Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
250 W US Highway 12
Burns Harbor, IN 46304-9745 Work Order No.:
September 10, 2019
Re:
Arcelor Mittal USA, Inc.
19I0103
Daily
Dear Teri Kirk:
Microbac Laboratories, Inc. - Chicagoland Division received 23 sample(s) on 9/4/2019
10:10:00AM for the analyses presented in the following report as Work Order
19I0103.
The enclosed results were obtained from and are applicable to the sample(s) as
received at the laboratory. All sample results are reported on an "as received" basis
unless otherwise noted.
All data included in this report have been reviewed and meet the applicable project
specific and certification specific requirements, unless otherwise noted. A
qualifications page is included in this report and lists the programs under which
Microbac maintains certification.
This report has been paginated in its entirety and shall not be reproduced except in
full, without the written approval of Microbac Laboratories.
Carey Gadzala
Project Manager
We appreciate the opportunity to service your analytical needs. If you have any
questions, please contact your project manager. For any feedback, please contact
Ron Misiunas, Division Manager, at [email protected].
Sincerely,
Microbac Laboratories, Inc.
Page 1 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
WORK ORDER SAMPLE SUMMARY Date: Tuesday, September 10, 2019
Client:
Project:
Lab Order:
Daily
Arcelor Mittal USA, Inc.
19I0103
Lab Sample ID Date ReceivedCollection DateTag NumberClient Sample ID
9/4/2019 10:10:00AM09/03/2019 06:10011011-Composite19I0103-01
9/4/2019 10:10:00AM09/03/2019 06:10011011-Grab19I0103-02
9/4/2019 10:10:00AM09/03/2019 06:25001001-Composite19I0103-03
9/4/2019 10:10:00AM09/03/2019 06:25001001-Grab19I0103-04
9/4/2019 10:10:00AM09/04/2019 06:46031031-Grab19I0103-05
9/4/2019 10:10:00AM09/04/2019 06:50Mixed LiquorMixed Liquor-Grab19I0103-06
9/4/2019 10:10:00AM09/04/2019 06:40J-BoxJ-Box-Grab19I0103-07
9/4/2019 10:10:00AM09/04/2019 07:00WWIIWWII-Grab19I0103-08
9/4/2019 10:10:00AM09/04/2019 07:40ColdwellColdwell-Grab19I0103-09
9/4/2019 10:10:00AM09/04/2019 07:50RSB FT OverflowRSB FT Overflow-Grab19I0103-10
9/4/2019 10:10:00AM09/04/2019 07:49RSB FT InfluentRSB FT Influent-Grab19I0103-11
9/4/2019 10:10:00AM09/02/2019 08:20WPLWPL-Grab19I0103-12
9/4/2019 10:10:00AM09/04/2019 08:27999999-Grab19I0103-13
9/4/2019 10:10:00AM09/04/2019 08:10BFTCBFTC-Grab19I0103-14
9/4/2019 10:10:00AM09/03/2019 08:15002002-Composite19I0103-15
9/4/2019 10:10:00AM09/03/2019 08:15002002-Grab19I0103-16
9/4/2019 10:10:00AM09/03/2019 08:00WALWAL-Grab19I0103-17
9/4/2019 10:10:00AM09/04/2019 00:00CM1CM1-Grab19I0103-19
9/4/2019 10:10:00AM09/04/2019 00:00CM2CM2-Grab19I0103-20
9/4/2019 10:10:00AM09/04/2019 00:00CM6CM6 Grab19I0103-21
9/4/2019 10:10:00AM09/04/2019 00:00HM2HM2-Grab19I0103-22
9/4/2019 10:10:00AM09/04/2019 00:00HM3HM3-Grab19I0103-23
Page 2 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Field Results Date: Tuesday, September 10, 2019
Client:
Client Project: Daily
Arcelor Mittal USA, Inc. 19I0103Work Order:
Client Sample ID:
Matrix:
Sample Description:
011-Grab
Aqueous
Sampled:
Received:
Analyses Result Units
19I0103-02Work Order/ID:
09/03/2019 06:10
09/04/2019 10:10
011
FLD_CL_TITR 0.00 mg/L
pH 7.8 pH Units
Client Sample ID:
Matrix:
Sample Description:
001-Grab
Aqueous
Sampled:
Received:
Analyses Result Units
19I0103-04Work Order/ID:
09/03/2019 06:25
09/04/2019 10:10
001
FLD_CL_TITR 0.00 mg/L
pH 7.8 pH Units
Client Sample ID:
Matrix:
Sample Description:
J-Box-Grab
Aqueous
Sampled:
Received:
Analyses Result Units
19I0103-07Work Order/ID:
09/04/2019 06:40
09/04/2019 10:10
J-Box
pH 8.3 pH Units
Client Sample ID:
Matrix:
Sample Description:
RSB FT Overflow-Grab
Aqueous
Sampled:
Received:
Analyses Result Units
19I0103-10Work Order/ID:
09/04/2019 07:50
09/04/2019 10:10
RSB FT Overflow
pH 9.0 pH Units
Client Sample ID:
Matrix:
Sample Description:
999-Grab
Aqueous
Sampled:
Received:
Analyses Result Units
19I0103-13Work Order/ID:
09/04/2019 08:27
09/04/2019 10:10
999
pH 8.0 pH Units
Client Sample ID:
Matrix:
Sample Description:
002-Grab
Aqueous
Sampled:
Received:
Analyses Result Units
19I0103-16Work Order/ID:
09/03/2019 08:15
09/04/2019 10:10
002
pH 8.2 pH Units
Client Sample ID:
Matrix:
Sample Description:
