TECHNICAL MEMORANDUM NO. 3 FOR REMEDIAL … · 2020-06-11 · Inorganics Technical Report for CITY...

.2-90

PELA- - - - - 4 9

TECHNICAL MEMORANDUM NO. 3

FOR REMEDIAL INVESTIGATION/FEASIBILITY STUDY

CITY DISPOSAL CORPORATION LANDFILL

(DUNN LANDFILL)

(PELA Reference No. 495201)

Appendix B.

Results of Analyses of Soil Samples and

Ground-Water Samples - Inorganics Technical Report (

r

February, 1990

P. E. LaMoreaux & Associates, Inc. __

Inorganics Technical Reportfor

CITY DISPOSAL CORPORATION LANDFILL

CA1371-CAI382CAI893-CAI894

Cttiln el catioay out Rtoairta lor ETC out Mtragtmtni Si/mm«y fttparttWASTE MANAGEMENT INC. 405

ETC Stmplt No. Comptny FK/llty Stmplt Point Out Tlmt Heart

Swep T. Davis

Pttsidtnt

U.S. EfA - CLP

COVER PAGE - INORGANIC ANALYSES DATA PACKAGE

Lab Name: ETC CORP.Lab Code: Case No.

Contract:SAS No.: SDG No.: M751W

SOW No.: 7/87

EPA Sample No.1GWB12RRIGWBlURR1GWB16RR1GWB17RR1GWB19RR1GWB7RR10WB9AR1GWB9RH1GWP1A1GWP2A1GWP3A1GWP3BFLDBLAHKX DUP

Were ICF interelement corrections applied?

Were ICP background corrections applied?If yes-were raw data generated beforeapplication of background corrections?

Comments:

Lab Sample 1C.CA1377CA1379CA1380CA1378CA1372CA137UCA1376CA1375CA1371CA1373CA1893CA189UCA1382CA1381

Yes/No YES

Yes/No YES

Yes/No YES

Release of the data contained in this hardcopy data package and in thecomputer-readable data submitted on floppy diilcettthe Laboratory Manager or the Manager's designeefollowing signature.

Lab ManageDate

COVER PACE - IN

>rized by

7/87

Methodology

for

CLP Analyis of Metals

The determination of metals is performed according to USEPAContract Laboratory Program (CLP) protocol. These methods arepublished in the July 1987 Statement of Work, "Inorganic-Analysis, Multi-Media/Multi-Concentration," SOW NO. 787.

Antimony, Arsenic, Lead, Selenium, and Thallium are analyzed bygraphite furnace atomic absorption. Potassium is determined byflame atomic absorption and total and inorganic mercury by coldvapor atomic absorption. The remaining analytes are determinedby inductively coupled plasma emission spectrometry.

Inorganic mercury is determined using modified versions of Method245.5 (Sediment/Soil) and Method 245.1 (Aqueous) where thepotassium permanganate and potassium persulfate oxidation stepsare omitted.

CLP MERCURY ANALYSIS

The determination of mercury is performed according to USEPAContract Laboratory Program (CLP) Protocol. These methods arepublished in the July 1987 Statement of Work, "InorganicAnalysis, Multi-Media, Concentration," SOW NO. 787.

Total mercury is determined by Method 245.5 (Sediment/Soil) andMethod 245.1 (Aqueous). Inorganic mercury is determined by usingmodified versions of these methods where the potassiumpermanganate and potassium persulfate oxidation steps areomitted.

METALS IDENTIFICATION CODES

On the following page is a listing of descriptive codes on metalsdata which can be used for verification purposes. These identiyall standards and quality control requirements for eachinstrument used.

LABELLING CODES FOR ICP ANALYSIS

CBBLK - Calibration Verification BlankSXBLK - Standard BlankSASI514A - Standard 1SBSI514B - Standard 2SCSI514C - Standard 3CSSIS14E - standard 4CSSI514D - standard 5DW - RinsewaterCSMIDCHK - Initial/Continuing Calibration

Verification SolutionCSX85IHT - Interference Check SampleCSLABCON/CSLABCN2 - Laboratory Control SamplesRSQXXXXX - Method BlankKKIFBPX - Method Blank SpikeRSXXXXXX - SampleKSIFBPX - Matrix SpikeQSXXXXXX - Duplicate SampleDSXXXXXX - Serial Dilution

SXBLKSASI121A -SBSI121B -SCSI121C -SMSI121E -SDSI121D -CSBLK/CBBLKCSFFLMCON -

RSQXXXXX -KKIFBPXRSQXXXXD -

RSXXXXXX -KSIFBPXRSXXXXXD -

QSXXXXXX -

LABELLING CODES FOR FLAME AA ANALYSIS

Standard BlankStandard 1Standard 2StandardStandardStandard 5- Calibration Verification BlankInitial/Continuing CalibrationVerification SolutionMethod BlankMethod Blank SpikeDilution of Method Blank(Used for spike recovery determination)SampleMatrix SpikeDilution of Matrix Spiked Sample(Used for spike recovery determination)Duplicate Sample

ETC

LABELLING CODES FOR GRAPHITE FURNACE AA ANALYSIS

BLANKSTANDARD 1STANDARD 2STANDARD 3STANDARD 4CSBLK/CBBLK -CSSTRCON

CSFNLAB/CSFNLAB2RSQXXXXXKKIFBFXRSXXXXXXKSIFBFXQSXXXXXX

Standard BlankSTD 1STD 2STD 3STD 4Calibration/Verification BlankInitial/Continuing CalibrationVerification Solution

Laboratory Control SamplesMethod BlankMethod Blank SpikeSampleMatrix SampleDuplicate Sample

LABELLING CODES FOR MERCURY ANALYSIS

QC-EPA - Initial Calibration Verification SolutionBLK - BlankCONTROL - Continuing Calibration Verification SolutionQXXX -1,2 - Method Blank in Duplicate

-Al - Method Blank SpikeXXXXXX-1,2 - Sample in Duplicate

-Al - Matrix SpikeKEYS TO ETC REPORTING

ND » Concentration Below IDLBMDL • Concentration Greater than IDL but Less Than MDL

CLP DATA QUALIFIERS

E - Indicates the reported value is estimated due to thepresence of interference.

S - Indicates the reported value was determined by Methodof Standard Additions (MSA).

N - Indicates spiked sample recovery is not within controllimits.

* - Indicates duplicate analysis is not within controllimits,

w - Post digestion spike for Furnace AA analysis is out ofcontrol limits (85-115%), while sample absorbance is lessthan 50% of spike absorbance.

METALS ANALYSIS DATA

INORGANIC ANALYSIS DATA SHEET

Lab Name: ETC CORPLab Code: Case No.:

Matrix (soil/water): WATER

Level (low/med): LOW

% Solids: 0

Contract:SAS No.:

I II 1GWP1A |

SDG No. : M751W

Lab Sample ID: CA13T1

Date Received: 09/19/89

Concentration Units (ug/L or ng/kg dry weight): ug/l

Color Before:

Color After:

Comments:

1ICAS No.1171,29-90-5| 7MUO-36-0l7W*0-38-2lTWtO-39-3I7UUO-141-7|7W*o-U3-9l7M»0-70-2|7M»0-UT-3|7l4ltO-U8-l4l7MtO-50-8I7U39-89-6I7U39-92-1I7U39-95-UI7W9-96-5I7U39-97-6I7UUO-02-0I7IAO-09-7I7782-U9-14I7M40-22-U!7«tO-23-5I714UO-28-0I7M40-62-2I7UUO-66-611

1 1 \ 11 Analyte |Concentration|C| M jq11 Aluminum1 Ant imony1 ArsenicI Barium __1 Beryllium1 Cadmium|Calcium_1 Chromium[Cobalt1 Copper __(IronILead ___1 Magnesium1 Manganese(MercuryI Nickel __1 Potassium1 Selenium[Silver1 Sodium[Thallium1 Vanadium"1 Zinc1 Cyanide

32.531.3

.857.3

.11.0

73100.03-86. 63-5

148.21.1

>4i6oo.o2.7

.\2.0

779-0.7

5.13260 . o

1.13-9

12v6.3M

Clarity Before:

Clarity After:

1 1|U| P|U| P|U| FIBI P|U| P|U| P1 1 P|0| P|U| P|U| P|U| PIUI F1 1 PIBI P\±\ ££IUI PIB! PIUI FIUI PIB| PIUI FIUI PIBI P

—

~

101 IS$

Texture :

Artifact

^^r Cl1-TABLE 1: QUANTITATIVE RESULTS

Metals - Analysis Data (QR52)

Chain of Custody Data Required for ETC Data Management Summary Reports

CAI37I WASTE MANAGEMENT. INC. 405 UI8WP1A 890918 1515 0

ETC S«vl« *fc. CoMfxny FKllity SMP!« Poiot D«l« Ti*t EHourtd

Compound

Boron

1

R.toltt

SampleGeneva.

U9/1

37

K)Lug/1

20

OCT 18. 1989OM700S1

U.S. EPA - CLP


Lab Name: ETC CORP.Lab Code: Case No.:



% Solids: 0

Contract:SAS No.:

EPA SAMPLE NO.

I 10WB19RR |I_________ I'

SDG No.: M751W

Lib Sample ID: CA1372


Concentration Units (ug/L or mg/kg dry weight): ug/L

1|C AS No.1| 7U29-90-5171*0-36-0|7M»0-38-21 7l4l40-39-3|7l4l40-l4l-7I7M40-U3-9171*0-70-2I714UO-U7-3|71*0-l48-U|7"*0-50-8|7l<39-89-6(7li39-92-l|Tl439_95.l,171139-96-51 7"i39-97-61 71*0-02-0171*0-09-7(7782-l»9-U171*0-22-1*171*0-23-5171*0-28-0(7liltO-62-2I7I4UO-66-61

11 Analytet1 Alum inum_|Antimony_1 Arsenic _I Barium __1 Beryllium1 Cadmium|Calcium_(Chromium1 Cobalt1 Copper __llronILead(Magnesium(Manganese(Mercury(Nickel __(Potassium(Selenium(Silver(Sodium|Thalllun_1 VanadiumIZinc(Cyanide

1 1Concentration! C| M

1 132.531.38.2

76.5.1

1.057600.0

3.86.83-5

1820.01.1

1*8100.0625.0

.V3.0

1720.0.7

5-112100.0

1.13.9

26.2

IUI P|U| PIBI FIB| pIBI p|U| P1 1 P|U| P|U| P|U| P1 1 P|U| F1 1 PIII Plul t,VIB| pIBI pIUI F|U| P1 1 P|U| FIUI PI I P

-III.

Q

—

MColor Before:

Color After:

Comments:

Clarity Before

Clarity After:

Texture:

Artifacts

c^Kr L l fc

TABLE 1: QUANTITATIVE RESULTS

Metals - Analysis Data (OR 5 2)

Chain ol Custody Data Required for ETC Data Management Summary Reports

CAI372 WASTE MANAGEMENT. INC. 405 W1GUB19RR 890925 1600 2

Compound

Boron

VO

1

ftoultf

SanpleConcen.

U9/1

45

MILU9/1

20

OCT 18. 1989QM7005I

U.S. EPA - CLP


Lab Nam«: ETC CORP.Lab Code: Case No.:

Matrix (soil/wat«r): WATER

L.v.l (low/med): LOW

% Solid!: 0

Contract:SAS No.:

EPA SAMPLE NO.

I II 1GWP2A |I_________ f

SDG No.: M751W

Lab Sample ID: CA1373


Concentration Units (ug/L or rag/kg dry might): ug/L

Color Before:

Color After:

Comments:

IICAS NO.I171,29.90-5I7UUO-36-0171*0-38-2l7MtO-39-3I7I4UO-U1-7J7UUO-U3-9I7UUO-70-2I7UUO-U7-3ITUUO-US-Ul7W»0-50-8171,39-89-6I7U39-92-1171.39-95-111 7U39-96-5I7U39-97-6I71AO-02-01 714UO-09-7I7782-U9-UI7UUO-22-UI7UUO-23-5|7ltUo-28-0I7UUO-62-2|7>il40-66-611

——————

11 Analyte1|Aluminum_1 Antimony|Arsenic_][1 Barium1 Beryllium1 Cadmium _1 Calcium _1 Chromium1 Cobalt _ ~1 Copper __llronILead1 Magnesium1 Manganese1 Mercury1 Nickel __1 Potassium1 Selenium1 Silver[Sodium1 Thallium1 Vanadium'IZinc1 Cyanide

1 1Concentrationl C| M

1 132.531.3

.8109.0

.11.0

78700.03.86.83-5

U8.21.1

1(2200. 02.3

.12.0

1820.0.7

5.117700.0

1.13-9

15.63-H

Clarity Before:

Clarity After:

IUI PIUI PIUI FIBI pIUI PIUI P1 1 P|U| PIUI P|U| PIU| PIUI F1 1 pIII pIfej UL|U| PIBI pIUI FIUI P1 1 pIUI FIUI PIBI PUi

Q

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10

c



Chain o( Custody Data Required (or ETC

CM 373 WASTE MANAGEMENT. INC.

Data Management Summary Reports

405 U1GUP2A 890926 0740 5

—Boron

1

Retails

SampleCancan,

ug/140

MDLug/120

OCT 18, 1989QM'OOSi

U.S. EPA - CLP

INORGANIC ANALYSIS DATA SHEETEPA SAMPLE NO.




% Solids: 0

Contract:SAS No.:

I1GWB7RR

SDG No.: MT51W

Lab Sample ID: CA137U



IICAS NO.I

i i nI Analyte |Concentration|C| M

1 1I IIQ II I

Color Before:

Color After:

Comments:

171429-90-5I7UUO-36-0(71, 1,0-38-21 71,1,0-39-3|7U,0-I*l-7|7ltUO-U3-9|7M,0-70-2|7M»0-li7-3|7MtO-lt8-U1 7M.O-50-81 71*39-89-6171-39-92-1I7U39-95-U(71,39-96-5!7l<39-97-6(7U,0-02-0(71,1,0-09-7I7782-U9-U|7ltUO-22-UI7W40-23-5I7UUO-28-0|7M<0-62-2I7UUO-66-611

{Aluminum1 Ant imony(ArsenicI BariumI Beryllium(Cadmium(Calcium _(Chromium(Cobalt _ 21 Copper __(Iron(Lead(Magnesium(Manganese(Mercury(Nickel __(Potassium(Selenium(SilverI Sodium(Thallium(Vanadium"1 Zinc(Cyanide

32.531.32.8

57.0.1

1.079100.0

3.86.8U.9

793.01.1

1*3600 . o789-0

.19.6

1390 . o.7

5.121UOO.O

1.13-9

U3-03-M

Clarity Before:

Clarity After:

|U| P|U| P|B| F|B| P|U| P|U| P1 1 P|S| p|U| P|B| P1 1 P|U| F1 1 PIII PIlil f.<i|B| P|E| P|U| F|U| Pl.l P|U| F|U| PI I PiQl

——

-

eTvxtur* :

Artifacts:

12



Chain ol Custody Oau R«Qu»ed for ETC

Ml 374 WASTE HWWGEHENT, INC.ETC S«vlt No. CMNMny

D*U Managcmenl Summary Report*

405 U1GUB7RR 890926 1236 1Elap>«4

Ito. Hours

Compound

Boron

CM

1

••tultt

SampleConctn.

ug/1

37

M)Lug/120

OCT 18, 1989QM700Si

U.S. EPA - CLP


Lab Name ETC CORP.Lab Code: Case No.:



% Solids: 0

Contract:SAS No. :

EPA SAMPLE HO.

I 1GWB9RR

SDG No.: H751W




Color Before:

Color After:

Commenti:

IICAS NO.I1 71*29-90-5I7UUO-36-0I7UUO-38-2I7UUO-39-3|7MtO-Ul-7I7UUQ-U3-9I7UUO-70-2I7UUO-U7-3I7UUO-U8-U|7UliO-50-81 7U39-89-6I7U39-92-1I7U39-95-UI7U39-96-5I7U39-97-6I7UUO-02-0|7ltltO-09-7I7782-U9-UI7UUO-22-I*|7"t UO-23-5|7WtO-28-0|7UltO-62-2I7UUO-66-611

——————

11 Analyte11 Aluminum1 Ant inony1 Arsenic _1 Barium1 Beryllium1 Cadmium|Calcium_1 Chromium1 Cobalt _ ~1 Copper __jlronHead1 Hagnes iun1 Manganese1 Mercury1 Nickel __1 Potass iun1 SeleniumI SilverI Sodium1 ThalliumI Vanadium'IZinc1 Cyanide

1 1 1Concentration |C| M |Q

1 132.531.362.8

667.0.1

1.0152000.0

3.817.0

3-523000.0

1.1113000.0

156.0.1

30.28510.0

.76.3

U1200.01.13-9

13.13.*/

Clarity Before:

Clarity After:

IUI P|U| P1 1 F1 1 PIBI P|U| P1 1 P|U| PIBI p

, |U| P1 1 P|U| F1 1 p1 1 p

j£l &IBI p1 1 P|U| FIB| p1 1 P|U| FIUI PIBI PM

—

—

S

5S

____ Texture :

Artifact

14

c




CAI375 WASTE MANAGEMENT. INC. 405 U1GUB9RR 890926 1539 0ETC SMPl« No. COMMA? Futility Swvlc Point Oil* Tup* Mnu"'

Compound

Boron

cn

Keiullt

S»-olcConceit.

U9/1

260

MDLU9/1

20

OCT 18. 1989QM7005I

u.ii. c.r*i -


Lab Kame: ETC CORP.Lab Cod*: Case No.:



% Solids: 0

Contract:SAS No.:

EPA SAMPLE NO.

I 1GWB9AR |I___________!•

SDG No.: M751W




1ICAS No.1|71l29-90-5171*1*0-36-01 7l»UO-38-2171)1*0-39-3I7UUO-U1-7171*1*0-1*3-91 7>*ltO-70-2l7liUO-l*7-3I7UUO-148-U|7>* UO-50-8| 7.39-89-6l7"*39-92-l|7li39-95-lt171*39-96-5I7U39-97-6171.1.0-02-0I7UUO-09-7I7782-U9-1.|7U1.0-22-liI7U140-23-5I7UUO-28-0!7ltUO-62-2|7>4UO-66-61

1 I \ \ \1 Analyte |Concentration|C| M 1Q1|Aluninum_1 Antimony"|Arsenic_Î Barium1 Beryllium1 Cadmium|C*lcium_(Chromium1 Cobalt1 Copper __1 IronILead1 Magnes iun[Manganese1 MercuryI Nickel __1 Potassium1 Selenium1 Silver1 Sodium1 Thallium1 Vanadium'IZinc1 Cyanide

32.531.313.6

138.0.1

1.0133000.0

3.811.710.2

16UO.O1.1

132000.0613.0

.133.6

2980.0.7

5.150UOO.O

1.13.9

1*5.03-1

l _ lIUI P|U| P1 1 PIII PIB! PIUI P1 1 Plu| PIBI P|B| Pl_l PIUI F1 1 Pn pwI B I PIBI P|U| F|U| P1 1 P|U| F|U| P1 1 p

ci

Color Before:

Color After:

Comments:

Clarity Before:

Clarity After:

Texture:

Artifacts:

16

c


Metals - Analysis Data (OR52)


CAI376 WASTE MANAGEMENT. INC. 405 U1GMB9AR 890927 0831 5C1C SMVl* He. COMOMV Facility 3«q»l« Point 0«IO TlMt ûrt"

—Boron

Resultc

S.»pl«Concen.

U8/1

280

M>L«g/l20

OCT 18. 1989QM7005I

U.S. EPA - CLP





% Solids: 0

Contract:SAS No.:

EPA SAMPLE NO.

I 1CWB12RR

SDG No.: M751W




1ICAS NO.1(71,29-90-5(71,1,0-36-0I7UUO-38-2(71,1,0-39-3|7M,0-Ul-7(71,1,0-113-9(71,1,0-70-2(71,1,0-117-3(7MtO-U8-li|7M<0-50-8(7li39-89-6I7U39-92-1171,39.95.1,(71,39.96-5|7li39-97-6I7UUO-02-0(71*0-09-7(7782-U9-U|7W,0-22-i(1 7UUO-23-5(71,1,0-28-0(71,1,0-62-2(71,1,0-66-61

11 Analyte1|Aluminum_(Antimony"

1 BariumI Beryllium(Cadmium _(Calcium _(ChromiumI Cobalt1 Copper __(Iron(Lead(Magnesium(Manganese1 Mercury(Nickel __(Potassium(Selenium(Silver| Sodium|Thallium_(VanadiumIZinc1 Cyanide


1 132.531.3

.8

.11.0

119000.03.86.83.5

5U.81.1

57000.0813.0

.112.1,

2120.0.7

5.16U60.0

1.13.9

10.2

|U| P|U| P|U| FIBI PIUI PIUI P1 1 PIUI PIUI P|U| PIBI PIUI F1 1 P1 1 P

JilIBI PIBI PIUI FIUI P1 1 pIUI FIUI PIBI P

Jil

Q

—

W

BColor Before:

Color After:

Comments:

Clarity Before:

Clarity After:

Texture:

Artifacts:

18

cTABLE 1: QUANTITATIVE RESULTS

Metals - Analysis Data (OR 52)

Chain of Custody Data Required for ETC Data Management Summary Report!

CAI377 WASTE MANAGEMENT. INC. 405 WIGUBI2RR 890927 0906 1[1C J«wl< No. Caviar Facility 3«vlt foiol O.I. \im, IM'""

Compound

Boron

VD

1

R.«ult,

Conctn.U9/1

48

U9/1

20

OCT 18. 1989QM7005I

U.S. EPA - CLP





% Solids: 0

Contract:SAS No.:

EPA SAMPLE NO.

I II 1CWB17RR |

SDG No.: M751W



Concentration Units (ug/L or mg/kg dry might): ug/L

1ICAS NO.1171*29-90-5171*1*0-36-0171*1*0-38-2171*1*0-39-3171*1*0-1*1-7|7Ul*0-l*3-9171*1*0-70-2171,1*0-1*7-3171*1*0-1*8-1*I7UUO-50-8171*39-89-6171*39-92-11 71,39-95-1*171*39-96-5171*39-97-6171*1*0-02-0171*1*0-09-717782-1*9-1*171*1*0-22-1*I7UUO-23-5171*0-28-0171*1*0-62-21 71*1*0-66-61

11 Analyte1|Aluminum_|Antimony_I Arsenic _1 Barium __1 BerylliumI Cadmium _1 Calcium _I Chromium[Cobalt1 Copper __llron[LeadI MagnesiumI ManganeseI Mercury[Nickel __{PotassiumI Selenium[SilverI Sodium1 Thallium|VanadiunT1 Zinc1 Cyanide


1 132.531.38.271.0

.11.0

71300.03.86.83.5

115.01.1

1*8500.070.6

.12.0

2060 . o.7

5.1621*0.0

1.13.918.7

IUI PIUI PIBI FIBI pIUI PIUI PLI pIUI PIUI PIUI PLI pIUI F1 1 pO PIUI PIBI P|U| F|U| P1 1 P|U| F|U| PIBI PJU\

Q

~

®

Color Before:

Color After:

Comments:

Clarity Before:

Clarity After:

Texture:

Artifacts:

20

c^HT--



Cluin of Custody Data Requited tor ETC

CAI378 WASTE MANAGEMENT. INC. 405 WIQUB17RR

ry Reports

890927 1503 2ETC tmelt Mi. C<M»«iiy FKiliiy s«*elt Point 0«l» IbM i«2y?t

Cmpound

Boron

N3_» 1

••lultt

SmmfltCoflccn .

"9/1

36

K>L1/9/1

20

OCT 18. 1989QM70051

U.S. EPA - CLP



Matrix (soil/Hater): WATER


% Solids: 0

Contract:SAS No.:

EPA SAMPLE NO.

I IGWBlURR

SDG No.: MT51W



Concentration Units (ug/L or mg/kg dry weight): uj/L

I" T I

Color Before:

Color After:

Comments:

ICAS NO.1171,29-90-5|7Ul*0-36-0171*1*0-38-2171*1*0-39-3I7UUO-U1-7|7l»Uo-l43-9171*110-70-2171*0-1*7-3I7MUO-U8-1*I7WO-50-8171*39-89-6171*39-92-1171*39-95-1*I7U39-96-5171*39-97-6171*1*0-02-01 7UW-09-717782-1*9-1*1 71*0-22-1*171*1*0-23-5|7ltUO-28-0171*1*0-62-2171*1*0-66-611

I Analyte1|Aluminum_|Antimony_1 ArsenicI Barium __1 BerylliumI Cadmium|Calcium_I ChromiumI Cobalt _ ~I Copper __llronILeadI MagnesiumIManganese1 MercuryIHickel __IPotassiumI SeleniumISilver| Sodium1 Thallium1 Vanadium"IZinc1 Cyanide

Concentration|C| M1 1

32.531-3

• 9111.0

.11.0

91500.03-86.83-5

93.21.1

55200.0112.0

.1l*-31*050 . o

.75-19150 . o1.13-9

18.72.4

Clarity Before:

Clarity After:

|U| PIUI PIBI FIBI p|U| P|U| P1 1 P|U| PIUI PIUI PIB| p|U| F1 1 PLI P

IBI p|U| FIUI P1 1 P|U| F|U| PIBI p

All

Q

—

—_

sTexture :

Artifacts

22

c^gg& 1.1*. "-" •




CA1379 WASTE WNAGEMENT. INC. 405 W1GWB14RR 890928 0834 4ETC 3««pl« N», CoMp»r Facility 3*»pl« Point 0at« Tiow E(taurt4

Compound

Boron

rO0-4 '

Remits

SampleCone en .

U9/1

70

M>1,"9/1

20

OCT 18. 1989QM7005I

U.S. ErA - CiP




Level (lou/med): LOW

% Solids: 0

Contract:SAS No.:

EPA SAMPLE NO.

I II 1GWB16RR |I______ !•

SDG No.: M751W




|CAS No.I I \\Analyte | Concentration^ I M1

IT'129-90-5I7UUO-36-0|7WiO-38-2I71AO-39-3I T U U O - U l - TJ7M40-U3-9J7UUO-70-2|7MiO-U7-3I T b U O - U S - U|7MiO-50-8I7U39-89-6|7>i39-92-l171.39-95-1)1 7lt39-96-5171139-97-6I7UUO-02-0I7M10-09-7ITT82-U9-UI7UUO-22-U|7MtO-23-5|7WiO-28-0I7U140-62-2I7I4UO-66-611

11 Aluminum^1 Antimony"I Arsenic1 Barium __I Beryllium1 Cadmium _1 CalciumI Chromium[Cobalt1 Copper1 IronI Lead ___1 Magnesium1 Manganese1 MercuryINickel __(Potassium1 SeleniumISilver| Sodium __|Thallium_{VanadiumIZinc|CyanI3e~

36.631.32.8

1*8.3.1

1.0116000.0

3-86.83-5

2710.01.1

57700 . 0U38.0

.\it. 9

708.0.7

5.111000.0

1.13-9

11.1o,A

1 1|B| P|U| P|B| F|B| P|U| P|U| P1 1 P|U| P|U| P|U| P1 1 P|U| F1 1 P1 1 Pl|&l d|B| PIBI P|U| F|U| P1 1 P|U| F|U| P|B| P|0| s

Color Before:

Color After:

Comments:

Clarity Before:

Clarity After:

texture:

Artifacts:

24

c^fcSr L11-


Metals - Analysis Data (QR52)Chain ol Custody Data Required lor ETC Data Management Summary Report!

CAI380 WASTE MANAGEMENT. INC. 40S WIGUBI6RR 890928 1321 1ETC S»»l« ». Coocior FKilily 9»l< Point D.I. Ita. Ci!J"°

CoHpounrf

Boron

ro 'tn

Results

Sa«pl«Concen.

U9/1

64

U9/1

20

OCT 18. 1989QM700SI

U.S. EPA - CLP


I"



Level (lov/med): LOW

% Solids: 0

Contract:SAS No.:

I X DUPI

SDG Mo . : M751W



Concentration Units (ug/L or mg/kg dry weight): ug/l

1ICAS NO.1171,29-90-5171*0-36-0171*1*0-38-2171*0-39-3171*1*0-1*1-7|7l,UO-U3-9171*0-70-2171*1*0-1*7-3171*1*0-1*8-1*171*1*0-50-8!7l*39-89-6171*39-92-11 7U39-95-1*171*39-96-5171*39-97-6171*1*0-02-0171*1*0-09-7I7782-U9-U171*1*0-22-1*171*1*0-23-5171*0-28-0|7"*l*o-62-21 7M»0-66-61

11 Analyte11 Aluminum1 Ant imony(ArsenicI BariumI BerylliumI Cadmium|Calcium_1 Chromium| Cobalt _ ~1 Copper __ilronILead1 Magnesium1 Manganese1 MercuryINickel __1 Potassium1 Selenium1 Silver1 Sodium|Thallium_(Vanadium1 Zinc1 Cyanide

1 1Concentration|C| M

1 132.531.33-7

1*8.2.1

1.0117000.0

3.86.83-5

2660.01-9

57600 . 01(28.0

.13.5

690.01.15-1

11000.01.13.9

|U| PIUI PIBI FIB| pIUI P|U| P1 1 PIUI P|U| P|U| P1 1 pIBI F1 1 P1 1 PJul d.IBIIBIIBIIUI1 1IUIIUI

—

—

—

Color B«for«:

Color Aft«r:

Comments:

Clarity Before:

Clarity After:

1

Texture:

Artifacts

26

w L1LTABLE 1: QUANTITATIVE RESULTS

Metals - Analysis Data (OR 52)

Chain of Custody Data Required for ETC Data Management Summary Report*

CAI38I WASTE MANAGEMENT. INC. 405 XOUP 890928 1321 0

ETC S«opl« Ma. Company Facility S«vl« Point 0«t« TMM H*hrt

Compound

Boron

ro»o ;

Httfltt

SampleConcen .

ug/i61

M>1ug/l20

OCT 18. 1989QM7005I

U.S. EPA - CLP





% Solids: 0

Contract:SAS No.:

EPA SAMPLE NO.

I II FLDBLANK II________!•

SDC No.: M751W




Color Before:

Color After:

Comments:

1ICAS NO.1171*29-90-51 7l4l40-36-01 71*140-38-21 71*1*0-39-3|7MtO-l*l-7|7ltUO-l43-9[7M40-70-2|7MK)-U7-3171*1*0-1*8-1*I7UUO-50-8171*39-89-6171*39-92-1171*39-95-"*171*39-96-5171*39-97-6171*1*0-02-0171*1*0-09-717782-1*9-1*171*1*0-22-1*I7WO-23-5171*1*0-28-0171*1*0-62-2171*1*0-66-611

1I Analyte11 Aluminum^(Antimony"(Arsenic _[Barium[Beryllium[Cadmium[Calcium[Chromium| Cobalt _ ~[Copper __1 Iron[LeadI Magnesium[Manganese[MercuryI Nickel __[Potassium[Selenium[Silver[Sodium __|Thallium_[Vanadium1 Zinc[Cyanide

1 1Concentrat ion I C |

1 13U31

1718

366

1*81

361*

21*7

5680

13

32a

Clarity Before

Clarity After:

i* IBI3 IUI8 |U|9 IUIi IBI0 |U|o I B I8 |U|8 |U|8 IBI2 |U|1 IBIo IBI6 IBI\ lul0 |U|7 IBI7 |U|1 |U|o IBI1 |U|9 lul2 \ 1Jjtil

M

PPFPPPPPPPPFP

HLppFPPFPP

Q

—

—

&

Texture:

Artifacts

28

••"•TABLE 1: QUANTITATIVE RESULTS

Metals - Analysis Data (OR52)

Chain of Custody Data Required for ETC Data Management Summary Report*

CAI382 WASTE MANAGEMENT. INC. 405 XfLDBUNK 890927 MOO 1ETC SMP!« Np. CoopMy Facility SMpl* Point D«t* Ti«e Eitau?»4

Compound

Boron

tOVD 1

RolulK

SanpleConcen.

U9/1

ISO

MM.ug/120

OCT 18. 1989QM7005I

U.S. EPA - CLP


Lab Nam»: ETC CORP.Lab Code: Case No.:



% Solids: 0

Contract:SAS No.:

EPA SAMPLE NO.

