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Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC;...

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18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East, Suite 100 Seattle, WA 98102 ALS Environmental received 11 samples on 14-May-2016 08:32 AM for the analyses presented in the following report. Project Manager Shawn Smythe Shawn Smythe Electronically approved by: Jeff Ogle The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. QC sample results for this data met laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Laboratory Group. Samples will be disposed in 30 days unless storage arrangements are made. The total number of pages in this report is 27. If you have any questions regarding this report, please feel free to contact me. Sincerely, ADDRESS 4388 Glendale Milford Rd Cincinnati, Ohio 45242- | PHONE (513) 733-5336 | FAX (513) 733-5347 ALS GROUP USA, CORP. Part of the ALS Group An ALS Limited Company
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Page 1: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

18-May-2016

PBSGregg Middaugh

Dear Gregg,

Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413

Fax:Tel: (206) 255-4659

2517 Eastlake Ave. East, Suite 100Seattle, WA 98102

ALS Environmental received 11 samples on 14-May-2016 08:32 AM for the analyses presented in the following report.

Project ManagerShawn Smythe

Shawn SmytheElectronically approved by: Jeff Ogle

The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested.

QC sample results for this data met laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Laboratory Group. Samples will be disposed in 30 days unless storage arrangements are made.

The total number of pages in this report is 27.

If you have any questions regarding this report, please feel free to contact me.

Sincerely,

ADDRESS 4388 Glendale Milford Rd Cincinnati, Ohio 45242- | PHONE (513) 733-5336 | FAX (513) 733-5347ALS GROUP USA, CORP. Part of the ALS Group An ALS Limited Company

Page 2: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Date: 18-May-16ALS Environmental

Project: SKY VALEY EC; Project # 41373.000Client: PBS

Work Order: 1605413Work Order Sample Summary

Lab Samp ID Client Sample ID Collection DateTag Number Date ReceivedMatrix Hold1605413-01 100-PCB-A Air 5/12/2016 5/14/2016 08:321605413-02 101-PCB-A Air 5/12/2016 5/14/2016 08:321605413-03 102-PCB-A Air 5/12/2016 5/14/2016 08:321605413-04 103-PCB-A Air 5/12/2016 5/14/2016 08:321605413-05 104-PCB-A Air 5/12/2016 5/14/2016 08:321605413-06 105-PCB-A Air 5/12/2016 5/14/2016 08:321605413-07 106-PCB-A Air 5/12/2016 5/14/2016 08:321605413-08 107-PCB-A Air 5/12/2016 5/14/2016 08:321605413-09 108-PCB-A Air 5/12/2016 5/14/2016 08:321605413-10 109-PCB-A Air 5/12/2016 5/14/2016 08:321605413-11 110-PCB-A Air 5/12/2016 5/14/2016 08:32

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Page 3: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Date: 18-May-16ALS Environmental

Project: SKY VALEY EC; Project # 41373.000Client: PBS

Work Order: 1605413Case Narrative

The analytical data provided relates directly to the samples received by ALS Laboratory Group and for only the analyses requested.

Results relate only to the items tested and are not blank corrected unless indicated.

QC sample results for this data met laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Laboratory Group. Samples will be disposed in 30 days unless storage arrangements are made.

CN Page 1 of 1

Page 4: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 100-PCB-ACollection Date: 5/12/2016

Matrix: AIR

Analyses

Client: PBS Work Order: 1605413Lab ID: 1605413-01

ALS Environmental Date: 18-May-16

Analytical Results

PCBS BY EPA TO-10 ETO10A Analyst: JEAMethod: Air Volume (L): 1988

µg/sample µg/sample mg/m3Reporting LimitDate Analyzed: 5/17/2016

Aroclor 1016 0.10ND <0.000050Aroclor 1221 0.10ND <0.000050Aroclor 1232 0.10ND <0.000050Aroclor 1242 0.101.3 0.00063Aroclor 1248 0.10ND <0.000050Aroclor 1254 0.10ND <0.000050Aroclor 1260 0.10ND <0.000050Aroclor 1262 0.10ND <0.000050Aroclor 1268 0.10ND <0.000050

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Page 5: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 101-PCB-ACollection Date: 5/12/2016

