1.10

1.20

1.10

1.93

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3


09/11/19


MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Serial_No:09111919:41

Page 24 of 45

Undecane

Dodecane (C12)


Naphthalene


Hexachlorobutadiene

Parameter Results

ND

ND

ND

ND

ND

ND


RL

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

0.200

0.200

0.200

0.200

0.200

0.200

Results

Dilution Factor

ND

ND

ND

ND

ND

ND

QualifierRL

1.28

1.39

1.48

1.05

1.48

2.13

1

1

1

1

1

1

ppbV ug/m3


09/11/19


MDL

--

--

--

--

--

--

MDL

--

--

--

--

--

--

Serial_No:09111919:41

Page 25 of 45


Propylene

Propane


Chloromethane


Methanol

Vinyl chloride

1,3-Butadiene

Butane

Bromomethane

Chloroethane

Ethyl Alcohol


Vinyl bromide

Acrolein

Acetone

Acetonitrile


iso-Propyl Alcohol

Acrylonitrile

Pentane

Ethyl ether

91

111

87

113

107

109

143

94

106

93

98

92

96

93

101

88

87

82

109

91

89

85

95

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

40-160

70-130

70-130

70-130

40-160

70-130

70-130

40-160

70-130

70-130

70-130

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Volatile Organics in Air - Mansfield Lab Associated sample(s): 01-05 Batch: WG1282448-3


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

09/11/19

Qual Qual

Q

Qual

Serial_No:09111919:41

Page 26 of 45

1,1-Dichloroethene

tert-Butyl Alcohol

Methylene chloride

3-Chloropropene

Carbon disulfide



1,1-Dichloroethane


Vinyl acetate

2-Butanone


Ethyl Acetate

Chloroform

Tetrahydrofuran

2,2-Dichloropropane

1,2-Dichloroethane

n-Hexane

Isopropyl Ether

Ethyl-Tert-Butyl-Ether




96

96

106

97

100

102

90

92

109

98

96

92

88

97

97

102

103

89

86

86

91

91

110

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

09/11/19

Qual Qual Qual

Serial_No:09111919:41

Page 27 of 45

1,1-Dichloropropene

Benzene


Cyclohexane

Tertiary-Amyl Methyl Ether

Dibromomethane

1,2-Dichloropropane


1,4-Dioxane

Trichloroethene


Methyl Methacrylate

Heptane





Toluene

1,3-Dichloropropane

2-Hexanone


1,2-Dibromoethane

Butyl Acetate

105

94

117

87

103

91

95

100

90

98

91

83

111

112

115

100

102

94

99

123

108

108

99

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

40-160

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

09/11/19

Qual Qual Qual

Serial_No:09111919:41

Page 28 of 45

Octane

Tetrachloroethene


Chlorobenzene

Ethylbenzene

p/m-Xylene

Bromoform

Styrene


o-Xylene


Nonane (C9)

Isopropylbenzene

Bromobenzene

o-Chlorotoluene

n-Propylbenzene

p-Chlorotoluene

4-Ethyltoluene


tert-Butylbenzene


Decane (C10)

Benzyl chloride

87

105

101

104

102

104

115

110

103

109

102

106

109

100

97

96

95

114

115

102

119

94

110

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

09/11/19

Qual Qual Qual

Serial_No:09111919:41

Page 29 of 45

1,3-Dichlorobenzene

1,4-Dichlorobenzene

sec-Butylbenzene

p-Isopropyltoluene

1,2-Dichlorobenzene

n-Butylbenzene


Undecane

Dodecane (C12)


Naphthalene


Hexachlorobutadiene

116

111

108

98

115

107

121

101

105

105

102

107

127

-

-

-

-

-

-

-

-

-

-

-

-

-

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

-

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1940152

09/11/19

Qual Qual Qual

Serial_No:09111919:41

Page 30 of 45

L1940152

10831


01264

2342

01096

2855

01245

2788

01240

187

01092

155

Media Type

SV20

2.7L Can

SV20

2.7L Can

SV20

2.7L Can

SV20

2.7L Can

SV20

2.7L Can

Media ID

L1940152-01

L1940152-01

L1940152-02

L1940152-02

L1940152-03

L1940152-03

L1940152-04

L1940152-04

L1940152-05

L1940152-05

Samplenum

L1938279-01

L1938279-01

L1938279-01

L1938279-01

L1938279-01

CleaningBatch ID

-

-29.6

-

-29.5

-

-29.7

-

-29.5

-

-29.3

Pressureon Receipt(in. Hg)

-

-7.3

-

-3.3

-

-6.6

-

-6.7

-

-5.9

InitialPressure(in. Hg)

17.4

-

18.6

-

18.5

-

18.5

-

19.9

-

Flow OutmL/min

14.8

-

18.9

-

16.2

-

16.4

-

17.3

-

Flow InmL/min

16

-

2

-

13

-

12

-

14

-

% RPDClient ID

SV-1

SV-1

SV-2

SV-2

SV-3

SV-3

SV-4

SV-4

SV-5

SV-5

09/11/19

Project Name:

Project Number:

Lab Number:

Report Date:

Canister and Flow Controller Information

08/28/19

08/28/19

08/28/19

08/28/19

08/28/19

08/28/19

08/28/19

08/28/19

08/28/19

08/28/19

DatePrepared

300597

300597

300597

300597

300597

300597

300597

300597

300597

300597

BottleOrder

-

Pass

-

Pass

-

Pass

-

Pass

-

Pass

Can LeakCheck

Pass

-

Pass

-

Pass

-

Pass

-

Pass

-

Flow ControlerLeak Chk

Serial_No:09111919:41

Page 31 of 45

FF


Propylene

Propane


Chloromethane

Freon-114

Methanol

Vinyl chloride

1,3-Butadiene

Butane

Bromomethane

Chloroethane

Ethanol


Vinyl bromide

Acrolein

Acetone

Acetonitrile


Isopropanol

Acrylonitrile

Pentane

Ethyl ether

1,1-Dichloroethene

Parameter Results

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL


BATCH CANISTER CERTIFICATION

CANISTER QC BAT

L1938279

0.200

0.500

0.500

0.200

0.200

0.200

5.00

0.200

0.200

0.200

0.200

0.200

5.00

0.200

0.200

0.500

1.00

0.200

0.200

0.500

0.500

0.200

0.200

0.200

Results

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

QualifierRL

0.707

0.861

0.902

0.989

0.413

1.40

6.55

0.511

0.442

0.475

0.777

0.528

9.42

0.842

0.874

1.15

2.38

0.336

1.12

1.23

1.09

0.590

0.606

0.793

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19

CAN 382 SHELF 2Client ID:08/22/19 16:00Date Collected:08/23/19Date Received:

Matrix: Air

Sample Location:

L1938279-01Lab ID:

Field Prep:


48,TO-1508/24/19 17:28TS

Not Specified

MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Air Canister Certification Results

Project Name:

Project Number:

Lab Number:

Report Date:

Sample Depth:

Serial_No:09111919:41

Page 32 of 45

Tertiary butyl Alcohol

Methylene chloride

3-Chloropropene

Carbon disulfide

Freon-113


1,1-Dichloroethane


Vinyl acetate

2-Butanone

Xylenes, total


Ethyl Acetate

Chloroform

Tetrahydrofuran

2,2-Dichloropropane

1,2-Dichloroethane

n-Hexane

Diisopropyl ether

tert-Butyl Ethyl Ether



1,1-Dichloropropene

Benzene


Cyclohexane

tert-Amyl Methyl Ether

Parameter Results

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL



CANISTER QC BAT

L1938279

0.500

0.500

0.200

0.200

0.200

0.200

0.200

0.200

1.00

0.500

0.600

0.200

0.500

0.200

0.500

0.200

0.200

0.200

0.200

0.200

1.00

0.200

0.200

0.200

0.200

0.200

0.200

Results

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

QualifierRL

1.52

1.74

0.626

0.623

1.53

0.793

0.809

0.721

3.52

1.47

0.869

0.793

1.80

0.977

1.47

0.924

0.809

0.705

0.836

0.836

1.00

1.09

0.908

0.639

1.26

0.688

0.836

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19


Sample Location:

L1938279-01Lab ID:


MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--


Project Name:

Project Number:

Lab Number:

Report Date:

Sample Depth:

Serial_No:09111919:41

Page 33 of 45

Dibromomethane

1,2-Dichloropropane


1,4-Dioxane

Trichloroethene


Methyl Methacrylate

Heptane





Toluene

1,3-Dichloropropane

2-Hexanone


1,2-Dibromoethane

Butyl acetate

Octane

Tetrachloroethene


Chlorobenzene

Ethylbenzene

p/m-Xylene

Bromoform

Styrene


Parameter Results

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL



CANISTER QC BAT

L1938279

0.200

0.200

0.200

0.200

0.200

0.200

0.500

0.200

0.200

0.500

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.500

0.200

0.200

0.200

0.200

0.200

0.400

0.200

0.200

0.200

Results

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

QualifierRL

1.42

0.924

1.34

0.721

1.07

0.934

2.05

0.820

0.908

2.05

0.908

1.09

0.754

0.924

0.820

1.70

1.54

2.38

0.934

1.36

1.37

0.921

0.869

1.74

2.07

0.852

1.37

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19


Sample Location:

L1938279-01Lab ID:


MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--


Project Name:

Project Number:

Lab Number:

Report Date:

Sample Depth:

Serial_No:09111919:41

Page 34 of 45

o-Xylene


Nonane

Isopropylbenzene

Bromobenzene

2-Chlorotoluene

n-Propylbenzene

4-Chlorotoluene

4-Ethyltoluene


tert-Butylbenzene


Decane

Benzyl chloride

1,3-Dichlorobenzene

1,4-Dichlorobenzene

sec-Butylbenzene

p-Isopropyltoluene

1,2-Dichlorobenzene

n-Butylbenzene


Undecane

Dodecane


Naphthalene


Hexachlorobutadiene

Parameter Results

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL



CANISTER QC BAT

L1938279

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

0.200

Results

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

QualifierRL

0.869

1.21

1.05

0.983

0.793

1.04

0.983

1.04

0.983

0.983

1.10

0.983

1.16

1.04

1.20

1.20

1.10

1.10

1.20

1.10

1.93

1.28

1.39

1.48

1.05

1.48

2.13

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19


Sample Location:

L1938279-01Lab ID:


MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--


Project Name:

Project Number:

Lab Number:

Report Date:

Sample Depth:

Serial_No:09111919:41

Page 35 of 45

Parameter Results RL



CANISTER QC BAT

L1938279

Results

Dilution FactorQualifierRL

ppbV ug/m3

09/11/19


Sample Location:

L1938279-01Lab ID:


No Tentatively Identified Compounds


Results Qualifier Units RDLDilution Factor

MDL MDL

1,4-Difluorobenzene

Bromochloromethane

chlorobenzene-d5

95

94

91


Criteria

60-140

60-140

60-140


Project Name:

Project Number:

Lab Number:

Report Date:

Sample Depth:

Serial_No:09111919:41

Page 36 of 45


Chloromethane

Freon-114

Vinyl chloride

1,3-Butadiene

Bromomethane

Chloroethane

Acetone


Acrylonitrile

1,1-Dichloroethene

Methylene chloride

Freon-113


1,1-Dichloroethane


2-Butanone


Chloroform

1,2-Dichloroethane


Benzene


1,2-Dichloropropane

Parameter Results

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

Volatile Organics in Air by SIM - Mansfield Lab


CANISTER QC BAT

L1938279

0.200

0.200

0.050

0.020

0.020

0.020

0.100

1.00

0.050

0.500

0.020

0.500

0.050

0.020

0.020

0.200

0.500

0.020

0.020

0.020

0.020

0.100

0.020

0.020

Results

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

QualifierRL

0.989

0.413

0.349

0.051

0.044

0.078

0.264

2.38

0.281

1.09

0.079

1.74

0.383

0.079

0.081

0.721

1.47

0.079

0.098

0.081

0.109

0.319

0.126

0.092

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19


Matrix: Air

Sample Location:

L1938279-01Lab ID:

Field Prep:


48,TO-15-SIM08/24/19 17:28TS

Not Specified

MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--


Project Name:

Project Number:

Lab Number:

Report Date:

Sample Depth:

Serial_No:09111919:41

Page 37 of 45


1,4-Dioxane

Trichloroethene





Toluene


1,2-Dibromoethane

Tetrachloroethene


Chlorobenzene

Ethylbenzene

p/m-Xylene

Bromoform

Styrene


o-Xylene

Isopropylbenzene

4-Ethyltoluene

1,3,5-Trimethybenzene


Benzyl chloride

1,3-Dichlorobenzene

1,4-Dichlorobenzene

sec-Butylbenzene

Parameter Results

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL



CANISTER QC BAT

L1938279

0.020

0.100

0.020

0.020

0.500

0.020

0.020

0.050

0.020

0.020

0.020

0.020

0.100

0.020

0.040

0.020

0.020

0.020

0.020

0.200

0.020

0.020

0.020

0.200

0.020

0.020

0.200

Results

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

QualifierRL

0.134

0.360

0.107

0.091

2.05

0.091

0.109

0.188

0.170

0.154

0.136

0.137

0.461

0.087

0.174

0.207

0.085

0.137

0.087

0.983

0.098

0.098

0.098

1.04

0.120

0.120

1.10

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19


Sample Location:

L1938279-01Lab ID:


MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--


Project Name:

Project Number:

Lab Number:

Report Date:

Sample Depth:

Serial_No:09111919:41

Page 38 of 45

p-Isopropyltoluene

1,2-Dichlorobenzene

n-Butylbenzene


Naphthalene


Hexachlorobutadiene

Parameter Results

ND

ND

ND

ND

ND

ND

ND

RL



CANISTER QC BAT

L1938279

0.200

0.020

0.200

0.050

0.050

0.050

0.050

Results

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

QualifierRL

1.10

0.120

1.10

0.371

0.262

0.371

0.533

1

1

1

1

1

1

1

ppbV ug/m3

09/11/19


Sample Location:

L1938279-01Lab ID:


MDL MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

1,4-difluorobenzene

bromochloromethane

chlorobenzene-d5

99

100

94


Criteria

60-140

60-140

60-140


Project Name:

Project Number:

Lab Number:

Report Date:

Sample Depth:

Serial_No:09111919:41

Page 39 of 45


L1940152-01A

L1940152-02A

L1940152-03A

L1940152-04A

L1940152-05A

Canister - 2.7 Liter





NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

NA Present/IntactCooler Custody SealCooler Information


10831

TO15-LL(30)

TO15-LL(30)

TO15-LL(30)

TO15-LL(30)

TO15-LL(30)

Project Name:

Project Number:

L1940152Lab Number:

Report Date:




Analysis(*)

09/11/19


FrozenDate/Time

FinalpH

Initial pH

Serial_No:09111919:41

Page 40 of 45

Report Format: Data Usability Report

GLOSSARY

Project Name:

Project Number:

Lab Number:

Report Date:

L194015290-02 168TH ST, JAMAICA, NY

10831 09/11/19

Acronyms

DL

EDL

EMPC

EPA

LCS

LCSD

LFB

LOD

LOQ

MDL

MS

MSD

NA

NC

NDPA/DPA

NI

NP

RL

RPD

SRM

STLP

TEF

TEQ

TIC






Not Applicable.


Not Ignitable.





-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

Footnotes

Serial_No:09111919:41

Page 41 of 45

Report Format: Data Usability Report

Project Name:

Project Number:

Lab Number:

Report Date:


10831 09/11/19

Terms


Data Qualifiers

A

B

C

D

E

G

H

I

J

M

ND

NJ

P

Q

R

RE

S

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-




Estimated value. This represents an estimated concentration for Tentatively Identified Compounds (TICs).

Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.

Not detected at the reporting limit (RL) for the sample.






-

Serial_No:09111919:41

Page 42 of 45




48 Compendium of Methods for the Determination of Toxic Organic Compounds in AmbientAir. Second Edition. EPA/625/R-96/010b, January 1999.

Project Name:

Project Number:

Lab Number:

Report Date:


10831

REFERENCES

09/11/19

Serial_No:09111919:41

Page 43 of 45











Mansfield Facility:




Serial_No:09111919:41

Page 44 of 45

Serial_No:09111919:41

Page 45 of 45

L1939567


10831

90-02 168TH ST, JAMAICA, QUEEN

Client:

Project Name:

Project Number:

09/06/19


Lab Number:

Report Date:


12A Maple Avenue


Jesse MausnerATTN:

ANALYTICAL REPORT

Certifications & Approvals: MA (M-MA086), NH NELAP (2064), CT (PH-0574), IL (200077), ME (MA00086), MD (348), NJ (MA935), NY (11148), NC (25700/666), PA (68-03671), RI (LAO00065), TX (T104704476), VT (VT-0935), VA (460195), USDA (Permit #P330-17-00196).

(973) 808-9050Phone:


Serial_No:09061913:32

Page 1 of 152

L1939567-01

L1939567-02

L1939567-03

L1939567-04

L1939567-05

L1939567-06

L1939567-07

L1939567-08

Alpha Sample ID

SESI-SB-1 (2-3)

SESI-SB-2 (3-4)

SESI-SB-3 (2-3)

SESI-SB-4 (2-3)

SESI-SB-5 (4-5)

SESI-SB-6 (1-2)

SESI-SB-7 (3-4)

SESI-SB-8 (2-3)

Client ID

JAMAICA, NY

JAMAICA, NY

JAMAICA, NY

JAMAICA, NY

JAMAICA, NY

JAMAICA, NY

JAMAICA, NY

JAMAICA, NY

Sample Location


10831



L193956709/06/19

08/29/19 10:10

08/29/19 10:35

08/29/19 11:05

08/29/19 12:05

08/29/19 12:35

08/29/19 13:30

08/29/19 14:30

08/29/19 15:15


SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

08/29/19

08/29/19

08/29/19

08/29/19

08/29/19

08/29/19

08/29/19

08/29/19

Serial_No:09061913:32

Page 2 of 152


10831

Project Name:

Project Number:

Lab Number:


09/06/19

Case Narrative

























Serial_No:09061913:32

Page 3 of 152



10831

Project Name:

Project Number:

Lab Number:


09/06/19

Report Submission


MDL column.


L1939567-01 and -08: The sample has elevated detection limits due to the dilution required by the sample

matrix.

Total Metals

L1939567-01 through -08: The sample has elevated detection limits for all elements, with the exception of


Cyanide, Total



original analyses are reported.




Serial_No:09061913:32

Page 4 of 152

ORGANICS

Serial_No:09061913:32

Page 5 of 152

VOLATILES

Serial_No:09061913:32

Page 6 of 152

FF

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.41

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

5.1

1.0

1.5

1.0

1.0

1.0

1.0

0.51

0.51

4.1

1.0

0.51

0.51

1.0

0.51

0.51

0.51

4.1

0.51

0.51

1.0

1.0

4.1

2.0

1.0

2.0

1.0

1.5

09/06/19


JAMAICA, NYSample Location:

L1939567-01Lab ID:



1,8260C09/06/19 01:27MV 93%Percent Solids:

MDL

2.3

0.15

0.14

0.24

0.13

0.14

0.27

0.20

0.13

0.71

0.26

0.17

0.11

0.28

0.16

0.16

0.16

0.25

0.17

0.17

0.56

0.14

0.96

0.60

0.34

0.46

0.24

0.14

Sample Depth:

Serial_No:09061913:32

Page 7 of 152

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

1.1

ND

ND

ND

ND

0.41

ND

ND

ND

140

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

0.51

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

1.0

2.0

1.0

10

10

10

10

10

10

2.0

10

2.0

2.0

1.0

2.0

0.51

2.0

1.0

1.0

2.0

2.0

2.0

3.1

4.1

1.0

1.0

4.1

4.1

09/06/19



L1939567-01Lab ID:


MDL

0.14

0.15

0.15

0.18

0.21

0.57

0.30

0.30

0.18

0.14

0.24

0.20

0.94

4.9

4.7

2.3

2.2

1.3

0.13

1.2

0.21

0.21

0.29

0.17

0.14

0.15

0.17

0.15

0.12

0.20

0.11

1.0

0.17

0.11

0.11

0.67

1.2

Sample Depth:

Serial_No:09061913:32

Page 8 of 152

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

1.0

2.0

2.0

2.0

2.0

82

2.0

2.0

2.0

2.0

5.1


Toluene-d8



120

111

121

91

70-130

70-130

70-130

70-130


09/06/19



L1939567-01Lab ID:


Total TIC Compounds

Unknown

Cyclotrisiloxane, Hexamethyl-

J

J

NJ

5.27

2.42

2.85

ug/kg

ug/kg

ug/kg

1

1

1


MDL

0.18

0.33

0.28

0.20

0.34

36.

0.18

0.39

0.20

0.35

1.4

Sample Depth:

Serial_No:09061913:32

Page 9 of 152

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.65

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

4.6

0.93

1.4

0.93

0.93

0.93

0.93

0.46

0.46

3.7

0.93

0.46

0.46

0.93

0.46

0.46

0.46

3.7

0.46

0.46

0.93

0.93

3.7

1.9

0.93

1.9

0.93

1.4

09/06/19



L1939567-02Lab ID:



1,8260C09/05/19 13:49NLK 96%Percent Solids:

MDL

2.1

0.14

0.13

0.21

0.12

0.13

0.25

0.18

0.12

0.65

0.24

0.16

0.10

0.25

0.15

0.15

0.15

0.23

0.15

0.15

0.50

0.13

0.87

0.54

0.31

0.42

0.22

0.13

Sample Depth:

Serial_No:09061913:32

Page 10 of 152

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

1.0

ND

ND

ND

ND

0.65

ND

ND

ND

180

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

0.46

1.9

1.9

1.9

1.9

1.9

0.93

0.93

0.93

0.93

1.9

0.93

9.3

9.3

9.3

9.3

9.3

9.3

1.9

9.3

1.9

1.9

0.93

1.9

0.46

1.9

0.93

0.93

1.9

1.9

1.9

2.8

3.7

0.93

0.93

3.7

3.7

09/06/19



L1939567-02Lab ID:


MDL

0.13

0.13

0.14

0.16

0.19

0.52

0.27

0.27

0.16

0.13

0.22

0.18

0.85

4.5

4.2

2.1

2.0

1.2

0.12

1.1

0.19

0.19

0.26

0.16

0.12

0.14

0.16

0.14

0.11

0.18

0.10

0.93

0.16

0.10

0.10

0.60

1.1

Sample Depth:

Serial_No:09061913:32

Page 11 of 152

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

0.93

1.9

1.9

1.9

1.9

74

1.9

1.9

1.9

1.9

4.6


Toluene-d8



123

108

109

95

70-130

70-130

70-130

70-130


09/06/19



L1939567-02Lab ID:


Total TIC Compounds

Unknown

Unknown


J

J

J

NJ

7.65

2.69

2.20

2.76

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1


MDL

0.16

0.30

0.25

0.18

0.31

33.

0.16

0.36

0.18

0.32

1.3

Sample Depth:

Serial_No:09061913:32

Page 12 of 152

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.56

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

5.2

1.0

1.6

1.0

1.0

1.0

1.0

0.52

0.52

4.2

1.0

0.52

0.52

1.0

0.52

0.52

0.52

4.2

0.52

0.52

1.0

1.0

4.2

2.1

1.0

2.1

1.0

1.6

09/06/19



L1939567-03Lab ID:




MDL

2.4

0.15

0.15

0.24

0.13

0.15

0.28

0.20

0.13

0.73

0.27

0.18

0.11

0.29

0.16

0.16

0.17

0.26

0.17

0.17

0.57

0.15

0.98

0.61

0.35

0.47

0.25

0.14

Sample Depth:

Serial_No:09061913:32

Page 13 of 152

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

1.0

ND

ND

ND

ND

0.56

ND

ND

ND

76

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

0.52

2.1

2.1

2.1

2.1

2.1

1.0

1.0

1.0

1.0

2.1

1.0

10

10

10

10

10

10

2.1

10

2.1

2.1

1.0

2.1

0.52

2.1

1.0

1.0

2.1

2.1

2.1

3.1

4.2

1.0

1.0

4.2

4.2

09/06/19



L1939567-03Lab ID:


MDL

0.14

0.15

0.16

0.18

0.21

0.59

0.30

0.30

0.18

0.14

0.25

0.20

0.96

5.0

4.8

2.3

2.2

1.3

0.13

1.2

0.21

0.21

0.29

0.18

0.14

0.15

0.18

0.15

0.12

0.20

0.11

1.0

0.18

0.11

0.11

0.68

1.2

Sample Depth:

Serial_No:09061913:32

Page 14 of 152

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

1.0

2.1

2.1

2.1

2.1

84

2.1

2.1

2.1

2.1

5.2


Toluene-d8



124

108

112

95

70-130

70-130

70-130

70-130


09/06/19



L1939567-03Lab ID:


Total TIC Compounds


J

NJ

3.09

3.09

ug/kg

ug/kg

1

1


MDL

0.18

0.34

0.28

0.20

0.35

37.