II 10WP3AI_____

SDG No.: M751W




Color Before:

Color After:

Comments:

1ICAS NO.1(71129-90-5(71*0-36-0(71*0-38-2|7"*0-39-3|7l*0-Ul-7(7UUO-U3-9(71*0-70-2|7ltUO-U7-3| 7UUO-U8-U1 7MtO-50-8171(39-89-6(7lt39-92-l(7li39-95-it1 71*39-96-5(71*39-97-6(71*0-02-0(71*0-09-7I7782-U9-U(7l*0-22-U(71*0-23-5I7UUO-28-0I7UUO-62-2(71*0-66-61

1 1 1 11 Analyte |Concentration|C| M |Q1(Aluminum(Antimony(Arsenic(Barium(Beryllium{Cadmium(Calcium _I Chromium(Cobalt _ ~(Copper __I Iron(Lead ___(Magnesium(Manganese(Mercury(Nickel __(Potassium(SeleniumI Silver(Sodium(ThalliumI Vanadium'IZinc(Cyanide

32.531.31.572.6

.11.0

66500.03.86.83-5

1020.01.1

35800.09"«.3

.\2.0

1920.0.7

5-1UlOO.O

1.13-916.334

1 1IUI P(01 PIBI FIBI pIBI p|U| P1 1 PIUI P|U| PIUI P1 1 pIUI F1 1 Pu p|U| PIBI p|U| F|U| PIBI p|U| F|U| PIBI PIUI

*"~"

m1

Clarity Before:

Clarity After:

Texture :

Artifacts:

30

LM-TABLE 1: QUANTITATIVE RESULTS


Chain of Cu»tody Data Required for ETC Data Management Summary Reports

CA1893 WASTE MANAGEMENT. INC. 405 UIGWP3A 891002 0947 5

ETC 3«N>I« No. C<MW«ny Facility Swvl* Point D«t« TiMC u"11

Conpound

Boron

04

i

Renltt

Sanpl«CoHcen.

ug/125

MDLug/120

OCT 18. 1989QM70051

U.S. EPA - CLP





% Solids: 0

Contract:SAS No.:

I 1GWP3BI_____

SDG No.: M751W

Lab Sample ID: CA189U


Concentration Units (uj/L or mg/kg dry weight): ug/L

1ICAS NO.I7U29-90-5I7UUO-36-0|7l»UO-38-2|7MtO-39-3iTWtO-Ul-T|7M»0-l43-9I7UUO-70-2I7IAO-U7-3|7>iUO-U8-UI7UUO-50-8|7l<39-89-6|7><39-92-lI7U39-95-U1 7U39-96-5I7U39-97-61 7M»0-02-0|7liltO-09-7I7782-U9-U|7WtO-22-UI7UUO-23-51 71(1*0-28-0171*0-62-2I7M40-66-611

11 Analyte1lAluminum_1 Antimony"1 Arsenic1 Barium1 Beryllium|Cadmium_[CalciumI Chromium[Cobalt[Copper __[IronILead|Magne«iumI ManganeseI Mercury[Nickel __(Potassium[SeleniumISilverI Sodium[Thallium1 Vanadium"IZinc1 Cyanide

1 1ConcentrationlCl M

1 132.531.3

.819.8

.11.0

60700.03.86.83.5

280.01.1

35100.0250.0

.12.0

1860.0.T

5-112100.0

1.13-9

17.1*3.M

IUI PIUI PIUI FIBI P|U| PIUI P1 1 PIUI PIUI PIUI P1 1 PIUI F1 1 Pf 1 P

Jfcl £JIUI PIBI pIUI FIUI P1 1 pIUI FIUI PIBI P|0|

Q

—

©

Color Before:

Color After:

Comments:

Clarity Before:

Clarity After:

Texture:

Artifacts:

32

c




CAI894 WASTE MANAGEMENT. INC. 405 WIGUP3B 891002 1603 2E1C S««lc M>. CoM»««r FKilily 3*-«il« »oii>l 0«t« Tim Havrt4

Compound

Boron

OJCM

1

Remit!

S««pUConceit.

ug/130

MDLug/120

OCT 18. 1989QM7005I

U.S. EPA - CLP

2AINITIAL AND CONTINUING CALIBRATION VERIFICATION


Initial Calibration Source: LLCALIBSTD

Continuing Calibration Source: LLCALIBSTD

Contract:SAS No. : SDC No.: M751W

Concentration Units: ug/L

11(Analyte1|Aluminum_|Antimony_(Arsenic _(Barium(Beryllium1 Cadmium1 Calcium _1 Chromium(Cobalt __1 Copper __(Iron(Lead(Magnesium1 Manganese1 Mercury(Nickel __(Potassium(Selenium(Silver(Sodium|Thallium_(Vanadium1 Zinc(Cyanide

1Initial Calibration 1

True Found %R(1) 11 1 1

1Continuing Calibration I

True Found %R(1) Found W ( l ) l1 I I I I

2500.01 267U.U3 (107.01 2500.01 2587.17 (103.51 25U5. 831101.81500.01 520.76 (10U.2I 500.01 U99.12 (99.8 I 502.UOI100.5I

3001 30.SB 1.1014 I 30.01 31.60 (105.31 30. 89(103. 0|1000.01 1038.89 (103.91 1000.01 1030.91 (103.11 1013.30(101.31

100.01 101.63 (101.61 100.01 101.62 (101.61 99.3H99.3 1100.01 108.75 Iio8.7l 100.01 96.93 (96.9 | 96. 36(96. U |

10000. 0110589. 5U (105.9(10000.0(10188.75 (101.91 9908.05(99.1 |300.01 323.76 1107.91 300.01 313.89 |10U.6| 308.52(102.81200.01 219.29 (109.61 200.0| 207.76 (103.91 199.89(99-9 1300.0| 318. Ul (106. 1| 300.0| 307.08 (102. U| 301. 16(100. U|

1000.01 10U3.U2 I10U.3I 1000.01 98U.86 (98.5 I 983. 88(98. U 13O-O)| SC.St? 1 l».m 30.01 30. U7 (101.61 31.UO|10U.7I

10000. 0|1058l. 07 (105.8(10000.0(10351.53 1 103. 51 10179- 1UI 101.81300.0| 318.87 (106.31 300.01 311.99 I10U.OI 307.U9I102.5I

3ol l.'u 1 %s,g 1 \-s\ >.M«- | si.-i i v.atJ qa.o 1300.01 319. UU (106.51 300.01 312. 5U (10U.2I 309.23(103.11

U O O O . O I U177-56 |10U.U| U O O O . O I U189.56 |10U.7| U115. 86(102. 91300'! 3MO 1 105.TI 30.0| 31. 1U |103.8| 31. 521105.11100.01 103.63 (103.61 100.01 98. U8 198.5 1 98.7UI98.7 1

50000.0152163.33 (10U.3I50000.OI51UOO.38 (102. 8(50550. 05(101.1130.01 27.18 (90.6 I 30.0| 27.83 192.8 I 27. 73(92. U I

300.01 319.61 (106.51 300.01 309. 5U (103.21 308.61(102. 91500.01 537.3U 1107.51 500.0| 505-98 1101.21 503.08(100.61

Sio-Ckl 3o.LCth>).U /ot>,ol <#•£> (99*1 /o i . fco i /oi.ial1

M

PPP

PPPPPPPPPP

PPPPFP

46

(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115

' FORM II (PART 1) - IN 7/87

34

U.S. EPA - CLP



Initial Calibration Source: LLCALIBSTD

Continuing Calibration Source: LLCALIBSTD

Contract:SAS No.: SDG No. : MT51W

Concentration Uniti: ug/L

111 Analyte11 Aluminum1 Ant imony_I Arsenic _1 Barium1 BerylliumI CadmiumI Calcium _1 ChromiumI Cobalt __1 Copper __llronILead1 MagnesiumI Manganese1 Mercury1 Nickel __1 Potassium1 SeleniumI Silver1 Sodium __

1 Vanadium"1 Zinc1 Cyanide1

1 I IInitial Calibration | Continuing Calibration I I

True Found %R(1) | True Found %R(1) Found %R(1) 1 1 M1 I I I I I 1 I I

2500.01 267U.U3 1107-01 2500.01 257U.89 1103.01 2688-96|107-6| | 1500.01 520.76 IIOU. 2| 500.01 U87.U8 197.5 1 536.391107.31 1 13o-o 1 30,56 I Wl.fc I 30.0| 30. 2U {100.81 UgU. 93199- 0 I I 1

looo.oi 1038.89 1103-91 looo.ol 1025.98 |102.6| 1038.181103.811100.01 101.63 I101.6J 100.01 100.01 1100.01 102.271102.311 I100.01 108.75 1108.71 100.01 97. Uo 197. U I 111. 551111. 6| I I

10000. OI10589.5U |105. 9|10000.0| 997U.1U 199-7' 110738. 861107. U| I 1300.0| 323.761107.91 300. 0| 315-61 |105.2| 32U.98ll08.3l 1200.01 219.291109.6! 200.0| 205-85 1102-91 222.86 1 111. lt| |300.01 318. Ul 1106.11 300.01 306.50 |102.2| 318.6U|106.2| I

1000.01 10U3.U2 I 1 0 U - 3 I 1000.01 1011.20 J101.ll 1053. 671105- U| I.30,01 .30.50 l-lOI-o,* 30.01 31.92 |106.U| 5S8.lU|111.6| I

10000.0110581.07 |105. 8110000. OJ10268. U3 |102,7|10602.51|106.0| I300.01 318.87 |106.3| 300.01 310. OU |103-3| 322.U8ll07.5l 1

300.01 319. UU llolTsi 300.01 310. U6 1103-51 325.5H108.5I IUOOO.OI U177.56 I10U.UI I | | I I I

3

3

3

3

3

3

3

A

-30.(X| . 31,10- 1 l«/7.: 30.01 30.05I100.2I1071.99I107.2M100.01 103.63 |103.6| 100.0| 97.96 198.0 I 106.291106-31 | P

50000.0152163.33 I IOU. 3150000. 0151223. 33 1102. U | 51880. U8 1103. 8|| P30.01 27.18 190.6 I 30.01 29-96 199-9 1 1 IIP

300.01 319-611106-51 300.01 307.69 1102. 6| 322.U7I107-5I 1 P500.01 537. 3U 1107.51 500.01 505-051101.01 5U3.U2I108-7I 1 P

(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115

FORM II (PART 1) - IK 7/87

35

U.S. EPA - CU


Lab Nao*:Lab Cod*: Ca«* No.:Initial Calibration Sourc*! Li-(LfiL IT&ST&Continuing Calibration Souros

Contract:SAS No.: SDG No.

Conc*ntration Unitss ug/L

I|Analyt*I|AluminumI Antimony"IArsanic_|BariumIBarylliumI Cadmium|Calcium_I chromiumI cobaltICopp*r__I Iron___|L*ad___IMangan***|M*reury_I Nic!c*l_IPota»«iua|s*l*niumI SilverI sodiumI ThalliumI vanadiumI Zinc|Cyanid«_|

Initial CalibrationTru* Found

Continuing Calibration > iTru* Found %R(1) Found %R(1)ii

i oo .o"' •yj.io ' 2ZZ(1) control Li»it«t lurcury 10-120; Oth«r lUtala »0-110» cy«aid« iS-lis

mot ZZ (PA« 1) - ZM 7/87

36

U.S. EPA - CLP

2BCRDL STANDARD FOR AA AND ICP

Lab Hame: ETC CORP.Lab Cod*: Cats* Mo.:

AA CRDL Standard Source: LLFNSTD

ICP CRDL Standard Source: LLICPSTD

Contract:SAS No.: SDO No.: MT51W


111I Analyte1I AluminumI Ant imony1 Arsenic _1 Barium1 Beryllium1 Cadmium1 Calcium1 ChromiumI Cobalt1 CopperllronILead1 MagnesiumI ManganeseI MercurylNick.11 PotassiumI Selenium1 Silver1 Sodium1 Thallium{VanadiumIZinc1 Cyanide1

CRDL

True

10.0

5 - 0

sooo.o5.0

10.0

Standard f

Found

5.12

U.W4

HOIO.OO5-20

10.12

sr AA

%R

51.2

88.8

\UO.£IOU.0

101.2

CRDL Standard for ICPInitial Final

True Found %R Found %R1 I I I

1000.01 1002.67 1100.31 U78 . 1*0 1 95 . 7200.0| 201*. 70 1102. l*| 90.11*190.1200.01 197.57 198.8 I 39-83179-71*00.01 1*03.21* 1100.81 201.701100.8

l40.0| 1*0.13 1100.31 9-70197.0U O . O I U0.59 1101.51 9.1*6|9U. 6

U O O O . O l 1»OU6.69 |101.2| 1987. 80199. 14120.0| 122. lU 1101.81 26.63188.8

80.0| 80.95 1101.21 38.06195.1120.0| 121. U8 |101.2| £0.251100. ItU O O . O I U03.02 1100.81 200.931100.5200.01 199-51 199.8 I l»9.86|99-7

U O O O . O I U036.96 1100.91 2011.7UI100.6120.0| 121.56 1101.31 29.5H98.1*

1 I I I120.0| 120.59 1100-51 60.121100.2

1*000.01 1*011.31 1100.31 1U O O . O I U09. UO |102.U| 51.1*7151.5

1*0. 0| 1*0-32 1100.81 19.6H98.020000 . 0 1 2009U . 68 1 100 . 5 1 10161 . 88 1 101 . 6

1 I I I120.01 121.37 1101. 11 62.211103.7200.01 202.86 1101.1*1 1*8.05196.1

1 I I I

FORM II (PART 2) - IN 7/87

37

U.S. EPA - CLP

3BLANKS

Lab Name: ETC CORP.Lab Code:

Contract:SAS No.:Case No.:

Preparation Blank Matrix: (soil/water): WATER

Preparation Blank Concentration Units (ug/L or mg/kg): ug/L

SDG No.: M751W

11lAnalyte1|Aluninum_(Antimony1 Arsenic _(Barium1 BerylliumI Cadmium|Calcium_(Chromium1 Cobalt __1 Copper __1 Iron(Lead ___{MagnesiumI Manganese1 Mercury1 Nickel __1 Potassium1 Selenium[Silver1 Sodium __1 Thallium1 Vanadium~1 Zinc(Cyanide

InitialCalib.Blank(ug/L)

32315

-2

1-214

363

148-5

-231

233-65

6813

1

53881538852073|02610193

f

1111

C|1I U IIUI

I B II B IIBIIUI

IBII B I

UIUI

I B IIUII U II U I

IUI

ContinuingBlank

1 C

32.531.3

.8-2-9

.11.0

20.1-14.146.83-5

U8.21.1

lU.O1.3

.12.0

39.2-.85.1

68.01.13-93-3

IUI

IBII B IIUIIUIIBIlulI U IIUIIUIIB|lu l|U|IBI

IU|IUIIUIIUIIUI

Calibration(ug/L)2 C

32.531.3

.8-3.5

.11.0

20.13.86.83.5

1(8.21.1

16.11.3

.1-2.3140.9

.75-1

68.01.13.9

%

IUI

I B IIBIIUIIUI

IUI101|U|IUIIBI

ffl-IBI|U|IUIIUIIUIIUI101

3

32.531.3

.8-3.2

.11.0

20.1-l(.26.83-5

1(8.21.1

20.141.3

— rV.7

5-168.0i.l3.93.3

i ri ini in

I U I I

IBMI B I Il u l ll u l lI B I Il u l ll u l ll u l l

Kl ll u l l1 I I

|U||

I U I II U I IMM

Prepa-rationBlank

32.531-3

.8-2.5

.11.0

53.63.86.83.5

148.21.1

13.31.3

. V2.0

-714.0.7

5-195-21.13-9>4.8

11I II I

Cl MI I

I U I I PI U I I PI U I I PI B I I PI B I I PI U I I PI B I I PI U I I PI U I I PI U I I P|U||PI U I I PI B I I PI U I I PItillCS/

' I U I I PI B I I PI U I I PI U I I PI B I I PI U I I FI U I I PI B I I P(Ull&Sl

FORM III - IN 7/87

38

U.S. EPA - CLP

3BLANKS

Lab Name: ETC CORP.Lab Code;

Contract:SAS No. :Case No.:

Preparation Blank Matrix: (soil/water): WATER

Preparation Blank Concentration Units (ug/L or mg/kg): ug/L

SDG No.: M751W

11111 Analyte1I AluminumI Ant imony1 ArsenicI Barium1 BerylliumI CadmiumI Calcium1 ChromiumI Cobalt1 Coppert IronILead1 Magnesiumj Manganese1 Mercury1 NickelI Potassium(SeleniumI Silver1 Sodium1 ThalliumI VanadiumIZincI Cyanide1

1Initial 1Calib. 1 Continuing CalibrationBlank 1 Blank (ug/L)(ug/L) C| 1 C 2 C 3

112. S I t l l 12.5 IUI 32.5 IUI•(1.1 IUI 31.3 IUI 31.3 IUIS.S IB! 10.8 1 1 16. U 1 1

-2.8 IB l -2.6 1BI -2.5 IBI.1 IBI .2 IBI .2 IB!

l.S |BI 1.3 IBI 1.8 IBI-5U.1 |BI 20.1 IUI 20.1 IUI

1.8 |t!l 3.8 IUI 3.8 IUI6.8 |UI 6.8 IUI 6.8 IUIl.S |UI 3.5 IUI 3.5 IUI

liB.2 |UI U8.2 IUI U8.2 IUI-«.n |B| 1.2 IBI 5.0 IBI

-51.7 |Bl 7.3 IUI 7.3 IUI11 |t!| 1.1 IUI 1.3 IUI

\ U M I I9.0 |I/| 2.0 IUI 2.0 IUI

33.2 I B I I I I I . . .-fi 6 |R| 8.8 1 1 2.0 IBI«..! |U| S.I IUI 5.1 |Ul

KR a |tl| 68.0 IUI 68.0 IUI1 . 1 I U I I I Mva |u| 1.Q IUI 3.9 IUIT T |ii| 1.1 |UI 3.3 IUI

1 | M \U\ 3-y M

T

c

.

11

1Prepa-rationBlank

'

|

1

C

n —iii1 M1I PI PIPI PI PIPI PIPIPI PI PIPI PI Pl£Î PI PIPI PI PIFI PI PW>

FORM III - IN 7/87

39

U.S. EPA - CLP

ICP INTERFERENCE CHECK SAMPLE


ICP ID Number: JA9000

Case No.:Contract:SAS No.: SDG Ho.: M751W

ICS Source: LLCALIBSTD


IAnalyteI______IAluminum_I Ant imonyI Arsenic_I BariumI Beryllium(Cadmium(Calcium_(Chromium(Cobalt'I Copper__(IronI Lead'

II TrueI Sol. Sol.

A AB

Initial Found

I Haguejium(Manganesej Mercury_(Nickel__(Potassium(Selenium(Silver_'(Sodium_(ThalliumI VanadiumI Zinc__'I Cyanide_I______

Final FoundSol. Sol.

A AB

11*370001'i__rI——Ti—53? rI 1*231"I 8151"(It6l000|

It22f

1*681"1631*001"

9361"1*71*00011*1*51;

59.21*145.81105.1*1"817.6 1100.31"

1*50210.3 197.7 I"1*27.6 1101.31"U23.2 (101.71"1*75-8 (101.71"

(163865.7 1100.31"I 81*9.9 (90.8 I"(5051*1*9.7 1106.61"I 1*56.1 1102.51"

Itlt2.2813.0

141*2365.11)28.3U18.91*73.8

163651*. 8862.1*

5038U7.51*59.1*

199.8196.0(101.5(100.71101.21100.2192.1106.31103.2

FORM IV - IK 7/87

40

U.S. EPA - CLP

5ASPIKE SAMPLE RECOVERY



Contract:SAS No.:

EPA SAMPLE NO.

I 1GWP1AI

SDG Mo.: M751W


Concentration Units (ug/L or mg/kg dry might); ug/l

IIIlAnalyteII Aluminum_I Antimony"I Arsenic _I BariumI BerylliumI Cadmium(Calcium1 Chromium| Cobalt _ ~1 Copper __llronILead{Magnesium1 Manganese1 Mercury1 Nickel __{Potassium{Selenium{Silver __{Sodium __IThallium_{Vanadium{Zinc ___ {Cyanide1

ControlLimit»

75-12575-12575-12575-12575-12575-125

75-12575-12575-12575-12575-125

75-125IS-ttlf75-12575-12575-12575-12575-12575-12575-12575-125•75 -iag

Spiked SampleResult (SSR) C

1920.00001*95.000038.9000

2050.0000149.UOOO143.8000

82300.0000190.00001*68.00002U6.0000997.000021.0000

51700.0000U85.0000

B.'lJOO1479.0000

20100.00009.6700

1*7.5000214000.0000

50.80001495.0000148)4.0000ff / . ' fao

-

_

~

~

~;

1 11 1Sample 1 Spike I

Result (SR) Cl Added (SA)| %R1 1

0.0000 |U| 2000.0 196.00.0000 |U| 500.0 199.00.0000 |U| UO.O 197.3

57.3000 |B| 2000.0 {99.60.0000 |U| 50.0 198.80.0000 |U| 50.0 {87.6

73100.0000 | | 10000.0 192.00.0000 |U| 200.0 195.00.0000 |U| 500.0 193.6o.oooo lui 250.0 198.140.0000 ID'1 1000.0 199.70.0000 JUI 20.0 1105.0

141600.0000 | | 10000.0 1 101.02.6500 jfl 500.0 (96.5o.oooo lu.1 i.o I13.Oo.oooo |u| 500.0 195. 8

779.0000 |B| 20000.0 196.60.0000 |U| 10.0 196.7o.oooo |u| 50.0 195.0

3260.0000 |B| 20000.0 1103.70.0000 |U| 50.0 1101.6o.oooo |U| 500.0 199.0

12.6000 |B| 500.0 I9l(.3o.oca? l(Jl IDO.O W-i

Q

~

~~

_~""

""

H

pffffff?pppFppii)pTppfpte

Comments:

FORM V (PART 1) - IX 7/87

41

U.S. EPA - CLP

5BPOST DIGEST SPIKE SAMPLE RECOVERY



Contract:SAS No.:

EPA SAMPLE NO.

I"1QWP2A

SDG Ho.: M751W


Concentration Uniti: ug/L

1111 Analyte11 Aluminum1 Ant imony1 Arsenic1 Bar ium1 Beryllium1 Cadmium1 Calcium1 Chromium1 Cobalt1 CopperllronILead(MagnesiumI Manganese1 MercuryI Nickel __1 Potassium1 Selenium[SilverI Sodium __1 Thallium1 Vanadium"1 Zinc1 Cyanide

ControlLimit

%RSpiked SampleResult (SSR) C

20.20

9-5U

9.67

19.00

1

-

-

-

-

SampleResult (SR) C

0.00

0.00

0.00

0.00

u

--u

-

u

SpikeAdded (SA)

20.0

10.0

10.0

U| 20.01

_

%R

101.0

9THT

9577"

95.0

Q

~

H

PP

PPPFPP

PPFPPFPP

FORM V (PART 2) - IH 7/87

42

U.S. EPA - CLP



Case No.:


Contract:SAS No.:

EPA SAMPLE NO.

I1GWB7RR

SDG No.: M751W



1111 Analyte1I Aluminum_|Antimony_1 Arsenic1 Barium1 Beryllium1 Cadmium(Calcium1 Chrom ium1 Cobalt1 CopperllronILead(Magnesium1 Manganese1 MercuryINickel(Potassium[Selenium(Silver(Sodium|Thallium_(Vanadium1 Zinc(Cyanide

ControlLimit%R


22.70

10.20

9-37

19.00

1

-

-

SampleResult (SR)

2.76

0.00

0.00

0.00

C

I

~

u

5

0

SpikeAdded (SA)

20.0

10.0

10.0

20.0

to

99-7

102.0

93.7

95.0

Q

~

~

-

M

PPFfPPPPPPPFPP

PPFPPFPP

Com

FORM V (PART 2) - IN 7/87

43

U.S. EPA - CLP

5BPOST DISEST SPIKE SAMPLE RECOVERY



Contract:SAS No.:

EPA SAMPLE NO.

I 1GWB9RR |

SDG No.: MT51W~

Level (low/med): Low


111lAnalyte

1 Aluminum1 Antimony"(Arsenic ~1 Barium

r~ —— i —————Control |Limit (Spiked Sample*R (Result (SSR) C

1 Beryllium I ——————1 Cadmium ~ ——————————1 Calcium |~ ————(Chromium(Cobalt ~(Copper(Iron1 Lead(Magnesium(Manganese1 Mercury(Nickel(Potassium(Selenium(Silver ~1 Sodium(Thallium1 Vanadium"(Zinc1 Cyanide

—————

-

—————————

&0.20

———— ———— •" ——————— -

———————— -

9.89-

__

- 6.69,_

17.70

1 ~ ——— —— ———— ————————— —————— —— ———————

~

~

~~~~

~~~~~~~~~

~

r~ ———Sample

Result (SR)

•

62. So'

.

._

0.00

1

.0.00 .-0.00

_-

C

_

~

~

~~~u

5

u"~~

1 —————Spike

Added (SA)

20.0---

10.0-

10.0

20.0

11

«JQ

5To~

957?"

SeTT

85\r

~~~~~~

~~

"~~~~£~~~

~_

M

PPFPPPPPPPPFP 1P

1P 1P 1F 1P 1P 1FP 1P 1

11

Comments:

FORM V (PART 2) 7/87

44

U.S. EPA - CLP


Lab Name: ETC CORP.Lab Cod*: Cast No.:


Contract:SAS No.:

EPA SAMPLE NO.

| 1GWB9ARI

SDG Mo .: MT51W

Level (loH/med): LOW


111lAnalyte1I Aluminum1 Ant imony1 Arsenic1 Barium1 Beryllium1 Cadmium1 Calcium1 Chromium1 Cobalt1 Copper[IronILead1 Magnesium1 Manganese1 Mercury(Nickel1 Potassium1 Selenium1 Silver1 Sodium1 Thallium(Vanadium1 Zinc1 Cyanide

ControlLimitW


33-90

11.50

9.16

17-70

1

-

-

-

-

_

SampleResult (SR) C

13.60

0.00

0.00

0.00

-

_

u~™

u

3

SpikeAdded (SA)

20.0

10.0

10.0

20.0

»

101.5

115-0

5O~

B5TI"

<J

__

;—

-

~I

~

~

-

M

———

Fff

PPFPPFPP

Comments:

FORM V (PART 2) - IM 7/87

45

U.S. EPA - CLP


Lab Hame: ETC CORP.Lab Cod«: Case No.:


Contract:SAS No.:

EPA SAMPLE NO.

I II FLDBLANK |I_______ I'

SDG No. : M751W

L«vel (low/med): LOW


1 11 | Control! I LimitlAnalyt* 1 %R1 11 Aluminum |[Antimony |Arsenic |

1 Barium IIBerylliuml1 Cadmium I1 Calcium I1 Chromium I1 Cobalt |1 Copper 1llron I1 Lead 1IMagnesiuml1 Manganese 11 Mercury |1 Nickel |Potassium I

1 Selenium |ISilver I1 Sodium I1 Thallium I1 Vanadium 11 Zinc I1 Cyanide I


20.50

11.70

10.30

19.90

1

-

SampleResult (SR)

0.00

1.1U

0.00

0.00

C

5

I_

u

0

SpikeAdded (SA)

20.0

10.0

10.0

20.0

»

102 5

105.6

103.0

99-5

Q

~

-

-

-

M

PPFPPPPPPPPFPP

PPFPPFPP

Comments:


46

U.S. EPA - CLP




Contract:SAS No.:

EPA SAMPLE NO.

I 1CWB12RR |i ______ rSDG No.: M751W



111(Analyte11 Alum inujn_(Antimony^(Arsenic1 Barium1 BerylliumI Cadin ium(Calcium1 Chrom ium(Cobalt|Copp«rllron(Lead1 Magnesium(Manganese(Mercury(Nickel

ControlLimit»

IPotassiuml|Sel«nium_(SilverI Sodium(Thallium(Vanadium"(Zinc(Cyanide


19.90

11.70

9-53

18.140

1

~_

~

~

-

SampleResult (SR)

0.00

0.00

0.00

0.00

C

5

U

V

U_

11

Spike IAdded (SA)| %R

111

20.0 (99-511111111

10.0 (117.011111

10.0 (95-311

20.0 192.0111

Q_

5

"

"~

M

PPFPPPPPPPPFPP

rFFPPFPP

Comments:

FORM V (PART 2) - IK T/8T

47

U.S. EPA - CLP


Lib Name: ETC CORP.Lab Code: Case No.:


Contract:SAS Ho.:

EPA SAMPLE NO.

I 1C.WB17RR II __________ I-

SDG No.: M751W



1111 Analyte1 ______1 Aluminum_1 Ant imony_1 Arsenic1 Barium1 BerylliumI CadmiumI CalciumI Chromium1 Cobalt1 CopperllronILead1 Magnesium1 Manganese1 Mercury1 Nickel1 Potassium1 Selenium1 SilverI Sodium(Thallium1 VanadiumIZinc1 Cyanide

ControlLimitw Spiked Sample

Result (SSR) C

21.00

11.00

9.16

18. UO

~*

-

SampleResult (SR)

8.21

0.00

0.00

0.00

1

C

B

U

5

U

SpikeAdded (SA)

20.0

10.0

10.0

20.0

%R

5O~

110.0

9TTT

92.0

Q

£

I

~

H

PPFPPPPPPPPFPP

PPFPPFPP

Comments:

FORM V (PART 2) - IK T/8T

48

U.S. EPA - CLP




Contract:SAS No.:

EPA SAMPLE NO.

I II 1GWB19RR II_________I'

SDG No. : M751W

Level (lo«/med>: LOW


111lAnalyte1(Aluminum^1 Antimony1 Arsenic ~[Barium1 Eery Ilium1 CadmiumI Calcium1 ChromiumI Cobalt1 CopperllronILead1 Magnesium1 Manganese1 Mercury1 NickelI PotassiumI Selenium1 Silver1 SodiumlThallium_I Vanadium'IZincI Cyanide

ControlLimit»


28.10

11.20

9-53

18.80

1

-

-

-

—

-

-

SampleResult (SR)

8.21

0.00

0.00

0.00

C

I

u__

0_5_

SpikeAdded (SA)

20.0

10.0

10.0

20.0

tt

99~r

112.0

95-3

9TTo~

Q

-

-

~

~

-

M

PPFPPPPPPPPFPP

PPFPPFPP

Com


49

U.S. EPA - CLP




Contract:SAS No.:

EPA SAMPLE NO.

I I| 1GWB1URR |I___________]•

SDG Ho.: M751W



111I Analyte11 Aluminum^1 Ant imony_1 ArsenicI Barium1 BerylliumI CadmiumI CalciumI ChromiumI Cobalt1 CopperllronILeadI Magnesium1 ManganeseIHercuryI NickelI Potassium1 SeleniumI Silver1 Sodium|Thallium_1 VanadiumIZinc1 Cyanide

ControlLimit*R

—————


21.00

10.70

9-53

19-50

1

-

-

~-

SampleResult (SR) C

.87

0.00

0.00

0.00

I

u

0_u

-

SpikeAdded (SA)

20.0

10.0

10.0

20.0

%R

100.6

107.0

95-3

97~T

Q

~

M

PPFPPPPPPPPrttftFPPFPP

Comments:

FOl'M V (PART 2) - IK 7/87

50

U.S.. EPA - CLP


Lab Name: ETC CORP.Lab Code: Ca.st No. :

Matrix (soil/vater): WATER

Contract:SAS No.:

EPA SAMPLE NO.

I II 1CWB16RR |I___________C

SDG Ho.: M751W



IIIlAnalyteII Aluminum_lAntimony_I ArsenicI BariumI BerylliumI CadmiumI Calcium{ChromiumI Cobalt(CopperI IronI LeadI Magnesium(ManganeseI Mercury(Nickel(Potassium[Selenium(Silver(Sodium(ThalliumI Vanadium(Zinc(Cyanide

ControlLimit%R

—————

—————


22.90

10.50

8.80

19.20

I

-

-

~

SampleResult (SR)

2.82

0.00

0.00

0.00

C

_

I_

5

™

u

u

SpikeAdded (SA)

20.0

10.0

10.0

20.0

XR

100. u

105.0

SO"

5O~

Q

""

I

""

~

I

4

3—3

"

PPFPPFPP

Comnenti:


51

U.S. EPA - CLP


Lab Name: ETC CORP.Lab Code : Case No . :


Contract:SAS No.:

EPA SAMPLE NO.

II X DUPI

SDG Ho.: M751W



1111 Analyte11 Aluminum1 Ant imony1 Arsenic1 Barium1 BerylliumI Cadmium1 Calcium1 Chromium1 Cobalt1 CopperllronILead1 Magnesium1 Manganese1 Mercury1 NickelI Potassium1 Selenium1 Silver1 Sodium1 Thallium1 VanadiumIZincI Cyanide

ControlLimitJ»

—————

—————


23.30

12.50

10.30

18.80

1

~

-

-

-

-

SampleResult (SR) C

3.68

1.92

1.10

0.00

B

-

B_

B

U

-

SpikeAdded (SA)

20.0

10.0

10.0

20.0

SS

9O~

10575

92.0

9"*.0

Q

~

~

~

-

M

PPFPPPPPPPPFPP

PPFPPFPP

Comments:

FORM V (PART 2) - IN T/87

52

U.S.. EPA - CLP


Lab Name: ETC CORP.Lab Cod*: Case No.:


Contract:SAS No.:

EPA SAMPLE NO.

