ANALYSIS OF WATER SAMPLES FROM SHPACK LANDFILL
ATTLEBORO MA
(Site No 5004620)
ERT PROJECT NO D931-137 April SB 1987
PREPARED FOR
Mr Peter Croteau WEHRAN ENGINEERING
Prepared by Analytical Chemistry Laboratory
ERT Resource Engineering Company 33 Industrial Way Wilmington Massachusetts 01887
ANALYSIS OF WATER-SAMPLES FROM SHPACK LANDFILL
ATTLEBORO MA
INTRODUCTION
This report represents the results of analysis conducted on various water samples received by the ERT Analytical Chemistry Laboratory on March 31 1987 The samples were to be selectively analyzed for volatile organic compounds priority pollutant metals and organiochlorine pesticides
SAMPLE RECEIPT AND CHAIN OF CUSTODY
Routine inspection of the samples revealed them to be packaged properly and received in good condition
Upon receipt information from the submitted samples was recorded in the Master Log Book ltand the LIMS computer system) and assigned ERT Control Numbers These unique sample labels were affixed to respective sample containers and subsequently utilized throughout the laboratory analysis procedures for positive traceab i 1 i ty
ANALYTICAL PROCEDURES
The water samples were analyzed according to procedures as out 1 ined in
a Guidelines Establishing Test Procedures for the Analysis of Pollutants Under the Clean Water Act 4-0 CFR Part 36 Federal Register Vol lt+9 No pound09 October 26 198^
b Methods for Chemical Analysis of Water and Wastes EPA-6004-79-020 revised March 1983
c Standard Methods for the Examination of Water- and Wastewater 16th Edition APHA 1985
QUALITY CONTROL PROCEDURES
Standard quality control procedures were implemented for all analyses Laboratory reagent (method) blanks laboratory duplicated samples and laboratory fortified control samples were analyzed concurrently with each case of submitted samples The laboratory normally prepares and analyzes one (1) blank one (1) fortified sample and one (1) duplicate sample for each case of samples received or for each twenty (EO) samples whichever is more frequent A case consists of a finite usually predetermined number of samples collected over a given time period from one particular site Duplicate sample analyses are performed only when sufficient sample volume is received The results of the analyses are reviewed by the laboratory quality control coordinator to insure compliance with established analytical contro1 limits
Laboratory prepared method b1ank samples and fortified samples are identified in the analytical result tables under the Field Identification number using a unique numbering system and also assigning one ERT sample number to each sample The Prefix MB refers to Method Blank and LF refers to Laboratory Fortification (ie a quality control recovery sample)
In most cases the analytical results willhave been corrected using mean method blank results
RESULTS OF ANALYSIS
Analytical results for the submitted samples are presented in the appended tables Summary tables for the results of duplicate blank and fortified control samples have also been provided in the Append i x
DISCUSSION
Review of the results of the quality contro1quality assurance samples analyzed concurrently with the submitted samples indicated that the analyses were within the acceptance criteria as established by the US EPA
VOLATILE ORGANIC ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Result3
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42145 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-Ol-101 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT ag1
PARAMETER RESULT ugi
CHLOROMETHANEVINYL CHLORIJEMETHYLENE CHLORIDECARBON DISULFIDE1 1-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-l3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
BROMOMETHANECHLOROETHANEACETONE 11-DICHLOROETHENETRANS-l2-DICHLOROETHENE12-DICHLOROETHANE111-TRICHLOROETHANEVINYL ACETATE12-DICHLOROPROPANETRICHLOROETHENE112-TRICHLOROETHANECIS-1 3-DICHLOROPROPENEBROMOFORM4-METHYL-Z-PENTANONE1122-TETRACHLOROETHANECHLOROBENZENESTYRENE
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED4 TOLUENEDB BROMOFLUOROBENZENE
11 108 98 108
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hezanone and 4-methyl-2-Pentanone is SO ug1
BDLMINASD
= BELOW DETECTION LIMIT 10 = MATRIX INTERFERENCE
= NOT ANALYZED = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42146 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RV-02-102 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ag1 ug1
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 1l-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENpound BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY S
1 2-DICHLOROETHANED4 122 BENZENE06 112 TOLUENED8 101 BROMOFLUOROBENZENE 108
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42147 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-03-I03 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugt ugS
CHLOROMETHANE BDL BROMOMETHANE VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 1 1-DICHLOHOETHENE BDL 11-DICHLOROETHANE BDL TRANS-1 2-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 1 11 -TH I CHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 1 2-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1 12-TRICHLOROETHANE BDL BENZENE BDL CIS-1 3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1 122-TETRACHLOROETHANE BDL TOLUENE -BDL CHLOHOBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 104 BENZENED6 104 TOLUENED8 101 BROMOFLUOROBENZENE 105
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42148 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RV-04-104 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI tig
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIliE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE bull BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 120 BENZENED6 117 TOLUENED8 106 BROMOFLUOROBENZENE 118
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42149 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-Q5-105 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI ugi
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORI3E BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL I1-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE bull BDL DI8ROMOCHLOROMETHANE BDL I12-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 115 TOLUENED8 108 BROMOFLUOROBENZENE 112
NOTE The detection l i m i t foi the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42150 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-06-106 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040687 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ug1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPHOPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE bull BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
l2-DICHLOROETHANED4 99
BENZENE06 90 TOLUENED8 8
BROMOFLUOROBENZENE 91
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42151 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-07-107 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
040387 DATE SAMPLED 033087
RESULT PARAMETER RESULT ugI n g I
BDL BROMOMETHANE 1JDL BDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-OICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
128
97
93
94
NOTE The detection l i m i t for the compounds Acetone 2-Hexanone and 4-methy 1-2-Pentanone is SO ugI
BDL s BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42132 CLIENT MSFATTLEBOROSHPACK LF FLO ID SHP-RW-08-108 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-1 3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
RESULT a g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BOL BDL BDL
137
99
95 93
PARAMETER RESULT ugI
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 112Z-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methyl-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 u g 1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42153 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RW-09-109 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ng1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIEE BDL CHLOROETHANE BDL METHYLENE CHLORIDE 90 ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMQDICHLOROMETHANE BDL 12-DICHLOROPROFANE BDL TRAMS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-l3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 129 BENZENED4 97 TOLUENED8 97 BHOMOFLUOROBENZENE 94
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42134 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
P A R A M E T E R R E S U L T PARAMETER RESULT T i g 1 agI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLbROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE bull BDL 12-DICHLOROPROPANE BDL TRANS--1 3-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1I2-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 126 BENZENEDltS 117 TOLUENED3 107 BROMOFLUOROBENZENE 119
NOTE The det e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug I MI = MATRIX INTERFERENCE NA = NOT ANALYZED -SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ANALYSIS OF WATER-SAMPLES FROM SHPACK LANDFILL
ATTLEBORO MA
INTRODUCTION
This report represents the results of analysis conducted on various water samples received by the ERT Analytical Chemistry Laboratory on March 31 1987 The samples were to be selectively analyzed for volatile organic compounds priority pollutant metals and organiochlorine pesticides
SAMPLE RECEIPT AND CHAIN OF CUSTODY
Routine inspection of the samples revealed them to be packaged properly and received in good condition
Upon receipt information from the submitted samples was recorded in the Master Log Book ltand the LIMS computer system) and assigned ERT Control Numbers These unique sample labels were affixed to respective sample containers and subsequently utilized throughout the laboratory analysis procedures for positive traceab i 1 i ty
ANALYTICAL PROCEDURES
The water samples were analyzed according to procedures as out 1 ined in
a Guidelines Establishing Test Procedures for the Analysis of Pollutants Under the Clean Water Act 4-0 CFR Part 36 Federal Register Vol lt+9 No pound09 October 26 198^
b Methods for Chemical Analysis of Water and Wastes EPA-6004-79-020 revised March 1983
c Standard Methods for the Examination of Water- and Wastewater 16th Edition APHA 1985
QUALITY CONTROL PROCEDURES
Standard quality control procedures were implemented for all analyses Laboratory reagent (method) blanks laboratory duplicated samples and laboratory fortified control samples were analyzed concurrently with each case of submitted samples The laboratory normally prepares and analyzes one (1) blank one (1) fortified sample and one (1) duplicate sample for each case of samples received or for each twenty (EO) samples whichever is more frequent A case consists of a finite usually predetermined number of samples collected over a given time period from one particular site Duplicate sample analyses are performed only when sufficient sample volume is received The results of the analyses are reviewed by the laboratory quality control coordinator to insure compliance with established analytical contro1 limits
