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STATE OF DELAWARE

:;TREGIlLATIONS GOVERNING-. -;. .,,,,if,'-

;HJA Z·~ R0-0 US ~;' WASTE.--

DIVISION OF ENVIRONMENTAL CONTROLDEPARTMENT OF NATURAL RESOURCES AND

ENVIBONMEN~.AL~ONTROL

JU L Y 2 8, 1 9 8 3

DELAWARE REGULATIONS GOVERNING HAZARDOUS WASTE

These regulations are effective since July 28,1983, except for the manifest, continuationforms and the related regulations. Final actionon these forms will be taken after the Environ­mental Protection Agency has promulgated theNational Uniform Manifest. In the meantime,only for the manifest and the associated regula­tions, the Delaware Hazardous Waste Regulationsas adopted November 19, 1980, and amendedSeptember 24, 1982, will continue to be effective.

lPart 26Q-BAZARDOUS WASTE

MANAGEMENT SYSTEM: GENERAL§260.2 Availability of information;confidentiality of information.

Subpart A-General

Sec.260.1 Purpose. scope, and app1ica

bility260.2 Availability of information;

confidentiality of information.260.3 Use of number and gender.

(a) Any information provided toDNREC under Parts 260 through 265 ofthese Regulations will be madeavailable to the public to the extentand in the manner authorized by 29Del. C. Chapter 100 and 7 Del. C.§6304 and DNREC regulationsimplementing 29 Del. C. Chapter 100and 7 Del. C. §6304.

Subpart a-Definitions

Appendix I-overview of Regulations

Subpart C-Rnlemaking Petitions

Subpart D-Public Participation

(b) \-lords in the singular includethe plural; and

§260.3 Use of number and gender.

When used in Parts 260 through 265of these Regulations. the followingterms have the meanings given below:

"Act" or "RCRA" means the SolidWaste Disposal Act. as amended by theResource Conservation and Recovery Actof 1976, as amended, 42 U.S.C. section6901 et seq.

(b) Any person who submits information to DNREC in accordance with Parts260 through 265 of these Regulationsmay assert a claim of businessconfiden tiality covering part or allof that information by following theproce dures set forth in 7 Del. C.§6304(c). Information covered by sucha claim will be disclosed by DNREConly to the extent. and by means ofthe procedures, set forth in 7. Del. C§6304(c). However, if no such claimaccompanies the information when it isreceived by DNREC. it may be madeavailab~e to the public withoutfurther notice to the personsubmit ting it.

As used in Parts 260 through 265of these Regulations.

§260.l0 Definitions.

Subpart B-Definitions

(a) Words in the masculine genderalso include the feminine and neutergenders; and

(c) Words in the plural include. the singular.

Definitions.References.

260.10260.11

(2) Section §260.3 establishesrules of grammatical construction forParts 260 through 265 of theseRegulations.

§260.1 Purpose, scope, and applicability.

Subpart A-General

(a) This part provides definitionsof terms. general standards, andoverview information applicable toParts 260 through 265 of theseRegulations.

(3) Section §260.10 definesterms which are used in Parts 260through 265 of these Regulations.

(b) In this part: (1) Section260.2 sets forth the rules that DNRECwill use in making information itreceives available to the public andsets forth the requirements thatgenerators. transporters, or owners oroperators of treatment. storage. ordisposal facilities must follow toassert claims of businessconfidentiality with respect toinformation that is submitted to DNRECunder Parts 260 through 265 of theseRegulations.

a(

"Department" means the Department ofNatural Resources and EnvironmentalControl of the State of Delaware.

"Designated facility· meanshazardous waste treatment, storage, ordisposal facility ~hich has received anDNREC permit (or a facility withinterim status) in accordance with therequirements of Parts 122 and 124 ofthese Regulations, or a permit from aState authorized in accordance with 40CFR Part 271 of these Regulations, thathas been designated on the manifest bythe generator pursuant to §262.20.

"Dike" means an embankment or ridgeof either natural or man-made materialsused to prevent the movement ofliquids, sludges, solids, or othermaterials.

"Discharge" or "hazardous wastedischarge" means the accidental orintentional spilling, leaking, pumping,puring, emitting, emptying, or dumpingof hazardous waste into or on any landor water.

"Dd spo sa.l n means the discharge!deposit, injection, dumping, spilling,leaking, or placing of any solid wasteor hazardous waste into or on any landor water so that such solid waste orhazardouus waste or any constituentthereof may enter the environment or beemitted into the air or discharged intoany waters, including ground waters.

"Disposal facility" means afacility or part of a facility at whichhazardous waste is intentionally placedinto or on any land or water, and atwhich waste will remain after closure.

"Division" means the Division ofEnvironmental Control.

"DNREC: hazardous waste number" meansthe number assigned by DNREC to eachhazardous waste listed in Part 261,Subpart D, of these Regulations and toeach characteristic identified in Part261, Subpart C, of these Regulations.

"EPA' identification number" meansthe number assigned by DNREC to eachgenerator, transporter, and treatment,storage, or disposal facility.

"EPA region" means the states andterritories found in anyone of thefollOWing ten regions:

"Active porClon means caac ror~~0n

or a facility where treatment, s co r ag e ,or disposal operations are being orhave been conducted after the effectivedate of Part 261 of these Regulationsand which is not a closed portion. (Seealso "closed portion" and inactiveportion" .)

"Activity" means construction,operation, or use of any facility,site, property or device.

"Administrator" means the Administrator of the Environmental ProtectionAgency, or his designee.

"Aquifer" means a geologic formation, group of formations, or part of aformation capable of yielding asignificant amount of ground water towells or springs.

"Authorized representative" meansthe person responsible for the overalloperation of a facility or anoperational unit (I.e., part of afacility), e s g , • the plant manager,superintendent or person of equivalentresponsibility.

"Certification" means a statementof professional opinion based uponknowledge and belief.

"CFR" means Code of FederalRegulations. "Commission" means theCommission on the Transportation ofHazardous Materials.

"Closed portion" means that portionof a facility which an owner or operator has closed in accordance with theapproved facility closure plan and allapplicable closure requirements. (Seealso "active portion'; and "inactiveportion".)

"Commission" means the Commissionon the !ransportation of HazardousMaterials.

"Confined aquifer" means an aauiferbounded above and below by impe~eablebeds or by beds of distinctly lowerpermeability than that of the aquiferitself; an a qud f e r containing confinedground water.

"Container" means any portabledevice in which a material is stored,transported, treated, disposed of, orotherwise handled.

"Contingency plan" means a documentsetting out an organized, planned, andcoordinated course of action to befollowed in case of a fire, explosion,or release of hazardous waste orhazardous waste constituents whichcould threaten human health or theenvt ronment.

physicalbegun; or

lRegion I-Maine, Vermont, New Hampshire,

Massachusetts, Connecticut, andRhode Island.

Region II-New York, New Jersey,Commonwealth of Puerto Rico, andthe U. S. Virgin Islands.

Region III-Pennsylvania, Delaware,Maryland, West Virginia, Virginia,and the District of Columbia.

Region IV-Kentucky, Tennessee, NorthCarolina, Mississippi, Alabama,Georgia, South Carolina, andFlorida.

Region V-Minnesota, Wisconsin,Illinois, Michigan, Indiana andOhio.

Region VI-New Mexico, Oklahoma,Arkansas, Louisiana, and Texas.

Region VII-Nebraska, Kansas, Missouri,and Iowa.

Region VIII-Montana, Wyoming, NorthDakota, South Dakota, Utah, andColorado.

Region IX-California, Nevada, Arizona,Hawaii, Guam, American Samoa,Commonwealth of the NorthernMariana Islands.

Region X-Washington, Oregon, Idaho, andAlaska.

"Elementary neutralization unit"means a device which:

(1) Is used for neutralizingwastes which are hazardous wastes onlybecause they exhibit the corrosivitycharacteristic defined in §26l.22 ofthese Regulations, or are listed inSubpart D of Part 261 of theseRegulations only for this reason; and

(2) Meets the definition of tank,container, transport vehicle orvessel in §260.l0 of these Regulations.

"Engineer" means an engineerregistered and authorized to practicein Delaware as a Professional Engineerbv the "Delaware Association ofP~ofessional Engineers".

"Equivalent method" means anytesting or analytical method approvedby the Secretary under Part 260Subpart C of these Regulations.

"Existing hazardous waste management (HWM) facility" or "existingfacility" means a facility which was

in operation or for which constructioncommenced on or before November 19,1980. A facility has commencedconstruction if:

(1) The ovne r or operatorhas obtained the Federal, State andlocal approvals or permits necessaryto begin physical construction; andeither

(2)(i) A continuous on-site,construction program has

(ii) The owner or operatorhas entered into contractualobligations which cannot becancelled or modified withoutsubstantial loss for physicalconstruction of the facility to becompleted within a reasonable time.Within this definition, "Federal,State and local approvals or permitsnecessary to begin physicalconstruction" means permits andapprovals required under Federal,State or local hazardous waste controlstatutes, regulations or ordinances.

"Existing Portion" means that landsurface area of an existing wastemanagement unit included in theoriginal Part A application, on whichwastes have been placed prior to theissuance of a permit.

"Facility or Hazardous WasteManagement (HWM) Facility" means allcontiguous land, and structures, otherappurtenances, and improvements on theland, used for treating, storing, ordisposir~ of hazardous waste. Afacility may consist of several treatment, storage, or disposal operationalunits (e.g., one or more landfills,surface impoundments, or combinationof them).

"Federal agency" means any department, agency, or other instrumentalityof the Federal Government, anyindependent agency or establishment ofthe Federal Government including anyGovernment corporation, and theGovernment Printing Office.

"Federal, State and local approvals or permits necessary to beginphysical c ons t ruc t Lon " means permitsand approvals required under Federal,State or local hazardous waste controlstatutes, regulations or ordinances.

"Food-chain crops means tobacco,crops grown for human consumption, andcrops grown for feed for animals whoseproducts are consumed by humans.

··Freebcard" means the verticaldistance between the top of a tank orsurface impoundment dike, and thesurface of the waste contained therein.

"Free liquids" means liquids whichreadily separate from the solidportion of a waste under ambienttemperature and pressure.

"Generator" means any person, bysite, whose act or process produceshazardous waste identified or listedin Part 261 of these Regulations orwhose act first causes a hazardouswaste to become subject to regulation.

"Geologist" means a geologistregistered by the "Delaware StateBoard of Registration of Geologists."

"Ground water" means water belowthe land surface in a zone ofsaturation.

"Hazardous waste" means ahazardous waste as defined in §26L 3of these Regulations.

"Hazardous Waste Constituent"­means a constituent which caused theSecretary to list the hazardous wastein Part 261, Subpart D of theseregulations, or a constituent listedin Table 1 of §261.24 of theseRegulations.

"Inactive portion" means thatportion of a facility which is notoperated after the effective date ofPart 261 of these Regulations. (Seealso "active portion" and "closedportion" .)

"Incinerator" means an encloseddevice using controlled flamecombustion, the primary purpose ofwhich is to thermally break downhazardous waste. Examples ofincinerators are rotary kiln,fluidized bed, and liquid injectionincinerators.

"Incompatible waste means ahazardous waste which is unsuitablefor:

theinto

the

means aat whichonto or

((2)Commingling with anotherwaste or material under uncontrolledconditions because the comminglingmight produce heat or pressure, fire orexplosion, violent reaction, toxicdusts, mists, fumes, or gases, orflammable fumes or gases.

(See Part 265, Appendix V, of theseRegulations for examples.)

(e.g., container inner liners or tankwalls); or

"Individual generation s t t e " meansthe contiguous site at or on which oneor more hazardous wastes are generated.An individual generation site, such asa large manufacturing plant, may haveone or more sources of hazardous wastebut is considered a single orindividual generation sf te if the siteor property is contiguous.

"In operation" refers to a faCilitywhich is treating, storing, ordisposing of hazardous waste.

"Injection well" means a well intowhich fluids are injected. (See also"underground injection".)

"Inner liner" means a continuouslayer of material placed inside a tankor container which protects theconstruction materials of the tank orcontainer from the contained waste orreagents used to treat the waste.

,. International shipment" meanstransportaton of hazardous wasteor out of the jurisdiction ofUnited States.

"Landfill" means a disposalfacility or part of a facility wherehazardous waste is placed in or on landand which is not a land treatmentfacility, a surface impoundment, or aninjection well.

"LandfLLl, cell" means a discretevolume of a hazardous waste landfillwhich uses a liner to provide isolationof wastes from adjacent cells orwastes. Examples of landfill cells aretrenches and pits.

"Land treatment facility'·facility or part of a facilityhazardous waste is applied

in a particularbecause it may

or decay ofmaterials

(1) Placementdevice or facilitycause corrosioncontainment

everyused ormeans of

biological character or composition ofthe hazardous waste. Examples ofthermal treatment processes areincineration, molten salt, pyrolysis,calcination, wet air oxidation, andmicrowave discharge. (See also"incinerator" and "open burning".)

"Totally enclosed treatmentfacility" means a facility for thetreatment of hazardous waste which isdirectly connected to an industrialproduction process and which isconstructed and operated in a mannerwhich prevents the release of anyhazardous waste or any constituentthereof into the environment duringtreatment. An example is a pipe inwhich waste acid is neutralized.

"Transfer facility" means anytransportation related facilityincluding loading docks, parkingareas, storage areas and othersimilar areas where shipments ofhazardous waste are held during thenormal course of transportation.

"Transportation" means themovement of hazardous waste by air,rail, highway, or water.

"Transporter" means a persoaengaged in the offsite transportationof hazardous waste by air, rail,highway, or water.

"Transport vehicle" means a motorvehicle or rail car used for thetransportation of cargo by any mode.Each cargo-carrying body (trailer,railroad freight car, e t c , ) is aseparate transport vehicle.

"Treatment" means any method,technique, or process, includingneutralization, designed to change thephysical, chemical, or biologicalcharacter or composition of anyhazardous waste so as to neutralizesuch waste, or so as to recover energyor material resources from the waste,or so as to render such wastenon-hazardous, or less hazardous;safer to transport, store, or disposeof; or amenable for recovery, amenablefor storage, or reduced in volume.

"Treatment Zone" means a soil areaof the unsaturated zone of a landtreatment unit within which hazardousconstituents are degraded,transformed, or immobilized.

"Underground injection" means thesubsurface emplacement of fluidsthrough a bored, drilled or drivenwell; or through a dug well, where thedepth of the dug well is greater thanthe largest surface dimension. (Seealso "injection well".)

"Unsaturated zone" or "zone ofaeration" means the zone between theland surface and the water table.

"United States" means the 50States, the District of Columbia, theCommonwealth of Puerto Rico, the U. S.Virgin Islands, Guam, American Samoa,and the Commonwealth of the NorthernMariana Islands.

"Uppermost Aquifer" means thegeologic formation nearest the naturalground surface that is an aquifer, aswell as lower aquifers that arehydraulically interconnected with thisaquifer, within the facility'sproperty boundary.

"Vessel" includesdescription of watercraft,capable of being used as atransportation on the water.

"Wastewater treatment unit" meansa device which:

(1) Is part of a wastewatertreatment facility whichis subject toregulations under ei therSection 402 or Section307(b) of the CleanWater Act; and

(2) Receives and treats orstores an influentwastewater which is ahazardous waste asdefined in §261. 3 ofthese Regulations, orgenerates and accumulates a wastewatertreatment sludge whichis a hazardous waste asdefined §261. 3 of theseRegulations, or treatsor stores a wastewatertreatment sludge whichis a hazardous waste asdefined in §26l.3 ofthese Regulations.

(3) Meets the definition oftank in §260.10 of theseRegulations.

Physical/Chemical Methods,"EPA Publication SW-846 (FirstEdition, 1980, as updated byRevisions A (August, 1980), B(July, 1981), and C(February, 1982) or (SecondEdition, 1982). The firstedition of SW-846 is nolonger in print. Revisions Aand B are available from EPA,Office of Solid Waste,(WH-565B), 401 ~ Street,S.W., Washington, D.C.20460. Revision C isavailable from NTIS, 5285Port Royal Road, Springfield,Virginia 22161. The secondedition of SW-846 includesmaterial from the firstedition and Revisions A, B,and C in a reorganizedformat. It is available fromthe Superintendent ofDocuments, U.S. GoverD~ent

Printing Office, Washington,D.C. 20402, (202) 783-3238,on a subscription basis, andfuture updates willautomatically be mailed tothe subscriber.

"Water (bulk shipment)" means thebulk transportation of hazardous wastewhich is loaded or carried on board avessel without containers or labels.

··Well" means any shaft or pit dugor bored into the earth, generally ofa cylindrical form, and often walledwith bricks or tubing to prevent theearth from caving in.

"Well injection": (See"underground injection".)

§260.ll References

(a) !..lhen used in Parts 260through 265 of theseRegulations, the followingpublications are incorporatedby reference:

"ASnf Standard Test Methodsfor Flash Point of LiqUids bySetaflash Closed Tester,"ASTM Standard D-3278-78available from AmericanSociety for Testing andMaterials, 1916 Race Street,Philadelphia, PA 19103.

"ASTM Standard Test Methodsfor Flash Point byPensky-Martens Closed Tester."

"Test MethodsSolid

for EvaluatingWaste,

(

AS~1 Standard D-93-79 orD-93-80. D-93-80 isavailable from AmericanSociety for Testing andMaterials, 1916, Race Street,Philadelphia, PA 19103.

"Flammable and CombustibleLiquids Code" (1977 or 1981),available from the ~ational

Fire Protection Association,470 Atlantic Avenue, Boston,Massachusetts 02210.

(b) The references listed inparagraph (a) of this sectionare also available forinspection at the Office ofthe Federal Register, 1100 LStreet, ~'W, Washington, D.C. 20408. Theseincorporations by referencewere approved by the Directorof the Federal Register.These materials areinc~rporated as they exist onthe date of approval and anotice of any change in thesematerials will be publishedin the Federal Register.

Subpar~ C-Rulemaking Petitions

Subpart D - Public Participation

those who arehazardous wastedetermine with

regulations they

Definition of Hazardous Waste

The first question which such aperson should ask himself is: "Is thematerial I handle a solid waste?" Ifthe answer to this question is "No",then the material is not subject tocontrol under Hazardous WasteRegulations and, therefore, the personneed not worry about whether he shouldcomply with these Regulations.

Section 261.2 of these Regulationsprovides a definition of "solid waste"which expands the statutory definitionof that term given in 7 Del. C.Chapter 63. This definition isdiagrammed in Figure 1.

Figure 1 explains that allmaterials are either: (1) garbagerefuse, or sludge; (2) solid, liquid,semi-solid or contained gaseousmaterial; or (3) something else. Nomaterials in the third category aresolid waste. All materials in thefirst category are solid waste.Materials in the second category aresolid waste unless they are one of thefive exclusions specified in §261.4(a).

designed to helpunfamiliar with thecontrol program towhich, if any, of theshould comply.

Definition of Solid Waste

of the policies andC. Chapter 63 andof providing an

encouraging publicthe efforts of the

a more effectiveManagement Program,

=n furtherancepurposes of 7 Del.in the interestopportunity forparticipation inState towardHaz a rdous WasteDNREC will:

(A) Investigate and provide~~itt2n responses to all citizencomplaints submitted in accordancewi th such reporting procedures as theSecretary may establish;

Where the Administrator of EPA hasciranted a ~u1emaking Petition pursuantto 40 CFR Part 260 §§260.20, 260.21 or260.22, the Secretary of DNREC, may inhis discretion, accept such determination and amend the Delawareregulations accordingly, provided thatt he person whose pe t I tion was grantedcan furnish appropriate evidence ofthe Administrator's action andprovlded further that the Secretary'':,~;:Qrmine3 such action to beconslstent with the policies andpurposes of the Hazardous WasteManagement Act of 1980 (7 Del. C.Chapter 63).

Appendix I. - Overview ofRegulations

(3) Not oppose intervention byany citizen where permissiveintervention may be authorized bystatute, rule, and regulation; and

The Department believes that thereare many people who suspec t , but areno~ sure, that their activities aresubject to control under the HazardousWaste regulations. This appendix iswr Lt t e n for these people. It is

(C) Publish and30 days for publicproposed settlementenforcement action.

provide at leastcomment on any

of a state

If a person has determined thathis material is a "solid waste", thenext question he should ask is: Isthe solid waste I handle a hazardouswaste?

Hazardous waste is defined in§261.3 of these Regulations. Section261.3 provides that, in general, asolid waste is a hazardous waste if:(1) It is, or contains, a hazardouswaste listed in Subpart D of Part 261of these Regulations, or (2) the wasteexhibits any of the characteristicsdefined in Subpart C of Part 261.However, Parts 260 and 261 alsocontain provisions which exclude(§§261. -o». Part 260 Subpart C)certain solid wastes from the

1. Is generated by a small quantitygenerator

definition of "hazardous waste". eventhough they are listed in Subpart D or

2. Is or is intended to belegitimately and beneficiallyused, re-used, recycled, orreclaimed.

3. Is a sludge: is listed in Part261. Subpart D; 0 r is a mixturecontaining a waste listed in Part261, Subpart D.

(

hazardous waste treatment, storage. ordisposal facilities, or (4) acombination of the above. Figure 4indicates that all of these peoplemust notify DNREC of their hazardouswaste activities in accordance withthe Not Lf i c a t Lon Procedures of 7 Del.C. Chapter 63 and obtain an EPAidentification number.

It should be noted that peoplehandling wastes listed in Subpart D ofPart 261 who have filed, or who intendto file an application to exempt theirwaste from regulation under theregulations governing Hazardous Wastemust also comply with the notificationrequirements.

If a person generates hazardouswaste. Figure 4 indicates that he mustcomply with the Part 262 rules. If hetransports it. he must comply with thePart 263 rules. The standards in boththese Parts are designed to ensure,among other things, properrecordkeeping and reporting, the useof a manifest system to trackshipments of hazardous waste, the useof proper labels and containers, andthe delivery of the waste to apermit ted treatment, storage, ordisposal facility.

If a person owns or operates afacility which treats. stores, ordisposes of hazardous waste, thestandards with which he must complydepend on a number of factors, Firstof all, if the owner or operator of astorage facility is also the personwho generates the waste, and the wa s t eis stored at the facility for lessthan 90 days for subsequent shipmentoff-s1 te, then the person must complywith §262.34 of the Part 262 rules.

All other owners or operators oftreatment, storage, or disposalfacilities must comply with eitherthe Part 264 or the Part 265 rules.'I'o determine wi th which of these setsof rules an owner or operator mustcomply, he must find out whether hisfacility qualifies for interim status.To qualify, the owner or operatormust: (1) Have been treating,storing, or disposing of the hazardouswaste, or commenced facility

the personFigure 3

provisions261 rules

Hazardous Waste Regulations

If this is the case,should look at Figure 3.depicts the specialspecified in the final Partfor hazardous waste which:

exhibit one or more of thecharacteristics defined in Subpart C.Figure 2 depicts the interplay ofthese special provisions wi th thedefinition of "hazardous waste". Itpresents a series of questions which aperson should ask himself concerninghis waste. After doing so. the personshould be able to determine if thesolid waste he handles is a hazardouswaste.

For each of these Groups, Figure 3indicates with which regulations (ifany) the person handling these wastesmust comply. Figure 3 also explainsthat, a r a person handles hazardouswaste which is not included in anyoneof the above three categories, hiswaste is subject to the regulationsdiagrammed in Figure 4.

Figure 4 is a flowchart whichidentifies the three categories ofactivities regulated under thecorresponding set of rules wi th whichpeople in each of these categoriesmust comply. It points out that allpeople who handle hazardous waste areeither: (1) generators of hazardouswaste, (2) transporters of hazardouswaste, (3) owners of operators of

construction on or before November 19.1980, (2) comply with thenotification requirements, and (3)apply for a permit under Part 122 ofthese Regulations.

If the owner or operator has doneall of the above, he qualifies forinterim status, and he must complywith the Part 265 rules. These rulescontain administrative requireuents,monitoring and closure standards, andan abbreviated set of technical andclosure and post-closure cost estimaterequirements. The owner or operatormuse comply with these standards untilfinal administrative disposition ofhis permi t application is made. If apermit is issued to the owner oroperator, he must then comply with thepermit which will be based on the Part264 rules.

If the owner or operator has notcarried out the above threerequi rements, he does not qualify forinterim status. Until he is issued apermi t for his faci Ii t y , the owner oroperator must stop waste managementoperations (if any) at the facility,and send his hazardous waste (if any)to a facility whose owner or operatorhas interim status or to a storagefacility following the Part 262 rules.

In order to apply for a permi t ,

the owner or operator must comply withthe procedures specified in Part 122of these Regulations.

It should be noted that theDepartment will be periodicallyrevising the rules depicted in Figures3 and 4. All persons are encouragedto wri te to DNREC to verify that theregulations which they are reading areup-to-date. To obtain thisverification, contact: D~"'REC, 89Kings Highway, P. O. Box 1401, Dover,DE 19903, (302) 736-4781.

FIGURE 1

DEFINITIO~ OF A SOLID wASTE(

Garbage, refuse01" 51-udge

All mat er Lal.sI

Solid, liquid, semi-solid orcontained gaseous material'.>lhich is:

l~ discarded

II

°tr~er

2. served its intendedpurpose

3. a manufacturin~ orminin~ by-~roduct

~

IS NOT ASOLID wASTE

YES I "r''Ul:I J..H ......

i---~·)i'-"---'---'------'

Does ~261.4(a) exclude yourmaterial from regulationunder 7 Del. C. §6304, becauseit is one of the following:1. domestic se~age

2. a~A point source c~scharge

3. Irrigation return flow~. AEe source, special nuclear

or by-product material5. ~~ situ minin~ waste

I!

''III

-,1/

NO

THE MATERIAL IS A SOLID \·JASTEirrespective of whether you:

1 discard it2. use i~

3. reuse it4. recycle it5. reclaiI:! it6. store it or accumulate it

for purposes 1-5 of above

FIGURE 2

DEFINITION OF A HAZARDOUS WASTE

i Does t~e waste exhibit~uny of t~e characteristics

specified in ?arL 261,Subpart C?

Is the solid wasteexcluded from regulation

under §261. 4 (b)?

Is the solid waste listedin P~rt 261. Subpart D.or is it a mixture that

contains a wastelisted in Subpart D?

jI YES

-1aas the waste or mix­ture been excluded from~he lists in Subpart Dor S26l.3 in accordancewith Part 260, Subpart C?

NO

THE 'i-iASTE ISA HAZARDOUS WASTE

(see figure 3)

YES

NO

YES

YES NO

i

\I!I

II\

IIII

I

I-«<

FIGURE 3

SPECIAL PROVISIONS ::OR CERTAI~ HAZ~~OUS WASTE

THE r";ASTE IS AH!\.ZA.1.DOUS WASTE(see figure 2)

YES

(

Is it generated by asmall quantity generator~s defined in §261.S?