Matrix: AIR

Analyses

Client: PBS Work Order: 1605413Lab ID: 1605413-02

ALS Environmental Date: 18-May-16

Analytical Results

PCBS BY EPA TO-10 ETO10A Analyst: JEAMethod: Air Volume (L): 1988

µg/sample µg/sample mg/m3Reporting LimitDate Analyzed: 5/17/2016

Aroclor 1016 0.100.90 0.00045Aroclor 1221 0.10ND <0.000050Aroclor 1232 0.10ND <0.000050Aroclor 1242 0.10ND <0.000050Aroclor 1248 0.10ND <0.000050Aroclor 1254 0.10ND <0.000050Aroclor 1260 0.10ND <0.000050Aroclor 1262 0.10ND <0.000050Aroclor 1268 0.10ND <0.000050

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Page 6: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 102-PCB-ACollection Date: 5/12/2016

Matrix: AIR

Analyses

Client: PBS Work Order: 1605413Lab ID: 1605413-03

ALS Environmental Date: 18-May-16

Analytical Results

PCBS BY EPA TO-10 ETO10A Analyst: JEAMethod: Air Volume (L): 1988

µg/sample µg/sample mg/m3Reporting LimitDate Analyzed: 5/17/2016

Aroclor 1016 0.10ND <0.000050Aroclor 1221 0.10ND <0.000050Aroclor 1232 0.10ND <0.000050Aroclor 1242 0.100.96 0.00048Aroclor 1248 0.10ND <0.000050Aroclor 1254 0.10ND <0.000050Aroclor 1260 0.10ND <0.000050Aroclor 1262 0.10ND <0.000050Aroclor 1268 0.10ND <0.000050

AR Page 3 of 11

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Page 7: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 103-PCB-ACollection Date: 5/12/2016

Matrix: AIR

Analyses

Client: PBS Work Order: 1605413Lab ID: 1605413-04

ALS Environmental Date: 18-May-16

Analytical Results

PCBS BY EPA TO-10 ETO10A Analyst: JEAMethod: Air Volume (L): 1974

µg/sample µg/sample mg/m3Reporting LimitDate Analyzed: 5/17/2016

Aroclor 1016 0.10ND <0.000051Aroclor 1221 0.10ND <0.000051Aroclor 1232 0.10ND <0.000051Aroclor 1242 0.100.85 0.00043Aroclor 1248 0.10ND <0.000051Aroclor 1254 0.10ND <0.000051Aroclor 1260 0.10ND <0.000051Aroclor 1262 0.10ND <0.000051Aroclor 1268 0.10ND <0.000051

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Page 8: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 104-PCB-ACollection Date: 5/12/2016

Matrix: AIR

Analyses

Client: PBS Work Order: 1605413Lab ID: 1605413-05

ALS Environmental Date: 18-May-16

Analytical Results

PCBS BY EPA TO-10 ETO10A Analyst: JEAMethod: Air Volume (L): 1960

µg/sample µg/sample mg/m3Reporting LimitDate Analyzed: 5/17/2016

Aroclor 1016 0.10ND <0.000051Aroclor 1221 0.10ND <0.000051Aroclor 1232 0.10ND <0.000051Aroclor 1242 0.100.40 0.00021Aroclor 1248 0.10ND <0.000051Aroclor 1254 0.10ND <0.000051Aroclor 1260 0.10ND <0.000051Aroclor 1262 0.10ND <0.000051Aroclor 1268 0.10ND <0.000051

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Page 9: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 105-PCB-ACollection Date: 5/12/2016

Matrix: AIR

Analyses

Client: PBS Work Order: 1605413Lab ID: 1605413-06

ALS Environmental Date: 18-May-16

Analytical Results

PCBS BY EPA TO-10 ETO10A Analyst: JEAMethod: Air Volume (L): 1997

µg/sample µg/sample mg/m3Reporting LimitDate Analyzed: 5/17/2016

Aroclor 1016 0.10ND <0.000050Aroclor 1221 0.10ND <0.000050Aroclor 1232 0.10ND <0.000050Aroclor 1242 0.100.77 0.00039Aroclor 1248 0.10ND <0.000050Aroclor 1254 0.10ND <0.000050Aroclor 1260 0.10ND <0.000050Aroclor 1262 0.10ND <0.000050Aroclor 1268 0.10ND <0.000050