Laboratory prepared method b1ank samples and fortified samples are identified in the analytical result tables under the Field Identification number using a unique numbering system and also assigning one ERT sample number to each sample The Prefix MB refers to Method Blank and LF refers to Laboratory Fortification (ie a quality control recovery sample)
In most cases the analytical results willhave been corrected using mean method blank results
RESULTS OF ANALYSIS
Analytical results for the submitted samples are presented in the appended tables Summary tables for the results of duplicate blank and fortified control samples have also been provided in the Append i x
DISCUSSION
Review of the results of the quality contro1quality assurance samples analyzed concurrently with the submitted samples indicated that the analyses were within the acceptance criteria as established by the US EPA
VOLATILE ORGANIC ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Result3
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42145 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-Ol-101 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT ag1
PARAMETER RESULT ugi
CHLOROMETHANEVINYL CHLORIJEMETHYLENE CHLORIDECARBON DISULFIDE1 1-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-l3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
BROMOMETHANECHLOROETHANEACETONE 11-DICHLOROETHENETRANS-l2-DICHLOROETHENE12-DICHLOROETHANE111-TRICHLOROETHANEVINYL ACETATE12-DICHLOROPROPANETRICHLOROETHENE112-TRICHLOROETHANECIS-1 3-DICHLOROPROPENEBROMOFORM4-METHYL-Z-PENTANONE1122-TETRACHLOROETHANECHLOROBENZENESTYRENE
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED4 TOLUENEDB BROMOFLUOROBENZENE
11 108 98 108
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hezanone and 4-methyl-2-Pentanone is SO ug1
BDLMINASD
= BELOW DETECTION LIMIT 10 = MATRIX INTERFERENCE
= NOT ANALYZED = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42146 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RV-02-102 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ag1 ug1
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 1l-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENpound BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY S
1 2-DICHLOROETHANED4 122 BENZENE06 112 TOLUENED8 101 BROMOFLUOROBENZENE 108
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42147 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-03-I03 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugt ugS
CHLOROMETHANE BDL BROMOMETHANE VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 1 1-DICHLOHOETHENE BDL 11-DICHLOROETHANE BDL TRANS-1 2-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 1 11 -TH I CHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 1 2-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1 12-TRICHLOROETHANE BDL BENZENE BDL CIS-1 3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1 122-TETRACHLOROETHANE BDL TOLUENE -BDL CHLOHOBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 104 BENZENED6 104 TOLUENED8 101 BROMOFLUOROBENZENE 105
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42148 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RV-04-104 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI tig
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIliE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE bull BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 120 BENZENED6 117 TOLUENED8 106 BROMOFLUOROBENZENE 118
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42149 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-Q5-105 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI ugi
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORI3E BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL I1-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE bull BDL DI8ROMOCHLOROMETHANE BDL I12-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 115 TOLUENED8 108 BROMOFLUOROBENZENE 112
NOTE The detection l i m i t foi the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42150 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-06-106 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040687 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ug1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPHOPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE bull BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
l2-DICHLOROETHANED4 99
BENZENE06 90 TOLUENED8 8
BROMOFLUOROBENZENE 91
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42151 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-07-107 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
040387 DATE SAMPLED 033087
RESULT PARAMETER RESULT ugI n g I
BDL BROMOMETHANE 1JDL BDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-OICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
128
97
93
94
NOTE The detection l i m i t for the compounds Acetone 2-Hexanone and 4-methy 1-2-Pentanone is SO ugI
BDL s BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42132 CLIENT MSFATTLEBOROSHPACK LF FLO ID SHP-RW-08-108 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-1 3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
RESULT a g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BOL BDL BDL
137
99
95 93
PARAMETER RESULT ugI
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 112Z-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methyl-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 u g 1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42153 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RW-09-109 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ng1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIEE BDL CHLOROETHANE BDL METHYLENE CHLORIDE 90 ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMQDICHLOROMETHANE BDL 12-DICHLOROPROFANE BDL TRAMS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-l3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 129 BENZENED4 97 TOLUENED8 97 BHOMOFLUOROBENZENE 94
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42134 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
P A R A M E T E R R E S U L T PARAMETER RESULT T i g 1 agI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLbROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE bull BDL 12-DICHLOROPROPANE BDL TRANS--1 3-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1I2-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 126 BENZENEDltS 117 TOLUENED3 107 BROMOFLUOROBENZENE 119
NOTE The det e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug I MI = MATRIX INTERFERENCE NA = NOT ANALYZED -SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
Laboratory prepared method b1ank samples and fortified samples are identified in the analytical result tables under the Field Identification number using a unique numbering system and also assigning one ERT sample number to each sample The Prefix MB refers to Method Blank and LF refers to Laboratory Fortification (ie a quality control recovery sample)
In most cases the analytical results willhave been corrected using mean method blank results
RESULTS OF ANALYSIS
Analytical results for the submitted samples are presented in the appended tables Summary tables for the results of duplicate blank and fortified control samples have also been provided in the Append i x
DISCUSSION
Review of the results of the quality contro1quality assurance samples analyzed concurrently with the submitted samples indicated that the analyses were within the acceptance criteria as established by the US EPA
VOLATILE ORGANIC ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Result3
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42145 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-Ol-101 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT ag1
PARAMETER RESULT ugi
CHLOROMETHANEVINYL CHLORIJEMETHYLENE CHLORIDECARBON DISULFIDE1 1-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-l3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
BROMOMETHANECHLOROETHANEACETONE 11-DICHLOROETHENETRANS-l2-DICHLOROETHENE12-DICHLOROETHANE111-TRICHLOROETHANEVINYL ACETATE12-DICHLOROPROPANETRICHLOROETHENE112-TRICHLOROETHANECIS-1 3-DICHLOROPROPENEBROMOFORM4-METHYL-Z-PENTANONE1122-TETRACHLOROETHANECHLOROBENZENESTYRENE
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED4 TOLUENEDB BROMOFLUOROBENZENE
11 108 98 108
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hezanone and 4-methyl-2-Pentanone is SO ug1
BDLMINASD
= BELOW DETECTION LIMIT 10 = MATRIX INTERFERENCE
= NOT ANALYZED = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42146 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RV-02-102 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ag1 ug1
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 1l-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENpound BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY S
1 2-DICHLOROETHANED4 122 BENZENE06 112 TOLUENED8 101 BROMOFLUOROBENZENE 108
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42147 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-03-I03 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugt ugS
CHLOROMETHANE BDL BROMOMETHANE VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 1 1-DICHLOHOETHENE BDL 11-DICHLOROETHANE BDL TRANS-1 2-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 1 11 -TH I CHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 1 2-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1 12-TRICHLOROETHANE BDL BENZENE BDL CIS-1 3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1 122-TETRACHLOROETHANE BDL TOLUENE -BDL CHLOHOBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 104 BENZENED6 104 TOLUENED8 101 BROMOFLUOROBENZENE 105
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42148 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RV-04-104 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI tig
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIliE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE bull BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 120 BENZENED6 117 TOLUENED8 106 BROMOFLUOROBENZENE 118
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42149 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-Q5-105 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI ugi
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORI3E BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL I1-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE bull BDL DI8ROMOCHLOROMETHANE BDL I12-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 115 TOLUENED8 108 BROMOFLUOROBENZENE 112