NO

Is it ~ntenced to be:8giti~tely and benefi­cially used~ ~e-used,

L8cycled, or =eclaimed?

YZS

'/

YES

NO

It is subject tothe special requi=e­ments of 526 L 5

Therefore. it must beintended to be discarded.

IT IS SUBJECT TO TIlEHAZ~~OUS WASTE REGu~A­

nONS DIAGRAHMED INHG'tJRE 4.

iIIs it a s l.udge or is it i

listed in Part 261. Subpart ~----...;;..-=-------?~

or is it a mixture containin~

a ~aste listed in Part 261, .Subp:1.rt J?

, !

IT IS S~BJECT TO ~~E FOLLOW­ING RLQUIPJ:ME1~S WITHRESPECT TO ITS TRJu~SPORTA­

TIO~ OR STORAGE:- ~otification under Del. C

~6304, 6306, 6307.- Parts 262 and 263

Parts 264, Supparts A through L- Part 263, Subparts A through E.

~nd G. ~t I, J, &~

IT IS NOT SUBJECT TOREG~TI~ATION GOVE~~ING

HAZARDOUS '..JASTE

FIGURE 4

REGULATIONS FOR HAZARDOUS WASTENOT COVERED IN DIAGRk~ 3

All personssubject toChpater 63

who handle hazardous wastecontrol under 7 Del. c.not covered in Figure 3

IINotify DNREcaccording toI 7 Del. C. Chapter 63

&

Obtain EPA ID Number

Owners or Operatorsof,T/S/D* Facilities

rGef\erat:ors

II!iI

I~

Part 262

ITr:mspor ters

II

iIIIII'f

Part 263-v

~262.34 orPart 262

I0/0** who

qualify forinterim status

i!Y

Pa;:t 265

i0/0 who don'tqualify for

Lnter tm statusI

I-}

-Stop operations, if any-Send waste inventory,if any, to a facilitywhose owner or operatorhas interim status, ora permit, following thePart 262 rules

-Apply for permit underPart 122 & resume orcommence operations onlyafter permit is issuedby D~TREC under Parts 122124 and 264.

* T/S/D stands for Treatment, Storage, or Disposal** % stands for ~wners or Operators

Subpart D-Lists of Hazardous Wastes

Subpart A-General

PART 201-IDENTIFICATION Al\l) LISTI1JG01" HAZARDOUS WASTE

Subpart B-Criteria for identifyingthe Characteristics of Hazardous ';.lasteand for Listing Hazardous Wastes

(1) Subpart A defines theterms "solid waste and "hazardouswaste, identifies those wastes whichare excluded from regulation underParts 262 through 265 and 122 through124 and establishes special managementrequirements for hazardous was~e

produced by small quanitity generatorsand hazardous waste which is used,reused, recycled or reclaimed.

Subpart A-General

(2) Subpart B sets forth thecriteria used by DNREC to ~aent~ry

characteristics of hazardous waste andto list particular hazardous wastes.

§26l.l Purpose and scope.

(a) This Part identifies thosesolid wastes which are subject toregulation as hazardous wastes underParts 262 through 265 and Parts 122through 124 of these Regulations andwhI ch are subject to the notificationand requirements of 7 Del. C. §§6304,6306 and 6307.

In this part:

Appendix II-EP Toxicity Test ProceduresAppendix III-Chemical Analysis Test

MethodsAppendix IV-(Reserved for Radioactive·

Waste Test Methods)Appendix V-(Reserved for Infectious

Waste TreatmentSpecifications)

Appendix VI-(Reserved for EtiologicAgents)

Appendix VII-Basis for ListingAppendix VIII-Hazardous Constituents

Hazarof

Criteria for identifying thecharacteristics of hazardouswa s t e s ,

Criteria for listinghazardous waste.

GeneralCharacteristic ofignitabili t y.Characteristic of corrosivity.Characteristic of reactivity.Characteristic of EP toxity.

Purpose and scope.Definition of solid waste.Definition of hazardous waste.Exclusions.Special requirements forhazardous waste produced bysmall quantity generators.Special requirements forhazardous waste which isused, re-used, recycled orreclaimed.Residues of hazardous wastein empty container.

261. 20261.21

261 .22261. 23261. 24

261. 6

261.2261. 3261. -4261. 5

261.10

261. 7

261. 11

261.1

Subpart C-Character1sticsdous Wastes

Section

Appendices

(3) Subpart C identifiescharacteristics of hazardous waste.

(4) Subpart Dparticular hazardous wastes.

261.30261.31

261.32

261. 33

GeneralHazardous wastes fromnon-specific sources.Hazardous was tes fromspecific sources.Discarded commercial chemicalproducts and associatedoff-specification materials,container and spill residues.

(b) Thissome of thehazardous wastesand §6308.

lists

Part identifies onlymaterials which areunder 7 Del. C. §63l0

Appendix I-Representative SamplingMethods

A material which is not ahazardous waste identified in this

"')art is still a hazardous ',.;aste for~urposes of those sections if:

(1) In the case of 7 Del. C.~6310, D~~C has reason to believe':hat the material may be a hazardousmste within the meaning of 7 Del. C.~6302( 7).

if it is discharged, deposited,injected, dumped, spilled, leaked orplaced into or on any land or water sothat such taa t e r t a I or any constituentthereof may enter z he e nvt ronme n t orbe emitted into the air or dischargedinto ground or surface waters.

(

(2) In the case of 7 Del.C. ~ 6308, the statutory elements are-s cab.l t shed ,

~26lo2 Definition of solid waste.

(a) A solid waste is any garbage,~efuse, sludge or any other waste'::iterial which is not excluded under~261.4(a).

(b) An "other waste material" isc~v solid, liquid, semi-solid or-0ntained gaseous material, resulting:'rom industrial, commercial, mining or::.gricultural operations, or from~o~unity activities which;

(e) A "cranufac t u r Lng or miningby-product" is a material that is notone of the primary products of aparticular ",anuEacturing or miningoperation, is i1 secondary andincidental product of t he particularoperation and ',.;ould not be solely andseparately manufactured or mined bythe particular manufacturing or rn t nt ngoperation. The term does not includean intermediate manufacturing ormining pr od uc t which result s from oneof the steps ~n 3. ~i1nufacturing ormining process ~nd' is ~YDically

processed through the next step nf theprocess within a short ti~e,

§261.3 Definition of Hazardous Waste

(3) is a manuf acu r i ng orc.i.ning by-product and s orie t i mes :5i Lsc ard ed ,

(1) Is discarded or is being~ccumulated, stored or physically,'~emically or biologically treated~~ior to being discarded; or

(2) Burned or incinerated,~xcept where the material is beingcu rned as a fuel for the purpose of~ecovering usable energy; or

(3) Physically,~r biologically treated·;'.lrned or incinerated) :'..n::"~."J!' ':0 being d i spo sed o f ,

. ') no t exc Lud ed f r omha za rd ou s ·';;>.ste und e r

(ii) It is listed inhas not been excludedin Subpart D under ?art

of these Regulations.

f '( .. .:... ::

regulation as C1

J:2 fJ L io. ( b; ;"! nd

Su bna r t l)'1ndErOiJ I::ce Li s t s260 SUCJDart C

(i) It exhibits any ofthe characteristics of haza rc ou s wa s t eiden:i~ied in Subpart C.

(iii) It is a ~ixture

of 3 solid waste and ~ hazardous ~aste

that is listed in Subpart 0 solelybecause it exhibits one or ~ore of thecharacteristics of hazardous was t eidentified in Subpart C, unless theresultant mixture no longer exhibitsany characteristic of hazardous ',,;.J,steiden:ified in Subpart Co

( a) A so 11 d wa s t e , as de fine din526:.2, is :1 hazc rd ou s f.<oI":.:1,ste if:

(2) It ~eets J~Y ~: the:ollowi~~ c~iter~~:

liet=. of or

chemically,(other ::han

i s "d i sea rd e d .. 1;­

(and ~ot used,or r ecyc Le d ) :,y

Has served its originaland sometimes is

A ma t e rd a L

abandonedreclaimed

(1) Disposed of: or

(c):"t 15

~e-used ,'Jeing:

( 2):'ntended use'.iscarded; or

(iv) It is a mixture ofsolid waste and one or more hazardouswastes li~ted in Subpart D and has notbeen excluded from this paragraphunder Part 260 Subpart C of theseRegulations; however, the followingmixtures of solid wastes and hazardouswastes listed in Subpart D are nothazardous wastes (except byapplication of paragraph (a)(2) (1) or(ii) of this Section) if the generatorcan demonstrate that the mixtureconsists of wastewater the dischargeor which is subject to regulationunder either Section 402 or Section307(b) of the Clean Water Act(including wastewater at facilities...hich have eliminated the discharge ofwastewater) and:

(A) One or more of the followingspent solvents listed in§261. 3l-carbon tetrachloride, tet-rachloroethylene trichloroethylene-provided that the maximum total weeklyusage of these solvents (other thanthe amounts that can be demonstratednot to be discharged to wast~water)

divided by the average weekly flow ofwastewater into the headworks ot thef ac f Li t y t s wastewater t r e a cmen t orpre-treatment system does not exceed 1part per million or

(3) One or more of the followingspent solvents listed in §261. 31-methylene chloride, l,l,l-trichloroethane, chlorobenzene, O-dichlorobenzene, cresols, cresylic acid,nitrobenzene, toluene, methyl­ethylketone, carbon disulf ide, iso­butanol, pyridine, spent chLoro f Luo rocarbon solvents-provided that themaximum total weekly usage ~f thesesolvents (other than the amounts thatcan he demonstrated not to bedischarged to wastewater) divided bythe average weekly flow of wastewaterinto the headworks of the facility'swastewater treatment or pre-treatmentsystem does not exceed 25 part s permillion; or

(C) One of the f oLlowi ng wasteslisted in §261. 32-heat exchangerbundle cleaning sludge from thepetroleum refLning industry DNRECR~zardous Waste No.KOSO); or

(D) A discarded cO~uercial

chemical produc t, or chemicalintermediate listed in §26l.33 arisingfrom de minimis losses of thesematerials from manufacturingoperations in which these materialsare used as raw materials or areproduced in the manufacturingprocess. For purposes of thissub-paragraph, "de minimis" lossesinclude those from normal materialhandling operations (e.g. spills fromthe unloading or transfer of materialsfrom bins or other containers, leaksfrom pipes, valves or other devicesused to transfer materials); minorleaks of process equipment storagetanks or containers; leaks fromwell-maintained pump packings andseals; sample purgings; relief devicedischarges; discharges from safetyshowers and rinsing and cleaning ofpersonal safety equipment; and rinsatefrom empty containers or fromcontainers that are rendered empty bythat rinsing; or

(E) Wastewater resulting fromLa Dora tory operations containing toxic(T) was t e s listed in Subpart D,prOVided that the annualized averageflow of laboratory wastewater does notexceed one percent of total wastewaterflow into the headworks of thefacility's was t ewa t e r treatment orpre-treatment system, or provided thewastes, combined annualized averageconcentration does not exceed one partper million in the headworks of t hefacility's wastewater treatment orpre-treatment facility. Toxic (T)wastes used in laboratories that aredemonstrated not to be discharged towas t ewa t e r dre not to be included inthis calculation.

(b) A solid waste which is no cexcluded from regulation underparagraph (a)(l) of this sectionbecomes a hazardous waste when any orthe following events occur.

(1) In the c a s e of a wastelisted in Subpart D, when the was t efirst meets t he listing descriptionset forth in Subpart D.

(2) .l.~ the case 0: ,'} mi xr ure'N.:1St2 a nd one or ':lore lis t2d

(pass

fOe:neans

sy s t .:-m·....o r c s

a sewer

"Jo~Qstic

ca s s e s t hrcug h'J u b 2.::' ': I ';-'Y';:1e d

u n c re s teet h rc uz h a

ha za rd oua':'s fi.:-stD

of sol i.ehazardous ',.;'.qstes, when'..a s t e listed ::1 Subpart~dded ~o the solid waste.

(3) In the case of any othervas t e (including a waste rrrixtu!'e),~hen :he waste exhibits any of thec na rac t e r t s t t c s identified ion Subpartc.

<2) I tld:.lstrial wa s t ewe t e rd i s c ha rg e s t;,at are point sourcedischarges subj~ct to regulation underSe c t i on ~02 ·')f :::e C'le a n ~'Tater Act asamended.

(c:) UriLe s s c nd until it meets thec!'it~r~~ of ?aragr~ph (d):

(1) A hazardous waste will!'~~ain n hazardous ~aste.

(2) Any solid '.JasteC';ene r a ted f r om the t re a t men t , s t o r ag eor disposal of. a hazardous Y.Jaste,Lnc Lud Lng any sludge, spill residue,a~h, emission conceal dust or leachate('--t:t 'lot inc l;..;.d iI".!l; precipitation·:-·_~n-o.f·~_)~ is .1. h·-z2.!"doU3 ::.Yaste ..

(COIT"...':'e~t : This e xc Lus Lo n a op lies onlyto t:-:e ac t ua L po Lrrt source discharge.I: does no t exclude industrialwas t ex....a t e r s '>Thile t hey are beingcollec:ed, stoced or treated beforedisc~a:r~e) ~or does it exclude sludges:~1.at a r e z e ne r a t ed by i:1dustrial~<:".0st;?·1a.t.:er t~~r~:e:"'!ent.. )

(3) Irc~02tion return flows.

(.~', »ou rc e , sp ec La I nuc Lea ro r JV-~r0c:~J.ct ma t e r i a I .'35 d e f Lris d by

as

toare

nots o Li d

1.93:',f.L': ·_;.'3.~1I 2011 et seq.

(5) ~aterials subjected~~,~~~ :cchn~~ues which

(~) 3aiid wastes ~hic~ are~a2arco~s ~asteso The f~llowing

~astes 2~~ ~0t ~~zar~ous ~ast~:

the'TIeets; ..

case of any solidexhi ~i. t any of t he

s o Li d -.•a s t e described inJ= ~~~s sect~Qn is ,ot a

:;;ast.e

cae; not

Any( " '\" '- :

'~l) In t net

f'.'"1 ~::''::.;jt).?r

~-..,.z;:.:.?:cif):':.s

c ha rac t e r i s tLc s of ha za rd ou sident~fiec i~ Subpart Co

re used .

~to!'~ci,

('" CT... ·_·6· ,

::ousehold

any wa s t e-, ::':112 :1..!cii!:.~ sar!Jage, t r a s h a nd

·'.n s e o t I c t anks ):O'.1o;;~~(':Ol.et5 ~:'_!"cluding

:;:"':!e.t.::r:, ·:':s?osed, recovered,:-·~":'...:s2-~·~!":'?ed ::'..:el) or.,::0 l..::-::. e "'10 1. d I'·;ast e means

~261.~ ~xclu~ions.

TJJ[3. sees.

(2) !n the case o f a f..;astewhic~ is 2. listed ~yaste ~l::de-r' 3ub:"Jar':':) ~ r.: ()"1 t ~ it! S ~ ::,~.~ S t e ~.: s t:e d < 2 !1C. e rSubpart D') or is d e r i ved :- :"0;71 :} ,:,<C,:lst~=

:"i'3t~-i i.::. Su bn.a r t D, ! ... :-:1..so has :'~e~

eAc.i~-::·~-=~ f r o:n u.s.ragrap:--l r.c) ·.~,::1ce~ :~.?.rt

260 Suo~art C of t~ese ~~gulations.

not solid wa s t e s for t:--te pu rp c s e ofthis Pa r r :

~0mestic sewage: and

(2) Solid wa s t e s ger:,::r:'.tcd:,y e ny of ~he following and YNhic~ .q r~

r~tG~~~d :0 t~~ soils as fert~liz2rs:

(ii) The raising ofnnimals, including animal manures.

(D) Sewer screenings generated bythe following subcategories of theleather tanning and finishingindustry; hair pulp/chrome tan/retan/we t f i nt s h ; hair save/chrome tan/retan/wet finish; r e t a n /we t finish; nobe amhou s e ; t h roug h-it he-r bLue ; andshearling.

(E) Wastewater treatment sludgesgenerated by the fa llowi ngsub-categories of the leather tanningand finishing industry ; ha I rpulp/chrome tan/retan/wet finish; hairsave/chrome tan/retan/wet finish;retan/wet finish; no beamhouse;through-tne-blue; and shearling.

(C) Buffing dust generated by thefollowing subcategories of the leathertanning and finishing industry; hairpulp/ chrome tan/retan/wet finish;hair save/chrome tan/retan/wet finish;retan/wet f i n.t sh ; no be amhous e ;through-tne-blue.

(B) Chrome (blue) shavingsgenerated by the followingsubcategories of the leather tanningand finishing industry; hairpulp/chrome tan/retan/wet finish; hairsave/chrome tan/retan/wet finish;retan/wet r i ru s n ; no beamhouse;through-the-blue; and shearling.

subcategories of the leather tanningand finishing industry; hairpulp/chrome tan/retan wet finish; hairsave/chrome tan/retan/ wet finish;retan/wet finish; no beamhouse;through-the-blue; and shearling.

overburden

the waste isexclusively)

(5) Drilling fluid s ,waters, and other wastes

with the explorationor production of crude

gas or geothermal energy.

(A) The chromium inexclusively (or nearlytrivalent chromium; and

(B) The waste is generated froman industrial process which usestrivalent chromium exclusively, (orne a r l y exclusively) and the processdoes not generate hexavalent chromium;and

(6) (i) Wastes which fail thetest for the characteristics of EP

toxicity because chromium is presentor are 1 i sted in Subpart D due to thepresence of chromium which do not failthe test for the characteristic or EPtoxicity for any other constituent orare not listed due to the presence ofany other constituent, and which donot fail the test for any otherc ha t-a c t e r i s t Lc , 'i r it is shown by ~i

waste generator or by waste generatorsthat:

(4) Fly ash waste, bottomash waste, slag waste, ana flue gasemission control waste generatedprimarily from the combustion of coalor other fossil fuels.

producedassociateddevelopment,oil, natural

(3) Minir..greturned to the mine site.

(ii) Specific wasteswhich meet the standard in (b) (6)(O(A), (B) and (C) (so long as theydo not fail the test for thecharacteristic of EP toxicity, and donot fai 1 the test for any othercharacteristic) are:

(F) ~astewater treatment slucigesgenerated by the following sub­categories of the leather tanning andfinishing industry; hair pulp/chrometan/retan/wet finish; hair save/chrometan/retan/ wet finish; andthrough-the-blue.

(G) Haste scrap leather from theleather tanning industry, the shoemanufacturing industry, and otherleather product manufacturingindustries.

is typically andin non-oxidizing

wasteThe( 0', '>oJ)

frequently managedenvironments.

(A)generated

Chromeby

(blue)the

trimmingsfollowing

(8) Ce~ent kiln dust waste.

(7) Solid waste from t heextration, beneficiation andprocessing of ores and '!lineral(including coal), including p ho spha t erock and overburden from the mining ofuranium ore.

(9) Solid waste whichconsists of discarded wood or woodproducts vhfch fails the test for t hecharacteristic of EP toxicity andwhich is not a hazardous ~aste for anyother reason if the waste is generated1:>;: persons who uti lize the3rsen~cal-treated wood ard woodproduc t s f o r these materials' intendedend us e ,

(c) Hazardous wastes which areexempted from certain regulations. Ahazardous waste which is generated ina product or raw ~aterial storagetank, a product or raw mat e r La ltransport vehicle or vessel, a productor r~w material pipeline, or in amanufacturing process unit or anassociated non-waste-treatment-manuf ac t u r Lng unit, is not subject toregulation under' Parts 262 through 265of these Regulations and Parts 122through 124 of these Regulatio~s or tothe ~otifi cation require~ents of I

Del. Code 630 4 , 6306 & 6307, until itexits the unit in wnlC::' it wa s

gener'\ced, unless the unit is asur f ac e impoundment, or unless t hehazardous waste remains in the ~nit

more tn3n 90 days after :he unitceases to be operated for manuf ac t ur'Lng , or for storage ortranspor-tation of product or raw

(

122 orto the

Do1

is beingfor the

sample isthe sample

The sample issample collector

a laboratory for

The sample islaboratory before

(iv)in a

(i) The samplet r an spo r t ed to a laboratorypurpose of testing; or

(iii)being stored by thebefore transport totesting; or

Parts 262 through 265 or Parts124 of these Regulations ornotification requirements of§§6304, 6306 and 6307 when:

(if) Thebeing transported back tocollector after testing; or

(v) The sample is beingstored in a laboratory after testingbut before it is returned to thesample collector; or

(vi) The sample isbeing stored temporarily in thelaboratory after testing for aspecific purpose (for example, untilconcl~sion of a court case orenforcement action where furthertesting of the sample may benecessary) .

(2) In order to qualify forthe exemption in paragraoh (d)(l)(i)and (ii) of this section, a samplecollec~cr shipping samples to alaboratory and a Labo ra t o ry returningsamples to a sa~ple collector must:

be Lng sto redtesting; or

(1) Comply '..rith U.S.De pa r t rie n t of Transportation(DOT) ,'''':.;). Po s t a L Service (USPS), or anyother applicable shipping rCQuirement s ; or

pigmentsludges

by tr:.e

(H) Wastewater treatnentfrom the production of Ti02using chromium-bearing oreschloride process.

(A) Assure thati~ormation acco~panies

materials.

(d) Samples. (1) Except asprovided in paragraph (d)( 2) of thissection, a sample of solid waste or asample of water, soil, or air, whfchis collected for the sale purpose oftesting to determine its character~_st:'cs or composition, is not subject:~ ;:l:,..... ~equirements of t hi s pa rt; of

f'o Llov.i ngcollectoror otherapply to

(it) Comply wLt h therequirements if the sampledetermines that DOT, USPS,

shipping requirements do notthe shipment of ~he sample:

the f ollowi. ngthe sample:

(2) The laboratory's name,mailing address, and telephone number;

(4) The date of shipment; and

The sample collector'saddress and telephone

requirements of this section.Hazardous waste tha_t is subjec t to thespecial requirements of §26l.6(b) isincluded in the quantitydeterminations of this section and issubject to the requirements of thissection.

(d) In determining the quantityof hazardous waste he generates, agenerator need not include:

theThe quantity of( 3)

samp Le :

(1)

name, mailingnumber;

(5) A description of the (1) His hazardous waste whenit is removed from on-site storage; or

(B) Package the sample so that itdoes not leak, spill, or vaporize fromits packaging.

(2) Hazardous waste producedby on-site treatment of his hazardouswaste.

(3) This exemption does notapp ly if the laboratory determinesthat the waste is hazardous but thelaboratory is no longer meeting any ofthe conditions stated in paragraph(d)(l) of this section.

(c) Hazardous waste tha t isbeneficially used or re-used orlegi timately recycled or reclaimed andthat is excluded from regulation by§261.6(a) is not included in thequantity determinations of thissection and is not subject to any

(0) Except for those wastesidentified in paragraphs (e) and (0of this section, a small quantitygenerator's hazardous wastes are notsubject to regulation under Parts 262through 265 of these Re'julations andParts 122 and 124 of theseRegulations, and the notificationrequirements of 7 Del. Code §6304,6306 & 6307, prOVided the generatorcomplies with the requirements ofparagraph (g) of this section.

§26l.5 Special requirementshazardous waste generated byquantity generators.

(1) A total of one ki logramof commercial chemical products andmanufacturing chemical intermediateshaving the generic names listed in§26l.33(e), and off-specificationcommercial chemical products andmaunufacturing chemical intermediateswhich, if they met specifications,would have the generic names listed in§261. 33( e).

(2) A total of 100 kilogramsof any residue or contaminated SOil,water or other debris resulting formthe cleanup of a spill, into or on anyland or water, of any commercialchemical product s or manufacturingchemical intermediates having thegeneric names listed in §26l.33(e), orany residue or contaminated soil,water or other debris resulting fromthe cleanup of a spill, into or on anyland or water, of any off-specification commercial chemical products ormanufacturing chemical intermediateswhich, if they met specifications,would have the generic names listed in§261. 33(e).

(e) If a small quantity generatorgenerates acutely hazardous waste in acalendar month in quanti ties greaterthan set forth below, all quantitiesof that acutely hazardous waste aresubject to regulation under parts 262through 265 of these Regulations andParts 122 and 124, and the notificaionrequirements of 7 Del. Code §6304,6306 & 6307:

forsmall

A generator is a smallgenerator in a calendar monthgenerated less than 1000

of hazardous waste in that

(.:1 )quantityif hekilogramsmonth.

(g) In order for hazardous waste;e~crated by a small quantity~~ner~tcr to ~e excluded from fullr~=c;uli1tion urid e r this section, the

':·.:-::2:"C:'.;'~JS ;'..ras t e on-site store i..~ in'~~olianc2 with the requirements 0E'.,r,\?",::<, (f) of this s e c t Lon : ( ,,!;1.r1

section 265 Subpart I & J:) and

f

(

re-uses,reclaims

generatorhazardous

qua n t i t y

:;rr;a 11 r;U:1 n tit Yt..as t e ·... i t h ;]

If :l

soLid~'-:.l':

(v) A facility which:

(A) 3eneficially uses orLeg Lt Lrna t e Ly recycles orwaste; or

orh-..~s

( :. )

"71:!.xec: ,i

'/;is tr:

(h) Hazardous waste subject tothe reduced requirements of thisse c t I o n ::l:1.y be mixed withno rr-ha z a rdou s waste and remain subjectto these reduced requirements eventhou0h the resultant mixture exceedsthe r:'uantity limitations identified int h I s s e c z t o n , u n l e s s the ra i x t u re meets.i ny c r t he characteristics ofhn z a rd ou s ·...·;3,sces I d e n t t f Led in SubpartC.

(iv) ?ernie:ed,licensed or =egistered by a St a t e ':0

manage ~unicipal C~ industrial solidwa s t e and ,... h i c h is approved by theDe pa r t me nt; to handle hazardous wastesfrom small quantity generators;

(3) Treats his wa s c e prior tobeneficial use or re-use, orlegitimate recycling or reclamation.

exc Lus i o n :et/~l 1):- ::-:':'3 sections the~::-:t:~rp ~s ~u:-,~~c~ to full r ez u La t Lo n ,

ofwith §262.11

he stores

(1) Cornp Ly:~~se ~egulations.

·~e"":era::or must:

(:) A small qu~ntity generatormay accumulate hazardous waste ons I t e , If he ac cumu La t e s , at any t Lme ,more than a total of 1000 kilogramsof his hazardous waste, or his acutelyha za rdous wastes in quanitites greatert~an set forth in paragraphs (e)(l) or(e) (2) of this section, all of thoseaccumulated wastes for which the~ccumulation liwit was exceeded aresubject to regulation under Parts 262through 255 of these Regulations and?~rts 122 and 124., and the~~t~::cation requirements of 7 Del.C"de §6304, 6306 & 6307. The timepe r i od 0: §262.34 for accumulation .ofwastes on-site begins for a smallquar.tity generator when the~ccu~ulated wastes exceed the3nplica~le exclusion level.