WAL-Grab
Aqueous
Sampled:
Received:
Analyses Result Units
19I0103-17Work Order/ID:
09/03/2019 08:00
09/04/2019 10:10
WAL
pH 9.0 pH Units
Page 3 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Field Results Date: Tuesday, September 10, 2019
Page 4 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
CASE NARRATIVE Date: Tuesday, September 10, 2019
Client:
Project:
Arcelor Mittal USA, Inc.
Daily
Lab Order: 19I0103
The Total Suspended Solids method residue requirement of 2.5 mg were not met for the following sample(s).
Due to insufficient sample volume remaining, re-analysis was not performed on the sample(s).
Laboratory ID Sample Name
19I0103-20 CM2-Grab
Page 5 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/03/2019 6:10
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-01
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
011-CompositeClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
011
Daily
Certs
RPLEPA 200.7 Rev 4.4
09/04/2019 10:36
Method:
Prep Date/Time:
Analyst:
Total Recoverable Metals by ICP09/04/2019 13:461A 0.0041 mg/L0.00750.0033Lead eij
09/04/2019 13:461A 0.010 mg/L0.0200.0073Zinc eij
ABGSM 4500-CN C/E-1999
09/04/2019 11:35
Method:
Prep Date/Time:
Analyst:
Total Cyanide09/04/2019 14:111A 0.0027 mg/L0.00500.0020Cyanide, Total eij
ABGSW-846 9014
09/04/2019 10:47
Method:
Prep Date/Time:
Analyst:
Free Cyanide09/04/2019 12:271A ND mg/L0.0062Free Cyanide
ABGEPA 350.1 Rev 2.0
09/04/2019 11:39
Method:
Prep Date/Time:
Analyst:
Nitrogen, Ammonia as N09/04/2019 13:581A 0.22 mg/L0.100.054Nitrogen, Ammonia (As N) ei
ABGEPA 420.4 Rev 1.0
09/04/2019 11:35
Method:
Prep Date/Time:
Analyst:
Total Phenolics09/04/2019 15:031A ND mg/L0.0100.0060Phenolics, Total Recoverable Ueij
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 2.6 mg/L1.01.0Total Suspended Solids eij
Page 6 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/03/2019 6:10
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-02
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
011-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
011
Daily
Certs
KMTEPA 1664B
09/04/2019 07:40
Method:
Prep Date/Time:
Analyst:
Oil & Grease (HEM) by SPE09/04/2019 13:551A ND mg/L5.01.4Oil & Grease (HEM) Ueij
Page 7 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/03/2019 6:25
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-03
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
001-CompositeClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
001
Daily
Certs
RPLEPA 200.7 Rev 4.4
09/04/2019 10:36
Method:
Prep Date/Time:
Analyst:
Total Recoverable Metals by ICP09/04/2019 13:511A 0.0028 mg/L0.0100.0013Copper eij
09/04/2019 13:511A ND mg/L0.00750.0033Lead Ueij
09/04/2019 13:511A ND mg/L0.0200.0073Zinc Ueij
BTMEPA 200.8 Rev 5.4
09/08/2019 12:49
Method:
Prep Date/Time:
Analyst:
Total Recoverable Metals by ICP/MS09/09/2019 13:391A ND mg/L0.000600.000053Silver Ueij
ABGSM 4500-CN C/E-1999
09/04/2019 11:35
Method:
Prep Date/Time:
Analyst:
Total Cyanide09/04/2019 14:121A 0.0022 mg/L0.00500.0020Cyanide, Total eij
ABGSW-846 9014
09/04/2019 10:47
Method:
Prep Date/Time:
Analyst:
Free Cyanide09/04/2019 12:321A ND mg/L0.0062Free Cyanide
ABGEPA 350.1 Rev 2.0
09/04/2019 11:39
Method:
Prep Date/Time:
Analyst:
Nitrogen, Ammonia as N09/04/2019 14:001A 0.20 mg/L0.100.054Nitrogen, Ammonia (As N) ei
ABGEPA 420.4 Rev 1.0
09/04/2019 11:35
Method:
Prep Date/Time:
Analyst:
Total Phenolics09/04/2019 15:041A ND mg/L0.0100.0060Phenolics, Total Recoverable Ueij
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 1.4 mg/L1.01.0Total Suspended Solids eij
Page 8 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/03/2019 6:25
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-04
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
001-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
001
Daily
Certs
KMTEPA 1664B
09/04/2019 07:40
Method:
Prep Date/Time:
Analyst:
Oil & Grease (HEM) by SPE09/04/2019 13:551A ND mg/L5.01.4Oil & Grease (HEM) Ueij
Page 9 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/04/2019 6:46
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-05
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
031-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
031
Daily
Certs
JAASM 9222 D-1997
