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Research activities in the fields of metal and glass forming

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UMR 8201 Research activities in the fields of metal and glass forming Keywords Cold and hot forming, Tribology, Surface functionalities, Material behaviour, defectology, Thermal analysis, heat treatments, Experimental and numerical developments.
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UMR 8201

Research activities in the fields of metal and glass forming Keywords

Cold and hot forming, Tribology, Surface functionalities, Material behaviour, defectology, Thermal analysis, heat treatments, Experimental and numerical developments.

UMR 8201

Staff 2012

Status Members 2009

Members 2012

Professors 4 4 + 2 (50%)

Associate Professors 2 4

Engineers / Technicians 1 / 2 1 / 2

Total of permanent staff 9 12

Post Doc. / Contract Researchers 3 7

PhD Students (on-going) 7 7

Total 19 26

Invited Professors 0 3

International Chair 0 1

Perm

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UMR 8201

Research activities according to two scientific themes…

…applied to five Strategic Projects justified by societal, environmental and industrial needs

Strategic Project 1

Strategic Project 2

Strategic Project 3

Strategic Project 4

Strategic Project 5

Scientific theme 1

Scientific theme 2

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Scientific Themes

Identification of objective data to characterize surfaces undergoing extreme loadings: high temperatures, high contact pressures, high sliding speeds. Example of scientific challenges

Unbiased measurement of roughness parameters;

Fluid/Solid coupling between rough deformable surfaces;

Damage of materials in the surface vicinity;

Thermal exchange at glass/mould interface.

Theme 1: material behaviour in the surface vicinity under extreme conditions

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Scientific Themes

Understanding of material structure and behaviour evolutions due to the complex thermo-mechanical loadings imposed by forming processes. Taking into account of material changes on process response. Example of scientific challenges

Downscaling of process analysis to define links between

manufacturing processes and material properties;

Objective prediction of the damage of materials in core

induced by thermal and/or mechanical loadings;

Accurate modelling of radiation in glass modelling.

Theme 2: material/process coupling.

UMR 8201

SP4: SAFETY QUALITY Defectology at high temperature

SP3: PRODUCTIVITY High speed processes

SP1: SENSORY QUALITY Roughness and surface functionalities

SP2: ENERGY SAVING Cold forming & lightweight design

SP5: NICHE RESEARCH in Glass forming and tempering

Strategic Projects:

LAMIH and TEMPO strategic goals

UMR 8201

Strategic Projects:

Sensory quality: roughness and surface functionalities

Reliability of roughness and hardness measurements

Effect of process on surface functionality (brightness, wettability, hardness…)

University of Lyon

Technical University of Compiègne

Theme 1

Theme 2

(M. Bigerelle, C. Hubert, R.Deltombe)

LAMIH-C2S Research team

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Strategic Projects:

Energy saving: cold forming & light weight design

Lubrication of cold forming processes

Defects induce by forming sequences. Developments of

fast sheet forming computations

Theme 1

Theme 2

Theme 2

Technical University of Compiègne

Technical University

of Denmark

(L. Dubar, M. Dubar, A. Dubois, C. Hubert, T. Garcon, B. Laurent)

UMR 8201

Strategic Projects: Productivity: high speed processes

Effect of process parameter on material behaviour

Theme 1

Theme 2 University of Bordeaux

University of Châlon/Champagne

Tribology of high speed machining

University of Basque Country

(L. Dubar, M. Watremez, C. Hubert, T. Garcon, B. Laurent)

TEMPO-DF2T research team

LAMIH-C2S Research team

UMR 8201

Strategic Projects:

Safety quality: defectology at high temperature

Lubrication and tool damage in hot rolling and forging Heat gradient and defect

occurrences. Work hardening/softening at high temperatures.

Theme 1

Theme 2

University of Venezuela

(M. Dubar, JD Guérin, A. Dubois, T. Garcon, B. Laurent)

UMR 8201

Strategic Projects:

niche research induced by the material Glass forming and tempering

Lubricants & lubrication of glass forming processes

Modelling of glass forming and tempering

Theme 1

Theme 2 Lab. Of Photoelasticity, Estonia

Fraunhoher Institute ITWM,

Germany

University of Cliveland

University of Princeton

(D. Lochegnies, F. Bechet, P. Moreau)

TEMPO-DF2T research team

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Some scientific bottleneck removed

Radiation in 2D glass forming modelling. Stress in-homogeneity analysis in glass tempering. (SP5)

Development of advance friction law for high speed sliding contact. (SP3)

Innovative staggered algorithm for modelling of rough surfaces lubrication. (SP2)

Expert system to analyses roughness effect on surface functionality. (SP1)

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Presentation of Scientific Project 1