II 1GWP3AI______

SDG No.: M751W

level (low/med): LOW


11lAnalyte11 Aluminum1 Antimony_I Arsenic1 Barium1 Eery IliumI CadmiumI CalciumI Chromium[Cobalt1 CopperllronILeadI Magnesium1 Manganese1 Mercury{Nickel1 PotassiumISelenium[Silver[Sodium[Thallium[Vanadium"[Zinc[Cyanide

ControlLimit»


20.50

10.70

9-53

19.90

1

-

-

-

SampleResult (SR)

1.52

0.00

0.00

0.00

C

i

~

"5

-

0

B

SpikeAdded (SA)

20.0

10.0

10.0

20.0

*R

§E7F

107.0

95.3

99.5

Q

-

~

_

M

PPFPPPPPPPPFPP

PPFPPFPP

FORM V ;PART 2) - IN 7/87

53

U.S. EPA - CLP



Matrix (soil/wattr): WATER

Contract:SAS No.:

EPA SAMPLE NO.

I10WP3B

SDG No.: M751W


Concentration Uniti: ug/l

111lAnalyte11 Aluminum^1 Ant imony_(Arsenic1 Barium1 Beryllium1 CadmiumI Calcium _1 ChromiumI Cobalt1 CopperllronHead1 Magnesium{Manganese1 Mercury1 NickelI PotassiumI Selenium1 SilverI Sodium1 ThalliumI Vanadium"1 Zinc

1 1Control I

Limit I Spiked Sample%R IResult (SSR) C

1111 19.00111111111 10.70111111 9.16111 19.2011

1 Cyanide I I1

-

_

SampleResult (SR)

0.00

0.00

0.00

0.00

C

5

u

u

u

-

SpikeAdded (SA)

20.0

10.0

10.0

20.0

W.

95-0

107.0

9O~

9O~

Q

_

~

~

-

H

PFPP

PPFPPFPP

Comments:

FORM V (PART 2) - IK T/87

54

U.S. EPA - CLP

DUPLICATES

Lab Same: ETC CORP.Lab Coda: Case No.:

Matrix (soil/wat«r): WATER

% Solids for Sample: 0

Contract:SAS No.:

EPA SAMPLE NO.

10WP1A |I________!•

SDG No.: M751W


% Solids for Duplicate: 0


1 1I I ControllAnalyte I Limit1|Aluminum_|Antimony_I Arsenic _I Barium __j Beryllium|Cadmium_I Calciumj ChromiumI Cobalt __1 Copper __llronILead(Magnesium(Manganese(MercuryIKickel __(Potassium1 Selenium1 SilverI SodiumI Thallium(Vanadium1 Zinc(Cyanide

200.060.010.0200.0

5-05.0

10.050.025.0100.05.0

15-0

CoTo"5000.0

5-010.0

5000.010.050.020.0

I III Sample (S)I I1 1 o1 1 oI I oII 57I I 0I I 01 1 73100I I 0II • 01 1 0II oI I o| I 141600I I 2I II I oII 7791 1 0II 01 1 32601 1 0II oII 12I I

00000000000030000000000000000000000000000000000000006500

00000000000000000000000000006000

1 1I IC| I Duplicate (D)I I

l u l ll u l ll u l lI B I Il u l ll u l l1 I II U I II U I IIUIIlulll u l l1 I IIBM1 IIl u l lIBMI U I IlullI B I II U I II U I II B I I1 I I

00058

073UOO

00000

U20002

00000000oooo6000063U00000000oooooooooooooooooooooooo8900

0.00008114.00000.00000.0000

3300.00000.00000.00008.71(00

C|| RPD

|U||I U I II U I II B I I 2.2I B I I!"!!-!.-l u l lI U I II U I Ilull|U||1 II 1.0IBM 8.71 IIIUIIiBii~inrl u l llullIBM 1.2l u l l

I IIIQI II II I

II"-!!-1I II II II I-I'-l l "I II III"

|U|| ||IBII 36.2 ||~1 I I I I

M

ppFppppppppFppppFppFpp

1

FORM VI - IN 7/87

55

DUPLICATESE?A SAMPLE t:o.

Contract:C*s« He.:Lab Cod«: _____

Matrix (soil/water):t Solids for Saapl*:

Concentration Onits (uo/L or aa/Xa: dry veiqht)

SAS Ko.: _____ SDC Ho. ;

L«v«l (low/cad):

% Solids tor Ouplicata:

|Analyt«IAlu»inua_|Antiaony_I Arsenic_IBariuaIBeryllluaI Cadaiua_ICalciua_IChroaiua

! I cobalt ~|Copp«r_I Iron__I Lead|Magn«siua(Mercury_IHicJcelIPota«slui|S«l«niuaI9ilv«rISodiua__(Thalliua|Vanadiua'I Zinc|CyanI3«|

~

ControlLiait saapl* (S)

I II II II II II II Ii tI I V I

c

11111_l

Duplicate (0): .

11111i n

RPO Q

rom vz - m 7/87

56

U.S. EPA - CLP

LABORATORY CONTROL SAMPLE


Solid LCS Source:

Cast No.:

Aqueous LCS Source: LLCONTROLSTD

Contract:SAS Ho.: SDG No.: MT51W

111 Analyte11 Aluminum^1 Antimony"1 Arsenic1 Barium1 Beryllium1 Cadmium1 Calcium1 Chromium1 Cobalt1 Copper1 IronILead1 Magnes ium1 Manganese(MercuryINickel1 Potassium1 Selenium1 SilverI Sodium1 Thallium1 Vanadium"1 Zinc1 Cyanide1

Aqueous (ug/L )True Found %R

1 12500.01 2532.19 1101.3

500.01 U9 14.99 199-030. ol 30. Q. 1 100-7

1000.01 997.28 199-7100.01 98.21 198.2loo.ol 100.53 1100.5

10000.0110008.27 1100.1300.01 307.66 1102.6200.0| 208.31 I10U.2300.01 296.50 198.8

1000.01 991.01 199.13oQ 1 30-8- IJM..

10000.01 9922.57 199-2300.01 301.5k 1100.5

J.ol \.1\ 1 gff.ff300.01 302. U6 1100.8

Uooo.ol 3809.91 195.230.0 ! 30-8- 1 I«U100.01 92.32 192-3

50000.0 | U9596. 80 199-230.01 27.83 192.8

300.0| 298.69 199-6500.01 502. uu 1100.5IQto.QI 101^0 U0<-f

TrueSolid (ng/kg)

Found C Limits

~

_

~

XR

FORM VII - IK 7/87

57

U.S. EPA - CLP

ICP SERIAL DILUTIONSEPA SAMPLE NO.



I| 1GWP1A

Contract:SAS No.: SDG No.: H751W

Leva! (low/mod): LOW


1 I I1 I | Initial SamplelAnalyte | I Result (I)1 I I1 Aluminum_| |lAntimony | |lArsenic I I1 Barium ! 1IBerylliumI || Cadmium | I1 Calcium _ | |I Chromium I j1 Cobalt I I1 Copper 1 1llron I IHead ||1 Magnesium! |1 Manganese | I1 Mercury I IINickel I I1 Potassium! I1 Selenium I II Silver __ I |I Sodium | |IThallium I 11 Vanadium I |IZinc ~| I(Cyanide | |1

-1.551.61

57.30.Olt.88

73100.00-.55

-2.152.00

111. 60

141600.002.65-.78

1.U33260.00

1-5312.60

1 1I I

CMI I

l u l ll u l l1 I II B I Il u l ll u l lL I I|U| ||U||l u l ll u l l1 I II B M1 I I|U||1 I I1 I Il u l lI B I I1 I Il u l lIBM1 I I

SerialDilutionResult (S)

0.000.00

U3.70.38

0.0075600.00

0.000.000.00

107.00

U3200.000.00

0.00

5.913^80.00

6.789-99

I I % I II I Differ- | |

C| 1 ence I l«I I I I

|U | | ||I U I I I I1 I I I IIBM 2 3 . 7 1 1 'I B M I I "|U| | ||1 I I —— 3~G|fl u l l I fl u l l ||I U I I | |1 I I I I1 I I I I1 I I 3.8|||0|| 100.011I I I I fl u l l I I1 I I I I1 I I I II B M I II B I I STfl lI I I I I "IBM ||IBM —— 2o77l f1 I I I I

11

M 11

NR|NR|

1P 1NR|NRIP 1NRINRINR|NR|

1P 1NRI

1NRI

11

NRIP 1

1NRINRI

11

FORM IX - IN 7/87

58

U.S. EPA - CLP

10HOLDING TIMES


Contract.SAS No.: SDG No.: M751W

EPASample No.

I 1GWB12RR1GWB1URR1GWB16RR10WB17RH1GWB19RR1GWB7RR1GWB9AR1GWB9RR1GWP1A1GWP2A1GWP3A1GWP3BFLDBLANXX DUP

Matrix

WATERWATERWATERWATERWATERWATERWATERWATERWATERWATERWATERWATERWATERWATER

1

1 11 1 Mercury1 1 Prep

Received | I DateI I

09/28/891110/11/8909/29/891110/11/8909/29/891110/11/8909/28/891110/11/8909/26/891110/11/8909/27/891 110/11/8909/28/891110/11/8909/27/891110/11/8909/19/891110/11/8909/27/891110/11/8910/03/891110/11/8910/03/891110/11/8909/28/891110/11/8909/29/891110/11/89

I II II II II II II II II I1 I

I IMercury I I CyanideHolding | | PrepTime | | Date

I I13 II l/>"t-**i12 11"12 II13 I I15 H1 U I I13 II1 U I I22 ||1U II8 I I8 I I13 II12 UN j

I II II II II II II II II II I

CyanideHoldingTime

4=

<£-$-la

4=*K <S "

-2^-

FORM X - IN 7/87

59

11INSTRUMENT DETECTION LIMITS (QUARTERLY)



Flame AA ID Number: PE5100

Furnace AA ID Number: PE5100

Contract:SAS No.:

Date:

SDG No. : M751W

Comment!:

1 1 11 ' | Wave-11 | length I Back-lAnalyte j (nm) 1 ground1 1 1I Aluminum 1 308.2211 Antimony 1217-5811 Arsenic 1 193.701 BZ1 Barium |U93.Ul||Beryllium|313.0U|1 Cadmium 1228.80 1I Calcium 1370.601I Chromium 1267.721I Cobalt ~|228.62|(Copper I32U.75Illron I271.W4IILead 1283.311 BZ1 Magnesium 1279- 81!1 Manganese |257. 6l|1 Mercury 1253.6511 Nickel 1231.6011 Potassium J766. 1491ISeleniun U96.03I BZ1 Silver ~ 1328.0711 Sodium 1589.591IThallium 1276.791 BZ1 Vanadium" 1 292. Uo|IZinc 1213.86!1 Cyanide I I

CRDL(ug/L)

20060102005550001050251005500015.2uo50005105000105020

IDL(ug/L)

32.531.3.8•9.11.020.13.86.83.51*8.21.17.31.3.12.01U.5.75.168.01.13.93.3

111I M1I PI PIFI PI PIPI PI PIPI PI PIFI PI PlevIPI AIFI PI PIFIPIP1

FORM XI - IN 7/87

60

U.S. EPA - CLP

12AICP INTERELEMENT CORRECTION FACTORS (QUARTERLY)

Lab Name: ETC CORP.Lab Code: Case Ho.:


Contract:SAS No.: SDG No.: M751W

Date: 10/06/89

IIIlAnalyteI(AluminumI Antimony(Arsenict BariumI Beryllium{Cadmium _I CalciumI ChromiumI Cobalt1 CopperllronILead(Magnesium(Manganese[Mercury{Nickel(Potassium1 Selenium(Silver(Sodium(Thallium(Vanadium"IZinc(Cyanide

1 1Wave- | | Intere lenientlength | |(nm) 1 1 AL CA

I I308.22 II217.58 I 1193.70 | | .003140U"•93.1H II313. Oil ||228.80 ||370.60 ||267.72 II228.62 ||32U.75 I I271. UU 1 1283-31 II -.000331279.81 ||257.61 (1253.65 I I231.60 1 1766. U9 II196.03 II328.07 II589-59 1 1276.79 II292. UO ||213.86 II

I |

-.000152

Correction

FE

-.0003911. OOOU21)

-.0002911

.000113-.002508

.000379

.000098

Factors for:

MO AS

-.000231

.000250

.01768U

FORM XII (PART 1) - IN 7/87

61

12BICP INTERELEMENT CORRECTION FACTORS (QUARTERLY)

Lab Name: ETC COUP.Lab Code: Case No.:


Contract:SAS No.: SDG Ho . : M751W

Date: 10/06/89

111lAnalyte11 Aluminum_1 Ant imony_1 Arsenic ~1 Barium __1 Beryllium1 Cadmium _I Calcium(Chromium1 Cobalt1 CopperI IronILead1 Magnesium1 Manganese1 Mercury1 Nickel __I Potassium1 Selenium1 Silver1 Sodium|Thallium_(Vanadium(Zinc(Cyanide

1 1Wave- I | Interelementlength I |(nm) t| CU CR

I I308.22 ||217.58 I I193. TO ||1*93.1(1 | |313.01* | |228.80 I |370.60 ||267.72 I I228.62 ||32U.75 1 1271. UU ||283.31 II279.81 II257.61 ||253.65 II231.60 ||766. 1*9 II196.03 II328.07 I I589.59 I I276.79 I I292. UO ||213.86 | | .001329

I I

.010000

.00621*6

Correction

V

.0111*69

. 008291

-.002575

.003203-.0011*00

-02

-.065530

.001329

Factors for:

II HI

-.002837.0022314

- . 057936

.001202

.002261

.000353.007911*

Comments:

FORM XII (PART 2) - IN 7/87

62

U.S. EPA - CLP

13ICP LINEAR RANGES (QUARTERLY)

Lab Uame: ETC CORP.Lab Coda:


Case No.:Contract:SAS No.: SDG No.: M751W

111 .I Analyte1I Aluminum|Antimony_I Arsenic _1 Barium1 BerylliumI Cadmium _[Calcium1 Chromium1 CobaltI Copper __ilronILead1 Magnes ium1 ManganeseI MercuryI Nickel __I Potass ium{SeleniumI SilverI Sodium __1 Thallium{VanadiumIZinc{Cyanide _

Integ.Time(Sec.)

6.06.06.06.06.06.06.06.06.06.06.06.06.0

6^06.0

6.0

Concentration(ug/L)

25000500050001000010001000

100000300020003000100005000

1000003000

3000

100001000

50000030005000

M

NR

m

m

NRI

Comments:

FORM XIII - IH 7/87

63

METALS SUBSIDIARY DATA - ICP

Project No._Book No.. TITLE.

Page No._

&&

CS>aC.I/D

P

(TSUJ/V

/m<?OfcS

f-f

/SO

Ovt/

/IT/

Gut 1111

Ou/OH/

A

tin/ tfo)

To Pagt No. —

itnciscd t Undtrtlood by mt. Ditt Invtnttdby

R*cord*d by

Ditt

cDUMP OF METALS BATCH FILE 80F7OS IF METALS THU. OCT 12. 1919. 11:42 AM PAGE 1

Standard Regreiiion Data Detection Limit Blank Data

Element Cor r . C o e f f . Slope Intercept Units Blank Mean Sttf. Dev. MDL

/AC 0.19116 995 4 1 43 "9/1 -1 00 -1 00 10.0

'AL 0 91119 1005 33 4 09/1 -1 00 -1.00 100

AS 0.11979 942.2 43 5 "9/1 -1.00 -1 00 100

/B O.llill 912.1 1.51 "9/1 -1.00 -1.00 20.0

/ BA 1.0000 171.2 191 ug/1 -1.00 -1.00 20.0

Sal 1.0000 963.7 0.0576 "9/1 -1.00 -1.00 1.00-/C* 1.0000 967.1 0 171 ug/1 -1.00 -1.00 200

- CD 1.0000 974.1 -0 173 "9/1 -1.00 -1 00 2 00JCO 0.19911 941.3 -1.62 "9/1 -1.00 -1 00 20.0At 1.0000 159.2 -00311 "9/1 -1.00 -1.00 10.0-/CU 1 0000 910.0 1.15 "9/1 -1.00 -1.00 10.0

V/FE 1.0000 137.1 13.1 ug/1 -1.00 -1.00 ISO

"MS 1 0000 117.6 21.1 ug/1 -1.00 -1.00 100'/MN 1.0000 154 0 0 343 ug/1 -1.00 -1.00 5.00

MO 1.0000 114.1 0.412 ug/1 -1.00 -1.00 20.0

l/NA 1.0000 1001 37 .0 ug/1 -1.00 -1.00 500

' </NI 0.99999 939.6 -0.241 ug/1 -1.00 -1.00 20.0

PB 0 III77 931.4 -0 949 ug/1 -1.00 -1 00 75 09^ •'SI 0 99914 994.1 6 14 ug/1 -1 00 -1 00 600

SE 099913 1005 -691 ug/1 -1 00 -1.00 100SN 0 99991 931 0 -1 29 ug/1 -1 00 -1 00 50 0

S« 0 99991 1014 -5 97 ug/1 -1.00 -1 00 20 0

TI 1 0000 114.1 -1.25 ug/1 -1.00 -1 00 SO 0

/V 0.11111 959.9 2 46 ug/1 -1.00 -1 00 20 0

Jl* 1.0000 951.9 0 .473 ug/1 -1.00 -1 00 200

cDUMP OF METALS BATCH FILE BQF7051F METALS THU. OCT 12. 1919. 11:42 AM PAGE 2

Initial and Continuing C a l i b r a t i o n Verification and Calib. Blank Data

EleaMnt: (AC) Units: 119/1 Element (At) Units: HJ./1

Posit ioe7*1110121116112021233«11S367f*14•*101102104ISIS52i«11• I

i Sanwle CalculatedSXBlK 0.1SISAS1S14ASBSIS14BSCSIS14CCSS1SI4BCSSIS14ECSS1S140C SMIDCHKCSXISINTC SCUTACSCRIBCSLABCONC SMIDCHKCSLABCOMC SMIDCHKC SMIDCHKCSLABCONC SMIDCHKC SMIDCHKCSCHIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

20.131 120041.1477911•I.S110

23.410.494 9II. S•1.091.7•1.0•2.395 9•7.7l*.l9.3*114

0.9210.41S-0.102-0.1021 941.11

Expected0

20 040 020031 1SOD1000100III20.0

0100100100100100100100100

20.00III

.00

.00

.00

.00

.00

.00

I Itec104

97 0100

1069S.S91.191 59i.l11796 991.591.091 791.092.395 997.791.0

99.*

-92.3-41 510.210 2-194-111

791110121116112021233611SI67691499101102104

153552661191

SXBLKSASI5I4ASBSI514BSCSIS14CCSSI514BCSSI5I4ECSSI5I4DCSMIDCHKCSXtSINTC SCSI ACSCBIBCSLABCONCSHIOCHKCSLABCONCSMIDCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINT

CBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

13 04909955000

99412100250002S60

459000S4124*25202590251025502570241025202570471242

450000

-10.1-1 24-16.14.412 10-2.10

050010005000

99S12500250002500

4170005000

250025002500250025002500250025005000

417000

-1 00-1.00-1.00-1.00-1.00-1 00

91.099 5r°99 t9k. !99 1102IDS109

101101101102101

96 6101103

95.7

103

10101241610-443-210210

o\

c cDUMP Of METALS BATCH FILE BQF70S1F .METALS THU. OCI 12. 19I>. 11:42 AM

Initial and Continuing Calibration V«rlfieilion and Cilib. Blink Data

EUnxnl : AS Unlit u9/l EUnwnt (iT) Unit! 119/1

6r91110121316112021233131S367691491101102104

153552661391

• SXBlKSASIS14ASBSIS14BSCSI 514CCSSIS14BCSS 1 5 MECSSI5UDCSMIDCHKCSXI5INTCSCIIAC SOU IBCSLABCONCSMIDCHKCSLA8COMCSMIOCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSCDIACSC II IBCSXISINT


1.07110til1000114

23104190SIS

-170131

35.049241741947147147050347112$

39.1-214

6 1211.50 640

13.932.119.4

010020010001112SOO5000$0000

SO 0$00500500500500SOO$00SOO0

$0.00

-1.00- .00- .00- .00- .00- .00

11093 110097 I92 693 9103

70.191.497 497.794 295.694 0101

9$. 7

79.7

-612-1150-64 0-1390-3210-1940

7911101213161120212336315367691499101102104

IS35$2661391

SXBLKSASIS14ASBSI514BSCSI514C

CSSIS14BCSSI514ECSSIS14DCSMIDCHKCSXI5INTC SCR I ACSC* IBCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKC SCR I ACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

2 1099 2197100019123904150504

19.210442 9507505510497SOI475492SOO96 240.127.0

15 1-6 19-7.73-1.01-4 49-5.37

010020010001972500SOOOSOO000

500500500SOO500SOOSOOsoo000

-1.00- 00- 00

::8S- 00

99.291.7100

,5°?97 0101

101101102

99 4100

95 191 4100

-1510619773101449537

o\Oo

c cDUMP Of HfTALS BATCH MU BOf 705IF METALS THU. OC1 12. 1919. 11:42 AM MQC 4

Initial and Continuing Calibration Verification and Calib. Blank Data

EleMHt:(BA) Until: UJ/1 Unit I ug/1

Pot it Ion San»l< Calculated6 SXBLK -1.6079 '11

101213161120212336315367691499101102104

153552661391

SASI514AS8SIS14ISCSIM4CCSSI5I4BCSSI514ECSSIS14DCSMIDCHKCSXI5INTC SCI I AC SC« 18CSLABCONCSMIDCHKCSLABCOHCSMIDCHKCSMIDCHKCSLABCONCSHIOCHKCSMIDCHKC SC« I ACSCRIBCSX65INTCBBLKCBBLKCBBLKCBBLKCBBIKCBBLK

201401200040B4100667010204S»211at.i1020103010201010103096210101020202(7.0465

2.152.943.473.213.033.30

EnptcUd0

200400200040150001000010004392000

100010001000100010001000100010002000

43*-1.00-1.00-1.00-1.00-1.00-1.00

X «ac10110010010196 196 7102105101102103102101103

96.2101102101106215294347321303330

Position Saavlt Calculated6 SXBlK 0 03137911101213161120212336315367691499101102104

153552661391

SASI514ASBSI514BSCSIS14CCSSI514BCSSI514ECSSI514DCSMIDCHKCSXISINTC SCSI ACSCRIBCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKC SCSI ACSCRIBCSX45INTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

20.039.9200

40.141196510144621.19.17102102101

99 3100

95.491 3100

20.09 70442

0.07690.06730.05760 05760.05760.0313

Eipected0

20 040 020039 950010001004230

10.01001001001001001001001000

10 0423

-1.00-1.00-1.00-1 00-1.00-1.00

X Rec

10099 1|100'l02n.296 5101105

91.710210210199 3100

95.491 3100

97 0105

-7.69-6 73-5.76-5.76-5 76-3 13

O\VO

cDUMP OF METALS BATCH FILE BQF70S IF METALS THU. OCT 12. Kit. 11:42 AM

Initial and Continuing Calibration Verification and Calib. Blank Data

Unilt: 119/1 El»ont :(&>) Unlit: Kg/1

67911

1012131611202123363153676914*•101102104IS3552(I1391

SXBIKSASISUASBSIS14BSCSI5UCCSSI514BCSSIS14ECSSIS14DCSMIDCHKCSXISINTC SCI I ACSCRIBCSLABCONCSMIDCHKCSLABCONCSMIOCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKC SCI I AC SCI IBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

-21.9204031*020000403047700•670010100450OOO2140(17I96010200997099109970933097701010019*0941

442000-23.412 76.0413.2

-11 1-24 1

02000400020000

399050000100000100004110002000

010000100001000010000100001000010000100002000

461000

- .00.00.0000.00.00

10299 1100

10195 496 7101

97 7107

99 6102

99.799 199 793 397 710199.416.0

2340-1270-604-132017102410

Potitio67911

1012131120212336315367691499101102104

IS3552661391

• SampUSXBLKSASI514AS8SIS14BSCSI 514C

CSSI514BCSSI514ECSSIS14DCSMIDCHKCSXISINTC SCd I ACSCRIBCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINT


:alculaUd0.031420 339.720037 0434I9S94 611119 79 51939694969790.;94.95119 46113

-0 1250 00220-0 0155-0 01730.171-0 125

Exp.cled0

20 040 0200

39 750010001001150

10 01001001001001001001001000

10 0115

-1.00-1 00-I 00-1.00-1 00-1 00

X Rec101

99.2 |100 '

93 3«6 719 594.6100

95.193.396 994 296 497.490 394 495 3

94 699.112 5

-0.2201 551 73

-17 112 5

o

DUMP OF METALS BATCH FILE BQF7051FMETALS THU. OCT 12. lilt. 11:42 AM

••• I n i t i a l »nd Continuing Cllibolion V o r l f l c i t l o n and Callb Blink Dlt> ••*

Eltmnl (cc> Unili ug/1 Eltnenl: y Uniti: ug/1

67911101213161120212111315]67691499101102104IS1552661391

SXBLKSASI514ASBSI514BSCSI514CCSSI514BCSSI514ECSSI514DCSMIOCHKCSXI5INTCSCIIIACSCRIBCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

-2.1744.171 4400

10.1947

1190201421M.I12.4204201202200201192191200

11.119 1419

-2.71-0.117-0 296-3.12-1.61-1.47

040 010 0400

71.41000200020041140.00

20020020020020020020020040.00

411-1.001.00

I'M1.00

11091 1100102

94 794 4104102

99.5102104101

99 9101

95.991 I100

95.1101271

11.7

J6I47

Pot 11 ionC79111012131611202121313153676«14991011021041535526613• 1

Suulo CSXSLKSASI514ASBSI5UBSCSI5UCCSSI514BCSSI5I4ECSSI514DCSMIDCHKCSXI5INTCSCIIIACSCRIBCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSCRIACSCRIBCSX65INTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

-0 63661 2120600119

14402190311428

61 127 631031431130931621930131460 526 6421

-1.50-4.43-3.40-4 It-0.722-2.19

060 0120600120

150030003004220

30 03003003003003003003003000

30 0422

- .00- .00- .00- .00- .00- .00

10299.61100A.i93.796 5104101

91 910)ins104103105

96 4103105

II 110115044334041172 2219

DUMP OF METALS BATCH FILE BQF7051F METALS THU. OCt 12. 1818. 11:42 AM PAGE 7

Initial and Continuing Calibration verification and Calib. Blank Data

EUaunt : Until: uf/1

Position SamU Calculaltd6 SXBLK -0.261791110121316112021233631S367691499101102104

153552661391

SASI514ASBSI514BSCSIS14CCSSIS14BCSSIS14ECSSI5UDCSMIDCHKCSXISINTCSCRIACSCIIBCSLABCONCSMIDCHKCSLABCONCSMIOCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

60.9119600120

14302(20306476

63.429.630S307303301307211299304

60.329 64742 570 5900 5900 02510.3130 177

Enpoctod0

60 0120600119

15003000300461

60.00

300300300300300300300300

60.00

461- .00- .00- .00- 00- .00- .00

X Rtc102

99 4100101

95 597 2102102106102102101100102

96 199 6101100101

-257-59 0-59 0-2 SI-31.3-17.7

Pot H ion Sampli Calculattd6 SXBlK 3 647911101213ieII2021233631S367(91499101102104153552661391

SASI514ASBS1514BSCSIS14C

CSSISI4BCSSI514ECSS 151 40CSMIDCHKCSXISINTCSCRIACSC* IBCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSCRIACSC II IBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

197399200031746SO93601010

16400022997 51030915

1000914

1010925913

100020175 1

114000

26 4-7 49-7 99

0.099423 9

-5.46

E»p<cte<i0

20040020003995000100001000

1630002000

100010001000100010001000100010002000

163000- 00- 00- 00.00

- 00- 00

X Roc91.499.1loo»to92 993.6101100114103

91 5100

91.4101

92 598 3100100

100-2640749799

-9.94-2390546

DUMP OF METALS BATCH FILE BOF70S1F.METALS THU. OC1 12. tilt, 11:42 AM PAQE I

Inlllll ind Continuing C a l i b r a t i o n Vlilftclllon ind Olib. Blink Dili

E Unit I: (HO) Unlll: U9/1 Eltm.nl: Unlll: ug/1

67911101213161120212336315367191499101102104153552661391

SXBLKSASI514ASBSI514BSCSIS14CCSSI514BCSSI514CCSSI514DCSMIDCHKCSXI5INTCSCRIACSCRIBCSLABCONCSMIDCHKCSLABCONCSMIOCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSCRIAcscmaCSXISINTCBBLKCBBLKittSCBBLKCBBLK

4.24201031102000040504130010000010300505000219010101000010400101001020010300155010000102002010993

50400013.114 0IS,1.70.1.24

020004000200003910500001000001000047400020000

100001000010000100001000010000100001000020000

474000- .00- .00- .00- .00- .00- .00

10199.5100102

96.6100103107107100104101102103

95 5100102101101

-1310-1400-1610-2040-170-124

Polltlon Simplo Cilculilid6 SXBLK -O.Ollt7111101213161120212136315367»1491101102104IS3552(613• 1

SASI5I4ASBSI514BSCSIS14CCSSIS14BCSSIS14ECSSIS14DCSMIDCHKCSXISINTCSCRIACSCR1BCSLABCONCSMIDCHKCSLABCONCSMIOCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKC8BLKCBBLKCBBLKCBBLKCBBLK

60 SIK600121

142021703014S663 930 530731230130731029030430960 729. S4S9

-0.134-0.312-0.134

-0 0199O.SI10.104

EnpocUd0

60 0120600119150030003004450

30 03003003003003003003003000

30.044S

-1.00-1. 00-1.00-1.00-1.00-1.00

X Me101

99. S11 00'1019'4.l95. «103103102102104103102103

16 6101103

91 410]

13 431.213 41.99

-51 1-10.4

DUMP OF MCTALS BATCH FILE BQF7051F METALS IHU. OCT 12, 1919. 11:42 AM PAGE 9

••• InltUl and Continuing Calibration Verification and Callb. Blank Oall •••

Elimnt: MO Until: ug/1 EUmnl : (NA) Until: tig/l

Poll lion Samp!* CalculaUd6 SXBLK -0.2547 .911101213161120\\31315317611419101102104IS3552161391

SASI514ASBSI514ISCSI514CCSSI514BCSSI5I4CCSSI514DCSMIDCHKCSXISINTCSCRIACSCRIBCSMIOCHKCSLABCONCSMIDCHK3SB3&CSHIDCHKCSHIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

41 .101on5001011 902420I*"5:2

i

''

42!f-11

-O.I

31E.3.45151504941334646.5033442529

0.241-0 254

42

EnptcUd0

50 0100500101

12502500250000

250250250250250250250250000

-1.00-1.00-1.00:!:88-1.00

% R«c99 6101100101

95.396 7102

101100

99.9999.93.91.91.3

144-125•2 •III-142

Poilllon S««pl« Calculated6 SXBlK 72 4911101213ItIt20212338315367«914991011021041!35521C13II

SASI514ASBSI514BSCSI5UCCSSI514BCSSI514ECSSI514DCSMIOCHKCSXISINTCSCRIACSCRIBCSLABCONCSHIDCHKCSLABCONCSHIDCHKCSHIDCHKCSLABCONCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLXCBBLKCBBLK

1010019100100000201002420004910005100014 7

10(005050S02005140050800506005120047100502005100010200S020

-0.115101

52 217 457 217.417.4

Enptcted0

10000200001000001910025000050000050000

010000

0500005000050000500005000050000500005000010000

00

- .00- .00- .00- 00- .00- .00

X Ric101

9,9.1,00llOl91.999.7102ioe100103101101102

95 6100102102

-10100-5220-6740-5720-6740-6740

DUMP OF METALS CATCH FILE BOF7051F METALS THU, OCT 12, 1119. 11:42 AM

I n i t i i l ind Continuing Calibration V e r i f i c a t i o n ind Cillb Blank Data

Until: ug/1 Elem.nl PB Unlit: ug/1

Poiition6791110121316II2021233631S367691499101102104153552661391

S>«pli CalculatedSXBLK -1.51SASIS14ASBSIS14BSCSI514CCSSISI4BCSSISI4ECSSI514DCSMIOCHKCSXISINTCSCRIACSCRIBCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIOCHKCSLABCONCSMIDCHKCSMIOCHKCSCRIACSCRIBCSXISINT


61 S120600120

1410213031163.431.1301313307309310290304310

60.121 9151

-0 645-1.14-2.33-1 100 0125-2.05

Exptclod0

60 01206001201500300030013960 0

0300300300300300300300300

60.00

119-1.00-1.00-1.00-1.00-1 00-1.00

X Roc

102100100100

94 194 4104101106

103104102103103

96 110110310010164.5114233110

-1 25205

Position SampU Calculated6 SXBLK 3 73791110121316II2021233631S367691499101102104IS3552C61391

SASIS14ASBSIS14BSCSI514CCSSIS14BCSSIS14ECSSISI4DCSMIOCHKCSXISINTCSCRIACSCRIBCSLABCONCSMIDCHKCSLABCONCSMIOCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

109116100019023404730502ISO101

49 451952051151951547949651094 449 9162

-3.54-11 S-3 20-3 50-2 112.44

Exptctod0

1002001000116250050005009360

50 0SOO500SOOSOOSOO5005005000

50 0936

-1 00-1.00-1 00-1. 00-1 00-1.00

X R«c

109

12.9 1too,10293.694.6100

90.1

91 1104104102104103

95 199 2102

99 792 13541150320350211-244

•v]en

DUMP Of METALS BATCH FILE BOF7051F METALS THU. OCT 12. 1819, 11:42 AM

Initial and Continuing Calibration Vtriflcallon and Calib. Blank Data

Ela Unit I: uj/1 EUnunt SE Unili: uj/l

Pout ion Sanpla Calculated6 SXBlK 10 . 17I11101213112021233131S31714It1011021041535526613II

SASIS14ASBSIS14BSCSIS14CCSSISUBCSSI5I4ECSSI514DCSMIDCHKCSXISINTCSCRIACSCRIBCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSIABCONCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

IJ 9100022724004170SOO103490499504502417431463415

90.121 31405 03

-13.2-20 7-9 12-11 1-5.20

E>piclld0

10020010001152500SOOOSOO0

1000

500SOOSOOSOO500SOOSOOSOO10000

.00

.00

.00

.00

.00

.00

% Roc92 917.3100117ts.t

99 3100103

II. 0It 1101100

17.17.9297.to.

