Separation Processes Lab Report

8/17/2019 Separation Processes Lab Report

http://slidepdf.com/reader/full/separation-processes-lab-report 1/15

SUBMITTED TO: Sir RizwanAli

SUBMITTED BY: 2013-CH-50 2013-CH-52 2013-CH-78 2013-CH-80 2013-CH-!

SeparationProcesses



LAB LAYOUT



LIST OF EQUIPMENT

1" I#n E$%&an'( A))ara*+,

2" a,(#+, Di.+,i#n A))ara*+,

3" Ol/ Di,*illa*i#n C#l+n

!" C#n*in+#+, Di,*illa*i#n %#l+n

5" Ba*%& Di,*illa*i#n C#l+n

" i+i/4i+i/ E$*ra%*i#n Uni*

7" a,4i+i/ E$*ra%*i#n Uni*

8" Tra Dri(r

" 6l+i/ B(/ Dri(r



EQUIPMENT DETAILS

CONTINUOUS DISTILLATION COLUMN

C#n*in+#+, /i,*illa*i#n %#l+n i, +,(/ *# /(#n,*ra*( *&( w#rin' # a

%#n*in+#+, /i,*illa*i#n9 I* i, al,# +,(/ *# )(r#r az(#*r#)i% /i,*illa*i#n9

BATCH DISTILLATION COLUMN

Siilarl *&( a*%& /i,*illa*i#n %#l+n in %#n,*r+%*i#n ;wi*& *&( ($%()*i#n #

r(#il(r"< i, +,(/ *# /(#n,*ra*( *&( a*%& /i,*illa*i#n )r#%(,, a* %#n,*an*

r(=+$ ra*i# an/ a* %#n,*an* )r#/+%* %#)#,i*i#n9 T&( (.(%* # )r#%(,,

>arial(,;li( r(=+$ ra*i#" ar( al,# ,*+/i(/9

LIQUID/LIQUID EXTRACTION COLUMN

?a%(/ %#l+n #r li+i/< li+i/ ($*ra%*i#n i, +,(/ #r %al%+la*i#n #

%#(@%i(n* # /i,*ri+*i#n #r li+i/-li+i/ ($*ra%*i#n9 6ir,* # all *&( ,#l+*( i,

($*ra%*(/ r# *&( ((/ +,in' an a))r#)ria*( ,#l>(n*9 T&(n #r ,()ara*i#n

/i,*illa*i#n ,,*( i, (+i))(/ wi*& %#l+n9

GAS/LIQUID ABSORPTION COLUMN

T&( a,#r)*i#n %#l+n i, +,(/ *# /(#n,*ra*( *&( )r#l(, # )a%(/

%#l+n ,+%& a, =##/in'< %&ann(lin' an/ (n*rain(n*9 ( %an al,# (a,+r(

*&( %&(i-,#r)*i#n (+iliri+ +,in' a 'ra>i(*ri% anal,i,9

GASEOUS DIFFUSION APPARATUS

T&i, a))ara*+, i, +,(/ *# (a,+r( *&( /i.+,i>i* # a >#la*il( %#)#n(n* a* a%#n*r#ll(/ *()(ra*+r(9

TRAY DRIER



Tr /ri(r i, +,(/ #r *&( ,*+/ # /ri(r an/ +n/(r,*an/ *&( *&(#r(*i%al

+n/a(n*al, li( /rin' %+r>(< (.(%* # *()(ra*+r( an/ air >(l#%i* #n *&(

/rin' ra*(< (*%9

FLUID BED DRIER

T&( ($)#,(/ ,+ra%( # w(* )ar*i%l(, %an ( 'r(a*l (n&an%(/ =+i/izin'