0.18

0.40

0.20

0.36

1.5

Sample Depth:

Serial_No:09061913:32

Page 15 of 152

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.36

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

4.9

0.98

1.5

0.98

0.98

0.98

0.98

0.49

0.49

3.9

0.98

0.49

0.49

0.98

0.49

0.49

0.49

3.9

0.49

0.49

0.98

0.98

3.9

2.0

0.98

2.0

0.98

1.5

09/06/19



L1939567-04Lab ID:




MDL

2.2

0.14

0.14

0.22

0.12

0.14

0.26

0.19

0.12

0.68

0.25

0.16

0.11

0.27

0.15

0.15

0.16

0.24

0.16

0.16

0.53

0.14

0.91

0.57

0.33

0.44

0.23

0.13

Sample Depth:

Serial_No:09061913:32

Page 16 of 152

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

0.77

ND

ND

ND

ND

0.36

ND

ND

ND

98

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

0.49

2.0

2.0

2.0

2.0

2.0

0.98

0.98

0.98

0.98

2.0

0.98

9.8

9.8

9.8

9.8

9.8

9.8

2.0

9.8

2.0

2.0

0.98

2.0

0.49

2.0

0.98

0.98

2.0

2.0

2.0

2.9

3.9

0.98

0.98

3.9

3.9

09/06/19



L1939567-04Lab ID:


MDL

0.13

0.14

0.14

0.17

0.20

0.55

0.28

0.28

0.17

0.13

0.23

0.19

0.89

4.7

4.4

2.2

2.1

1.2

0.12

1.2

0.20

0.20

0.27

0.16

0.13

0.14

0.16

0.14

0.12

0.19

0.10

0.97

0.16

0.11

0.11

0.63

1.1

Sample Depth:

Serial_No:09061913:32

Page 17 of 152

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

0.98

2.0

2.0

2.0

2.0

78

2.0

2.0

2.0

2.0

4.9


Toluene-d8



126

107

112

95

70-130

70-130

70-130

70-130


09/06/19



L1939567-04Lab ID:


Total TIC Compounds


J

NJ

2.96

2.96

ug/kg

ug/kg

1

1


MDL

0.17

0.31

0.26

0.19

0.32

34.

0.17

0.37

0.19

0.33

1.4

Sample Depth:

Serial_No:09061913:32

Page 18 of 152

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.53

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

4.6

0.92

1.4

0.92

0.92

0.92

0.92

0.46

0.46

3.7

0.92

0.46

0.46

0.92

0.46

0.46

0.46

3.7

0.46

0.46

0.92

0.92

3.7

1.8

0.92

1.8

0.92

1.4

09/06/19



L1939567-05Lab ID:




MDL

2.1

0.13

0.13

0.21

0.11

0.13

0.24

0.18

0.12

0.64

0.24

0.15

0.10

0.25

0.14

0.14

0.15

0.23

0.15

0.15

0.50

0.13

0.86

0.53

0.31

0.42

0.22

0.12

Sample Depth:

Serial_No:09061913:32

Page 19 of 152

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

0.81

ND

ND

ND

ND

0.53

ND

ND

ND

150

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

0.46

1.8

1.8

1.8

1.8

1.8

0.92

0.92

0.92

0.92

1.8

0.92

9.2

9.2

9.2

9.2

9.2

9.2

1.8

9.2

1.8

1.8

0.92

1.8

0.46

1.8

0.92

0.92

1.8

1.8

1.8

2.8

3.7

0.92

0.92

3.7

3.7

09/06/19



L1939567-05Lab ID:


MDL

0.12

0.13

0.14

0.16

0.18

0.51

0.27

0.27

0.16

0.12

0.22

0.18

0.84

4.4

4.2

2.0

2.0

1.2

0.12

1.1

0.19

0.18

0.26

0.15

0.12

0.13

0.15

0.13

0.11

0.18

0.10

0.92

0.16

0.10

0.10

0.60

1.0

Sample Depth:

Serial_No:09061913:32

Page 20 of 152

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

0.92

1.8

1.8

1.8

1.8

74

1.8

1.8

1.8

1.8

4.6


Toluene-d8



124

108

112

92

70-130

70-130

70-130

70-130


09/06/19



L1939567-05Lab ID:


Total TIC Compounds


J

NJ

2.70

2.70

ug/kg

ug/kg

1

1


MDL

0.16

0.30

0.25

0.18

0.31

32.

0.16

0.35

0.18

0.31

1.3

Sample Depth:

Serial_No:09061913:32

Page 21 of 152

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.64

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

6.1

1.2

1.8

1.2

1.2

1.2

1.2

0.61

0.61

4.8

1.2

0.61

0.61

1.2

0.61

0.61

0.61

4.8

0.61

0.61

1.2

1.2

4.8

2.4

1.2

2.4

1.2

1.8

09/06/19



L1939567-06Lab ID:




MDL

2.8

0.18

0.17

0.28

0.15

0.17

0.32

0.24

0.15

0.84

0.31

0.20

0.13

0.33

0.19

0.19

0.19

0.30

0.20

0.20

0.66

0.17

1.1

0.70

0.41

0.55

0.29

0.17

Sample Depth:

Serial_No:09061913:32

Page 22 of 152

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

1.1

ND

ND

ND

ND

0.64

ND

ND

ND

14

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

0.61

2.4

2.4

2.4

2.4

2.4

1.2

1.2

1.2

1.2

2.4

1.2

12

12

12

12

12

12

2.4

12

2.4

2.4

1.2

2.4

0.61

2.4

1.2

1.2

2.4

2.4

2.4

3.6

4.8

1.2

1.2

4.8

4.8

09/06/19



L1939567-06Lab ID:


MDL

0.17

0.17

0.18

0.21

0.24

0.68

0.35

0.35

0.21

0.17

0.29

0.24

1.1

5.8

5.5

2.7

2.6

1.6

0.15

1.4

0.25

0.24

0.34

0.20

0.16

0.18

0.20

0.18

0.14

0.23

0.13

1.2

0.20

0.13

0.13

0.79

1.4

Sample Depth:

Serial_No:09061913:32

Page 23 of 152

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

1.2

2.4

2.4

2.4

2.4

97

2.4

2.4

2.4

2.4

6.1


Toluene-d8



127

109

113

96

70-130

70-130

70-130

70-130


09/06/19



L1939567-06Lab ID:


Total TIC Compounds


Unknown Alkane

J

NJ

J

6.70

3.93

2.77

ug/kg

ug/kg

ug/kg

1

1

1


MDL

0.21

0.39

0.33

0.23

0.40

43.

0.21

0.47

0.23

0.41

1.7

Sample Depth:

Serial_No:09061913:32

Page 24 of 152

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.38

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

6.4

1.3

1.9

1.3

1.3

1.3

1.3

0.64

0.64

5.2

1.3

0.64

0.64

1.3

0.64

0.64

0.64

5.2

0.64

0.64

1.3

1.3

5.2

2.6

1.3

2.6

1.3

1.9

09/06/19



L1939567-07Lab ID:




MDL

3.0

0.19

0.18

0.30

0.16

0.18

0.34

0.25

0.16

0.90

0.33

0.22

0.14

0.35

0.20

0.20

0.20

0.32

0.21

0.21

0.70

0.18

1.2

0.75

0.43

0.58

0.31

0.18

Sample Depth:

Serial_No:09061913:32

Page 25 of 152

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

1.2

ND

ND

ND

ND

0.38

ND

ND

ND

220

ND

27

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

0.64

2.6

2.6

2.6

2.6

2.6

1.3

1.3

1.3

1.3

2.6

1.3

13

13

13

13

13

13

2.6

13

2.6

2.6

1.3

2.6

0.64

2.6

1.3

1.3

2.6

2.6

2.6

3.9

5.2

1.3

1.3

5.2

5.2

09/06/19



L1939567-07Lab ID:


MDL

0.18

0.18

0.19

0.22

0.26

0.72

0.37

0.37

0.22

0.18

0.31

0.25

1.2

6.2

5.9

2.9

2.8

1.6

0.16

1.5

0.26

0.26

0.36

0.22

0.17

0.19

0.22

0.19

0.15

0.25

0.14

1.3

0.22

0.14

0.14

0.84

1.5

Sample Depth:

Serial_No:09061913:32

Page 26 of 152

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

1.3

2.6

2.6

2.6

2.6

100

2.6

2.6

2.6

2.6

6.4


Toluene-d8



128

108

116

96

70-130

70-130

70-130

70-130


09/06/19



L1939567-07Lab ID:


Total TIC Compounds

Unknown Alkane

Unknown

Unknown Alkene

J

J

J

J

11.7

3.41

3.62

4.66

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1


MDL

0.22

0.41

0.35

0.25

0.43

45.

0.23

0.49

0.25

0.44

1.8

Sample Depth:

Serial_No:09061913:32

Page 27 of 152

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.47

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

5.6

1.1

1.7

1.1

1.1

1.1

1.1

0.56

0.56

4.4

1.1

0.56

0.56

1.1

0.56

0.56

0.56

4.4

0.56

0.56

1.1

1.1

4.4

2.2

1.1

2.2

1.1

1.7

09/06/19



L1939567-08Lab ID:




MDL

2.5

0.16

0.16

0.26

0.14

0.16

0.30

0.22

0.14

0.77

0.28

0.18

0.12

0.30

0.18

0.18

0.18

0.27

0.18

0.18

0.60

0.16

1.0

0.64

0.37

0.50

0.26

0.15

Sample Depth:

Serial_No:09061913:32

Page 28 of 152

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

1.0

ND

ND

ND

ND

0.47

ND

ND

ND

230

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

0.56

2.2

2.2

2.2

2.2

2.2

1.1

1.1

1.1

1.1

2.2

1.1

11

11

11

11

11

11

2.2

11

2.2

2.2

1.1

2.2

0.56

2.2

1.1

1.1

2.2

2.2

2.2

3.3

4.4

1.1

1.1

4.4

4.4

09/06/19



L1939567-08Lab ID:


MDL

0.15

0.16

0.16

0.19

0.22

0.62

0.32

0.32

0.19

0.15

0.26

0.22

1.0

5.3

5.0

2.5

2.4

1.4

0.14

1.3

0.23

0.22

0.31

0.18

0.15

0.16

0.18

0.16

0.13

0.21

0.12

1.1

0.19

0.12

0.12

0.72

1.3

Sample Depth:

Serial_No:09061913:32

Page 29 of 152

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

1.1

2.2

2.2

2.2

2.2

89

2.2

2.2

2.2

2.2

5.6


Toluene-d8



126

109

111

95

70-130

70-130

70-130

70-130


09/06/19



L1939567-08Lab ID:


Total TIC Compounds


Unknown

Unknown

J

NJ

J

J

11.1

5.24

3.11

2.76

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1


MDL

0.19

0.36

0.30

0.21

0.37

39.