NOTE The detection l i m i t foi the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42150 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-06-106 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040687 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ug1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPHOPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE bull BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
l2-DICHLOROETHANED4 99
BENZENE06 90 TOLUENED8 8
BROMOFLUOROBENZENE 91
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42151 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-07-107 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
040387 DATE SAMPLED 033087
RESULT PARAMETER RESULT ugI n g I
BDL BROMOMETHANE 1JDL BDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-OICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
128
97
93
94
NOTE The detection l i m i t for the compounds Acetone 2-Hexanone and 4-methy 1-2-Pentanone is SO ugI
BDL s BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42132 CLIENT MSFATTLEBOROSHPACK LF FLO ID SHP-RW-08-108 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-1 3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
RESULT a g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BOL BDL BDL
137
99
95 93
PARAMETER RESULT ugI
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 112Z-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methyl-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 u g 1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42153 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RW-09-109 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ng1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIEE BDL CHLOROETHANE BDL METHYLENE CHLORIDE 90 ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMQDICHLOROMETHANE BDL 12-DICHLOROPROFANE BDL TRAMS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-l3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 129 BENZENED4 97 TOLUENED8 97 BHOMOFLUOROBENZENE 94
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42134 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
P A R A M E T E R R E S U L T PARAMETER RESULT T i g 1 agI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLbROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE bull BDL 12-DICHLOROPROPANE BDL TRANS--1 3-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1I2-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 126 BENZENEDltS 117 TOLUENED3 107 BROMOFLUOROBENZENE 119
NOTE The det e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug I MI = MATRIX INTERFERENCE NA = NOT ANALYZED -SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
VOLATILE ORGANIC ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Result3
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42145 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-Ol-101 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT ag1
PARAMETER RESULT ugi
CHLOROMETHANEVINYL CHLORIJEMETHYLENE CHLORIDECARBON DISULFIDE1 1-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-l3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
BROMOMETHANECHLOROETHANEACETONE 11-DICHLOROETHENETRANS-l2-DICHLOROETHENE12-DICHLOROETHANE111-TRICHLOROETHANEVINYL ACETATE12-DICHLOROPROPANETRICHLOROETHENE112-TRICHLOROETHANECIS-1 3-DICHLOROPROPENEBROMOFORM4-METHYL-Z-PENTANONE1122-TETRACHLOROETHANECHLOROBENZENESTYRENE
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED4 TOLUENEDB BROMOFLUOROBENZENE
11 108 98 108
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hezanone and 4-methyl-2-Pentanone is SO ug1
BDLMINASD
= BELOW DETECTION LIMIT 10 = MATRIX INTERFERENCE
= NOT ANALYZED = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42146 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RV-02-102 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ag1 ug1
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 1l-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENpound BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY S
1 2-DICHLOROETHANED4 122 BENZENE06 112 TOLUENED8 101 BROMOFLUOROBENZENE 108
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42147 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-03-I03 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugt ugS
CHLOROMETHANE BDL BROMOMETHANE VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 1 1-DICHLOHOETHENE BDL 11-DICHLOROETHANE BDL TRANS-1 2-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 1 11 -TH I CHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 1 2-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1 12-TRICHLOROETHANE BDL BENZENE BDL CIS-1 3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1 122-TETRACHLOROETHANE BDL TOLUENE -BDL CHLOHOBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 104 BENZENED6 104 TOLUENED8 101 BROMOFLUOROBENZENE 105
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42148 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RV-04-104 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI tig
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIliE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE bull BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 120 BENZENED6 117 TOLUENED8 106 BROMOFLUOROBENZENE 118
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42149 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-Q5-105 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI ugi
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORI3E BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL I1-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE bull BDL DI8ROMOCHLOROMETHANE BDL I12-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 115 TOLUENED8 108 BROMOFLUOROBENZENE 112
NOTE The detection l i m i t foi the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42150 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-06-106 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040687 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ug1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPHOPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE bull BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
l2-DICHLOROETHANED4 99
BENZENE06 90 TOLUENED8 8
BROMOFLUOROBENZENE 91
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42151 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-07-107 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
040387 DATE SAMPLED 033087
RESULT PARAMETER RESULT ugI n g I
BDL BROMOMETHANE 1JDL BDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-OICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
128
97
93
94
NOTE The detection l i m i t for the compounds Acetone 2-Hexanone and 4-methy 1-2-Pentanone is SO ugI
BDL s BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42132 CLIENT MSFATTLEBOROSHPACK LF FLO ID SHP-RW-08-108 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-1 3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
RESULT a g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BOL BDL BDL
137
99
95 93
PARAMETER RESULT ugI
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 112Z-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methyl-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 u g 1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42153 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RW-09-109 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ng1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIEE BDL CHLOROETHANE BDL METHYLENE CHLORIDE 90 ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMQDICHLOROMETHANE BDL 12-DICHLOROPROFANE BDL TRAMS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-l3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 129 BENZENED4 97 TOLUENED8 97 BHOMOFLUOROBENZENE 94
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42134 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
P A R A M E T E R R E S U L T PARAMETER RESULT T i g 1 agI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLbROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE bull BDL 12-DICHLOROPROPANE BDL TRANS--1 3-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1I2-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 126 BENZENEDltS 117 TOLUENED3 107 BROMOFLUOROBENZENE 119
NOTE The det e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug I MI = MATRIX INTERFERENCE NA = NOT ANALYZED -SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42145 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-Ol-101 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT ag1
PARAMETER RESULT ugi
CHLOROMETHANEVINYL CHLORIJEMETHYLENE CHLORIDECARBON DISULFIDE1 1-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-l3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
BROMOMETHANECHLOROETHANEACETONE 11-DICHLOROETHENETRANS-l2-DICHLOROETHENE12-DICHLOROETHANE111-TRICHLOROETHANEVINYL ACETATE12-DICHLOROPROPANETRICHLOROETHENE112-TRICHLOROETHANECIS-1 3-DICHLOROPROPENEBROMOFORM4-METHYL-Z-PENTANONE1122-TETRACHLOROETHANECHLOROBENZENESTYRENE
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED4 TOLUENEDB BROMOFLUOROBENZENE
11 108 98 108
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hezanone and 4-methyl-2-Pentanone is SO ug1
BDLMINASD
= BELOW DETECTION LIMIT 10 = MATRIX INTERFERENCE
= NOT ANALYZED = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42146 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RV-02-102 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ag1 ug1
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 1l-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENpound BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY S
1 2-DICHLOROETHANED4 122 BENZENE06 112 TOLUENED8 101 BROMOFLUOROBENZENE 108
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42147 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-03-I03 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugt ugS
CHLOROMETHANE BDL BROMOMETHANE VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 1 1-DICHLOHOETHENE BDL 11-DICHLOROETHANE BDL TRANS-1 2-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 1 11 -TH I CHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 1 2-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1 12-TRICHLOROETHANE BDL BENZENE BDL CIS-1 3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1 122-TETRACHLOROETHANE BDL TOLUENE -BDL CHLOHOBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 104 BENZENED6 104 TOLUENED8 101 BROMOFLUOROBENZENE 105
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42148 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RV-04-104 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI tig
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIliE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE bull BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 120 BENZENED6 117 TOLUENED8 106 BROMOFLUOROBENZENE 118