-50313202070912

1110520

17t1110121316112021233631S367It14It1011021041535526613II

SXBlKSASI514ASBSI514BSCSI514CCSSISUBCSSISUECSSI514DCSMIDCHKCSXISINTCSCRIACSCRIBCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINT

CBBLKCBBLK 'CBBLKCBBLKCBBLKCBBLK

0.6491114132000

409494010100III90 3201

75.21020104019510201020929140915114

51 5111

-5.11-2.36-2 97-4 57-60 0

02004002000413SOOO100001000

00

100100010001000100010001000100010000

1000

-1 00- 00- .00- .00- .00- .00

13 1103 1....

Jt b01.1101II. I

75 2102104

99 5102102

92 994 099 5

51.5

51123629712104576000

ON

DUMP OF METALS BATCH FILE BOF70S1F METALS THU. OCI 12. llll. 11:42 AM PAGE 12

Initial >nd Continuing OUbr»tlon Vtrlflotlon ind Cilib Blank Dili

EUmnl: SN Unlit: uj/1 EUimnl : S* Unlli: ug/1

Pol It Ion SuwU ClUul»l«d6 SXBLK 3.17711110121311112021233631S367•«14It101102104IS3SS2e«13it

SASISI4ASBSISUBSCSISUCCSSISI4BCSSISI4ECSSISUDCSM10CHKCSXISINTCSMIACSCIIBCSLABCONCSMIOCHKCSUBCONCSMIDCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSC*IACSCKIBCSXISINTCBBLKCBBLKCB8LKCBBLKCBBLKCBBLK

1*13112000

ISOO

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X Ktc

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II. 113.1IS.OII. 1

17.2II I17.411.3• 1.411. S14.117.1

-S2I-1121010121-sso11.3

17I1110121311112021233131S317II14•1101102104IS351113II

SXBLKSASIS14ASBSISUBSCSISUCCSSISUBCSSISUECSSISUDCSMIDCHKCSXISINTCSCP.IACSC* IBCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSCKIACSC* IBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

1 1710111710001912420SOIOS03

42.7•7.142.7414S034174<1413460417411

11.231.234.1-4.67-11.1-1S.1-15.1:llo!

010020010001(72SOOSOOO500000

500500500500500500500500000

- .00- .00- .00- .00- .00- .00

101• 1.6tooU•6.1101101

II. 1101• 7.• 1.it11.•7.••.

4671110151015101110403

DUMP OF METALS BATCH FILE BQF70S1F.METALS THU. OCT 12. 1919. 11:42 AM PAGE 13

••* Inllul »nd Continuing C«libf»tlon Verif ication and CUlb. BUnh Data •*•

Element: TI Until: m/1 ' tlt»«»l{_v) Unlli: iig/1

Pol 11 ion Simple Calculated6 SXBlK -1 5779111012131«112021233631S367691499101102104ISi!669.

SASIS14ASBSIS14BSCSIS14CCSSIS14BCSSIS14ECSSISI4DCSMIDCHKCSXISINTCSCRIACSCRIBCSLABCONCSMIOCHKCSLABCONCSMIDCHKCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSC* I ACSC* IBCSXISINTCBBLKceeiKCBBLKCBBLK .8KK

10220010002012410419050025.0107

41. S514507516496SOI469493500102

41. S25.4-l.ll:!:!!3:8

Elpected0

10020010002002SOOSOOO500000

SOOsoo$00soosoosoosoosoo000

-1.00:!:g8:i:88-1.00

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10196.497.199.9

103101103

99 3100

93.191 6100

16111317214717S201

Poll lion Samplt Calculated6 SXBtK -0 497791110121316112021233<31S3(7611499101102104IS355268Si

SASIS14ASBS1514BSCSIS14CCSSIS14BCSSIS14ECSSIS14DCSMIOCHKCSXISINTCSCRIACSCP.IBCSLABCONCSMIOCHKCSLABCONCSMIDCHKCSMIOCHKCSLABCONCSMIDCHKCSMIDCHKCSCRIACSC* IBCSXISINT


62 1lit600121

1420211030S4S46S.230.230331030230930121630230662 230 14SS

0.0601-0 6790.0601-0 6790.2421.17

Expected0

60 0120600111

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0444

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X Roc103

91.6 I1100 'juizit 195 9102102109101103101103103

95 5101102104

102-6.0167 9-6 0167 9-24 2-117

DUMP OF METALS BATCH FILE BQF70S1F.METALS THU. OCT 12. 1911 11:43 AM PAQE 14

••• Initial ind Continuing Calibration Vtrlllcltlon >nd C.Hb Blink Dill •••

Elimnl:/ZNJ Unltl: ug/1

17-11110121311112021233131i?ii14• I101102104IS35II13II

1 !8ti* cSASIS14ASBSIS14BSCSIS14CCSSIS14BCSSISI4ECSSIS140CSMIOCHKCSXISINTC SCI I ACSC* IBCSLABCONCSMIOCHKCSLABCONCSMIDCHKCSMIOCHKCSLABCONCSMIOCHKCSMIOCHKCSCHUCSC* IBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBSLK

.,«„,.,..101III1000202Hi.Ill114

41. tSi,4*5503SOS414417S04II. S41.11(2

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MTALI 00 DATA: DUPLICATI/SEftlAI. DII/BUNK/MATP.IX SPIKE INFORMATION THU, OCT II, lilt, 1:23 AM PAOI

Bitch Fill : BQF7091F Job Id : 070091 Sequence Pot I : 41 Until : UJ/1 Spiking Lot Id : IFBPW

Blink/HitrIn Spike Information

ElemnlAOALBABECA

CDCOCDCUFEMOMNNANISBVZN

Pol4141414141414141

414141414141414141

Spiked41.11140209041.91020049.1909111291109010900S0«21000909471911912

Unipiked.11112.10.012193.1.421.tit0.9119.7213.3.21119.200.4244.12

Added90.02000200090.01000090.090020029010001000090020000900900900900

X Be.11.4

16.4103II. t101

10.110111.9100104

10910110910119. 1103101

METALI QC DATA! DUPLICATE/«ERIAL DIL/ILANK/HATRIX SPIKE INFORMATION THU, OCT It, ttlt, «:23 AM PAGE f

Bitch Flit : BOF7051F Job Id : 07051B Slqutnct Pot I : 72 Unltl : ug/1 Spiking Lot Id : KI514D

Blink/Matrix Spikt Information

EUnunt Poi Splktd Uniplkod Addtd % RccovtryB 72 203 0 200 102

VOCM

METALS OC DATA: DUPLICATE/SERIAL DIL/BLANK/MATRIX SPIKE INFORMATION THU, OCT 19. 1919 9:23 AM PAGE

Bllctl Flit : BQF7051F Job Id : CA1371 Sequtnce Pol I : 44 Unltl : gg/1 Spiking Lot III : IFBPW

Blink/Matrl» Spikt Information

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0

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X Rtcovtry92.196.099.691.792.015.193.695.097.695.510196.5

104

95. 191.791.794.3104

MITAL6 QC DATA: UUPLICATE/StHIAL OIL/BLANK/MATRIX SPIKE INFORMATION THU, OCT It, 1919, 1:23 AH

Bitch Flit : BQF7051F Job Id : CA1371 Stqutnci Pol I : 45 Unlli : ug/1

EltmtntAOALBABECACDCOCDCUFEMOMM

NANISBVZNB

VOtn

uupi

Pot454545454545454545454545454545454576

S.mplt1.43-1.5557.3.035973100.679-2.15-.5512.0041.6416002.653260-.7771.611.5312.636.5

lUplicite1.1619.756.6.063473400.242-.6051.091.7115.6420002.193300-1.99-11.5.9776.7435.7

KPD19.1571234.1602.2433155.3677.409556113.649-112.160606.90615.633469.1955.9569316.664251.21951-67.6762-236.12944.116536.17622.21606

PAGE

Bitch

ElomentASALBABECACDCOC«CUFEMQ

HN

NA

NI

SBV

ZN

B

voON

Flit : BOF7051F Job Id

Strlil Dilution Info

Pol474747474747474747474747474747474771

SampU1.43-l.SS57.3.035173100.179-2.15-.5512.0041.6416002.651260-.7771.611.5312.636.5

Sirlal5.91-.29543.7.31575600-2.621.41-22.22.9510743200-.0993410

-10.7-14.06.719.99.731

Dll % Dill313.217-10.967723.7347972.4243.41997391.066-165.511-3929.0447.5000157.2123.14615103.7366.74147-1277.09969.565343.13720.714397.9973

TITLE

From Page No. _

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ifti6o

oCj

c£

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To Page h

Witnessed S Understood by me. Date invented by g?

Recorded by

Date

DUMP OF METALS BATCH FILE BOP9100A.METALS WED. OCT II. 1*1*. 9:53

EUmnt

AO

ALASBBABECACOCOC«CUFEMQMNMONA

, NtPB

VO SB00 se

SNs*TIVZH

C«rr. Co«ff.

0.999901.00000.999190.1999*0.999910.999990.999910.999960.9*1990.999910.991*70.999970.999911.00000.999991 . 00000.««(«70.999730.99*140.*99S*0.999941.00001.0000

O.l*«*70.*9«*7

Slop*

10451004

999.1•13 4*75.9995.2973.3992.09*3.0999.0993.9*S*.21001

19*.*177.11001953.7993.*10151011

971.51019

*II.O•77 6149.9

n Dili

Intirctpt

0.3**-7.03-9.40-5.1*-5.59-0.441-35.4-0.4111.4*-3.31-1.1229.7-34.1-1.12-2.79-1*9-1.14-12.3-17.4-27.9-0.5993.11-1.301.3t-3.18

Unlti

ug/1"g/1

"9/1»9/l«9/l«9/lug/1Ul/1

u*/lU</1

ug/l«g/l«g/lu*/lUS/1»•/!y*/i"I/I•1/1"•/Iu*/lu»/l«g/i«9/lug/l

Dtttctlon

Blink M««n

-1.00-1.00-1.00-1.00-1.00-1.00-1. 00-1. 00-1.00-1.00

-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00'-1.00

Limit Blank

Sld. OKI.

-1.00-1.00-1.00-1.00-1.00-1.001.00-1.00-1.00

-1.00

-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00

-1.00-1.00

-1.00-1.00

Dltt

MDL

10.0100100

20.020.01.002002.0020.010.010.01501005 0020.050020.075.090.0100

50.020.050.020.020.0

MM* OF MITALI IATOH ULI IQMkOOA.MITAtl MID, 0«T kl, 111*, lilt AM MOI a

••• Inltltl >nd Continuing CilibriUon VtriflotUn and Cillb. Blink Dili •••

Eltmnt: *a Unlti: ug/1 Elinenl: AL Units: us/1

s7 •11011112IS171120223747SISISI•114314tss

SXBLKSASI514ASASIS14ASBSIS14BSCSI514CCSSIS14BCSSIS14ECSSIS14DCSMIDCHKCSCIIACSCRIBCSXISINTCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSCIIACSCIIBCSXISINTCBBLKC8SLKCBBLKCBBLK

-0.31155 J'ioS42.5411USII. 120.11.0171$

SI.OII. 1II. 1II. 111. 11.237IS

O.ISI-0.311-l.ll1.91

020.020.040.0200

41.4500

1000SOO.00

III100100100100

20.00III

-1.00-1.00-1.00-1.00

12.1104104II. 1102

II. 119. S91.1104

II. SSI.OII. 191.1Si:!11.4

-IS.I31.1111

-111

S1710

11121517112022374751515911143141SS

SXBLKSASI514ASASIS14ASBSIS14BSCSI514CCSSI514BCSSIS14ECSSI514DCSMIDCHKCSCIIACSCRIBCSX8S1NTCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLK

-7.43504SOS9995000100012400250002530413224

4310002110254025102540514250

43300040.115.1

-13.1-13.1

0500500

10005000999

12SOO2500025005000

43700025002500250025005000

437000-1.00-1.00-1.00-1.00

101101

99.9[ootoo

99.2100101

11.799.1IDS102100102103

99.1-4080-151013101310

VOV£>

DUMP OF METALS BATCH FILE BQP6100A.METALS WED. OCT II. lilt, 1:53 AM PAGE 3

Inltiil and Continuing C«libr«lIon Verification ind Ctllb. Blind Dili

Cltnnl: AS Unlit: «9/l EU Unlit: 119/1

p.,1,,.,

•7110

i!151711202237475651566114364655

SXBlKSASI514ASASI514ASBSI5I4ISCSI514CCSSI514ICSSI514ECSSI514DCSMIDCHKCSCIIIACSXI5INTCSMIDCHKCSMIDCHKCSMIDCHKCSCIIIACSC1IBCSXI5INTCBBLKCBBLKCBBLKCBBLK

-7.6016.564.6226665116

'ii?136•363443412434410106

45.3-3573.31

-0.6164.4311.1

0100100200

1000221250050005000

50.00

5005005005000

50.00

-1.00-1.00-1.00-1.00

11.514.6115

•6.511.4•5.0•6.5•0.251.211.7•6.416.4•6.1•0.6

-33161.6-443

-1110

67110

1112IS171120223747565156• 114364655

SXBLKSASIS14ASASI514ASBSIS14BSCSI514CCSSI514BCSSIS14ECSSIS14DCSMIDCHKCSCIIIAC SCH IBCSXI5INTCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISIHTCBBLKCBBLKCBBLKCBBLK

-2.2099 9100203•••20124504130490101

45.923 44764(2477411

•7.143.011.3

10.7-2.76-3.SS-4.02

0100100200

100020325005000SOO000

SOOSOOSOOSOO000

-1.00-1.00-1.00-1.00

11.9100

ioi•1.2• 7.1•6.5• 7.«

•5.2•1.5•5.3• 7.7

-1070276355402

oo

DUMP Of MITALI IATCH fill IQM100A.MTAhl WID, OOT II, kill, 1:13 AM •AOE 4

Inltlil ind Continuing Cillbratlan Vtrlficillon ind Ctlib. Blink Dili •••

El•mini: BA Eltm.nl: BE Unlll: uj/1

lllonS1711011112IS171120223747SISIs:1436a

1 SMBlO C>SXBLKSASIS14ASASIS14ASBSIS14BSCSIS14CCSSIS14BCSSIS14ECSSIS140CSMIOCHKCSCRIACSCRIBCSXISINTCSLABCONCSMIOCHKCSMIOCHKCSMIOCHKC SC« I ACSCKIBCSXISINTCBBLKCBBLKCBBLKCBBLK

1.J1.IU

IS?2014072000407411017001000200•1.344010001020•101010199

•S.I4311 19-6.01-S.I*-5.99

E»p«ct.d0

2002004002000407

10000100020043110001000100010002000

431-1.00-1.00-1.00-1.00

X R>c100100102•9.9100• 1.217.0100too100100102

tl.O101••.S•I.I-111101III

Petition S»mpU CllcuUUd5 SXBlK -0.441e7i1011112IS17112022374756SISI11143141SS

SASIS14ASASIS14ASBSI514BSCSI514CCSSI514BCSSI514ECSSI5140CSMIDCHKCSCRIACSCRIBCSXISINTCSLABCONCSMIOCHKCSMIOCHKCSMIOCHKCSCRIACSC* IBCSXISINTCBBLKCBBLKCBBLKCBBLK

20.120.040.420040 949116711.720.21.73417•6.1100

97.2•9.319.91 46411

1.13-0.441-0.410-0.422

Exptctid0

20.020.040.020040.4SOO10001000

10.04231001001001000

10.0423

-1.00-1.00-1.00-1.00

X ««c100100

foi•!01• 1.216.7•9.7• 7.3• 1.616.1100• 7.211.3• 4.6• 7.1-11344.149.042.2

DUMP OF METALS BATCH FILE BOP9100A.METALS WED. OCT II. 1919. 9:53 AM

InltUl and Continuing Calibration Vtriliollon and Calib. Blink Dili

Elimnl: CA Uniti: ug/1 Elamant: CD Unltt: u«/l

Position SimpU Calculated5 SXBLK -13.09T110911it171120223747SISI5911143149SS

SASIS14ASASIS14ASBSI514ISCSI514CCSSI514BCSSIS14ECSSIS140CSMIDCHKCSCIIAC SC« IBCSXISINTCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKC SCB I AC SC« IBCSXISINTCBBLKCBBLKCBBLKCBBLK

20402030403020000401049200970002030

4190001930101009170100002010•55

40900072.7

-51.4-77.9-SI. 4

E»p«cttd0

20002000400020000403050000100000100002000

491000100001000010000100002000

0411000-1.00-1.00-1.00-1.00

X Rtc102101101

91.1101

91.597.0101101•0.399.3101

91.7100100

11.7-7270514077905140

Potition Simpla Calculated5 SXBLK -0.919971091112IS17112022374756SIS911143141SS

SASIS14ASASIS14ASBSIS148SCSI 5UCCSSI514BCSSIS14ECSSIS14DCSMIDCHKCSC III ACSCRIBCSXISINTCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKC SCSI AC SC«. IBCSXISINTCBBLKCBBLKCBBLKCBBLK

20.320.040.9200

39.945090194.517.29.4172317 914 793 194 117 41.43720

0.591-1.71-1.31-0.131

Enpactad0

20.020.040.0200

40.150010001000

10.01151001001001000

10.0115

-1.00-1.00-1.00-1.00

X Rtc101100 .iS90.090.194. S94.111.717.114.713.114.1 .14.311.3-58 1176131

13.1

oIVJ

BUMP Of MITALI IATCH Fill IQPUOOA.METALS UID, DOT II, llll, III! AH

••• Inltlil ind Continuing Ctllbrttlon Verification »nd Ollb. Blink Dtti •••

Cltmnt : CO Units: ug/1 E Union!: CD Unit I: uj/1

Petition6711091112IS171120223747SISISI61143641SS

Sunplo C.lcultUdSXBlK -0.241SASIS14ASASIS14ASBSIS14BSCSIS14CCSSIS14BCSSIS14ECSSIS14DCSMIDCHKCSCRIACSC* IBCSXISINTCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLK

!,!12.1400

79.1914

1900191

43.711.0394195209199203

39.122.7394

3.77-1.243.35

-1.42

Eipoctod0

40.040.010.0400

12.110002000200

40.00

411200200200200

40.00

411-1.00-1.00-1.00-1.00

X Doc96.491.6103

99.19S.I91.49S.291.9109

94.197.6104

91. S101

99.494.1-377124

-33S142

PetitionS1711011112IS171120223747SISISI1114314135

Samplo ClSXBLKSASIS14ASASIS14ASBSI5HBSCSI514CCSSIS14BCSSI514ECSSIS14DCSMIDCHKCSCRIACSCRIBCSXISINTCSIABCONCSMIDCHKCSMIDCHKCSMIDCHKCSCRIACSCRIB .CSXISINTCBBLKCBBLKCBBLKCBBLK

llcuUtod-3.1080.759. 112S599120

14702110303

10.124. 53«7302310303301

S9.126.3391

o.eis-2.00-2.17-0.177

E«poctod0

10.010. 0120eoo12S

1SOO30003000

30.04223003003003000

30.0422

-1.00-1.00-1.00-1.00

X Roc101

11.4104ff16.1II. 016. 0101

11.614.0101103101103

17.713.7

-II. 5200217

17.7

DUMP Of METALS BATCH FILE BQPI100A.METALS WED. OCT II. llll, «:53 AM PAGE 7

••• Inlll.l ind Continuing Cillbr.tlon Verification ind Olib. BUnk Dill •••

Elonnnt : CU Unlll: ug/1 EUmnt: FE Unlll: ug/1

7 •11091112IS171120223747SISIS911143141SS

SXBLKSASISUASASISUASBSISUBSCSISUCCSSIS14BCSSIS14ECSS I 5 140CSMIDCHKCSCRIACSCRIBCSXISINTCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLK

-2.1711 3

Ml1221410215090259. 721.14543 0521430057.227.74432.42-2.31-5.50-2.10

I.MCI..-10.010. 01201001221500300030010.0

041130030030030010.0

0411

-1.00-1.00-1.00-1.00

10299.1102

91.191.1II. 191.2101

99.191.197.5102

91.0100

95.394.7-242231550210

17i10g1112is17IS223747SISIs>11143141SS

SXBLKSASISUASASISUASBSIS14BSCSIS14CCSSIS14BCSSIS14ECSSIS14DCSMIDCHKCSCRIACSCRIBCSXISINTCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSCRIACSC* IBCSXISINTCBBLKCBBLKCBBLKCBBLK

3. S32071143142000417

414014101010210102

1510001040>9I172991172

73.91SOOOO5.0711.0

-15.09.70

02002004002000394SOOO100001000ZOO0

1130001000100010001000200

113000-1.00-1.00-1.00-1.00

10497.291.4

Hlot91.194.9101105

92.3104

99.197.299.1II. 091.9-507-19001500-970

DUMP Or MCTALI IATCM Fill IQM100A.METALS WIO, OCT 11, III*, Ilia AM PAM I

Inltlil tnd Continuing Cillbrtlion Vtrlflotion and Ctllb. Blink Dili •••

E1MMHI : MO Uoltl: ug/1 Eltmnl: MM Unit I: U(/1

131001210J0103400

P..U1.,1711011112IS17112022374758SISI1114314155

SXB[KSASIS14ASASIS14ASBSIS14BSCSI514CCSSIS14BCSSIJ14ECSSIS14DCSHIDCHKCSCRIACSCRIBCSXISINTCSLABCONCSMIOCHKCSMIOCHKCSMIOCHKCSCftlAC SC« IBCSXISINTCBBLKCBBLKCBBLKCBBLK

-1.1410.210.2121100122

1470211030410.421.142230030130130B10.329 54233.S4

-1.01-1.12-1.31

010.010.0120100121

1SOO30003000

30.044S3003003003000

30.0445

-1.00-1.00-1.00-1.00

100100 ,SOI0001.111.2101

91.114.1100103100102

11. 485.0-354101162131

Oin

DUMP Of METALS BATCH FILE BQP9100A.METALS WED. OCT II. 1911, 9:53 AM PAGE I

'•• Initial tan Continuing C.librlUon Verification tut Calib. Blink Data •••

Eleeunt: MO Unlti; ug/1 . Element: NA Until: ug/1

Petition1711091112IS1711202237475951911411SS

Sample CalSXBLKSASIS14ASASIS14ASBSIS14BSCSI514CCSSIS14BCSSIS14ECSSIS140CSMIOCHKCSCRIACSCRIBCSXISINTCSLABCONCSMIDCHKCSMIOCHKCSMIOCHKCSCRIACSCRIBCSXISINTCBBLKSULK •CBBLK

culated0.11449.4SO.IBl.lsoo1021230m21.2B.97247255241253

47.124.93.791.03-2.790.1190.349

Expected0

SO.OSO.O100SOO91.1125025002SO00

250250250woi

-1.00-1.00-1.00-1.00

X Rec91.1102

91.1100103

91.299.599.2

19.0102

91.4101

-10327911.9-34.9

PotltioiSe711091112IS171120223747SISIS991143949SS

n Sample CSXBLKSASIS14ASASIS14ASBSI514BSCSIS14CCSSI5U8CSSIS14ECSSI5140CSHIDCHKCSCRIACSCRIBCSXI5IHTCSLABCONCSMIOCHKCSMIDCHKCSMIOCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLK

alculated-19910000100002010010000020100241000SOOOOO49900100004900-21449000S070049100S0200»9404900-234S19-141-191-171

Expected0

10000100002000010000020100250000SOOOOOSOOOO10000

00

SOOOOSOOOOSOOOOSOOOO10000

00

-1.00-1.00-1.00-1.00

t Rec100100

1010010099.4100

99.9100

91.0101

91.2100

99.4

-S1900141001910017100

PUMP OF MCTALI IATOH Mil 19*1100*.HITALt WID, OCT II, till, 1:19 AM PAQI 10

*•• Inlttil ind Continuing Cillbntlon Vtrlflcition and Cillb. Blink D«l« ••*

Unlll: at/I ElOMnt : PB Unlit: ug/1

Poll! Ion Simple CilcylilodS SXBlK -2.517110I1112IS171120if47SI51SI111436;;

SASIS14ASASI514ASBSISUBSCSIS14CCSSISUBCSSI514ECSSISUDCSMIDCHKCSCRIACSCRIBCSXISINTCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLK

SI I'«!Sll1231410214030410.029.376521130130430710.0'!.,-1:81-III

060.060 01206001221500300030060.0•3$30030030030060.00

13*1.00.00

..001.00

-1-1

X R<c102

99 8102

II.I100

17.214.1100

11.2II S103101102100

11.5-1SI16SIII

Petition56710g11ifit

2022374756SISIII14364655

Simpl.SXBLKSXB...SASI514ASASIS14ASBSISUBSCSI514CCSSI514BCSSI514ECSSIS14DCSMIDCHKCSCRIACSCRIBCSXISINTCSLABCONCSMIDCHKCSMIDCHKCSMIOCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLK

Cllculltod-1.53 'SI.S216•1721124504760505log

52.3798477517SIS521107

54.3104

1.51-3.67-3.01-1.10

01001002001000218250050005000

50.0•365005005005000

50.0936

-1.00-1.00-1.00-1.00

16.•• I. 5iOI•'•.767. •15.1101in

IS.l15.4103103106log15. g

-151367301110

DUMP Or METALS BATCH FILE BQP9100A.METALS WED. OCT II. 1911, 9:53 AM

Initial and Continuing Cillbnllon Verification and Callb. Blank Data

Elimnt: SB Unlti: ug/1 Eltin.nl : SE Unite ug/1

517110911121517112022374759SI59ei14394955

SXBlKSASI514ASASIS14ASBSI514BSCSIS14CCSSIS14BCSSI514ECSSI514DCSMIDCHKC SCd I ACSCRIBCSXISINTCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLK

1.5192.093 e2091000197

2410S01049310.120.112.9443501415495

75.351.0111

-5.22-27.9-14.3-15.3

010010020010002062500500050010000

50050050050010000

-1.00-1.00:i:88

92.093.1103100

95.999.2100

91.910.1

11.9too97.191.975.3

522279014301530

Position S.mpl. Calculated5 SXBLK -24.9>711091112IS17112022374756SI5991143>4tSS

SASI514ASASI514ASBSI514BSCSI514CCSSIS14BCSSI514ECSS I 5 140CSMIDCHKCSCRIACSCRIBCSXI5INTCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLK

1102274241990412

S0109910995155107

-90.99349799101020240

57.021.75.29-14.7-4.51-7. IS

Expoctod0

20020040020004245000100001000

01000

10001000100010000

1000

-1.00-1.00-1. 00-1.00

X Roc90.2114SOB•'>,00

99.199.5107

93.497.991.0102

57.0

-529147045 1715

oCO

DUMP Of MITAkl MTCH Fill IQMIOOA.MITAU WU, OOT Hi ill*, lilt AM MOI 12

••• Initial ind Continuing Cillbritlon Virlflcitlon ind Cillb. Blink Diti "•

EltMot: SN Unltl: ug/1 EUmtnt : S* Unlit: uj/1

S»M>USXBLKSASI5UASASI5HASISI914ISCSISUC

X «<c103101102

11.9• 7.497 e14 6

102

••.4101

-IW

PoiUlonS•7

10I

1112IS17II20229747sesist11143141SS

SMUtllsxaUSASIS14ASASIS14ASBSIS14BSCSSS14CCSSIS14BCSSIS14CCSSIS14DCSMIDCHKCSCKIACSCRIBCSXISINTCSLABCONCSMIDCHKCSMIDCHKCSMIOCHKCSCRIACSC*IBCSXISINTCBBLKCBBLKCBBLKCBBLK

Ctlcullltd-0.7SI

10288 I111

1000200

2SOOSOIOSOOII. ISO.23S.I471SOI417SOS102

Sl.S31. S4.41

-0.7SI1.20

O.S47

0100100200

1000111

2SOOSOOOSOO00

soSSOOSOO900000

.00

.001.001.00

X R«c102

II. I .II.I Iloo

-1-1

it.«IS.I101

11.4101

-44179.1-120

-94.7

OSO

DUMP OF METALS BATCH FILE BQPI100A.METALS WED. OCT tl. lilt. 1:53 AM

••• Inltlil and Continuing Calibration Varltlcatlon and Ctlib. Blink Data

Elowrit: TI Unite lig/1 EUwnt: V Unlit: 119/1

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.71O71.021i O . 1 4.1198. 267. 7.5O . SO.7242.S4B3.5147.994 1' . 0~*.2. 4928.5189.7106.5481

RSFA343O

-.0035.0182.0202. 3348.0896. oooo41 .95- . OOOS. O i 7'?.OOil.0143.07.75

. O098

.O4O6. .O14O. 1 1 7.4.0492.4543.OS 51.OO75.O472

DW

- OOiO. IO41. 1097,- OO30. >OO2. 10O1-.07.52-.0001- . OOO8- . OO34--OOO9-.01 50. OO4 5- . OOO2. OO02,O6~6.0003. OO~ 9.O1O7. 0027. OO07-.OO26. OOOO- . 0006. OOO2

RSFA3448

-.0015-02o4.O259.1127. 0003. OOOO.1369. OOO3- . OOO2.OO 13- . 0003-.0127

. 021 7

.02- 5

.0178- .0166. O i 7. 1i 146. 1382. >119. >727.