5261. 6hazardousre-used,

Special requireoents·..a s t e ·...hich is

recycled or reclaimed.

forused,

(3) Sither t r e a t or di. sp o s e'): h~..s ~<.1zardous wa s r e i n an on-:::i::e:-'1ci':'ity, or e n su r e c e Li ve r y to .~._

[)~ ~ s :. ~ '? S ~ 0 r 3 g e , : rea t:-:: e n ~ a r ~ i .3 :::0 -: :11.

~~cili~y, eit~er of ~hic~ i3:

PemittedPart

under PartsR.egulations.

( if)122

Inand

under

inte ri::! status265 of these

(;1) '::xcept CiS otherwise providen::1 p a r a g r ap h (j) of this section, ,'1

':2::ardous wa s t e which :r:eets a ny of the:o':lo~·""in~ criteria is no t su o j e c t tot"egul~tion un~er Parts 2S2 through 2~5

0f ?arts 122 through 12~ of these re--uLa t Lou s and i.s no t sub i e c t to the:1otification require~ents of -: Delo C.556304, 6306 and 6307 un t i l s uc h tbeas the Secretary Dromulgatesregulations to the contr~~::

(iii) Authorized to~an~ge hazardous waste by the De~a~are

~~izardous ~l'aste ~fanagement Pro g r.am.rnc ro ved under ·~O CPR ?:t:-t 123;

( L) It is jeing be ne f Lc La Ll y usedor reused or legitimately recycled orrecl~iI':i.ed•

(3) it is one of the followingmaterials being used, reused, recycledor reclaimed in the specified manner:

(5) Applicable provisions ofSubparts A through L of Part 265 ofthese regulations.

(4) Applicable provisions ofSubparts A through L of Part 264 01:

these regulations.

(2) Part 262 of theseregulations.

(3 ) Part 263 of theseregulations.

container or anfrom a containerhazardous waste,is a compressed

identified inRegulations, is

(0)(1) A

inner liner removedthat has held anyexcept a waste thatgas or that is§26l.33(c) of theseempty if:

(ii) no more than 2.5c e nr Lmet e r s (one inch) of residueremain on the bottom of the containeror inner liner, or

(i) all wastes havebeen removed that can be removed usingthe practices commonly employed toremove materials from that type ofcontainer, e.g., pouring, pumping, dndaspirating, and

(11i)(A) no more than 3percent: by weight of the totalcapacity of the container remains int:he co n t a I ne r or inner liner if thecontainer is less than or equal to 110gallons in size, or (B) no more than0.3 percent by weight of the totalcapaci ty of the container remains inthe container or inner liner if thecontainer is greater than 110 gallonsin size.

(2) Any hazardous waste ineither (i) a container that is notempty or (ii) an inner liner removedfrom a container that is not empty, asdefined in paragraph (b) of thissection, is subject to regulationunder Parts 261 through 265, and Parts122 and 124 of these Regulations andto the notification requirements of 7Del. Code 6304, 6306 & 6307.

(a)(l) Any hazardous wasteremaining in either (i) an emptycontainer or (ii) an inner linerremoved from an empty container, asdefined in paragraph (b) of thissection, is not subject to regulationunder Parts 261 through 265 of theseRegulations or Parts 122 or 124 ofthese Regulations or to thenotification requirements of 7 Del.Code 6304, 6306 & 6307.

toofand 124

respect

dccuillula~eci,

chemically orprior to

or legitimate

122with

Notification7 Del. C. §§6304,

(1)requi rements under6306 and 6307.

(b) Except for those wasteslisted in paragraph (a)(3) of thissection, a hazardous waste that is asludge, or that is listed in §§261. 31or 26l.32, or that contains one ormore ~azardous wastes listed in§§261. 31 0 r 261 • 32 : and t hatistransported or stored prior to beingused, reused, recycled, or reclaimedis subject to the followi~;

requirements with respect: to suchtransportation or storage:

(6) Partsthese Regulationsstorage facilities.

(2) It is beingstored, or physically,biologically treatedbeneficial use or re-userecycling or reclamation.

(i) Spent pickle liquorwhich is reused in wastewatertreatment at a facility holding aNational Pollutant DischargeElimination System (NPDES) permit orwhich is being accumulated, stored, orphysically, chemically or biologicallytreated before such reuse.

§261. 7 Residues ofempty containers.

hazardous waste in(2) A container that

held a hazardous waste thatcompressed gas is empty when

hasis a

the

?ressure in the container approRchesa r mo sphe r Lc . be:

( ? \, - J The c!laracteristic can

(3) A container or an innerliner removed from a container thathas held a hazardous waste identifiedin §261.33(c) of these Regulations isempty if:

(i) the container orinner liner has been triple rinsedusing a solvent capable of removingthe ccmmercial chemical product or~Qnuf~ct~~in~ c~p.~ical i~ternediate;

(i) i1easured by anavaila01e standardized test methodwhich is reasonably within thecapability of generators of solidwa s t e or private sector laboratoriesthat are avai:able to serve generatorsof solid waste; or

(ii) Reasonablydetected by g e ne ra t o r s of solid •...a s t ethrough their knowledge of their waste.

(

(i L) the containe r orinner liner has been cleaned byanother method that has been shown inthe scientific Lf t e ra t ure , or by testsconducted by the generator, to achieveequivalent removal; or

(a) The S~cretary shall list a301ic! waste as a hazardous waste only-rp ort determining that the solid waste~eets one of the following criteria:

(iii.) in the case of ::;.

§26l.l1 Criteriahazardous waste.

fo::- listing

5261.10 Criteria for identifying thecharacberistics of ~zardous ~aste.

hazardous waste in Subpart C o n l y '.-:::'cn

cete~i~tn~ that:illness.re ve r s Lb Le ,

(1) :!:t exhi hi ts any of thecha r ac t e r i s t ic seE hazardous waste:.dent~fied in Subpart C.

(2) It has been found to beE'l':al ':0 humans in low do s e s or, in':he ~bsenc2 of data on human toxicity,~ r h2S J~e:1 s ho-vn i n studies to have~~ o ra I :".J 50~cx:ici:y (rat) of less:~~~ 38 ~illigr~ms ~er kilogran, an~~h~lat~on LC 50 toxicity (rat) of~'2ss t han 2 ::.illigrams perl.ite:a, or 2

ce~al LD 50 toxicity (rabbit) of less~~3n 200 ~illigra~s ?er kilo~ra~ or is~:~er~ise capable nf ca\!sing orsignificantly c:ontriJuting to an:~c~~~se in serious :r~eversible or

~ t ne ri nne r

Secretary shall identifya cha rac t e r i s t i c :)'"

thecontact of :~e co~~e~C:3~

produce or ~~nufac:~~~~~

intermediate Nith ~~~

has been removed.

(a) The8.nd define

c ori t a Lne r ,prevented

, • 1cnemlca.:..che!!lica2.container,

Subpart B-Criteria for Identifyingthe Characteristics of Hazardous ''';aste::nd f o r !.isting i!::l.zarcous :;';as~e

(ii) Pose a substantialpresent or potential hazard to humanhealth or the environment when it isimproperly treated, stored, cransported , disposed of or otherwise nanaged :unJ

(3) i>- c orit a.i n s a ny of thet ox i c c or.s t i t ue rrt s Li s t ec i.n Appendixr.~III unless, ~£~e~ c ons td e r t ng ;1~Y of~~e :01lowing f2ctors, :hc Secretaryc onc Lud e s that the ~aste is no t

~apable of 70sing ~ substantialp r e s errt o r po t e nt i.a L hazard to humanhe~lth 0r the environ!!lent ~hen

impro?er~y treated, stored~

of,disposedort r ansp o r't e d

':0 ~J 1""'1

::'nc:-easeLnc ap ac ;

significant~y contribu:eincrease in mortality o r anin serious irreversible, ortati~g rGversible illness; or

(c) The Secretary will use thecriteria for listing specified in thissection to establish the exclusionlimits referred to in §261.5(c).

(b) The Secretary may listclasses or types of solid waste ashazardous waste if he has reason tobelieve that individual was t e s wi thinthe class or type of waste, typicallyor frequently are hazardous under thedefinition of hazardous waste found in7 Del. C. Chapter 63.

(i) The nature of thetoxicity presented by the conscituenc.

(ii) The concentrationof the consticuent in the waste.

(iii) The potential ofthe constituent or any toxicdegradation product of the constituentto migrate from the waste into theenvironment under the types ofimproper management considered inparagraph (a)(3)(vii) of this section.

(iv) The persistence ofthe constituent or any toxicdegradation product of the constituent.

(Wastes listed inthese criteria willToxic wastes.)

accordance withbe designated

(viii) The quantitiesof the waste generated at individualgenerations sites or on a regional ornational basis.

(vi) The degree towhich the constituent or anydegradation product of the constituentbio~ccumulates in ecosystems.

(ix) The nature andseverity of the human hec l.t h andenvirolli~ental damage that has occurredas a result of the improper managementof wastes concaining the constituent.

(x) Action taken byother governmental agencies orregulatory programs based on thehealth or environmental hazard posedby the waste or waste constituent.

of

§261. 20 General

(a) A solid waste, as defined in§26l.2 which is not excluded fromregulation as a hazardous waste under§261. 4(b), is a hazardous waste if itexhibits any of the characteristicsidentified in this Subpart.

(b) A hazardous waste which isidentified by a characteristic in thissubpart, but is not listed as ahazardous waste in Subpart D, isassigned the DNREC Hazardous waste~umber set forth in the respectivecharacteristic in this Subpart. Thisnumber must be used in complying wi ththe notification requirements of 7Del. C. §§6304, 6306 and 6307 andcertain recordkeeping and reportingrequirements under Parts 262 t hrcug n265 and Part 122 of these regulations.

(c) For purposes of this Subpart,the Secretary will consider a sampleobtained using any of the applicablesampling methods specified in AppendiXI to be representative sample withinthe meaning of Part 260 of theseregulations.

Subpart C-CharacteristicsHazardous Waste

(Comment; §262.11 of these Regulations setsforth the generator's responsibilityto determine whether his wasteexhibits one or more of thecharacteristics identified in thisSu bpa r t )

plausibleto which

(v) The potential foror any toxic degrad

of the constituent tonon-harmful constituents

of degradation.

(vii) Theimproper managementcould be subjected.

the constituenta c i on productdegrade intoand the rate

types ofthe was t e

(xi) Such other factorsas may be appropriate. Substanceswill be listed on Appendix VIII onlyif they have been shown in scientificstudies to have toxic, carcinogenic,mutagenic or teratogenic effects onhumans or other life forms.

(b) A solid waste that exhibitsthe characteristic of t gm t a bt Lt t y ,

but is not listed as a hazardous wasteI n Subpart D, has the DNREC HazardousW~ste Number of D001.

(Comment: Since t he Appendix Isamp Li ng methods are not beingf orrnaLl y adoptee by the Secretary, aperson who desires to employ analternative same ling method is notrequired to demonstrate theequivalency of his method under theprocedures set forth in Part 260Subpart C.

§261.22corrosivi ty.

Characteristic of

(

(a) A solid waste exhibits thechar~cteristic of ignitability if arepresentative sample of the waste has:lny of the follow~ng properties.

(2) It is not a liquid andis cap~ble> under standard temgeratureand pressure, of causing f i r e throughf r t c t on , absorption of no t s t ure 0:"

spontaneous chemical changes and whe n~gnited burns so "rigorously a ndpe~sistently ~ha~ it creates a hazard.

(1) It is a liquii, otherthan an aqueous solution containingless than 24 percent alcohol by volume~nd ~as flash point less than 60degrees C (140 degrees F) , asdetermined by a Pensky-Martens ClosedCup Tester, using the test methodspecified in AST:"f Standard D-93-79 orD-93-30 (incorporated by reference see§260.1l), or a Setaflash Closed CupTe s t e r , using the test methodspecified in ASTM Standard D-3278-78Uncorporated by reference, see5260.11), or as determined by anequivalent cest method approved by theSec::.-et3.ry under procedures set forthin Part 260 Subpart Co

( 2) I tis a li quid a ndcorrodes steel (SAE 1020) at a rate'sI"eater than 1).35 ::lm (0.250 inch) per

'7:ethod

()[ 55~) a.s

tQ!:!Derc:l~Ure

degreesthe t e s t

It ~s aqueous a nd has aore q ua 1 to 2 0 r g re ate r

by

test

(1)

p H less t ha n

(2.) A solid waste exhibits thecharacteristics of corrosivity if arepresentati "Je s arnpLe of the waste haseither of the following properties:

3peci£ied in XACE (~ational

Association of Corrosion ErizLne e r s )Standard ~1-0l-69 as standardized in"Test :'~ethods for the Evaluation ofSolid Waste, Physical/Chemical\':ct~ods" (incor~orated b:v" r e f e re nc e ,see j260.1l) or an equivalent ~est

~ethod aporoved jy the Secretary underthe o r oc edu r e set forth ).'1. Part 260SubDar: COl

year 2t acegrees Cdetermined

than or equal to 12 05, as determinedby a pH meter us:n~ either an EPA testmethod or ::In ecuivalent test methodapproved by the Secretary under theo rocedu re s set forth In Part 260Subp~rt C. The EPA test ~ethod :-or pHis specified as :1ethod 5.2 in "Test:1ethods for the Evaluation of SolidWaste, Phy s I c.t Lz Chemfc a I ~'!ethods"

(i.ncorporated by re f e r e nc e , s ee

§260.11).

ofCharacteristic§261. 21Ignita bili ty •

(3) It is an .:'snita:'le,c ornp re s sed gas a s defined in 6.9 C?R173.300 and 3.S deter:tined by the testmethods described in that regulationo. equivalent test methods approved bythe Secretary under Part 260 Sub9art C.

('0) A so Li d was t e that exhibitst he cha rac teristic of c o r r o s I vi t y , butis not 2.isted ,-:15 ;'1 haza rdous was t e inSubpart D, ha s the DN'REC Hazn rd ousWaste Numoer of D002.

(4) It is an oxidizer asdefined in 49 CFR 173.151.

§261. 23reactivity.

Cha rnc teris tic of

(a) A solidcharacteristic of

waste exhibitsreactivity

~epr~sentative ~a~?le of the Haste h~~

~'Y of t~e followin~ oro~e~t~es:

(3) It forms potentiallycXJLosive ~ixtures with water.

(1.) Ie is no rrna l Ly uns t ao.l eand ~e2djly undergoes vioi~nc changewit~out detonating.

(4) When :nixed with water,it ~ener2tes toxic gases, vapors orfu~~s in a quantity sufficient topresent a danger to human health orthe an vi ronment.

'J.SLE I -MAXIMUM CcNCENTRATlON OF CON­

rA/oliNAHT$ FOR CHARACTERISTIC OF EPTOXiCITY

(b) A solid waste that exhi bitsthe characteristic of EP toxicity, butis not listed as a hazardous waste inSu bpa r t 0, has theDNREC1Iazardous WasteNumber specified in Table I whichcorresponds to the toxic contaminantcausing it to be hazardous.

representative sample of the wastecontains any of the contaminantslisted in Table I - at a concentrationequal to or greater than therespective value given in that Table.Where the waste contains less than 0.5percent filterable solids, the wasteit self, after f Ll t e r Lng , is consideredto be the extract for the purposes ofthis section.

It r e ac t s violently with( ? \~)

(5) It is a cyanide orsulfide bearing waste which, whenexposed to pH conditions between 2 and12.5 C2n generate toxic g a s e s , vap o r sor fumes in a qua n t Lt y sufficient too r o se n t ;1 d.3.n~2r to hunan health ort:;2 crivf r onme n t .

(0; It is c~rable ordetonation or explosive reaction if itis subjected to a strong ~nltiating

source or if heated under confinement.

~b) .~~ Jolla wa s t e ~f:.u.t a xhLb Lt sL:'"1E c h.s r a c t e r i s c i c or r e a c r f v t t y , butis no t 1.1.3ced a s a hazardous waste ir;Su bpa r t :J, .ia s t:,eDNREC Haza rd cus ~,last:e

Surabe r 0:'- uG03.

(3) It is rt forbiddenexplosive as defined in 49 CFR 173.51,or a Class A explosive as rie f i ne d in!t9 C?~ ':73 .. 5J o r 3. Class E cxp Lo s i ve

as dcfinrd in 49 C~R 173.88.

10

os

100

10.0

2.017

DOtS

D01J

,-,~.. ... i~~ ·..· 1 solXoO'>..... : 8"""", ..; 1000c:~ " lC~ I 10rror ; 0w'0mlum.. ..::::':1 so,))Co/! " ; L"'<l . ·" " .." "_ ".,, 1 5.0

~ ". "!~ ". "":"'''':':.:'' :::.. "'.1 ~ ~~:; I~"(·;:2:3:4·:;·ii:';O~.1 so

I 10<0-1.1__, 0.02

i 1."'a,5.&J,a,~I 1, • ...-.00. ..-.00-5.8-0_i &r<>naoI>~

...!~ P.2.J,4,5.&-NI... cNor,, ~.Ilt"e. Olr'nn'\ll 1Ol'nfIir. I'~"",h<ot (I.1,1.7""~I"",,";

1 2.2-00. (po""""""""' .: p..~l.t"-Ml. ;, TOr8()l"\~ 'C.~H,,,o.. T~S( i

cNor'W'1Al'IC ~'I~. d7-€.; :;>fVC~ cr-.lQr.ne)

.. 2.'-0 '.2,'- iJ.,:;-.:oroc~ryt!C~ -.c-I('!l

.2.4 S rp 'Y.~ i"..c .r,'>1Ct"'JIO-;

"''''''''''''''':>'CJ<lOO<'oC 000,

Dl'."'REC!!'lcla.rooue I

."~f' 1,..,."".

It is r e ad i l y capable orexplosive decomposition

at stanrlard temperatureor r c ac t I o nand pressure.

(7)

c e t ona t t on or

(::i) A solid waste exhibits thecharacteristic of ;::P t ox i c i t y if,using the test methods de~c,ibed inAppe nd i x II or equivalent methods

§261. 24Toxicity.

approved byp r oc e d u r e sSubpart C,

Characteristic

t he Sec r e t a rvset forth :n

the extract

of

under

rzoom

EP

the260

Subpart D- Lists of Hazardous Wastes

§26l.30 General.

(a) A solid waste is a hazardouswaste if it is listed in this Subpart,unless it ha s bee n excluded from thislist under Part Z60 Subpart C.

(0) The Se<:retar;· '...ill Lnd l c at e

his ba s i s for I is t t ngtypes of ~astes listedby' emp LoyI ng one orfollpwing Hazard Codes.

l<JM_w ..~W""I.Q~-:T1"V'A W.1tct . . _.........•.........

FP r" w:W."'" _ .Jw::ut4 H"l'lI"r'rJlJ! W~I1.

Tnne 'Nl"!qt"

the c La s s es Or'

in this Subpartmo re of the

ADpe~dlx VII identifies theconstituent '""hich caused the Sec re t a ryto list the waste an an EP Toxic Waste(E) or Toxic '..Taste (T) in §§261. 31 and2111. 32.

(c) Each hazardous was t e listedin this Subpart is assigned a DNREC:~.1z~rrJous Waste Number ,.•hi c h p r ec ed e s':'1e name of the was t e , This number~ust he used in complying with the~otification requirements of 7 Del.C. §6304, 630(, and 6307 and certainr ec o rd keep Lng and reporting7e0uirements unc~r Parts 262-265 and?art ~2: of these regulations.

(d) T1:e following hazardous~astes listed in §261.31 or §261.32a re s ub j ec t to the exc Lus t ori limi tsCor rtcutely hazardous wastesesta~lished in §261.5.

~lry and h.&z.,6ous 'I~.8S'- "'0

r ---.I I-!.:uard

_._----------~~--

Fro3

rOO5.

rooe

;:019.FOOl.

FOO9

FOtO

FOil

FO'2

ji The I~Q~ hil~!ttoe:' ~..."l, v!ooed." d(oQ"p.S'''Q t~lrach5("lt~1".,..lp~ i (i)f tf1.chol(wOf"I~. 1'n(I~~ ~ I It IncNort'l'e'lh",....... r:.:rtxw-s Irlt.cn10'..,.... iI 1M c"Iof",.,rd "'vorOl'"...arnon..-r. ,l'"\CJ ,lvdg-tt'J frO"" l~ rKOV""" ni f'No"l;l!' ~,."''l n I

{~9(t"lt'l:ng oPftfllJOon'\ I

j Tt\e 'n"""""l •o..." halo9""*'f'<! _ .. '~"ac~",,''''''~'''' ""',""''''.....c_ I (T)ltacr';orOftlt¥~ne. 1.1.f.~t"f'tT\.I". ~obc!nzPt"fle. ,.1,1·tne:~ ..~1.2.Ztntkxw· i

f a.m,,,.. ()t1hQ·d-c"'"otot)rrllflnof and tnc"~ofIuot~I"'.""" and 1M a"" OONomt IIrom the ,t!tC.OYtot"y ot fho8.....~t! l'

T'htI foHowtng ~p."t non h.a~'f'd~lS wytf!l"fI .c~l~. f"thyt aceLall!'. ethyl fit~nlf"\€'. f!fhyt .,Nw I'nf'tnyf~il:.l~ "·butyl .te~. CYC~t.a~. andmethanol lno th4i 'l:NC b(ttlO"1!!1 "'om th4ar~ of U"'l'f'U' JOh'tt1"'f'l :

The~ t.()il'fn' non-n.~.'«f SO'v'f.."H1 CT~sol'S and ern"'..: 1m. Ind t fT)l"lII'ttobflntP~; and rtWl I'tI'! OO"O-!I hom ~ reeov'")' ot l~'" SOl"v"nlf, I

The lottowtnq ,,!)4tni non-l'Ui~~fIId"""""~, 1~r'WJ. ~1""" f'lh¥, k"'lone. urbon f (I. 1)d'!uthrifIi. ~1Iint;;f and~. anet """ sllft bonom!l ftom the 'f'COYt!'f"V of fheSft I~~t I'

""' Wa,lIhwllttr "".lmftl"'lt 'l~ to-om @loKtroofl"""9 oPf"31.l()n'l "wcP't)l from fh«: mI

~oi"o*"'9 OfocP.''!I!eS t n tui"t\.rc 100 lnootttnq of aiurTlrnum. '2') lin plltlt\Q en 1CtVtIon st..: C3l ttnC "'Iunc;) f""7~alf'd e..lIsl on ca:'bon \.I~l. i.el Ih,Jt""'"lJm r:- f

I nnc·~ D1abng' on c.art;:licn ,t~: cs, e6ea"""9/l~ a~!oOO&led Mlh brI, I, 210<: and aU'nInum pteW"9on CW"'t)()tt Sl..... I.nd f6t ~f 181etwnQ .nd ml'l~ of II a~ I\ WU1••I\!tw fr1tafmJ!Wtis~~~e~ ~~'Ofl CI::l>al",? of l~l"iI.)I1\ i (n

.j .5c>dnl C'Ylntd~ 011''''''9 baM ~-:x:nt: tTorn P'!Pctl'~alW"'oQ ClO'RfI~ (a.ceol lOt i {A, nI ,''',c''''-'' "",'al. fM<:b'O(lla""9~ cya.- ""1JnV b.",~l \

..... ·...1P'faf"'9 balh l"udqfts fron'l "'- bon:m of plebnQ batM from ItleCttooil'btwJ ()pf"t~t,.w.)n, ; fRo T}whtMlIt evano6As af.~ .., in. O'OCM.s fne-Ql for S""CJOV'I ~lal'l eJectloof,;auno I

i ~I""" bAlh """"""1 '! $of,nl 1tr~ litllj CtlU!t"lonQ ~:"'" ~tIO"'& trom ~lrr-;>lflllJnq OOt'f~tJOt1'\ ~ft tR,lti C'ylnoce....~ tr!~ ~ thoI~ (nct!'P1 for pt~ metJIls ai1l'l'C"ootaUt"'O ospenf

, S""""",,? end ~''''''':I bath~I..f Ou«r-.:~ balh :;~ "'om oi t-Ilhl hom """"lsl hell bf'llrnq ooerlhO'" wt\fif'{'l ~. n

I C"'f8N1j4t'l". ~~ .., tN~ (~.~ 'er preoclOU' ~1 ..1, h.ftlllb~811t'lQ

! qupnchtng bath s~!I1 I

......,' Sow"' CYI,...j.e 8O'~Jh(""'" hom s&'! hath pot c1"If"lM'l(} /'tom tT"4U:1 1'\0.1 1I@11""'9\fAnop.et'll~ «flYC1'\'Pf f()t prfICc::JuS .....,.r.f1; htoal tr.lllnq !>O"Wlt cyan.o. ~t.",~ from I

lunbllh~c~.~J !...i~~ • .,1....1.. bellmllJnt P~!1 from rnefJ;1 helt U.,lbntJ 00.-.,.hon1 .h9tl!t I(T)I cyIntdt't1 ate u-!flod .., ~ ~, (exef!pl k::Jr preoous """Lal,, ~Il tt .. ll"",;I ~""f1Q .lstftWalIW tT"et1hPnt ~s. I

§ 261.32 HszardoUR wasteR (rom Rpedfic .ource~.

lnduo"Y .nd haz~ i~tf .. No '

-----------------------0:----

lnotQ.an.c~IIKOO2 .

i<oo3 __

K~

X.OO5,.Kooe

K0071<00S

Cn;;.n"C chem.cai,KOOIl __

KOIOKOll .K013 __

: oo!1om ;...-iomenl sh.Jd.J18 from fhr8 tf'61l'T\oe'n( of ""''IStf''WfIllillWS !'rom wood lXft'~t'oQ i en; Pi'0C'ft,~'" lhal lI4I4 crf'loO~l. a~ ..01' p"nlachlcw()(lf'WJnc)l I

____ -' W.......,......~.."""" '''-'''9<' In:rM .... P'OdvCtJon 01 c"'~ Y-"o .. and ",.~. : (T)I ~,. 1

.1 W!!l:lewlilltf tlelf"'i!"nl~ hom ttl4 t"oducl.<m of ~el. orl~ p.~nl! .; rnI W8'!le"'l!l~f tf •• lrTWIn! ..~ trom ~ ptoaucllOn of line .,."llOW D'?rn~t1: : '.1")

.......; W.'I~wIl"" tresl",.. n! ,~ frtln't tr'Je prOOucf..w::)n 01 c~~e QI'~n ~"'I' iT,.. ....i W.slewalet lu)alrTWltnt .It.rlge frOt'" "... P'~ 01 chro""", o ...~s ~.,.n ptorn~nl' rn

I :."""",,,,,, 1M """'.,"'""j' W.,tftwIlttf 1'~.'rnfllOI a~ tr()m t""IIfl' PfOdoc'bOn 01~ t-r......, poq~l'. Ow." tl.1(Jvft from rna pt'0C'\.lctJ()n ef c:nrom.e o~ r:re-en ptQmftof'\tl,. J Qr,ftH.,l(')n bO'f1("lm'J 'f~ lhe~~ acet.a'd-ehvde ",om ftl1"ry'l"'f\4. m...!L)~I,n"JQn ,"';'8 cuI. 110m ~ ,.odt..Jc'~ Of tca!t/lhiel"PyC" f'forn ttrr-rytel"lo4 _... iT}I BO!fnrn tl'e811"! from fhiol .I~I-II ..s~ ..., f1'l" prOOV-!I()M (')r .C"",.,.onltrill 11=4, nI Bot!C'lm 11' ...'" from :,.." "C ..,~ ("1"ltul"nn !"I"I "'" C"'M,""!l1')'" Oi t!'ryi')n"!nft> r:':l T)

~n'tr-'l. 'r1"'...... , ....., "r"ll'"oNt',,_ 0'"1..-::\1""",,, r::n"''''''' .n INit ~OOUC'"'" {'II ACfVi(W"'ll,,~

:-.! ~I I"".~f'll't.~ Ifll'" 'f\(to r":1"1,'!,,ilt'" '." ~~l • ~''1'f'r1n

....'?I'IYy .t"ft'l ('fI 1:'OI!'II""I!It ..... ,ro .. 'C"1!...... I,,,,,,, II,p :'Yf<!o!!xllO~ "f C~!~ !~I't':C!"!~!rl~

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The following materials or itemsarc hazardous wastes if a nd when theyare discarded or intenaed to bediscarded:

(el) Any commercia.l c heml c a Lproduct, or manufacturing chemical.i nt e rmed La t e having the generic namelisted in paragraph (e) or (f) of thissection.