Modelling of Lubrication Mechanisms at Mesoscale

presented by Cedric HUBERT

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Context of the study Mixed lubrication regime

is often required

• to reduce friction • to master the final surfaces roughness

The real contact area is of major importance in the contact management

Two phenomena are involved

in the contact

• the dry tool/workpiece contact • the lubricant pressurization

part

tool

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15

Developed modelling strategy

Simplified surface topography

Real surface topography

Fluid/Structure interaction model Experimental tribotest

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Finite Element model of the process

Finite Element strip profile

16

Developed modelling strategy

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Developed modelling strategy General procedure

lubricant film thickness

pocket pressure

tool/strip relative speed

lubricant film thickness

plateau length

lubricant viscosity

lubricant flow

initiates the first F/S increment

starts new F/S increment

calculates the fluid exchanges

sets fluid fluxes as boundary conditions

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Developed modelling strategy General procedure

initiates the calculation

(fully coupled F/S)

starts new F/S increment

calculates fluid exchanges sequentially

sets fluid fluxes as boundary conditions

Micro Plasto Hydro-Static Lubrication (forward escape)

Micro Plasto Hydro-Dynamic Lubrication (Backward escape)

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The experimental setup Tribotester

Strips surface profile

triangle cross sectioned grooves

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Experimental investigations Running conditions • 2 drawing speeds, 2 viscosities

• Parameters are crossed

aluminium strip

Vs1 = 5mm.s–1

Vs2 = 50mm.s–1

η1 = 60cSt (η1 = 0.054Pa.s)

η2 = 660cSt (η2 = 0.595Pa.s)

η1 = 60cSt

η2 = 660cSt

reduction: r = 16%

viscosities are given at 40°C

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21

Experimental investigations Validation of the fluid exchange assumption • Exchange by backward escape (MPHDL)

• Exchange by forward escape (MPHSL)

Vs = 5mm.s–1, η = 60cSt, 125fps, played at 30fps

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Experimental investigations Model calibration • Determination of h by means of roughness measurements

• h is assumed to be the arithmetic roughness of the plateaus • measured by means of a laser interferometer, normal to drawing direction

drawing

Vs2 = 50mm.s–1, η1 = 60cSt

0µm

-3µm

1 2 3

Vs2 = 50mm.s–1, η2 = 660cSt

-10µm

0µm 1 2 3

Vs2, η1 Vs2, η2

h (µm) 0.3µm 0.747µm

• Determined values of h (µm)

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Experimental/numerical comparison Pockets depth evolution • Result for case Vs1, η1

2 1 3

• Contact gap behaviour • 1: contact entry, the pocket (opened) loses a large amount of lubricant • 2: the pocket is closed and exchanges lubricant with the neighbouring ones • 3: contact exit, the pocket is opened and releases the remaining pressure

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Ongoing investigations on surfaces

Example of initial surface

Example of final surface

initial pocket region

deformed pattern

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25

Ongoing investigations on surfaces

Hydrostatically deformed plateaus surface

Affects the h parameter measurement Can not be reproduced in the present model

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26

Ongoing investigations

Determination of a reliable, less local and statistical

film thickness

Analysis of virgin and deformed surfaces to understand

the lubricant paths

Scale down the whole model or parts of it

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27

Presentation of Scientific Project 2

Advanced frictional laws for high speed machining

presented by Michel WATREMEZ

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High Speed Processes

Context: Numerical approaches are necessary for:

• productivity • tool wear • residual stresses.

Existing numerical approaches with current friction models: not very good correlation with process variables.

Advanced frictional laws for high speed machining

Error related to contact conditions in the tool-chip interface: - rheological behaviour - representative friction model.

Tool

Workpiece

Chip

Zone 1

Zone 2

Zone 1:

Ø Low sliding velocity Ø Contact pressure value higher than 1 Gpa Ø Interfacial temperature about 1075 K

Zone 2:

Ø High sliding velocity (Vchip) Ø Lower contact pressure Ø Interfacial temperature up to 1375 K

originality:

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Study of the first zone with the Upsetting Sliding Test Input parameters

• Geometry of contactor • Temperature of contactor from ambient to 150°C • Displacement velocity from 0 to 0.5m.s-1

• Geometry of specimen • Temperature of specimen from ambient to 1200°C • Relative penetration Output parameters • Normal force until 30 kN • Tangential force until 25 kN • Track (profilometry) • Temperature (pyrometer)

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contactor

tangential force

specimen

Friction track

p

normal force

contactor moving

direction

UST parameters: • relative penetration • contactor geometry • sliding velocity • contactor and specimen temperatures.

Specimen

Friction track

Contactor

50 mm

30 mm

19 mm

Numerical model of UST

• first to determine input parameters • then to evaluate m by inverse method

Contactor

Specimen part

UMR 8201

METHODOLOGY FOR FRICTION ANALYSIS

Numerical machining model

Numerical model of U.S.T.

Test performance

1) Numerical machining model à Contact characteristics (contact pressure, sliding velocity, temperature).