RSFA29O9

-.003 5.3258-.0021.1124..Oo4B

10.95- . OOO3- . OOO4.0571. O6267.8013.423.1373. 003011 .77.0296.0244-.O041.0119-.OO93.2877. 07O8.OO 19.1579

DW

. OOO5-.':i07,6.OO2O-.OO36- . OOO8. OOOO- . 0294- . OOO3- . \>O 14-.OO 16-.OO 14- . OO86

.Oi 76

.3523

. )284

. >367

. >214

. 4O43

.1O16

.OO69

.0481

RSFA3O95

- . OO4 54.546. O2OB.0871. O6OS.OOO1123.9- . OOO3-.OOO2.O157.01402.9523.126.0851.027.792.47. 0033.0349-.0152.0434.0057.6959.2556.OO46.0368

CBBL K

-.0023-.OOel.O108.0021- . OOO4-.OOO1-.O437- . OOO9.OO 19.OO12- . OO-.7- . 04 35

-.002 5. 0 171-.0164. 0283-.01 14-. IO77- . >OOS- . >054-. >OOS

R5F.S 7.2=9

.O4O9-.O27S.0469. OOO2. OOOO.13OO. OOO7- . OO7.8.OO73-.OO 14- . 07,78.0100.0105. OOO7. 1 7=57-.OO 16. 0 1 3O.0057.01 44- . C.O90-.OO45.0414- . OO33.07.51

CSMIDCHK

.O92O2 . 508.4521 ..495O1.O21.1OO 4i 0 . 1 5. i 07 1.2058.7157• . 2996.9926

- . OOO5. OO89-.O1O3. 0 1 7 1. 0083- . OO4 5- .OO04. OOO6-.OO 19

RSFA7.429

-,-.--.0571. OO63.0649.007.3. OOOO

.OOO1- . 0038-.OOO1.OO11-.OO7041 .07.0467. 007.474.46- .OO27.0197. :'173-.002 9-.005 5. O263.07.69-.0033. 0229

DU

-.OO07- . 0.072.02 14-.oo:,3. OO02.0001-.0186-.OO02.OOOS. OO72- . -X'07-.O113

117

ana

«

1314151617181920212223242*

*

1234567391O1112131415161 71819202 i222~"'2G25

ivsis Re DC

El ement

ng279B<1n2576Mo2020Na58=6'•112316Pb22O4Sfc2OsSS»196O9ni900Sr9999T17349V 2924Zn2139

E '. ement

Ao728iA i 3092As 1977B_2497Ba4934Ee3170Ca3777Cd2289C02286Cr2677Cu7249-e27i«MQ279SMn.25'6M02O2CN3?8<?oMl 1 3 1 6P&22043b2O63Sel96OSnl9OOSr9999~ 1 7749V_2924Zn2139

AM

RSFA347O

3OO.71-.M3.O45276,_33.O137-O229..0444-.1684-.0121.167.4. O4 1 4- . OO5O. 0523

RSCA17.75

- . OO20-.0170. 0207.07 11. 07O1. OOOO15.64. OOO1- . OO3O.OO46-.OO232 . 36811 .27.O169.OO234 . 089. 0036.Ol 84.OO39.01O5.OO1O.0231-.0009-.OO39.OOO1

sra?Bs

RSFA3448

. 1 237

.OO21. .OO 53.4974-.OOO5.01O9.Ol 60.O427-.0185- . OO70.0405. OOOO.O24O

RSCA17.76

- . OOO7-.OO2S-.OO99-O725.0149.OOOi13.72. OOO7.-.OOOI. OOO4. OOOO.15131 3 . 06. 0637. OOO25 . 1 09. OO3O.0075-.OO10- . OOO6- . OO67.0243- . 0002-.0004.0038

DW

.0289

. 0001- . 0.026.0199-.0015.0100-.OO 13.0426- . OO86- . OO64- . OO02- . 0027.-.OOO7.

R5CA1777

. OOO7- . 0093. OO98.OO28.OO 5 6. OOOO12.22- . OO07.. O03O.002 5-.OO31-.01725.756.0870.OO23.6218-.OOO5.02O1.OO45.Ol 48. 0089.OO45-.OO12-.0027- . 0008

TUB 10-1-

CBBLK

. OO46

. OOOO

.0019

.OO5O-.0016.0096. OO7.O. 023O-.O055-.002 6-.OOO?- .OO36-.OO10

RSCA1730

-.OOI 5-.OO85-.OO35.OO48.OO4 7.. OOOO11 .97.- . OOO6- . 0039-.0015-.OOI 7.26185.912.04 SO. OOO91 .084-.OOO5.O1O6.0110.0213.OO31. OO32-.OO17-.OO19- . OOO2

--8= 10:0<

CS!*IDCHk-

9 .892.7119.254548.66.7201.5464.4991.92561 .027..487.8.5014. 307.10.57.71

RSCA17.81

- . OO27-.0170-.O2OO.OO64.O044. OOOO12. OS- . OOO2-.0027-.OO38-.0071. 23026.O05.04 7 4-.OO121 .104-.OO 13. OO85-.OO 14.O211-.0079. OO26-.OOi?-.O038- . OOO8

~: it -"

DW

. 0 1 7 2-.0002.OO72.0547. OOO3. 0 1 0.7. O30O.017.9- . OOS9- . OOO6. OOO7- . OO i 2- . OOO2

DW

-.O027. OO4 5-.O17O-.0049- . OOO6. OOOO-.0257- . 0002- . ooos. ooos-.OOI 7-.O322.0052- . OOO 1.OOOO.OOOO-.0016.0137. 004 9- . OOf 5-.OiOO-.O051.OOOI-.O073-.OO12

E1ement CBBLK CSMIDCHK DW CSCRIA CSCR1B

1 AQ72912 Ai7O823 As 19 -74 B_24975 6*497,46 Be717O7 Ca37778 Ca2239

. OO 1 5-.O061.0175.0017- . 0004. OOOO- . O277- . OOO4

.09352.537.4989. 5O701 .044.102610.28. 1 04 1

-.0035.0081-.0240-.OO47- . OOO7. OOOO-.O409-.OO07

.0177

.5193

.1143

.1061

. 2097

. O2O92.O91.O201

. OO75

.2559

.0529

.0499

.104O

.O102.1 .Ol 4. 0099

-.OC 2O. OOOO-.0155- . OC.1 4 1.0001.0001-. :.'4o?-.OOC 7

118

wr, a :

tt

' 91011121314151617181920212227.2425

*

1234567S9101112131415161718192C>2122232425

L vsi 5 r*e

Element

Co228602677Cu324SFe2714

Mn2576M02O20N»5896Ni2316Pb2204Sb2068Sel960Snl900s,9999Ti3349VJ2924Zn2139

Element

Ag3281A13O82Asl937B_2497Ba4934Be313OCa7,737Cd2289C02286OI677Cu7Z4SFe2"14M02798Mn2576M02O2ONa5896NJ2316Pb2204Sb2068Sel960Snl9OOSr9999Ti3749V 2924Zn2139

C.B3LK

-.0030J3037- . QO03

. 0008

. OOO2

. OO32- . 005O-.OO1 4-O116. OO2O. 02O5. O064- . OO32. OOOO-.0015- . OO 1 4

CSXS51NT

.75O7431 .11 . 1 86. 3997,.4550. 424742O.O.74e,8.4079.4111.45O5150.6443.5.4376. OO67.04 4 8. 8O6O.7216.0763-Ol 27.1266.032O.0622.4281.8169

CSMiDCHK DW

.2096 -.0017

.3204 -OO2 4. .3061 -.X>1-1.O12 -.O4B71O.O7 -.OO71.3177 .OOOO.2614 .OO1249.94 .07,98.7,27.2 -.0026. 56O3 . 0299.5O82 -.OO851 . 07,2 - . OO57,1.O21 -.O209.4915 -.OO26.5114 .OOOO.7.O91 -.OO33.5196 -.OOO7

DW

.0095

.1200-.O503-.OO41- . OOO4. OOOO.0462- . OOO4-.OO1 4-.OO 3 6-.OOO 6.0182.1056- . OOO9. OO23.0199- . OOO4-.OO16-.0138.0123-.O143-.OO77.OOO4-.OO35.OOO2

' ->e 1O-.

CSCRIA

.O399

. 0644

.0598

.15292.O10. 067,9.05181O.O3.0641.1238.0921.2643.2108. O967.1O2O. 06O2. 1 067

CSCKIB

. 022O

. O3O6

.O299

.04 99

. 9980

.0321

.0237,5.O24.03 18. 0689.0677.0837.O995.04 68. O5O4. O284.O54O

O6 : . 5 -«

DW

- .OO37- . OO2O-.0003-.0311. OO4 5. OOO1.OO 14.0696-.0025.0103- . OO32. OOO8-.OO9-- . -107.B-.OOO1- .0021-.OO01

race 3

119

ETC

METALS SUBSIDIARY DATA - FLAME AA

120

On/

cf/eeo

I i (-\ OL Ia3

JK3(e<o

On/

fiXAMI/So

/39V

/30C.SfriOi tit:

/it?

DI.V

/So

i

"5*

m3

To Page Nt//

essed & Understood by m«. Oil* Invented by/}«-

Rtcordtd by

o... 1)21^"/d"';

Project No._Book No.. T,TLE

Page I

••• —uses & u-ie'siootf Cy m« Oate :^,vtntec ay , rûN

= ....... •.

To Page No _

Date 1

•cli i 1|22

DUMP OF METALS BATCH FILE BQP7049C.METALS FM. OCT 27. 19(9, 9:40 <

0«l.cllon Limit BUnk Dili

Std. D«v

AQ 0.99999 9(9.2 1.27 ug/1 -1.00 -1.00 10.0AL 1.0000 9(4.9 9.59 ug/1 -1.00 -1.00 100AS 0 99991 9(1.4 -1.95 ug/1 -1.00 -1.00 100I 0.99997 9(5.( -5.99 ug/1 -1.00 -1.00 20.0BA 1.0000 9(9.1 -1 89 ug/1 -1.00 -1.00 20.0BE 1.0000 (57.( 0.111 ug/1 -1.00 -1.00 1.00CA 0.99999 975.9 -79.0 ug/1 -1.00 -1.00 200CD 0.99999 944.4 0.329 ug/1 -1.00 -1.00 2.00CO 0.99999 959.2 -0.395 ug/1 -1.00 -1.00 20.0C» 0.99999 959.7 -0.4(9 ug/1 -1.00 -1.00 10.0CU 0.99999 975.3 0.475 ug/1 -1.00 -1.00 10.0Ft 0.99999 953.3 -7.07 ug/1 -1 00 -1.00 150

-1.00 500-1.00 100-1.00 « 001.00 20 0

-l.oo -onHI 1.0000 940.2 -0.392 ug/1 -1.00 -1 00 20.0PB 0.99999 9(2.( 4.77 ug/1 -1.00 -1.00 75.0SB O.((((l 9(7.7 0.5(3 ug/1 -1.00 -1.00 (0.0SE 0.((((7 ((7.5 1.07 ug/1 -1.00 -1.00 100SN 0.99999 9(0.0 5.27 ug/1 -1.00 -1.00 50.0TI 0.99994 972.9 -3.29 ug/1 -1.00 -1.00 50.0V 0.99999 9(5.2 0.9(9 ug/1 -1.00 -1.00 20.0ZN 0.((999 994.9 -1.00 ug/1 -1.00 -1.00 20.0

.At

0.999991.0000

0999>l0.(99971.00001.00000.99999O.»9llO.II9II0.999990.999990.999911.00001 . 00000.199990.999991.00001.00000.999990.999910.999(70.999910.999940.999(90.99999

(•9.2(94.9911.4991. 1991.1937. 997S.9944.4959. 2959. T975.3953.31007992.7(59.19(2.3997.0940.29(2.9917.79(7.59(0.0(72.99(5.2994.9

1.279.59-1.95-5.99-1.990.111-79.00.321-0.395-0.4190.475-7.0752.97.70

-0.757-0.00959

-27.9-0.3924.770.5(31.075.27-3.290.199-1.00

ug/iUg/1

•19/1ug/1I>9/1«9/l"9/1U(/l

U(/l

U9/1ug/1ug/1ug/1ug/1U(/l

U(/l

U(/l

U(/l

ug/1U9/1ug/1ug/1ug/1ug/1ug/1

0«l.c

-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1 00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00-1.00

DUMP OF MtTAll IATOH fill BOP704IO.MCTALf FRI, DOT 2?i 1661, 1:40 AM

Initial ind Continuing Cillbrdlon Vtrlflotlon ird Ctllb. Blink Dili ••«

Eltmnt: Ad Unlit: uj/1 EUmnt: AL Unlit: uj/1

Poiitlon567110111121517It20313346411275It10311711112012t1311321341430J!74II102116121

Simpll ClSXBLKSASI514ASASI514ASBSI514BSCSI514CCSSI514BCSSI514ECSSI514DCSMIDCHKCSXISINTCSCRIACSCRIBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLK .CBBIKCBBLKCBBIKCBBLKCBBLK

0.11111.0 .

20040.1413114103141

21.714.2104

tl.l104

12.3108103104101107

11.517.1

15^2171

2.210.1132.71.71.15.42.65Ik

020.020.040.0200

40.35001000100III20.00

10010010010010010010010010010010020°8

0III.00.00.00.00.00.00.00.00

- .00

14.1II 2101100101

16.7II 4103

15.8101104

11. 1101

12.3101103104101107

11.517.1101113

tt.O-221

-11.3-271

-242•465-371-235

Poiltlon Simplt CllcuUttd5 SXBlK 3.0167110g111215171120313346411275II103117iiS121131132134144?1174II102116121

SASI514ASASI514ASBSIS14BSCSI514CCSSI514BCSSI514ECSSI514DCSMIOCHKCSXI5INTCSCRIACSCRIBCSMIDCHKCSLABCONCSMIOCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKaitSCBBLKCBBLKCBBLKCBBLKCBBLK

414500100050001030

• 12600255002650

501000531436261025102670253026102740271027502730247025102770522211

S2100010.01.015.2111.13.011.21

-3.1210.03.46

Expccttd0

50050010005000100012500250002500

4370005000

2500250025002500250025002500250025002500250025005000

437000-1.00-1.00- .00- .00- .00- .00- .00- .00- .00

X R«cII. 1100100100102101toe106115101107100107101101101101110101II. 1103111104lit

-1000-601-521

-1110-301-126312

-1000-346

DUMP OF METALS BATCH FILE BOP704(C.METALS FKI. OCI 27. 1119. 1:40 AM

Inlllll ind Continuing Calibration Virlflcltlon Ind Cillb. (link Dill

ElMMDt : AS Uflltl: ug/1 Unit I: uj/1

Position567110911121517192031334641627519103117119120129131132134143045

II102116121

SliwU CllSXBLKSASI514ASASI514ASBSI514BSCSI514CCSSI514BCSSIS14ECSSIS14DCSMIDCHKCSXI5INTCSC* I*CSCRIBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIOCHKCSCRIACSCRIBCSXI5INTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

-1.6599.1104116

11322304410460-41212.441.1476440473445495419495520530484452517101

77.1-3061.46ill10.11.15.24.26.24.

0100100200100011125005000500J0

50.05005005005005005005005005005005005000

50.00

-1.00-1.00-1.00- .00- .00- .00- .00- .00- .00

99.1104

91 8100

92.119.119.692.0

96.295.3II. 194.119.0

S?:?99.1104101

12.190.4103156

-146-333-512-1010-1140-1510-2450-2140-2450

t7110>111215171920313346416279191031171191201291311321341430456174II102116121

SXBLKSASI514ASASI514ASBSIS14BSCSIS14CCSSI514BCSSIS14ECSSIS14DCSMIDCHKCSXI5INTCSCRIACSCRIBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSHIDCHKCSCRIACSCRIBCSXI5INTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

-3.1391.910020599920023404670501-371100

50.9502410502415502501499510506471477510

95.447.5-3952.73-in1.530.934l.OS-2.23-2.05-3.79-4.56

D100100200100020525005000500000

500500500500500500500500500500500500000

-1.00-1.00-1.00- .00- .00- .00- .00- .00- .00

91.9100103

99.997.493.793.1100

10091.1

. 10097.0100102

99.9102101K-.I102

-273111-153-93.4-105223205379456

DUMP Of MITALS IATCH FILE BQP704IO.MITALI P H I , MT JT, Itll, 1:40 AH

••• Inliul tnd Continuing Cilibntlon VtrlflciUon >nd Cillb Blink Dili • ••

Climnl: BA Unlll: ug/1 ElMMnt : BE Uniti: ug/1

5171109111215171920313346418275191031171111201291311321341430451174II102IK

SXBLKSASI514ASASIS14ASBSI514BSCSI514CCSSIS14BCSSIS14CCSSIS14DCSMIDCHKCSXISINTCSCRIACSCRIBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

«.,.,.„

log4012000407

412097101030463201101

104010001040197

104010601050106010601000

205106411

-1.13-2.72-2.71_2 . 54_2 . |0

-2'. 27-2.13

I.,....*2002004002000403SOOO1000010004312000

1000100010001000100010001000100010001000100010002000

439-1.00-1.00-1.00-1.00-1.00-1.00

-I 00

99.9100100101

91.497.1103106101104100104

99.7104101105101106100101101102110193272271256254

III

se7110t1112IS171920313346416275191031171111201211311321341430456174It102116121

SXBLKSASI514ASASIS14ASBSI514BSCSI5UCCSSI514BCSSIS14ECSSI514DCSMIDCHKCSXISINTCSCRIACSCRIBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCRIACSC* IBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

0.053519.119.940.1200

40.1415957101431

19.910. S102

91.4102

91.2102103102105104

95.195.2106

20.410.1455

0.1610.05350.1400 1610.1970.1110.2550.1970.140

020.020.040.0200

40.1500

10001004230

10.01001001001001001001001001001001001000

10.0423.00.00.00.00.00.00

- .00- .00- .00

99.499.7100100

99.997.095.7101104105102

91.4102

91.2102103102105104

<5.t95.2106101101

-11. 1-5.35-14.0-18.1-19.7-11.1-25.5-19.7-14.0

DUMP OF METALS BATCH FILE BQP7049C.METALS FRI. OCT 27. 1919, 1:40 AM PAGE 5

Initial and Continuing Calibration V e r i f i c a t i o n and Calib. Blink Dili

Eleaunl : CA Unite «9/l EUMnt: CD Unlti: uj/1

Poiitien Sample Calculated5 SXBLK -21.11711091112151719203346418275191031171191201291311321341430451174II102111121

SASI514ASASIS14ASBSI514BSCSI514CCSSI514BCSSI514ECSSIS14DCSMIDCHKCSXISINTCSCRIACSCRIBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCRIACSCRIBCSXISINTCBILKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

11901*1020000

401041700110001050045700020401110107009190

101001000010700101001070010900109009100

101001090020501070

477000-10.9~24 ' 3-u!t-11. t-1.33-5.49-17.1-69.1

Expected0

200020004000200004050SOOOO1000004610002000

010000100001000010000100001000010000100001000010000100001000020000

461000-1.00-1.00- .00- .00- .00- .00- .00- .00- .00

X Rec99 499.7101100101

97 491 0105

19 2102107

91.9106100107101107109109

91.0101109103103

1090I960243016901190633549

17106910

Petition Sample Calculated5 SXBLK 0.101711091112IS17112031334641627519103117119120129131132.134j430451174II102111121

SASIS14ASASI514ASBSI514BSCSI514CCSSIS14BCSSIS14ECSSIS140CSMIDCHKCSXISINTCSCRIACSCRIBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSHIDCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

19.519.140.6200

41.3471950107171

20.111.1101100109101112110110114114

99.491.5114

23.113.2929

0.7240.151

1.471.291.751.232.212.211.29

Expected0

20.020.040.0200

40.6500

10001001150

10.01001001001001001001001001001001001000

10.0115

-1.00-1.00-1.00- .00- .00- .00- .00- .00- .00

% Roc17.799.2101100102

107101111109100109101112110110114114

99.491 511413;114

-72 «-15.)

-14)-129-175-12!-221-221-129

PUMP OF METALS IATCH FILE BQP7046C. METALS OflT IT. 1666, 1:40 AM MM *

••• Inlllil ind Continuing Cillbntion V«rlUcition ind Clllb. Blink Dill **•

EUMCll: CO Unltl: uj/1 Eltnunt: CD Unlli: u«/l

56711011112IS1711203133414162751610311711*12012*13113213414116174102116121

SXBLKSASIS14ASASIS14ASBSI514BSCSIS14CCSSI514BCSSI514ECSSI514DCSMIDCHKCSXISINTCSCHIACSCIIBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCHIACSC II IBCSXISINT

itsCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

"Jo3*40.*11.040013.11731140

4$20 621120521*20122322422422122*20120743*023.*4*5

0.3050.612-0 299•I 31-1 64-I.lt0.211-1.56

040.040.010.040011.01000200020041*40.00

200200200200200200200200200200

40.041*.00.00.00.00.00.00.00

1.001.00

100101101

99. (103(7.3(6.610710410210*102110104111112112114114104104io!112

-30.5-61.294 129 9131164211

-21.1156

Petition S.mpl. CilcuUtod5 SXBLK • -1 41t7110t1112IS171120313341418275It103117lit1201211311321341430456174II102116121

SASI514ASASI514ASBSI5I4BSCSI514CCSSI514BCSSIS14ECSSI514DCSMIOCHKCSXI5INTCSCftlACSCRIBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKcscmACSCIIBCSXISINTC8BLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

56.660.112260012314602190317441

•62.131 532430432430132S32932733033230430433162.133.6466

0.0267-0.325-0.611-0.402-0.364-O.tll-1.070 356-1.54

Evpoctod0

60.060.0120600122150030003004220

30.03003003003003003003003003003003003000

30.0422

- .00- .00- .00- .00- .00- .00- .00- .00- .00

* Roc99.3100102

99 9101

97 I16 5106106

105101101101103101110101110111101101110112110

-2.6732 561.140.236.461.1107

-35.6154

NO00

DUMP OF METALS BATCH FILE BOP7049C.METALS FBI. QCT 27. lilt. 1:40 AH

Inltlll »nd Continuing Clllbrillon V e r i f i c a t i o n ind Ctllb Blink Dill

EUmilt: CU Unlll: u|/l EUm.nl: FE Unlll: (It/I

Poiltion S»»U C«U»UUd5 SXBLK -0.7056 SASI514A 59.17 SASIS14A 59.71 SBSIS14B III10 SCSI514C «009111215171920313341416275,0s11711912012*13113213414JO56174II102116121

CSSIS14*CSSIS14ECSSI514DCSMIDCHKCSXI5INTCSCHIACSCDIBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCIIACSCIIBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

1221470295031*493

60.434.2319299311297319323319325324293294321

13.634.1511

0.121-0.1100.7090.9430.9430.7092.011.770.709

Expected0

60.060.0120600121

15003000300411

60.00

300300300300300300300300300300300

.2°J60.00

461.00.00.00.00.00.00.00.00.00

X ««c

99.799.5101100100

91.391 5105105101101

99 1101

91.1106101106101101

97.791.1109101109

-12.111.0

-70.9-94.3-94.3-70.9-201-177

-70.9

Poiitlon Simpl. CllcuUtod5 SXBlK -7.5367110111121517192031334641127519103117119120129131in1430456174II102111121

SASI514ASASI514ASBSIS14BSCSI514CCSSI514BCSSI514ECSSI514DCSMIDCHKCSXI5INTcscmACSCP.IBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCRIACSCDIBCSXI5INTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

2022044032000401

415096101030

170000211159

105010101040991

1050106010601010101091110001090232110

171000- .23- .31- .41- .19- .00

.44- .10

.7017.3

Elptctod0

20020040020004035000100001000

1630002000

10001000100010001000100010001000100010001000

0113000

.00

.00

.00

.00

.00

.00

.00

.00

.00

X ««c

101102101

99.9101

97.196.1103104109105101104

99.1105106106101101

19.1100109116109623131141511500

-544110

-770-1730

DUMP OF METALS IATCH FILE BQF704IC.METALS F«I, OCT IT. llll. 1:40 AM FAOE I

Elwtnl^K/

**• Initial and Continuing Calibration varlflcallon and Callb. Blank Data •*•

Until: ug/1 • Eltmnt: MQ Unlit: ug/1

Position Samplt Calculattd5 SXBLK 21.21711011112IS171120313341411275II1031171111201311321341430

74II102111121

SASI514ASASIS14ASBSIS14BSCSI514CCSSI514BCSSIS14ECSSIS14DCSMIDCHKCSXISINTCSCHIACSC* IBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSMIDCHKCSCIIACSC* IBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

111011104010200004070411001000004220-1*01110113042103710411031104110412040104170410035403670401011001010-23251. •-20.1III40.14.1131.64.03-56.0

Exptcttd X Rtc0

200020004000200004010900001000004000

000

400040004000400040004000400040004000400040004000

000

- .00.00.00.00.00.00.00.00.00

11.3II. 1100100101

11.2100109

105«4.0104

15.2109103102104102

II. 1• 1.1102

-SIIO2010-3320-3120-4010-411-3160-4035100

67110111121517112031334141•275II103117111120

ill134143045• 174II102111121

SXBLKSASI514ASASI514ASBSISUBSCSI514CCSSI514BCSSI514ECSSI514DCSMIDCHKCSXISINTCSCRIACSC* IBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCftlACSC* IBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

-11.01110200040402000040704120011300109004110002090121010100«I701010011201010010100101001010010700151011001010020501100

507000-1.63-13.3-23.7-3.11-2.11-11.0-11.03.79

-2.13

0200020004000200004040900001000001000047400020000

1000010000100001000010000100001000010000100001000010000100002000

474000-1.00- .00- .00- .00- .00- .00- .00- .00- .00

11.9II. 1101100101

11.311.3105104102101

11.7101

11.210110110610110715 1II. 01011031071631330237031121111001100-375213

DUMP OF METALS BATCH FILE BOP7049C.METALS FKI. OCT 27. 1(19. 1:40 AM

Initial ind Continuing Calibration Virldcillon ind Callb. Blink Dili ***

Eltawnl: MN Unlll: UJ/1 EUnwnl: MO Unit I: iig/1

Politio51

1

1215171120313346411275II103117til120129

ill1430451174II102111121

' IxStK* °SASI514ASASIS14ASBSI514BSCSI514CCSSI514S

§I514CI514DIDCHK

CSXISINTCSCRIACSCRIBCSMIDCHKCSLABCONCSLABCONCSMIOCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCRIAci»,I?NTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

-0.101

lil1221410290031547210. «31.732030031130232232132233032921130033362.733.4414

-0.392-0.124-0.312-0.312-0.312-0.312-0.241-0.241-0.241

010.010.0120100122150030003004450

30 03003003003003003003003003003003003000

30 0445.00.00.00.00.00.00.00.00.00

99 410010110010197.396.7105106106107100106101107109107110110

99 3100111111111

39.212.431.239.239.239.224.124.124.1

Poiltlon Samplo Cllculatod5 SXBLK -0 77667110Iii171120313346416275191031171191201211311321341430456174II102116121

SASI514ASASI514ASBSIS14BSCSI514CCSSI514BCSSI514ECSSIS14DCSMIDCHKCSXI5INT-0.0CSCRIACSCRIBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIOCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCRIACSCRIBCSXISINTCBBLK -0CBBLK CCBBLK -0CBBLK 0CBBLK (CBBLK -(CBBLK -(CBBLKCBBLK 0

49.749.110250010212202420263065152 525 5261?5026725427227421021221225126121153.421.02.17.642.371.776.621.244.257.7711.15.111

Expoctod0

50.050.010050010212502500250000

250250250250250250250250250250250250000

.00

.00

.00

.00

.00

.00

.001.001.00

% Roc19.4II. 1102II. (1005iJ107100107101109110112113113104104114

64 2-3777-62-242577-115

-11 I

II TALI BATCH fILE BQP704IC.MITALI MI, OCT 97, 1911, Ii40 AM

"• Initial and Continuing Calibration Verification

El«unt: NA Unlll: uj/1

5 SXBLK -31.71 SASI514A 19107 SASI514A 11101 SBSI514B 2010010 SCSI514C 1000001 CSSI514B 2020011 CSSI514E 24100012 CSSI514D 41100015 CSMIOCHK 51100171120313341411275II10311711112012113113213414304574it102116121

CSXISINTCSC*CSC*CSMICSLACSMICSLACSMICSMICSMICSMICSMICSLACSLA

AINKCONCHKCONCHKCHKCHKCHKCHKICONICON

CSMIOCHKCSCIIACSCKIBCSXISINTCBBLKCBBLKaft*CBBLKCBBLKCBBLKCBBLKCBBLK

-54010000524051100413005220041100511005330052300521005210041300S020053700101005310-SSO12.2-34.2-11.4-11.1-1.34-11.4-3.17-11. 1-23.4

10000100002000010000020100250000500000SOOOO

010000

0SOOOOSOOOO500005000050000SOOOOSOOOOSOOOOSOOOOSOOOO500005000010000

00

- .00- .00::88- .00- .00- .00- .00- .00

99 699 1100100101

99.199.7104100104

11.6104

99.2104107105101105

11.5100107101

-1220342016401110134164036716602340

56711011112IS171120313346411275191031171191201211311321341430451174II102111121

•AOI 10

anil Callb. Blank Data "•

EUn.nl: NI Unlll: ug/1

sxSIVSASI514ASASIS14ASBSIS14BSCSISUCCSSI514BCSSISI4ECSSI514DCSMIOCHKCSXISINTCSCRIACSCRIBCSMIOCHKCSLABCONCSMIOCHKCSLABCONCSMIOCHKCSMIOCHKCSMIOCHKCSMIOCHKCSMIDCHKCSLABCONCSLABCONCSMIOCHKCSCRIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

-0.122Sl.l60.112110012314402150315137

62.029.432430131130232132132133333330130333563.634.1193

0.6910.259-0 9160.3720.212-2.47-O.lll• 1.41-0.945

010.010.01206001211500300030013960.0

0300300300300300300300300300300300300

60.00

139- .00- .00::88.00.00.00.00.00

99.4101100100102

95.994.9105

99.7103101100106101109109109111111100101112106106

-69.1-25.991.6~21 224711.9-14194.5

CMNJ

DUMP OF METALS BATCH FILE BQP704IC.METALS FB.I. OCT 27. 191*. 1:40 AM PAOE 11

Initial and Continuing Calibration Varllication and Callb. Blank Data •••

Eltinont: PB Unlti: 119/1 ElMMnt: Unlti: uj/l

iltlon Saiapla Calculated Enpacttdt SXBLK -0.449 0I SASIS14A 102 1007 SASIS14A 91,1 1001 SBSISI4B 260 2001091112IS171920313341411275II10311711912012913113213414I?1174II102111121

SCSISUC 1001gSSI514B 201CSSISUD 4171CSMIDCHK S3!CCSXI5INT IISCK I A 10

CSCKIB 51.CSMIDCHK 55C(CC

SLABCON 41SMIDCHK 54SLABCON 51SMIDCHK 55SMIDCHK SI

) 1000200

! 2SOOSOOO5009310

! so.oSOO500SOOSOO500SOO

CSMIDCHK 514 SOOCSMIOCHK 572 SOOCSMIOCHK SI2 SOOCSLABCON 514 SOOCSLABCON 411 SOOC(SMIDCHK SI!sen i A 11SCI IB 13.

CSXISINT 93

SOO0

50.0r 931CBBLK -4. 35 - .00CBBLK 2.25 - .00CBBLK -4.91 - .00(CCCC

BBLK 3.2'BBLK 4.1SBLK -7 . 1'IBLK -S.OIBBLK 1.7'

- .00.00.00.00

1 .00CBBLK -7.33 .00

X ««c

10291.199.1100103

97.097.5107

92.010411099.1109103112114113114111103

99.7113121100435-225411

-324-411714501

-174733

S171101

I!IS171920313341411275191031171191201211311321341430451174II102111121

SXBLKSASIS14ASASIS14ASBSI514BSCSISUCCSSIS14BCSSIS14ECSSIS14DCSMIDCHKCSXISINTCSC It I ACSCRIBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCIIIACSCRIBCSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

-I.2SII. 110720S99920024404940513

31.1104

S2.7521414S21495531545542541552490417550105

59.715.22.13

'2.340.1713.112.03-1.19-7.073.01

-1.31

010010020010002052500SOOOSOO0

1000

500SOOSOOSOOSOO500500500SOO500SOOSOO10000

-1.00-1.00-1.00- .00- .00- .00- .00- .00- .00

II. 1107102

11.997.197.591.1103104105II. 1104

99.0107101101110110

II. 097. S110105

-213-234

-17.1-319-203111707-301131

CcJCM

DUMP OP MCTALS IATCH FILE BOP704IC.MITALI PHI, MT IT, Illl, 1:40 AM PAOI II

••• Initial «nd Continuing Cillbrttlon Virlflcttlon and Cillb. Blink D.ti •••

(Until: SC Unlit: uj/1 Cltmnt: SN Unltl: uj/1

% lUc101

IS.S102

II. I100

17.117. S104

101-H105101107101107111110

II. I•1.4111121

-IS-!?.-IS?