(b) Any off-specificationcommercial chemical product ormanufacturing chemical intermediatewh i c h , if it met specifications, wou Ldhave the generic name listed inparagraph (e) or (f) of this section.

(c) Any residue remaining in acontrtine. or an inner li~er removedrrom a container that has held anyco~mercial chemical product ormanufacturing chemical intermediate.'havlng the generic name listed inpa r ag r ap h (e) of this section, unlessthe container is empty as defined in§261.7(b)(3) of these Regulations.

theirWaste

wastes andDNREC Hazardous

[Comme n t :

regulatedhaz a rd ous

:'hesecorrespondingNumbers are:

For the convenience of thecommunity the primary

properties of these materials r.ave been indicated by theletters ~ (Toxicity), and R(Reactivity). Absence of a letterindicates that the compound only islisted for acute toxicity. J

any land or wa t e r of any commercialchemical product or manufacturingchemical intermediate having thegeneric name listed in paragraph (e)or (f) of this section, or any residueor contaminated soil, water or otherdebris resulting from the cleanup of aspill, into or on any land or water)of any off-specification chemicalproduc t and manufacturing chemicalLn t e rmad La t e which, if it metspeclIlcations, would have the genericname listed in paragraph (e) or (f) •

(e) The commercial chemicalproducts, manufacturing chemicalintermediates or off-specificationcommercial chemical products ormanufacturing chemical intermediatesreferred to in paragraphs (a) through(d) of this section, are identified asacute hazardous wastes (H) and aresubjec t to the small quantityexclusion defined in 261.5(e).

Discarded commercialproducts off-specification

container residues, and spillthereof.

[Comment: Unless the residue isbeing beneficially used or reused, orlegi timately recycled or reclaimed; orbeing accumulated, stored, transportedor treated prior to such use, re-use,recycling or reclamation, EPAconsiders t ne residue to be I n t e ndedfor disca~d, and thus a hazardouswaste. An example of a legitimatere ru se or the residue would be wherethe residue remains in the containerand the container is used to hold thesame commercial chemical product ormanufacturing chemical product ormanufacturing chemical inte~ediate itpreviously held. An example of thed I Beard of the residue would be wherethe drum is sent to a drumreconditioner who reconditions thedrum but discards the residue.]

§261.33chemicalspecies,residues

(d) Any residuesoi I, water or otherfrom the cleanup of a

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Cf) The ~ommercial chemlcalproducts, manufacturing chemicalintermediates, or off-specificationcommercial chemical products referredto in paragraphs (a) through (d ) ofthis section, are identified as toxicwastes (T) unless otherwise designatedand are subject to the small quantityexclusion defined in 26l.5(a) and (f).

[Cornmen t : For the convenience of theregulated c omrauni t y , the primaryhazardous properties of thesematerials have been indicated by theletters T (Toxicity), R (Reactivity),I CIgnitability) and C (Corrosivity).Absence of a letter indicates that thecompound is only listed for toxicity.]

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Appendix:!echocis

I-Representative s8mpli!1g

~~ast~,

ponds,- "?ond:1e t hc d s

The met~ods ~nd equip~ent used forsampling waste ma t a r La Ls r... ill va rywith the form and cosistency of thewaste ma t e r i a Ls to be sampled.Samples collected using the samplingprotocols listed below :or sampling'..;aste with properties similar to theindicated materials, will beconslder0ci by the Department to bercpr~sent~tiv~ of the ~aste.

S:~~-:-0mel:; viscous liquid-AST.1S'::;;."d;;ta ~140-70 Crushed or powde re d"'~tct~n:-ASr1 St3ndard D346-75 Soil or::"oc'-(.-li'.:e :caterL11-ASTX Standar-dJL.;::i)-;~9 Soil Li ke mat~ri.:II-AST:~

St~nd~rd DI452-~5

?J..? ,\c;h-like materi.;ll-ASTI1:~ ':..'0 ~Qa n' J:2J~-76 (ASTM Standards rl re~~~,f:1;~12b~2 ::,:,om :\S'I:1, 1916 Race Street,o~~12~el~~!~. ?A 19103)

Con t·::i ne::-:' zed Ii cu i d '..las t e s-'$:':!';L:~TASA" Desert ~~r;d in "!I~st ~~ethods

for the ~vaulation of Solid ~H-5638

~aste, ?~yslcal/Chemical ~ethods*,

Uc S ~ Env i r onme nt a i Pro t e c t ion A~ency,

~H-565S Off:ce of Solid ~2ste,

Washi~gton~ D.Ce ~O~60

~tq~:d w~ste in ~it~,

Lazooris , 0.'1d :::lr:ti.l;lr r e se vo Lr sS.'1'.:1?ler" de sc r i be d i.n "Testfor tje Eval~~c1on or Solid?~ysical/C~e~ic0~ ~ethods.~

(

~~c ~anual ~lso

s:.:!dit:G71~l }.nfcrmation o ncontai:1s

C1Pplication

i-tHznrrjous "Jaste Streams ..60012-80-018. January

"::;PA

1980.

Appendix II - EP Tox fci.ty TestProcedures

A. Extrac~ion Procedure (EP)

1. A representative sampleof the waste to be tested quinimumsize 100 grams) shall be obtainedusing the methods specified inAppendix I or any other method capableof yeilding a represen~ative samplewithin the meaning of Part 260. (Fordetailed guidance on conducting thevarious aspects of the EP ToxicityTest see "Test Methods for theEvalua~ion of Solid Waste, Physical/Chemical ~1ethods" incorporated byreference, see 9260.11).

2. ~,e ~ample shall beseparated into its component liquidand solid phases using the method de­scribed in "Separation Procedure" b e Low ,If the solid residue obtained usin~ thismethod totals less than 0.5% of theori6inal weight of the waste, theresidue can be discarded and theoperator shall treat the liquid phaseas the extract and proceed i~mediately

to Step 8.

The percent solids isdetermined by drying the filter padat 80 degrees C until it reachesconstant weight and then calculacingthe percent solids using the following2Cjuation:

% solids = (weight of pad + solid)- (tare wei~ht of Dad)

initial weight of sampleX 100

3. The solid materialobtained from the Separation Procedureshall be evaluated for its particlesize. If the solid material has asurface area per gram of materia1 2equal to, or greater than, 3.1 cm orpasses through a 9.5 u~ (0.375 inch)standard sieve, the operator shall

proceed to Step 4. If the surfacearea is sIT~ller, or the particle sizelarge than specified above, the solidmaterial shall be prepared forextraction by crushing, cutting orgrinding the material so that itpasses through a 9.5 mrn (0.375 inch)seive or, if the material is in asingle piece, by subjecting the

mat e r i a l to the "Sr ruc t ur a l IntegrityProc edure " described below.

4. The solid material obtained i.nStep 3 shall be ,,,reigned and placed 1. nan extractor with 16 times its weightof deionized water. Do not allow thematerial to dry prior to weighing.For purposes of this test, "in accept­able extractor is one which willimpart sufficient agitation to themixture to not on Ly p r e ve n t stratifi­cation of the sample qnd ~xtracti.on

fluid out also insure t ha t ;111 samplesurfaces are continuously b r oug h t i.ntocontact wit~ well mixed extractionfluid.

5. Af tel:" the soEd rnat e r t a L and~~tonized wate~ are p13ccd in t~c

extractor the operator shall begin.1:::itat:""'lr. a nd measure the pH oE thesc iu t t on in the e xt r ac z o r • r~ the pH1.S greater t ha n 5.0, tne ~i-i of theso Lut i o n shall be decreased ~o S.C ::0.2 by adding O.S~ acetic ac:d. Ifthe pH is equal to or less than 5.0,no acetic acid should be .add e d , Thep~ of the solution shall Je monitored,:C'" d e sc r Lbed below, during the courseo ; t be extraction and i f the pH rises:1~ove 5.:, c. S~ acetic acid shall belr:ded ':0 ann.,; the pH d own to S. 0 ~

0.2. ;-{oweve't',1.n no event shall the2?,gregct.e amount of acid added to theso Lu t Lo n exceed 4 n l of ac i d per g ram':'f301id. The ra Lx t u re "hall be-:-:.gitated for 24 hours and rnai rit a i ned

(

,', ",. 20 degrees 40- 104 degrees

d e g re e s C:' ,~.,,.;,,,..

'.: "_... .-1.''::;'

(68this

t i rn e , It is r ec omtne nd e d ~h~t t he

operator ~onitor an~ 3djust ~~e Dr:

during the cou~se of the ~xtr2ctlon

with ~ device such as the :y~e 45-A D~

Corit o l.Le r -nanuf ac t u r ed h'f~" Chemtrix,Inc .• Htllsboro, Gregon 97::.23 o r itse qu i va l~nt. :'n cOiljuc::icn~etering ~ump ~nd r~se~vior of Oe5~

acetic ,".cic. I: such a system is notavailable, the following manua I?rocedure shall he employed:

(a)C,11.i bra t e d 1. n

pH meteracco rdanc e

shall'.-ith

be:he

6. At the end of the 24 hourextraction period, deionized watershall be added to the extractor in anamount determined by the followingequation:

v = (20)(W) - l6(W)-AV = ml deionized water to be addedW = weight in grams of solid chargedto extractorA ml of O.5N acetic acid addedduring extraction

(d) If at the end of the 24-hourextraction period, the pH of thesolution is not below 5.2 and themaximum amount of acid (4ml per gramof solids) has not been added, the pHshall be adjusted to 5.0 ~ 0.2 and theextraction continued for an additionalf our hours, during which the pH shallbe adjusted at one hour intervals.

(b) The pH of the so Lut Lon shallbe checked and, if necessary, 0.5Nacetic acid shall be manually added tothe extractor until the pH reaches 5.0+ 0.2. The pH of the solution shallbe adjusted to IS, 30 and 60 minuteintervals, moving to the next longerinterval if the pH does not have to beadjusted more than 0.5N pH units.

(iii) The reservoirshall be slowly pressurized untilliquid begins to flow from thefiltrate outlet at which point thepressure in the filter shall beimmediately lowered to 10-15 psig.filtration shall be continued untilliquid flow ceases.

(iv) The pressure shallbe increased stepwise In lOpsiincrements to 75 psig and filtrationcontinued unit flow ceases or thepressurizing gas begins to exit fromthe filtrate outlet.

(ii) The waste shall bepoured into the filtration unit.

Separation Procedure: Equipmenc: Afilter holder, designated forfiltration media having a nominal poresize of 0.45 micrometers and capableof applying a 5.3 kg/cm2 (75 psi)hysdrostatic pressure to the solutionbeing filtered, shall be used. Formixtures containing nonabsorptivesolids, where separation can beeffected without .Lmpos Lng a 5.3kg/cm2 pressure differential, vacuumfilters employing a 0.45 micrometersfilter media can be used. (Forfurther guidance on filtrationequipment or procedures see "TestMethods for Evaulating Solid Waste,Physicall Chemical Methods"incorporated by reference, see§260.11). Procedure:

(i) Followingmanufacturer's directions, the filteruni t shall be assembled with a filterbed consisting of a 0.45 micrometerfilter membrane_ For difficult orslow to filter mixtures a prefilterbed consisting of the followingprefilters in increasing pore. size(0.65 micrometer mebrane, fine glassfiber prefilter, and coarse glassfiber prefilter) can be used.

procedureleast 6

The adjustmentcontinued for at

7. The material in theshall be separated into itsliquid and solid phases as

under "Separation Procedure."

extractor

( c)shall behours.

componentdescribed

8. The liquids resultingfrom Steps 2 and 7 shall be combined.This combined liquid (or waste itselfif it has less than 1/2 percentsolids, as noted in Step 2) is theext ract and shall be anaylzed for thepresence of any of the contaminantsspecified in Table I of 261. 24 usingthe Analytical Procedures designatedbelow.

(Part 261, App. II

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(v) The filt~r llnit

sha LI be depressurized, t ne so l t dmat e r LaI removed anci ...;eighed and t he ntransferred to the extractonapparatus, or, in the case of finalfiltration prior to analysis,discarded. Do not allow the materialretained on the filter pad to dryprior to weighing.

o. Structural Integrity Procedure:Equipment: A Structural Integrityt e s t e r having 3.18 em (1.25 in.)diameter hammer weighing 0.33 kg (0.73Lbs • ) and having a free fall of 15.24em (6 in.) shall be used. This deviceis available from Associated Designand Manufacturing Company, Alexandria,VA 22314, as Part No. 125, or it naybe fabricated to mee t thespecifications shown in Figure 1.

This procedure is intended toYeult in separation of the "Free"Liquid portion of the waste formany solid matter having a particle31ze greater than 0.45micrometers. :f the sample willnot filter, various otherseparation techniques can De usedto aid in the filtration. As~escribed above, ~ressure

filtration is employed to speed upthe filtration process. This doesnot alter the nature or theseparation. If liquid does notseparate during filr:ration, thewaste can be centrifuged. Ifseparation occurs duringcentriugation, the liquid portion(centrifugate) is filtered t hro ug nthe 0.45 micrometers filter priorto becoming mixed with the liquidportion of the waste obtained fromthe initial filtration. Anymaterial that ~ill not passthrough the filter aftercent r i f ug a t ion is considered asolid and is extracted.

Procedure

sample holder shallthe Structural

then the hammerits maximum heightshall be repeated

(2) Thebe placed intoIntegri ty Tester,shall be raised toJnd dropped. Thisfifteen times.

2. (Reserved)

Ine ;:est methods for analyzing theextract are as follows:

Analytical Procedures for Analyzing2xtract Contaminants

For all analyses, t he methods ofstandard addition shall be used rorquantification of speciesconcentration.

(3) The material shall beremoved from the sample holder,weLg hed , and transferred to theextraction apparatus for extraction.

(1) The sample holder shallbe filled with the material to betested e If the sample of waste is alarge monolithic block, a portionshall be cut from the block haVing thedimensions of a 3.3 em (1. 3) diameterx 7.1 em (2.8 Ln , ) cylinder. For afixated waste, samples may be cast inthe form of a 3.3 em (1.3 Ln , )diameter x 7.1 em (2.8 in.) cylinderfor purposes of conducting this test.In such cases, the waste may beallowed to cure for 30 days prior tofurther testing.

1. For arsenic, barium,cadmium, chromium, lead, mercuri,se Le n i um, silver, erd r i n , lindaneoethoxychlor, toxaphene,2A-D(2J4-dichlorophenoxyacetic acid)or 2~4j>-TP (2~ 4.1 5-trichlorophenoxypropionic acid): "Test methods forthe Evaluation of Solid Waste,Physical/Chemical Methods"(incorporated by reference, see260.11) •

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C:"';~M1CAlS CO~AINEO !~.l S'/1-846

Appendi~ III-t~lewical Analysis :28t21ethod3

Tables 1, 2, and 3 specify theappropriate analytical proceduresdescribed in "Test ~ethods f o rEvaluating Solid l.Jaste, Phy s Lc a L'Chemical :·1ethods" (incorporated byreference, see 260.11), ~hich ~hal~

be used to determine whether a samplecontains a given Appe nd Lx VII or VIIItoxic constituent.

Table 1 identifies each Appendix"a::: or '.'111 organic constituent a Long<..lith t he approved measurement me t hod ,Table 2 identifies the correspondingmethods for inor.ganic species. Table3 summarizes the contents of SW-846and supplies spec if ic sec tion andmethod numbers for sampling ~nd

"na1y3i3 methods.Prier to final samplinq and

anaLy s Ls method se Lec t Lo n t':-:Q .mc Lys t

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Frs! oci~

~ ! ~;;"-.xl

~ of Soo1d W.s:es ._. T.OEl~_ at "-",,,,".Af.. s..."",,,"'1 p...,... \..0 _..I

~",.totv and SOon'""" 0!::>Gc....... 1..o-~ __.2F~ Stz=ol CGnc.eots .• \.o-.J I IBa'-: Sb::s:ll:l!l StrlIf"9"._ 1.~7 I' "

Sm<:M Itandom s.a".~ _: sn"""",~ s.:I1',::(onq "'- i j

~I_ Rcndcm S""-O::""9-------------t-----------'8lle=l ~non. 1.~7 ~ I

eon-tl! S-<m~.-----. ~ !_!---...j.

s..c..-lllld1o;_ f ICoot >f!d lDu~. , I'

1l7\01e_:lOft 01~q Pl.2n - ' ...0-7 j _j'~aI~€~_____ .

eo..~~ 'HUt. s..mcl.lv_________ :u.' L-_-lW""l"'Od 8a~ J.2.2 I 1--c.oc:"" U.J I ,n...-t. :1.2.4 k lr____ azs l-- :

kYj8'I ~ ~.5! :Sel:ct'~-OWOCon~ ---1 .;-~ r:::::-.._-·:~ llt"C St~ 01 $.i~s....,_ :..J ~-__----l

C'QC'>S'I""9':.JUOI'\ ci O"...JJn C'f CU:s~o::y .. • :'0 l !s.m.,.. uo.o. .. . ~'

~ 5o-..uS .._ .• J

Appendices - IV, V, VI [Reserved]

A?PZNDIX VII-BASIS ~'OR LISTINGHAZAliOOU5 W JlSTE

EPA"""oro­"".

Wft'5~.

No.'

: I'AhH.fAfd·

EPAt\allJr(j..

OlJ~

.....a~le

Nil.

'." ,,1,,"hlllYII""

K106

Kl05

N A - 'oNR,tn ~ t':ftl.l~S becAu~ It taUs tt'Ie lelt lor tJ"aeCns:l!tclensttc of l'J".t.t~uty. COtfOSMfY. Of rMCtM:y.

Ke97

K085 .....1 S..n79..... d<cl\lo<ao<>n.-s. lnchtorooen_. I...i Ul\cnforooenz9't"lleS. cen1ac~obenf(u'"". n...I AchJo<cl><ln,,,,,e. benzyl cnlonoe

1<086 : Lead. hexavalenl chfOt'/"lllt.Jrm.

1<081 IPn<onol. osonl""I"".,.1<093 I Phlnshc 'M~". ma4iloc InhydndeK09' , Phlholl(; 0"""""""'. .K095 j t,1,2·lnchlor",,'h_. f. t.t.2-letrachJo<oelna...

: 1.I.Z.Z·to.rftC/'__ -,096 ..... l'.;·d<chioro<t,hone, 1.I,1·'nchloroothane, 1.1.2·

I lrl(;~toroe"'H.ne.

. Chl"'dor"" ~hlotio:rAp.OOn~

I z.a-o ...nlo<~, Z.'.Il-lnchlotcoMno/.: HOYI'VIIliQnt cnrotnum. lead, Cadmium! Ar.,OnJC

r\r~rtnrc

Aflrhne. nllrobenZene ~yl~.tTWl.

AnIline. ~lf)f"'llQ. C1tpOenyt&t"Mttle. rutl"'OOenl1tt"le.

, p!'":'A~amlne.

, B."lene. mono<:hloroben.zene. doch6orobenzenes., Z_'.& IncNorop/>enol.; Mercury

i

ElhYIAf1C dld'tlor~. 1 t.1·lnchlorOi··lhPlt'\fll 1.1,2-

f(K'nlr'W'f')f"OlhAnA. 1&lrAcnlrwonlhHn(1" (t.! 2.2·10­

Ir .. r:hlrv~ltlJ"(l41 I'4nrt I 1 • .l1f11ll'M"hk)rOOlhAnfl).

Ir/{;hIOf'nt'tlh"(iRrtO :~lt8Chlnf~lf'1lhviflf"lO CArbon

tolf,.r.hk,f~lt' Lhk>tolorm, vlnyi U1tOrlda. vmyh­

r......nr- r:h!oor,H

FlhVlonA 111rhlof'KiP 1 t 1.1tlrhl(y0fl'lhAflO, I, t ,2.rr,.hlr.rOf"lh,l('\(' 111Ir:,\chl()(onll't-,!"lO" i \. f'2.lp­

'OF hln((~lhRn($ aM t.l.1.? lJololrllrh;tYOAlhanAI.

It,,"hl()t()pl"~ll\n~_ lolr!lChk)(OOlhyinnf'" carooo1('\lrAchlOflcto Crll(,:ft")l()(m, vrnyi chl{)(tde. vmyu­rl(.,,.-~ ,:hlor!f1R

AniiolTlnny 1+l'IrtlOn 1f'lrArhI0lIC1A. cnkltofnrm

P~OI IAr", l~<;ll(". fttOfMR11C :"Iydtoc.arbonsJ

f"'hlhnlt4" Rn"yth'lN,. maio.<: "l"Invnr.~

j'lllhRllt· "flnYi~f'rlfi \." ~"P"\lhnl1IWn()nfll

UltlR ,11lHlrnf}('n/r'''4''t 2." l}trlllf'llnlt;fl(W\

PWol:l.lpr,v<1n. PVfl(l!f'W'I". ; rwc-nl',.,.TOluon n 111te.t".>rVAn...lllllt lnll,,*,r-o; 'Clamr"'"

1.J 1 lr!1 N<'w'Ol'\lnAf\A. v~yl c.r1INlOP

i.7 (l1('~1,.,,~11'o,"OA I 1 I IrtrM"lr")"'ln1't~ .... In·(1

!,hllll,,1A \I1t'l/h1nrwt chlorto:lt" 1.l-l;orol0tm

Hf'."rnlt'''lU}ho1'''/n~ hrtll'oiCtlIOrn/1{jIPlt1Hlnf' n.,•..JPoCT'\Ir)(t)6'1I"w'·r ! 1 : .' j~I(~C"lnr()('!I"'A~ .

1 1 ? ) IAlrAI r1IOtr>oAlnAnf'. OlhylAnf) dJCI'\lorK1a

Ar'\l'u'K:

;";01' 1'H"nlnrr:y;YClf,onr.: "lt11f'lf'\(t

, j U_ Ar hl()(()("y'_l('lplln lA, hFlnf'

" .... <'lLhlC>focVCi()p{rnIRrl'fU"lt'

\:rn()'\('Jlfl ct!".c;;nn.n nAOhlh"lono IluOtAnlhllne

t.on!f)fI)J H,.orAnlhl1!\fJ. t}l::Iol()(AloyronA.

,nfl/U'.tl{17.J·r:rtf pyrnno. t!fm7o("\I~nlhr"Cnnlt

d'~n/O(;:tJ8nlhrAC(lnn ArAt\Ar!"'lIt'!Alt"'lr\~ .

TOIIl<An>A. ~ho~pnorOdII~04C and Pho!:OMOfOlhlO+C

ROO o5tnr,

TOhJ'l'H"l>A. ;'tt"C~PhOfOdflhIOC sod C{'\()spt'l<)(othIOtC

"Ir:K1 I)SlfJl'~

Pl"tnr-.tR lc,fm,.ll1nn\,rio, :1I":O"'onOf'C'd:lhI()1C <)nrj

ftl"ln",Ohor'-:llh,o'r R,-lt! t1qtAr~

PhO~i,hof'\Ajllh,OW"" ",,(j nho~onCiolr,;()IC Bod

K.Ol0

,020

KOl9

KO"i6

K0/\ .l<r.:nlofn]1

<'037

KCJ8

FOO7FOOR

HXi'."0:0F";j1 ~

rel:;'F01\{

KOO!

kOO2 lo-iexl'l"'HiOnl , ~fomrl..m. if'1lI0

lo(f'.()1 ....a.nv"'ifltnl ,nrcm,\;m ..-ao1(00.01 ~>tll& ...t1h·tnl ,-~'H-:,~u"'"

)(OO~ j-h!J;~vlS!r,nl ,:"'rClT'lf(j(T'\ !8aU

w::~W')t\ . l'1tul'lv"iunl (NomlUm

f(1)f)l i ClIU,..d¥ J<.:orr:;ffluJo(1J h4Ja.".lent ct'W()t'nIum.

KI~,()i\ ;'-'UlldvMl .. nl Clll:'}(T'llum

"I)O~ Ch;,)IOIOlm. lCW'''''t\.{1ef'ylje. me ll"tyl6ne ChlOfi<Jit.

,n...:r-yl r hI01'w:':tJ. :H'fitio.hrnvdn !ormlC acod)(J)lQ (hl/lfl\lr)/'m ll)fmaIOtlT'\V,j.H melnVlttn6 cnk')l1lje.

r"olt,'V" ,1,i0'i'(loo, llllfM:dltl'yIlU If;rfT"looC dCt'(l. t::l10'.

,001 , i TI!tac.nl.orOG~. I~.e~ cf"I.lonc'.. tI1cn4Or.i lWth~ 1.1,t-~oott\ane. careoo !1ttt.j C"'OfldO. crwonn.t~ fhoJC;tOCdfbof'ts

Foo2 ..... ; T",r3cnl"r~I"""""". """"'1"""" cnioooe. u....r«·o-thyt~. 1.1.1-~nc;tlt.()fOoatn.alW.cr'lfOfCJlOef\Zene.'. I ,';Z·lrtC'hlr.xo-l.2.2·tnl1uoroetl"'llnG. ort"ho-dJCf'1-

I \QtOQfOnZe.... lrChI<ltOIIucJromo>II'I&ne.FOO3 , N.AFOc.e _.; OoSOf. aod etfl1l'11'ic aod, nttfOOOnze-n4tFOO5 i TOi",,"". """hyl ~'hy1 k"''''''', cartlOn d:sulhde,

j 1J.CC....U1ncw. poynd:ne.