*&( ,#li/ )ar*i%l(,< *&(r(#r( *&( ra*( # /rin' in%r(a,(, ,i'ni%an*l9 T&i,

la-,%al( (+i)(n* i, +,(/ *# /(#n,*ra*( *&( =+i/ (/ /rin' )rin%i)l(9

ION-EXCHANGE APPARATUS

a*(r ,#*(nin' an/ ,(>(ral #*&(r in/+,*rial #)(ra*i#n, a( +,( # *&( i#n

($%&an'( )r#%(,,9 T&( a))ara*+, i, +,(/ #r*&( /(#n,*ra*i#n # %a*i#ni%an/ ani#ni% r(,in, #r *&i, )+r)#,(< *# (a,+r( *&( ($%&an'( %a)a%i*<

n#ral #)(ra*i#n an/ r('(n(ra*i#n # *&( i#n-($%&an'( ,,*(9



SAFETY RULES

• 6#ll#w all *&( in,*r+%*i#n, %ar(+ll9 I #+ /# n#* +n/(r,*an/ a

/ir(%*i#n #r )ar* # a )r#%(/+r(< a, #+r *(a%&(r (#r( )r#%((/in'

wi*& *&(

• Man+al ,&#+l/ ( r(a/ (#r( *ain' an r(a/in' ;#r ,*()" in *&(

la#ra*#r

• D# n#* w#r al#n( in *&( la#ra*#r9 Alwa, +n/(r,*an/ *&( *(a%&(r,

in,*r+%*i#n r,* *&(n ,*ar* #+r ($)(ri(n*

• Una+*&#riz(/ ($)(ri(n*, ar( n#* all#w(/9 ?(r#r #nl *&#,(

($)(ri(n*, a+*&#riz(/ #+r *(a%&(r

•

D# n#* *#+%& an (+i)(n*< %&(i%al,< #r #*&(r a*(rial, in *&(la#ra*#r ar(a +n*il #+ ar( in,*r+%*(/ *# /# ,#

• D# n#* (a* #r /rin an*&in' in *&( la#ra*#r

• Alwa, w#r in a w(ll->(n*ila*(/ ar(a

• #r ar(a, ,&#+l/ ( ()* %l(an an/ *i/ a* all *i(,9

• E+i)(n* # la ar( >(r ($)(n,i>(< ,# *&( ,&#+l/ ( &an/l( wi*&

'r(a* %ar( an/ +,* ( +,(/ +n/(r *&( ,+)(r>i,i#n # *(a%&(r #r in

)r(,(n%( # la a**(n/an*

• SO?, # *&( (+i)(n* +,* ( #ll#w(/



THEORY OF DISTILLATION

Di,*illa*i#n i, #n( # *&( #,* %##n li+i/-li+i/ ,()ara*i#n )r#%(,,(,< an/%an ( %arri(/ #+* in a %#n*in+#+, #r a*%& ,,*(9