-1170-1130-573

Potltlon Suiplo CilculittdS SXBlK -0.2BI1711011112IS171120313341411275II103117III121131132134

4°\\102iiJ

SASI514ASASI514ASBSI514BSCSIS14CCSSIS14BCSSIS14CCSSI514DCSMIDCHKCSXISINTCSCftlACSC* IBCSMIDCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCHIACSC* IBCSXISINT

aftSCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

11320040120004014ISOIB701050

-11.3200107

1070111

1070101011001110111011501140105010(01110211117

-12.5

;!;!!-5 34-3.11-5.20

E»poctod0

20020040020004015000100001000000

100010001000100010001000100010001000100010001000000

1:881.00

_ J QQ

-iloo-1.00

X HocIB. 4100102II. 1II. •• 7.1•B.7105

107II. 110710111011111111511410510B111

411214170212120

1140534311520

Ovl

DUMP OF METALS BATCH FILE BQP7049C. METALS Fill. OCT 27. 1919. 1:40 AM

Initial and Continuing Calibration Verification and Cillb. Blink Data

El««tnl: TI Unlit: us/l Elamnl: V Unite U9/1

Positiont710111121517It20313341411275It103117litIII13113213414JO5

tl74II102111121

Sanpla Calculated ENpactadSxilK -7.11 0SASI514ASASI514ASBSI514ISCSI514C 1

03 10003 10003 200It 1000

CSSIS14B 204 203CSSIS14E 2410 2500CSSI514D 4CSMIDCHKCSXISINT 5CSCRIACSCftlB 4CSMIDCHKCSLABCONCSMIDCHK !CSLA8CON 1CSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHK

1°, 5?22.1 004 05 015 50003 50014 50003 50017 50026 SOO19 50030 SOO21 500

CSLABCON 533 500CSLABCON 532 500CSMIDCHK 531 SOOCSCRIACSCIIB 4

07 0.4 0

X R«c103103101

tl.l101

tl.t17.9102

103101103101103105104101101107lOt107

CSXISINT 10.1 0

CBBLK -CBBLK -CBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

41 -1.003t -1.0077 .00SO .0075 .0017 .0030 .0011 .0011 .00

641139177150175117130lit111

Position Sample Calculat.d5 SX8LK 0.0274I71101u15171120313341411275It

1 171 191201211311321341430451174II102lit121

SASI514ASASI514ASBSI514BSCSIS14CCSSI514BCSSIS14ECSSIS14DCSMIDCHKCSXISINTCSC*IACSC* IBCSMIDCHKCSLABCONCSMIOCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCHIACSC* 18CSXISINTCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLKCBBLK

Sl.t59.9121too12214702930317411

10.433.132029932029932232332132732129729133014.031.35011.21

0.1122.252.402. It1.523.122.141.14

Elpocted0

10.0to.o120too12115003000300444to.o0

300300300300300300300300300300300300to.o0

444-1.001.00.00.00.00.00.00.00.00

* *oc11.2II. 1101100101

17.917.5101110101107

19.7107

99 1107101107109109

tl.t11.4110107114

-129-11.2-225-240-211-152-312-264-114

tr>

OUMP OF METALS IATCH FILE BOP704IC.MCTALI F«I, MT If, till, (|41 AM

••• Initiil <nd Continuing Cillbritlon Verification ind Ciltb. Blink D»t« •••

Clemnt: ZN Unlit: uj/1

loctld * Rtc0

100 11.4100 II.I??0 101

100100

11.517.0101

11.5101101101107100101110101111111

II.011.7112115103100110145130121147117

-121111

Position SmoU CllcullUd5 SXBLK -1.4117110111121517II2031334*411275II103117111120121131132134

SASI514AySI514ASI514BSI514C

CSSI514BCSSI514CCSSI5140CSMIOCHKCSXISINTCSCIIACSCRIBCSMIOCHKCSLABCONCSMIDCHKCSLABCONCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSMIDCHKCSLABCONCSLABCONCSMIDCHKCSCRIACSCRIBCSXISINT

II 4II 1201100020324104150521100

53.1531504537502543541544555551410414511104

57.7111

-1.00

3:1-1.171.21

-1.11

CMO\

Roporl" .10 27 1-9 0 0 : 2 9 : 2 9 AM

!>;impl (; F.i ] o 'I'imo Op TO '.I'ypoj .H

1 nw2;t nw4 HUNKs :;xnr.K

7 HA:; rs.i'0 !W!ifr> 140

10 :;c::rr,i4c11. e:;:ur. UK12 <::;:; r s i 4 f>1:1 nw14 CBIU.K.is c:;M;nc:trx16 nw10 nw19 ciiCkTA20 c:;cR.rn21 nw22 RiiMni.i2:1 R::nnr.2

2S H:;Mni.4

27 RiiMlir.62.0 R:;Mnt.729 OW.10 CMIIU.K.11 c::;Mrnc:i(T<;i2 nw

owR:;QKKfl-'llPW

.17

.111 RSCA1970

.19 R:1CA197640 R.';CA197941

2 R:;CA2066

OWcnm.Knw

4« R: ;O/OOSI49 «Kf|.'llPW

R:U:AI:V/Ir.2

P7049CP7049CP7049CP7049CP7049CP7049CP7049CP7049CP7049CP7049CP70'»9CP7049CP7049CP7049CP70490P7049CP7049CP70490P7049CP7049CP7049CP70490P70490P70490P7049CP/049CP7049CP70490P7049CP70490i>7049cP70490P70490P7049CP7049CP7049CP70490P7049CP7049CP7049CP7049CP7049CP7049CP70490P7049C('•J0490P7049<:P7049CP7049CP7049CP70490P7049CP 70 490

KTCICI'AIWCrCPA10.1'CTCPAt'TCTCPAKTC 1 CPAliTC 1 CPAKTCMCPAKTC 1 CPAKTCICPAETC; CPAIO'1'CICPAI'i'l'CtCPAic.rc.fcPAKI'CVCI'AI'M'C 1 CPAicn: i CPAwrc/cpAwe; CPAKTCICJI'AK'.I'CTCPAE'l'Cl CPAKT(;;CPAicrc/GPA10.1'C.ICPAic.rc.rcpAic.rc.rcpArc.ro rci'AtcrcrcpAicrcicpAio.rc.TCPAH'.l'CfCPAJCIXMCPAETCfCl'AicrcicpAtcrcrcpAicrc.tcpAjo.ro r CPAICI'CMCPAicrcrcpAicvc.i(;pAE'l'CfCPAICTCfCPAICI'CICPAicrcicpArororcpAicrcicpAKTCfCPAlore r CPAicrc i CPAlonucpAtoroiCPAic.rcrcpAlorercpA

10//!()/B9.10/26/11910/26/119I0/?f)/(1910/?.6/fl910/26/11910/26/0910/26/H910/26/11910/26/11910/26/1)910/26/1191.0/26/H910/26/11910/26/11910/2(>/H910/26/11910/26/11910/26/119 .10/26/11910/26/0910/26/0910/26/0910/26/11910/26/11910/26/11910/26/0910/26/0910/26/0910/26/0910/26/1)910/26/0910/26/09 .10/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/26/09j 0/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/2.6/09

1: :)2 HR1 ::)4 «.K1 :;17 KM1 ::19 HH1:42 RK.1 :'('> SI)1:47 R«1 : 49 KR.1 :S2 RR.1 : S4 RRl.:!>7 RR1 : 89 RH2:02 Id)2:04 HH2:07 RH2:09 RR2:12 RR2:14 RH2:17 RR2:19 RR2:22 RR2:24 H«2:26 RR2:29 RR2::il HR2: H't RR2:. 1 6 RR2:1)9 RR2:'il RR2:44 RR2:46 HH2:49 RR2:51 RR2:84 RR2:86 RR12:!>9 RR:>:0l HR:l:04 RR1:06 RR1:09 HR1: 1 1 RR1:14 RR1:16 RR1: 19 RR1:21. RR1:24 RR1:26 HR1:29 RRl:!ll RH1:114 RR1:40 RR1: hi RR:i:S;l RR

CONCCOMC

! COMC> CONCi CONCs CONC:• CONC1 CONCi CONC

CONC; CONC1 CONC•i CONC> CONC! CONCT cow;1 CONCT CONCT CONCi CONCi CONCT CONC"> CONC; CONC; CONCi CONC

CONC1 CONC; CONC; CONC', CONC; CONC-> CONC1 CONCi CONC:i CONC:i CONCi CONC

COMC:i CONC> CONC! CONC

CONC:', CONC•. CONC:> CONCi OC'.NC1 CONCi COMC

CONC:T CONC:i CONC:i CONC

137

_™___-__-JZ;2z22Z252z222222zS2222Z22Z2Z222222SZ2553rZ22Z 2s. B88888838888 8888888886-8 88 SB B888888B8888 8888888888 8888SJ;,

C1 11 II I" II 11 H 11 I" II II II 11 II " II il

=s a _c .1 o c c c •

r^r^^

1 a*- w- 9*- 5* c- c- c*

li 2 r: -.-; r\:-. r >• r tr vcr-ccrÔ'C'— ™-c^r^T*-r**vccc;C'3> ^ * .- .- "'"' i

C d C - X -. . _ .s 5 s s rr » 3= ~ » » § s ? .v » -c- c •- . -". 'C r- cc C1 c —

pl 1 1 Nc.ullO

Kri .10 27 89 00 :29 :29 AM p,i«u .!

Mol'liori l)al:o T.inm Op/0 Type Motln

10!) R.'iQ700'tO1091 10.1 1.1 Q!!CA19B!i112 RiiCA 19321.13 H15CAI933

1 1 B OW.116 ClUlf.K11; o.'iMrnciiK1 1 R OW119 C:;I.AUCON120 (r.r.AiicoN121 nw123 H15CA1939.1.2'» K\'JCAJ9r,6

126 «iiCA19/!;12.7 OW12:1 cnnrjf12.9 c::nrm:»K1:10 ow131 CilCRTAu;>1:1:1 owi :i K nw

P7049CP70't9CP7049CP70't9CP70'»9CP7019CP70't9CP70't9CP7049CP70'i9CP7019CP7049CP70't9CP7049Cl)70 9(;P70'i9CP7049CJ'70'»9CP7049CP70't9CP7049CP70'i9CP70'»9CP70'i9Cl''/0't*)('[)'/()/Jt) JP70't9CP70't9C

CTCICPAro'i'crci'Aui'crcpAKI'crcPACTCCCPA(•rrcicpflKP<;I.CPAKTCICPAICPC; i CPAKPC 1 CPAKTCICPAKPC I CPA[•rpc.rcpArax; (CPAKPCJCPAKPC .[ CPAI'iTC 1 c;i'AKPC/CPAKPC.ICPAra'ci'CPArac/ci'Ai'"p(;rcpAK'P(M'CPAE'p(;f(,'PAPPCTCPAi'i'i'c.t<;pAKIXMCPAICPCTCPA

1(1/26/09.10/26/8910/26/0410/26/091.0/26/8910/26/8910/26/0910/26/0910/26/0910/26/8910/26/8910/26/8910/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/26/0910/26/091.0/26/0910/26/0910/26/04

.161616161616.161616.1616161 6161 6161616.1 616.1717.1717.17.17.1717

:.l 1.: 13: .1. 6: 1 8:21: 23:26:28:31:33:36:38:'».!:((3: '> 6:'t8: ;i.l:!i:i: S16:bB:0.1:03:06:08: 1.1: 13: 16: 1.0

HHHHHHHHHHHHHHHHHHHRHRHHKKKHHHKHHHHHKHHHHHHHRHHHHHHKHHHH

CONC! CONC1 CONC; CONCi CONCI CONC> CONC! CONC'; cowi ( 'i >NC1 CONC! CONC

CONCi CONC; CONC: CONC-< CONCi CONC;! CONCi CONCi CONC•> CONC:i CONC"> CONC• CONC1 CONC; CONC- CONC'

139

Analysis Hu

» KlonuinU DW MIDCIW OW

P.r.i 1 0 - 2 / - U 9 0«:J9:29 TM

HC.ANK :iAUTS.14A

fl7R9

10.11

AK3280A.I 3461A; i t936n 2497H.i't1?:)'!IV.<3130C,l 31 7 4(M72(i5

C.r2fiV7CII37.47Vo2599

766414 MB7.7 9015 MII2576.16 Mo2070.17 N.I5895IB N1731614 Pl)220370 il)200»7.1 VI960

73 I'i334924 V 292425 Zn2138

.13

1 /7 Al34613 A«19364 D 74975 H.149346 n<«31307 Ca3179n (M22659 Co27.86

10 Ci-26771 1 Cu.124712 K«i2S99.13 K 766414 Mr, 2 7 9015 Mii257616 Mn2070

N.-15H95N i 2 3 1 6

171.119 l'l)27037071227.3; 4

;b7.06il;<-ii 460.'II.1B99

V 7.92'.

.0062

.1353

.0266

.0306

.0571

.0051

.5334

.0053

.0108

.0165

.0154

.0518

.5325

.518.1

.0159

.01747 . 5 1 1.0159.0249.0759.0576.0447.0224.0.159.0273

::AST514A i

.0189

.4431

. 1078

.1094

.7091

.02072.123

• ' *.

'J.9.147.002 ..0633.051810.05.0650.0976. 1076. 1963.7071'. 109;1..06.1 :.

.1017.2.603. 5.1 51.53901 .066.105910.73. .1 1 08.7.2.15.3294.3204I .0024. 10510.5.1..3274.268351.89.3328.5377.5208.1 .053.1 .079.5236.37.21. 5447

iBiiTS14n

.0403

.9902

.2030

.7.105

.4186

.041.84 . 226,0426.0849.1278.1241.43023.9294.059.1275.105570.10.1286.7.022.7.067.4221.'•202.2113.124!)

.0009.0026.0006

.0012

. 0000

.0001.0141.000.1..0001. 0004.0007.0005.0298.0105. 0004.0003.0398.0001. 0068. 0009.0043.0121.0041.0002. 0004

era i si 4ii

. 04001.007.2061.2210.4221.04224.261.0435.0871.1287.1246.43513.9894 . 093. 1287.105820.30.13.15. 2090.2027.4221. 4200.2K17.. I2f>0

.000').0000.0032.0024.0006.0001

.061.1.0005.0005

. 0000.0016.001.1..045.1.0.197..0002. 0004. 0009.0009.0118. 0066.0082'.0094.0037.0007.0002

r»c::iis.i40

.205.15.0161 .02.11 .04.12.067.20077.0.57. 7 1 .1 4.4176.6253.6.1442 . 1 0419.8020.13.6261.51931 00 . 3.6384.1 .0341.0.102.0652.0771 .030.fc20i

.0003

.0066. 0000.0026.0000.000.1..0583.0002.0010.0010.00.12.0005.0315.0239.0001.0008.0040.0005.0054.0069.0029.0058.0039.0009.0005

era/ 5.1 4K

.490012.462.5122.5285.007.511150.00. 50701.0.161 .5181.5115 .10049.1749.521.5251.2687.48.61 .5302.5102.4705.0365.054?.S361.521

.0.183

.4070

.1-034

. 1083

. 2084

.020(>2.11 7.07.03

. .047.3.067.6.0608.21.891.9.101.997.0630.05.16 ..1 0 . 02.0638.1012.0967. 2004.1953. 1000. 060 1.1040

Cfi.'i 1 5 1 41)

1.01425.315.0555.03310.101.0041 00 . 5.1 .0042.0233.0163.029.1 0 . 0999.4499.403.0312.517500 . 43.0745.0535.02210.071 0 . 08li.3343.0-i.l

140

An,s.1yais Moport-. AvoraKuti )'Y.i 10 2/119 00:7.9:29 AM

It Kltmicnt: .'1ASJ314A ;>Hr>t514H en.'! Till 4B nCH.r5.l4C C.'iSJ 5.1 /.]•: on.'! T 51 40

It Klonunil:

2 A.I 39613 As 19364 JB 2497

6 lU.t31.10

0 Ctl22659 Co 17116

10 Cr76/71 1 Cn324/12 Po759913 K 766414 M«779015 Mn757616 Mo7.0.7.017 Nrt509510 N1231619 Pb720370 ,2.1 :inl96072 :in1H9923 T1334974 V 797475 7n213(l

It Kl tMiiruit:.

1 AK37.HO

3 Aw 19364 n 7497

I1.i49.16IUi.1.130C,<3179

Co 7. 7. 116

Cn324V

13 K 76f414 MR7/90

Hii2576Mo 7.0 20

.1!'.1617II)197.0

Ni7:)16

> 70 fill

.1044

DW

.007.11

.033(1

.0063

.0179

.0133

.00.14

.125

.007.0

.0037

.0050

.0075

.0147

. 1 5117

. 1 345

.0047

.0044

.6653

.0093

.0079

.01211

.0193

.0000

.0025

.0053

.0091

Cf.CRlA

.0211

.5249

.1059fnw •jM»s»sBS*YSMjjta'..TCJ9-.0652.06.14 '.23641 .9737.054.0641.054610.06.0663. 1073.1055

.2113

CBB;J<

.0010

. 0004

.0037.

.00117

.0001

.000.1

.06011, 0004.0007.0005.0004.0009.0059.0144.0004.0007.0400.0011.0095

. 00 1 6.0039.0106.0032. 0004. 0000

CHCRtn

.0.1.34

.4239

.0584

.0610'.1064.01091 .292.0122.02.19.0333.0346. 1741.1 .073.1 .216.0339.02665.2H7.0316.0400.0530

.2126

CSMJ'DCIIK

.10502.62.1.52.14.54551.067.106710.07.1 132.2243.3309.37.371.0924 . 1 3 1.10.56.3300.273052.12.3354.5506.52.10.1 .077.1 .01)5. 5262.3279.5501

0W

.0026.0150. 0044.0046. 0002.0001.0042.00.10.0005

.0001

.0017

.0016

.0553.0249. 0006.0019

.0251. 00 1 9.0050.0066

.1 .037

DW

.0021

.0004

.0100

.0052

.0003

.0001.0110.0007.00.10.0003

.0019

.00.1 1

.0417,OJ?.2.0000,00.11.0677.'0012. 0020.0049.0079.0130.0040

.0016.0003

J<™

.02.1.1

.0991

.1020

.1052

.0050

. 0005

.2.155

. 0064

.0227

.0225

.0123

.2.3321 .015.0351.0150.0423.3063.0105.1064. 1105

2.51 0

csxBSiwr

.11757.507.47 . 490.6227.41107.4509460.6.9009. 44911.4671. 50541711.3. 2407

495.0.4940. 0000.1656.1)903.7970.1317.0209.0630.0627. 57,06.9311

Hf.MI);,2

.0245

.1049

.1123

. 1 063

. 0052

. 0006

.2.18.1

.0071

.0235

.027.0

.0137

.237.11 .061.0366.0155.0442.3131.0130.1116. 1164

5.046

DW

.0065

.1907

.0095

.0005. 0004.0003.2200.00111.00.12.0001.0025.1001.0927.2130.0010.0013.0223. 0006.0000.0074.0075.0157.0045.0030.0000

K:3M01.3

.0245

.1049

. 1.070

.1071

.0053

.0007

.2226

.0076

.0247

.07.35

.0137

.23001 . 066 ..0426.0156.0435.3092.0140.1151..1.137. 141

Analysis fleport. Avu.r<iK»n<

»

2.122232425

It

.1234H671!9

.101.1.12.13.14I S1.6171819207\}.?.232.425

.V123/i567(19

10111 2j 314I S16

K.ltsmonU

.'iol960

.'lu.1899T 13349V 2924Zn?..138

Kl onion t-

Ar,32BOA 13 9 6.1An .1936B 2497n,>49341V)3.K)0Crt3.1 79(M226S(!o2206Oi-2677Cu3247Ko2!i99K 7664M«2790Mii257fiMo2020N.15I195N 123 16Pb2203ib2068«•) 960i l l l B 9 9Pi 33497 2924/ H 2 1 3 B

Klomuiil:

Ar,3280A] 396]A.s193611 2497(Vi493411031300,13179(;d2268C»2286Ci-2677Ou3247fr'o2599K 7(164MR2790Hi 1 2 5 7 6Md2020

Cr.OBPA

V •.2134.2028..1105.0617.J056

.. R5MDr'<t

.0222

. 1005

.0971

.1053

.0049

.0006

.2144

.0061

.02.25

.022.0

.0125

.2.35.11.016.0349.0153.0430.29110.0096.0972. 1 1 06. 1044.2135.0100.0117.0200

cr.M/OCIlK

;Vio*6j ifarjjino •r, 8386 v";-847J 'J.O74 ".107711.02. 1 1 59.2280.3377.32611.1064. 1.2610.fi!).3.144.27112

CSCKIH

. 1 1 1 9

. 1060

.046.1

.0341

.0570

Rsatm.5

.0240

.1075

.1.104

. 1067

.0055

.0006

.2233

.0070

.0253

.0244

.0.143

.2302.1 .065.0433.0150.0435.3167.0136.110].1.171.1305.2227.0.12.0.OJ36.0206

DW

76014. --.0071

.0000,,0033-.0001. 0002

.0167.0010.0004.001.1

.0007

.0006

. 0000.0112

.0005.0009

DW

.0040.01.52.0040

.0010.0004

RfiMW.6

.0231

. 1014

.10.15

.1041

.0049

.0006

.2130

.0067

.0232

.02] 3

.0131

.23441 .035.0301.0153. 0424. 3020.0.109. .1 090.1087.1005.2106.0107.0.1)9.0278

<^*Bttatt

.09342 . 480.4906.52301.036.10361.0.21. 1 061.2142.31.74. 30641 . 0663.6799.934.3141.2602

l''.r.i 10 .2

K!lMm..l

..1070

. 2245

.0.1.1.1

.011.2

.02113

KilMlH.7

.02.32

.0956

. 1034

.1042

.0049

.0006

.2147

.0067

.023.1

.0224

.0125

.2.3461.007.-0262.0153.0423.3067.012].0991.1051.0972.2.140.0113.OJ21.0283

""......

.002.7

. 0048

.0089

.0043

. 0002

.000.1.-.0.131.0003.002.1.0014.0013.0012.0374

.0070.0007.00.12

/ 09 0 0 : 2 9 : 2 9 AM

HHHIM-2

.1201

.22.42

.01.1.4

.0130

.0203

DW

.0023. 0040

.0063

. 002.7.0009

.0001.022.1

. 0000

.0006

. 0004

.0014

. 0003

.041.7.0144

.0005

. 0000

.0153

.0010.00.1.1

.0055

. 0 1 00. O J 0 7.0044

.0019. 0007

Rf.070052

.005.1. 0040

.0095.015.)

. 0004

.000].0230

.0017

.0001

.001 1

.0033.0016

.1770

.0] 10

.01)00. 00 1 6

WiMDLL'

. 1.242

.22.1 1

.0.116-

.0134

.0200

CBIUJC

.0004

.0035.0051.0039.0007.0001

.0599. 0002

.001.1

. 0002.0006.0014.0731.0212.000.1.

. 0004. 0066

. 0007.0026

.0010

.0022.0004.0032.0007.0001

KKJIWW

.04531 .9101.066.03042.00.1..0530.10.78.0535.8326. 2069.2569.1 .00719.3410.8.1. 5206

.0001 142

c

Xl l^^— -• -SI X. N;.O.^,G,SX; = > -< iu ; : c iO^ — a o y. ^: 3* v. x; cr» \i N

OC- • CO* - ^ •^ - C C O O C O C S V

- vc x o cj •< tr- c*. x •*< c n

c o o - o • o- oc- cCCCOCCCCO-— CCMO'— C — COO*-COi-U>*••„•» oo^cs!oc^*-^-{-j

3E p -_,c •_ o - •_ o — •_ o •_ -_ o -_ o •_ •_ c •2i

o- b- • • • • o- • • • boo - • c •' • •'— b b •o c c c c o o c c s c c c c o o o o o y - c c ^ - c c :MJfc-tT. C C i O f f * C W t - O C £ C » O ! O H - O O \ C C C l

r: - o- - o o - o oa» c o o o ' — o o o * -•-* o i- o o •— -j» o ^ cr\\c o cr* •-; u» ;-* ci o •?• o

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Ana.lva.in Rupert. AvoraROS Kr.l 30 27 i!9 011:29:2!') AMi

» Kloniont RSCA.I374 K3CA137!! R.'ICA 1 ;ii!2 DW CIMILK CKHTOOIIK

9 Co228610 C.i-7.677.1.1 OU37.47.12 Fn2K9933 K 76641ft MK2790.15 MU2576Hi Mo?.020.17 N,iSll95.IB N.17.3.1619 )>b22037.0 :il>206H21 ;>«196072 Un.111997.3 T.i':)3ft97ft V 292f t25 X i ) 7 1 3 H

It KloilK.Mlt.

1 A ' I 7 H O2 A] 39633 Aa1936ft 11 7497!i n*49346 tto31307 Ori.11 798 Oil 2 2 659 0<)22R6

10 0.1-26771 1 Oii3747.17. LWS9913 K 76fi43f t M«2790.15 Mi>2!'>7616 Mo202017 NaS89S11) N.i7.33A.19 Pl.7.20320 :;i>7.ofii)71 Sul 96072 :;iill)997;) T.i33497ft V 292425 7i»21 30

II Kl . .m.M>l

1 ft - 1 7 1 )2 A.f.19613 AD.193Cft 1) 7497

-.0008.0046.0023.0253.7554f t 3 . 0 7.0050.000ft3.323.0003

.0040. 0060- .0104-.007.7.0076.0096.0.1 12

nw

.0025

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.0003

.0626

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c cDUMP OF METALS BATCH FILE BQF70S1A.METALS TUE. OCT 17. 1119. 2:41 PH PAGE 1

Sttndird Kigrtillon Dili Detection Limit Blink Dili

ElMMnt Cort . Co«l( Slop* InUropt Until Blink M»n Std. Dtv. MDL

AS O.IIM3 111.4 0.220 ug/1 -1.00 -1.00 10.0

SE O.IMM 211.2 -0.1)7 «9/l -1.00 -1.00 5.00PB 0 «9»IS 17S.9 -0.131 yg/1 -1.00 -1.00 S.OO

c cDUMP or METALS BATCH FILE BQf70SIA.METALS TUE. OCT 17. 1999. 2:4* PM PAOC a

lull 111 and Continuing Calibration Verification and Callb Blank Data •••

EUnwnt: AS •9/1 Eltawnt: SC Unltt: U9/1

Poiltlon Sufi* Calculate1 SXBU 0.2202341112143(1034

SASISTRASBSISTIISCSISTRCCSSISTBOCSCRACSSTRCONCSFNLABCSSTRCONCBBLKCBBLK

!.I44.:!57.9S.1230. S1110.2200.402

E»p<cUd0

10.020.040.0«0 010.030.030.030.0-1.00-1.00

X Roc91.491.110096. SSI. 210210110S

-22.0-40.2

Position Stmfl, Calcglattd1 SXBLK -0.1(71

111214361034

SASISTRASBSISTXBSCSISTHCCSSISTRDCSCHACSSTICONCSFNLABCSSTRCONCBBLKCBBLK

10. (19. S40.151.15.2031.130.131.1

-0.1(7-0.7(3

E«p«et.d10.020.040.0(0.05.0030.030.030.0-1.00-1. 00

X Roc

10697. (fOO

•id104103104

18 778 3

Eloaxnt: PB Until: «J/1

Poaltlon SMDK CalolatodSXBIK -0.311SASISTRASBSISTRBSCSISTRCCSSISTRDCSCRA

12 CSSTRCON14 CSFNLAB3( CSSTRCON10 CBBLK34 CBBLK

10.220.339.153.54.4430.530.930.5-1. 01-1.01

E«poctod0

10.020.040.0(0.05.0030.030.030.0-1.00-1.00

X «ac10210199.599.291.9102102102101101

cnoo

segress.on analysis Degree: 1Data f i l e : P7051A started on 101399 at 134722Eiement As

Sta pointsRepi Repe Aver

It ABS ABS - • ABS

1 0 001 -0.000 0.0002 0.033 0.054 0.0333 0.107 0.110 0.1084 0.2SO 0.220 0.220

Coeff 1 « 0 220156.;oef f 2 • 181 . 41463*Coeff of correlation (1st aegree) ;

Repi Rep2PJS

5-1

.^"--,3

•f;,

"••'.•

. ;

.

.;

' 3• 31 4• A• «

.._

;'

• ?\ 1;si •)1920ao

*«J1 a;

Name

B i ankCiSlSTSD

ZSCSA~5CRA;BBLK .

IviTFCON"s5TP'-C'N-iFN.AB15FNI.AB

- =• j~'jQI1. • i --BF\U, . . - BF U- .•;- joi i- »;-: •:; i•<T':» • 37 :F;:J < -.71

• i ' FBF*.•ili • J71;;.:» -:-7i= ;.;-! :-73Kj'IA t 574= i-: A 1373Ri-CA 1373;SBLKCBBUKCSSTRCONC3STRCON

-ess -in ana

ABS

-0.0030000000000000000000000003000o0o0

iy-5.a f • • « P703 1 A

316.412.0271410021 131082681662630031 14212317301: 163031 132133220031 130021 14014124344438.002. 112172278

3

ABS

-00.00 .0 .-000.000000000000000000000-0o.0.0.

Degreestarteo on

.002321410027133.0021 141062711642630021 142133190011 160011 152123210011 13003107014124346444.0001 12173377

! 1

101289

CONC ( ug / I )

0.0010.0020 .0040.00

0 . 999927

AverABS

-000.0 ,0,0.000O000.00.00000000.00.0.0.0.00.0.0.0.

at 1

.00231841 10271330001 131672691652670021 142133180011 160021 142133210021 140021 100141243434410011 12173278

34722

RSta Dev

29.31 .20.20.22.9904.40 41 . 00. 91 00.727.20 40.30. 323 20.277 61 . 31 00 344 91 . 149 04.3030.50 .30.9167 .7021 .302

Caic coneug/ i

-037745

25020304930480203837.0

2102038.380.200.20.2.22.62.80.0203130

. 143

. 910

.782 n.rec«

. 1 18

.233 %rec«

. 220

. 720 y ec-

. S17./

.021 nrec-

. 1S4W<5S8 %rec-.S33\X.902 %rec-862f'910 %rec»402 <X"294 %rec«583 -902 %rec«862434 tree-583 i/9O2 %rec>383 </174 -yec-760 \/716 %rec-808 *^.224 i.rec-.402.539 %rec-603/.634 %rec-

/i r r\

84. 3i

100 69

102. 5C

02 32

92 33

101.39

93 24

104. 31

101 . 39

97.96

101 . 39

97.96

99.78

87.08

100.69

93.24

159AuerABS

Regression analysis Degree 1Data f i l e : p70stA started on 101289 at 134722Element Se

sta pointsRepi Rep2

* ABS ABS -._.

1 -0 . 00 1 0 001i 0.035 0.0343 0.044 0,0474 0135 0.135

COOff 1 " -0 147010

AverABS

-0 0000.0340.0440. 135

COOff 2 • 293, 177381coeff of correlation (1st aegree) :

RepiPos Name ABS

' 1 Blank o ooo5 CSS I STRO 0.1*45 CSSI'sTRO 0.2224 CSCRA 0 . 02O4 CSCRA 0.0517 CBBLK • -0.0007 CBBLK 0.033S CSSTRCON 0 105S CSSTRCON 0 1 349 C3FNLAB 0 1059 CSFNLAB 0 13510 R3Q70051 0 00010 RSQ700S1 ° O3411 » k IFBFW 0 03711 > K IFBFW 0 07012 *SC'700I1 -0.00012 RSO70051 0.03413 RSCA1371 0 002

' 13 RSCA1371 0 03014 f 3 IFBFW 0 03214 I.SIFBFW 0.0591 5 QSCA 1371 0 . 00215 QSCA 1371 0.02914 R3CA1373 0 00113 RSCA1373 O.03217 RSCA1374 0.00117 RSCA1374 0.03113 RSCA1375 -0 0011S RSCA137S 0 02319 CSBLK -0 00219 CBBLK 0.032£0 CSSTRCON 0. 10520 CSSTRCON 0 139

Rep2ABS

o.ooo0 . 1»70 . 2240 .0170 052-0 0010 0330. 1040 1380 1040 1340 0010 0350 0380 0720 OOO0 03"0 0030.0310 0330 04OO.O010 0300 OO10 0340 OOO0 0320 0000.023-0.0020 0340. 1050. 139

CONC cug/ i :

0. 0010.0020.0040.00

0.99944O

AverABS

0.0000. 1»70 2240.0180.052-0.0000.0330. 10S0. 1370 1040. 1340.0010.0340 0380.0710.000O.034O 0020 0310 0330 059O.OO20.030O.OO1O.O330 0000.032-0 0010.023-0 0020.0330. 1090 139

t

Rsta oev

44.70.41 3941 .8113.10. 40.70.70.70.4124 . 53. 12. 11 .7198 31 .037.02.7381 .250.83.210.03.889. 13.6155.82. 116.74.90.30. 3

:efs;r s r r ";*,;,., « 13.7,,E i ement PO

sta po i n t sRepi Rep2 Aver ..... . - •

Ca i c coneug/ i

-0. 14758.57444 425 Xrec-5.20015. 338 v.rec--0 . 1479.473 xrec-

31 . 142V40. 483 xrec-30 343 I--"40.385 %rec-0.131 L--*9.971 %rec-

1 1 144 1^-21 004 %rec--0 147t---10. 547 %rec>0 429 i --9.074 %rec-».473u/17.425 urec-0.429 ^8.778 xrec-0 131 l*S9 473 xrec--0 147|/9.375 xrec--0 4451--4.491 xrec--0.7439.473 xrec-

31 . 142''41 .280 Xrec-

160

30 51

101 .33

94.73

95 42

9S 42

98 40

99 40

101 87

84 47

77 S3

83 49

95 42

J3 71

44 41

94 73

101 38

19 CBBLK1* CBBLK£0 CSSTRCON20 CSSTRCON

-0 0020 .0320 1050. 139

-0.0020 .0340. 1050 . 139

-0 00.20 .0330 . 1050 139

16. 74.90 .30. 3

-0.ioJ9.873 %rec-

41.280 %rec- 101.38

Regression analysis Degree: 1Data f i l e : P7051A startea on 101289 at 134722Element• PO

sta pointsRepi Reps Aver

* ABS ABS ABS

1 0.004 0.001 0.0032 0.063 • 0.063 0 0633 0.121 0. 120 0. 1204 0.231 0.231 0.231

Coeff 1 - -0.838972Coeff 2 • 175.913396Coeff of correlation list aegree) :

Repi Rep2POS Name

1S56077SS9910101 11 1121 213131414151516161717181819192020

Blank •CSSISTRDCSSISTRDCSCRACSCRACBBLKCBBLKCSSTRCONCSSTRCONCSFNLABCSFNLABRSO7005 1RSO700S1> 1. iFBFWl.K IFBFWRSQ700S1RSQ70051RSCA137 1RSCA1371KS IFBFWhS iFBFWOSCA1371OSCA 1 37 1RSCA1373RSCA1373RSCA1374 'RSCM374RSC-137!RSCA137SCBBLKCBBLKCSSTRCONCSSTRCON

ABS

00.0.0.00 .0.00.0.00 .000-0000.00.000.0.o0 .00 .-00 .00.