09/04/2019 11:38
Method:
Prep Date/Time:
Analyst:
Fecal Coliform by Membrane Filtration09/04/2019 11:381A ND CFU/100ml1.01.0Fecal Coliform Ud
EFSM 5210 B-2001
09/04/2019 16:51
Method:
Prep Date/Time:
Analyst:
Biochemical Oxygen Demand09/09/2019 14:061A 2.2 mg/L2.02.0Biochemical Oxygen Demand eij
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 3.4 mg/L1.01.0Total Suspended Solids eij
Page 10 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/04/2019 6:50
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-06
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
Mixed Liquor-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
Mixed Liquor
Daily
Certs
DATSM 2540 F-1997
09/04/2019 10:43
Method:
Prep Date/Time:
Analyst:
Settleable Solids09/04/2019 10:431A 200 ml/L1.01.0Settleable Solids i
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 2100 mg/L1.01.0Total Suspended Solids eij
Page 11 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/04/2019 6:40
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-07
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
J-Box-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
J-Box
Daily
Certs
ABGEPA 350.1 Rev 2.0
09/04/2019 11:39
Method:
Prep Date/Time:
Analyst:
Nitrogen, Ammonia as N09/04/2019 14:031A 0.37 mg/L0.100.054Nitrogen, Ammonia (As N) ei
ABGEPA 420.4 Rev 1.0
09/04/2019 11:35
Method:
Prep Date/Time:
Analyst:
Total Phenolics09/04/2019 15:061A ND mg/L0.0100.0060Phenolics, Total Recoverable Ueij
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 11 mg/L1.01.0Total Suspended Solids eij
Page 12 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/04/2019 7:00
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-08
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
WWII-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
WWII
Daily
Certs
ABGSM 4500-CN C/E-1999
09/04/2019 11:35
Method:
Prep Date/Time:
Analyst:
Total Cyanide09/04/2019 14:141A 0.0066 mg/L0.00500.0020Cyanide, Total eij
Page 13 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/04/2019 7:40
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-09
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
Coldwell-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
Coldwell
Daily
Certs
RPLEPA 200.7 Rev 4.4
09/05/2019 09:00
Method:
Prep Date/Time:
Analyst:
Total Recoverable Metals by ICP09/05/2019 12:231A 0.094 mg/L0.00750.0033Lead eij
09/05/2019 12:231A 0.60 mg/L0.0200.0073Zinc eij
ABGSM 4500-CN C/E-1999
09/04/2019 11:35
Method:
Prep Date/Time:
Analyst:
Total Cyanide09/04/2019 14:161A 0.080 mg/L0.00500.0020Cyanide, Total eij
ABGEPA 350.1 Rev 2.0
09/04/2019 11:39
Method:
Prep Date/Time:
Analyst:
Nitrogen, Ammonia as N09/04/2019 14:051A 44 mg/L1.00.54Nitrogen, Ammonia (As N) ei
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 99 mg/L1.01.0Total Suspended Solids eij
Page 14 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/04/2019 7:50
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-10
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
RSB FT Overflow-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
RSB FT Overflow
Daily
Certs
RPLEPA 200.7 Rev 4.4
09/05/2019 09:00
Method:
Prep Date/Time:
Analyst:
Total Recoverable Metals by ICP09/05/2019 12:381A 0.0093 mg/L0.00750.0033Lead eij
09/05/2019 12:381A 0.031 mg/L0.0200.0073Zinc eij
ABGEPA 350.1 Rev 2.0
09/04/2019 11:39
Method:
Prep Date/Time:
Analyst:
Nitrogen, Ammonia as N09/04/2019 14:081A 6.1 mg/L0.100.054Nitrogen, Ammonia (As N) ei
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 10 mg/L1.01.0Total Suspended Solids eij
Page 15 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/04/2019 7:49
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-11
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
RSB FT Influent-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
RSB FT Influent
Daily
Certs
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 15000 mg/L1.01.0Total Suspended Solids eij
Page 16 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/02/2019 8:20
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-12
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
WPL-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
WPL
Daily
Certs
DATSM 4500 H+ B-2000