Di,*illa*i#n w#r, *&( a))li%a*i#n an/ r(#>al # &(a* *# ($)l#i*

/i.(r(n%(, in r(la*i>( >#la*ili*9 T&( &(a* %a+,(, %#)#n(n*, wi*& l#w(r

#ilin' )#in*, an/ &i'&(r >#la*ili* *# ( >a)#riz(/< l(a>in' l(,, >#la*il(

%#)#n(n*, a, li+i/,9 Mi$*+r(, wi*& &i'& r(la*i>( >#la*ili*i(, ar( (a,i(r *#

,()ara*(9 T&i, a(, ,()ara*i#n, # %l#,(-#ilin' an/ az(#*r#)i% ((/,

/i@%+l*< ,# ,)(%ial /i,*illa*i#n *(%&ni+(, &a>( *# ( +,(/ *# ,()ara*( *&(,(

i$*+r(,9

Di,*illa*i#n %an ( +,(/ *# ,()ara*( inar #r +l*i-%#)#n(n* i$*+r(,9

Man >arial(,< ,+%& a, %#l+n )r(,,+r(< *()(ra*+r(< ,iz(< an/ /ia(*(r

ar( /(*(rin(/ *&( )r#)(r*i(, # *&( ((/ an/ *&( /(,ir(/ )r#/+%*,9 S#(

,)(%ializ(/ %#l+n, )(r#r #*&(r +n%*i#n,< ,+%& a, r(a%*i>( /i,*illa*i#n

%#l+n,< w&i%& %#in( r(a%*i#n an/ ,()ara*i#n # )r#/+%*, in*# a ,in'l(

+ni*9

T&( ((/ (n*(r, a )la*( %#l+n *#war/, *&( i//l( # *&( %#l+n9

C#n%(n*ra*i#n /i.(r(n%(, %a+,( *&( l(,, >#la*il( %#)#n(n*, *# *ran,(r

r# *&( >a)#r ,*r(a *# *&( li+i/ ,*r(a9 T&( >a)#r ($i*in' *&( %#n/(n,(r

%#n*ain, *&( #,* >#la*il( %#)#n(n*,< w&il( *&( l(a,* >#la*il( %#)#n(n*,

($i* *&r#+'& *&( r(#il(r in *&( li+i/ ,*r(a9

SIEVE PLATE

T&( )la*( #r *ra %#l+n i, *&( #,* wi/(l +,(/ *)( # /i,*illa*i#n %#l+n9

T&( n+(r # *ra, #r ,*a'(, in *&( %#l+n i, /()(n/(n* #n *&( /(,ir(/

)+ri* an/ /i@%+l* # ,()ara*i#n9 T&( n+(r # ,*a'(, al,# /(*(rin(, *&(

&(i'&* # *&( %#l+n9 In *&( la#ra*#r 8 )la*(, ar( +,(/9

APPLICATIONS

T&( a))li%a*i#n # /i,*illa*i#n %an r#+'&l ( /i>i/(/ in #+r 'r#+),:

la#ra*#r ,%al(< in/+,*rial /i,*illa*i#n< /i,*illa*i#n # &(r, #r )(r+(r an/

(/i%inal ;&(ral /i,*illa*(" an/ ##/ )r#%(,,in'9 T&( la**(r *w# ar( /i,*in%*

r# *&( #r(r *w#< in *&a* in *&( /i,*illa*i#n i, n#* +,(/ a, a *r+(



)+ri%a*i#n (*&#/< +* #r( *# *ran,(r all >#la*il(, r# *&( ,#+r%(

a*(rial, *# *&( /i,*illa*(9

T&( ain /i.(r(n%( (*w((n la#ra*#r ,%al( /i,*illa*i#n an/ in/+,*rial

/i,*illa*i#n i, *&a* la#ra*#r ,%al( /i,*illa*i#n i, #*(n )(r#r(/ a*%&-wi,(<

w&(r(a, in/+,*rial /i,*illa*i#n #*(n #%%+r, %#n*in+#+,l9 In a*%& /i,*illa*i#n<

*&( %#)#,i*i#n # *&( ,#+r%( a*(rial< *&( >a)#r, # *&( /i,*illin'