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42149 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-Q5-105 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI ugi
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORI3E BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL I1-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE bull BDL DI8ROMOCHLOROMETHANE BDL I12-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 115 TOLUENED8 108 BROMOFLUOROBENZENE 112
NOTE The detection l i m i t foi the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42150 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-06-106 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040687 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ug1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPHOPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE bull BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
l2-DICHLOROETHANED4 99
BENZENE06 90 TOLUENED8 8
BROMOFLUOROBENZENE 91
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42151 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-07-107 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
040387 DATE SAMPLED 033087
RESULT PARAMETER RESULT ugI n g I
BDL BROMOMETHANE 1JDL BDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-OICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
128
97
93
94
NOTE The detection l i m i t for the compounds Acetone 2-Hexanone and 4-methy 1-2-Pentanone is SO ugI
BDL s BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42132 CLIENT MSFATTLEBOROSHPACK LF FLO ID SHP-RW-08-108 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-1 3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
RESULT a g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BOL BDL BDL
137
99
95 93
PARAMETER RESULT ugI
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 112Z-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methyl-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 u g 1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42153 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RW-09-109 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ng1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIEE BDL CHLOROETHANE BDL METHYLENE CHLORIDE 90 ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMQDICHLOROMETHANE BDL 12-DICHLOROPROFANE BDL TRAMS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-l3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 129 BENZENED4 97 TOLUENED8 97 BHOMOFLUOROBENZENE 94
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42134 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
P A R A M E T E R R E S U L T PARAMETER RESULT T i g 1 agI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLbROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE bull BDL 12-DICHLOROPROPANE BDL TRANS--1 3-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1I2-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 126 BENZENEDltS 117 TOLUENED3 107 BROMOFLUOROBENZENE 119
NOTE The det e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug I MI = MATRIX INTERFERENCE NA = NOT ANALYZED -SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42146 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RV-02-102 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ag1 ug1
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 1l-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENpound BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY S
1 2-DICHLOROETHANED4 122 BENZENE06 112 TOLUENED8 101 BROMOFLUOROBENZENE 108
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42147 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-03-I03 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugt ugS
CHLOROMETHANE BDL BROMOMETHANE VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 1 1-DICHLOHOETHENE BDL 11-DICHLOROETHANE BDL TRANS-1 2-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 1 11 -TH I CHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 1 2-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1 12-TRICHLOROETHANE BDL BENZENE BDL CIS-1 3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1 122-TETRACHLOROETHANE BDL TOLUENE -BDL CHLOHOBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 104 BENZENED6 104 TOLUENED8 101 BROMOFLUOROBENZENE 105
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42148 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RV-04-104 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI tig
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIliE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE bull BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 120 BENZENED6 117 TOLUENED8 106 BROMOFLUOROBENZENE 118
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42149 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-Q5-105 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI ugi
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORI3E BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL I1-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE bull BDL DI8ROMOCHLOROMETHANE BDL I12-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 115 TOLUENED8 108 BROMOFLUOROBENZENE 112
NOTE The detection l i m i t foi the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42150 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-06-106 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040687 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ug1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPHOPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE bull BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
l2-DICHLOROETHANED4 99
BENZENE06 90 TOLUENED8 8
BROMOFLUOROBENZENE 91
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42151 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-07-107 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
040387 DATE SAMPLED 033087
RESULT PARAMETER RESULT ugI n g I
BDL BROMOMETHANE 1JDL BDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-OICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
128
97
93
94
NOTE The detection l i m i t for the compounds Acetone 2-Hexanone and 4-methy 1-2-Pentanone is SO ugI
BDL s BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42132 CLIENT MSFATTLEBOROSHPACK LF FLO ID SHP-RW-08-108 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-1 3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
RESULT a g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BOL BDL BDL
137
99
95 93
PARAMETER RESULT ugI
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 112Z-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methyl-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 u g 1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42153 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RW-09-109 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ng1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIEE BDL CHLOROETHANE BDL METHYLENE CHLORIDE 90 ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMQDICHLOROMETHANE BDL 12-DICHLOROPROFANE BDL TRAMS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-l3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 129 BENZENED4 97 TOLUENED8 97 BHOMOFLUOROBENZENE 94
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42134 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
P A R A M E T E R R E S U L T PARAMETER RESULT T i g 1 agI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLbROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE bull BDL 12-DICHLOROPROPANE BDL TRANS--1 3-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1I2-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 126 BENZENEDltS 117 TOLUENED3 107 BROMOFLUOROBENZENE 119
NOTE The det e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug I MI = MATRIX INTERFERENCE NA = NOT ANALYZED -SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42147 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-03-I03 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugt ugS
CHLOROMETHANE BDL BROMOMETHANE VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 1 1-DICHLOHOETHENE BDL 11-DICHLOROETHANE BDL TRANS-1 2-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 1 11 -TH I CHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 1 2-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1 12-TRICHLOROETHANE BDL BENZENE BDL CIS-1 3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1 122-TETRACHLOROETHANE BDL TOLUENE -BDL CHLOHOBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 104 BENZENED6 104 TOLUENED8 101 BROMOFLUOROBENZENE 105
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42148 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RV-04-104 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI tig
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIliE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE bull BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 120 BENZENED6 117 TOLUENED8 106 BROMOFLUOROBENZENE 118
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42149 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-Q5-105 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI ugi
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORI3E BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL I1-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE bull BDL DI8ROMOCHLOROMETHANE BDL I12-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 115 TOLUENED8 108 BROMOFLUOROBENZENE 112
NOTE The detection l i m i t foi the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42150 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-06-106 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040687 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ug1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPHOPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE bull BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
l2-DICHLOROETHANED4 99
BENZENE06 90 TOLUENED8 8
BROMOFLUOROBENZENE 91
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42151 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-07-107 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
040387 DATE SAMPLED 033087
RESULT PARAMETER RESULT ugI n g I
BDL BROMOMETHANE 1JDL BDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-OICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
128
97
93
94
NOTE The detection l i m i t for the compounds Acetone 2-Hexanone and 4-methy 1-2-Pentanone is SO ugI
BDL s BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42132 CLIENT MSFATTLEBOROSHPACK LF FLO ID SHP-RW-08-108 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-1 3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
RESULT a g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BOL BDL BDL
137
99
95 93
PARAMETER RESULT ugI