0.20

0.43

0.21

0.38

1.6

Sample Depth:

Serial_No:09061913:32

Page 30 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Analytical Date:

09/06/19

Analyst: AD

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

5.0

1.0

1.5

1.0

1.0

1.0

1.0

0.50

0.50

4.0

1.0

0.50

0.50

1.0

0.50

0.50

0.50

4.0

0.50

0.50

1.0

1.0

4.0

2.0

1.0

2.0

1.0

1.5

0.50

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Volatile Organics by EPA 5035 Low - Westborough Lab for sample(s): 01 Batch: WG1280939-5

MDL

2.3

0.14

0.14

0.23

0.12

0.14

0.27

0.20

0.13

0.70

0.26

0.17

0.11

0.27

0.16

0.16

0.16

0.25

0.17

0.17

0.54

0.14

0.93

0.58

0.34

0.45

0.24

0.14

0.14

Serial_No:09061913:32

Page 31 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Analytical Date:

09/06/19

Analyst: AD

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

1.0

2.0

1.0

10

10

10

10

10

10

2.0

10

2.0

2.0

1.0

2.0

0.50

2.0

1.0

1.0

2.0

2.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

0.14

0.15

0.17

0.20

0.56

0.29

0.29

0.18

0.14

0.24

0.20

0.92

4.8

4.6

2.2

2.2

1.3

0.13

1.2

0.20

0.20

0.28

0.17

0.13

0.14

0.17

0.15

0.12

0.19

Serial_No:09061913:32

Page 32 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Analytical Date:

09/06/19

Analyst: AD

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.0

3.0

4.0

1.0

1.0

4.0

4.0

1.0

2.0

2.0

2.0

2.0

80

2.0

2.0

2.0

2.0

5.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier




MDL

0.11

1.0

0.17

0.11

0.11

0.65

1.2

0.17

0.32

0.27

0.19

0.33

35.

0.18

0.38

0.19

0.34

1.4

Serial_No:09061913:32

Page 33 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Analytical Date:

09/06/19

Analyst: AD




Toluene-d8



124

107

111

92

70-130

70-130

70-130

70-130


Criteria

MDL

Serial_No:09061913:32

Page 34 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Analytical Date:

09/06/19

Analyst: MV

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane






1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

Parameter Result

ND

ND

0.17

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

5.0

1.0

1.5

1.0

1.0

1.0

1.0

0.50

0.50

4.0

1.0

0.50

0.50

1.0

0.50

0.50

0.50

4.0

0.50

0.50

1.0

1.0

4.0

2.0

1.0

2.0

1.0

1.5

0.50

J

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

2.3

0.14

0.14

0.23

0.12

0.14

0.27

0.20

0.13

0.70

0.26

0.17

0.11

0.27

0.16

0.16

0.16

0.25

0.17

0.17

0.54

0.14

0.93

0.58

0.34

0.45

0.24

0.14

0.14

Serial_No:09061913:32

Page 35 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Analytical Date:

09/06/19

Analyst: MV

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

Xylenes, Total



Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

1.0

2.0

1.0

10

10

10

10

10

10

2.0

10

2.0

2.0

1.0

2.0

0.50

2.0

1.0

1.0

2.0

2.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

0.14

0.15

0.17

0.20

0.56

0.29

0.29

0.18

0.14

0.24

0.20

0.92

4.8

4.6

2.2

2.2

1.3

0.13

1.2

0.20

0.20

0.28

0.17

0.13

0.14

0.17

0.15

0.12

0.19

Serial_No:09061913:32

Page 36 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Analytical Date:

09/06/19

Analyst: MV

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

p-Ethyltoluene


Ethyl ether


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.0

3.0

4.0

1.0

1.0

4.0

4.0

1.0

2.0

2.0

2.0

2.0

80

2.0

2.0

2.0

2.0

5.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier




MDL

0.11

1.0

0.17

0.11

0.11

0.65

1.2

0.17

0.32

0.27

0.19

0.33

35.

0.18

0.38

0.19

0.34

1.4

Serial_No:09061913:32

Page 37 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Analytical Date:

09/06/19

Analyst: MV




Toluene-d8



120

108

114

93

70-130

70-130

70-130

70-130


Criteria

MDL

Serial_No:09061913:32

Page 38 of 152

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

91

106

100

105

97

102

107

98

95

95

115

108

99

127

104

107

104

105

93

107

114

149

107

92

107

101

106

97

100

106

98

95

96

115

108

102

126

103

110

107

102

94

107

114

143

108

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-139

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

52-130

57-147

1

1

1

1

0

2

1

0

0

1

0

0

3

1

1

3

3

3

1

0

0

4

1

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Volatile Organics by EPA 5035 Low - Westborough Lab Associated sample(s): 01 Batch: WG1280939-3 WG1280939-4


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual Qual

Q Q

Qual

Serial_No:09061913:32

Page 39 of 152

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

104

75

96

93

90

98

101

98

109

108

104

92

93

110

185

128

101

82

108

123

117

116

88

104

74

97

93

90

99

102

101

111

106

103

92

92

109

182

113

102

79

110

119

116

109

85

67-130

50-151

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

70-130

70-130

30-146

54-140

59-130

70-130

70-130

70-130

68-130

70-130

70-130

0

1

1

0

0

1

1

3

2

2

1

0

1

1

2

12

1

4

2

3

1

6

3

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual Qual

Q Q

Qual

Serial_No:09061913:32

Page 40 of 152

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

116

104

113

100

98

117

111

112

114

120

108

106

116

115

106

118

116

98

106

114

117

82

108

118

102

111

100

100

119

113

114

115

119

111

104

115

116

108

111

116

101

105

116

119

83

109

70-130

70-130

69-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

68-130

67-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

65-136

70-130

2

2

2

0

2

2

2

2

1

1

3

2

1

1

2

6

0

3

1

2

2

1

1

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual Qual Qual

Serial_No:09061913:32

Page 41 of 152

p-Ethyltoluene


Ethyl ether


108

111

93

133

109

110

93

138

70-130

70-130

67-130

70-130

1

1

0

4

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


12010911293

70-13070-13070-13070-130

11910811193


09/06/19

AcceptanceCriteria

Qual Qual

Q Q

Qual

Serial_No:09061913:32

Page 42 of 152

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

86

96

92

92

90

97

100

90

89

86

107

97

92

117

96

98

99

98

86

98

103

143

107

88

97

92

94

92

96

99

89

88

87

105

96

92

118

97

100

96

97

86

97

104

127

103

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-139

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

52-130

57-147

2

1

0

2

2

1

1

1

1

1

2

1

0

1

1

2

3

1

0

1

1

12

4

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual Qual

Q

Qual

Serial_No:09061913:32

Page 43 of 152

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

94

67

88

84

81

92

95

91

104

98

95

85

85

101

166

105

93

92

100

111

110

110

84

94

67

88

86

82

93

93

91

102

96

94

84

86

102

168

105

94

72

102

106

105

97

84

67-130

50-151

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

70-130

70-130

30-146

54-140

59-130

70-130

70-130

70-130

68-130

70-130

70-130

0

0

0

2

1

1

2

0

2

2

1

1

1

1

1

0

1

24

2

5

5

13

0

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual Qual

Q Q

Qual

Serial_No:09061913:32

Page 44 of 152

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

n-Propylbenzene





1,4-Dioxane

p-Diethylbenzene

107

100

104

91

93

108

104

105

106

109

103

98

107

106

103

104

108

96

99

106

110

82

99

106

96

104

92

92

107

105

104

106

108

94

98

106

106

99

105

107

92

95

107

110

79

99

70-130

70-130

69-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

68-130

67-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

65-136

70-130

1

4

0

1

1

1

1

1

0

1

9

0

1

0

4

1

1

4

4

1

0

4

0

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual Qual Qual

Serial_No:09061913:32

Page 45 of 152

p-Ethyltoluene


Ethyl ether


100

105

87

128

99

102

89

121

70-130

70-130

67-130

70-130

1

3

2

6

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


11710811592

70-13070-13070-13070-130

12011011394


09/06/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09061913:32

Page 46 of 152

SEMIVOLATILES

Serial_No:09061913:32

Page 47 of 152

FF

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

J

Dilution Factor

340

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

6100

ND

ND

ND

ND

ND

ND

ND

ND

160

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

710

880

530

790

880

880

880

880

880

880

880

530

880

880

1000

950

880

2500

710

790

880

790

710

880

880

880

880

880

09/06/19



L1939567-01Lab ID:


D



1,8270D09/05/19 10:13RC


93%Percent Solids:

MDL

91.

100

99.

120

88.

160

150

150

230

180

150

100

94.

130

150

88.

130

800

140

110

110

130

100

140

300

220

170

300

Sample Depth:

Serial_No:09061913:32

Page 48 of 152

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

Dilution Factor

ND

ND

3200

2800

3600

1500

2800

510

1400

1900

440

4600

380

2200

4700

ND

ND

ND

ND

ND

250

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

880

880

530

710

530

530

530

710

530

710

880

530

530

710

530

2000

880

880

880

880

880

1000

880

880

530

880

880

790

880

1900

1200

4200

2300

710

880

880

1300

09/06/19



L1939567-01Lab ID:


D

MDL

82.

180

99.

220

150

140

92.

140

170

100

86.

110

100

120

88.

200

160

170

170

360

84.

110

92.

110

170

130

100

140

290

330

360

410

420

190

130

140

140

Sample Depth:

Serial_No:09061913:32

Page 49 of 152


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

J

Dilution Factor

ND

ND

ND

690

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

5

5

5

5

5

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

880

2900

880

880

130

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

86

89

83

76

88

67

25-120

10-120

23-120

30-120

10-136

18-120


09/06/19



L1939567-01Lab ID:


D

Total TIC Compounds

Unknown PAH

Unknown PAH

Unknown PAH

Unknown

Unknown PAH

J

J

J

J

J

J

4120

752

740

775

894

954

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

5

5

5

5

5

5


MDL

170

890

270

86.

41.

Sample Depth:

Serial_No:09061913:32

Page 50 of 152

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

J

Dilution Factor

47

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

1100

ND

ND

ND

ND

ND

ND

ND

ND

39

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

140

170

100

150

170

170

170

170

170

170

170

100

170

170

200

180

170

480

140

150

170

150

140

170

170

170

170

170

09/06/19



L1939567-02Lab ID:




1,8270D09/05/19 03:30RC


96%Percent Solids:

MDL

17.

19.

19.

23.

17.

30.

29.

29.

45.

34.

29.

19.

18.

26.

29.

17.

25.

150

27.

22.

20.

25.

19.

26.

58.

42.

32.

57.

Sample Depth:

Serial_No:09061913:32

Page 51 of 152

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

Dilution Factor

ND

ND

630

550

690

280

580

27

190

330

53

710

100

370

960

ND

ND

ND

ND

ND

33

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

170

170

100

140

100

100

100

140

100

140

170

100

100

140

100

380

170

170

170

170

170

200

170

170

100

170

170

150

170

360

240

810

440

140

170

170

240

09/06/19



L1939567-02Lab ID:


MDL

16.

35.

19.

41.

28.

27.

18.

26.

33.

20.

16.

20.

20.

24.

17.

39.

31.

32.

32.

70.

16.

20.

18.

21.

32.

25.

20.

27.

56.

63.

69.

79.

81.

37.

25.

26.

26.

Sample Depth:

Serial_No:09061913:32

Page 52 of 152


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

J

Dilution Factor

ND

ND

ND

74

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

170

550

170

170

25

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

100

106

107

84

97

65

25-120

10-120

23-120

30-120

10-136

18-120


09/06/19



L1939567-02Lab ID:


Total TIC Compounds

Unknown

Unknown Ketone

Unknown PAH

Unknown PAH

Unknown PAH

Unknown PAH

Unknown PAH

Unknown PAH

Unknown

Unknown

J

J

J

J

J

J

J

J

J

J

J

4080

1390

156

229

175

140

168

211

164

1310

137

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1


MDL

32.

170

52.

16.

7.8

Sample Depth:

Serial_No:09061913:32

Page 53 of 152

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

1000

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

160

200

120

180

200

200

200

200

200

200

200

120

200

200

240

210

200

570

160

180

200

180

160

200

200

200

200

200

09/06/19



L1939567-03Lab ID:




1,8270D09/05/19 03:05RC


84%Percent Solids:

MDL

20.

23.