%#)#+n/, an/ *&( /i,*illa*( %&an'( /+rin' *&( /i,*illa*i#n9 In a*%&

/i,*illa*i#n< a ,*ill i, %&ar'(/ ;,+))li(/" wi*& a a*%& # ((/ i$*+r(< w&i%& i,

*&(n ,()ara*(/ in*# i*, %#)#n(n* ra%*i#n, w&i%& ar( %#ll(%*(/ ,(+(n*iall

r# #,* >#la*il( *# l(,, >#la*il(< wi*& *&( #**#, ;r(ainin' l(a,* #r n#n-

>#la*il( ra%*i#n" r(#>(/ a* *&( (n/9 T&( ,*ill %an *&(n ( r(%&ar'(/ an/ *&(

)r#%(,, r()(a*(/9

In %#n*in+#+, /i,*illa*i#n< *&( ,#+r%( a*(rial,< >a)#r, an/ /i,*illa*( ar( ()*

a* a %#n,*an* %#)#,i*i#n %ar(+ll r()l(ni,&in' *&( ,#+r%( a*(rial an/

r(#>in' ra%*i#n, r# #*& >a)#r an/ li+i/ in *&( ,,*(9 T&i, r(,+l*, in a

(**(r %#n*r#l # *&( ,()ara*i#n )r#%(,,9



EXPERIMENT NO: 1

OBJECTIVE

U,( # *&( r(ra%*#(*(r *# /(*(rin( i$*+r( %#)#,i*i#n,9

EQUIPMENT SETUP

T&r#+'&#+* *&( ($)(ri(n*al )r#%(/+r(, %arri(/ #+* #n *&( C#n*in+#+,

Di,*illa*i#n C#l+n< i* I (,,(n*ial *# &a>( %#n>(ni(n* +i% (*&#/ #

/(*(rinin' *&( %#)#,i*i#n # *&( inar i$*+r( *a(n r# *&( >ari#+,

,a)l(, #n *&( (+i)(n*9 S+%& a (*&#/ in>#l>(, *&( +,( # r(ra%*#(*(r9

Sin%( *&( r(ra%*i>( in/($ # *&(,( i$*+r(, >ari(, wi*& %#)#,i*i#n,9 T&(

#nl (+i)(n* n((/(/ in a//i*i#n *# *&( &an/ &(l/ r(ra%*#(*(r i, a

(a,+rin' %lin/(r 0-100 l< a ,+i*al( %#n*ain(r *# i$ *&( ,a)l( in a

#**l( # (a%& # *&( )+r( %#)#n(n* # *&( inar i$*+r( *# analz(9

SUMMARY OF THEORY

6#r *&( ,,*(< wa*(r4(*&an#l i$*+r(< # *&( n#wn %#n%(n*ra*i#n %an (

a/( +) an/ *&(ir r(ra%*i>( in/($(, %an ( (a,+r(/9 T&( r(ra%*#(*(r

(a,+r(, *&( %ri*i%al an'l( # *&( li+i/ +n/(r *(,* an/ (a%& %#n%(n*ra*i#n

will ,&#w a /i.(r(n* %ri*i%al an'l(9

Cri*i%al An'l(

B(#n/ *&( %ri*i%al an'l( i, /arn(,, an/ r(ra%*#(*(r ar( %alira*(/ al#n'

*&i, li'&*4/ar #+n/ar9

PROCEDURE

M(a,+r( *&( r(ra%*i>( in/($ ;RI" # )+r( wa*(r an/ )+r( (*&an#l9

6#r 25 #l( )(r%(n* (*&an#l i9(9 75 #l( )(r%(n* wa*(r9

M#l(%+lar w(i'&* # wa*(r 18

M#l(%+lar w(i'&* # (*&an#l !

D(n,i* # wa*(r 1 '4

D(n,i* # (*&an#l 0978 '4

6#r %al%+la*i#n )+r)#,(,<



C&(i%al E E*&an#l

C&(i%al a*(r

A*(r ,i)liin'< *&( nal ($)r(,,i#n i,<

F#l+( ;T#*al" 3 G 092 G F#l+( ;E*&an#l"F#l+( ;T#*al" 198 G F#l+( ;E*&an#l" T&+, #r 100 # i$*+r(< +an*i*i(, r(+ir(/ will (Ethanol = 53.76

Water = 46.24



EXPERIMENT NO: 2

OBJECTIVE

T# ,*+/ *&( )r(,,+r( /r#) a%r#,, *&( %#l+n a'ain,* >ari#+, #il-+) ra*(,

THEORY

T&( )r(,,+r( /r#) a%r#,, *&( %#l+n i, *&( ,+ # *&( r(,i,*an%( #.(r(/ *#

*&( >a)#r, *&( ,i(>(, *ra an/ *&( r(,i,*an%( #.(r(/ *&( li+i/, *# *&(

>a)#r, *# )a,, *&r#+'& *&(9

T&( >a)#r >(l#%i* i, /ir(%*l r(la*(/ *# *&( )r(,,+r( /r#)9 A, *&( >(l#%i* i,in%r(a,(/< )r(,,+r( /r#) a%r#,, *&( %#l+n in%r(a,(,9 Fa)#r >(l#%i* i,

%#n*r#ll(/ *&( )#w(r in)+* *# *&( #il(r ,# a, *&( )#w(r in)+* in%r(a,(,

>a)#r >(l#%i* in%r(a,(,9 T&+, in%r(a,in' *&( #il +) ra*( will in%r(a,( *&(

)r(,,+r( /r#) a%r#,, *&( %#l+n

&(n n# li+i/ i, )r(,(n* *&(,( ,i(>( (&a>(, a, #ri%( an/ )r(,,+r( /r#) i,

/ir(%*l )r#)#r*i#nal *# ,+ar( # >(l#%i*9 &(n li+i/ i, )r(,(n* *&( >a)#r,

&a>( *# #>(r%#( *&( li+i/ &(a/9 S# *&( r(la*i#n will %&an'(9 in *&( l#'-l#'