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 112Z-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methyl-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 u g 1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42153 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RW-09-109 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ng1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIEE BDL CHLOROETHANE BDL METHYLENE CHLORIDE 90 ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMQDICHLOROMETHANE BDL 12-DICHLOROPROFANE BDL TRAMS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-l3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 129 BENZENED4 97 TOLUENED8 97 BHOMOFLUOROBENZENE 94
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42134 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
P A R A M E T E R R E S U L T PARAMETER RESULT T i g 1 agI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLbROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE bull BDL 12-DICHLOROPROPANE BDL TRANS--1 3-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1I2-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 126 BENZENEDltS 117 TOLUENED3 107 BROMOFLUOROBENZENE 119
NOTE The det e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug I MI = MATRIX INTERFERENCE NA = NOT ANALYZED -SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42148 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RV-04-104 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI tig
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIliE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE bull BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 120 BENZENED6 117 TOLUENED8 106 BROMOFLUOROBENZENE 118
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42149 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-Q5-105 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI ugi
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORI3E BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL I1-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE bull BDL DI8ROMOCHLOROMETHANE BDL I12-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 115 TOLUENED8 108 BROMOFLUOROBENZENE 112
NOTE The detection l i m i t foi the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42150 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-06-106 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040687 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ug1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPHOPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE bull BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
l2-DICHLOROETHANED4 99
BENZENE06 90 TOLUENED8 8
BROMOFLUOROBENZENE 91
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42151 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-07-107 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
040387 DATE SAMPLED 033087
RESULT PARAMETER RESULT ugI n g I
BDL BROMOMETHANE 1JDL BDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-OICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
128
97
93
94
NOTE The detection l i m i t for the compounds Acetone 2-Hexanone and 4-methy 1-2-Pentanone is SO ugI
BDL s BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42132 CLIENT MSFATTLEBOROSHPACK LF FLO ID SHP-RW-08-108 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-1 3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
RESULT a g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BOL BDL BDL
137
99
95 93
PARAMETER RESULT ugI
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 112Z-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methyl-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 u g 1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42153 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RW-09-109 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ng1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIEE BDL CHLOROETHANE BDL METHYLENE CHLORIDE 90 ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMQDICHLOROMETHANE BDL 12-DICHLOROPROFANE BDL TRAMS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-l3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 129 BENZENED4 97 TOLUENED8 97 BHOMOFLUOROBENZENE 94
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42134 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
P A R A M E T E R R E S U L T PARAMETER RESULT T i g 1 agI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLbROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE bull BDL 12-DICHLOROPROPANE BDL TRANS--1 3-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1I2-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 126 BENZENEDltS 117 TOLUENED3 107 BROMOFLUOROBENZENE 119
NOTE The det e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug I MI = MATRIX INTERFERENCE NA = NOT ANALYZED -SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42149 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-Q5-105 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ugI ugi
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORI3E BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL I1-DICHLOROETHENE BDL 1 1-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 1 2-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE bull BDL DI8ROMOCHLOROMETHANE BDL I12-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 115 TOLUENED8 108 BROMOFLUOROBENZENE 112
NOTE The detection l i m i t foi the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42150 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-06-106 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040687 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ug1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPHOPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE bull BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
l2-DICHLOROETHANED4 99
BENZENE06 90 TOLUENED8 8
BROMOFLUOROBENZENE 91
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42151 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-07-107 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
040387 DATE SAMPLED 033087
RESULT PARAMETER RESULT ugI n g I
BDL BROMOMETHANE 1JDL BDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-OICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
128
97
93
94
NOTE The detection l i m i t for the compounds Acetone 2-Hexanone and 4-methy 1-2-Pentanone is SO ugI
BDL s BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42132 CLIENT MSFATTLEBOROSHPACK LF FLO ID SHP-RW-08-108 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-1 3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
RESULT a g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BOL BDL BDL
137
99
95 93
PARAMETER RESULT ugI
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 112Z-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methyl-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 u g 1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42153 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RW-09-109 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ng1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIEE BDL CHLOROETHANE BDL METHYLENE CHLORIDE 90 ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMQDICHLOROMETHANE BDL 12-DICHLOROPROFANE BDL TRAMS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-l3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 129 BENZENED4 97 TOLUENED8 97 BHOMOFLUOROBENZENE 94
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42134 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
P A R A M E T E R R E S U L T PARAMETER RESULT T i g 1 agI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLbROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE bull BDL 12-DICHLOROPROPANE BDL TRANS--1 3-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1I2-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 126 BENZENEDltS 117 TOLUENED3 107 BROMOFLUOROBENZENE 119
NOTE The det e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug I MI = MATRIX INTERFERENCE NA = NOT ANALYZED -SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42150 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-06-106 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040687 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ug1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPHOPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE bull BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
l2-DICHLOROETHANED4 99
BENZENE06 90 TOLUENED8 8
BROMOFLUOROBENZENE 91
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42151 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-07-107 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
040387 DATE SAMPLED 033087
RESULT PARAMETER RESULT ugI n g I
BDL BROMOMETHANE 1JDL BDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-OICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
128
97
93
94
NOTE The detection l i m i t for the compounds Acetone 2-Hexanone and 4-methy 1-2-Pentanone is SO ugI
BDL s BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42132 CLIENT MSFATTLEBOROSHPACK LF FLO ID SHP-RW-08-108 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-1 3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
RESULT a g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BOL BDL BDL
137
99
95 93
PARAMETER RESULT ugI
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 112Z-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methyl-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 u g 1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42153 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RW-09-109 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ng1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIEE BDL CHLOROETHANE BDL METHYLENE CHLORIDE 90 ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMQDICHLOROMETHANE BDL 12-DICHLOROPROFANE BDL TRAMS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-l3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 129 BENZENED4 97 TOLUENED8 97 BHOMOFLUOROBENZENE 94
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42134 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
P A R A M E T E R R E S U L T PARAMETER RESULT T i g 1 agI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLbROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE bull BDL 12-DICHLOROPROPANE BDL TRANS--1 3-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1I2-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 126 BENZENEDltS 117 TOLUENED3 107 BROMOFLUOROBENZENE 119
NOTE The det e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug I MI = MATRIX INTERFERENCE NA = NOT ANALYZED -SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42151 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RV-07-107 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