22.

27.

20.

36.

34.

35.

53.

40.

34.

23.

21.

30.

34.

20.

29.

180

32.

26.

24.

29.

22.

31.

69.

50.

38.

67.

Sample Depth:

Serial_No:09061913:32

Page 54 of 152

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

Dilution Factor

ND

ND

520

560

700

280

430

100

68

360

ND

130

91

400

940

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

200

200

120

160

120

120

120

160

120

160

200

120

120

160

120

450

200

200

200

200

200

240

200

200

120

200

200

180

200

430

280

950

520

160

200

200

280

09/06/19



L1939567-03Lab ID:


MDL

18.

42.

22.

48.

33.

32.

21.

31.

39.

23.

19.

24.

23.

28.

20.

46.

36.

38.

37.

82.

19.

24.

21.

24.

38.

30.

23.

32.

65.

74.

81.

92.

95.

44.

30.

31.

31.

Sample Depth:

Serial_No:09061913:32

Page 55 of 152


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane


ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

200

640

200

200

30

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

108

112

113

91

109

75

25-120

10-120

23-120

30-120

10-136

18-120


09/06/19



L1939567-03Lab ID:


Total TIC Compounds

Unknown

Unknown PAH

Unknown PAH

Unknown

J

J

J

J

J

3600

1550

162

268

1620

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1


MDL

38.

200

61.

19.

9.1

Sample Depth:

Serial_No:09061913:32

Page 56 of 152

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

J

Dilution Factor

95

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

2400

ND

ND

ND

ND

ND

ND

ND

ND

60

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

150

190

120

170

190

190

190

190

190

190

190

120

190

190

230

210

190

550

150

170

190

170

150

190

190

190

190

190

09/06/19



L1939567-04Lab ID:




1,8270D09/05/19 07:17RC


85%Percent Solids:

MDL

20.

22.

22.

26.

19.

34.

33.

34.

51.

38.

33.

22.

20.

29.

33.

19.

28.

170

31.

25.

23.

28.

22.

30.

66.

48.

36.

65.

Sample Depth:

Serial_No:09061913:32

Page 57 of 152

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

Dilution Factor

ND

ND

1300

1100

1200

500

1100

270

590

800

160

1900

210

850

2200

ND

ND

ND

ND

ND

84

38

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

190

190

120

150

120

120

120

150

120

150

190

120

120

150

120

440

190

190

190

190

190

230

190

190

120

190

190

170

190

410

270

920

500

150

190

190

280

09/06/19



L1939567-04Lab ID:


MDL

18.

40.

22.

47.

32.

31.

20.

30.

37.

22.

19.

23.

22.

27.

19.

44.

35.

37.

36.

79.

18.

23.

20.

24.

36.

29.

23.

31.

63.

72.

78.

89.

92.

42.

29.

30.

30.

Sample Depth:

Serial_No:09061913:32

Page 58 of 152


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane


ND

ND

ND

230

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

190

620

190

190

29

09/06/19



L1939567-04Lab ID:


Total TIC Compounds

Unknown Ketone

Unknown

Unknown Ketone

Unknown PAH

Unknown PAH

Unknown PAH

Unknown

Unknown

Unknown PAH

Unknown Thiophene

Unknown

Unknown PAH

Unknown PAH

Unknown PAH

Unknown PAH

Unknown

Unknown PAH

Unknown

J

J

J

J

J

J

J

J

J

J

J

J

J

J

J

J

J

J

J

4620

158

217

170

242

283

301

159

397

223

169

483

175

242

157

333

487

262

166

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1


MDL

37.

190

59.

19.

8.8

Sample Depth:

Serial_No:09061913:32

Page 59 of 152



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

93

99

96

78

98

60

25-120

10-120

23-120

30-120

10-136

18-120


09/06/19



L1939567-04Lab ID:


MDL

Sample Depth:

Serial_No:09061913:32

Page 60 of 152

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

150

190

110

170

190

190

190

190

190

190

190

110

190

190

220

200

190

540

150

170

190

170

150

190

190

190

190

190

09/06/19



L1939567-05Lab ID:




1,8270D09/05/19 02:15RC


89%Percent Solids:

MDL

19.

21.

21.

25.

19.

34.

32.

33.

50.

38.

32.

22.

20.

29.

32.

19.

27.

170

30.

24.

23.

28.

21.

29.

65.

47.

36.

64.

Sample Depth:

Serial_No:09061913:32

Page 61 of 152

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

190

190

110

150

110

110

110

150

110

150

190

110

110

150

110

430

190

190

190

190

190

220

190

190

110

190

190

170

190

400

260

900

490

150

190

190

270

09/06/19



L1939567-05Lab ID:


MDL

17.

39.

21.

46.

32.

30.

20.

29.

36.

22.

18.

23.

22.

26.

19.

44.

34.

36.

35.

78.

18.

23.

20.

23.

36.

28.

22.

30.

62.

70.

76.

87.

90.

41.

28.

29.

29.

Sample Depth:

Serial_No:09061913:32

Page 62 of 152


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane


ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

190

610

190

190

28

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

86

91

86

76

91

69

25-120

10-120

23-120

30-120

10-136

18-120


09/06/19



L1939567-05Lab ID:




MDL

36.

190

57.

18.

8.6

Sample Depth:

Serial_No:09061913:32

Page 63 of 152

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

60

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

160

210

120

180

210

210

210

210

210

210

210

120

210

210

250

220

210

590

160

180

210

180

160

210

210

210

210

210

09/06/19



L1939567-06Lab ID:




1,8270D09/05/19 02:40RC


79%Percent Solids:

MDL

21.

24.

23.

28.

20.

37.

35.

36.

55.

41.

35.

24.

22.

31.

35.

21.

30.

190

33.

27.

25.

30.

23.

32.

71.

52.

39.

70.

Sample Depth:

Serial_No:09061913:32

Page 64 of 152

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

J

J

Dilution Factor

ND

ND

39

ND

47

ND

34

ND

ND

27

ND

29

ND

ND

48

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

210

210

120

160

120

120

120

160

120

160

210

120

120

160

120

470

210

210

210

210

210

250

210

210

120

210

210

180

210

440

290

990

540

160

210

210

300

09/06/19



L1939567-06Lab ID:


MDL

19.

43.

23.

50.

35.

33.

21.

32.

40.

24.

20.

25.

24.

29.

20.

48.

38.

40.

39.

85.

20.

25.

22.

26.

39.

31.

24.

33.

68.

78.

84.

96.

99.

45.

31.

32.

32.

Sample Depth:

Serial_No:09061913:32

Page 65 of 152


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane


ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

210

670

210

210

31

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

96

99

95

82

96

75

25-120

10-120

23-120

30-120

10-136

18-120


09/06/19



L1939567-06Lab ID:


Total TIC Compounds

Unknown

Unknown

J

J

J

1230

595

639

ug/kg

ug/kg

ug/kg

1

1

1


MDL

40.

210

63.

20.

9.5

Sample Depth:

Serial_No:09061913:32

Page 66 of 152

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

J

Dilution Factor

97

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

770

ND

ND

ND

ND

ND

ND

ND

ND

210

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

190

240

140

220

240

240

240

240

240

240

240

140

240

240

290

260

240

680

190

220

240

220

190

240

240

240

240

240

09/06/19



L1939567-07Lab ID:




1,8270D09/06/19 03:13EK


69%Percent Solids:

MDL

25.

27.

27.

32.

24.

43.

41.

42.

64.

48.

41.

27.

26.

36.

41.

24.

35.

220

39.

31.

29.

35.

27.

37.

83.

60.

45.

81.

Sample Depth:

Serial_No:09061913:32

Page 67 of 152

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

J

J

J

Dilution Factor

ND

ND

400

340

430

160

350

81

180

240

100

700

65

260

700

ND

ND

ND

ND

ND

50

120

ND

59

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

53

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

240

240

140

190

140

140

140

190

140

190

240

140

140

190

140

540

240

240

240

240

240

290

240

240

140

240

240

220

240

520

330

1100

620

190

240

240

340

09/06/19



L1939567-07Lab ID:


MDL

22.

50.

27.

58.

40.

38.

25.

37.

47.

28.

23.

29.

28.

33.

24.

55.

44.

46.

45.

99.

23.

29.

25.

30.

45.

36.

28.

38.

79.

90.

98.

110

110

52.

36.

37.

37.

Sample Depth:

Serial_No:09061913:32

Page 68 of 152


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

J

Dilution Factor

ND

ND

ND

79

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

240

770

240

240

36

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

96

102

98

80

99

66

25-120

10-120

23-120

30-120

10-136

18-120


09/06/19



L1939567-07Lab ID:


Total TIC Compounds

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

J

J

J

J

J

J

J

3450

221

230

416

546

1680

359

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1


MDL

46.

240

73.

23.

11.

Sample Depth:

Serial_No:09061913:32

Page 69 of 152

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

J

Dilution Factor

130

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

3200

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

810

1000

610

910

1000

1000

1000

1000

1000

1000

1000

610

1000

1000

1200

1100

1000

2900

810

910

1000

910

810

1000

1000

1000

1000

1000

09/06/19



L1939567-08Lab ID:


D



1,8270D09/05/19 10:38RC


81%Percent Solids:

MDL

100

120

110

140

100

180

170

180

270

200

170

120

110

150

170

100

150

920

160

130

120

150

110

160

350

250

190

340

Sample Depth:

Serial_No:09061913:32

Page 70 of 152

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

J

J

J

Dilution Factor

ND

ND

1600

1100

1500

600

1400

280

640

690

240

2500

170

780

2300

ND

ND

ND

ND

ND

110

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

1000

1000

610

810

610

610

610

810

610

810

1000

610

610

810

610

2300

1000

1000

1000

1000

1000

1200

1000

1000

610

1000

1000

910

1000

2200

1400

4800

2600

810

1000

1000

1400

09/06/19



L1939567-08Lab ID:


D

MDL

94.

210

110

250

170

160

100

160

200

120

98.

120

120

140

100

230

180

190

190

420

96.

120

100

120

190

150

120

160

330

380

410

470

480

220

150

160

160

Sample Depth:

Serial_No:09061913:32

Page 71 of 152


Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

J

Dilution Factor

ND

ND

ND

470

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

5

5

5

5

5

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

1000

3300

1000

1000

150

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

86

85

79

74

76

63

25-120

10-120

23-120

30-120

10-136

18-120


09/06/19



L1939567-08Lab ID:


D



MDL

190

1000

310

98.

46.

Sample Depth:

Serial_No:09061913:32

Page 72 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567



09/06/19

Analyst: RC

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA




Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

130

160

100

150

160

160

160

160

160

160

160

100

160

160

200

180

160

470

130

150

160

150

130

160

160

160

160

160

160

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

17.

19.

18.

22.

16.

30.

28.

29.

44.

33.

28.

19.

18.

25.

28.

17.

24.

150

27.

22.

20.

24.

19.

26.

57.

42.

31.

56.

15.

Serial_No:09061913:32

Page 73 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567



09/06/19

Analyst: RC

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

160

100

130

100

100

100

130

100

130

160

100

100

130

100

380

160

160

160

160

160

200

160

160

100

160

160

150

160

360

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

35.

19.

40.

28.

26.

17.

26.

32.

20.

16.

20.

19.

23.

16.

38.

30.

32.

31.

69.

16.

20.

17.

20.

31.

25.

20.

27.

55.

62.

Serial_No:09061913:32

Page 74 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567



09/06/19

Analyst: RC

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

230

800

430

130

160

160

240

160

540

160

160

25

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

101

105

97

91

106

102

25-120

10-120

23-120

30-120

10-136

18-120


Criteria



MDL

68.

77.

80.

36.

25.

26.

26.

32.

170

51.

16.