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Page 10: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 106-PCB-ACollection Date: 5/12/2016

Matrix: AIR

Analyses

Client: PBS Work Order: 1605413Lab ID: 1605413-07

ALS Environmental Date: 18-May-16

Analytical Results

PCBS BY EPA TO-10 ETO10A Analyst: JEAMethod: Air Volume (L): 1979

µg/sample µg/sample mg/m3Reporting LimitDate Analyzed: 5/17/2016

Aroclor 1016 0.10ND <0.000051Aroclor 1221 0.10ND <0.000051Aroclor 1232 0.10ND <0.000051Aroclor 1242 0.100.77 0.00039Aroclor 1248 0.10ND <0.000051Aroclor 1254 0.10ND <0.000051Aroclor 1260 0.10ND <0.000051Aroclor 1262 0.10ND <0.000051Aroclor 1268 0.10ND <0.000051

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Page 11: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 107-PCB-ACollection Date: 5/12/2016

Matrix: AIR

Analyses

Client: PBS Work Order: 1605413Lab ID: 1605413-08

ALS Environmental Date: 18-May-16

Analytical Results

PCBS BY EPA TO-10 ETO10A Analyst: JEAMethod: Air Volume (L): 1974

µg/sample µg/sample mg/m3Reporting LimitDate Analyzed: 5/17/2016

Aroclor 1016 0.10ND <0.000051Aroclor 1221 0.10ND <0.000051Aroclor 1232 0.10ND <0.000051Aroclor 1242 0.100.36 0.00018Aroclor 1248 0.10ND <0.000051Aroclor 1254 0.10ND <0.000051Aroclor 1260 0.10ND <0.000051Aroclor 1262 0.10ND <0.000051Aroclor 1268 0.10ND <0.000051

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Page 12: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 108-PCB-ACollection Date: 5/12/2016

Matrix: AIR

Analyses

Client: PBS Work Order: 1605413Lab ID: 1605413-09

ALS Environmental Date: 18-May-16

Analytical Results

PCBS BY EPA TO-10 ETO10A Analyst: JEAMethod: Air Volume (L): 1988

µg/sample µg/sample mg/m3Reporting LimitDate Analyzed: 5/17/2016

Aroclor 1016 0.10ND <0.000050Aroclor 1221 0.10ND <0.000050Aroclor 1232 0.10ND <0.000050Aroclor 1242 0.100.52 0.00026Aroclor 1248 0.10ND <0.000050Aroclor 1254 0.10ND <0.000050Aroclor 1260 0.10ND <0.000050Aroclor 1262 0.10ND <0.000050Aroclor 1268 0.10ND <0.000050

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Page 13: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 109-PCB-ACollection Date: 5/12/2016

Matrix: AIR

Analyses

Client: PBS Work Order: 1605413Lab ID: 1605413-10

ALS Environmental Date: 18-May-16

Analytical Results

PCBS BY EPA TO-10 ETO10A Analyst: JEAMethod: Air Volume (L): 0

µg/sample µg/sample mg/m3Reporting LimitDate Analyzed: 5/17/2016

Aroclor 1016 0.10ND NAAroclor 1221 0.10ND NAAroclor 1232 0.10ND NAAroclor 1242 0.10ND NAAroclor 1248 0.10ND NAAroclor 1254 0.10ND NAAroclor 1260 0.10ND NAAroclor 1262 0.10ND NAAroclor 1268 0.10ND NA

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Page 14: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 110-PCB-ACollection Date: 5/12/2016

Matrix: AIR

Analyses

Client: PBS Work Order: 1605413Lab ID: 1605413-11

ALS Environmental Date: 18-May-16

Analytical Results

PCBS BY EPA TO-10 ETO10A Analyst: JEAMethod: Air Volume (L): 0

µg/sample µg/sample mg/m3Reporting LimitDate Analyzed: 5/17/2016

Aroclor 1016 0.10ND NAAroclor 1221 0.10ND NAAroclor 1232 0.10ND NAAroclor 1242 0.10ND NAAroclor 1248 0.10ND NAAroclor 1254 0.10ND NAAroclor 1260 0.10ND NAAroclor 1262 0.10ND NAAroclor 1268 0.10ND NA