040387 DATE SAMPLED 033087
RESULT PARAMETER RESULT ugI n g I
BDL BROMOMETHANE 1JDL BDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-OICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
128
97
93
94
NOTE The detection l i m i t for the compounds Acetone 2-Hexanone and 4-methy 1-2-Pentanone is SO ugI
BDL s BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42132 CLIENT MSFATTLEBOROSHPACK LF FLO ID SHP-RW-08-108 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-1 3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
RESULT a g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BOL BDL BDL
137
99
95 93
PARAMETER RESULT ugI
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 112Z-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methyl-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 u g 1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42153 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RW-09-109 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ng1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIEE BDL CHLOROETHANE BDL METHYLENE CHLORIDE 90 ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMQDICHLOROMETHANE BDL 12-DICHLOROPROFANE BDL TRAMS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-l3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 129 BENZENED4 97 TOLUENED8 97 BHOMOFLUOROBENZENE 94
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42134 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
P A R A M E T E R R E S U L T PARAMETER RESULT T i g 1 agI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLbROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE bull BDL 12-DICHLOROPROPANE BDL TRANS--1 3-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1I2-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 126 BENZENEDltS 117 TOLUENED3 107 BROMOFLUOROBENZENE 119
NOTE The det e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug I MI = MATRIX INTERFERENCE NA = NOT ANALYZED -SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42132 CLIENT MSFATTLEBOROSHPACK LF FLO ID SHP-RW-08-108 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-1 3-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
RESULT a g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BOL BDL BDL
137
99
95 93
PARAMETER RESULT ugI
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 112Z-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methyl-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 u g 1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42153 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RW-09-109 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ng1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIEE BDL CHLOROETHANE BDL METHYLENE CHLORIDE 90 ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMQDICHLOROMETHANE BDL 12-DICHLOROPROFANE BDL TRAMS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-l3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 129 BENZENED4 97 TOLUENED8 97 BHOMOFLUOROBENZENE 94
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42134 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
P A R A M E T E R R E S U L T PARAMETER RESULT T i g 1 agI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLbROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE bull BDL 12-DICHLOROPROPANE BDL TRANS--1 3-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1I2-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 126 BENZENEDltS 117 TOLUENED3 107 BROMOFLUOROBENZENE 119
NOTE The det e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug I MI = MATRIX INTERFERENCE NA = NOT ANALYZED -SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42153 CLIENT MSFATTLEBOROSHPACX LF FLD ID SHP-RW-09-109 SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040387 DATE SAMPLED 033087
PARAMETER RESULT PARAMETER RESULT ng1 ug1
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIEE BDL CHLOROETHANE BDL METHYLENE CHLORIDE 90 ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMQDICHLOROMETHANE BDL 12-DICHLOROPROFANE BDL TRAMS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-l3-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
1 2-DICHLOROETHANED4 129 BENZENED4 97 TOLUENED8 97 BHOMOFLUOROBENZENE 94
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42134 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
P A R A M E T E R R E S U L T PARAMETER RESULT T i g 1 agI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLbROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE bull BDL 12-DICHLOROPROPANE BDL TRANS--1 3-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1I2-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 126 BENZENEDltS 117 TOLUENED3 107 BROMOFLUOROBENZENE 119
NOTE The det e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug I MI = MATRIX INTERFERENCE NA = NOT ANALYZED -SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42134 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 040287 DATE SAMPLED 033087
P A R A M E T E R R E S U L T PARAMETER RESULT T i g 1 agI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLbROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE bull BDL 12-DICHLOROPROPANE BDL TRANS--1 3-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 1I2-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 126 BENZENEDltS 117 TOLUENED3 107 BROMOFLUOROBENZENE 119
NOTE The det e c t i o n l i m i t for the compounds Acetone 2-Hexanone and 4-methyI-2-Pentanone is SO ug1
BDL = BELOW DETECTION LIMIT 10 ug I MI = MATRIX INTERFERENCE NA = NOT ANALYZED -SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
EHT NO 42204 CLIENT CONFIDENTIAL FLD ID MB870I27 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040287
PARAMETER
CHLOROMETHANEVINYL CHLORDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
I2-DICHLOROETHANED4 BENZENEDiS TOLUENED8 BROMOFLUOROBENZENE
NOTE The detection l i m i t
RESULT ug1
BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
108 106 2 100
DATE SAMPLED 040287
PARAMETER RESULT ug1
BROMOMETHANE 1JDL CHLOROETHANE BDL ACETONE BDL 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 1 2-DICHLOROETHANE BDL 111-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL THICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds Acetone 2-Hexanone and 4-methy1-2-Pentanone is SOug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42206 CLIENT MSFATTLEBOROSHFACK LF FLD ID MB870128 SAMPLING SITE ERT WILMINGTON MA DATE ANALYZED 040387 DATE SAMPLED 040387
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIJE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM SQL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL TRANS-13-DICHLOROPROPENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL I122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 130 BENZENED6 100 TOLUENE08 99 BROMOFLUOROBENZENE 9i
NOTE The detection l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 ugI MI = MATRII INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42208 FLD ID MB870133 DATE ANALYZED 040487
PARAMETER
CHLOROMETHANEVINYL CHLORID2METHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANE TRANS-13-DICHLOROPROPENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENED6 TOLUENED8 BROMOFLUOROBENZENE
NOTE The d e t e c t i o n l i m i t
RESULT u g I
BDL BDL
BDL BDL
BDL BDL NA
BDL BDL
BDL BDL
BDL BDL
BDL BDL
BDL BDL BDL
101
89
93 88
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON MA DATE SAMPLED 040687
PARAMETER RESULT u g I
BROMOMETHANE BDL CHLOROETHANE BDL ACETONE 61 11-DICHLOROETHENE BDL TRANS-12-DICHLOROETHENE BDL 12-DICHLOROETHANE bull BDL 11I-TRICHLOROETHANE BDL VINYL ACETATE BDL 12-DICHLOROPROPANE BDL TRICHLOROETHENE BDL 112-TRICHLOROETHANE BDL CIS-13-DICHLOROPROPENE BDL BROMOFORM BDL 4-METHYL-2-PENTANONE BDL 1122-TETRACHLOROETHANE BDL CHLOROBENZENE BDL STYRENE BDL
for the compounds A c e t o n e 2-Hexanone
and 4 - n e t h y 1 - 2 - P e n t a n o n e is SO u g I
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
u g 1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42205 FLD ID LF870174
PARAMETER
11-DICHLOHOETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
108
105
130
104
97
DATE SAMPLED 040287 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42207 FLD ID LF870176
PARAMETER
11-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
RECOVERY
89
1 1 2
104
103
94
DATE SAMPLED 040387 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 42209 FLD ID LF870182
PARAMETER RECOVERY
11-DICHLOROETHENE 92
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROBENZENE
112
98
104
98
DATE SAMPLED 040487 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Analyses
Method Blank Results
Quality Control Sample Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42155 DATE SAMPLED 033087 FLD ID SHP-RW-01-101 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER BDL 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42 ISA DATE SAMPLED 033087 FLD ID SHP-RV-02-102 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY SDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 043 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42157 DATE SAMPLED 033087 FLD ID SHP-RV-03-103 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mgI mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 54 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC BDL 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42158 DATE SAMPLED 033087 FLD ID SHP-RW-04-1Q4 CLIENT MSFATTLEBOROSHPACK LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT ing 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 011 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42159 DATE SAMPLED 033087 FLD ID SHP-RW-05-105 CLIENT MSFATTLEBOROSHPACX LF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg 1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 023
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 11 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 1 2 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42142 DATE SAMPLED 033087 FLD ID SHP-RV-08-108 CLIENT MSFATTLEBOROSHPACK IF
SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMIT mg 1 mgI
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0042 025
LEAD BDL 05
MERCURY BDL 001
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 0 34 05
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
PARAMETER
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42143 FLD ID SHP-RV-09-109
RESULT mg 1
BDL
HDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
DATE SAMPLED 033087 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION LIMIT mg1
10
10
025
025
05
025
05
001
05
10
05
10
05
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT NO 42155A CLIENT MSFATTLEBOROSHPACK LF FLO ID LF870172 SAM P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
PARAMETER
A N T I M O N Y A RSEN I C B E R Y L L I U M C A D M I U M