7.6

Serial_No:09061913:32

Page 75 of 152

Acenaphthene


Hexachlorobenzene


2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene





Hexachlorobutadiene


Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA

98

93

102

94

96

98

88

89

90

116

116

104

97

95

76

101

90

64

94

109

94

98

99

88

75

98

77

84

68

60

64

97

110

106

101

89

94

62

91

74

52

66

94

81

81

96

31-137

38-107

40-140

40-140

40-140

40-140

40-140

28-104

40-140

40-132

40-140

40-140

40-140

40-140

40-140

40-117

40-140

40-140

40-140

40-140

40-140

40-140

36-157

11

21

4

20

13

36

38

33

7

5

9

3

9

1

20

10

20

21

35

15

15

19

3

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual Qual Qual

Serial_No:09061913:32

Page 76 of 152




Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

106

120

121

124

132

105

102

103

92

97

103

97

98

103

110

104

95

114

118

98

103

82

115

94

122

120

122

132

104

95

104

90

92

98

98

88

101

120

96

95

124

128

96

94

78

106

32-121

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

35-142

37-127

40-140

47-134

12

2

1

2

0

1

7

1

2

5

5

1

11

2

9

8

0

8

8

2

9

5

8

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual Qual Qual

Serial_No:09061913:32

Page 77 of 152

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene


Acetophenone


p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol


Pentachlorophenol

Phenol

2-Methylphenol



Benzoic Acid

Benzyl Alcohol

Carbazole

83

98

101

95

100

104

105

113

108

107

102

111

105

84

120

84

94

111

117

108

64

110

104

87

94

93

84

89

88

91

99

90

95

90

96

100

87

118

85

81

97

103

100

64

95

103

26-129

41-125

40-140

40-140

40-117

14-144

30-130

26-103

25-102

30-130

30-130

30-130

11-114

4-130

10-130

17-109

26-90

30-130.

30-130

30-130

10-110

40-140

54-128

5

4

8

12

12

17

14

13

18

12

13

14

5

4

2

1

15

13

13

8

0

15

1

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual Qual

Q

Q

Q

Qual

Serial_No:09061913:32

Page 78 of 152

1,4-Dioxane 71 38 40-140 61 50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


10711310899111104

25-12010-12023-12030-12010-13618-120

80968986107101


09/06/19

AcceptanceCriteria

Qual Qual

Q

Qual

Q

Serial_No:09061913:32

Page 79 of 152

PCBS

Serial_No:09061913:32

Page 80 of 152

FF

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

9.22

ND

ND

9.22

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

35.4

35.4

35.4

35.4

35.4

35.4

35.4

35.4

35.4

35.4


Decachlorobiphenyl


Decachlorobiphenyl

66

36

60

59

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/06/19



L1939567-01Lab ID:




1,8082A09/05/19 04:21HT

EPA 3546



93%Percent Solids:

MDL

3.14

3.54

7.50

4.77

5.30

3.87

6.53

4.49

3.66

3.14

A

A

A

A

A

A

B

A

A

B

Column

Sample Depth:

Serial_No:09061913:32

Page 81 of 152

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

32.6

32.6

32.6

32.6

32.6

32.6

32.6

32.6

32.6

32.6


Decachlorobiphenyl


Decachlorobiphenyl

58

38

57

62

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/06/19



L1939567-02Lab ID:




1,8082A09/05/19 05:11HT

EPA 3546



96%Percent Solids:

MDL

2.89

3.26

6.90

4.39

4.88

3.56

6.02

4.14

3.37

2.89

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09061913:32

Page 82 of 152

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

38.2

38.2

38.2

38.2

38.2

38.2

38.2

38.2

38.2

38.2


Decachlorobiphenyl


Decachlorobiphenyl

70

39

68

63

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/06/19



L1939567-03Lab ID:




1,8082A09/05/19 05:23HT

EPA 3546



84%Percent Solids:

MDL

3.40

3.83

8.11

5.15

5.74

4.18

7.07

4.86

3.96

3.40

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09061913:32

Page 83 of 152

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

ND

9.40

ND

ND

ND

9.40

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

37.0

37.0

37.0

37.0

37.0

37.0

37.0

37.0

37.0

37.0


Decachlorobiphenyl


Decachlorobiphenyl

64

38

62

65

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/06/19



L1939567-04Lab ID:




1,8082A09/05/19 04:58HT

EPA 3546



85%Percent Solids:

MDL

3.29

3.71

7.85

4.99

5.56

4.05

6.84

4.70

3.84

3.29

A

A

A

A

A

A

B

A

B

B

Column

Sample Depth:

Serial_No:09061913:32

Page 84 of 152

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

36.2

36.2

36.2

36.2

36.2

36.2

36.2

36.2

36.2

36.2


Decachlorobiphenyl


Decachlorobiphenyl

66

40

64

65

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/06/19



L1939567-05Lab ID:




1,8082A09/05/19 05:36HT

EPA 3546



89%Percent Solids:

MDL

3.21

3.63

7.67

4.88

5.43

3.96

6.69

4.60

3.75

3.21

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09061913:32

Page 85 of 152

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

41.3

41.3

41.3

41.3

41.3

41.3

41.3

41.3

41.3

41.3


Decachlorobiphenyl


Decachlorobiphenyl

63

40

59

62

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/06/19



L1939567-06Lab ID:




1,8082A09/05/19 05:48HT

EPA 3546



79%Percent Solids:

MDL

3.67

4.14

8.76

5.57

6.20

4.52

7.64

5.25

4.28

3.67

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09061913:32

Page 86 of 152

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total

Parameter Result

J

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

28.4

ND

13.6

42.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

46.1

46.1

46.1

46.1

46.1

46.1

46.1

46.1

46.1

46.1


Decachlorobiphenyl


Decachlorobiphenyl

64

53

63

67

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


09/06/19



L1939567-07Lab ID:




1,8082A09/05/19 02:46HT

EPA 3546



69%Percent Solids:

MDL

4.09

4.62

9.77

6.21

6.91

5.04

8.51

5.85

4.77

4.09

A

A

A

A

A

A

B

A

B

B

Column

Sample Depth:

Serial_No:09061913:32

Page 87 of 152

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

38.8

38.8

38.8

38.8

38.8

38.8

38.8

38.8

38.8

38.8


Decachlorobiphenyl


Decachlorobiphenyl

60

27

53

45

30-150

30-150

30-150

30-150

Acceptance Criteria

Q

A

A

B

B


09/06/19



L1939567-08Lab ID:




1,8082A09/05/19 04:33HT

EPA 3546



81%Percent Solids:

MDL

3.44

3.88

8.22

5.23

5.82

4.24

7.16

4.92

4.02

3.44

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09061913:32

Page 88 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567



Cleanup Method:

EPA 3546


09/06/19


Analyst: HT

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

32.8

32.8

32.8

32.8

32.8

32.8

32.8

32.8

32.8

32.8

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier



Decachlorobiphenyl


Decachlorobiphenyl

75

47

73

73

30-150

30-150

30-150

30-150


Criteria



MDL

2.92

3.29

6.96

4.42

4.92

3.59

6.07

4.17

3.40

2.92

Column

A

A

A

A

A

A

A

A

A

A

A

A

B

B

Serial_No:09061913:32

Page 89 of 152

Aroclor 1016

Aroclor 1260

80

60

80

63

40-140

40-140

0

5

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


72477172

30-15030-15030-15030-150

AABB

63426165


09/06/19

AcceptanceCriteria


A

A

Serial_No:09061913:32

Page 90 of 152

PESTICIDES

Serial_No:09061913:32

Page 91 of 152

FF

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

J

JIP

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

1.69

1.34

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

1.62

0.676

0.676

1.62

0.812

1.62

3.04

0.676

2.03

1.62

1.01

1.62

1.62

3.04

1.62

1.62

0.676

3.04

30.4

2.03

2.03

13.2

09/06/19



L1939567-01Lab ID:




1,8081B09/04/19 17:54BM

EPA 3546



MDL

0.318

0.302

0.192

0.615

0.364

0.572

0.913

0.277

0.710

0.418

0.507

0.375

0.579

1.30

0.383

0.542

0.322

0.947

8.52

0.565

0.536

5.38

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

B

A

A

Column

Sample Depth:

Serial_No:09061913:32

Page 92 of 152



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Decachlorobiphenyl


Decachlorobiphenyl

70

58

93

97

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/06/19



L1939567-01Lab ID:


MDL Column

Sample Depth:

Serial_No:09061913:32

Page 93 of 152

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

1.61

0.670

0.670

1.61

0.804

1.61

3.01

0.670

2.01

1.61

1.00

1.61

1.61

3.01

1.61

1.61

0.670

3.01

30.1

2.01

2.01

13.0

09/06/19



L1939567-02Lab ID:




1,8081B09/04/19 17:11BM

EPA 3546



MDL

0.315

0.299

0.190

0.609

0.360

0.566

0.904

0.274

0.703

0.414

0.502

0.372

0.573

1.29

0.380

0.537

0.319

0.938

8.44

0.560

0.530

5.32

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09061913:32

Page 94 of 152



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Decachlorobiphenyl


Decachlorobiphenyl

93

91

92

96

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/06/19



L1939567-02Lab ID:


MDL Column

Sample Depth:

Serial_No:09061913:32

Page 95 of 152

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

1.89

0.787

0.787

1.89

0.945

1.89

3.54

0.787

2.36

1.89

1.18

1.89

1.89

3.54

1.89

1.89

0.787

3.54

35.4

2.36

2.36

15.4

09/06/19



L1939567-03Lab ID:




1,8081B09/04/19 17:22BM

EPA 3546



MDL

0.370

0.352

0.224

0.716

0.424

0.665

1.06

0.323

0.827

0.487

0.590

0.437

0.674

1.52

0.446

0.631

0.375

1.10

9.92

0.658

0.624

6.26

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09061913:32

Page 96 of 152



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Decachlorobiphenyl


Decachlorobiphenyl

101

104

103

93

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/06/19



L1939567-03Lab ID:


MDL Column

Sample Depth:

Serial_No:09061913:32

Page 97 of 152

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

1.80

0.752

0.752

1.80

0.903

1.80

3.38

0.752

2.26

1.80

1.13

1.80

1.80

3.38

1.80

1.80

0.752

3.38

33.8

2.26

2.26

14.7

09/06/19



L1939567-04Lab ID:




1,8081B09/04/19 17:34BM

EPA 3546



MDL

0.354

0.336

0.214

0.684

0.405

0.636

1.02

0.308

0.790

0.465

0.564

0.417

0.644

1.45

0.426

0.603

0.358

1.05

9.48

0.629

0.596

5.98

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09061913:32

Page 98 of 152



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Decachlorobiphenyl


Decachlorobiphenyl

89

73

87

85

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/06/19



L1939567-04Lab ID:


MDL Column

Sample Depth:

Serial_No:09061913:32

Page 99 of 152

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

1.74

0.726

0.726

1.74

0.872

1.74

3.27

0.726

2.18

1.74

1.09

1.74

1.74

3.27

1.74

1.74

0.726

3.27

32.7

2.18

2.18

14.2

09/06/19



L1939567-05Lab ID:




1,8081B09/04/19 17:46BM

EPA 3546



MDL

0.341

0.325

0.206

0.661

0.391

0.614

0.980

0.298

0.763

0.449

0.545

0.403

0.622

1.40

0.412

0.582

0.346

1.02

9.15

0.607

0.575

5.77

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09061913:32

Page 100 of 152



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Decachlorobiphenyl


Decachlorobiphenyl

102

81

100

85

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/06/19



L1939567-05Lab ID:


MDL Column

Sample Depth:

Serial_No:09061913:32

Page 101 of 152

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

IP

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

1.93

0.805

0.805

1.93

0.966

1.93

3.62

0.805

2.41

1.93

1.21

1.93

1.93

3.62

1.93

1.93

0.805

3.62

36.2

2.41

2.41

15.7

09/06/19



L1939567-06Lab ID:




1,8081B09/04/19 17:57BM

EPA 3546



MDL

0.378

0.360

0.228

0.732

0.433

0.680

1.09

0.330

0.845

0.497

0.604

0.447

0.689

1.55

0.456

0.645

0.383

1.13

10.1

0.673

0.637

6.40

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09061913:32

Page 102 of 152



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Decachlorobiphenyl


Decachlorobiphenyl

100

87

98

97

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/06/19



L1939567-06Lab ID:


MDL Column

Sample Depth:

Serial_No:09061913:32

Page 103 of 152

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

IP

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

2.71

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

2.26

0.942

0.942

2.26

1.13

2.26

4.24

0.942

2.82

2.26

1.41

2.26

2.26

4.24

2.26

2.26

0.942

4.24

42.4

2.82

2.82

18.4

09/06/19



L1939567-07Lab ID:




1,8081B09/05/19 15:27SL

EPA 3546



69%Percent Solids:

MDL

0.443

0.421

0.268

0.857

0.507

0.796

1.27

0.386

0.989

0.582

0.706

0.523

0.806

1.82

0.534

0.755

0.448

1.32

11.9

0.787

0.746

7.49

A

A

A

A

A

A

A

A

A

A

A

A

B

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09061913:32

Page 104 of 152



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Decachlorobiphenyl


Decachlorobiphenyl

70

57

88

123

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/06/19



L1939567-07Lab ID:


MDL Column

Sample Depth:

Serial_No:09061913:32

Page 105 of 152

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

IP

J

JIP

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

1.68

ND

ND

ND

ND

ND

ND

ND

0.796

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

1.95

0.811

0.811

1.95

0.973

1.95

3.65

0.811

2.43

1.95

1.22

1.95

1.95

3.65

1.95

1.95

0.811

3.65

36.5

2.43

2.43

15.8

09/06/19



L1939567-08Lab ID:




1,8081B09/04/19 18:21BM

EPA 3546



MDL

0.381

0.362

0.230

0.738

0.436

0.685

1.09

0.332

0.852

0.501

0.608

0.450

0.694

1.56

0.460

0.650

0.386

1.14

10.2

0.678

0.642

6.45

A

A

A

A

A

A

A

A

A

A

A

B

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:09061913:32

Page 106 of 152



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


Decachlorobiphenyl


Decachlorobiphenyl

98

90

98

94

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


09/06/19



L1939567-08Lab ID:


MDL Column

Sample Depth:

Serial_No:09061913:32

Page 107 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567



Cleanup Method:

EPA 3546


09/06/19

Analyst: BM

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.59

0.664

0.664

1.59

0.796

1.59

2.99

0.664

1.99

1.59

0.995

1.59

1.59

2.99

1.59

1.59

0.664

2.99

29.9

1.99

1.99

12.9

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Organochlorine Pesticides by GC - Westborough Lab for sample(s): 01-06,08 Batch: WG1279418-1


MDL

0.312

0.297

0.188

0.604

0.357

0.561

0.896

0.272

0.697

0.410

0.498

0.368

0.568

1.28

0.376

0.532

0.316

0.929

8.36

0.555

0.526

5.28

Column

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:09061913:32

Page 108 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567



Cleanup Method:

EPA 3546


09/06/19

Analyst: BM


Organochlorine Pesticides by GC - Westborough Lab for sample(s): 01-06,08 Batch: WG1279418-1


Decachlorobiphenyl


Decachlorobiphenyl

98

87

111

109

30-150

30-150

30-150

30-150


Criteria


MDL Column

B

B

A

A

Serial_No:09061913:32

Page 109 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567



Cleanup Method:

EPA 3546


09/06/19


Analyst: SL

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

Toxaphene

cis-Chlordane

trans-Chlordane

Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.59

0.664

0.664

1.59

0.796

1.59

2.99

0.664

1.99

1.59

0.995

1.59

1.59

2.99

1.59

1.59

0.664

2.99

29.9

1.99

1.99

12.9

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Organochlorine Pesticides by GC - Westborough Lab for sample(s): 07 Batch: WG1280616-1



MDL

0.312

0.297

0.188

0.604

0.357

0.561

0.896

0.272

0.697

0.410

0.498

0.368

0.568

1.28

0.376

0.532

0.316

0.929

8.36

0.555

0.526

5.28

Column

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:09061913:32

Page 110 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567



Cleanup Method:

EPA 3546


09/06/19


Analyst: SL


Organochlorine Pesticides by GC - Westborough Lab for sample(s): 07 Batch: WG1280616-1


Decachlorobiphenyl


Decachlorobiphenyl

96

73

106

86

30-150

30-150

30-150

30-150


Criteria



MDL Column

B

B

A

A

Serial_No:09061913:32

Page 111 of 152

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

cis-Chlordane

trans-Chlordane

136

124

140

134

129

123

126

138

88

140

139

134

145

143

117

132

133

125

107

116

138

125

138

132

129

123

129

142

64

143

143

135

150

147

120

137

131

127

111

119

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

1

1

1

2

0

0

2

3

32

2

3

1

3

3

3

4

2

2

4

3

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Organochlorine Pesticides by GC - Westborough Lab Associated sample(s): 01-06,08 Batch: WG1279418-2 WG1279418-3


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual Qual Qual

Q

Column

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:09061913:32

Page 112 of 152

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Organochlorine Pesticides by GC - Westborough Lab Associated sample(s): 01-06,08 Batch: WG1279418-2 WG1279418-3


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


9981111101

30-15030-15030-15030-150

BBAA

9686107107


09/06/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09061913:32

Page 113 of 152

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Heptachlor epoxide

Endrin

Endrin aldehyde

Endrin ketone

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

Methoxychlor

cis-Chlordane

trans-Chlordane

133

119

132

127

121

121

118

126

101

122

128

126

131

126

112

119

116

109

102

109

137

123

135

132

124

123

125

136

73

132

140

138

143

131

119

129

119

113

110

117

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

3

3

2

4

2

2

6

8

32

8

9

9

9

4

6

8

3

4

8

7

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Organochlorine Pesticides by GC - Westborough Lab Associated sample(s): 07 Batch: WG1280616-2 WG1280616-3


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual Qual Qual

Q

Column

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:09061913:32

Page 114 of 152

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Organochlorine Pesticides by GC - Westborough Lab Associated sample(s): 07 Batch: WG1280616-2 WG1280616-3


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567


967210793

30-15030-15030-15030-150

BBAA

9493105104


09/06/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:09061913:32

Page 115 of 152

METALS

Serial_No:09061913:32

Page 116 of 152

FF

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

SAMPLE RESULTS


Matrix: Soil


L1939567-01Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

J

3140

0.892

3.97

63.4

0.168

0.875

2180

8.44

3.84

20.9

8940

127

923

207

0.168

9.94

300

0.395

ND

134

ND

17.6

85.4

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

8.41

4.20

0.841

0.841

0.420

0.841

8.41

0.841

1.68

0.841

4.20

4.20

8.41

0.841

0.067

2.10

210

1.68

0.841

168

1.68

0.841

4.20

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 15:57

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

09/05/19 13:16

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

GD

LC

LC

LC

LC

LC

LC

LC

LC

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/05/19 04:20

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 93%

MDL

2.27

0.320

0.175

0.146

0.028

0.082

2.94

0.081

0.140

0.217

0.759

0.225

1.30

0.134

0.044

0.204

12.1

0.217

0.238

2.65

0.265

0.171

0.246

Sample Depth:

Serial_No:09061913:32

Page 117 of 152

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

SAMPLE RESULTS


Matrix: Soil


L1939567-02Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

J

2550

ND

2.49

22.4

0.193

0.379

106000

9.35

5.34

10.3

10900

17.3

46600

478

0.581

9.54

256

0.298

ND

131

ND

20.2

49.2

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

20

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

8.06

4.03

0.806

0.806

0.403

0.806

80.6

0.806

1.61

0.806

4.03

4.03

8.06

0.806

0.065

2.02

202

1.61

0.806

161

1.61

0.806

4.03

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

09/05/19 14:24

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

09/05/19 16:00

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

09/05/19 13:20

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

GD

LC

LC

LC

LC

LC

LC

LC

LC

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/05/19 04:20

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 96%

MDL

2.18

0.306

0.168

0.140

0.027

0.079

28.2

0.077

0.134

0.208

0.728

0.216

1.24

0.128

0.043

0.195

11.6

0.208

0.228

2.54

0.254

0.164

0.236

Sample Depth:

Serial_No:09061913:32

Page 118 of 152

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

SAMPLE RESULTS


Matrix: Soil


L1939567-03Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

8080

ND

3.44

93.0

0.466

0.181

1150

11.5

4.90

15.2

11900

248

999

396

0.116

6.44

258

0.762

ND

304

ND

18.4

61.5

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

9.52

4.76

0.952

0.952

0.476

0.952

9.52

0.952

1.90

0.952

4.76

4.76

9.52

0.952

0.075

2.38

238

1.90

0.952

190

1.90

0.952

4.76

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 16:04

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

09/05/19 13:25

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

GD

LC

LC

LC

LC

LC

LC

LC

LC

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/05/19 04:20

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 84%

MDL

2.57

0.362

0.198

0.166

0.031

0.093

3.33

0.091

0.158

0.246

0.860

0.255

1.47

0.151

0.049

0.230

13.7

0.246

0.269

3.00

0.300

0.193

0.279

Sample Depth:

Serial_No:09061913:32

Page 119 of 152

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

SAMPLE RESULTS


Matrix: Soil


L1939567-04Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

11600

ND

3.52

98.1

0.396

0.221

3350

19.0

6.71

13.9

15700

113

2500

443

0.263

9.93

465

0.405

ND

220

ND

31.5

60.6

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

9.20

4.60

0.920

0.920

0.460

0.920

9.20

0.920

1.84

0.920

4.60

4.60

9.20

0.920

0.074

2.30

230

1.84

0.920

184

1.84

0.920

4.60

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 16:07

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

09/05/19 13:43

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

GD

LC

LC

LC

LC

LC

LC

LC

LC

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/05/19 04:20

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 85%

MDL

2.48

0.350

0.191

0.160

0.030

0.090

3.22

0.088

0.153

0.238

0.831

0.247

1.42

0.146

0.048

0.223

13.2

0.238

0.260

2.90

0.290

0.187

0.270

Sample Depth:

Serial_No:09061913:32

Page 120 of 152

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

SAMPLE RESULTS


Matrix: Soil


L1939567-05Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

10100

ND

1.49

35.6

0.148

0.174

689

20.4

8.31

14.4

17900

5.15

2120

224

ND

15.6

908

ND

ND

232

ND

32.0

23.5

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

8.70

4.35

0.870

0.870

0.435

0.870

8.70

0.870

1.74

0.870

4.35

4.35

8.70

0.870

0.071

2.18

218

1.74

0.870

174

1.74

0.870

4.35

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 16:10

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

09/05/19 13:48

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

GD

LC

LC

LC

LC

LC

LC

LC

LC

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/05/19 04:20

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 89%

MDL

2.35

0.331

0.181

0.151

0.029

0.085

3.04

0.084

0.144

0.224

0.786

0.233

1.34

0.138

0.046

0.210

12.5

0.224

0.246

2.74

0.274

0.177

0.255

Sample Depth:

Serial_No:09061913:32

Page 121 of 152

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

SAMPLE RESULTS


Matrix: Soil


L1939567-06Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

9330

ND

3.86

132

0.518

0.469

2110

15.5

4.38

18.3

11500

231

1310

230

0.286

8.38

405

ND

ND

246

ND

21.0

114

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

9.97

4.98

0.997

0.997

0.498

0.997

9.97

0.997

1.99

0.997

4.98

4.98

9.97

0.997

0.079

2.49

249

1.99

0.997

199

1.99

0.997

4.98

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 16:14

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

09/05/19 13:52

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

GD

LC

LC

LC

LC

LC

LC

LC

LC

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/05/19 04:20

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 79%

MDL

2.69

0.379

0.207

0.174

0.033

0.098

3.49

0.096

0.166

0.257

0.900

0.267

1.54

0.158

0.052

0.241

14.4

0.257

0.282

3.14

0.314

0.202

0.292

Sample Depth:

Serial_No:09061913:32

Page 122 of 152

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

SAMPLE RESULTS


Matrix: Soil


L1939567-07Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

J

7310

0.761

8.32

238

0.318

1.04

4820

18.5

6.53

60.3

12700

717

1380

158

0.745

13.4

403

1.65

ND

372

ND

28.0

221

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

11.4

5.68

1.14

1.14

0.568

1.14

11.4

1.14

2.27

1.14

5.68

5.68

11.4

1.14

0.090

2.84

284

2.27

1.14

227

2.27

1.14

5.68

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 16:24

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

09/05/19 13:57

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

GD

LC

LC

LC

LC

LC

LC

LC

LC

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/05/19 04:20

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 69%

MDL

3.06

0.431

0.236

0.198

0.038

0.111

3.97

0.109

0.188

0.293

1.02

0.304

1.75

0.180

0.059

0.275

16.3

0.293

0.321

3.58

0.358

0.230

0.333

Sample Depth:

Serial_No:09061913:32

Page 123 of 152

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

SAMPLE RESULTS


Matrix: Soil


L1939567-08Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Mercury, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

J

J

J

8930

0.390

4.92

144

0.486

0.209

2060

16.4

5.31

19.8

13300

576

1230

416

0.712

9.12

376

0.504

ND

277

ND

24.7

91.5

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

1

2

2

2

2

2

2

2

2

9.52

4.76

0.952

0.952

0.476

0.952

9.52

0.952

1.90

0.952

4.76

4.76

9.52

0.952

0.078

2.38

238

1.90

0.952

190

1.90

0.952

4.76

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 16:27

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

09/05/19 14:01

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

GD

LC

LC

LC

LC

LC

LC

LC

LC

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/05/19 04:20

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 81%

MDL

2.57

0.362

0.198

0.166

0.031

0.093

3.33

0.091

0.158

0.246

0.860

0.255

1.47

0.151

0.051

0.230

13.7

0.246

0.269

3.00

0.300

0.193

0.279

Sample Depth:

Serial_No:09061913:32

Page 124 of 152

FF

Parameter

Parameter

Result

Result

Dilution Factor

Dilution Factor

Qualifier

Qualifier

Units

Units

RL

RL


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

DateAnalyzed

DateAnalyzed

AnalyticalMethod

AnalyticalMethod

Analyst

Analyst

Date Prepared

Date Prepared

09/06/19

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

Mercury, Total

J

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

4.54

ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

4.00

2.00

0.400

0.400

0.200

0.400

4.00

0.400

0.800

0.400

2.00

2.00

4.00

0.400

1.00

100

0.800

0.400

80.0

0.800

0.400

2.00

0.083

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 12:48

09/05/19 15:04

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,6010D

1,7471B

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

LC

GD

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/04/19 00:25

09/05/19 04:20




Prep Information

MDL

MDL

1.08

0.152

0.083

0.070

0.013

0.039

1.40

0.038

0.066

0.103

0.361

0.107

0.616

0.064

0.097

5.76

0.103

0.113

1.26

0.126

0.081

0.117

0.054

Serial_No:09061913:32

Page 125 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19


Prep Information

Serial_No:09061913:32

Page 126 of 152

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

66

156

105

90

96

102

84

94

97

97

90

97

78

89

100

78

102

93

95

99

96

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

51-149

19-249

70-130

75-125

75-125

75-125

73-127

70-130

75-125

75-125

38-162

71-128

63-137

76-124

70-131

60-140

63-137

69-131

37-162

68-132

65-135

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual Qual Qual

Serial_No:09061913:32

Page 127 of 152

Zinc, Total

Mercury, Total

97

99

-

-

70-130

60-141

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery





Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Serial_No:09061913:32

Page 128 of 152

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Vanadium, Total

8010

ND

3.24

112

0.117J

2.60

43500

19.4

6.62

30.5

12600

137

11800

207

13.0

2220

0.425J

ND

427

ND

25.2

11000

49.0

17.1

330

5.60

5.60

52200

43.8

55.8

91.7

21000

184

10400

316

65.6

3680

13.4

32.9

1620

9.81

84.0

1410

92

109

103

106

55

820

115

93

231

7920

87

0

206

99

138

105

103

112

77

111

10000

43.6

16.6

323

5.31

5.40

39000

42.3

53.6

55.7

14700

185

10400

291

61.4

3680

12.6

31.7

1480

9.31

81.1

989

87

111

105

106

54

0

114

93

100

2090

94

0

167

96

145

104

105

105

77

111

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

10

12

3

2

5

4

29

3

4

49

35

1

0

8

7

0

6

4

9

5

4

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 01-08 QC Batch ID: WG1279778-3 WG1279778-4 QC Sample: L1939834-01 Client ID: MS Sample

212

53

12.7

212

5.3

5.41

1060

21.2

53

26.5

106

54.1

1060

53

53

1060

12.7

31.8

1060

12.7

53

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual

Q

Q

Q

Q

Q

Q

Q

Q

Qual

Q

Q

Q

Q

Q

Q

Q

Qual

Q

Q

Q

Serial_No:09061913:32

Page 129 of 152

Zinc, Total

Mercury, Total

143

0.183

161

0.191

34

6

170

0.190

54

6

75-125

80-120

5

1

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits



53

0.126

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Q

Q

Q

Q

Serial_No:09061913:32

Page 130 of 152

INORGANICS&

MISCELLANEOUS

Serial_No:09061913:32

Page 131 of 152

FF



Matrix: Soil


L1939567-01Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

93.4

ND

%

mg/kg

1

1

0.100

1.0

08/30/19 13:09

09/03/19 12:46

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 22:55

09/06/19

MDL

NA

0.22

Sample Depth:

Serial_No:09061913:32

Page 132 of 152

FF



Matrix: Soil


L1939567-02Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

96.4

ND

%

mg/kg

1

1

0.100

0.96

08/30/19 13:09

09/03/19 12:47

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 22:55

09/06/19

MDL

NA

0.20

Sample Depth:

Serial_No:09061913:32

Page 133 of 152

FF



Matrix: Soil


L1939567-03Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

83.5

ND

%

mg/kg

1

1

0.100

1.2

08/30/19 13:09

09/03/19 12:48

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 22:55

09/06/19

MDL

NA

0.25

Sample Depth:

Serial_No:09061913:32

Page 134 of 152

FF



Matrix: Soil


L1939567-04Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

85.0

ND

%

mg/kg

1

1

0.100

1.2

08/30/19 13:09

09/03/19 12:49

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 22:55

09/06/19

MDL

NA

0.25

Sample Depth:

Serial_No:09061913:32

Page 135 of 152

FF



Matrix: Soil


L1939567-05Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

88.6

ND

%

mg/kg

1

1

0.100

1.0

08/30/19 13:09

09/03/19 12:52

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 22:55

09/06/19

MDL

NA

0.22

Sample Depth:

Serial_No:09061913:32

Page 136 of 152

FF



Matrix: Soil


L1939567-06Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

78.9

ND

%

mg/kg

1

1

0.100

1.2

08/30/19 13:09

09/03/19 12:53

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 22:55

09/06/19

MDL

NA

0.26

Sample Depth:

Serial_No:09061913:32

Page 137 of 152

FF



Matrix: Soil


L1939567-07Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

69.3

ND

%

mg/kg

1

1

0.100

1.4

08/30/19 13:09

09/03/19 12:54

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 22:55

09/06/19

MDL

NA

0.29

Sample Depth:

Serial_No:09061913:32

Page 138 of 152

FF



Matrix: Soil


L1939567-08Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

80.8

ND

%

mg/kg

1

1

0.100

1.2

08/30/19 13:09

09/03/19 12:55

121,2540G

1,9010C/9012B

RI

ML

Date Prepared

-

09/02/19 22:55

09/06/19

MDL

NA

0.26

Sample Depth:

Serial_No:09061913:32

Page 139 of 152

FF



Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

DateAnalyzed


Date Prepared

09/06/19

Cyanide, Total ND mg/kg 10.84 09/03/19 12:20 1,9010C/9012B ML09/02/19 22:55


MDL

0.18

Serial_No:09061913:32

Page 140 of 152

Cyanide, Total 64 70 80-120 35 35

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual Qual

Q Q

Qual

Serial_No:09061913:32

Page 141 of 152

Cyanide, Total ND 9.6 93 9.0 90 75-125 6 35


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits


10

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:


10831

L1939567

09/06/19

Qual Qual Qual

Serial_No:09061913:32

Page 142 of 152

Solids, Total 93.4 92.5 % 1 20


General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG1278788-1 QC Sample: L1939567-01 Client ID: SESI-SB-1 (2-3)


10831

Project Name:

Project Number:

L1939567Lab Number:

Report Date:


09/06/19

Qual

Serial_No:09061913:32

Page 143 of 152


L1939567-01A

L1939567-01B

L1939567-01C

L1939567-01D

L1939567-01E

L1939567-01F

L1939567-01X

L1939567-01Y

L1939567-01Z

L1939567-02A

L1939567-02B

L1939567-02C

L1939567-02D

L1939567-02E

L1939567-02F

L1939567-02X

L1939567-02Y


















A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent



10831

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)



NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)



NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

Project Name:

Project Number:

L1939567Lab Number:

Report Date:




Analysis(*)

09/06/19


30-AUG-19 14:55

30-AUG-19 14:55

30-AUG-19 14:55

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09061913:32

Page 144 of 152


L1939567-02Z

L1939567-03A

L1939567-03B

L1939567-03C

L1939567-03D

L1939567-03E

L1939567-03F

L1939567-03X

L1939567-03Y

L1939567-03Z

L1939567-04A

L1939567-04B

L1939567-04C

L1939567-04D

L1939567-04E

L1939567-04F

L1939567-04X

L1939567-04Y

L1939567-04Z

L1939567-05A

L1939567-05B

L1939567-05C

L1939567-05D
























A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent


10831

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)



NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)



NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

Project Name:

Project Number:

L1939567Lab Number:

Report Date:



Analysis(*)

09/06/19

30-AUG-19 14:55

30-AUG-19 14:55

30-AUG-19 14:55

30-AUG-19 14:55

30-AUG-19 14:55

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09061913:32

Page 145 of 152


L1939567-05E

L1939567-05F

L1939567-05X

L1939567-05Y

L1939567-05Z

L1939567-06A

L1939567-06B

L1939567-06C

L1939567-06D

L1939567-06E

L1939567-06F

L1939567-06X

L1939567-06Y

L1939567-06Z

L1939567-07A

L1939567-07B

L1939567-07C

L1939567-07D

L1939567-07E

L1939567-07F





















A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent


10831



NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)



NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)



Project Name:

Project Number:

L1939567Lab Number:

Report Date:



Analysis(*)

09/06/19

30-AUG-19 14:55

30-AUG-19 14:55

30-AUG-19 14:55

30-AUG-19 14:55

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09061913:32

Page 146 of 152


L1939567-07X

L1939567-07Y

L1939567-07Z

L1939567-08A

L1939567-08B

L1939567-08C

L1939567-08D

L1939567-08E

L1939567-08F

L1939567-08X

L1939567-08Y

L1939567-08Z













A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent


10831

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)



NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

Project Name:

Project Number:

L1939567Lab Number:

Report Date:



Analysis(*)

09/06/19

30-AUG-19 14:55

30-AUG-19 14:55

30-AUG-19 14:55

30-AUG-19 14:55

FrozenDate/Time

FinalpH

Initial pH

Serial_No:09061913:32

Page 147 of 152


GLOSSARY

Project Name:

Project Number:

Lab Number:

Report Date:

L193956790-02 168TH ST, JAMAICA, QUEEN

10831 09/06/19

Acronyms

DL

EDL

EMPC

EPA

LCS

LCSD

LFB

LOD

LOQ

MDL

MS

MSD

NA

NC

NDPA/DPA

NI

NP

RL

RPD

SRM

STLP

TEF

TEQ

TIC






Not Applicable.


Not Ignitable.





-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

Footnotes

Serial_No:09061913:32

Page 148 of 152


Project Name:

Project Number:

Lab Number:

Report Date:


10831 09/06/19

Terms


Data Qualifiers

A

B

C

D

E

G

H

I

J

M

ND

NJ

P

Q

R

RE

S

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-











-

Serial_No:09061913:32

Page 149 of 152




1

121



Project Name:

Project Number:

Lab Number:

Report Date:


10831

REFERENCES

09/06/19

Serial_No:09061913:32

Page 150 of 152











Mansfield Facility:




Serial_No:09061913:32

Page 151 of 152

Serial_No:09061913:32

Page 152 of 152

Date post:	07-Mar-2021
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