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Page 15: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 100-PCB-ACollection Date: 5/12/2016 Matrix: AIR

Analyses Result Qual Units Date AnalyzedReport Limit

Client: PBSWork Order: 1605413

Dilution Factor

Lab ID: 1605413-01

ALS Environmental Date: 18-May-16

PCBS BY EPA TO-10 ETO10A Analyst: JEAPrep Date: 5/16/2016Aroclor 1016 5/17/20160.10 µg/sample 1NDAroclor 1221 5/17/20160.10 µg/sample 1NDAroclor 1232 5/17/20160.10 µg/sample 1NDAroclor 1242 5/17/20160.10 µg/sample 11.3Aroclor 1248 5/17/20160.10 µg/sample 1NDAroclor 1254 5/17/20160.10 µg/sample 1NDAroclor 1260 5/17/20160.10 µg/sample 1NDAroclor 1262 5/17/20160.10 µg/sample 1NDAroclor 1268 5/17/20160.10 µg/sample 1ND Surr: Decachlorobiphenyl 5/17/201635.7-104 %REC 183.6 Surr: Tetrachloro-m-xylene 5/17/201645.7-110 %REC 182.4

AR Page 1 of 11

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Page 16: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 101-PCB-ACollection Date: 5/12/2016 Matrix: AIR

Analyses Result Qual Units Date AnalyzedReport Limit

Client: PBSWork Order: 1605413

Dilution Factor

Lab ID: 1605413-02

ALS Environmental Date: 18-May-16

PCBS BY EPA TO-10 ETO10A Analyst: JEAPrep Date: 5/16/2016Aroclor 1016 5/17/20160.10 µg/sample 10.90Aroclor 1221 5/17/20160.10 µg/sample 1NDAroclor 1232 5/17/20160.10 µg/sample 1NDAroclor 1242 5/17/20160.10 µg/sample 1NDAroclor 1248 5/17/20160.10 µg/sample 1NDAroclor 1254 5/17/20160.10 µg/sample 1NDAroclor 1260 5/17/20160.10 µg/sample 1NDAroclor 1262 5/17/20160.10 µg/sample 1NDAroclor 1268 5/17/20160.10 µg/sample 1ND Surr: Decachlorobiphenyl 5/17/201635.7-104 %REC 185.2 Surr: Tetrachloro-m-xylene 5/17/201645.7-110 %REC 180.8

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Page 17: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 102-PCB-ACollection Date: 5/12/2016 Matrix: AIR

Analyses Result Qual Units Date AnalyzedReport Limit

Client: PBSWork Order: 1605413

Dilution Factor

Lab ID: 1605413-03

ALS Environmental Date: 18-May-16

PCBS BY EPA TO-10 ETO10A Analyst: JEAPrep Date: 5/16/2016Aroclor 1016 5/17/20160.10 µg/sample 1NDAroclor 1221 5/17/20160.10 µg/sample 1NDAroclor 1232 5/17/20160.10 µg/sample 1NDAroclor 1242 5/17/20160.10 µg/sample 10.96Aroclor 1248 5/17/20160.10 µg/sample 1NDAroclor 1254 5/17/20160.10 µg/sample 1NDAroclor 1260 5/17/20160.10 µg/sample 1NDAroclor 1262 5/17/20160.10 µg/sample 1NDAroclor 1268 5/17/20160.10 µg/sample 1ND Surr: Decachlorobiphenyl 5/17/201635.7-104 %REC 186.4 Surr: Tetrachloro-m-xylene 5/17/201645.7-110 %REC 187.4

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Page 18: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 103-PCB-ACollection Date: 5/12/2016 Matrix: AIR