09/05/2019 12:48
Method:
Prep Date/Time:
Analyst:
pH09/05/2019 12:481A < 2 S.U.2.00pH Heij
EFSM 2710 F-2004
09/04/2019 15:29
Method:
Prep Date/Time:
Analyst:
Specific Gravity09/04/2019 15:291A 1.31 T/4 C0.01000.0100Specific Gravity
Page 17 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/04/2019 8:27
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-13
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
999-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
999
Daily
Certs
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 1.5 mg/L1.01.0Total Suspended Solids eij
Page 18 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/04/2019 8:10
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-14
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
BFTC-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
BFTC
Daily
Certs
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 36 mg/L1.01.0Total Suspended Solids eij
Page 19 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/03/2019 8:15
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-15
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
002-CompositeClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
002
Daily
Certs
ABGSM 4500-CN C/E-1999
09/04/2019 11:35
Method:
Prep Date/Time:
Analyst:
Total Cyanide09/04/2019 14:181A ND mg/L0.00500.0020Cyanide, Total Ueij
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 1.8 mg/L1.01.0Total Suspended Solids eij
Page 20 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/03/2019 8:15
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-16
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
002-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
002
Daily
Certs
KMTEPA 1664B
09/04/2019 07:40
Method:
Prep Date/Time:
Analyst:
Oil & Grease (HEM) by SPE09/04/2019 13:551A ND mg/L5.01.4Oil & Grease (HEM) Ueij
Page 21 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/03/2019 8:00
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-17
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
WAL-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
WAL
Daily
Certs
KMTEPA 1664B
09/04/2019 07:40
Method:
Prep Date/Time:
Analyst:
Oil & Grease (HEM) by SPE09/04/2019 13:551A 16.2 mg/L5.01.4Oil & Grease (HEM) eij
EFSM 2710 F-2004
09/04/2019 15:29
Method:
Prep Date/Time:
Analyst:
Specific Gravity09/04/2019 15:291A 0.999 T/4 C0.01000.0100Specific Gravity
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 8.4 mg/L1.01.0Total Suspended Solids eij
Page 22 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/04/2019 0:00
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-19
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
CM1-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
CM1
Daily
Certs
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 11 mg/L1.01.0Total Suspended Solids eij
Page 23 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/04/2019 0:00
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-20
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
CM2-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
CM2
Daily
Certs
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 8.0 mg/L1.01.0Total Suspended Solids eij
Page 24 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/04/2019 0:00
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-21
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
CM6 GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
CM6
Daily
Certs
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 10 mg/L1.01.0Total Suspended Solids eij
Page 25 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/04/2019 0:00
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-22
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
HM2-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
HM2
Daily
Certs
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 14 mg/L1.01.0Total Suspended Solids eij
Page 26 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Aqueous
09/04/2019 0:00
09/04/2019 10:10
Client:
Client Project:
Matrix:
Work Order/ID: 19I0103-23
Sampled:
Received:
Analytical Results
Analyses AT Result RL Qual Units DF Analyzed
Date: Tuesday, September 10, 2019
HM3-GrabClient Sample ID:
Sample Description:
MDL
Arcelor Mittal USA, Inc.
