32 APPENDIX A RESEARCH PLAN Title: CHARACTERIZATION OF Terminalia catappa (TALISAY) OIL FOR BIODIESEL PRODUCTION Objective: To produce a biodiesel, comparable to Coconut and Lumbang biodiesel. MONTH ACTIVITY REMARKS JUNE Proposing and Approval of research title(s) Accomplished Looking for a consultant Accomplished Data gathering Accomplished JULY Dealing with the consultant Accomplished Making the letter request Accomplished Making Chapter I Accomplished AUGUST Meeting with the consultant Accomplished Preparing the raw materials Accomplished SEPTEMBER Revision of Chapter I Accomplished Making Chapter II Accomplished OCTOBER Extraction of oil Accomplished NOVEMBER Testing the properties of oil Accomplished DECEMBER Making the product Accomplished Revision of Chapter I and II Accomplished JANUARY Testing the properties of the Talisay, Coconut and Lumbang biodiesel Accomplished Making Chapter III and IV Accomplished Compilations of all the chapters Accomplished Editing the research papers Accomplished FEBRUARY Making the tarpaulin Accomplished Making the PowerPoint presentation Accomplished Science Congress Accomplished Doing some revisions and Testing the Product in the Engine Accomplished MARCH Revision of Papers and Bookbinding Accomplished Submission of research papers Accomplished RALPH ANGELO B. BISAIN Proponent LERIDA B. BISAIN Mother
Transcript
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APPENDIX A
RESEARCH PLAN
Title: CHARACTERIZATION OF Terminalia catappa (TALISAY) OIL FOR BIODIESEL PRODUCTION
Objective: To produce a biodiesel, comparable to Coconut and Lumbang biodiesel.
MONTH ACTIVITY REMARKS
JUNE
Proposing and Approval of research title(s) Accomplished
Looking for a consultant Accomplished
Data gathering Accomplished
JULY
Dealing with the consultant Accomplished
Making the letter request Accomplished
Making Chapter I Accomplished
AUGUST
Meeting with the consultant Accomplished
Preparing the raw materials Accomplished
SEPTEMBER
Revision of Chapter I Accomplished
Making Chapter II Accomplished
OCTOBER Extraction of oil Accomplished
NOVEMBER Testing the properties of oil Accomplished
DECEMBER
Making the product Accomplished
Revision of Chapter I and II Accomplished
JANUARY
Testing the properties of the Talisay, Coconut and Lumbang biodiesel Accomplished
Making Chapter III and IV Accomplished
Compilations of all the chapters Accomplished
Editing the research papers Accomplished
FEBRUARY
Making the tarpaulin Accomplished
Making the PowerPoint presentation Accomplished
Science Congress AccomplishedDoing some revisions and Testing the Product in the Engine Accomplished
MARCH
Revision of Papers and Bookbinding Accomplished
Submission of research papers Accomplished
RALPH ANGELO B. BISAIN Proponent
LERIDA B. BISAIN Mother
JACQUELINE T. URETA Research adviser
ESTRELLITA M. DE VERA Principal III
APPENDIX B
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CHARTS
Flow Chart
The chart indicates the summarized the procedures regarding the study.
Gathering Terminalia catappa
kernels as raw materials
Extraction of Oil
Characterization of Oil
Biodiesel Production
Comparing the Properties of Talisay,
Coconut and Lumbang Biodiesel
Testing the Biodiesel in the Engine
Gantt Chart
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Title: CHARACTERIZATION OF Terminalia catappa (TALISAY) OIL FOR BIODIESEL PRODUCTION
Objective: To produce a biodiesel, comparable to Coconut and Lumbang biodiesel.