FOOtL l CldrrMJm, r.OllltVa'-"i d"w'otNum, I"'-eket. C'YanG(comOl6aedl

'0: Ct,nl<.le {l\.8da,.

: C.,.arlW'1R(!I/llll\).

I C':-.\lo~.ltf ""iI ••.i C....4~., \ ....1111

: etarllH., (SItU,,:

; C,:,ar.l(le ICt,H'nu1exGC).

, Ha:r• ...,IIl;en1 chr<>mtum. cyande {C~...edl.

: PMl.~"C"IOf~. phon'>t. 2·ct\lorOOhel"l()l, p.-1.)llQto·m·c.ffJ""'. }.,,·c.metnytpt'\4lnyt. 2... ·Qtnfttl)o

nl"~ro{)i. 1(1oCh~~I.. !"lr&C~••

• J _".(MWWOO'lo«t(Jt. Ct.IO"~:•. chrv_Uf\08. nlic"ma·10'.... CIXJ(.nlh~. t....enlOt'b)ll...x)l.r,I~.

!~t\ZOfdIDyll}n-fJ. ,,...a"no( 1.2.3-COIPY'e,......

u~n/llt)",d"l("t:'O'. ,::.oen.zl.laflINac81"Wl. aceo­

iH.l~I"ftIOI'U

r.c ··..':H"ttth' 1t"::HIO{\.I("~ h',(~rocyAI"'\.: 5CkJ

"-, j I '! ~. ", "ol, ....1" ... ,\...,~ "'L'·l'~"n!:"'..... &L@I()l'\lII,IO

",t)i.ol ,'\, "'01'llfi'l' i'1l.J'f.ltlTlotOd

K()t~ ..'II .....' ,;itup',,"illenll. :H~."cnl('W"ot:IUIK(1(~ camen

!'HI!:Sl.lt:r...'Oe. htJ.l4ChiQt0t:t1hana. ~cnIOtC!"tltthy.

"l)~ I ~_J', "':,)fOnydPl ...:rHc.to'dl~lf'J [ tl'~lcn1C"'OlT..elnYI)

,,'f ... l n' ;,! 0l~ ;~'Lhh')(06111yll 61h(l11:11. lfiChlorc>

i'" ·t,a, ,() diLt"!i(}tIY,.JfUtJtlCoUilS

f<..QIEl I,' ,I:, ;1!\;lC·,llnano. ,r,(,.r1:0fVtilhvlen-& ' .... J.ChlQro-

~ ... t!dJ'I'fll' iH1J;lt ...~I()(O{)u(lrdf\Q

":.C43

i Pt,Or;:uo. t""'(;ll'ljrlnnyr~ phO"'DnorCdllhlo~ and

=''''''''rH'''.r}fOlhIQIC ~r:lrt A~Ift(!J

j "l'"',t-.p h n r'\11

: HClxAr: .....'nrt">Mn'~n9 0r,hO.r1~chic,rcoon"Zen8

~ 2.4'lt,r n loroonenol. 2.6·dlr.htorOOhenoc, 2.4.6-tnch.

I !'}rophnr\Q1

NAr.( A

.: ,.0''<1....: A

~ !-'\)O(;'\V,.!Rn\ ::hr.""\m,um, inAO

'-;l';¥Av",Anl (;'lfllmll,m. IAao

, J."'\:lAvntonl ,'h")fT:H;m

lo J~: -.j~:t;;"'A:~t)1 ChfOmlum. ;IlQO

"O~7 L~P,r1

Ioi.::.oo ~ ·:Y""'!1ifJ. r:aplhaIAn., Pi"enoltc comJX)Unds. &r-

..... ..;.,

;(073 ..

,,084

~ .. yAVH: ••('\1 Cilfi\m!um AAd. cadmIUm

:-1Q'lI:~"'''l~:''l! Chromrum. leAd

h61J;av",gnl chrr}m'um 16Rd. CAClfMlUm

l"'\"-r.llr".

C;"'If",rt)INm ,-"·1'loOtl (Q\r,.r.hl(",.fln..-. !'I"~.cn~"lirO*ln.

~r.A :!I{""~I('jrnnlf'lAf'lA. IAlrllCf'llnt'04"lhylfW'l4, diCh.

't,r()o:tlhVlI.nA ' r 1';>'!Alr"C~iOrOf'\h,,-floII'

Anlilna nlpt'lenyil\mlne. nllTQO.enzene, O/"'l.env1ttne­Cl>1m,~o

Ar!t.enlC

/"4"'1 iJ1IS 1\.. v I J1 ~ 1 I:: 1,IlJ." ,U:!

(:IUI::~ l !'llJ.'-:l i'~

I'lltll,lI11te (1,2·neld. bl:i( 2·Nhyl·

• 'I'll<' nhllre\'lallon N.D.S. (not otherwise'i.1'dl h·d,. shmllics tho.se membus 01 the,o'IH:ml CIa.S.1 nol s!lccJ(leu.lly IIHteli by nllmeIIi lhl3 aVPl.'I,' ,,""';-

C:l1>l'.:!:4t:l .....'I.~Jl1(~eCII.ll"lI I.flaulfltlc (Cart.en bl!tllilltj~l

Curbuu J"yClUlIlld,' (('MI){H1yl IhlOrldc)Chlur"j (Acdaltldlyile, t rtch loro-)Chlorll:"t,lIcll (Blltlll1cdt sctd. «·(bb(~·

c h IG'-.,.:\ II yl) armuo Irl('I,ulw·1Cillo ...1.11"! "1I~.ha aud I"Unmll IsOrlleLI) (-1:1·

!\1ell\l\l;olnchm. 1,:.!.·I,5,tl,7,8,8·0cllldtluru·l.-t:I,71l-tetrahy,lro·1 (1llphll lind V,,1.111 IIH\

l.'iUlfllorh)

Chludn:l! cd bcnzenca, N.6s."Cldurlllatc~1l et.hune, N.O.I:>.·Clllorltlllll,(1 flllOrllflLfhollli, N.D.S."Chlollnulcd nupht hulcne, N.O.S."CIlIo)r1I1,u"d p henol, N.O.S.·Cl ilo ro.na-t I\lddlyde (!\Cdl'JdchYlte• .:hll)l·"Ch lurua lk yl ct hers, N.O.S.'IH~hlom.lIlflinc(13"1 ,•. <:ll;;lIIlne, ·j·chloro·)CltI'H o"ellL""I~ (B"II'I.<:nr, e ht» ro· I'CIII"rull'·II/.lIilll~ (Bt'lIzcnet<"etlc fie ld, 4·

eli 1,)III·.llphll·( 4·cIIIOfOphCIIY) )'lllphll­h~'dfllKY" <'lhyl "at,'r)

p·CItIIlIo)·III·en::101 (1'/11'1101, 4·chl,,,,·0·3·n",lhyll

{·(:IIII1'" 2,:J,,'po~n)ro,)<Il1e t Ox lrnue. 2·Ic'hlorOllldh\'1 ).)

2·CI\I,}fIJl·tlly) vinyl Hiler n~!hcllc. (2 "hl"r·IIl'l.hoxy)·)

Chllllo(orril (MNhllflt" tfleldero-)CltI"rOriwtlllllle (Mdhyl fhlorillc)Cltlolonwtllyl llIethyl dher (MI~II.,<IIe.

c1110rumdhoxy·):.!'CllloflHlnphtlt"lene (1IIIphlhlllo~IIC, h'~ll\'

ch loro·)2·Chlof{lllllCllul (1'l\dlol, lJ·chloro-)1·(IJ·Cltlor"ph'~i1yllthIOIH(," (ThI<Ju,·.:a. (2·chlofIJ1)"Cn~'I)·1

3Th IOfl)ll\,0lJlollllrllc (l'ropnJlCnltrlle, Ji-chloro·)

Chromlllll\ III1.j e'~llll'O"'I,b.N.D.S.'ChrY';"Ill: (1.:~·I.kllzphcllillll.hrclld

Cllrlls red No. 2 (2·N~r.htlloft, H(2.5-dlnlethu:{Yllhcnyllt';f.i,l· I'

CllilllflrsCop!'t'r eY"H1ldeC""c ,:,ole (Creo:iole. wood)Cf.:sols ICre_'iyllc acidl (Phl~1I0I, methyl·)C .... loJllnl,kll;:de (:.!.BlitenllllCYl\lrldes (solullie salts IIl1d complex,'s),

N.O.S.'Cy.IIlO~CII (1':I.h'\lIclllnll.rlle)C:.Ifll\:)l(ell bfllllllLle (Hromlne cyallldcl(:yiirHlUen cillo, 1.11, fChlorlllc cyanide)(:ye'lsln t1xtl\·I)·Glueollymuo.:,ldc, (methyl-

ONN'll2oxy 1r,ldhyl·)2·Cyclol\l'x 1I1·4.d·dlnltrophcnol (Phenol, ;l ..

cyclotw x y 1·-t,O·dlnlt 1'0')

CycllJphO:iphbflllde (:.!H·I.3,2. ·0" !U.8iJtIO$-IJ11III'lne, (Ill;( ~!·chloftlctllyll).fI\lnoHclra·hydro',2'1»)(lde)

DUlllIlJlIlydn t~.12·1hphlhllCcncdlone. (&:i.ds) II ticelyl·IO·((J·junlno·2.3.6·trhll:ox:t}­flll'lI,,·!. I~' '\(J·hcxlJl,yr I1Il00:jyl )oxy }·7.8.11,.!Jl;.tcifahydro·tl,8,II·trlhYdroxy·l·mclho~' \

......1II01Ill·

( l\letllllllC,t:tller

;~:.;j:,.,I....' (lU·l,2.~i.'l'IL,.,(,t<i ill'i.llk)

,\ 1;lj:J~": ( .... ;I~IC·.4:,.II\lllille'

;\1 rt!'lUL}' IUllJ cl)nlp:.luild~~ N.O.S,·.~I IIl~le (Sllltllrt)lI~ il.clt!, :l·t'hluA"t':I1.'thyl·. 2­

: tt t ,I·, It''I'''ltyli'lllylll!hl''''J.~Y )·1·'lfUi\·lo'! hyl • :,(I'r!

"\:~'l'IlIC u n.t n,ull:I,llIlds. i'l () ..s, •;\1 :.I'llil~ nl'lll t ~),.'.)lllil r:~I,'1111" (tt'ld)"\1 :.I'ltlC ',H~lllq:Ud,: t Ar.... ·U!c I V) 1))( Ide)\1" rue 1.1 1.,-,lol,' II\C.I 111.(' 1111 ~ o xhh-)

1\"11111111111' tlll'II:.(·II;lillllh\

,.IIIoU'd,,:ld"YlloI:,1 N.N ·/lIl1l1'thyl·,JI:': 111"1 II UkJ1'ldl')

\: ... -I"llnt' 11.·~\.il·r1lil·. di"'-:',ll"'lnLI' (I.':ilcr»jl .ruun .rrnl 1,~dIIlIIC·Uill.h. i/.1 ~.S.·

Ililr.IIIIlI'j';I'IlItII.'

1l1'1\:II'llu'lldlnt' (J.t Ui'II/:U Iliiilll"):1.''''( .i Iu nt Ilr:tC!'il<' CI.:!' (I.-nc·.:lIIHlfIl"cIlC)III :i'!.I·I~I~ I L'~·dlllh·.';l1 r u-ru-)I" 1!!,I'lIl'llf.'lIJnlt: ul'ld I t\r :11l1>.: Ht'ld. ~Ihcuy!,)

il: :lto·,II' • .11,,1\ 10l'lJlII<'l II \'1 • Ikm,11 t 111,)[1,1;0)!I, Ili."ild \l11l1 ('1'1\1"1,1><11101)Ill'il/ldllte If IY·lllpllt'III'11 ·I.! .11:11111111')'kl!/.I)[hHhL..HlllllIt1~llt~ ~ l ..l !i:·Il~~~>lllh)nUllh·

I~lle )

1!"Il.'.u[Jlf luor uut neue 17.1l j ll'II.'./) 111,,11'.\11 t 1\.l'i:L')

H.,or,.. I)( u lpyrcne O ..l·If,·lIi.llpyn·l\c);1 Hel\11lllul\II)IlC (1.4 ·('yelidll' x lutll'II.~<llond

lJ.:or:.lltrldllorldc I 1l'·IlLt'II.'. trl('ltlonlllwtllyl·I

Il,·nl.yl chlllrh.1l' (Bt'nzl~lIe, (drlor>lIlll'lhyll·)Ih'ry II I II III Illid I'UIIlIHlllllds, N() -'" •IIhI2·dllorodl\oKY)lIwlhllllt· '1':LIIIIIW. 1,1'·

[iiiI'! lIyll:llt'hlli(Oxy IHoIs( :l· ... lluro·l)I!!;C2-('I1I,ltl\d\lyl) dlwr I Etlllilte, 1,1'·

1l,}IlIs( 2·"hloro-))N.:-/· HU( 2·e IIlurod 1\yl)· :.!·IH'll I11.1\ YIfllIIll1t~

IClllllrlllll'llilt.lIIl')IIh' ~'d"orolsol'rOllyl) I'llwr (PrOpIUlc. 2,2'·

')Xl<l)bI2·cllloro-ll11101 l'illolIUllIdhyl)

lI\ybb(cllloro·] )lhI2·"tltylllcxyl)

111'11/ i~ nc dlcurbo)( yllcIlex}'I) ester)

IinuiI0;,.:donc (2·PropIU\I,IlC, I·bromo-)1l,,,nlllmdl1'\lIc (McLhyl bflllllldl"lI BIll,"oplttuyl plll'nyl ,'lller 'I"'m,cnc, I·

t·rullh)·'1 phl."l10XY·)ilr"dllc (Slrychnlrllll·IO,ollc, 2,3·dllllcUwxy,

I

2 1IL11.I:JIOne I;~roxldo~ (Mi:lhyl ",th}'1 keto lie,pelU:<ld~)

1I'.llyl tlclizyl llilII ,,1l,.lte 0,2·lIcliullcdlcltrboxJ'11c 11,,1<1, butyl phenyl·IlIdhyl e:itcn

1 s,'c Butyl·.,lhllnllfGpllcliol (DN 1'11')c1'1 "'IWI. 2,4·<llnlt(O·I)·( I·rnethylprnpyll-)

C",llIIllIHI lind COmlh)(!Il1b, N.O S'Cah'lum chrolllllte (Chrol'itic lIcld, calchlffi

slllI) .

Ac', (1',.lInk ,ElIIi,,;, lolt,II,~1

1\I'l·t')i>h~~llddt: t F! (;1:1I(l1~1~. l ~,lh\:II:,'I)

J. (it hJllIl.' /\I.~I·l cu YIt I.-,n/.~'I)I ,.

h:;dt"IL'j.'C~>lIl:'oIulh "11111 -. '.11:; (\Vllrflulll)

·2, ,\,"t'()' IHI,lilloIlIlIJI. nl~ (Ai ·~l ;Htll,)e. N-I :lU,1I1 ~'.II I 11"~· j-' I ). )

.\l'I·1 yl 4 lilliCl.I.' i ;'': L .. i.: :,'11 ldUJ Id.')1 A~'I·t}J·:': (1IItIioll'l\ (.\.· ..·l,·i::lik. N (;Ir::dn

011,1,) """il'(hyl)·).~.n··dl·lll (~~ ~')It'lol'llill~

A'Iyll;lIl!dl: ('2 Prill ( •. ;11 .j .... )

A.·rH.llilIAn...· (:~!"Id~ ,!).'idld\,·)AI! ·.:;,.\In!.i

I'\hhln (,.:~.:,.(:., Id 1{\ :\I~I'ltllJ(G'

1.·t·1IA.:l.a.n.Jo .!)i , ~;., .... ;.II~ .I.':J-, 11 •.:o.t:xo·1.-6 .5.1!·A 1Ia"Lt',r II 0:\\1)1' :4J)j I t1,11 h~IH;)

Allyl i1h'O:'IPI (~ Ptll(i"Il-} ul)t\JllitlllH.lft1 IJil,~·~!)l.lll~c

~ ,;r.>1llnl.l1,,,.·II,1 (II 1'liI"lllol::I) ·!llIul".')d·/\Jllltio ..l.la .'~.n.i~'l.);il LI';dihj'd(0 d-

i I.YI.t'rv.\:} 1,ld hyl) Hil ,t1.·tIIlH..y·5 li,\:lIlrl·CI,t'1h':I:LII~' il';l il:IJ{:l,'.:i'::J..ltl./rrulld I,:.!·II H, 1\" "e·~:1 IIlun". ('. ',I ':f) (i',IIt"'llyd" C)(.1 ;~! r! IIri{ 2':" .3 .:1h):,' r .-ulllt J. 2 c)1 Ilt.ll)Ie-· ·~:I-d~~)t:o.:, 0"'\11:111\) B-(l(UfIlIIIO",·.u:l' .. lIyl )oJ~ Y),c,,:(11 yl J I,Ll .•.8':I,I.till·li",,,,h::,I.-o·1l '!l(I"t!;r;xy 6·,'\o'd,)'·)

~·c Alui, "lind hyl )·.1 1'.1" ,li."I'JI I JI '~II ).1:(0) .(fl'

'Ltd,lllt', 5·( IlJLI"',i'IH:1 tl)·I)·) 1,,', IJ\lnopyrl­dl ..,,~ ('I·l'y.-roJ!ln, ,,,I,,l'l

DUl) (Dlchiorodlphenyldkhlorodhane)(EI.I)l\nr\ 1.I·diclllol'O·2,2·ois( n-cntoro-plwnrl ).)

DOt: I Elllylene, 1,l·<llchloro·2,2-bls( 4-chlor·oplH'lIyll' I

DI)T (Dlchinrodiplll'nylt.richloro·elhllf\e)(f:I ha /I". 1.1.1'\ r irhlorn ·2.2· bl~( p-cnlorr:pl,,·oyl)·)

/),,,11,,11' (S·l2.3·alchlonllillylldll"ol,rOpy Ill,lncarbl'n1I,l,')

DIt,..·/I/.III.lllacridin(' (1,2.5.0 Dil;c'Ilzncrldlne)/)i1), '/0/.111.11 ae r IIlml' ( I. 2:1.1l· DIII",v/ll-rlcllrll' IDd 11'11 1.1 a.11 lun: (,rhCI'Il" (1.2.5.1>·D,ll/'/IlAIllt I,-

r(1n"II' )

'i I1 flil"'llO'lJlc.ldc"rba/.olc I 3.•.5.6-Diben]'(,lIr·b:J./oll'l

Oll;"n/o(ll,dpyrene (1.2.4.5·n,h",,,~pyr'·lw)

DlllI'oW(ll.lIlpyrl'nr (1.2.5.6-[)ltll'll7.pyn·l1l')Drluuzo l a.i Ipyrenc (1.2:1.8 Dih"I\/.lIyr,·Ilf'l1.2· Drbrnrno l·/,hloroprop,lIH' (PrOI""I\". 1.2-

<IlbrrllllO·:I·chloro· )1.2· DilHO",oNhl,nt' {EI hylt',w 11lbrOinli/c'lDIIJro(\lof/i"lhalw (M ('lll ylt'rll' 1;, u/IIi'k IDin olltyl phl.halall' (1.2-

Uem.,'ol'd'Clil boxylic "ncl. dlblll yl l'sl "f lu·[)lchlnrnl;",wI'I\'· (1\1·n/.,·IH'. 1.2 d,d,lol (I )

hl-f)Il'Il!orotwlI/,I'ne '1l,·II/,t"W. LJ·L!lchloro 1

II O,chlornlll'n/.I·IH' (Bell".'·III'. 1.1 ,h('llIoro"fJlI·ldil,ob"II/.I·III·, NOS 0 'B,'Il/."III'.

dl:.II1I'ro. N.n.S 0)

3,:' D,CllluIOIH:lll.idlllc' <I1,I·UILoIll·IIyIJ·'1.1··IlInJdine, J.3··dlchloro-)

1,4 Dlctlloro·2·butl'ne 1;l·lI"I,·"", 1,1-I1ICII101'0' )

Dlchl,lfodl (I11oroml'lhnne (Met IlIlIlt' , ellch·lorc',dlfl"oro·j

I, I·Dlcllloroi.'thllnl' (El hylldl'nl' olC'hlol'idelI,:l· [)Icllloroet.hane (Elh .vII·'.... dlcll1olld,,)111l(ls·J,2-DlchloroellH'lH· (1.:l·[Jlc'hlnrc\I'1 hy·

lenc)Dlclllorodhylt'llc, N.O.S.· (ElIl<'llc. did,·

loro,. N.O.S.·)1,I·DlcllloruNhylcllc (Elhene. 1,1·t!I"hloro·)J)lchloromclhane (MeUlYlelle dllur:de)2,1·Dlcllloro"henol (Phcnol. 2,1·d1chla("O·)2,IlDlchlorophenol (Ph('nol, 2.l1-dlehll)ro-)2,.llichlorophelloxyncellc I\cld (2,4·D), ~;/lIIS

lI.nu e~lers (Aeellc acid. 2,4·dlcll1oroplwll­OXY-. salG und eslers)

I Jit'hI0rophl:nyla.rslne (Phenyl dichloroar·51111')

DlchlornprOllllne. N.O.S.· (Propane. dld',-lura-, N.O.S.") .-- .

1.2·DldiloroprO;1llIle (Propylene: lllchioriddl1lchloropropa.nol. N.O.S.· If'ropanol, dlcl,­

low-, N.O S.·)D!:hlol'opropene. N.O.S." (Pr,-,pcne. dleh­

loro·. N.OS."I1,3· r)(cllioropropene II·Propene, 1,3'dlch­

luro·11.I!t-I.~rlll (1.2,3,4.10.1O·he>.l,clllol v·6,'1-cDOXY­

1.4,1 ••.5. ,6:I.a,04·-{J<.'(.tt-Ilydw-erdo.e ):0-

1,4: 5,a'Dime! hhf\OTlnph th,den ~)

1.:< :3.• ' DltpvJlybutnne (2.2'·l:lloxlfllr:e)Dli'lhl'Ir,r,IIlI' (Ar~lnc, dld.hyl·)1:,'" lJll'lI'rlhj'IlI,,;.Jm~ (Hydi ..... im'. 1.2·

."

O.O·[)ldhl'l S·methyl e~ll'r (.r phosphor,,·dll hloic IU'ld t Phosnhorodtt hiu«: 110'111.O,O·dll'lhyl S,oll'lhyl ester

O.O·Dldh>·lphosphorir: acid,' O·p·nltrophenyl ester (Phosphoric acrd. dldhyl IInit rophr-n yl ester)

Di ct h yl ph(lIlllnle (I ,2· [l(,Il/.t'r,,··c1icr,rbox yll'­11...11, dlCI nyt ost er)

O.O-Dll'lhyl 0-2-pyrll,.7,inyl phn~pl)()rtll hhHIlI' r Phosphorot.hioic acld. O,O·dlC'lIl.1'1O·pyra.L,inylt'sIPr

DI,~lllylsllllll'.<,II~101 (4.4' ·811101'11I',lln/.nlpll;t,nlt,hn'llINIIYI, bl5(dillydl'o"cn pIli"pllale, (1~)·1

Dillydrm,a[rolt' (Benze-ne, 1.2·rnclily/l·III'diux y·4· ~'rllllyl·1

3.1· DI h ydrux y ·alpha·( met.h ylnm mo in 11'1 n vtb,·llI.yI a lcotiot (1.2-UI'I\I,,'ncdlol. 1·ll·I,y·dro xy. ;l.( mr-t hylanur.o )1'1111'/ J.)

DII:;"I)fClpylfllloropllOsphalc (LlI"P) I "Ie ...,IllIorllfinorldlc acid. bb( 1·1lH'1I1y",(lIyl)f':.l -r )

1l1l1lC'lllci.",1 e (l'hospllClr(ldli lIiolc aru]. 0.0·((11111'1I,yl ,s·l ~ (,ud "ylalHi"" )-:!,o,,,,,·L1I.\·11('..... 11'1'

:J.:r· ()lIlI,'IIIIIX .1'1I,'III.ld IIII' I ( I. l'·llil" 1I'llyll1.1'<1"""11'1', :1·3·-!JII"C'1I\IJ"y-)

P·[)'II"'llIvlnrnillO:Il.nlll·n/.1'1I1' (1.li'I,!."Il'WIIIlI',N.N ·lInll,'1 Ilyl 1-(ptll'llyl:lI.0)-)

'1. I~· UllIn' IbyILll'llzl" Illlllllflll""le ( I.:l·l)e'l·/./lill IIrae'·Il,·. ·1.l2·(/lrnelhyl·1

J .:1 .1)'''\I't h yllll'llIlclirw (!IY-f:j Iphe nyll·1,'\··111,11.1111". :1,:J··dlllll'lhyl·)

Dill ",I II\' Icarhanlllyl ch lorlele (Carblll)luyi!'IlI"rlclt-,llImelllyl·1 .

1,1·1J,I1II·lhylhyclru.:t.llle (H >·drlL(.IIl,~. 1.I·dl·1I1I'1I1 yl·)

1.~-Dicllt'lhylhydrll..Zlne (Hydnalnc. 1,2-dl·ml'lhyl-)

:l.:\-[), II1<'( Ilyl·I·(rnelh.vlll"o)·2·bllllHlon~. O·(I rllt'lhyl(1I111110) c><ruonylJoxlmc (Tlllo·lh"OX)

nlolll,.p.lphn·Dlllwl.loylptll'l)('lhyle-mln(~(t:th·allanl ilH', 1.I·dlllWlh yl-2·phenyl-)

2.1· Dlrnclhylpheoul (\'henol. 2,4 ·dllll~thyl·)

DlfIIl'lhyl phthalale (1,:1·B':ilzenedlellruoxylle lIc1d, dimethyl c,;l<'f)

Dlrnt.'lhyl 5ulfa/e (SulfurIc acid. c1lm£'lhylel.ler!

