r TBPB NMR Analysis, solvent: DMSO-d6Method File Name : TBPB.lcm Batch File Name : 20170731.lcb Data...

ppm (t1)0.05.010.0

0

10000

20000

30000

40000

50000

6000010.8

34

7.21

97.

207

7.20

27.

141

7.12

67.

113

6.97

06.

961

4.12

13.

387

3.00

52.

857

2.83

02.

508

2.31

11.

984

1.95

61.

928

1.73

91.

711

1.64

91.

483

1.45

51.

431

0.96

4.933.00

1.02

1.992.03

7.72

2.104.002.00

6.18

TBPB, d6-DMSO

MedKoo Biosciences www.medkoo.com [email protected]

MedKoo Biosciences Product Quality Control Data www.medkoo.com [email protected] MedKoo Biosciences Product Quality Control Data www.medkoo.com [email protected] MedKoo Biosciences Product Quality Control Data www.medkoo.com [email protected]

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MedKoo Cat#: 522531 Name: TBPB CAS#: 634616-95-8 Lot#: X7P07R31 Chemical Formula: C25H32N4O Exact Mass: 404.2576 Molecular Weight: 404.558

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TBPB NMR Analysis, solvent: DMSO-d6

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2017-7-31 15:36:51 1 / 2

D:\Reverse HPLC\Date of 201707\TBPB.lcd


min

mV

0 5 10 15 20 25 300

1000

Det.A Ch1

min

mV

0 5 10 15 20 25 300

1000

2000 Det.A Ch2

Det.A Ch1/220nm1Det.A Ch2/254nm2

Column : Inertil ODS-3，5um 4.6*150mm Mobile phase : Solvent A: H2O(0.05%H3PO4) Solvent B:ACN(0.05%H3PO4) Temperature : 40 ℃

Flow rate : 1mL/min Run time : 3min gradient(50%B), 15min gradient (50%-95%B),5 min(95%B),then 7min @(50%B) Detector : UV

Wavelenth : 220/254 nm User name : TBPB E-005

Notebook page : Sample description : in ACN

Injection Volume : 2 uL

HPLC Report

PeakTableDetector A Ch1 220nmPeak#

1 2 3

Total

Ret. Time 7.306 9.612 16.244

Area 33998 5087

14343838 14382923

Area % 0.236 0.035 99.728

100.000

Theoretical Plate# 14662.783 14814.947 68515.013

Data File Name :TBPB.lcdMethod File Name : TBPB.lcmBatch File Name : 20170731.lcbData Acquired : 2017-7-31 15:01:12Data Processed : 2017-7-31 15:36:40

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TBPB HPLC Analysis

2017-7-31 15:36:51 2 / 2


PeakTableDetector A Ch2 254nmPeak#

1 2 3

Total

Ret. Time 7.306 16.245 17.832

Area 10834

19379315 5117

19395266

Area % 0.056

99.918 0.026

100.000

Theoretical Plate# 14533.178 66286.849 71213.400

*** End Of Report ***

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TBPB HPLC Analysis

2017-7-31 14:20:17 Page 1 / 2

D:\Data\TBPB.lcd

LC-MS Condition Column :YMC-Pack Pro C18,150*4.6mm,3um,JH-008Mobile Phase :Solvent A:H2O:FA=99.95:0.05 Solvent B: MeCNTemperature :30℃.Flow rate :0.8 mL/min.Run time :3min@40%B, and then 15min (40-80%B),then 5 min 80%BDetector :UVWavelength :254/263nmMass range :50-1000Scan :Postive/NegativeUser name :SZJNotebook page :---Sample description :1 mg/ml in MeCNData Filename : TBPB.lcdBatch Filename : 20170716.lcbMethod Filename : positive-negative 3min-1.lcmVial # : 1-99Injection Volume : 5 uLDate Acquired : 2017-7-31 14:01:36Date Processed : 2017-7-31 14:20:00

<Sample Information>

LC-MS Report

MS Chromatogram

min

55,503,551 (-0.133min Delay)

(x10,000,000)

0.00

2.00

4.00

0.00 0.25 0.50 0.75 1.00 1.25 1.50 1.75 2.00 2.25 2.50

TIC(+)@1TIC(-)@2

1 /

0.21

2 1

/ 0.

211

MS Spectrum

ChromatogramD:\Data\TBPB.lcd

min

uAU

0.00 0.25 0.50 0.75 1.00 1.25 1.50 1.75 2.00 2.25 2.50 2.75

0

100000

PDA Multi 1 254nm,4nm

0.2

66

Peak TablePDA Ch1 254nm

Peak# 1

Total

Ret. Time 0.266

Area423457 423457

Area%100.000 100.000

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TBPB LC/MS Analysis

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D:\Data\TBPB.lcd

Peak#:1 R.Time:0.211(Scan#:20)MassPeaks:534Spectrum Mode:Averaged 0.175-0.225(18-22)BG Mode:Calc Segment 1 - Event 2

m/z

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100 200 300 400 500 600 700 800 900

111

179

207

249

291

334

403

449

471

529

589

609

657

711

768

808

829

897

950

Peak#:1 R.Time:0.212(Scan#:19)MassPeaks:522Spectrum Mode:Averaged 0.167-0.217(17-21)BG Mode:Calc Segment 1 - Event 1

m/z

5000000

100 200 300 400 500 600 700 800 900

105

188

203

242

301

342

405

427

505

539

596

627

663

695

752

809

831

869

927

978

***** End Of Report *****

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TBPB LC/MS Analysis

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r TBPB NMR Analysis, solvent: DMSO-d6Method File Name : TBPB.lcm Batch File Name : 20170731.lcb Data...

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