Analyses Result Qual Units Date AnalyzedReport Limit

Client: PBSWork Order: 1605413

Dilution Factor

Lab ID: 1605413-04

ALS Environmental Date: 18-May-16

PCBS BY EPA TO-10 ETO10A Analyst: JEAPrep Date: 5/16/2016Aroclor 1016 5/17/20160.10 µg/sample 1NDAroclor 1221 5/17/20160.10 µg/sample 1NDAroclor 1232 5/17/20160.10 µg/sample 1NDAroclor 1242 5/17/20160.10 µg/sample 10.85Aroclor 1248 5/17/20160.10 µg/sample 1NDAroclor 1254 5/17/20160.10 µg/sample 1NDAroclor 1260 5/17/20160.10 µg/sample 1NDAroclor 1262 5/17/20160.10 µg/sample 1NDAroclor 1268 5/17/20160.10 µg/sample 1ND Surr: Decachlorobiphenyl 5/17/201635.7-104 %REC 182.6 Surr: Tetrachloro-m-xylene 5/17/201645.7-110 %REC 187.6

AR Page 4 of 11

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Page 19: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 104-PCB-ACollection Date: 5/12/2016 Matrix: AIR

Analyses Result Qual Units Date AnalyzedReport Limit

Client: PBSWork Order: 1605413

Dilution Factor

Lab ID: 1605413-05

ALS Environmental Date: 18-May-16

PCBS BY EPA TO-10 ETO10A Analyst: JEAPrep Date: 5/16/2016Aroclor 1016 5/17/20160.10 µg/sample 1NDAroclor 1221 5/17/20160.10 µg/sample 1NDAroclor 1232 5/17/20160.10 µg/sample 1NDAroclor 1242 5/17/20160.10 µg/sample 10.40Aroclor 1248 5/17/20160.10 µg/sample 1NDAroclor 1254 5/17/20160.10 µg/sample 1NDAroclor 1260 5/17/20160.10 µg/sample 1NDAroclor 1262 5/17/20160.10 µg/sample 1NDAroclor 1268 5/17/20160.10 µg/sample 1ND Surr: Decachlorobiphenyl 5/17/201635.7-104 %REC 181.6 Surr: Tetrachloro-m-xylene 5/17/201645.7-110 %REC 185.2

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Page 20: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 105-PCB-ACollection Date: 5/12/2016 Matrix: AIR

Analyses Result Qual Units Date AnalyzedReport Limit

Client: PBSWork Order: 1605413

Dilution Factor

Lab ID: 1605413-06

ALS Environmental Date: 18-May-16

PCBS BY EPA TO-10 ETO10A Analyst: JEAPrep Date: 5/16/2016Aroclor 1016 5/17/20160.10 µg/sample 1NDAroclor 1221 5/17/20160.10 µg/sample 1NDAroclor 1232 5/17/20160.10 µg/sample 1NDAroclor 1242 5/17/20160.10 µg/sample 10.77Aroclor 1248 5/17/20160.10 µg/sample 1NDAroclor 1254 5/17/20160.10 µg/sample 1NDAroclor 1260 5/17/20160.10 µg/sample 1NDAroclor 1262 5/17/20160.10 µg/sample 1NDAroclor 1268 5/17/20160.10 µg/sample 1ND Surr: Decachlorobiphenyl 5/17/201635.7-104 %REC 179.4 Surr: Tetrachloro-m-xylene 5/17/201645.7-110 %REC 177.0

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Page 21: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 106-PCB-ACollection Date: 5/12/2016 Matrix: AIR

Analyses Result Qual Units Date AnalyzedReport Limit

Client: PBSWork Order: 1605413

Dilution Factor

Lab ID: 1605413-07

ALS Environmental Date: 18-May-16

PCBS BY EPA TO-10 ETO10A Analyst: JEAPrep Date: 5/16/2016Aroclor 1016 5/17/20160.10 µg/sample 1NDAroclor 1221 5/17/20160.10 µg/sample 1NDAroclor 1232 5/17/20160.10 µg/sample 1NDAroclor 1242 5/17/20160.10 µg/sample 10.77Aroclor 1248 5/17/20160.10 µg/sample 1NDAroclor 1254 5/17/20160.10 µg/sample 1NDAroclor 1260 5/17/20160.10 µg/sample 1NDAroclor 1262 5/17/20160.10 µg/sample 1NDAroclor 1268 5/17/20160.10 µg/sample 1ND Surr: Decachlorobiphenyl 5/17/201635.7-104 %REC 187.8 Surr: Tetrachloro-m-xylene 5/17/201645.7-110 %REC 190.6