'ra)& # )r(,,+r( /r#) a'ain,* #il-+) ra*(, r,* i* will ( %#n,*an* an/ *&(n

a*(r #ain' a lar'( )r(,,+r( /r#) will ($i,*9 A ,all %&an'( in #il-+) ra*(will %a+,( lar'( )r(,,+r( /r#)9

EQUIPMENT SET-UP

T&( (+i)(n* will ( ,(*+) *# #)(ra*( a* *#*al r(=+$9 All >a)#r will (

%#n/(n,(/ *# li+i/ an/ r(*+rn *# %#l+n9 # *#) #r #**# )r#/+%* will (

#*ain(/ an/ ((/ i, #n%( %&ar'(/ in *&( r(#il(r *&r#+'& *&( ll(r %a)9 T#

%al%+la*( *&( #il-+) ra*(, a (a,+rin' %lin/(r an/ ,*#) wa*%& i, al,#

r(+ir(/9

PROCEDURE

B(#r( ,*ar*in' *&( ($)(ri(n* %l#,( all *&( >al>(, ($%()* F10 #r *&( r(=+$9

O)(n *&( ll(r %a) # *&( #il(r an/ ll 10 li*(r, # *&( ,#l+*i#n in #il(r an/

%l#,( *&( #il(r ll(r %a) )r#)(rl9 #w #)(n *&( wa*(r >al>( #r *&(



%#n/(n,(r F59 #w ,(* *&( *()(ra*+r( n# #n T ,&#win' *&(

*()(ra*+r( # *&( r(#il(r #n *&( %#n*r#ll(r ,%r((n9 T&(n *+rn #n *&( #il(r

an/ ,(* *&( )#w(r *# 0975 9 T&( #il(r will ,*ar* *# &(a* +) *&( li+i/9 O)(n

*&( >al>(, # *&( %#l+n %#nn(%*(/ *# *&( an#(*(r< F F79 Ini*iall

*&(r( will ( n# )r(,,+r( /i.(r(n%( ,# *&(r( will ( n# r(a/in',9 Cl#,( *&(

>al>(,9

A*(r ,#(*i( *() # *&( %#l+n will ,*ar* in%r(a,in' an/ >a)#r will #>(

+) *# *&( %#n/(n,(r9 A*(r %#n/(n,(r li+i/ will #>( in *&( /i,*illa*( >(,,(l

an/ #>( in *&( >al>( ;w&i%& i, ,wi*%&(/ #."9 #w a, w( ar( #)(ra*in' *&(

%#l+n #n *#*al r(=+$ ,# all *&( li+i/ will #>( a% *# *&( %#l+n9 T&i,

>al>( i, ,wi*%&(/ #n r# *&( %#n*r#ll(r9

T&( li+i/ will *&(n %a,%a/( /#wn #rin' a l(>(l #n *&( *ra,9 B+l(, will

)a,, *&r#+'& *&( li+i/ an/ *&( ,,*( will a%&i(>( an (+iliri+ )#,i*i#n

w&(n *&( *()(ra*+r( #n *&( *ra, i9(9 r# T1 *# T8 (%#(, %#n,*an*9

T# %al%+la*( *&( #il +) ra*( >al>( F3 i, #)(n(/ an/ ,a)l( i, *a(n in a

(a,+rin' %lin/(r an/ *&( *i( i, r(%#r/(/9 On( )r(%a+*i#n i, >(r

i)#r*an* w&il( (a,+rin' *&( #il +) ra*(9 B(#r( ,*ar*in' *# %#ll(%* in a

(a,+rin' %lin/(r< li+i/ r# *&( )i)( ,&#+l/ ( )#+r(/ in ,()ara*( =a,

an/ w&(n li+i/ i, =#win' ,*(a/il in *&( )i)(< *&( (a,+r( *&( #il +) ra*(

;li+i/ in (a,+rin' %lin/(r in a r(%#r/(/ *i("9

A*(r %al%+la*in' *&( #il +) ra*( )r(,,+r( /r#) i, %al%+la*(/ #)(n #*& *&(