DlnllrolJenzenc. N.O.s'" (Delwent. dlnltro-,N O.S.·)

-l.6·Dinllro·o·crc~ol and salls (Phenol. 2.-l·dI1lIll'l>·6·rnclhyl,. and salts)

:!.4-Dlnllroplwnol {Phenol. 2.4-dlnllro-12,~·Dlllltrololul'ne (Ben:zene. 1-methyl·:!,.­

alnll ro-)2.6·D1nllrololu~ne (Beru,:ene, 1-melhyl·:l.6­

dlnilrv-)DI·n.octyl phthalate <1.:1-

Bfllb~r\t:dic,;rb()llyllc acid, dketyl ellt~l')

l ..I·DII1\;l;;I,' (1.4-Dldhykne Oi(;':!;;)

Di"l>("nyllwdnc Cf.lenztmlwtli',e. N·~.he:1l'I-1

1,2·Diphzl-.ylhydra,Zlne (Hydr"zlne. l.:I-dl-phl·nyl·)

Dl"I'l'r')l!yl1l1t rOl,amlnc (N-Nilroco)-dl,n·pro·1 ' I • : " v . • ~ ,

Dlsultot on (O.O·dIHhyl S·l2·lelllyllhlo)l'lnyl J pllospl\(,rDdiUI icut e l

2,t·Dllhioblurct IThloimldodiclJ rt.onre dra­mldc)

EII110$ul(IHI 15,Norbornenc, 2,3·dlllll'lIHHIOI,1,'o,5.6:1.7·ht'xaehloro-. cyclic >julfil ..·)

~:ndrlll Rod metabolites 11,2,:1.1,1U,IO·11I·1laelduro'a,7 -t-po xy-I ,1.4a.5,6.7.A,8a·oclnltydro·cndo,endo·I,1:5,8,dllllC'lhanollaphlllalcne. and nu-tubolltes)

f:thyl curnama t c I Urclhan I t Cnr bnuur ru-Id,et h yl esu-r :

~:(ltyl e:ranlll,' (propant'llil.ril,')•.:lllrll'llt·b,sdllhiocarbamll' :'lC'lcI, $I"t~ nnd

.. ,I ers I l. 2-Et h 1111<'<1 , YIhbcllr!.J'lIl1utllllllo,,·acrd. sah.s anu I'.,ll'r:;

F:lllr1t-llcirnill" rAztr idine ).:IIl,I(l1l· "xllI,' rOxrrane )E( II 1'I"IWlt\l('11rca I 2·lm inazo: idillt'lh ill/w)~:llIrl mct hnr-r , 1:1(" 11·ProP,·IIIlII· anti. 2·

mcltl)'I·. l'lhyl ,'slcrlI::thYI IIll'lhall('suIfOIl~,l" IMt'lIHlIlI'-'l,IfIlIl;"

nrld, ,'I h y l ".,l,·r).'I/lUfIllIl h,'III' (IJtom:o[ J,k Hillorl''''')PIIIlJr Inc2 1"llItJfUllCr'U'Ol:dt· (Acdanlld,', 2·(1""1'.. ·1~'IIIur()a,·,'t1c aeicj, sodlu,,) sail I A,'t'l ic aCid.

f1l1oro·, sodillm snlll .POllnalddIYU(' (Ml'l lIyl.·III' ox II/to)~'Il,nIlC llCIlIIMt'llwnoie aci((l(il,'flClylulddlYcl(' (I,P:opflnol·2,:J,(·poxylIIl1lornetharw, N.O S·1I,'plllchlnr 14:I·Mt"I hano·1 Ii ·illd"IlI'.

1.1.5.6.7.1J.a·lleplIlch loro·3R, 4,7.711'It'tmhYllro·1

Ill'Plllclllor epollide (1IIpha. bNa, andK'Hllrna isolllers) (·1,7·Melh;tClo-llI·indene.1.1.5,6,7,8,6· h('plllchloro·2.3-('poxy-3a,4.'1 ,7­"'l.r"hYdro-, alplla. bela. IIIHI fo(ummn Is,)·/II,'rs)

l1t-xaelllorobeOl,eClc (B~nzene. hexRcl)loro·)Ifl'xllchloroblltaclienc (1,3·Buladit·ne.

1.I,2.:J,4,4·IlL'xaehloro· )l/"\I\,:illorocyclohexnnc {1111 lsmnersl (Lin­

dlllle n nd !somers)""xlll:hlorocyclopenladkne (1,3-Cyclopen-

lndICnt:, 1,2,3,4.5.5·hexachloro·1IIcxRfhloroethnne (Ethane. 1.1.1.2.2.2-hex­

Ilfhloro·)1.2.3,•. 10,I0-l1exnchloro-l ••. 4a,5,8.8a­

Ill'xahydro·I, 4:5.6-endo.endo­dllllclhllllolinph lhll.lclleIlle xachlorohe xah Ydro·endo.endo­dlmclhlulollaphlhnlcnc)

",'xllchlorophene (2.2' ·Melhylenebla(3,-l.6­lrkhloropllenol)1

1I"xIU'hloropropene (l-Propene, 1.1.2.3.3,3­",·xllehloro· )

llt-~IH"lllyl lelrapho.sphate (Telrapholl-I\ll<Irlc neili. hexaelhyJ esler)

Il,·tlmzlll" ([)lllmloe)(1)'drul'YIlIlIc ncld (Hydrol{en cyanIde)Ilydlo!luorlc Ilcld (H~droll'en nuorlde)Ill'llroK"Il suiliell' (RlIlrur hydride)III IIr(l.\ydl/lll'lhylar~lne oxide (Ca.codyllc

~ ,1,11

Ind"no{ I.2,3·t:llipyrc-IIC (1,IlH 1.2-p/lcn~' Iene Ip}'rt'!I'i' I

loo,)melh:lC)('! H.!l!lh}'llc.d!j.:~

Iron dcxt ran (Fcrr ic d,,)(ll/\/I)b.'X)oli/lIC add methyl ester (!I.·lelt,yl l!;.)-

c.Y~\nltlr:) •

l~()butyl alcohol t t-Procanot, 7-1'ilf'llo.l-I-)bo!,alruil' (U;:-n;:l:'llf. 1,2·/lll:l.IlyICf,:.:,.;lm.), .• ,

all.\' I·)Keporu- (Dt'('·,j"chIOI'OOClllhydro·l.3, ~ M,.,t,h­

11110· 211·c ~·c1obulfo.fcd lpenlnlen,:!-ollc)Lnxlocnr ptru- 12·Butenoie acid, 2'\lI('lhyl-; 't :

II 2.~.cl,II.\'llrox}' 2·{ I-m ..lllo:~yt'l.hyl ).3 .nu-t h}'I-I-oxobllloxy )Illelhyl J·2,3,~;,7a.It'l r;11I.\',lro·lIl·pyrroli,.In·l·yl est er l

''''lId and c·O/llPCIUIIQ:i. N.O.S,"lA'IHI nCI'lall: IAI'Hie acid. 1"lId salt)IA'a,\ phusphal(' IPho:,phorlr acid. lend salt)I A'illl sUb:u·l'la l.." (Leud, blsr ncetuto-

o 'ldra hydfox :r'lri· )1Io1111el(' Olnl,ydrid,· (2.5,PuraocllonelMal"it, It.vdrllzid.· 11.2·Dlhytlro.3.tl.pylld"'''.I!·..

l'dlulI,'1"1 a /I '/ltllI il.ri It" (1'''''1);( fI(o(l i ,-,j lrlll!)M,'lplt,dan IAla/lIlIt·. 3.!p.bl:.(2-

"lllul'll,'lI,yl )ami!llt Iplll'nyl·. L-;MI'n'''''y 1,,1I"I/lul., (fo'ullllllilc IICld. fIIercury

sail I

M"IJ'ur.\' i'llltl cOlnpcHICHh. N.().S.·M"'II:"'rylt,"ilnlt- ':l·PnlIH'IP,,.dlrilc, 2·

IIldhrl· )MI'I IHtlll'l1l1ol (ThiollH'lflrlnollMl'lllapynl"llI' 'Pyridll\(', 2·[(2-

11111\1'1 lIyl:unino l<'lllyll· 2 l hellylR,n Ino.)Melllul"lYI IAet:lllnidlc neill. N·

( 1ll"lhylenrbarnoyl )oxy Jll'llo·. meliiyl('sl"r

M'·lhoxyr.lllor 'Elham·. 1.1,I·lrlcllloro·2,2'­hlSI p·nH·llll}XHJllellyl).)

2·Ml'lllylli.l.lrldilll- Il,2·Propylf'nlmlne)3-Mt'1 hylcholalll IIr....ne

(Hcw.lJ)ncl·snlhrylt-ne, 1,2·dlhydro·3·melilyl-'

Mdhyl chlorocll'.ftKJrllll.e (Cl\rboflochlorl.1icacid. methyl e.lcr)

•• 4'-Melhylclll,bls( 2-ch loroanillne) {BeN,i'lIallllne, 4.4'-methyltllwbi:H 2·chloro·1

Melh~'1 elhyllu:"lolll' (MEK) (2·Bullll'lulldMelhyl hydr£l.Zlnc (f!ydmzllle. methyl·)2·Melhylluelonllrlle {Prop/lncnilrllc. 2-lly-droxy-2-rneth~·I·1

Melhyl mcthw:ryll\le (2-PfOpenolc acid. 2·ml"lhyl-. methyl c>jlt:rl .

Methyl rncthaMsullonltlt: (MelhiUlt~st:lI'onle

acid, methyl esler)2-Mclltyl.:/-( rnethyllhlo Ipl'oplonllJ de hyric-- (,.(nll~thylcarbonyll olClme (ProPL>nld, 2·methy!-2..(m!:lhyllhlo)·. O·[( mclhylli.rnlno lCI\l'l:}onyJ JOliIme)

N-Methyl·N'-nltm·n ·nltro~oguII.I1ldlfle

(GlIanldlne. N ·nllrcwo,N-mel hyl- N' -r,ll",:,·)M'?thyl PUlltltlOIl (O.O·<!lrnel.hyl 0·(4·n:Uo

• phenyJ) phoophorothloate)Methylthiouracil (4·IH-Pyrlmldlnone. 2)

dlhydro-ll·melhyl-2·thIO)(o-~. .MIl11.~r.-l'jlM (::lll'''ri" t>1,1?·,.hlm;,"':h~\l )

(Dillllvs·

\ 1 U1JliUI.dllllh',

11.~·NIll'IIII"ll&-llI~·

l ,:!l,';a (P!.,,·}~;I·,IJI.,(;;:l)it: .• ' Id, t).()·

d ~. , , i~' I \) , t, :: II I. ,:.1.1 i; '.I I I I • ill'

~

·,YIII·Tnllltruhl·Il·WIW I Bt'llzl,rll'. 1.:1.5·1rll·.l ·t ru- )

'l'rl:,( I·at.ri<lillyl) IIho~phlllc sllIlILlI~ (1'1 ',)j

pililll' "lllfi(!I'. tfl~i l·a".lrI(1InyJ.)'l'rbl :1..:1 dlt.rlllllOlln'llyll plln~phall' (I· Pro

1""'"1. :!.l dihrlllHo,. plllhptHltl'}Tr l'!':11l hhll' (~.7 -Nnpht haj;ollt'IIi'olllt," ,I(:

a.,t!. ~.;I' 11:1,3' dlllll'lllylll.l··l.lljJh.'liYII·.,4' tJlyll""( a/.O) Illb( 5',lIllli,o' ~·hy(l!"~Y'.ktra,"Hliulll salLl

l/l'ill'll lll11slanl (Uracil 5,1 t.\bl '/..d,lul'IH'llIY·\lamll,ol· r

Vau,ullt, and. anUI\Onlllln !il\ll (BlnUU,l'Iilllilvanadil ll'»

Vaillulllllll\lt.·nloxlde (Vanadium I VI o x ulc )Villyll·hlori.tl' (F;lll(·IlI'. entoro-)l.ill('I')lal\lIl"

1'.111(' Illlo~lltllde

! I,,;.' TI 1, ..ddlnl'lll;.IlI' 11,:thillU', 1,1,1,:': fl~

11.,,'1 ,IHrll'): 'l.'~ TI'ILl.'iilurl'lllitlW If,~lh;lnl', I,I.',~ '..! ".'Ir,ll'illuro·)

1', !':It'hlo"ol'lllllll" (f;lhl·nL·. 1.1.:2.~ Id.-:ldl!"rlj )

1',·I,:,,'tli.JllHII,·lllan(' '(':lI hUll II'! ra<'lllul'l.", )~ 1.1.li.·'I'I·tr.ll·lllllfhpl"·1I111 11'1"'11,,1 ~. I .1./.

!dludlli,fo,)

1',11;11'1 hyl>hlliiolllyropl ....~pllatl· I (}111""l'yr·III,IIll,pIIOI'lC acid. 1,·(r:ll'lh.vl·I",(.'·r1

1"'lllll'lhyl kiltJI (1'IUlIlh.lIl1·.II·lfal'lllvl·111·11.lrlllylpy·rophosphatt· (I'y' r"pt" "ld">I'II'

:tndt', ld :'11"1 Atyl l'~,I.('f I

Tl'lliuUlrtlllh'lltaUc.' (t\h,tltan.', l,'t f:lllil rU-1

l'I,allllllll ;1I11l l'(,"lplJulllh. NOS.·1'1 la II,,' 0.\1.11' 1'1'11,1 IIi IIIII (111' ."i1kl11,,,1111111\ III IIn·lal,· I A.·..ah' .•('101. II"dliollll

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Section

:Ouhp.:1rt B-The Manifestimport s

State ofwi th thegenerators

(c) Any person whohazardous waste into theDelaware must complystandard s applicable toestablished in this Part.

(D) A ge~erator who treats,stores, or disposes of hazardous wasteon-site must only comply with thef o Llowl ng sections of this Part withrespect to that waste: Section 262.11for determining whether or not he hasa hazardous waste, §262.12 forobtaining an EPA identificationnu~ber, §262.34 for accumulation ofhazardous waste, §262.40(c) and (d)for Recordkeeping, §262.43 foradditional reporting and ifapplicable, §262.5l for farmers.

Gener.:1l requirements.Acquisition of manifests.~umber of copies.Use of the manifest.

~u~pose, scope, and applicao t Lt t y .

:tdzdrdous Waste determination.EPA identification numbers.

"} (.... 'J .\ ('I_v_ .. _,-,

?!~T 262--ST~~~P~S APPLICABLE TOCZlilBATORS Of It-\ZARDOUS I.JASTE

Subpart A-General

rr.,-;

Subpart A-General

(d) A farmer who generates wastepesticides which are hazardous wasteand who complies with all of ther e quI rements of §262. 51 is notrequired to comply with otherstandards in this Part or Parts 122,264, or 265 with respect to suchpesticides.

(2) A ~erson who generates ahazardous waste as defined by Part 261is subject t o the compliance requirc­.ne n c s arid penalties prescribed in 7Del. C. 6309 if he does not complywith the requirements or this Part.

(f) An o~~er or operator whoinitiates 2. shipment of hazardouswaste iro~ a treatment, storage, orJi5~osal :dcili:y must comply wit~

:~e ~enerato~ standards established_,. this Pa r t , (No t e : 1:he provisions0: §262.3':' are applicable t o tt;ecn-site accurr.ulation of hazardouswaste by generators. Therefore, theprovisions of §262.34 only apply toowners or operators who are shippinghazardous waste which they generatedat that facility.)

Pa r mc r s .

~cco r d ke e p i ni; ,

Annual repurtin~.

Exception rcpo~ti~~.

Additional reporti~~.

P'l a c a rd i ng ,Accumulation time.

International shiprnents.

:.':1~elil1g.

~'fCi r k.i r.g .

.)

262.34

'::62. S0

- ..... ,.-

_~' _ '" -.. L

2i!2.42262.43

Annual ~eport (D~REC Form 8700-l3).

Appendix-I

Subpart D-Recordkeeping and Reporting

Appendix II - Uniform Hazardous Waste~faniiest (D~'REC Forms 8700-22 and8700-22A and Instructions).

Subpart C-Pre-Transport Requirements

Subpart E-Special Conditions

(~) These regulations establish~'.indards foe ,;;enerdtor-s or ha za rd ous'..:aste.

§262.l0 Purpose,appLfc abt Lt t y ,

scope, and Note: A generator who treats,stores, or disposes of hazardouswaste on-site must comply with theapplicable standards and permitrequirements set forth in Parts 264,265, and Part i22.

§262.11 Hazardous waste determination.

A person who generates a solidwaste, as defined in §261.2, mustdetermine if that waste is a hazardouswaste using the following :nethod:

(c) A generator ~ust ~ot offerhis hazardous '..;aste to' t r an sp o r t e r s orto treatment, storage, or disposalfacilities that have not received n nEPA identification number.

Subpart B-The Manifest(a) He

the waste isII nde r §261. 4.

should first determine ifexcluded from regulation §262.20 General requirements.

(b) He must then determine if the;·;aste is listed as a hn za r.l o us waste inSubpart D of Part 261.

Note: Even if the waste is listed,the generator still has an opportunityunder Part 260 ,Subpart C to demonstrateto the Secretary that the W;"lste from hisparticular facility or o pe r a t Lo n is not~ hazardous waste.

(a) A ,~enerator who transports,or offers Ear transportation,hazardous ~aste for off-sitet re a t me n t , s t o r ag e , or disposal mustprepare a manifest, using formssupplied by the Department, beforetransporting the waste off-site.

(b) A gennrator must designate onthe manif~st one facility which is;;er;,lttl'd to handle the wa s t eL!Gscribed on the ~anlfest$

(c) Lt the waste is not listed as a'1.1zarrlous waste in Su bp a r t J of Pa r t

261, he must deternine whether the wastei s identified in Subpart C of Part 261'):: e it he r.

(1) Testing the waste2ccordin~ to the methods set forth inSubpa r t C of Pa r t 261, or according to~n e0.uivalent ~ethod approved by theSecretary under Part 260 Subpart C; or

(

the t r a n s po r t c r :{~ !l:::!~l~

the ha za rd cu s va s t e to thefa c f l I t Y 0 r the ;} 1 t c r na t e

the

:\ ~enera tor ~:lY .i is oon the ma nI f e s t one

:'acilitj w~ich is p e rrnLt t e dhis '...a s t e in the event ano r c ve n t s delivery of the

Cd) :fto deliverdesignated

( c )

:acil.i.ty, the generator nu s t eitherde s i g na t e a no t be r facility or instructthe t r a n sp o r t e r to return the wa s t e .

lies t gna t e.i Lt e r n.i t eto handleome r'z e nc y'-J::i s t etc::

knowledge of theof the waste inor the processes

(2) Applying~azard characteristiclight of the materials

526:.12 EPA identification numbers.§262.2l. .~quisition of ~anifests.

~~i A ~e~erator =ust ~ot t~eat,

store l (~:. s p o s e of, t r ans po r t , or offer:::r t r.t n s c o r t a t Lo n , hazardous •ua s t e;".,·:.t~0U: ha v i ng r ec e i ve d an EPA:c~~ti=ic3ti8n n~~ber frcn t~e Secretary~

t h t s Pa r t ,

§262.22 Nu~ber of Copies

The rnan.i f e s t consists of the numbe r ofc o p t e s ·..hich provide a CO?y for '~:.lch

t r ans p o r t e r , the generator state, t.hef ac Ll i t y state a nd the copy which ismaLl e d from the facility to theg ene r a t c r . This p r cc e s s is discussedin detail in the instructions formani:est ~reparation Append:x II ofthe

not:generator ~ho hasEPA id~rltffica~ion number

to theDelaware

Aan

Cb)re c e f. vedmay 0 )tain one by app Ly t ngSecret2ry using "State ofXotification of C!azardousAc t i v i t v " rOrTI. Upon r e ce Lv t ns

-::q°.lest, the S~cre~;1!"Y' ....;ill <~ssign

to

§262.23 Use of the manifest.(f) for

or water

designatedsolely by

(if) Theif transported

Subpart G-Pre-Transport Requirements

(iii) The last railtransporter to handle the waste in theUnited States if exported by rail.

facilityrail; or

NOTE: See §§263.20(e) andspecial provisions for rail(bulk shipment) transporters.

manifest

of this fonn \-li11the generator and

the requirements of264.7l(a)(5), or

or if necessary

The generator must:

(1) Sign thecertification by hand; and

~OTE: Photocopiesbe necessary forfact lity to meet262.23(a)(3);265.71(11.)(5) ;262.23(c) & (d).

(4) Send il copy of themanifest to the State in '.vh i c h theGenerator is located o.nd [0 the Statein which the facility is located.

(2) Obtain the handwrittensignature of the initial transporterand date of acceptance, on themanifest; and

(b) The generator raus t give thetrnnsporter the remaining copies ofthe manifest in accordance withinstruct i o ns on the uniform manifestform.

(c) For shipments of hazardouswaste within the United States solelyby water (bulk shipments only), thegenerator must send three copieS ofthe .nan t f e s t dated and signed inaccordance with this section to theowner or operator of the designatedfacili t y or the last water (bulkshipment) transporter to handle thewo.ste in the United States if ex?ortedby ',.;ater. Copies of the manifest arenot rcquLred for each transporter.

Before transporting or offeringhazardous waste for transportation off­site, a generator must label eachpackage in acco rdance wi th theapplicable Department ofTransportation regulations onhazardous materials under 49 CFR Part172.

§262.30 Packagir~.

§262.3l Labeling.

(a) Before transporting oroffering hazardous waste fortransportation off-site, a generatormust mark each package of hazardouswaste in accordance with theapplicable Department of Transportati8nregulations on hazardous materialsunder 49 CFR Part 172;

§262.32 Marking.

Before transporting hazardouswaste or offering hazardous waste fortransportation off-site, a generatormust package the wa s t e in accordancewith the applicable Department of Transportation regulations on packagingunder 49 CFR Parts 173, 178, and 179.

incopy(3) Retain oneaccord~nce with 262.40(a).

(d) For rail ship~er.ts ofhazardous waste wi thin the Uni tedStates which originate at the site ofgeneration, the generator must send atleast three copies of the manifestdated and signed in accordance withthis section to:

(i) The next non-railtransporter, if any; or

(b) Before transporting hazardouswaste or offering hazardous waste fortransportation off-site, a generatormust mark each container of 110gallons or less used in suchtransportation with the followingwords and information displayed inaccordance with the requirements of 49CFR 172.304:

H.A2ARDOUS HASTE--Federal Lav

Prohibits Improper Disposal. :£

found, contact the nearest police orpublic safety authority or the U.S.Environmental Protection Agency.

Generator's Name and Address----------­Manifest Document Number---------------

must remain on-site for longer than 90days due to u nfo r e s e e n c, temporary, rinduncontrollable circumstances. Anextension of up to 30 days may begranted at the discretion of theSecretary on a case-by-case oasis.

(

§262.J3 Placarding. Subpart D-Recordkeeping and Reporting

Before transporting hazardouswas t e or offering hazardous waste fortransportation off-site, ~ generatornus t placard or offer the initialtransporter the appropriate placardsaccording to Department of Transportation regulations for hazardousma t e r La Ls under 49 C:OR Part 172,Subpart Fe

§262.34 Accumulation time.

§262.40 Recordkeeping.

(a) A generator mus t keep a copyof each manifest signed in accordancewith §262.23(a) for three years oruntil he receives a signed copy fromthe designated facility which receivedthe wa s t e . Thi s signed copy must ber~tained as a record for at leastthree years from the date the '..;asee'..r:1S accepter! by the initialt rn ns oo r t e r ,

( ..1) .\ ;;encr[!cor ~ay ic c umu La t c;::>'z3~doU3 wa s r e on-site :cr qo Cd::'; o rl e s s wi t hou t a ?er~it n~ :.Jithou:.:~avin~ inter~~ status provided that:

(1) The waste is placed incontainers and the generator complies.,ith Subpart I of Part 265, or t hewaste is placed in t a nks and thegenerator complies '",ith Su boa r t J o i'Part :65 except §265.19J;

(2) The date u oo n ·.. h i c h e a c i:

(h) A ge ne ra t c r nus t keep a copy0f c3ch Annual Report and Exception":E'Clort for a period of at least three':-:2rs from the due date of the report:">!.1rch 1)"

(c:) ,\:;enerator nus t keep records.,f :,[1:-.' t e s t results, ·...aste a naLy s e s ,)"; )t~;cr' riete::"::1i:1ations '";Jade in~ ceo rd il nc e ';,J i t h §2 6 2 . 11 for a t ~ e a s t:hr'ee years Ero~ the date that the';,J~ste was last sent to on-site or off­site treat~ent, storage, or disposal.

(

~erio~ of accu~ulation ~e~~~s 'j

..r Le a r Ly raar ked arid v i s Lc I e -:-')t"

~~3pec::cn on each cont~:~e~;

(3) ~Jhile ~ei:1g ~ccum~lated

on-site, each contal~er ~r.d ~~r.< ~=

:~~elec or ~arked c~early ~it~ the"..;orcs<t n~.:.lzardous ~';aste"; a nd

(d) 7he p e r I od s or retentionr c f e r r c c t o in this section are0xte~ded ;luto~atically during thec ou r s c 0: '~n:~" unresolved enforcementt c r i c n r~.r;~'.rdl.ng the r ag u La r e d

.!ct:";'.t·! "r ~\S requested by the,.,ec r e t: 2 i» e

(~) The gene~ator co~~lies

~,:i.th t::e requirement:s -:01:"' owne r s Or'

ope r a t o r s :"n Su bpa r t s C and D :'n Pact265 and ~ith §265.16.

(3) A gene ra t o r whohazardous waste o f r r s I teAnnual Reports:

ships hismus t submit

D~REC f o rm s 8700-13(b) A generator ~ho accumulates

hazardous waste for more t ha n 90 daysfs an operator of a s t o rag e f ac i l Lt y.md is su b j ec t to ::he requirements ofPar t 264 and 265 :'inn the permit:"l:~cr~i!"ernent of Pa r t 122 unl e s s '":1;.1 ·~2.S

(1) Ona nd 8700-13ALns c ruc c i ons on~?Dendix to this

a c c o rd Lngt:--:e fO!"!71

Fa r t ) :

to(See

thethe

Such ,=:·::e!1sion nay :~

e:-:~c~sion

~~zarc.ous: ::-y D:-JR;::C- .... ,; ..... -: (l,··

(J) No later than Harrhfor the preceding calendar year.

(b) Any generator who treats,store's, or disposes of hazardous wasteon-site must submit an Annual Reportcovering provisions of Parts 264, 265and 122.

§262.43 Additional reporting.

The Secretary, as he deems necessaryunder 7 Del. C. 6305(a)(10) , mayrequire generators to furnishadditional reports concerning thequantities and disposition of wastesidentified or listed in Part 261.

§262.42 Exception reporting Subpart E-Special Conditions

?pneriltor must:

§262.50 International shipments.

(1) Notify t he Administratorarid Se c r e t a ry In .... riting four (4)weeks before the initial shipment ofho z.r rd ou s \oi,1ste to each country inerich c-;,; l e ndn r y e a r ;

(a) Any person who exportshazardous waste to a foreign countryor imports hazarrlous waste from aforeign country into the United Statesmust comply wi t h the requirements ofthis Part and with the specialrequirements of this section.