AR Page 7 of 11

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Page 22: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 107-PCB-ACollection Date: 5/12/2016 Matrix: AIR

Analyses Result Qual Units Date AnalyzedReport Limit

Client: PBSWork Order: 1605413

Dilution Factor

Lab ID: 1605413-08

ALS Environmental Date: 18-May-16

PCBS BY EPA TO-10 ETO10A Analyst: JEAPrep Date: 5/16/2016Aroclor 1016 5/17/20160.10 µg/sample 1NDAroclor 1221 5/17/20160.10 µg/sample 1NDAroclor 1232 5/17/20160.10 µg/sample 1NDAroclor 1242 5/17/20160.10 µg/sample 10.36Aroclor 1248 5/17/20160.10 µg/sample 1NDAroclor 1254 5/17/20160.10 µg/sample 1NDAroclor 1260 5/17/20160.10 µg/sample 1NDAroclor 1262 5/17/20160.10 µg/sample 1NDAroclor 1268 5/17/20160.10 µg/sample 1ND Surr: Decachlorobiphenyl 5/17/201635.7-104 %REC 191.0 Surr: Tetrachloro-m-xylene 5/17/201645.7-110 %REC 193.2

AR Page 8 of 11

Note:

Page 23: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 108-PCB-ACollection Date: 5/12/2016 Matrix: AIR

Analyses Result Qual Units Date AnalyzedReport Limit

Client: PBSWork Order: 1605413

Dilution Factor

Lab ID: 1605413-09

ALS Environmental Date: 18-May-16

PCBS BY EPA TO-10 ETO10A Analyst: JEAPrep Date: 5/16/2016Aroclor 1016 5/17/20160.10 µg/sample 1NDAroclor 1221 5/17/20160.10 µg/sample 1NDAroclor 1232 5/17/20160.10 µg/sample 1NDAroclor 1242 5/17/20160.10 µg/sample 10.52Aroclor 1248 5/17/20160.10 µg/sample 1NDAroclor 1254 5/17/20160.10 µg/sample 1NDAroclor 1260 5/17/20160.10 µg/sample 1NDAroclor 1262 5/17/20160.10 µg/sample 1NDAroclor 1268 5/17/20160.10 µg/sample 1ND Surr: Decachlorobiphenyl 5/17/201635.7-104 %REC 196.4 Surr: Tetrachloro-m-xylene 5/17/201645.7-110 %REC 193.8

AR Page 9 of 11

Note:

Page 24: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 109-PCB-ACollection Date: 5/12/2016 Matrix: AIR

Analyses Result Qual Units Date AnalyzedReport Limit

Client: PBSWork Order: 1605413

Dilution Factor

Lab ID: 1605413-10

ALS Environmental Date: 18-May-16

PCBS BY EPA TO-10 ETO10A Analyst: JEAPrep Date: 5/16/2016Aroclor 1016 5/17/20160.10 µg/sample 1NDAroclor 1221 5/17/20160.10 µg/sample 1NDAroclor 1232 5/17/20160.10 µg/sample 1NDAroclor 1242 5/17/20160.10 µg/sample 1NDAroclor 1248 5/17/20160.10 µg/sample 1NDAroclor 1254 5/17/20160.10 µg/sample 1NDAroclor 1260 5/17/20160.10 µg/sample 1NDAroclor 1262 5/17/20160.10 µg/sample 1NDAroclor 1268 5/17/20160.10 µg/sample 1ND Surr: Decachlorobiphenyl 5/17/201635.7-104 %REC 184.4 Surr: Tetrachloro-m-xylene 5/17/201645.7-110 %REC 192.2

AR Page 10 of 11

Note:

Page 25: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Project: SKY VALEY EC; Project # 41373.000Sample ID: 110-PCB-ACollection Date: 5/12/2016 Matrix: AIR