2) Numerical model of U.S.T. à input parameters (penetration, temperature and displacement velocity).

3) Tests à Forces in both normal and tangential directions.

4) Numerical model of U.S.T. (inverse

method) à Friction coefficient

à Several configurations: frictional law.

5) Numerical machining model.

Methodology for friction analysis

UMR 8201

TOOL

WORPIECE

Exit chip

Exit material

Entry material

32

Machining model

• ALE (Arbitrary Lagrangian Eulerian) formulation. • take into account the area closer to the cutting edge, where the chip is formed. • workpiece: deformable body / tool: rigid. • workpiece composed with one entrance and two exits. • thermoviscoplastic behaviour: Johnson-Cook constitutive law.

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33

0. =¶¶

-nTk

0. =¶¶

-nTk

0. =¶¶

-nTk

)(. TKnTk D=

¶¶

-

0. =¶¶

-nTk

0. =¶¶

-nTk

)(. ¥-=¶¶

- TTKnTk

)(. ¥-=¶¶

- TTKnTk

WORKPIECE

TOOL

Machining model

• ALE (Arbitrary Lagrangian Eulerian) formulation. • take into account the area closer to the cutting edge, where the chip is formed. • workpiece: deformable body / tool: rigid. • workpiece composed with one entrance and two exits. • thermoviscoplastic behaviour: Johnson-Cook constitutive law.

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Machining model

Progress of chip formation during an orthogonal cutting Simulation for a machining time of 12 ms

(a) 0 ms

(b) 0.4 ms

(c) 0.8 ms

(d) 1.2 ms

(e) 1.6 ms

(f) 2.0 ms

(g) 2.5 ms

(h) 12 ms

The chip thickness and the chip-tool contact length gradually

change to their final size.

Geometry and forces: stabilized after 2,5 ms

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Number of tested configurations 1 2 3 4 5 6 7 8 9 10 11

Penetration (mm) 80 80 100 100 80 80 100 100 120 120 120

Speed (mm.s-1) 200 400 200 400 200 400 200 400 60 200 400

Temperature (K) 650 650 650 650 750 750 750 750 950 950 950

0

2,5

5

7,5

10

12,5

20 30 40 50 60 70 80 90Déplacement (mm)

Forc

es (k

N)

Stationary zone

Fn

Ft

Displacement (mm)

Tests results of the sixth configuration.

Test conditions n° Tspe (K) p (mm) V(mm.s-1) FT (kN) FN (kN) FT/FN

6 752 0.084 400 3.1 10.6 0.30

Numerical model of U.S.T. Using of an iterative method to optimize the friction coefficient of Coulomb by minimizing the gap between experimental and numeral data for each configuration.

m = 0,24

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Numerical post-treatments results Local contact variables extracted from numerical modelling for the sixth configuration:

• Contact pressure distribution, • Temperature gradient field, • Relative sliding velocity

• average contact pressure of 1 Gpa • average interfacial temperature of 880 K • average sliding velocity of 340 mm.s-1

Specimen Specimen

Specimen Contactor

1.5 GPa 1120 K

1185 K

heterogeneity

m = 0,24

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Implementation of the advanced frictional law in the developed numerical model of orthogonal cutting :

432

int1cc

gc

n Tvc ×××= sm

c1 c2 c3 c4 0.919 -0.251 -0.463 0.480

Improvement of predicted process variables

0,31

0,41

0,5

Contact lengths (mm)

µ constant Advanced law Experimental results

0

200

400

600

800

1000

Cutting force (N) Thrust force (N)

µ constant Advanced law Experimental results

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38

Ongoing activities Extrapolate the law for higher velocities • High speed tribometer developed by Tempo

Tool

Workpiece

Chip

Zone 1

Zone 2

Contactor (H13A)

Pin (C45)

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39

Integration of physical, rheological and microstructural phenomena in modelling of high speed machining: Most researches with Johnson-Cook model • Strain rates unsuitable for high speed machining

• No recrystallisation taken into account in the chip

Microstructural analysis chip

Development of sub-routine to

consider recrystallisation phenomenon in simulations

Lurdos’s law

Voce’s law

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Austempered Ductile Iron (ADI) Spheroidal graphite (SG) iron heat treated from its austenitic temperature

Manufacturing ADI components

40

Mechanical properties Lower Bainite 250 °C < Quench < 325 °C

Rm (MPa) 1400 – 1600

Re 0,2 (MPa) 960 - 980

A (%) 1 - 2

Usual spruing : after cooling

Automotive connecting rod

Surface degradation

The spruing operation is done before graphitization to save energy

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Experimental study Hot cutting test bench : LMPF Châlons en Champagne