When s h i pp I ng hazardous wastethe United States, the

( b)

outside

(a) A generator who does notr0ceive A copy of the manifest witht ho hand written signature of theOWT1('r or operator of the designatedf a r Ll t t y within thirty-five (35) daysof the d a t e the waste was accepted bythe initial transporter must contactt h e transporter and/or the owner oro pr-r a t o r of the d e s i z na t e d facility tod e t e rrn f.ne the status of the ha za rd o usWi1st"P, .lon rf [t n.1:' not hor-n

deliverNj the genera.to r must identifyt ho shlp:'1ent .1nn rr- po r t i r bytelephone to the State in which theshipment originated.

(iii) These notices mustbe sent to: Office of InternationalActiVities A-106, United StatesEnvirol1lnental Protection Agency,W~shington, D. C. 20460, .andDep':Htment of Natural Resources andEvnironmental Control, P. O. Box 1401Dover, Delaware 19903. '

was t e must behazardous waste

and its DOT

(b) A generator must s u bm i t anExc e p r t o n Report to the m;Rf.C [f !lr'

h;JS not received a copy of themi1nifest/shipping paper with theha ndvr i t t e n signature of the owner orop('rator of the designated facilitywithin 45 days of the date the wastewas accepted by the initialt r a nsp o r t e r a nd the geneLltor rnn s t

also notify the State in which then.mf f e s t rrto s i g na t ed facility i slocated .t nd the State to vh i cb t h.:shipment may have been delivered or to

EPA in the case of unauthorized states.

The Exception Report must include:

(i) Theidentified by its EPAidentification numbershipping description;

(ii) The nameaddress of the foreign consigneehe included in this notice;

andmust

(2) A cover let te r signed hyrbp ~cnprator or his authorizedrepresentative explaining the efforu;taken to locate the hazardous waste.1nd the results of those efforts.

ma n t f o s t

no t have

(1) A legible copy offor wh l c h the generi1tor

confirmation of delivery;

therI0(' S

(2) Require that the foreignconsignpe c o nf I rrn the delivery of thewas t e in the foreign country. A copyof the manifest signed by the foreignconsignee may be used for this purpose:

(3) Heet the requirementsunder §262.20 (a) and §262.21 f o r themanifest except that:

(d A generator must file anSycent:on ~eport, if:

(i) In r1ace of theTI2.me, add r e s s , and EPA identificationnum be r o f the designated facility, the~"r.:e and address of the foreignc0~si3nce must be used;

(ii)i'ientify t he point:h~ enited States~aste nust travel~'):'~i.~n count:'y.

The generator mustof departure fromthrough which thebefore entering a

or 265 for those wastes p r o v t ded hetriple rinses each emptied pesticidecontainer in accordance with§261.7(b)(3) and disposes of thepesticide residues on his own fann ina manner consistent wi th the disposalinstructions on the pesticide label.

(AppendiX I - Annual Report­(DNR'EC Form 8700-13))

(

(1) He has not received a~0~Y 0= the manifest signed by the~,~~sporter stating the date and placeG~ ~eD~rture from the United States',o:th:'n 45 days from the date it was.c c c o t o-! by the initial transporter;

or

(2) '..iithin 90 days from the:~::lte the waste was accepted by the>~tLl1 transporter, the generator has~ot received written confirmation from... '-,..., ~oreign consignee that the:::? za r c ou s waste -:';3S r e c e I ved.

Cd) ~hen importing hazardouswas~e ~ person must ~eet all there qu i r erne n t s specified in §262 020 (a)~nd S262.21 for the manifest except

(1) In place of the-cne r a t o r ' S name , address and EPA:~en:~~!catton ~umberl :~e name ~~d

(

.idd r e s s of t he~he i.:::porterls

f 0 reign:::e ne r a to rname , ad d r e s s Q.nd

d rid

i d e n t i Li c a t i.o n nua be r raus t Je used.

(2) In place of thegenerator's signature on thecertification statement, the U.S.importer or his agent must sign anddate the certification dod obtain thesignature or the initial transporter.

§262.51 Farmers.

A fa~er disposing of waste'.),=st':ciccs from his own use whd c h are-.~_::::.:.~r:-:)~.:c:: ~;aste~ ~!:; ~0t :"t::quired t:0

':~ry~y ~~th :~e st2ndar~s in this ?ar~

APPE~1)IX I -FORM-ANNUAL REPORT(FORM 8700-13)

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i II

PA~C __ OF __

General Instructions, Hazardous wasteReport (D~~~C Form 8700-13)

Important: READ ALL INSTRUCTIONSBEFORE COMPLETING THIS FORM.

Section I. Type of Hazardous WasteReport

Part A: Generator AnnualRepo r t r-r-Fo r generators who s n i p theirwaste off-site to facilities whicht ho y d o not own or operate, fill inthe reporting year for this report(e.g<, 1982).

Section VI. ~nstallation Contact

Enter the name (last and first)and telephone number of the person whomay be contacted regarding informationcontained in this report.

Section VII. Transportation ServicesUsed (For Part A-Reports Oh~Y)

List the EPA identification Numberfor each transporter whose servicesyou used during the reporting year.

Section VIII. Cost Estimates forFacilities (For Part B Reports ONLY)

Note--Generators who shipha z a rd ou s waste off-site to a facility A. Enter the most recent costwhich they own or operate must estimate for facility closure incomplete the facility (Part B) report dollars. See Subpart H of Parts 264instead of the Part A report. or 265 for more detail.

Part B: Facility AnnualReport--for owners or operators oron-site or off-site facilities thattreat, store, or dispose of hazardouswaste, fill in the reporting year forthis report (e.g., 1982).

B. For disposal facilities only,enter the most recent cost estimatefor post closure monitoring andmaintenance. See Subpart H of Part s264 or 265 for more detail.

Sectic~ IX. CertificationPart C: Unmanifested ;';aste

Report--for facility owners oroperators who accept for treatnent,s t o r ag e , or disposal any hazardouswaste from an off-site source withoutan a c c ompa ny Lng manifest, fill in thedate the waste was received at thef~cility (e.g. 04-12-1982).

thru Section IV.LD. Number, Name ofand Installation :1ailing

Section V. Location of Installation

Note--Since more than one page isrequired for each report, enter thepage number of each sheet in the lowerright cor~er as well as the totalnumber of pages.

AGenerator Annual Report, PartInstructions (DNREC Form 8700-l3A)

The generator or his authorizedrepresentative (Part A reports) or theowner or operator of the faci Li ty orhis authorized representative (Parts 0and C reports) mus t sign and date thecertification where indicated. Theprinted or typed name of the personsigning the report must also beincluded where indicated.

aTT1.1.

receiveSection

If you did notprepri n t e d label, completethrough Section IV.

Section IIInstallationInstallation,Address

If your installation locationaddress is different than the mailing~ddrcss, enter the location address ofyour installation.

Generatorgenerators whowaste off-sitethey do not own

Annual Report forship their hazardousto facilities which

or operate.

=~po:"t.:lnt: ?EAD ALL INSTRUC'I'IONS3EFO;?£ CO:1?LZTING THIS REPORT.

For un I i s t e d ha za rd ou s !"';l~t('

u nd e r ').;~'!"'"t 7'_·61, Su bp a r t C';i. den t if i e<i . f c; n. - - -

C,elicve best describe5 the wa s t c .Include' th('snecific m;lnuf.1ct\lrin~ o rother process generating the wa s t e( s Lcd ge from ~iaget,,('.g. :;ree:l -.,~<1nllfrtcturi!1g) and 1.£ known, thechem i c o L or generic chemical name or

Section :CNum be r

Enternumber.

Generator r S

your EPA

Identification

identification

:?:1ter the descript:'on whi c h

(

Section XIV-B. DOT Hazard ClassI ...j x QfNf"ATO'I"'tfJll4fO.MO. 7"-

btl..~llili /211 iJ 18 i~ c:I1

Section XI.Ident~fication Number

Facility's

En t e r the t:·~..o dlgi t code r rom.. . o nd s 1"_0 the DCTTn b l e 1 '..;illen c o r r-e sp '1,'

hazard class of the t.....aste described./ ~r- t"ha W'Clst(1o described ha s be e n\ ......~hipped under more than one DOT hazard

~e~~t"ate line for e;'lch.:1.ass, use n,,:":)f)T haztlrd t.:L~lSSe >

i::nter the EPA identification number o ft~e f~cility to which you sent t~0.

va s t e described below in Section XIVC, se pa r a t e sbr-e t must ~(' us"rj ,-"r-

each facility to wh I c h you sent1-1:1 za rd 0 II S '.';<1S t e. )

Section XII. Facility Name

TAHlE: I

,1).lu

; '",1""'1" ",non I

, ,:"""l"\,,,,P J'i

; '"';",,vu H

~ .""",,.,.,t,,,,, ':"' ...

-···:" ....'1 ,n,'·""

:'~nte r the

CC' r r e s po nd i ng: " P n t i ~ ~ c n. t ion

name of th~ facili~y

to the facility's ~PA

nurnher in Se~t~on Xl.1. 1,\",,-, ..... ~

Section XIII. Facility Address

Enter ther:orrE'spondingt("~pnt i fi c a t ion

ad d r e s s of the f ac t Lt t vto the facility's EPAnumber in Section XI.

Section ~IV. ~aste IdentificationSection XIV-C. D~REC Hazardous WAste;:Ul!loer

Section XIV-A. Description of ~aste

~,~thDt:1rt_-:: (....._.,. -O!:"':: ~'h.·t~

-,.,...'".'_:\:. 't

Fo r liSt",d '....a s t e s , e n t e r t~('DNREC

~zA.rdous :.J;'!.~te ~Ju~~pr flam Pa r t 2St,3ubnart ), ~hich ~dentifies the ~~~~te~

For a. rn i x t u r e of raor e t ha n o neItsted wa s t e , ert,-'r e ..ac h of t hr-applicable DNREC ~~zardous ~:lste

~;um;'ers. cO'.1t" S f.' Cl c e s a rc p r o v Lde d .IE more space is needed, continue onthe next line(s) and leave all otherlnfonnation on t ha t li.ne blank.

Foe <:~l.<.~':"d ':azarcous w;Jste<;,t""'!'1ter the DNREL:~..j~;lrdOtts :AJd~te :;um~erq

t ha tareSUbpt1rt D,a',)hrevL·--;tpri

F'Jr ha za rdous wastes1i..~tC'd under Pnr t 2i)1,{''itnr t he lt~t{?d :1;!fl'!e,

All 1Clformation ':n this section::"ust "'(' "'ntered by l~ne num be r , c.a c nI!~p entry will descrihe the total:If',r1U,ll .irnou n t of ea c h \';,3ste shipped tothe E2cillty identified in Secti.on XI,

~oi2i\Z.-Jj.-6...JiI" Q S '1 it{]jt- ,,,\ t!j~ 4;, Ilj.,.~ , .. .. .. ...lj '~ 6 ~.

Section XIV-D. Amount of Waste

Enter the anount of this waste youshipped to the facility identified inSection XI and include the weight ofcontainers if left at the treatment,storage, or disposal facility.

Section XIV-E. Unit of Measure

Enter the unit of measure code forthe quantity of waste described onthis line. Units of measure whichr.111St be used in this report and theappropriate codes are:

Un i ts of measure

PoundsShort tons (2,000 Ibs)Kilo';; ramsTonoes (l,OnO kg)

Code

PTK

Units or vo Lume nay not De usedror ~eportjn~ hut wust be ~onverted

into one of the above units of weighttaking into accollnt the appropriatedensity or specific gravity or thewaste.

Section XV. Comments

Th i s space rnav beor clarify any entry.<J cross reference toSec t i on n urnbcr.

~otc.-Stnce no r ereport,shce t

r-equired for each

used to explainIf used, enter

the ap p r op r i a t e

one rage LS

enter this1:1 ~_;'e lower

:"or::1 3700-22

D~REC

Solid '..Jas t e :;anagemen t B'ranc hB9 K:~~s ~i~hway

.., 06 Jc:-: 1401Jover. JS 19903

!den~~~v your shipment category and follow 3.

~o. of Wastes according~o UGSO DOT shi~Di~2 n~~e

4 or less t~3.n

more t::'J.n.:. or :tlSS _:. ....-

........ .:. ~ 1

~or.....: t ,;::::

.:1

-:str:..:ctio:1S .\

i n s t r uc t Lon s ::or

l~' ~ '_ :.:":

(

" _~ ..... 1.", """-

1'- - • -: State .... ; \~. . : '""

- ""

1" Generator c ornp Le te s t.he Cerie'r a t o r por t i.onor t h e ~bnifest and has 'I'r anspo r t e r ;;0. 1sign and certify receipt of the shipment.

2. TIle Generator detaches the Green Copy andsends it to the Generator State and sendsa photocopy of the Green Copy to theFacility State. The Generator retains aphotocopy of the Green Copy.

3. Tr~nsporter No.1 carries the re~aining

copies of the manifest along wit~ theshipment.

4. Upon delivery or the shipment to theDegignatcd TSD Facility or Transporter~~o. 2, Tr~lnsporter Xo. 1 3i~ns an~i

ccrcifi2s Jeliv~ry of ~l:~ ~ni?~e~[~ ob­Lains the signnturc :lnd cer~ific3[ion ofthe TSD Facilitvfs ~uthcrizQd re~resentative

or 'fransporter ~o. ~ a~d J~taclles ~nd re­t8ins the Green Copy of the manifest.

').. 'G;)i)n d c l Lve r v Ot7 the: sh i.pmen c to the

De~ignated TSD Facility. ~ransport~r No.2sig~s 2IIJ certifi~s delivery of the ship­ment. obtains the signature and certifi­cation of the TSD Facility's authorizedrepresentative and detaches and retainsthe 1;·tnite Copy of the manifest.

6. The TSD Facility detaches theBlue Copy and retains a photocopy and sends the Blue andYellow Copies to the respectiGenerator and Facility States~nd sends the Pink Copy to thGenerator.

7. Note the above instructionshold for Interstate and Intrastate shipments. If thereare any questions or clarific,tion regarding the instructio!please contact the D~REC,

Solid Waste Mana~ement Branch? O. Box 1401. 89 KingsHighway, Dover, DE 19903 orcall (302) 736-4781.

JNIFO~~ ru~ARDOUS ~ASTE

I~S7~UCTIONS (Form 8700-22)

~~ ALL INSTRUCTIONSCOHPLETI~G THE FO~~.

JEFOP.E Fl,,(:ILI-:'IEsRESP0~S rELE FC\R CO~P~E7::C8N

?OLLc)WI;~G ~::·;FOP.Y:.J\T :0:';:c·:

(

This f o rm ~3S designed to be used >J~": ;J

~2-:)itch (elite) t ynewr i t c r , :;0 v;e \1e r ,

a fi r:n point pe n may be u se d -- p r e s s

d ovn hard.

.~ * * * * * * * * * * * * * * * * * * *

GENE~~TO~S: ---------------------------

7EDERAL ~£.GULATIONS F.EQU!RE ~2E OFIJ~;r?O?.M :BZA.'illOUS WAS;:'!:: "'AN r?;;:ST ?O?l13700-2~\ CONT::ruATION S~EET (:7NECESSA..::tY) BY OPERATORS OF ~·L4_Z_AR2)CUS

~~5T~ ~A~AG~~NT FACILITIES (TSu:s) ,~

Item

En t e r y cu r EPA ID numbe r t n

::h e fir !; t t ve 1ve 5 p (..1 c e s " Ln.:he last five spaces a ~umb~r

mus ; :c.ppear wh i c h Ls unique

co e a c h shipment made during:?{lc~ c a Le nd a r y ea r bv t~l£-\

~or purposes,'1 s a i pme nt;~,r::lnsf)ort of

oft he '11 ani f e s t ,refers t a thehazardous waste

:~itially acceptedz r a n s po r t a c Lcn in <l

~ra~sport vehicle.

forsing Le

Con:i!:.uc:ion, .... t-, ...

-:o u to cC"lplete

of

and~. ,c ne o t )

- ., ~ L:= ~:~:: " -:0 rex ~~"7l P1. e ) i f~:~n -~~i~est only consists of-'c, ··:-·~t ,age (:0:"":' 370 f)-22)

-, ."; , r C.'-.~ -

~ .... ,-, -: ' ...,I _ ___ .. l,. 1 _

.J nc ,-' ,j( '?0 '::;-;

c o r r e c t... ,"c v'

';enerator' 'S

Item 4- GENERATOR PHONE ~1P.1BER:

Enter a telephone numberwithin your organizationwhere a knowledgeable personmay be reached who can giveinformation in response to anemergency.

Item 10- EPA I.D. NUMBER:

En t e r the EPA :m numbe r andphone number of thedesignated facilityidentified in Item 9 to whichyou are sending the wastelisted on this manifest.

Ite~ 5- T&fu~SPORTER #1:

Enter the first transporter'sname.

Item 11- U.S. DOT DESCRIPTION(Including ProperName, Hazard Class.I.D. Number (UN/NA»

Shippingand DOT

2PA I.~. :.ftJ1iBER:

~·.~CI2 r, . .. J.ppli.c3Dle, '[['iesecond transporter's name.

Item 6-

Item 7-

Item 8-

EPA I. D. t-,'UHBER:

Enter the EPA IDphone number oftransporter.

number andthe first

Enter the DOT proper shippingname, hazard class and DOTI.D. number (UN/NA) for eachwaste entry. The U.S. DOT(Department ofTransportation) regulationsnus t be c ompLd.e d wi th inc ompLe t I ng this part. Youcan find these regulations inTi t Le 49 of the Code ofFederal Regulations (49 CFRPart 172).

(~~OTE :

En t e r , if applicable, the EPAIJ number and phone nuzabe r ofthe second transporter.

If additional transporters areused, their narne s and EPA LD.n~mbers must be entered in thespace p rovI dcd on theContinuation Shee tf D::JREC Eo rmB700-22A). each ContinuationSheet ·,.;i II ac c ommod a t e t vo

It2m 12- CONTAI~~RS: :N~BER AN~ TYPE

Enter the number ofcontainers for each waste inthe appropriate columnfollowed by the appropriateabbreviation from Table I forthe type of each containeryou are using to oanage thewaste described on each line.

.dd i t i o na l transporters. TABLE I

Ite~ 9-

~~very c r a nsp o r t e r usee between2nd

design.:ltQc f a c i Lt t y ~::ust ~--:

li seed on the rnan i f e s t in t hec o r r e c t order.)

DESIGNATED FACILITY _~~D SITEADDRESS:

Enter the name a nd s i t eaddress of the designatedfacility to which you aresending the wa s t e listed onthis ma rn f e s t . ..ne a.td r e s sentered c::ust d e s c r i be thesite l cc a t i on a c d r e s s aDO 25

such Clay be d i f f e r e n t f r onthe site's ~3iling ciGCr~ss.

(:ype of Containers)

~etal drums, barrels, keysWooden drums, barrels, keys

F~~f~!"~O.1.r-d o r p La s r i c ~ruz:s,

:;i.lrr(~· l s , keys;''r)r·t;:.~le t a nks •~~~~0 :anks (tank trucks)T,qni-.: C.::lrs:JUr."!.D 7rucl<C'..~ 1 i.nd (~ r s

~e:al boxes, cartons, casest i ~c ~ ~G.in6 ro .!.l-of f s ):.-, :~,:r c r plastic boxes, c a rt o n s ,

~.\ ·~~~s ~3de of ~urlap, cloth, paper0t" )~.:l-;tic

I tern 13- TOTAL QUANTITY A...''iD UNIT (We./ 'Io!...). :~\ZAP..D CODE A.."lD \';ASTE NUMBER:-----Item 14-

Item 16- GE~~RATORfS CERTIF!CATIO~:

Read the cerci f i c a t Lo n statement.Type or print your name a nd s I g nyour name on the ap p ro p r i a tt' line.

INTERi~ATIONAL SHIPMENTS:

Generators must enter j n the"Special Handling Instructions"box the poi n t of departure (Ci t yand St.:lte) for those shipmentsd e s t f nc d Cor treatment, storage ordisposal outside the jurisdictionof the United State"'. Be sure toleave e noug h sp ac e for thetransporter to enter the date theship~e!1t Left the United States.

(

Fo r '.;"e waste described on each~~r:I>, « nt e r the t o t a I qua n i t i t y of~~1t.: '.,,·.~st .... u Item 13 the and the.o o r o o r io t c unit of rnea su rc:jor,'vi.,ltio:1 (from 7,'lble II,':.1\;1.::1) c od e a nd Waste Numbe r in

(:':0,,[2: : \11Cor

0: thewh i c h

a bo ve informationt h e generator is:-:Jay Se ;"lrept"inted

the nand'.. ritten

*~**************************************

T.c-\BLE II(Units of ~easure)

(liquids only) L litersTRA1"IS PoRTE?.S

(liquidso~LY:---------------------

name of thematerials ontransporter.

and date thespace upon

thethe

first

o r type

acceptingo t t he

?~int

"erson':Q::(11~

:'~:J.::: pe r s o a must s i z ncani:est in this

only)Kf Log r arns Item 17- T?ANS?O?.TSR I AC~:Q';.n.EDGE}(.E~1T

me t r i c :::ons 0;: ?ECEIPT 02 :1ATERL',LS:K

;: r o ..~ i. ,:-: 2{~ ,-.

S:-~~e t :~?~~-

cescipr.:'0ns,raus t be e n t e re c

If .add t t t cna I s o ac e i.s rc cu i r e c:or waste':':1':or.:Jation

poundsto!1Sc u h : c V:1 rc q

?

second~hatevent

; ~ !~-:2 : ..'.. '.

info~a~ior!., if u s e d , and point ofdenacture fro~ the ~nit2d St2tCS(for' .~:1ternational s h t ornen t s ) cus t

t r e a t ae n t ,

Lnf o r-na t Lon ,

r r.t n so o r t e r is used to t r a n so o r t~~'= ~/:.3s:e~ 7ri:1c o r t y p e t rie ~~lm~

0: the person acc e p t t ns,; tr:er a t e r i a Ls on. be na Lf of the secondt rn s noo r t e r . That person 1:tUSt

si~n anc Jate the manifest in :::~is

s?~ce unon assuming custocy or the'.... a s t e ,

co

hand La r:.g

:'Y'special transport~t:on,

storage or d Lsco s a IAlter~ate facility

indicdr.:e:or

INTE~~ATIONAL SHIPMENTS:

ADDITIONAL TR&~SPORTERS:

(NOTE: Additional transportersmust a c k now Led g e receipt of was t eshipments rrom?re'lioustransporters on the ContinuationSheet' (EPA Form 8700-22A). Seethe instruction for theContinuation Sheet.)

The transporter who takes theW;lste identified on the manifest outof the United States must enter thedate the hazardous waste leaves theUnited States. This entry must bemade I n Item 15 "Special HandlingInstructions" after the g e ne r o c o r ' s~ntry Eor point of departure (city ands ta t e ) •

the person accepting therepresents an alternate

that person must so

Transporters taking hazardouswaste outside the jurisdiction of theUnited States are, in addition totheir normal hazardous waste managmentrequirements, required to indicate thedate the shipment left the UnitedStates.

SPECIAL NOTE CONCERJ.'HNG INTERN·ATIONALSHIPMENTS:

Shipments of hazardous wastedestined for a foreign country butoriginating within the United Statesmust comply with Sec. §262.50 and263.20 of the Delaware regulationsgoverning Hazardous Waste.(Generators are advised that foreigncountries may require specific formsfor use in their country.)

(NOTE: Ifshipmentfacility,indicate. )

TSDF'sOFOPERATORS

Item 19- DISCREP.~~CY I~ICATION:

OwNERS A...'fDONLY----

In Lhis space the authorizedreprcsenrativi or the designatedor .i l t o r na t c ) "?cility's owner or

op e r.r r o r must no t e any sign.i.ficantdiscrepancy between the wastede sc r i be d on the manifest and thewaste actually received.

If v o u cannot resolve significantdiscrepancies within 15 days ofreceiving the waste, you mustsubmit a letter with a copy of themanifest at issue to theDepartment describing thediscrepancy and your attempts toreconcile it.

Shipments of hazardous wasteregulated by 7 Del.C. Ch. 63 ando r i g Lna t Lng outside the United Statesmust be accompanied by a manifest.Transporters of such hazardous wasteare responsible for completing themanifest when hazardous waste istransported into the United Statesfrom abroad (40 CFR Part 263.10(c)(l)of the Delaware regulations governing~lzardous Waste.

Item 20- FACILITY OWNER OR OPERATOR:CERTIFICATION OF RECEIPT:

Print or type the name of theperson accepting the materialsrepresented by the manifest onbe ha l.f of t he vowner or operator ofthe facility. That person mustsign and date the manifest in thisspace indicating receipt of thewaste described on the manifest.

"'7",=,'. .~ ... ,,~ - ~ -' ~

?.:.',~e ::\~ 0:::71(1 t.:'O!1 :.:1 :~e

of __ ;shaG~d ~r~n ~s noc~, ""~~1';':' -J{'J ~ ...,. (~der.:1.L l...a~~

State Marliics: Nurnoer

(

?)..,one ::t

Phone if

Phone if

\I

'1 Designated r2cility and Site Address lOj EPA LD. Number

6] EPA IO~G Numbe~II

~ 1 Transpcr ter 2 :h~ -_.'-' -_._-----.-- .•. :·S-1 £1'A·-'::.l..-.-;D:;-.-;N:;:'u~-=m:;:b:-e~r:-----""':::..:lQI~...:J.~--------------I

(1 Generacor ?hone ~umber (---_ !rs.nspQrt~r 2. :iame

_~_} U.StI ::0:' Jesc.r~_?::.on (i:1cl:..:dit:(~ P~"oper ShippingHazard Class, 2rid lD Num6er)

~ --;T"J"i----.,.--:-----:--=--~-------_ame t C3nt~iners

~,! 0, ~ 1'vT) 12;• 1. ,

I

I--------_._........_-----,.._---

IiI

iI--.-. -.-.;,- -+- ~__...l. _

i 1! :;

I

!._-,----,--.._--~-~-..;.------_ ..._..._-- ...._-------------_._---

.Jj Special nandlign Instruction and Additional :o:or~~t~cn

classifi~d, cicsc=ibed, packaged, ~a~ked.!~2nc l~~eled and are in prcpe~ conditicr\ fortr~,spor:~~ic~ accoraing ~o :~e a~p~ic3D~c re~ul~:ions of t~e Dept. ot Transportat~on ~ 2P~i

.)1 Generat~='s Certification;

~.()n C.:l !.)C<" '~·:~O r!·r

:~81 Transpo'Cter I Acknowledgement or 3.ecei?c O~ Y:.lter2..:i ... 5

'.{

Ddte

;~tonen L:ay!

.. . ,-... '- 4.

:9] Discrepance Indication Space

.... ,..~·r.::.~f.~.r:.·.