C H R O M I U M COPPER LEAD N I CICEL S E L E N I U M
SI LVER T H A L L I U M
ZINC
RESULT
ugml
195
187
203
1 97
202 198
01
02 1 80
208
1 85
202
DETECTION L I M I T ugml
010 010 0 0 2 5 0 0 2 5 0 0 5 0 0 0 2 5 0 0 5 0 0 0 5 0 0 1 0 0 0 5 0 0 1 0 0 0 5 0
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y C O N T R O L CHECK SAMPLES M E TALS SCAN
ERT NO 421558 C L I E N T MSFATTLEBOROSHPACK LF FLO ID LF870173 S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
PARAMETER
ANT IMONY
A R S EN 1C
B E RYLLIUM
C A D M I U M
C H R O M I U M
COPPER LEAD
NICKEL
S E L E N I U M
S ILVER
T H A L L I U M
ZINC
R E S U L T
ugrnl
1 98
1 86
1 96
195
1 96
1 91 1 95
1 96
1 83
207
1 90
1 97
DETECTION LIMIT
ugml
010
0 10
0025 0025 0050 0025 0050
0050 010
0050
010
0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S Q U A L I T Y CONTROL CHECK SAMPLES
M E T A L S SCAN
ERT MO 42390 CLIENT MSfATTLESOROSHPACK LF
FLO ID MB870126 SAMPLING SITE j ERT W I L M I N G T O N
DATE SAMPLED 040187
P A R A M E T E R RESULT D E T E C T I O N L I M I T ugml ugml
A N T I M O N Y BDL 010 A R S E N I C BDL 010
B E R Y L L I U M BOL 0025 CADMI U M BDL 0025
C H R O M I U M BDL 0050 COPPER BDL 0025 LEAD BDL 0050 N I C K E L BDL 0050 S E L E N I U M BDL 010
SILVER BDL 0050
T H A L L I U M BDL 010 ZINC bull- BDL 0050
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S Q U A L I T Y C O N T R O L CHECK SAMPLES
M E R C U R Y
CLIENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N D ETECTION L I M I T 000074 ugmt
ERT NO FLD ID RESULT mg I
42160A LF870179 000456
42160B LF870180 000466
42188 HB870130 BDL
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y OF A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLES
METALS SCAN
ERT NO 42391
FLD ID LF870172
PARAMETER
A N T I M O N Y
A R S E N I C
B E R Y L L I U M
C A D M I U M
C H R O M I U M
COPPER LEAD
N I C K E L
S E L E N I U M
S I LVER
T H A L L I U M
ZINC
C L I E N T MSf A T T L E B O R O S H P A C K IF
S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED 040187
X R E C O V E R Y
98
94
102
99
101
99 101 101 90 104 93
101
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
METALS SCAM
ERT NO 42392FLO ID LF870173
P A R A M E T E R
A N T I M O N YA R S E N I CB E R Y L L I U MC A DMIUMC H R O M I U MCOPPERLEADN I C K E LS E L E N I U MS I L V E RT H A L L I U MZINC
C L I ENT MSFATTLEBOROSHPACK LF S A M P L I N G SITE ERT W I L M I N G T O N
DATE SAMPLED ~040187
X R E C O V E R Y
99 93
98 98 98
96 98
98 92
104 95
99
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
E R T A N A L Y T I C A L L A B O R A T O R Y SUMMARY OF ANALYTICAL RESULTS Q UALITY CONTROL CHECK SAMPLES
M E R C U R Y
C LIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLO ID X RECOVERY
42189
42190
LF870179
LF870180
91
93
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
PESTICIDES ANALYSES IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Sample Results
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
E R T A N A L Y T I C A L L A B O R A T O R Y
S U M M A R Y O F A N A L Y T I C A L R E S U L T S
SELECTED
C LIENT HSFATTLEBOROSHPACK If S A M P L I N G SITE NO R T O N A T T L E B O R O MA
PESTICIDES
P A R A M E T E R
ERT NO
FLD ID
a- BHC b- BHC 9- BHC
d- BHC
HEPTACHLOR A L D R I N H E PTACHLOR EPOXIDE E N D O S U L F A N I
p p 1 DOE D I E L D R I N
E N D R I N ENDampSULFAN II
p p ODD
E N D R I N A L D E H Y D E ENDOSULFAN SULFATEpp1
RESULT (ugl)
42164
SHP- RUshy
01-101
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005 lt010 lt010 lt010 lt0 10 lt010 lt010
DOT lt010
42167 SHP- R W shy
04-104
lt005
lt005
lt005 lt005
lt005 lt005 lt005
lt005 lt0 10
lt010
lt010 lt0 10
lt010
lt0 10 lt0 1 0
42168 S H P - R W shy
05-105
lt005
lt005 lt005
lt005 lt005 lt005 lt005
lt005 lt010 lt010
lt0 10
lt0 10
lt010
lt0 10
lt010
42165 SHP bullR W shy
C_- 1 02
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt010 lt010 lt0 10 lt0 1 0
lt010
lt010
lt010
42166 SHP- RWshy
03-103
lt005
lt005 lt005 lt005
lt005 lt005 lt005 lt005
lt0 10 lt0 10 lt010 lt010 lt0 10 lt0 10 lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y OF A N A L Y T I C A L R E S U L T S
SELECTED
C L I E N T MSFATTLEBOROSHPACK If
S A M P L I N G SITE NOR TONATTLEBORO MA
P ARAMETER
ERT NO 42169
FLD ID S H P - R W -06-106
a- BHC lt005
b - B H C lt005
g - B H C lt005 d- BHC lt005
H E P T A C H L O R lt005
ALDR IN lt005
H E P T A C H L O R EPOXIDE lt005
E N D O S U L F A N I lt005
pp 1 DDE lt010 D I E L D R I N lt010
ENDJUM lt010 ENDOSULFAN II lt010 pp 1 DDD lt0 10
E N O R I N A L D E H Y D E lt010
E N D O S U U F A N SULFATEpp 1 DDT lt010
PESTICIDES
RESULT (ugl)
42170 42171
S H P - R W - SHP- R W shy
07- 107 08- 108
lt005 lt005 lt0 05 lt005
lt005 lt005 lt005 4lt005 lt005 lt005 lt005 lt005 lt005 lt005
lt005 lt005 lt010 lt0 10
lt010 lt010
lt010 lt0 10
lt010 lt010
lt0 10 lt010
lt010 lt0 10
lt010 lt0 10
42172 S H P - R W shy
09-109
lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 lt0 10 lt010 lt0 10 lt0 10 lt0 10 lt0 10
42445 HB870131
lt005 lt005
lt005 lt005 lt005 lt005 lt005 lt005 lt0 10 ltC 10
lt0 10
lto ro lt010
lt0 10
lt0 10
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
E R T A N A L Y T I C A L L A B O R A T O R Y S U M M A R Y O F A N A L Y T I C A L R E S U L T S
Q U A L I T Y CONTROL C H E C K SAMPLE RESULTS S ELECTED P E S T I C I D E S
C L I E N T M S f A T T L E B O R O S H P A C K If
S A M P L I N G SITE ERT W I L M I N G T O N
P A R A M E T E R X RECOVERY
ERT NO 42446 FLD ID LF370181
a - B H C 120 b - B H C 123 g - BHC 110 d - B H C 137 HEPTACHLOR 100 A L D R I N 87 HEPTACHLOR EPOXIDE 106 ENDO S U L F A N I 75
pp DDE 119 D I E L D R I N 110
ENDR IN 123 ENDOSULFAN II 79
pp1 DOD 82
E N D R I N A L D E H Y D E 55 E N D O S U L F A N SULFATEpp DDT 114
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
CHAIN - OF - CUSTODY RECORDS
MSF ATTLEBORO SHPACK LANDFILL
NORTONATTLEBORO MA
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
SAMPLE RECEIPT CHECK LIST
Client
COC Record s) ltpound -- lt
Matrix Container ERT (s)
VO -A
Yd SshyJc shy
1 Were samples shipped or hand-delivered
Notes Yes No
2 Was COC record present upon receipt of samples D t
Notes Yes
3 Was COC tape presentunbroken on outer package
Notes ltUo lltx|raquo-pound_
4 Were samples received ambient or chilled C XX
Notes Yes
5 Were any samples received brokenleaking (improperly sealed D KlnfAG O bull r f v I ft Notes otCuf^A^ -amp-ltlt3nlaquoJi_ Jf^eelt
- No 6 Were samples properly preserved or D
Notes JTxcep-1- fcctttj) pound poundbull
7 Were COC types presentunbroken on samples r r Notes
Yes No 8 Any discrepancies between sample labels and COC records D
Notes Yes No
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in by Date
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
I (gtJiltjj
VOLATILE ORGANIC COMPOUND ANALYSES
IN WATER
Summary of Analytical Results
Method Blank Results
Quality Control Check Samples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42301 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHP-RW-10-110 SAMPLING SITE NORTONATTLESORO MA DATE ANALYZED 042187 DATE SAMPLED 041087
PARAMETER RESULT PARAMETER RESULT ugI ugI
CHLOROMETHANE BDL BROMOMETHANE BDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE BDL CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DICHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-3UTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL 12-DICHLOROPROPANE BDL THANS-13-DICHLOHOPROFENE BDL TRICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE SDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED4 7 TOLUENED8 101 BROMOFLUOR03ENZpoundNE 113
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-HeKanone and 4-methy 1-2-Pentanone is SO ugI
BDL = BELOU DETECTION LIMIT 10 ugI MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42302 CLIENT MSFATTLESOROSHPACK LF FLD ID SHP-RV-11-H1 SAMPLING SITE NORTONATTLEBCRO MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECARBON DISULFIDE11-DICHLOROETHANECHLOROFORM2-BUTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETRANS-1 3-DICHLOROPRO-PENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLUENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BENZENEDamp TOLUENED8 BHOMOFLUOROBENZENE
042187 DATE SAMPLED 041087
RESULT PARAMETER RESULT ugI ngI
BDL BROMOMETHANE BDL HDL CHLOROETHANE BDL
BDL ACETONE BDL BDL 11-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE BDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETHANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
73 78 82 87
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is SO ugI
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug1
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 42303 CLIENT MSFATTLEBOROSHPACK LF FLD ID SHIPPING BLANK SAMPLING SITE NORTONATTLEBORO MA DATE ANALYZED 042187 DATE SAMPLED 040287
PARAMETER RESULT PARAMETER RESULT ugI agl
CHLOROMETHANE BDL BROMOMETHANE 1JDL VINYL CHLORIDE BDL CHLOROETHANE BDL METHYLENE CHLORIDE BDL ACETONE 150 CARBON DISULFIDE BDL 11-DICHLOROETHENE BDL 11-DICHLOROETHANE BDL TRANS-12-DCHLOROETHENE BDL CHLOROFORM BDL 12-DICHLOROETHANE BDL 2-BUTANONE NA 111-TRICHLOROETHANE BDL CARBON TETRACHLORIDE BDL VINYL ACETATE BDL BROMODICHLOROMETHANE BDL I2-DICHLOROPROPANE BDL TRANS-1 3-DICHLOHOPRO-PENE BDL THICHLOROETHENE BDL DIBROMOCHLOROMETHANE BDL 112-TRICHLOROETHANE BDL BENZENE BDL CIS-13-DICHLOROPROPENE BDL 2-CHLOROETHYL VINYL ETHER BDL BROMOFORM BDL 2-HEXANONE BDL 4-METHYL-2-PENTANONE BDL TETRACHLOROETHENE BDL 1122-TETRACHLOROETHANE BDL TOLUENE BDL CHLOROBENZENE BDL ETHYL BENZENE BDL STYRENE BDL TOTAL XYLENES BDL
SURROGATE RECOVERY
12-DICHLOROETHANED4 102 BENZENED6 108 TOLUENED8 112 BROMOFLUOROBENZENE 122
NOTE The d e t e c t i o n l i m i t for the compounds Acetone 2-Hesanone and 4-methy1-2-Pentanone is 50 ug1
BDL BELOW DETECTION LIMIT 10 ug1 MI = MATRIX INTERFERENCE NA = NOT ANALYZED 3D = SAMPLE DILUTED
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS IN WATER
ERT NO 43084 CLIENT ERT QAQC CHECK SAMPLE FLD ID MB370217 SAMPLING SITE ERT-WILMINGTON MA DATE ANALYZED
PARAMETER
CHLOROMETHANEVINYL CHLORIDEMETHYLENE CHLORIDECAHSON BISULFIDE1 1-DICHLOROETHANECHLOROFORM2-8UTANONECARBON TETRACHLORIDEBROMODICHLOROMETHANETHANS-1 3-DICHLOROPROJENEDIBROMOCHLOROMETHANEBENZENE2-CHLOROETHYL VINYL ETHER2-HEXANONETETRACHLOROETHENETOLiENEETHYL BENZENETOTAL XYLENES
SURROGATE RECOVERY
12-DICHLOROETHANED4 BpoundNZENE06 TOLUENED8 SROMOFLUOROBENZENE
042187 DATE SAMPLED 042187
RESULT PARAMETER RESULT ugI ugI
BDL BROMOMETHANE BDL BDL CHLOROETHANE BDL
BDL ACETONE 53 11 1 1-DICHLOROETHENE BDL
BDL TRANS-12-DICHLOROETHENE BDL BDL 12-DICHLOROETHANE BDL NA 111-TRICHLOROETHANE BDL
BDL VINYL ACETATE BDL BDL 12-DICHLOROPROPANE SDL
BDL TRICHLOROETHENE BDL BDL 112-TRICHLOROETHANE BDL
BDL CIS-13-DICHLOROPROPENE BDL BDL BROMOFORM BDL
BDL 4-METHYL-2-PENTANONE BDL BDL 1122-TETRACHLOROETKANE BDL
BDL CHLOROBENZENE BDL BDL STYRENE BDL BDL
65 69 74 82
NOTE The detection limit for the compounds Acetone 2-Heianone and 4-methyI-2-Pentanone is 50 ug1