41

Rake angles : -10°; 0°; +10°

Cutting speeds : 0.8; 1.3; 1.6 m/s

Isothermal work-holding device

Specimen SG iron (EN-GJS-700) Temperature : 1000°C

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Experimental study Hot cutting test bench : LMPF Châlons en Champagne

42

Rake angles : -10°; 0°; +10°

Cutting speeds : 0.8; 1.3; 1.6 m/s

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Recrystallization during experiments

43

Ductile behavior linked with dynamic recrystallization of the matrix

Brittle behavior explained by a dynamic recrystallization delay Assessment

• For low cutting speeds : hot deformation with local dynamic recrystallization Restoring deformability –> Ductile fracture • Higher cutting speed with negative rake angle Surface degradation –> Brittle fracture

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Numerical modelling Thermo-mechanical behavior of SG iron

44

Vc

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Strain rate study

45

Cutting speed (1.3 m/s) Width 3 mm Width 4 mm

250 °C 221 s-1 132 s-1

550 °C 208 s-1 103 s-1

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Ongoing activities Shear tests: compression on hat shaped specimens Split Hopkinson Pressure Bar (SPHB) at high temperature

46

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Scientific production Key figures 2009-2012

Peer reviewed papers

10

20

2009 2010 2011 2012

Conferences & workshops Books / chapters in book

10

20

2009 2010 2011 2012

44 40

Peer reviewed papers / year / researcher (1 year = 6 man months)

UMR 8201

Scientific production Key figures 2009-2012

PhD Thesis defended 7

HDR defended 2

HDR: French post-doctoral degree to supervise PhD Student

MOCELLIN K. (2011). from CEMEF, Sophia Antipolis, France New strategies to the numerical simulation of forming processes

KUBIAK K. (2012). from University of Leeds, UK Morphology of surfaces in solid-solid and solid-liquid dynamic interfaces and its influence on friction, wear and wettability

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Industrial partnerships Key figures 2009-2012

Ñ Bosch Ñ Agrati

(PSA, Volkswagen, BMW…) Ñ Auberts & Duval Ñ Setforge Ñ CETIM

Ñ Condat S.A. Ñ Fuchs Ñ Mobil Oil Ñ Sogelub

Ñ PSA Ñ Daimler Ñ SNECMA

Ñ APERAM (Arcelor-Mittal Steel)

Ñ Tata Steel Ñ Vallourec

Steel metallurgists

Lubricant manufacturers

Car & aerospace manufacturers

Car & aerospace subcontractors

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Examples of industrial transfer: Key figures 2009-2012

innovative rolling schedules; (increase of production of 20%)

lubricant selection methodology;

(ability to test new environmentally friendly lubricants for industrial application in cold/hot forging or rolling)

edge-trimming process optimization;

(new process adjustments to suppress the “saw tooth” defect)

new lubricant for glass forming. (development of a new lubricant to limit glass/mould sticking)

UMR 8201

Academics partnerships Key figures 2009-2012

CRIBC SIRRIS

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Focus on some scientific and/or socio-economics impacts

Key figures 2009-2012

Organisation of Friction and wear in material processing symposia of ESAFORM conferences since 2008 ICFG Permanent Member, corresponding member for France; Organiser of ICFG 46th plenary meeting in 2013 On-going application to CIRP.

Vice-Chairman of National Committee of Rolling; member of GDR Verres 3338; member of TC25 Glass Forming of the International Commission on Glass.

UMR 8201

Short term prospective: direct continuation of present studies

STRA

TEG

IC P

ROJE

CTS

RESEARCH THEMES THEME 1: Surfaces under extreme loading

THEME 2: Coupling materials / forming processes

SP1: Roughness and surface functionalities SP2: Cold forming & light weight design

SP3: High Speed Processes

SP4: Defectology at high temperature SP5: Glass Forming and Tempering

Tool life in cold heading of steel parts with white lubricants Study of white layers, wear by diffusion in High Speed machining

oxide layer fracture and roll defect in hot rolling

Effect of lubrication formulation on tribology

Roughness of material with temperature

Electrical and thermo-mechanical behaviour of CuNiSi alloys (railway app.) Hopkinson bars to characterise flow curves for High Speed Processes at high temperatures soft hardening associated with dynamic recrystallization of stress strain curves of steels

2D model for the tempering of a glass sheet with radiation

High precision measurement of hardness

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Middle & long term perspectives: Focus on the evolutions of the microstructure of material during forming and their effects on material behaviour.

new numerical developments • fluid/solid/thermic

interactions at asperity scale, • meshless method to

detect crack initiation, • computation of

damage.

Downscaling of analyses: • new testing benches to

access local data (stress, strains...)

• The possibility to test material within SEM

or tomograph will be investigated.

formulation of a super element, able to predict damage in surface vicinity, taking into account the microstructure evolution with thermal and mechanical loading history.

Experimental actions

Numerical actions

Final objective

UMR 8201

Thank you for your attention


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