Analyses Result Qual Units Date AnalyzedReport Limit

Client: PBSWork Order: 1605413

Dilution Factor

Lab ID: 1605413-11

ALS Environmental Date: 18-May-16

PCBS BY EPA TO-10 ETO10A Analyst: JEAPrep Date: 5/16/2016Aroclor 1016 5/17/20160.10 µg/sample 1NDAroclor 1221 5/17/20160.10 µg/sample 1NDAroclor 1232 5/17/20160.10 µg/sample 1NDAroclor 1242 5/17/20160.10 µg/sample 1NDAroclor 1248 5/17/20160.10 µg/sample 1NDAroclor 1254 5/17/20160.10 µg/sample 1NDAroclor 1260 5/17/20160.10 µg/sample 1NDAroclor 1262 5/17/20160.10 µg/sample 1NDAroclor 1268 5/17/20160.10 µg/sample 1ND Surr: Decachlorobiphenyl 5/17/201635.7-104 %REC 185.4 Surr: Tetrachloro-m-xylene 5/17/201645.7-110 %REC 192.8

AR Page 11 of 11

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Page 26: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

Date: 18-May-16ALS Environmental

Project: SKY VALEY EC; Project # 41373.000

Client: PBSWork Order: 1605413

QC BATCH REPORT

Batch ID: 35902 Instrument ID GC3 Method: ETO10A

QualRPD Limit

Analysis Date: 5/17/2016Prep Date: 5/16/2016

Analyte Result %REC %RPD

Units: µg/sample

PQL

Client ID: SeqNo: 1282754

MBLK

Run ID: GC3_160517B

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID MBLK-35902-35902

Aroclor 1016 0.10NDAroclor 1221 0.10NDAroclor 1232 0.10NDAroclor 1242 0.10NDAroclor 1248 0.10NDAroclor 1254 0.10NDAroclor 1260 0.10NDAroclor 1262 0.10NDAroclor 1268 0.10ND

000.25 Surr: Decachlorobiphenyl 81.8 41.6-11600.2045000.25 Surr: Tetrachloro-m-xylene 88 45.7-11000.22

QualRPD Limit

Analysis Date: 5/17/2016Prep Date: 5/16/2016

Analyte Result %REC %RPD

Units: µg/sample

PQL

Client ID: SeqNo: 1282755

LCS

Run ID: GC3_160517B

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID LCS-35902-35902

005Aroclor 1260 71.80.103.592000.25 Surr: Decachlorobiphenyl 86 35.7-10400.215000.25 Surr: Tetrachloro-m-xylene 87.4 45.7-11000.2185

The following samples were analyzed in this batch: 1605413-01A 1605413-02A 1605413-03A1605413-04A 1605413-05A 1605413-06A1605413-07A 1605413-08A 1605413-09A1605413-10A 1605413-11A

QC Page: 1 of 1Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Page 27: Shawn Smythe - WordPress.com · 18-May-2016 PBS Gregg Middaugh Dear Gregg, Re: SKY VALEY EC; Project # 41373.000 Work Order: 1605413 Fax: Tel: (206) 255-4659 2517 Eastlake Ave. East,

ALS Environmental

Sample Receipt Checklist

Client Name: PBS-SEATTLE

Work Order: 1605413

Date/Time Received: 14-May-16 08:32

Received by: JNW

Checklist completed byeSignature Date

Reviewed by:DateeSignature

Matrices:Carrier name: UPS

Shipping container/cooler in good condition? Yes No Not Present

Custody seals intact on shipping container/cooler? Yes No Not Present

Custody seals intact on sample bottles? Yes No Not Present

Chain of custody present? Yes No

Chain of custody signed when relinquished and received? Yes No

Chain of custody agrees with sample labels? Yes No

Samples in proper container/bottle? Yes No

Sample containers intact? Yes No

Sufficient sample volume for indicated test? Yes No

All samples received within holding time? Yes No

Container/Temp Blank temperature in compliance? Yes No

Yes No No VOA vials submittedWater - VOA vials have zero headspace?

Water - pH acceptable upon receipt? Yes No N/A

Temperature(s)/Thermometer(s): 4.2

Login Notes:

Cooler(s)/Kit(s):

16-May-16 16-May-16 Stephanie Harrington Shawn Smythe

pH adjusted? Yes No N/ApH adjusted by:

CorrectiveAction:

Comments:

Client Contacted: Date Contacted: Person Contacted:

Contacted By: Regarding:

SRC Page 1 of 1


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