BDL = BELOW DETECTION LIMIT 10 MI = MATRIX INTERFERENCE NA = NOT ANALYZED SD = SAMPLE DILUTED
ug I
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES VOLATILE ORGANIC COMPOUNDS
ERT NO 43087 FL0 ID LFS70286
PARAMETER
1 1-DICHLOROETHENE
TRICHLOROETHENE
BENZENE
TOLUENE
CHLOROSENZENE
RECOVERY
109
131
124
121
126
DATE SAMPLED 042187 CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
SELECTED PESTICIDES ANALYSES
IN WATER
Summary of - alytical Results
Method Blank Results
Quality Control Check SaTxples
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
PESTICIDES AND PCBS
CLIENT MSFATTLEBOROSHPACK LF SAMPLING LOCATION NORTONATTLEBORO MA
ERT NO FIELD ID
PARAMETER
ALDRIN i-BHC b-8HC d-SHC g-SHC 4 4 -DOD 44-DDE ENDOSULFAN I ENDOSULFAN II EN003ULFAN SULFATEP E 44-DDT
ENDRIN ENDSIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOZIDJEE
43504 SHP-RVshy01-110
u g I
lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 05 lt0 10 lt0 10 lt 0 0 5 lt 0 1 0 lt 0 _ 1 0
lt 0 1 0 lt 0 1 0 lt0 05 lt 0 0 5
43507 SHP-RVshy11-111
a g I
lt 0 0 5 ( 0 0 5 lt 0 0 5 lt 0 0 5 lt 0 0 5 lt0 10 lt0 10 lt0 05 lt 0 1 0 lt 0 1 0
lt 0 1 0 lt0 10 lt 0 0 5 ( 0 05
42507 MB870U1
u g 1
( 0 0 5 ( 0 0 5 ( 0 0 5 ( 0 05 ( 0 0 5 (0 10 (0 10 ( 0 0 5 (0 10 lt 0 1 0
(0 10 ( 0 1 0 ( 0 0 5 ( 0 0 5
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
PESTICIDES IN WATER
ERT NO 42508 FLD ID LF87021
PARAMETER
ALDRIN n-BHC D-3HC d-BHC g-SHC 4 4-DDE 44 -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHY-DE 4 4-ODD
HEPTACHLOR HEPTACHLOR EPOXIDE
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON DATE SAMPLED 041787
RECOVERY
97 123 131 122 128 152 114 141 81 66
133 122 142
116 113
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
PRIORITY POLLUTANT METALS ANALYSES
IN WATER
Summary of Analytical Results
Duplicate Sample Results
Method Blank Results
Quality Control Check Samples
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42304 DATE SAMPLED 041087 FLD ID SHP-RV-10-110 CLIENT MSFATTLEBOROSHPACX LF DATE ANALYZED 042887 SAMPLING SITE NORTONATTLEBORO MA
PARAMETER RESULT DETECTION LIMI1 mg 1 mg1
ANTIMONY BDL 10
ARSENIC BDL 10
BERYLLIUM BDL 025
CADMIUM BDL 025
CHROMIUM BDL 05
COPPER 0 18 025
LEAD BDL 05
MERCURY BDL 0006
NICKEL BDL 05
SELENIUM BDL 10
SILVER BDL 05
THALLIUM BDL 10
ZINC 021 05
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
METALS SCAN
ERT NO 42305 FLO ID SHP-RV-11-m DATE ANALYZED 042887
PARAMETER RESULT mg1
ANTIMONY BDL
ARSENIC BDL
BERYLLIUM BDL
CADMIUM BDL
CHROMIUM BDL
COPPER BDL
LEAD BOL
MERCURY BDL
NICKEL BDL
SELENIUM BDL
SILVER BDL
THA LLI UM BDL
ZINC BDL
DATE SAMPLED 041087 CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA
DETECTION L IT mg 1
10
10
025
025
05
025
05
0006
05
10
05
10
05
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
EHT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS QUALITY CONTROL CHECK SAMPLES
METALS SCAN
ERT NO 42647FLD ID MB870154
PARAMETER
ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUMCOPPERLEADNICKELSELENIUMSILVER THALLIUMZINC
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE ERT WILMINGTON
DATE SAMPLED 042887
ANALYTICAL RESULTS DETECTION LIMIT tigml ugml
BDL 0010 BDL 0010
BDL 0023 BDL 0025 BDL 0050
BDL 0025 BDL 0050
BDL 0050 BDL 010
BDL 0050 BDL 010
BDL 0050
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
MERCURY
CLIENT MSFATTLEBOROSHPACK LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 000044
ERT NO FLD ID RESULT Tigml
42262A42262B
LF370210 LF370211
000478 000549
42482 MB870157 BDL
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
EHT A N A L Y T I C A L LABORATORY SUMMARY OF A N A L Y T I C A L RESULTS Q U A L I T Y CONTROL CHECK SAMPLES
MERCURY
CLIENT MSF ATTLEBORO SHPACK LF SAMPLING SITE ERT WILMINGTON
ERT NO FLD ID R E C O V E R Y
42483 LF870210 94
42484 LF870211 110
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
TOTAL CYANIDE ANALYSES IN WATER
SUmmary of Analytical Results
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT ANALYTICAL LABORATORY SUMMARY OF ANALYTICAL RESULTS
TOTAL CYANIDES
CLIENT MSFATTLEBOROSHPACX LF SAMPLING SITE NORTONATTLEBORO MA DETECTION LIMIT 005 DATE ANALYZED 041387
ERT NO FLD ID RESULT mg1
42308 SHP-RV-06-106 BDL
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
CHAIN - OF - CUSTODY RECORDS
SHPACK LANDFILL
ATTLEBORONORTON MA
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
C S- eg2gt or gt co c C OT O raquoshy
LU to O co
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
SAMPLE RECEIPT CHECK LIST
COC Record (s) 773 pound-7 bull
Matrix Container ERT (s)
^laquo^U VOA 3oAi-o4raquo bull3o) shy ^cjyo^ Ato VeJIOX ^P^CX^
-lt -fast y5Jlt^ $OJ07 (^jjshy bull bullbullbull 4^3-^5^shy
1 Were samples shipped or hand-delivered W^^ ampLampvltLpoundampT
Notes -
2 Was COC record present upon receipt of samples
Notes
3 Was COC tape presentunbroken on outer package
Notes
4 Were samples received ambient or chilled ltshy
Notes
5 Were any samples received brokenleaking (improperly sealed
C J bull ^7 9 l~fNotes jlaquo^rT ltt^ -frtvj7^ltj SaAff -pound+ amppoundJHM44itshy0 Were samples properly preserved
Notes
7 Were COC types presentunbroken on samples l
Notes
8 Any discrepancies between sample labels and COC records
Notes
9 Were samples received within holding times
Notes
Additional Comments
Samples inspected and logged in hv ~2ampy~poundtd(Lst
tshy
bull
bull
Yes No iir ^^
a
Yes D
Yes
Yes D
Yes a
Yes
Q 1
No
No D
No
NoNO or
No D
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ANALYTICAL SERVICES 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070 RECEIVED
By A DOArK
WEHRAN ENGINEERING MSTHUEN MA
REPORT OF ANALYSIS
Wehran Engineering Job Identification Private Well 100 Milk Street Methuan MA 01844 Samnles Shoack Site
Date Received 33187 Attn Mr Peter Croteau
CHAS Lab 36357 - 36365
PO f 50046-20
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific QAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate y Joseph Lentini
Radiological Supervisor
MA KINGSTON MA NATICK MA SOUTH BOSTON MA SOUTH PCRTUNO WE AlEANY NV PROVDSCE Rl 16171 39-1800 I617I 565 -511 1617) 655-8863 16171 269-5330 12071 799 8111 (5181 434-0149 14011 plusmn01-1300
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
Client Wehran Engineering
Sample Identification
SHP-RW-01-101
SHP-RW-02-102
SHP-RW-03-103
SEP-RW-04-104
SHP-RW-05-105
SHP-Rtf-06-106
SHP-RW-07-107
SHP-RW-08-108
SHP-RW-09-109
Parameter
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
Gross Alpha Particle Gross Beta Particle Radon-222
CHAS Lab s 36357 - 36365 Date Received
Result
13 + 06 13 + 05 7580 + 100
07 + 05 15 + 05 1860 + 50
04 + 04 10 + 04
1940 + 50
-00+02 06 j- 03 2170 + 60
02 + 04 09 + 04 2260 + 60
31 + 14 68 + 11 1570 + 50
06 + 05 18 + 04 4070 + 80
20 4- 07 20 4- 04 6320 + 100
04 + 04 30 +_ 05 1110 -f- 40
33187
Units
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
pCi1 pCi1 pCi1
Notes Error = 2 standard deviations
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ANALYTICAL SERVICES RECEIVED 325 WOOD ROAD BRAINTREE MA 02184
(617) 849-6070
APR 3 01987
WEKRAN ENGiNEtiiElNG METMUEN MA
REPORT OF ANALYSIS
Wehran Engineering Co Job Identification Water Samples 100 Milk Street Methuen MA 01844
Date Received 41387 Attn Mr Peter Croteau
CHAS Lab 36399 - 36401
PO Croteau
Enclosed are the results for the sample(s) delivered to our laboratory on the date indicated above
Should you have any questions concerning this work please do not hesitate to contact me
This laboratory follows quality assurancequality control procedures outlined in EPA Publication EPA 6004-79-019 Handbook for Analytical Quality Control in Water and Wastewater Laboratories March 1979 and specific OAQC requirements of the procedures used
The information contained in this report is to the best of my knowledge accurate and complete
PerDate1^ _ bdquo Josebh Lentini x Radiological Supervisor
BRAINTREE MA KINGSTON MA MATICX MA SOUTH SOSTCN WA SOUTH PORTLAND ALBANY NY 1617) S49-180O (6171 585-5111 (617) 655-8863 16171 269-5330 (516 434-0149 (2071 799 811 1
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
Client Wehran Engineering Co CHAS Lab-s 36399 shy 36401 Date Received 41387
Sample Identification Parameter Result Units
SHF-RW-10-110 Gross Alpha Particle 06 +04 pCi1 Gross Beta Particle 08 + 13 pCi1 Radon-222 240+ 50 pCi1
SHP-RW-11-111 Gross Alpha Particle 0+02 pCi1 Gross Beta Particle 02 + 13 pCi1 Radon-222 80 + 50 pCi1
Shipping Blank Radon-222 90 + 50 pCi1
Notes Error shy 2 standard deviations
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
A RESOURCE ENGINEERING COMPANY 696 VIRGINIA ROAD CONCORD MA 01742 (617) 369-3910
ERT Ref No 102-APP-020 environmental and engineering excellence ERT Proj No D921-137
April 28 1987
Mr Peter Croteau Wehran Engineering 100 Milk St Methuen MA 01844
Dear Mr Croteau
Enclosed please find six (6) copies of the-report of analysis for various water samples submitted from the SHPACK landfill site (5004620) Attleboro MA on March 31 1987 The cost for these analyses is $510300 and will be invoiced separately
Sincerely
Arthur P Paradice Program Manager Analytical Chemistry
APPpjp
cc memo only
M Devine E Lang J Mastone M Sparlin T Trainor K Burger Wehran Engineering
+ disposition letter M Lynn
+ report Chemistry File
CALIFORNIA bull COLORADO bull ILLINOIS bull MASSACHUSETTS bull PENNSYLVANIA bull TEXAS bull WASHINGTON
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
ERT 33 Industrial Way Wilmington MA 01887 (617) 658-6399
From LABORATORY MANAGER
Date of Issuance April S8 1987
Subject SAMPLE RETENTION TERMS
Client MSF SHPACK Attleboro (D9S1-137)
Date Sample Received March 31 1987
Number cf Samples ReceivedMatrix 9 water
It is the policy of ERT to dispose of unanalyzed portions of samples thiry (30) days following submittal of the pertinent final analytical results report This letter serves as notification that the above samples will be due for disposal Sample extracts for organic analyses will be archived for one (1) year Separate notification wi l l be sent to you prior to disposal of sample extracts
A ERT will return to you all unused samples at your expense (Federal Express) or
B ERT will maintain custody of the samples at a cost of fifteen dollars ($1500) per sample per quarter for refrigerated storage and three dollars ($300) per sample per quarter for ambient storage You will be billed in advance each quarter based upon the number of samples in storage at the beginning of the quarter The minimum storage fee per project will be fifty dollars ($5000) per quarter to cover administrative costs
YOU MUST RETURN THIS LETTER TO THE LABORATORY MANAGER WITH PROPER AUTHORIZATION (ie Purchase Order Number Federal Express Number etc) SAMPLE OPTION SIGNATURE AND DATE WITHIN THIRTY (30) DAYS OF ISSUANCE OR THE SAMPLES INDICATED ABOVE WILL BE DISPOSED
OPTION
AUTHORIZATION NO (Federal Express)
(Purchase Order)
SIGNATURE
DATE