00130735103008900005917823018O233002064125178OOO062007067124178009067000OS»ooe063005061002054178227

ABS

0.0.0.0.0.

002311356029087

-0.00100.0000 .0.00.00 .00o0.0.o.0 .0.0o.00.-0000

oeo179228179231003063121177000061007068125177008067002ose007062005061.001055177229

CONC (ug/ I >

O.OO10.0020.0040.00

0.99984S

AverABS

0O.0.0.0.

002309354030088

-0.0010.00.0.0.000.00.000000000.000.0-0000

059178229179232002064123177000061O07067124177008067001059006063005061001055178228

Caic coneRSta Dev ug/ I

32. 31 .00.8091 .7154.51 .60 30 70.40 . 547. 11 .02 20 6141 .81 . 44 3060.60.05.80 1104 01 715. 11 . 02. 10766 91 .20606

-0S361414- 193039303*-0102030-090102030010-09010b9

- 183039

. 487

.518434 %rec-.438.641 v.rec-. 01S. 540 •krec-.474.X. 445 %rec-650f'.973 irec-. 487 i^.416 v.rec-79Sf"'298 'Aree-.839 .892 %rec-. 39c \*S"447 %rec-.974 I/".298 %rec-568v/$47 urec-eesw^"540 %rec-217 iX244 rurec-04 H/892 V.rec-.015836 %rec-474 «/2«* %rec«

79

102

95

39

?>3

104

94

98

-.05

93

103

95

100

98

88

S7

. 16

03

40

.72

23

. 1*

. 99

.92

55

.23

7»

. 40

37

51

36

96

161

TITLE-Pro|«et No,_

_ BookNo..

From P«g» No._

O-

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Mr"

CAMft. . - —\S-__-—Jfe

To Pago No.-

Wltnntod 4 Understood by m«, I DIM llnvontod by

c cDUMP Of METALS BATCH FILE BQF70S1E.METALS TUE. OCT 17. 1(1*. 2:46 PM PAGE 1

St.nd.rd H.gr.tll.ll Dill D.t.ctlon Ll«lt Slink Dili

Elm*! C»ri. C»«ff. Slop. lnl.rc.pt U.llt BlHk M..K Std. D.v. MDL

AS O.IM73 215 « -0.201 «9/l -1.00 -1.00 10.0

SE O.illtl 3(1.S 0.000763 ug/1 -1.00 -1.00 5.00

PB O.tBM* 2SI.7 -0.671 iig/1 -1.00 -1.00 5.00

0\

c cDUMP Of NCTALS BATCH Hit 80f70Ht .METAL* TU1. OCT IT. Ill*, »i4( PM

Initial Mt Continuing Calibration Virlflcatlon and Callb. Blink Dili ••*

Fltawnl: AS Unlit: •*/! »••»<: SE Unitl: ug/1

Poll! Ion1| •

I1123*1034

Petition234It123*1034

Saenle CalculatedSXBlK 0.441SASISTRASBSISTRBSCSISTRCCSSISTRDCSCRACSSTRCONCSSTRCONCBBLK 0CBBLK

Clement: PB

Jo'lft!30.*30.2

.00(51-0.422

Eipoctod0

10.020.040.0eo o10.030.030.0-1.00-l.OO

X Roc95.199 410011.741. t103101

-0.15142.2

Petition Sample Calculated1 SXBLK 0.0007(3234«1123(1034

SASISTRASBSISTRBSCSISTRCCSSISTRDCSCRACSSTRCONCSSTRCONCBBLK 0CBBLK

1.9020.239.959.05.5031.530.1

.0007(30.3*7

Enpoctod X Rec0

10.020.040.010.05.0030.030.0-1.00-1.00

tt.O10199.1

•it105100

-0.07*3-3*. 7

Unlit: UJ/1

Saaole CalculatedSXBlK -0.1S4SASISTRASBSISTRBSCSISTRCCSSISTROCSCRACSSTRCONCSSTRCONCBBLKCBBLK

10.220.03*.*51.34.7*31.431.1

-0 (71-O'.(71

*p*co*10.020.040.0(0.0'5.0030.030.0-1.00-1.00

x Roc10210099.117.215.2105101•7.117.1

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O C O O I >• >- i tn <- • o c o ' 0' rtm cr- c- i -i-> o ru iu

o c o o o-* o o o oo OB r-j c- ^ *<• ro c« o *> •

' O C C' C O C' O C- C- C I I * >- - . - . . - O I 0 ' <

c- c -• - c> <.< c- o r« rn < o* »- *• C- *.•* f" *• O C- h' '." t'.' C- I -

"

O C' O C O •

- o o o o «o 9> M c- r-i •et ru c- - ci •

c- c r- ^• c -o. -i

. * r- * •.- c »•• - - c-

f - •: - -c- -i - -i -*• w *•• i o - - r- o i c -i •

. -i _. o - c- r - • c - f i-. r o r-- j. i

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36Project No._

Book No._ TITLE.

From Pigt No._

w-

As. TL

_ ^. v/

__ 163- .--—-To Pig« No..

Witnened » Underttood by me, I Oil* I Invented by Date

lR*eerd»d bv

c cDUMP OF METALS BATCH FILE BQF70S1B.METALS TUE. OCT IT. lilt. 2:41 PM PAQE 1

Slodtrd H.jr.nlon Dili D.t.ctlon limit Blink D»t>

El.MUt Corr Ce.tf. SUp« Inl.rc.pl Unltl Blink H«» Sld. D.y. MDL

TL • O.MN2 321.1 -0.310 uj/1 -1.00 -1.00 10.0

O\VO

c cDUMP Of MTALI BATCH FILf BQF70S1B.METAL! TUE. OCT 17, !••*, 2:47 PM

••• InltUl and Continuing Cillbtillon Verification and Callb. Blank Data

CUxnl: TL U.lll gg/1

Position Sn»l« Calculated Ei»«ct«4 X l«c1 SXBlK -0.310 02 SASISIIA 10.1 10.0 1013 SBSISTRB 20.« 20.0 1034 SCSISTBC M.( 40.0 11.1

CSSISTUD 52.4 10.0 17.44.1s4.12 CSSTRCON 27.2 30.0 »0 6

14 CSFNLAB 27.1 30.0 (2.131 CSSTRCON 27.1 30.0 »2 I10 CBBLK -0.70* -1.00 70.134 CBBLK . -0.310 -1.00 31.0

Regression analysis Degree. 1Data f i l e : P70S1S Started on 101389 at 040330clement Ti

sta pointsRepi Rep'2

* ABS ABS

1 -0 00 1 0 . 0002 0 032 0 0323 0.044 0.0654 0.121 0. 123

Coeff 1 • -0 380401Coeff 2 « 328 080758Coeff of correlation (1st

RepiPos Name ABS

,i556677839910101 11 1•21213i ;1414AS15141 •}1 7171313191920SO

BianKCSS 1 STROCSS 1 STROCSCRACSCRACBBLKCBBLKCSSTRCONCSSTRCONCSFNLA8CSFNLABRSQ700S1RSO700S1KR IF8FW«:K IFBFWr.iC.70031RSC70051RSCA 1371RSCA 1371t. 3iF5FWKSiFBFWQSCA1371OSCA1371RSCA 1373RSCA 1373Si.:A1374RSCA 1 574RSCA 1375RSCA 1375CBBtKCBBLI>CSSTRCONCSSTRCON

00000-00000000000-00000000000-000

000. 161.201015

. 0690.000.054085

. 131087

. 131001057144

.191

. 000

. 0610 000060153204001059.OOO057001.0580020540 000059.035. 129

AverABS

-0. 0000. 0320 0440. 122

degree) :

Rep2ABS

00 .0 .0.0.-00 .00.000000-00 .-00000.0.-000.0.00.0000 .

000161198014046.002056033129085135000056148139.001061000059154202002060.00006000105«001056000059036131

CONC <ug/ i )

0. 0010.0020 . 0040.00

0 999620

AverABS RSta Dev

o.ooo0.1610 2000.0150.068-0 0010.0550 0840 . 1300.0860. 1330.0010.0560. 1460 190-0.0000.061-0 0000.0600. 1560.2030.0020.0600.0000 0590 0010 0590 0010.055-0 0000 .0590 0860 130

24.40 11 .04.53 2125 32.71 .81 . 11 .420115.71 .01 . 70.6267.40 . 370.00.52.00. 532.41 . 2756 64232.7044O 61 .7231 9030 .71 . 1

caic coneug/ i

-052654

21-017.2742.2743-0174741 .-0.1*-0.19SO66.0 .19.-0.13-018-017-0182742

.380

. 441

.236

.541

.929

. 70S664

. 1732708352S4052992512255

%rec«

Urec-

%rec»,__,%rec-i_Mrec-iMrec«i— -%rec-

63. ia

36. 44

88. 32

75 .46

77 . lO

S9.96

72. 13380 L--43338030480022027*l304

•/.rec-^%rec-l^%rec«L--

*rec«

98 . 1 «

96. 52

77 1C

95. 14380 (X976

976052.664. 380.976. 335270

t,rec*^^%rec-Lv.rec»

•urec-IX"v.rec«

94 .83

94. 33

38 32

94.83

72 IS

171

*h Project No._TITLE SHOPS'!______________________ Book No..

From P«9« No —

Sea-.

TV

PrrArrilor

o-\>_________U--y^_________\^-

_ Cft\%^ __.CAS9!i_._._.

Crartkid____v^____iX

_——._..——:_... 172 .

To Pige No._

Wltnessed a Understood by me, I Date (Invented by I Date\ol n(81

cI ""

DUMP OF METALS BATCH FILE BOf 7OS10.METALS TUE. OCT 17. 1119. 2:57 PM MOE 1

Standard (Ugriulon D«n DataclUn Halt Blank Data

Elanwnt C»rr. C»«ll. Slop* Inttropl Until Blank Mtan Std D«v MDL

TL 0 MIJI 371.I -0.167 ug/1 -1.00 -1.00 10.0

cDUMP Of MTALS BATCH FILE BQfJOMQ.METALS TUE. QCT 17. lilt. 2:57 PM

••• Initial and Continuing Calibration Vtrificatlon and Calib. Blank Data

CloMnt: TL Uniti: u|/l

Position Smelt C>lc«Ut«d1 SXBLK -0.1102341112361034

SASISTIA. SBS1STKB

SCSISTICCSSISTtDCSCIACSSTICONCSSTICONCBBLKCBBLK

10.*21.031.35S.35 0427.730.0

-O.S3I-O.U7

E>p«ct«40

10.020.040.010.010.030.030.0

-1.00-1.00

X R*c10610SII. 112.1SO. 4•2.4•I.IS3.I11.7

Regression analysis Degree: 1Oata f i l e : P70!1O started on 101439 at 130417Element: TI

std pointsRepi Rep2

* AB3 ABS

1 -0 003 -0.0012 0.030 0.0293 0.040 0 0334 0 . 104 0 . 10S

COOf f t - -0. 146334COOf f 2 - 371 . S27042Coeff of correlation (1st

RepiPOS

i356«77839910101 11 1121213131414131514t<51717181819192020

Name

B lanxCSS 1 STRCCSSISTRDCSCRACSCRACBBLKCBBLKCSSTRCONCSSTRCONR3CA1332RSCA1382RSCA1 37 JFSCA1376RSCA1377RSCA1377RSCA1378R5CA1378R-3CA1372RSCA1372RSCA1379R3CA1379R3CA1380R3CA1380RSCA1381R-3CA1381R3CA1893RSCA1893RSCA1394RSCA1394CSELKCBBLKCSSTRCONCSSTRCON

ABS

0 0010 1490. 1970.0140. 071-0 .0020 0380.0770. 123-0.0000 . 0340 0040 048-0 .0010 048-0 . 0000 043-0.0000 0520 0010 033O.OOO0. 033-0.0010 0310 0010 033-0 0000 0330 000o ose0 0810 123

AverASS

-0 0020.029

. 0.0370. 106

degree)

Rep£ABS

0 0030. 1490. 19S0.0140 0690 .0000.0370.0730 1240 0000 034-0 0000 049-0. 0010 0510.0000 0520 0010.0500.0010.051-0.0000.032-0.0010.031-0.0010.0320.001O.OS1-O 0010 OS7O.0820 131

CONC (ug/ i >

O 0010.0020 0040.00

0.998381

AverABS

0 .0.000-0000.-00.00.-00-000.0.0.0.-00.-00.0.000-0000.

002149197014070001037075124000034002048.001030.OOO030001OS1001033.000032001

031000034000032.000ose081129

RStd Dev

41.9 '0. 10.31 .62.2143 81 .83.81 . 2214.30.9173. 1O S44.34 2396 46 1149 43 30.85.4692 60.33. 4o.e463 13.6318.52.3327. «1 . 40 71 . 3

Caic coneug.' i

03573323-0212743-019017-018-018018019-019.-018-019-019-0202947

. 377

.251103.040.348538.033. 723.952. 167918.577686

. 533430

. 167

. 430203802.205346

. 167

. 174

%rec»

%rec«

%rec«U-" '%rec«U—%rec«

i_ -%rec»\_—%rec«u—%rec-C--%rec-

>_-'•urec-Li.rec»

39

104

105

91

90

35

92.

92

92.

94

95

. 24

. 14

17

12

39

54

13

13

98

70

87538 ,8021J7918

. 167

. 174

. 167661960

. 812

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rtrec-I/xrec"

94.

Si

93

103

89

01

59

87

31

24

175

cHETAIS OC DATAi DUPLICATE/SI «IAl. DIL/BLANK/MATP.IX SPIKE INFODHATION TUE, OCT IT. 1(19, 1:2( PM PAGE

Bitek F1U : BQF7051B Job Id : 070051 Sequence Pol I : 41 Units : ug/1 Spiking Lot Id : IFBPU

Blink/Hitrl» Spike Intorutlon

EltMnt Poi Spiked Uniplked Added X RecoveryTL II 47.S 0 50.0 (5.0

c cMTAL* 00 OATAI DUPIIOATE/UHIAI DIl/BlANX/MATRIX SPIKI INFOKMATIOH TUE, OCT IT. llll. till PM PAOC J

B«tck F1U : BQT70S1A Job 14 : CA1371 S.qu.nct Pol I : 44 Unltt : uj/1 Splkinf Lot Id : IFBPU

Blank/Hitrl< Splk« IntorKitIon

CloiMCil Pol Splk<d Uniplkod Addod X KocovtryAS 24 91.I .5(3 40.0 (S.ISE 24 » «7 .421 10.0 (2.4PB 24 21.0 .3*2 20.0 103

CD

c cMETALS OC DATA: DUPLICATE/SERIAL DIL/BLANK/MATKIX SPIKE INFORMATION TUE. OCT 17. Itll, 3:2« PM PAOE

Bit CD f 11. : 8QF70S1A JOB III : CA1371 Soo.u«nct Pol • : 45 Unlit : nj/l

Dypltot* I«f«ra»tlen

ElOMnt Pol Stmf.lt l(pliciU IPDAS 21 .513 .513 0SE 21 \42I .42t 0PS 21 .3*2 .5*1 31.1167

\O

cMTALS OC DATA: DUPLICATE/SERIAL DIL/BLANK/MATIIIX SPIKE INFWMATION TUC. OCT 17. 1119. 3:2* PM PAGE 2

Bllcb Flit : BQF70S1B Job Id : CA1371 S«qu«oc« Pot I : 44 Unlit : 119/1 Spiking Lot Id : IFBPW

Bl»k/M>lrt> SpU< Infomtlloil

EloMiil Poi Splkttf Uniplktd Addod X locovoryTl 24 SO.I 0 50.0 102

COO

C (MTALt QC DATAl OUPLICATf/UIIIAI. DIL/flANK/MATIlIX SPIKf INFOftHATlOM TUE. OCT IT. Ill*, 1 III PM PAGE 3

••Ick Fllo : MF705U Job Id : CA1371 Soqoonco Pot I : 45 Unlli : yj/1

Oupllcatt Information

EltMiil Pol S»vl> lopllcalo "TOTL 21 -.310 .271 -1211.54

ETC

METALS SUBSIDIARY DATA - MERCURY

182

Project No.__ Book No..

Pig* No._

o-s.\ -o

10-O v

-A\

-a.

FA301S

C.AV3SI-I .

183To Pag* No. ——

tn*»*d * Understood by m*, Dat* Invented by

R*cord*dby ^_. x-SflW

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SI ootr i

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Commands /£

Degree of equation: 2

Y-!ntsrcept: -.eiH8

Degree I Coefficient; .85675Degree 2 Coefficient: ,9ee36Coefficient of Correlation: .99378

Intersection (enter /E uhen done>.....

X - :BY • I.71Bx • ::.sY - 1.45B« - 15Y - .322x • i .eY - ,B4Sx - eY • -.ei iX - 1.5Y - .e?sx - s.sY - .312X - 22.5Y - I.45tX - I .eY - ,e«6x • 15.5Y - .956X • 21.5Y • :.377X - 22Y • I.413

167

xttrii kttriioe nii« oe ••!>« i»i>e «»!»• i»u<•——J**—— LO/00 >—•;

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188

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CYANIDE DATA

197

7C

i~)Jfo$ «^ro

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198

Data:

CLP CYANIDE LOG

Analyst:

Batch: Paga:_(_of

Cup ETC IDWT/vol

InitrCone. Oil.

LiquidX (0.5)

Soil W«t Wt.X (.251/wt %R %Solid

FinalCone-

PSB

,3001004

/J'O ICC. I l-S'CIcl

So

/ OP. (a

COftSti

a oolctt.5

S'Q.fe106.8

'0

'76iJ/arr l.aS.tt

lou lol.l 10)proa s'.os

O.I?

199

Data:

CLP CYANIDE LOG

Analyst : _

Batch: Page; o? of /

11Cup # ETC IDWT/ f ln»trVol Cone. Oil.

LiquidX ( 0 . 5 )

soil w«t wt.X ( .25)/Wt %R %Solid

FinalCone-

O.cR o.o?27 0.33 0-31

Cft evil° 0.33

0.18X

3399.5

35 •r-610 0.0(0W-1370

x 0. II37 o.os' x

37o Quf • 1C 0,01

31 "73yo .57 ft.O? $*>V/ ft*

•w 0-0? fi.clya 33 n.ol "77 o.os

ttrt- O.Ob'

jbi C.6/5 :a2al££k

X cni*200

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Batch:

CLP CYANIDE LOG

Analyst:

Page»:s3_ofj£_

Cup I ETC IDWT/vol

InstrCone. Oil.

Liquidx (0.5)

Soil w«t wt.x (.25)/wt %R tSolid

FinalConc-

SCO

Cff 600/n&o

1573 500

X

DfiL1.63

0,1357 X

>o3ScDmio 1-5SOD

a.n Xi.te

i¥rt

X(,8 0.09-

X

73.

201

^

'w

Data:

Batch

Cup *737i75I \0

CLP CVANIDE LOG

lb'S-$i Analyst: W//0^x2-fl^

; q^QO"7?

ETC ID

f*^V

LOW*

C.CJ3

<LCA/

WT/VolSOD

///

to/f?/9InctrCone.

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Page: 7 of 7

Dil.////

Liquidx ( O . S )

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202

Data:

Batch:

CLP CYANIDE LOG

Analyst; (ij

Page: / of

arco VojrV

^fr/•//?/»

Cup ETC IDWT/Vol

InstrCone. Oil.

Liquidx (0.5L

Soil W«t Wt.x (.25)/wt %R %Solid

FinalCone-

Joo z;oo-sz Mi. IOD

I0

zleuaco

uailol.b IOI.D l o l

z ZI if mi, z z

SCO

600' z111 600 Z

203

V

Pat.:

CLP CYANIDE LOG

Analyst: M llrt1&£JL*U

Batch : Page: 8. of O

Cup « ETC IDWT/Vol

InstrCone. Oil.

LiquidX (0 .5)

Soil W«t Wt.X ( .25)/wt %solid

FinalCone-

5^00 X (bU5-00

317 COINS' TOO0.13

I-33

OWf3c> MS 0-3S X

0,31 0-3133 X

o.art35 o.y/t

X37 X lot. SL X3* f.ot ofiff 0-0^ 0-05

OL x ft. Of 13 o-oMs-.o*.

ft. Ifitf 93*>/

ft X o-oEV3 x O-dlyy OW94.H X fo

X O - l ? o-nlo.l O.b"!

X JlH•<&*

5-3 D X204

QTCO Very

Date:_

Batch:

CLP CYANIDE LOG

Analyst:__(^

MLPage; J"? of

CUP * ETC IDWT/VOl

InstrCone. Oil.

LiquidX (0.5

Soil Wat Wt.X (.25)/wt %R %Solid

FinalCone-

Of 03

Xifc3.fr X/•3*7 X O.Lfl 0-61

I6 / /0506(1.16 X 1038ioo

IW.G,I*?,*? X

X lA

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. JL X-TI"7-oa .2> C, 20

It* 0-31o.no x0-33

XX

Qfl&JI 0.51iff CW/97J X O.ll

X o.fl

1Lca/G

Xx205

Data;

Batch :f'lfl/M

CLP CYANIDE LOG

Analyst; C

Page: V of J

Cup I ETC IDWT/Vol

InstrCone. Oil..

Liquidx (0.5)

Soil w«t Wt.X ( .25)/Wt %Solid

FinalCone-

a.r75- 'IT. an.

5oo aii.o77 too

300

3.15oo

z.500

aoo

O.ISS

50Q

1..CH(71 IS

3.03 /.r93 a-a

300 JJ_

206

Date:_

Batch:

CLP CYANIDE LOG

Analyst! Lf

Page: _^_o t Q

Cup *

O

'W

/o3

1*1

ETC ID

CX16

cat/

WT/Vol

X

X

Xx

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LSI

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X

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Soil Wat Wt.x ( .25)/wt

X\lt).3

X£3

%SolidFinalCone-

ictti.r\*

207

T-'oi nt skip is 4; can save 16 hours'.

Poi nt skip is 4t can save 16 hours.

Point skip is 4; can save 16 hours.

Point sl:ip is 4; can save 16 hours.O +

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34 SBPL 27 1.02- B-

37 SBPL 2B - .1*6 Br

38 SBPL 29 - .211 B-

39 SBPL 30 .459 B-

40 3BPL 31 .179 B-

41 SBPL 32 .114 B-

42 SKPL 33 - .144 B-

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DIGESTION LOGS

215

SAMPLE PREPARATION LOG - METALS

BATCH

SAMPLEDUMBER

FLAMEINITIAL .

/ICAPFINAL

FURNAN:EINITIAL FINAL MERC TRYINITAL FINAL

/ 0

CAI2H:

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ETC IFB / TSK* - ICP SPIKE - WATERS

Batch # __(3./

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IFBICPA

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10 ppm

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IFB FN B

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CHAIN OF CUSTODY

122

• ^^^ EHVIflONUEHTAL TESTING IM CERTIFICATION Seal No. Q/^~777j ETC.Inh« CA1371

CHAIN OF CUSTOD Y FORM (CC1) ORIGINAL Date Sealed e9/°8x°1 By: $• d

Company:. PELft

CITY DISPOSALFacility/Site: c/0 HOLIDAY in

Address:. I9OX/EXIT 12 AND IB EAST, MADISON, UI 93704

. 31»0

SAMPLE IDENTIFICATION

Facility: I f P f 1^

| -M- |

Source CoderWW..IW) Ogllall.. (0| SonomSeaiment....{SI Suclece Impoundment... .<l| UKBmCoueMlonSn.... .<Q Oum .Soil...(8) RivefBlreem IR1 Qeneretlon Point ... .(G) Tfeelment Fecllny . . . . . . fT) LehefOceen .............. .(li Speelty

SHUTTLE CONTENTSBOnLE

Me

2

1

2

2

1

Type

UOC

TB

EXT

EX1

MET

am40

40

1000

1000

1000

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NONE

ocxns

none

none

HN03

ANALYSIS

UOLATILES

TRIP BLANK

EXTRBXMS

PSTXPCB

nETALS

SAMPLERnurr/Ni Observations

S

S

S

^

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LABObeonatlont

^

t/ ^

i/ ^

//•

^

CHAIN OF CUSTODY CHRONICLE

1.

2.

3.

4.

Shuttle OpenedAy: (prn0 «^<kja QjucaJSignature: J/î&jC

Date: P -f. f< Time: /-% . j <•^ ^ Seal*: CUSTTT 3 Intact: ^^

I have received these Materials in good condition from the above person.Name: Signature:

Date: Time: Remarks:

1 have received these materials in good condition from the above person.Name: Signature:

0 \


Shuttle Sealed By: (print) /l/ai/lbi/ /jij/XfVSignature- / J4^L T7*\

Date:Seal*

dff//f/09 Time: i~ . — -

LAS USE ONLYE ONLYpMntxl By. .r • T ^

.Time:

ETC FIELD PARAMETER FORM (CC2)• •

ETCJOB* C.A/17/

int liSd LSouTcTcott

FIELD PROCEDURES

SSTttBSg•UMOI OATf(YY MMODl

SAMPLING METHOD: ___________________

| .. i A-Subimrilblt Pump D-Olpwr/Botll.Sampler Type I C- I B-isco E-BIIIW

———' C-Blnuw Pump P-Seoop/3hov«l

Sampler Material \Jt-'

Tubing Material | ft-

Sample Composited I Y/£)

ILUMOMM W.TI.TOLC.llNOTOL^C. VOLUM1PWM.O

C-PolyttnyUntD-Sllicon

FIELD MEASUREMENTS

Depth to Ground water (ft) I I 1 'I JPl I Sample Depth (non-well) (ft)Groundwater Elevation (ft msl) L

1 1 1 1

1st 1st

2nd

|- .

i i \(0\P\5\I I I I I I

I I I I I I I LJi_^J LJ

<ihif

I ' l / t ' l

4th i i

Mb

FIELD COMMENTSSample Appearance:.Weather Condition.: UJAfM________r»H«r M.P. !<. n TuP Of ete/f/C-

llL

FILTERING: Use Chain of Custody (CC1) to indicate which bottlM w»r« flltertMt

Sampler: Employer

I certify that sampling procedures were in accordance with applicable EPA state and corporate protoq^l? 4

The ORIGINAL

ENVIRONMENTAL TESTING tut CERTIFICATION Seal No. 6TC Job #

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Dat<, s. d S-A-M

r-nmp.ny / /TlTT

F.rillty/Rit«. -J)l/nO f4*f}Aim • ^ jVin hjitn

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\t Lfl Lift

i , i , 1 |0|ViVi*l \l£i5\&\ | T-rl1

Source CoOtt:Well .(Wl OuKcll . . (Ol Bottom Stdlmtnt.Soil (S) RtvtiffSlrnm .(R) Otntrchon Pom I .

.<B) SufUC.lmpwjrxjm.nl .(I) LueniiltCollMttonftyt.. ...|Cti Fictllly .... ..<T> Uh«*OcMi>.............. ,HJ

SHUTTLE CONTENTSBOTTLE

No

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Type

t°

V

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Affi

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Aj'fAÂtL flAiA~» A.t

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Observation!

./

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LASObeenatlora


1.

2.

3.

4.

Shuttle Open«(fBy: (prjft Jr

Signature: Jê^ ~&4Date: f t-T-B-V Time: OTiff

r Seal »: £>o<t.i<t » >vo Intact: -Î nave received these materials in good condition from the above person.Name: Signature:


I nave received these materials in good condition from the above person.Name: Signature: 225

Date. Time: Remarks:

Shuttle Sealed By: (print) gj^^, L/IJKfV

Signature:

Date:Seal

MlitlM Tima: /7.'3<?t: Jl)%£>~2> intact: <rfc_.

LAS USE ONLY Opened By:

ETC FIELD PARAMETER FORM (CC2) Form 0008Sampla Management-

08/M

ETC JOB «Sample Point Ifcd i i i I

FIELD PROCEDURES

ssrwssSAMPLING METHOD:

I /) ISampler Type I O I B-ISCO1———' C-Bladder Pump

Sampler Material

Tubing Material _

Sample Composited [_Yj

A-Submerelble Pump D-Dlpper/BottleE-Baller XOiherF-ScoopfSnovelC-PVC0-Plaillc X-otherC-Polyethylene0-Sillcon X-Othei

_ FIELD MEASUREMENTS

Well Elevation (ft/msl) I l/PlPJTl0l well Depth (ft) I I I _____Depth to Ground water (ft) I I I3I01PIVI Sample Depth (non-well) (ft) I I I 1 I IGroundwater Elevation (ft msl) I I? I/ 1° \5\3\

1st J"101 1st

ZndLLMltj •"»

i

3rd I

2nd

3rd I I

4th I I

J I I I I I I I__I

l^l^l

Sample App««f«nc«-weatheroih«r

FIELD COMMENTS

Of

_WMD J-

FILTERING: Ust Chain of Custody (CC1) to indicate which bottlM w»r« <llt»r»d

Sampler: Employer

I certify that sampling procedures were in accordance with applicable EPA state and corporate protocols.

fMlltltt<(*>•>/ 7 ii-flN

I TESTING iMCeRTIFICtTION

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Date SealedSeal No. 0/-S77L7 ETCJ0h» cft1372

89/08/01 -By:.

Company:. PELA DAN GREEN

F.ciH,y/Si,e: g,' ?^ ,,,,M

Address:. I90//EXIT 12 AND 16 EAST, HAD1SON, UI 53704


Facility: L

Sample Point:bu=«i i i i i

Tool Scmpi* 00.nl 10

•» 'Option* MmpM Pwhi OnciipTwmi

l3! \l\*\**\ I l l L<T

Sowrc* Coott:W«II..(W) Oultcil . . . . . .(0) Bottom 5Hlm«nt...(B) SurfM* Impoundmtnt..., |l) LuehM* CoUMUon tyt...Soil <S) RiWSIrtam. .(Bl Ovncntton Point ... .|Q| TrMlmcnt Fielllly . . . . . . (T) t htfOCMn ............

SHUTTLE CONTENTS """""

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..|tl <nclly.

BOTTLENo

2

Type ANALYMSAMPLER

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EXT loot EXTRB/MS

EXT 1000 PSTXPCB

MET 100C HNQ3 METALS'**

t.'t*" A/

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W t/Tee ___________________ IV

CHAIN OF CUSTODY CHRONICLE(ZfrmJ OUt:Shuttle Opened^y: (print)

// A-/Signature: -

g.f-f1 Time:Seal#: OifTi ntact:

1 nave received these materials in good condition from the above person.Name: * , _-._ . . Signature:

Remarks:Date: £>P-e>3-f1 Time: $:el»~.

I have received these materials in good condition from the above person.Name. Signature: O O 7


Shuttle Sealed!Signature: f j£ Seal*: A

Time:Intact:

LAB USE ONLY Opened 8•HUTTUl -

FIELD PARAMETER FORM (CC2) Swnpl* M*niQ«m«ntMM

ETC JOB # __

Sample Point 1 1 I&|W|ft (iSiUmpwtaMt

£l Rl 1 1

FIELD PROCEDURESIl|«-l<a4l I l/Lfl I I 1 i i i /i5l'

«»"«»SAMPLING METHOD:

i . I j A-SubfnSampler Type IVM. uscol-*»* C-BI«M« Pump

Sampler Material

Tubing Material

Sample Composited'

A-Subminltab Pump D-olppwfflottM

F coopanomC.PVCO-PIMtlC

X^thw .

XOtlMf .

X-Oth«l .