HM3
Daily
Certs
KMTSM 2540 D-1997
09/04/2019 10:57
Method:
Prep Date/Time:
Analyst:
Total Suspended Solids09/04/2019 12:591A 11 mg/L1.01.0Total Suspended Solids eij
Page 27 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
ANALYTE TYPES: (AT)A,B = Target Analyte
I = Internal Standard
M = Summation Analyte
S = Surrogate
T = Tentatively Identified Compound (TIC, concentration estimated)
QC SAMPLE IDENTIFICATIONSBLK = Method Blank ICSA = Interference Check Standard "A"
DUP = Method Duplicate ICSAB = Interference Check Standard "AB"
BS = Method Blank Spike BSD = Method Blank Spike Duplicate
MS = Matrix Spike MSD = Matrix Spike Duplicate
ICB = Initial Calibration Blank ICV = Initial Calibration Verification
CCB = Continuing Calibration Blank CCV = Continuing Calibration Verification
CRL = Client Required Reporting Limit OPR = Ongoing Precision and Recovery Standard
PDS = Post Digestion Spike SD = Serial Dilution
QCS = Quality Control Standard
CERTIFICATIONS (Certs)
Below is a list of certifications maintained by the Microbac Merrillville Laboratory. All data included in this report has been reviewed for and
meets all project specific and quality control requirements of the applicable accreditation, unless otherwise noted. Complete lists of individual
analytes pursuant to each certification below are available upon request.
d Illinois EPA drinking water, wastewater and solid waste analysis (#200064)
e Illinois DOPH Micro analysis of drinking water (#1755266)
i Kansas Dept Health & Env. NELAP (#E-10397)
j Kentucky Wastewater Laboratory Certification Program (#108202)
FLAGS, FOOTNOTES AND ABBREVIATIONS (as needed)
H: Sample was analyzed past holding time.
MDL: Minimum Detection Limit
RL: Reporting Limit
RPD: Relative Percent Difference
U: The analyte was analyzed for but was not detected above the reported quantitation limit. The quantitation limit has
been adjusted for any dilution or concentration of the sample.
Page 28 of 34
Microbac Laboratories, Inc.
250 West 84th Drive | Merrillville, IN 46410 | 800.536.8379 p | 219.769.8378 p | 219.769.1664 f | www.microbac.com
Cooler Receipt Log [TOC_1]Cooler Receipt[TOC]
Cooler ID: Default Cooler Temp: 5.9ºC
Cooler Inspection Checklist
Ice Present or not required? Yes
Shipping containers sealed or not required? Yes
Custody seals intact or not required? Yes
Chain of Custody (COC) Present? Yes
COC includes customer information? Yes
Relinquished and received signature on COC? Yes
Sample collector identified on COC? Yes
Sample type identified on COC? Yes
Correct type of Containers Received Yes
Correct number of containers listed on COC? Yes
Containers Intact? Yes
COC includes requested analyses? Yes
Enough sample volume for indicated tests received? Yes
Sample labels match COC (Name, Date & Time?) Yes
Samples arrived within hold time? Yes
Correct preservatives on COC or not required? Yes
Chemical preservations checked or not required? Yes
Preservation checks meet method requirements? Yes
VOA vials have zero headspace, or not recd.? Yes
Page 29 of 34
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