ActivitiesMonth
June July August September October November December January February MarchProposing and Approval of research title(s)
Looking for a consultant Data gathering Dealing with the consultant Making the letter request Making Chapter I Meeting with the consultant Preparing the raw materials Revision of Chapter I Making Chapter II Extraction of oil Testing the properties of oil Making the product Revision of Chapter I and II Testing the properties of the Talisay, Coconut
and Lumbang biodiesel Making Chapter III and IV Compilations of all the chapters Editing the research papers Making the tarpaulin Making the PowerPoint presentation Science Congress Doing some revisions and Testing the Product in the Engine, Revision of
Papers and Bookbinding Submission of research papers
RALPH ANGELO B. BISAIN Proponent
LERIDA B. BISAIN Mother
JACQUELINE T. URETA Research adviser
ESTRELLITA M. DE VERA
Principal III
Graphs
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Sap. Number
170 175 180 185 190 195
Sample 3
Sample 2
Sample 1
Graph A. Saponification Number of the Three Samples
FFA Number
28.7 28.8 28.9 29 29.1 29.2 29.3 29.4 29.5 29.6
Sample 3
Sample 2
Sample 1
Graph B. Free Fatty Acid Number of the Three Samples
Specific Gravity
0.835 0.84 0.845 0.85 0.855 0.86 0.865 0.87 0.875
Sample 3
Sample 2
Sample 1
Graph C. Specific Gravity of the Three Samples
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Viscosity
21.5 22 22.5 23 23.5 24
Sample 10
Sample 9
Sample 8
Sample 7
Sample 6
Sample 5
Sample 4
Sample 3
Sample 2
Sample 1
Graph D. Viscosity of the Ten Samples
Peroxide Value
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
Sample 2
Sample 1
Graph E. Peroxide Value of the Two Samples
Talisay
Coconut
Lumbang
0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6
Trial 3
Trial 2
Trial 1
Graph F. Volatility of Talisay, Coconut and Lumbang Biodiesel
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APPENDIX C
PHOTOGRAPHS
Terminalia catappa (Talisay) Tree(Photo taken from: http://www.agroforestry.net/tti/T.catappa-tropical-almond.pdf)
Terminalia catappa (Talisay) Seeds(Photo taken from: http://www.agroforestry.net/tti/T.catappa-tropical-almond.pdf)
Terminalia catappa (Talisay) Mature Seeds(Photo taken by: Ralph Angelo B. Bisain)
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Talisay Seed Kernels Meeting with the Consultant (Photo taken by R. A. Bisain) (Photo taken by: R. A. Bisain)
Collecting Talisay Seed Potassium Hydroxide (Photo taken by: R. A. Bisain) (Photo taken by: R. A. Bisain)
Oil Extraction Potassium Iodide (Photo taken by: R. A. Bisain) (Photo taken by: R. A. Bisain)
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Extracted Oil Chloroform (Photo taken by: R. A. Bisain) (Photo taken by: R. A. Bisain)
Saturated Sodium Chloride Sodium Thiosulfate (Photo taken by: R. A. Bisain) (Photo taken by: R. A. Bisain)
Phenolphthalein Hydrochloric Acid
(Photo taken by: R. A. Bisain) (Photo taken by: R. A. Bisain)
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Saponification Number Test Viscosity Test (Photo taken by: R. A. Bisain) (Photo taken by: R. A. Bisain)
Specific Gravity Test Free Fatty Acid Number Test (Photo taken by: R. A. Bisain) (Photo taken by: R. A. Bisain)
Peroxide Value Test Biodiesel Production (Photo taken by: R. A. Bisain) (Photo taken by: R. A. Bisain)
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Combustibility Test Recording the Data
(Photo taken by: R. A. Bisain) (Photo taken by: N. Panlilio)
Putting the B2 Combination (0.5L) Engine Testing (Photo taken by: R. A. Bisain) (Photo taken by: R. A. Bisain)
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APPENDIX D
LETTERS
Excuse letters
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Letter of Request for the Consultant
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Endorsement Letter
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Recommendation Slip
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APPENDIX E
STATISTICAL ANALYSIS
Analysis of Variance
Mean Variance
Talisay 1.49 1.54 1.51 1.51 0.00063
Coconut 1.02 1.08 1.10 1.10 0.0074
Lumbang 0.39 0.49 0.43 0.43 0.003
1. Ho: The volatility of the three biodiesel is the same.
Hi: There is one better biodiesel.
2. dfN : 3-1 = 2
dfD : 9-3 = 6
3. GM : 1.01
4. SST : 1.83
5. SSE : 0.0022
6. SSB : SST – SSE = 1.81
7. CV= 5.14
Sources of Variance Degree of Freedom Sum of SquaresMean Square or the
VarianceF
Between 2 1.81 0.905 245
Error 6 0.022 0.0037
Total 8 1.83
F > CV, 245 > 5.14
TUKEY ANALYSIS:
a. For Talisay biodiesel vs Coconut biodiesel
q= 11.16
b. For Talisay biodiesel vs Lumbang biodiesel
q= 30. 75
c. For coconut biodiesel vs Lumbang biodiesel
q= 19.09
d. CV= 3.46
e. 11.67 > 3.46 - significant
30.47 > 3.46 - significant
19.09 > 3.46 - significant
Conclusion: Therefore, there is a significant difference on the volatility of Talisay Coconut, Lumbang biodiesel. Talisay biodiesel is the best
among the three biodiesel. Based from the analysis of variance, results shows that Talisay values are greater than the critical value.