>al>(, F F79 I* +,* ( ()* in in/ *&a* F ,&#+l/ ( #)(n(/ r,* *&(n

F7 an/ w&il( %l#,in' *&( >al>(, a*(r (a,+rin' *&( )r(,,+r( /r#) F +,*

( %l#,(/ r,* an/ *&(n F79 T&i, #r/(r i, #ll#w(/ *# )r(>(n* *&( >a)#r,

(n*(rin' in*# *&( an#(*(r r# %#l+n9 R()(a* *&( r(a/in' +n*il *w# in a

r#w ar( airl %l#,(9

R()(a* *&( ,a( )r#%(/+r( #r /i.(r(n* #il +) ra*(,9 i>( a *i( # 5-10

in+*(, *# a%&i(>( ,*(a/ ,*a*( in *&( %#l+n9 U,in' an in%r((n* # 250

wa** *a( r(a/in', +) *# 1959



EXPERIMENT NO: 03

OBJECTIVE

T# /(*(rin( #>(rall (@%i(n% # %#l+n a* >arin' #il-+) ra*(,

THEORY

T# %al%+la*( *&(#r(*i%al n+(r # )la*(, #r a 'i>(n ,()ara*i#n a* *#*al r(=+$

FENSKE’S METHOD

nJ1 4 l#'KLLa>&(r( n +(r # *&(#r(*i%al )la*(,$a #l( ra%*i#n # #r( >#la*il( %#)#n(n*$ #l( ra%*i#n # l(a,* >#la*il( %#)#n(n*aa> a>(ra'( r(la*i>( >#la*ili*

S+,%ri)*, D an/ B r()r(,(n*, /i,*illa*( an/ #**# r(,)(%*i>(l

LN KL9L/

T&( (@%i(n% i, 'i>(n

E P 1OO Q

n#win' *&( %#)#,i*i#n # /i,*illa*( an/ #**# an/ *&( %#rr(,)#n/in'

>#la*ili*i(,< *&( %#l+n (@%i(n% %an ( (a,il /(*(rin(/9

EQUIPMENT SETUP



T&( (+i)(n* i, ,(*+) *# #)(ra*( a* *&( *#*al r(=+$ ,# *&( %&ar'( # *&(

((/ i$*+r( %an ( /ir(%*l l#a/(/ in *&( r(#il(r *&( ((/ %a) )r#>i/(/

wi*&#+* r,* %&ar'in' # *&( ((/ *an,9 A* *#*al r(=+$ *&(r( will ( n# ((/ #r

*#) )r#/+%* #r #**# )r#/+%*,9

Ma( 1O li*(r, # *&( i$*+r( # wa*(r an/ (*&an#l wi*& 5OQ #l( )(r%(n* # #*&9 R(+ir(/ >#l+(, #r *&( i$*+r( ar(

a*(r !98 li*(r,

E*&an#l 5911 li*(r,

( al,# r(+ir(

• 25O M (a,+rin' %lin/(r

• S*#) wa*%&

• Han/ &(l/ r(ra%*#r

PROCEDURE

S*ar* *&( a))ara*+, an/ ll *&( r(#il(r wi*& 1O li*(r, # *&( i$*+r(9 S(* *&(

&(a* %#n*r#ll(r &i'& a* r,*< *&(n r(/+%( *&( &(a* a, r(=+$ i, in*r#/+%(/ *#

'i>( ,*(a/ +lin' a* all *ra an/ *#*al r(=+$9 (a>( *&( ,,*( #r a* l(a,*

3O in+*(, ,# *&a* ,,*( %an r(a%& a* *&( (+iliri+ ,*a*(9

M(a,+r( *&( #il +) ra*( a, /(,%ri(/ in ($)(ri(n* A +,in' >al>( F39 D#

*&i, *&r(( *i(, an/ +,( an a>(ra'( >al+(,9 Ta( a ,a)l( # *&( #>(r&(a/,

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Separation Processes Lab Report

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