DEPARTHENT OF NATURAL RESOURCES A.i.\'1) ENVIROJ:0fENTl.J.. CONTROL

Form 8700-22.:\

DNRECSolid W~ste'Managcment Branch89 King::; HighwayP. O. Box 1401Dover, DE 19903

INSTRUCTIONS FOR PREPA~\TION

Routiw; of the Continuation Sheet

Instructions B

DE-A-

:1ailed byGenera tor t o

Gener:ltorState

:-:ailcd byFac ility to

GeneratorState

:-failed byFacility to

FacilityState

Hailed byFacility to

Generator

Retained by

TransporterNo. 1

Retained by

TransporteNo. 2

Gree:1 copy OL Blue copy of Yellow copy of Pink Copy or Orange Copy of ~fuite CopyManifest & :ianifest 5. :ianifest & Manifest & Manifest & Manifest &Cant. Sheet Cant. Sheet Cant. Sheet Cant. Sheet Cant. Sheet Cant. Sheet

(Generator shail mail a 7hotocopy of the Green Copy of the Manifest & Continuation Sheet tcthe ?acility State and retain a copy.)

(Facility shall retain a photocopy of the Blue Copy of the ~anifest & Continuation Sheet.)

1. Generator CO~?l0tes ~lanifest and a Continuation Sheet ~nQ h~s Tr~nsporter ~o. 1 signand certify receipt of the shipment.

2. Follow the instructions A-2 through A-7 for both the Manifest and the ContinuationSheet.

C0Pi.~S •

ro F.lcillty SUI

Ru t a Jn s photo-

IS~nds Yelluw I,: o p y 0 f H;, ni f,~ .: I I;\11.1 c on (-. ;;;l:-.:l: t I

I

,..'-_ •. -."""

...-.---=~·~=_=~:.t~ _FACILITYn;.'",:;\'(;l:-i'El( ~lll t;

1'l.'I,.iIl6 \lllil~~

,-dFY .,f c ou t.. ~1,J1L ,:t .

: ~ ,." .. l I J•

Or ~:ln!~c

etolll,

1-_'i,

'j.C\IJ~;P(Jl(ILR ~,I)" -;

IkLl insl"1PY o f

- ..~,I ~,lie c l .

. 1 i ·d._.- "",,'

I ,-~ , \ .. j •

HetaillS_ til. i rec. Q PY u l' L _ ,I' if,., :jl

..., -.... . .J'I\ANSl'IJKn:H i.o. '2

,-'"

Rura Jn s OLJI1(~e

cnpy of III',n.! f',:l.1

(._.......--_.._------_.-

- - --.- --.------ "1 '-------~r.._··..-- - _.-.. _.--..----- ------- . -. 111(\- te."r' •. ' S'L3-

..... . h'~o- ,- -.. .. , H.'0'-' (3 lO-'" .- ,y o~-;-Genc;........ eO\~;t t_. .10

0--::\",0,.---..-- OS ---'l',n"--"-'t Sen _. t 1

....-:"Il\\)·\., c-, • • ---'Coo t "CILlTY

·~'''Otoc"".O"o( c-; . -' I l.,Clild CU-;}ti~I;;:1 (7)~-~I--;-~"~.'..':":!l.- ..£-~.fY---.2!_!Il'ln i r('s~t-".__ STAT!

'n "h L t (1) }';J c 1. 1i ty e'---t _________

., '''''. ~ .

.;.- -~----_.,.. ,>------- "fIONS C---------- ltlS']'~~!l:- _-- --,----:;j',\'1'£

l,j-;;fRATOR

_~ . Ji.:-~! ~~l :!..L ! ~U~'...'_ '::~ l~ 'i :. ~.~ .!.!~ :~.i, !,. ,_:~~.~-- ::.~~ ~

l. [:'-;;Eri~\~Oi{---'-l trRAi~~;f;()i;-'j;I~-I{-Nn].:C~'I.JS Crecu copy

" f UI;ll1 i f e s t and-'Ollt sheet to(-L'll~ r a tor S t a re ,f"---;'

p,!L~ins photo-copies.

I'll',,,q: cdll IlHREC office at (02) 736-4781 for c ornp l e t e detailsIor I,,'LII C t. II typ e s of transactions .

.-....-- - --_..•.._._---,._._--_._--._._._.._--_._-- -- ..-_ .

Sends all f ou rYe 1 I ow cop i e s r oFuc i.] t t y State,

_. 1 Ret a :in s Ph <Jto-­--.II

cop i e s of al l '.pink copies.

WI i t econ t .

and 2

Retainscopy ofSIH!C t 1

-~~\Ns;~I~~~l;:~·:(~-!---I~~~~-~~~~·;-~~t l'Y"·-"--'·"···

--)

Or augeCall toand 2.

Retainscopy ofshc e t 1

THANSPORTER NO.TRANSI'OH'fER NO. 2

I:l~ r a in s t,Jh i t I~

c o I'y 0 f Hi III if c" t

1 .m d r'llniL-:,t:2

.5."':Jll,b..j.ll L.lQ!!LrJn1.(!'...Q2..i e.~_ ..tQ...~cl~e l:clt or

I H.\i,jSI'Oj(I'LR hf\

1-:('1,1 i ,1:> (jr,dq',,~

': .... I.y o I !'Idld 1'1',,(

. >11 ;111 d : 1. .u i f '-',; l ~)

-....,r~~~. ..I; I;: J-,RATOR~;, 11.1::; Cr e.(

ecn COlI

t P l i1 1 L) f --, I 0,1..l1i[e,stl [, ')t. '<lilt- "I ~,_) .' kC't I" •. I{el.idns1)I., ' t c t' c .. ' .. .p i e s C-

:111 L' ~ 0, '. I Cr e en

~:~.~l~~/ •~-=~~nds"... .. ... ..........,-.,. ,-,

co",") hot ,.~0.: s- f-------- Oc°1" ' --.-,---o 1'--'_ les . '--dt~ "1"- of . ~ •

, 1 _ 1 t:--- d 11 .--._--., y S"" P ----.....~ t.l ,.---.""" .. _.~- ....,

l:; 'O"r> _..... _...-.. "'1 e --~,~"" • - ---- --_.-

... •",.Ol< ".

:,(\n: . '. --~ scnds all foo~.S"1'~,-,..~_J.. , ..' ... ,- __",----~ s . t'V' ... ' ,_". "- ,---------- . ' "'-.. ",oe r a to' ta ,.. -----...

INSTR_ .. ,_-"CTlONS J) ------.--..__.._ -------------f FA;;:'~;Y--~ STArE

/_.\

This form was designed to be used by al2-pitch (elite) typewriter, however,a friw point pen may be used -- pressdown hard.

THIS FORM (8700-22A) HAS BEEl~

DESIGNATED FOR USE BY GENERATORS AJ."IDTRANSPORTERS OF HAZARDOUS W~~TE ANDOWNERS AND OPERATORS OF TREATMENTSTORAGE AND DISPOSAL FACILITIES. ITIS THE RESPONSIBILITY OF THE GEN~~TOR

TO INITIATE A CONTINUATION SHEET IFEITHER OF THE FOLLOWING CONDITIONSEXIST:

INSTRUCTIONSFORM 87-22A

(Continuation Sheet)

RR~D 4~ INSTRUCTIONSCOMPLETING THE FOfu~.

BEFORE

Item 22- PAGE OF

Enter the page number of this form(Form 8700-22A) in the first blankand the total number of pages ofthis manifest [front pages (Form8700-22) plus all ContinuationSheets (Form 8700-22A)] in thesecond blank. For example, ifthere is one front page and oneContinuation Sheet, then thecorrect entry here is "Page 2 of2". If there is one front page;ith two Continuation Sheets, thenthe correct entry for the firstContinuation Sheet would be "Page2 of 3" and for the secondContinuation Sheet the correctentry would be "Page 1 of 3".

Item 23- GENERATORS NAME:

a

a

MORE THAJ.~ ?WO TRANSPORTERSARE TO BE USED TO TRANSPORTTHE SHIPMENT

MORE THAJ.~ FmJR KINDS OFWAST/l1ATERIALS ~~~D/oR TYPESOF CONTAINERS ARE PART OFTHE SHIPME..~T

Enter the generator'sappears in Item 38700-22).

Item 24- TRANSPORTERItem 25-Item 26-Item 27-

name as it(on Form

If you require more than twotransporters to complete theshipment of the hazardouswaste described on thismanifest, enter the name,EPA I.D. Number and phonenumber of each additionaltransporter in the order inwhich they will transportthe waste. Be sure toindicate in the spacefollOWing the word"Tran spo r t er " the order inwhi ch they carry the waste(e.g., 3rd, 4th, etc.).

If you require additionalspace to list the hazardous

ing Proper Shipping Name,Hazard Class, DOT Identifica­tion Number); CONTAINER &~D

TYPE: QUANTITY;

STATE REGUL.A..TIONS RZQUIRE USE OF EPAHAZARDOUS WASTE MANIFEST FOR..'1 8700-22AND 8700-22A CONTL~ATION SHEET (IFNECESSARY) BY GENERATORS A.~"D

TR..~.NSPORTS OF HAZARDOUS UASTE AJ."iDOWNERS OR OPERATORS OF HAZA.ZDOUS WASTEMANAGE...'1.EN'T FACILITIES (TSDFs) ..;5 ACONDITION OF TRANSPORTATION.

STATE LAW ALSO MAKES GENE..1{ATORS ANDTIL~"iSPORTERS OF ~~OUS WASTE ~~m

OWNERS OR OPE..~TORS OF HAZARDOUS WASTEMANAGE...'1B~T FACILITIES (TSDFs)RESPONSIBLE FOR COP..PLETION OF THEFOLLOWING INFOfu~TION:

GENERATORS:-----

Item 21- H}J~IFEST DOCL~E..~T ~~BER:

Enter the same Manifest Docu~ent

Number here that appears on thefirst page of the manifest (foro<3700-22) •

Item 28-CInclud­Item 29­Item 30­Item 31-

u.s, DOT DESCRIPTION

Enter ~ny special handlinglns~=uctions ~cre which are

c'?,e last t r ans por t er ',;::'0

carries wa s t e inside t:"cjurisdiction of the UnitedStates ~e£ore it is exported~ust indicate the exportdate in item 15, SpecialHandling Instruction andAdditional In£or;nation, onform 8700-22.]

rwiDLIXG

~ ..~ ,

e n t er their:£or"::ation

SPECL\L

was t es'"Jal'.ifest,a?propriatencr e , [See Las t r uc t Lons fo::G~~er~~o~s (For~ J700-22)0]

INDICATIONDISCREPANCYSPACE:

OWNERS A1~D OPmLATORS OF TSDFs ONLY:----

Item 35-

vas t ethe':0~?ec:':::':::

desc~ibed the sameContinuation Sheet. (Thisspace :'s for use by the

to i.ndicatetr:ansportation~

generatorspecialtreatment, storage Qrdisposal information.Altern3te facilityin£o::mJ.tion, Lf used, and?o2..nt o f d.~parture from the0nited States forinternational shipments mustalso be entered in thisspace. States are notautho::ized to requireadditional, new or differentinformation. in this space.)

***************************************

INOTE: All of the above informationfor which the generator isresponsible may be printec.]

***************************************

l~ this soace you must note anysignificant discrepancy betweenthe waste described on th manifestand the waste you actuallyr e cerved . Discrepancies should. bedo cuaie n t e d on tile f o r a wh i.chcontains a discrepancy.

SPECIAL NOTE CONCflUHNG n;TERNATIONALSHIPHE:iTS:

Shipmen ts o f aazardous ;';o3.s t edestined for a foreign country Jutoriginating ~~thin the U~i~eci Statesmust comply with Section 262.50. and263.20 of the DeLavare regulationsgoverning hazardous Haste (Generatorsare advised that foreign countries mayrequi~e specific for~s for use intheir c o un t z y e)

L"..\SS?ORTE..-q,S O:'1'1Y-----

5ig~at~=~s ~=e ~ot =0~'~i~~d

on t n e ·:on::":1t.1a.tio::. ~~l2~~t.

vas t e63 and

·~()verr.i::~

hazardousStates are

. ,:-:J.zaro.ous

r:of

~_'2gulatiQr:s

:Section 263.l0(c)(1) ofabroJ.dDelaware

Ship::entsr e gu La tee. 'by -

fo!:':nt~~e

Transporters taking~aste outside the United~equir~d to :nC~cate the date thes~~p=ent leaves t~e C~itcd States.

or i g i na t i rg ~)lJ.ts:'de t:le 7.:nitcd St.3,tes~ust oe acco~?anied by a ~ani£est.

Trans?orters o~ suc~ ~aza:dous riastear e r e spon s i bLe ~or completing the~an~=est ~he~ hazardous ~aste istransported into the ~nited States

thistheseand

Pr~~t or type the name oft~e persen ac ccpc i ng ::~:c:

~ate~ials on :ehalf of t~e

additional transporters.Thos e persons aus t sign anddate the ~ani£est in theappropriate space. If thereare no more than twot!'a~sporters,

:'..n£crr::2.tion

Item 33- :::'A"iSPORTER. ACKXm.;rT....:DG~{E.'l'T

C~ P3C.E~!'T 8: :!.A.TE2~.~S:

I!:e~ 34-

~'12.ni:E2S!: Documen t ~~umber

E?A LD. Number!211

. lrL-\STE ~1i;};IrEST Form( Con:.:inua t ion S;,,-,C ~;;;..L_..:;;8...7-,,00-2 2A:...;.- _

jl2.j~PaQ:eI ,"

_--' 1 orLn f ormat fon

~31 Generator Name State l-fanifes~ Nurnber

Phone if25] EPA I.D. Number

i~ameTransporter

"?~-I

+-1

2-

4- ]- - - - - - - - ­

II ') 5'1- J

28]

I '\- II .

! ! !

I II i

I 1,

le1,

i[--

J!

!321 Sptci.J.l H.:J.nJling Instruction .md ..;ddi[i0n~1l. En f o rrna t i on

!

:10n t n Day Ye,J,r--------------

'..::'r::msporter _Acknowledgement or Re cc i p t of >latcrials

"-'?rln-t2:(T7T~)pCd- -;'7t:iriie .-.---- ----- ----Sl~ritl[u-r-c

D..-\TE

:!ontn Day '{ear

I I-_._._--- - ._-_._---- ----Printccl/T'::Jcd ~i;:ne

=-------~---=---=---------------..::::..:.::..::..::.-_-

--------------------------Transporter _Acknowledgement of Receipt of :'laterials

351 Discrepancy Indication Space

Subpart A-General

Subpart A-General

Subpart C-Hazardous Waste Discharges

§263.l0 Scope.hazardous

States from

of hazardouswi th Part 262,

Generators of

Transportsthe United

(c) A transporterwaste must also complyStandards Applicable toHazardous Waste, if he:

(a) A transporter must nottransport hazardous wastes withouthaving received an EPA identificationnumber from the Secretary.

§263.ll EPA Identification number

(2) ~ixes hazardous wastes ofdifferent DOT shipping descriptions byplacing them into a single container.

0)waste into:lbroad; or

A transporter who stores manifestedshipments of hazardous waste incontainers meeting I:. he requirements of§262.30 at a transfer facility tor d

period of ten (10) days or less is ~oc

§263.l2 Transfer Facility Requirements

(b) These regulations do notapply to on-site transportation ofhazardous waste by generators or byowners or operators of permittedhazardous waste management facilities.

(b) A transporter who has no t

received an EPA identification numbermay obtain one by applying to theSecretary using "St a c e of De Lawa reNotification of H~zardous :1asteActivity" f o rrn and EPA Form 8700-12.Upon receiving t he request: theSecretary will assign an EPAidentification number to thetransporter.

DOT has revised its ha z a rd ousmaterials t r an sp o r't a t i o n regulationsin order to encompass the transportation of hazardous waste and toregulate intrastate, as well asinterstate, transportation ofhazardous waste. Transporters ofhazardous waste are cautioned thatDOT' ~ regulations are fully applicableto their activities and enforceable byDOT. These DOT regulations arecodified in Title 49, Code of FederalRegulations, Subchapter C.

The manifest systemCompliance with the manifestRecordkeeping.

ScopeEPA identification numbers.Transfer facility requirements

263.20263.21263.22

263.30 Immediate action.263.31 Discharge clean up.

(a) These regulae ions establishstandards which apply to personst ra n spo r t f.ng hazardous waste within t ceUnited States if the transportationrequires a manifest under Part 262.

Subpart B-Compliance With t:he ManifestSystem and Recordkeeping

PART 263--ST~~ARDS APPLIC~~LE TOTR}~SPORTERS OF HAZARDOUS WASTE

Section263.10263.11263.12

Note: The regulations set forth inParts 262 and 263 establish theresponsihilities of generators andt r a ns p o r r e r s or hazardous waste in thehandling, transportation, and!nanagemenl of thac waste. Ln theser cg u La t ions, D}JREC has expresslyan op t e d c e r t a i n regulae ions of theDepartment or Transportation (DOT)governing the transportation ofh.:1ZarOOlls materials. Theseregulations c o nc e r n , arno ng otherthings, labeling, marking, placarding,using proper containers, and reportingdischarges. DNREC's adoption of theseDOT regulationsensures consistency with the requirements of DOT and thus avoids theestablishment of duplicative orconf lie ting requi rement s wi th re spec tto these matters. These DNREC regulations which apply to intrastatetransportation of hazardous waste a r eenforceable by D~~EC.

subject264 a ndre spec c

to regulation under Parts 1.22,Part 265 of these Regulations with

to the storage of those wastes.

identification numbers, ~cnerator

c c r t i f Lc a t i.on , a nd s t g na t u r e s )~ccoD?nnies the hazardous waste; ~nd

pap e rwa t e r

in

the

I) A c o p y of che shippingx r 'r:lnifest is retained by e a c h(~ulk shipment) transporterac c o rda nc e w'i.th §263.22.

( J)

obtainsdelivering t r an s po r t e r

date of delivery andha ndwr i t t e n signature o f tr:e owne r or

o pe r a t o r of the designated facilityo n e i t hc r the manifest or t he snipping

(4) The ~erson delivet"f.n,~ ~~1(,

ha z a rd ou s was t e to t he ':'niti;11 watet'"(:-,uL: shipment) t r a ns po r t e r o b t a i nsthe '!at>:~ of d e Lf ve ry and signature oft':e r•."a.ter (bulk shipment) cr a n s oo r t e ro n t;~e man i f e s t .i nd f o rwa rd s ;t to r hedesi~n~ted facility; and

(0.) A transporter may not accepth~zard0US wast~ from a generator unless~t is accompanied by a manifest, signed~v :~e ~enerator in accordance with the;: "'-01)!;; ', ~~ -l !) '1 S 0 of ?:-l:':: 262 e

Subpart g-Compliance With the ManifestSystem and Recordkeepip~

~263.20 The manifest system.

~ '::1) Before transporting the~~zarrious waste, the transporter ~ust

sign 2nd date the manifest.ic know Ledg t ng acceptance of the:1:lzardous waste from the generator.~~e transporter must return a signedcony to the generator '::Jefore Leavi~g

the generator's property.

(c) The transporter must ensureth~t the manifest accompanies thehn z a rd ous waste.

Cd) A transporter who delivers ac'"zarcous waste to a no t he r transportee«r :0 t~e d e s Lg na t e d f ac t Li t y must:

':::) For s h t nne n t s i nvo Lv i ng railtt:':lnsoor:ation, the re qu i r eme n t s o rpa r o c ru p ns (c), ·~d) a nd (e) do no t

appl::1nd the f o Ll owing requirementsdo ~;1D 1:::

(1 \ ~,;;.,"!., :lCC,"pt in'!. ;lil7;1!"dous'.-/3. S t err0 m -3. ~ () n -!' .'! : 1 ::r a !1 so 0 r t e r , ~~ h {.!

(~) Obtain the date ofr..:;~ive~Y' ana the haridwr i t t e n signature,r that transporter or of the owner or

:"'"Jerato:r of the designated facility on:~c ~n~iCest; a~d

(:) Sig'1manifest ~c\n0wleGging

the ha z a rd ou s I.};t>~te;

and datea c c e p t a nc e

theof

( ') '\\. ~ /

:71~etain one copy of the

~ccordance wLth §263~22; ~ ' , I

t r a n s po r t o r :

( . , \" 1 ~ ;

n.m I "est'O..etur:1

':0 the'3 igned

non-,<lil

Gi~\te the r emaLni ng copieso f ': f:e ma n i f e s t t o the acc e o t Lnz:ra~spor~er ~r cesign~ted fncility

t~=ee COpi~3 of ~~e ~anifcst to:

r e q u i r eme n t s of paragraph(f) of this section do notwa ce r (bulk shipment)

if:

t r a n sp o r t e r , if .mv : f) r

(B) The designatJ:=d [.:1c1li~y\ -;~

the ship~ent i.s delivered to thatfaci!ity ~y r~i!; or

tr3n~nort0rr a I 1The l a s t

to ':andleI~ C)

designated

is

(.?) The" c), ( d ) andapply tot r an sp o r t e r s

(1) The hazardous wastedelivered by water (hulk shipment)~o tne cesignated facility; rtnd

( , ...'-" ..

(2) A shipping naper containing:~0 ~~~or~at10n ~(~quired on :he~:

: -'\ - ~ ': r : .. ,,1: '. -: C : s ~ : '" -~ : ": -: .. '~:-2 •

(2) Rail transporters mustensure that a shipping pap~r

containing all the informationrequired on the manifest (excludingthe EPA identification numbers,generator certification, andsignatures) accompanies the hazardouswaste at all times.

§263.21 Compliance with the manifest.

(3) Return a signed copy ofthe manifest to the generator.

(a) The transporter must deliver theentire quantity of hazardous waste whichhe has accepted from a generator or atransporter to:

facility(1) The designatedlisted on the manifest; or

transportersei ther the

Note: Intermediate railare not required to signmanifest or shipping paper.

(ii) Retain a copy of themanifest in accordance with §263.22.

(3) When delivering hazardouswaste to the designated facility, a railtrnnsporter must:

(ii) Retain a copy of themanifest or signed shippir~ paper inaccordance with §263.22.

(4) :.,rhen delivering hazardouswaste to a non-rail transporter a L11 L

transporter must;

thethe

designatednext

place outsidedesignated by

The( 3)transporter, or

(a) ~ transporter of hazardouswaste ClUSt keep a copy of the manifestsigned by the generator, himself, andthe next designated transporter or theowner or operator of the designated~acility for a period of three yearsfrom the date the hazardous waste wasaccepted ~y the initial transporter.

(4) TheUni ted Statesgener3tor.

(b) For shipments delivered to the

designated facility by water (hulkshipment), each water (bulk shipment)transporter must retain a copy of theshipping paper containing all theinformation required in §263.20(e)(2)for a period of three years from thedate the hazardous waste was accepted bythe initial transporter.

(b) If the hazardous waste cannotbe delivered in accordance withparagraph (a) of this section, thetransporter illUSt contact the generatorfor further directions and must revisethe illaniiest according to thegenerator's instructions.

§263.22 Recordkeeping.

(2) The alternate designatedfacili t y , if the hazardous waste cannotbe delivered to the designated facilitybecause an emergency prevents delivery;or

andw i t h

manifestleft the

accordance

on thewaste

the raan i f e s t

in

Indicatehazardousand

Transporters who transportwaste out of the United Stat0s

(2) Sign

one copy(c); and

retain§263.22

(g)hazardousmust:

(5) Before accepting hazardouswaste from a rail transporter, anon-rail transporter mus t sign and cia tethe manifest and provide a copy to therail transporter.

(i) Obtain the date ofdelivery and the handwritten signatureof the next non-rail transporter on themanifest; and

(1)the date theUnited States;

(i) Obtain the date ofdelivery and handwritten signature OL

the owner or operator of the designatedfacility on the manifest or the shippingpaper (if the manifest has not beenreceived by the facility); and

(c) For shipments of hazardous~rtste by rail within the United States:

(i) The initial railtransporter must keep a copy of themanifest and shipping paper with all theinformation required in §263.20(f)(2)for a period of three years from thedate the hazardous waste was accepted bythe Initial transporter; and

~n official (State or local governrner.tor a :ederal Agency) acting within thescope of his o f f Lc ia1 re spo ns j hi li t I e sdetermines that immediate removal ofthe waste is necessary to protecthuman hea 1 t h or the environment, thatofficial may authorize the removal ofthe 'Naste;,y transporters who do nothave CPA identification numbers andwithout the preparation of a manifest.

Note: Intermediate railtransporters are not required to ,~eep

records pursuant to thes~ regulations.

(d) A transporter who transportsha za rd ou s waste o u t of the UnitedStates mus t k.eep a copy of themanifest indicating that the hazardouswaste left the [nited States for a?eriod of three ~2ars :rom the datethe ha z a rd cu s ·...as t e "..:as .ic c e p t ed bythe inlti31 tr~nsporter.

(ii) The final railtransporter must keep a copy of thesigned manifest (or the shipping paperif signed by the designated facilityin lieu of the manifest) for a periodof three years from the date thehazardous waste was accepted by theinitial transporter.

263.31 Discharge clean up.

(2) Report in writing asrequired by 49 CFR 171.16 to theDirector, Office of Hazardous~terials Regulations, :faterialsTransportation Bureau, Department ofTransDortation, NBshington, D.C. 20590.

(d) A wa t e r (bulk. s h i orne n t )

transporter who has dischargedhazardous waste must give ~he samenotice as required by 33 CPR 1 ~13. 203Eor oil ~nd hazardous substances.

(c) An air, rail, highway, orwa t e r transporter who has dischargedhazardous w~ste must:

A transporter ~ust clean up ~ny

::2.zardous :vaste discharge that occurs:uri.::g t r ..e nsp o r t a t Lon a nd restore the

(1) Give notice, if requiredby 49 CFR 171.15, to the ~ationa1

Response Center (800-424-8802 or (202)!l.26-2675), and give notice to theDepartment of Natural Resources andEnvironmental Control ((302)-736-4781or (302) 736-4580) immediately; and

of re tent ionSection a r e

The periodsto in t h i sClutomaticallyany unresolved e~for=e~en~

regard i.r..g ::::'eo r :::.s re cue s t e ciac t i v it y

SecretarYe

(e)referredextendedcourse ofaction

Subpart C - Hazardous WasteDischarges

§263.3Q Immediate action.

(a) In the event of a dischargeof hazardous waste duringtransportation, the transporter musttake appropriate immediate action toprotect human health and theenvironnent (e.g., notify local~uthorities, dike the discharge area).

spill area to the original conditionexisting be f o r e the spill or take suchac t ion as may be requi red or approvedJV Federal, State, or local officialsso that the hazardous ..va s t e discharge'10 Lo ng e r presents a hazard to humanhealth or the ~nviro~ment~

(b) T~... r a discharge of hazardousc.l..!ri~~ t!",~_:1sportaticn a nd


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