Well Elevation (ft/msl)Depth to Ground water (It)Groundwater Elevation (ft msl)

1 1 1 i 1 1

FIELD MEASUREMENTS

I I I I i I I Well Depth (ft) ______I—1—I 2"l6i3|fel sample Depth (non-well) (ft) I I I 1I I I I 1 I I

1st I

2ndL

1st

«„

LJ

\b\k\4\

II MX

INTU

LJ

FIELD COMMENTSSample Appearance:.Weather Conditions:_2u«ui±

MP•2" 4

. f -6 -/STFILTERING: Us* Chain of Custody (CC1)1o indicate which o«l*s w«r* Illterad

I certify that sampling procedures we>^ in accordance with applicable EPA state and corporate protocols.

-rrs-Th.1 ORIGINAL

ENVIRONMENT*!. TSSTINO •/!« C£HTIFIC*TION Seal NO. ETC Job # &A I-31A

CH4/N OF CUSTODY FORM fCCIJ ORIGINAL nataSMi.rt f-J-/9

Company /I-/"17" Alln .; /1/Jjn

Far.ilhy/SI,.- h LLnn f*l*f) Dhnn.- &A^ J ,

Artrtr.,.-

Ry "Vv i '

y?

A7^.f?/J/


Parillly 1 1 1 1 1 1 1 14/IJ iSl \3i

S.mpl. Pnlnl- IjjJ-l 1 if-rt/jpll tflRjEj 1 1 I8tfl(lilfl2lil Ultlfilfi

1inpitorai

I ia51(I'Offl MIOW , (ltd lultilyl (VYIMMfDOl 12400 fir. elott) •WilHa>

Sourct Codes:Will .(W) Oultill . . . . ,(0) Bottom 3*dim«nt ....(8) Surface impoundment... .(I) UMcr»l«Coll«etton9y*.. .-.(C) OUwr . . . . . .


Ne

f

/

1.

2.

3.

4.

LABSHU

Type

•f

f9

Site

,34-fl

^JVfilJ

'•

Preierv.

0

lUvtJ.

ANALYSIS

X/Xu lA AtjJ^naf,

J,,/J»* TA?« '

SAMPLERPHI rnw

fj

A/

Observations

^

S

LABObeenraUene

y/*tf.f/flu)^\/

CHAIN OF CUSTODY CHRONICLEShuttle OpenedJiy: (pri

Signature: -X2^ "^Ci"KJ- G-a^ Date: 8-1-8S Tima: on .s

n — Seal »: 00*1 4 H« ntact: — •I have received these materials in good condition from the above person. /T)Name: (*fA-f-rf»J /LiYirj-SFV Signature: //fc"X y^-^^/f^

Date: t^g /fa* -^ Time: /^^ Remarks: p/tt' ^/ V

I have received these materials In good condition from the above person.Name: Signature:


Shuttle Sealed By: (print) £.(.44^$^ £fn.&s*rt/ D*le: Jj J«v <yf Tlm*: /&<&<?Signature- X&arfJr — ^ "-X«I- Seal* etifSf, Intact: «»£.

USE ONLY OpenTTLS« T/4P -C «A» SEil • JTII. COMB wZ/jA^. ————————

ETC FIELD PARAMETER FORM (CC2) Form 0002Simpu Muugnrwnt

M/M

ETC JOB *Sample Point |U4 I

Sourc* COMI I

FIELD PROCEDURES

W.TMVOLO.l.NO

SAMPLING METHOD:

Sampler TypeI,,/. |X/£"-t— '

A-Sut.m.filbl« Pump D-DlppMBottltB-iscoc-BKdd«r Pump

Sampler Material

Tublnfl Material

Sample Composited

E-BilltfF-Scoop/snovtiC-PVCD-PlullcC-Boly«ihyl.ntD-Slllcon

X-Otllw

X-Otlw

Well Elevation (ft/msl)Depth to Ground water (ft)Groundwater Elevation (ft msl)

FIELD MEASUREMENTSI I I I i I I Well Depth (ft) I I3I3ISLS1I I \Z \fl3 fc» I Sample Depth (non-well) (ft) I I I 1 I II I I I i I I

1st

3rd

1st

2nd

3rd

i iI I J I I I I I I I__I

4thl__LH£L?d»™

FIELD COMMENTS

Weather Conditions:Other.

. 95'- 2$.-Z£-a &-V1' X . IkS^J/ff s AgfeXFILTERING: Us« Chain ol Cuttody (CC1) to Indicate which bottl»»

Sampler J LJtUf&Bl/ Employer


230

. TESTING tna CERTIFICATION ' Saal No, 0 / *^~7 ~7la ^ ETC Job »

CHA/N OF CUSTODY FORM (CCt) ORIGINA. Date Sealed 99x08/01 By: . r - r .

Company:. PELft DAN GREEN

(414) 631 - 3150

&rldfA»- I90^XEXIT 12 AND IB EAST, MADISON, UI 53704


Facility: I f P ? I I I I I I I LFeVClllWSitt CM*

Sample Point:

Source CMM:Will . (W) OulfiM ...Soil (31 NlvtrfSlmm

Tour S*mpM Potfii(Hit lulli(y)

.(0) Bottom Stdimenl.(M) Oenerition Point .

. IB) Surleee impoundmenl.... (I) LeMtwe Colleetlon Sy*.... 4Q - Other .,|Gl Tfeetment Facility . . . . . .{T> Uhe/Oceen ...............flj' <pectty


No Typt Stot PrMmr. ANALYSISSAMPLER

uo* 40 NONE UOUAT 1 LES N/TB 40 GC/MS TRIP BLANK

EX1 1000 EXTRBXnS A/EXT 1000 PST/PCB A/tlEI 1000 HNQ3 METALS

uA/A/ I/

A/CHAIN OF CUSTODY CHRONICLE

Shuttle Opened/py: (prinSignature:

Date: c.j. 0f Timr ^.Seal #AI *r m /. t Intact: 3

1 have received these' materials In good condition from the above person.Name: > Signature:

Date: Tlm«: Remarks:

\ have received these materials in good condition from the above person.Name; slBnalu":Date: Time: Remarks:

rShuttle Sealed By: (print)

Signature: !l/&~j£n

Date: Time:Intact:'

IAB USE ONLY Opened By:.SHUTTLE I .TEMP.'

ETC FIELD PARAMETER FORM (CC2) Form 0002Sample M«n«g«m*nt

OS/M

ETC JOB* P.AIA1.*,

Sample Point Ifi3 l- i * !2!Sotlfc* Cod* tempi*

I I I I

FIELD PROCEDURESI i fid

SAMPLING METHOD:

Sampler Type

Sampler Material | /e,\

A-Submmlblt Pump D-Dlpptr/BottltB.ISCO E-BllltrC-BIKIdw Pump F-Scoop/ShovM

B-M«t«l

Tubinfl Material

Sample Composited \fl(u

C-PVCD-PIMtlc

C-PolyttnylinlD-Slllcon

X-Otrw

X-Otlwr

X-Otlw


FIELD MEASUREMENTSI lfl5U,Ulffl well Depth (ft) I

1st

I I vl 2 | 1 /1 / |

I

Sample Depth (non-well) (ft) I I I I I I

3rd I I

1st

2nd I I•*••.*)•«»<.

3rd I I IHfill

4th 4th | | 1^1812.1

FIELD COMMENTSSample Appearance:Weather Conriiiionii-Other

FILTERING: Use Chain ol Cmtody (CC1) to IndlciU which bottltt w«r« IIIUiwl

Sampler: C2//4-f-7&/V &/V£ysa<____ Employer f^L^————————I Flint) 7 •


t>&&TtwEnvin

^^^^ fHvmONHeNTALTeSTINGinOCePTIflCtTION • Seal No 4jQ-'l't6 ETC Job* tLA131-3

CHAIN OF CUSTODY FORM (CCt) ORIGINAL Date Sealed _£i^£___ By:

Company:

Facility/Site: - fan/in

Address:

Attn.: ~J


Facility:

Sample Point:t: lH-l / !

I. I IMcmtytSil* Ci

\4\6\f\, ,

«ou>» Coo, Si«Ft 0*H ' Sun

:notionfi

I iyi(JIMMdMOW*

Itfom MIO*| |i«(1 lustily) [YY/MM/OOl (2*00 to. ctoM}

Source CodM:W*ll ,(W) Oultill.. ... ,(O) Bottom S«dlm«nl .. ,|8> Surltec Impoundment... ,|i) LMChat* Collection By*... .(C) Ott»«r ..Soil .(Si Hiw/SlrMffi. |R| 0«fWttion Potni .., ,|G) Trmnwil Pact Illy ..., ..m LiheiOcMn ............. ,(U tpoclty .

SHUTTLE CONTENTSBOnLE

No

,

/

1.

2.

3.

4.

Type

yT°

Site

Jtfo

Afo

•

Preserv.

d

tLs&L

ANALYSIS

Aftutt+nnt. /krAÂ

AjJJhtt TbS

tfJ*,TltlJ

SAMPLERFIIL (YIN)

^

y

Observations

S

S

'

LASObeenetlom

faff ,i. fad

x/

CHAIN OF CUSTODY CHRONICLEShuttle Opened Ift: (priSignature: fc.

& >,ku G,a«B>J Date: 8--|-ai Tlme; on MSr _ Seal»:oa«tT» *<vo Intact: -^

1 nave received these material! In good condition from the above person. __Name: /?/ , ^^ * Signature: / .- 4^- *./

Date: 0f/*i/&4 Time: /^.'fty> Remarks: -** -

I nave received these materials in good condition trom the above person.Name: Signature:

Date: Time: Remarks: 233

Shuttle Sealed By: (prin

Signature: o* feT3t" &L»/-rtn/ LlMDlenf Date: eiluifa Time: /</*f-.. jf--f*M ' Seal*: &rf>s8T- »«•«: <?* —

•HUTTLEt TEMP.

Date:SEAL*

.Time: 13-6»-ft! .CONO. _x,

FIELD PARAMETER FORM (CC2) Form 0002Swnpto Mliugmwnt

M/M

ETC JOB # .Sample Point Uy I / KS-iUiiPiZ.i/^1

taure* COM S«m»M tainl 1.1 ^ 1

FIELD PROCEDURESI \f\-d

"saw"SAMPLING METHOD:

Sampler Type

Sampler Material |d|ct

Tubing Material

Sample Composited

A-Submmlbto Pump D-OlppMBottMB-ISCO E-BailwC-BlKXttr Pump F-Scoop/SIMwl

C-PVCD-PlutlcC.Poly.thyl.n«D-Slllcon

X-Otfw

X-Otlwt

Well Elevation (ft/msl) LDepth to Ground water (ft) LGroundwater Elevation (ft msl) L

i« LLZiiHJ *» ist L2ndl_liUl2j «™> 2nd L __

3rd I IÎ^KI BTB> 3rd I I Ifelftl I I %£%

FIELD MEASUREMENTS

w.iiD.pth(ft, I l\*\Sample Depth (non-well) (ft) I I I i I I

I I I I I I

Lla Ir« I I'

FIELD COMMENTSSample Appearance:__£^£4Weather Condiiipn«: <JJA/^ O-/SMJ//

Tef

V .FILTERINQ: Ust Chain of Cmtody (CC1) to Indicate which bottlst w«r» nit«r«d

Sampler: d^fyTZW £/4JDS£y______ Employer

I certify that sampling procedures W i In accordance with applicable EPA state and corporate protocols.234

ORIGINAL

^^ ENWflONMEA/ML TESTING mi CCPTIflCtTION ' Seal No. °l^^/£f*7 ETC .Inh« Cfl1774

A/N OF CUSTODY FORM (CCt) ORIGINAL Date Sealed _89/oe/oi_ By. /<.g-

Company: . PELAAttn.: DAN GREEN

C'TY DISPOSALe;rj not i PAY i UN mo i SON . Phone: (414) 631 -

Address- 12 AND IB EAST, HADISDN, Ull 53704


Facility: I f P F I I I I I I IF«tililyr8ll« COM

Sample Point: llJ-ll i6-il I i 14rllrom MH>wl (1«lt lultl'yl (vvrMM

Soufct Coon.Well .(Wt Oultftll . . . .<O> ftotlwn Sidtm«nt... .IB) Surlact Impoondmtnt.Soil 181 Hiv»f<Slf««m (HI Qtn«rinon Poinl ...IQ1 Tftilmtnl facllily .,.

..<ll L«KniltCollwtl«nSy«.....(Cl Otfwr .IT) Ukwoctan.............T.-.tlJ • apKlty

SHUTTLE CONTENTS

Ne Type ANALYSIS SAMPLER

UOf NONE UOLATILES

TB GC/TtS TRIP BLANK n/EX loot EXTRBxtlS

EXT 1000 PST/PCB L/

MET 1000 HNQ3 METALS

A/

A/A; (X

llfCHAIN OF CUSTODY CHRONICLE

Shuttle Opened/fty: (prif

Signature: /cJt^.

Date: g_g-a^Seal *:',

Time:

1 have received these materials in good condition from the above person.Name:




Shuttle Sealed By: (prin Time:Intact:"

LAB USE ONLY WMB B([_^SHUTTLE I t'lls TEMP 'C

Tin-SEAI • 'sl/'5'Ltl8ff- conn I^

FIELD PARAMETER FORM (CC2) Fom ODD:Swnpto Managwrwnt

oe/ss.

ETC JOB * _Sample Point Ldl l| i£rilt3 Ri-freiQ i r I

Sourci Coda Swne* PMfll I.D.

FIELD PROCEDURESI i i5T J2dJ

SAMPLING METHOD: ___________________

i v i i A-SubmwilbW Pump r>Dlpp*HBonitSampler Type W(l B-ISCO E-Biiitr

' lw C-Bl.dd«rPump F-Scoop/Sho»l

Sampler Material I'yJA. tkTe"" SpuSiicTnhlnn u.t.rj.i l //»l *-T«llon C-Poly«lhyHn«Tubing Material I /Ci s-Tygon r>sincon

Sample Composited

FIELD MEASUREMENTS

I I I I i I I Well Depth (ft) I l;Well Elevation (ft/msl) _ __ _____ r _________Depth to Ground water (ft) I I |3 U 101? I Sample Depth (non-well) (ft) I I I 1 I IGroundwater Elevation (ft msl) I I I I 1 I I

1st I I

3rd I

4th 1

,.,

2nd I

3,d I

..TO, 4lh |

I l J I I I I I I L I

I I I

J I

CO

Sample Appearance:__U£tf&.Weather Conditions:.Other:.

FIELD COMMENTS

FILTERING: Ust Chain of Custody (CC1) to indicitt which oottlss w«r« tllt«r»d

Sampler: Employer

I certify that sampling procedures we,re in accordance with applicable EPA state and corporate protocols.

236

«^^^^ ENVIRONMENTAL TESTING ma CERTIFICATION • Saal No 4.^-4^0 ETC Job»

CHAIN OF CUSTODY FOflM (CC1) ORIGINAL DateSealed f.j.fl By.

Company: _

Facility/Site: nunn

Address: _____

hlrnr Attn.:. f->jAnn


Facility:7 I I I I I I I lf\ L3C.

Sample Point: i6(UlB|-?l BRl I I \8rt\<M\Z.\(o\ I / 13 H Ifal I I l_5TSou'ci Coot Yout Samoi* *wnt 10 Sun DII« Sttwi TUM(tfW MIOW) Httt jullitT) (YV/MMlDDl (1400 M. ettCfct

Source Cod«: • " •WtM . (W) Oulf*ll. .. ...(01 Bottom s«dim«nt... .IB) Surlwi impoundment... .(I) LtKfW«C«tHRtlOflSy».... .(CÔtH* .

BOTTLENo

1

t

1.

2.

3.

4.

Type

^

V

Sin

£%>

Ifa

\

.»

Pr*»ry.

0

yÂ/

SHUTTLE CONTENTS

ANALYSIS

AMtS*AOS, fajAÂ*,

^///.^ T&.C

VATS, 7VV

SAMPLERFill (Y/N) Obtervatlem

.x

^

LABObaenMIona

CHAIN OF CUSTODY CHRONICLEShuttle Openeo^fiy: (pr

Signature: jUt~ *&C- :' ~b*u CiiLeej D«'»: oB-o-i-8-* Tim*: o~i MS, _ . Seal »: oot-M * •*« Intact: — '

1 have received these materials in good condition trom the above person.

Date: d$/3,f/fy Time: j/0fxa f*si Remarks: f£—

1 have received these materials in good condition from the above person.Name: . Signature:

Date: Time: Remarks: L 6 /

Shuttle Sealed By: (print, j/^J^ £.Jk*. °«'«; M/ltkl Tim*: /^f5~Signature: 6&^4*7

LAB USE ONLY Open•UUTTLEI

X -l /. - / Seal*: ffaf&f lnt»°<: «*.^m- •tfl1(u\Sj\ll+- "•••• 9-Jl-tt -nm.- l*:te

FIELD PARAMETER FORM (CC2) Form 0002Sample Mwtg«m«ntoa/M

ETC JOB «Sample Point ll*3 I I i6HtL

Sourct CM«I -I I

ItmoM fowl 1.0

FIELD PROCEDURESI i j.5l I i ifmol

WATEH VOL IN CASINO VOLUMf FUMIO

SAMPLING METHOD: ___________________

IV//..I A-SubmtnlDM Pump D-OlpMr/BottKSampler Type ytJLA B-ISCO E-B«n«r

**"" C-ai>ddir Pump F-Scoop/Slwwl

Sampler Material! ]

Tubing Material ^

Sample Composited 1-tVN I

C-PVCD-PinticC-Poly«tByl«n«D-Slllcon

XOtlMr

X-Otlwi

X-Otlw

Well Elevation (ft/msl)Depth to Ground water (tt)Groundwater Elevation (ft msl)

FIELD MEASUREMENTSI I I I I I I Well Deoth (ft)I I I ' \' jy|5i

iVellDeDth(ft) I I I ! "^ \li fcSjlJDle Depth (non-well) (ft) I I I 1 I I

2nd J I I I I I I I__I

3rd I '»'»> 3rd I I |7|g|g| —•

«TDi 4th I_L

I I ITiflra

Sample Appearance:.Weather Conditions:.Other:.

FIELD COMMENTS

S.FILTERING: Use Chain of Custody (CCl)4o indicate which bottUt war* tllterad

Sampler: Employer

I certify that sampling procedure^ were in accordance with applicable EPA state and corporate protocols.2. oo

ENVIRONUCNTAL TESTING MS CSRTIflCtTION ' &m*(Ho ETC Job »CA1375

CHAIN OF CUSTODY FOflM (CC1) ORIGINAL p.t.8.. 89x08/01 By.

Company:. PELA

Facillty/Site:-^^^^ . Phone: (414) 431 - 3190

Address:. 190/xEXIT 12 AND 18 EAST, MADISON, UI $3704


Facility: I f P J,,., 1 ' ' • ] L

Sample Point: liiHl»«|I Samplt M«fli ID

i i 1 !Srt.l/jlrtlz.iCol\avifmnQ

Li i3

Sourct CoOtt:Wtfi . .(W) Outfall...... ,<0) BoiiomSwlifiwni. ..(B) Surf«c«lmpoundni*>m....(» LnchaMCoilMttOASyt.....|P) OttsJf ...


Me

2

1

2

2

11

I|

1

|

J_

Type

UOPTB

EXT

EX1

MET

Slse

40

40

1000

1000

1000

41$-:I"*.-1ST '

Ss«nS"'\zr

Prnen.

NONE

CCxns

none

none

HN03

r*«e.*r I'D

A/*<*»J

*^T>

ANALYSIS

UOLATILES

TRIP BLANK

EXTRB/tlS

PSTXPCB

METALSpfVfAC*/7^)

^hcx«L>

Of+H i-df

CUlcMCA'O^1

T0<-

SAMPLERFlit (YfN)

/urV»

(0

r5

yrV

•JAJA/«/

Obtenwlloni

S

S

ssy*-^*~^„ _

LABObeeraetlera

\^

~/

^

*-^~^-

^^

(^/^

L-

^/

^

^


1.

2.

3.

4.

Shuttle Opened BV: (priSignature: -X .

n'V ~b»,ki <?w2.(r»vJ Date: 8-S--*-? Time: Ilvo8â-.— Seal»:anm^-i Intact: ~*

1 have received these materials in good condition from the above person.Name: .* , i / _ «,- Signature:

C-lA^TOA C_tXj.tS**j

Date: ~i£ SefO* Time: S^BffS Remarks: f>^

\ have received these materials in good condition from the above person.Name: Signature:

Date: Time: Remarks: £07

Shuttle Sealed By: (print) * / , C.r*jl3e*i, D*'*:

Signftur*- /ÂT3

LAB USE ONLY OM»

SHUTTLE* y/

— S7 Y< ' — '•zt.**** T""«; />n

Seal*: *i<^-S£. lnttcl: at:

r •(««?«• f s«ii conn tK&^r/

ETC FIELD PARAMETER FORM (CC2) FormOOOaSample M«nag«iTwit

oa/w

ETC JOB #.Sample Point M I

Iwjre* C«o*I I

|gffidr«?iZjdFIELD PROCEDURES

I i iajWATIB VOL. IN CASINO VOUMH njn

IQMMAM

SAMPLING METHOD:

Sampler Type

Sampler Material

Tubing Material

Sample Composited

A-Subnw»lbl« Pump D-Dlppw/BoHKB-ISCO E-B«ll«rC-BlKMw Pump F-Scoop<Shov«l

»-T«(lonB.M.I.IA-TiiionB-Tyjon

C-PVCD-Plutlc

C-PolytlnyltntD-Slllcon

X-Otlwr .

XOIh«i .

Well Elevation (ft/msl)Depth to Ground water (It)GroundwaterElevatlon (ft msl)

I I IFIELD MEASUREMENTS

_J—i I I Well Depth (ft)J Sample Depth (non-well) (ft) I I I 1 I I

1st L

2ndL

I I i2nd liTl fel /

3rd

I l / IOl2Jro

3rd I I IjfJLSlgl XTc

4th I I 1 ISlfeL3l STcI M I 1 IMTU

J I I I I I I |_|

FIELD COMMENTSSample Appearance:. _Weather Conditions: SMMX-IOlh.r Ujt.ll '

58* /*

FILTERINQ: Us* Chain of Custody (CC1) to Indlcat* which bottl*s w*r* tllterad

Sampler: Employer.


TIM B ORIGINAL

. • • fHi/iaanufuTti res-nun fnacearif ir.trinn ' c»i M« U.SO.'J-Ja

CHAIN OF

Company:

Facility/Site: _,

Address:

CUSTODY FOflM (CC1J ORIGINAL Date Sea|ed f.^.fg

ijimr Aim • /W

ETC job » (LAiSIff

/?

f)M*-4/jt


Facility: L i i i i i i \4\a\J\ \3i 1Sample Point: IfjM/ l&Hdl 6l lfllg| I I I Igfll^qiafel I / IJ13 l*?l I I ;3I

Sou'ct COM vour SampM ftmt 10 Stirt 0«M tun Tim* IMMd Ham(from M'Owl d.tt lutl.lyt (YVfUMfOO) 13400 hr. etoefel

Soure* Cod«»:Well , .(W) Outfall. (01 Bottom SWimtnt... .|8) Surf act impoundment... .(I) LucnutcCollMUonSyt... ..I

.-(T)


No

t

f

Type

10

•f

•'••

SIM

Affl

AST)

* ' • •- '•

Praunr.

/j

iLSM.

ANALYSIS

JVMJJ»»»A SluAÂS,

+ttf-f/Jftrt . jMrVC

A/j/^ "TÂ/

SAMPLERFDLcrmi Obtirvilioni

S*

^

LABObMnatlm


1.

2.

3.

4.

Shuttle Opened^By: (pnSignature: M~.^/C.

^" "brXu <S.e*wJ Date: A-T— S*\ Time: ^" -. |5"„. — Seal »:0o«V1«v *•>*•& Intact: —

I nave received these materials in good condition from the above person. ~Name: top*/ waxy siflnatu™: n^^fLû.Date: £ft/t£i9j Time: Jjfifp^f^^ Remarks: O&Ji U

1 have received these materials in good condition from the above person.Nam. : Signature: . 941


Shuttle Sealed By: (print) £uH/f6J/ LjA/ESfl/Signature: /^£w£^

LAB USE ONLY OpenfUlJTTI t t

Date: 09/u/M Tlme: /^d"*?Seal*: ^^S<f Intact: < (Ll.

TEMp'-f! 4* SEAL* *ft7 nONH ^JflJtLfA ———

FIELD PARAMETER FORM (CC2) Form 0002Sampl* Muiagimttit

OB/M

ETC JOB * _Sample Point lu^ I 1 ifriUi Riî/tiRi i ^ I

aouiu Cod* S4IWM Point 1.0

FIELD PROCEDURESl/lTJtfl I I l3l I I ! /L5ill

WATCH VOL IN CASINO

SAMPLING METHOD:

Sampler Type

Sampler Material |<4/c|

Tubing Material

»-8uDm«rtlbW Pump D-DlpoMBottlinsco E-B«II«c-BUddtjr Pump F-ScoopfShovilA-T«flonB-Mltll

C-PVCO-PlutlcC-Poly«thyltntD-Sllicon

X<»lwr

X-Olh«i

Sample Composited I ON I

Well Elevation (ft/msl)Depth to Ground water (It)Groundwater Elevation (It msl)

FIELD MEASUREMENTS

I—I I I i I I Well Depth (It) I3IV1.513II I I ~2\f[T-te'\ Sample Depth (non-well) (It) I_|_I I I I i I I

1 I I

t I 18, I \ l \ f \ k \ 8 \

2nd I I / ISlfal I I

J I I I I I

2ndL_LM±LLJ •«H

3rd I \l>[^\\\ »™ 3rd I I I I5l5"l8l#> «*M.««M.

4th I I { . 1 3 1 »T»p 4th I I

FIELD COMMENTSSample Appearance:.Weather Conditions:.Other:.

3V.53-FILTERING: U»« Ch«ln ol Custody (CC1) to Indicate which bottlM w«r» tllt»r«d

Sampler: <J-+*+»t- (^•^•st* _________ Employer:(P"mi ' 7

I certify that sampling proceduMpfwere In accordance with applicable EPA state and corporate protocols.

242

ENVIRONMENTAL TESTINQ ana CERTIFICATION Seal No. CA1?76

CHAIN OF CUSTODY FORM (CCt) ORIGINAL Date sealed. 89X08/01 -By:.

Company: PELft DON GREEN

Facilitate: _ . Phone: (414) «31 - 3150

Afldress. 190//EX1T 12 ftNO IB EAST, HAD ISDN, Ul 53704


Facility: I f P P I I I I I I I |_

Sample Point: fcjl-11 tflrViftl<?lAlg| I I I Iflfl Irfl <?lSOU'C* Coot Your Sampi« h>tni ID SUM CW«

{Optional S*mpi« Point D

S&irYMMfDD]

SoufC* Codes:wall .(W) Outfall.....Soil (SI River/Stream

.(0) Bottom Sadlmant. , ,.(B1 Surtaea impoundment ...(R) Generation Point . . . . (01 Treatment Facility ...

.. (II Laacnate Colloetlon Sv*. . .£4C} . O. (T) Lake/Ocean .......... .....fU apa


No

2

1

2

2

1

,

1

1

f

1

1

1.

2.

3.

4.

lype

uo<TB

EXT

EX1

HE!

' ii

Sin

40

40

1000

1000

1000

3~

«£

i&\T.f

1Z.<

Proton.

NONE

GC/ns

none)

none)

HN03

k*«>%• rê.•J^toa>AOX«aJiS

ANALYSIS

UOLflTlLES

TRIP BLANK

EXTRBxnS

PST/PCBMETftLS

Cto****"rlZ^f^WW/i/

r'Wo«.f'Dff'

TZ3C.

SAMPLERFill (YIN)

wAJ/^fj

yA^t>fjtJ/

Observations

y

•S oteU(<.

S

S

y

——

^~

^

^

^

LABObsonttlons

^y^L/

tXiS

L^

L/l^/,^s

CHAIN OF CUSTODY CHRONICLEShuttle Openecv«y: (pri

Signature: f2L-'*$.

Date: g.^-ei Time: \(e-<50-. __ . Seal#:oi«TT*-~» Intact: -^

I nave received these materials in good condition from the above person. /j s~ ^^ f 1Name: _j. __ fJiiJMjf. Signature: /L/rs' JK^^^^ ~ *-^<^

Date: Zl^Cf "^ Time: QK£>1$ Remarks: // 6*~L — S


Date: ' Time: Remarks: 243

Shuttle Sealed By: (prinSignature: &/fJ -

-• TtrP Êl46L/VMIS Date: •a-i**** Time: Hif\^Z^~^^ Seal#:disnn4e ln«act: < *_

LAB USE ONLYIHUTTLE*

.Date: .Time: .//>' AST

ETC JOB »_Sample Point Ikd \ I tfjLA St f( At a i i. I

9owc« COM Same* Mm 1.0

•s&va1SAMPLING METHOD:

FIELD PROCEDURESlMifli3ill I iftSl I i ffiftfl I i i 1 1 i4.l •

I V / J A-SubmwtlDK Pump D-DlpMrtBotll. ,Sampler Type IX/n B-ISCO E-B«II« x-othw U t.1 1

'?*" C-Biiddw Pump F.scoop«Shovti

Sampler Material f p i u c xotiwr

Tubino Material [j

Sample Composited I«N I

FIELD MEASUREMENTSWell Elevation (ft/msl) I I I I i I I Well Depth (ft) IDepth to Ground water (ft) I I l^|5i/|y)| Sample Depth (non-well) (ft) I I I 1 IGroundwater. Elevation (ft msl) I I I I i I I

1st l6Ue.ll I«™ 1$t I i /J_j_ljplftl XT* I ^_^ I I I M I I

*J IUAI 11»"» 2na I IMMjTjyi SR I ^^^ I I I M I I LJ

3rd I ll^lQlSI "™> 3rd I I | \H I Y\(jo I iJSx I__________I I I I I I I I__I

»", 4th I I /iVjJIfcl HR I w)___î I I I M I

FIELD COMMENTSSample Appearance:.Weather CnndiiiBns- ^j*/*is* ^^SV A/M^ O-g Hftt FfOH Soon/r»h.r /A/ flair*,*-. 'f4P ~l* **>?* &* fV*- (tWcn- <3>t£/AJA- 2."'til'*•

FILTERING: Us* Chain of Cu*tod/(CC1) to Indfcitt which bottltt w«r» tllUr-d

Sampler: Teff- g^<^(w*Mt>___________ Employer. Pel A

I certify that sampling procedures were in^ceerdance with applicable EPA atate and corporate protocols.244

^———-«B_Bm..___..__ .The Envkonm-nM Secvlcee Campeny ORIGINAL

^^^^^ £HVIKONUENTAi TESTING ini CePTIP/CHTION ' Seal No 4^9-4^0 ETC Job « (LAlAlb

CHAIN OF CUSTODY FORM (CC1) ORIGINAL DateSealed f.^./g By.

Company:,

Facility/Site^.

I, IMF Attn.:.

Phone: (t*/)f)

Address:.


Facility: \ti\t \f\

Sample Point: M-l I i&iUiftiSiA-lRi I i I \8ft\AA\Zft\ lfTJlfil3l\l I \5i£[Sou'ctCoot Your $«mpi« Poim ID Stuni CWifl ' Siwl Tint tIMOM Houri

Sou'Ct CoOtiWtM . (Wl Oulfill....... 10) Boitoiti StrtimtntSoil (8) Rivt r/Strttm (fl) Omtxatlon Poini

..(B) Surftct impoundmtjnl.. ..(It Lt«hittCo«*w«on$yt,.., .(Q Ottwr ...• Kfr TfMltrmnt Facility . . . . . .fn_ LWiVOcttn ...............ft j ftNelfy .


No

,

,

Type

Y?

V

Sin

A5O

10)

f "' ..

" '.r • •

PreMrv.

^

\jjjS&L

ANALYSIS

AjMtJ,^*, />AJ*^ft*.

v6///A// 77K

fJtlt TTffJ

SAMPLEDnit (rmi

(U

1

ObMmtloni

^

^

LAiObeanattene

/^/ /»/ffl~)/

,/


1.

2.

3.

4.

Shuttle Opened^y: (priSignature: xj* - ^

"V ^4^ G*etfJ&*~-

Date: ff.-j.gi Tim«: OTÎS-Seal #: Oatl^ J- fo Intact: -^

I have received these materials In good condition from the above person. — xOName: -r- .- _ Signature: //,//- \ 2-»-»_Z.XJff& &tJGlsj/& rrra "i •~»-*f— 'Date: Z^S^S*? Time: C'^Vf Remarks: fe^f (y

1 have received these materials in good condition from the above person.Name: Signature: 245


Shuttle Sealed By: (prmSignature: /2^^- \-

" Jfwoev^«Â7N D"*: ,2-?s<v0«? T""t: /%>^•«-t_ ,X Seal*: ^/jTwSZ. '"«•««: ai'

LAB USE ONLY <*M»ti£/JCULSHUTTLE*

/£k>.TEMP.

Tim*.COND. _xJLcd&e&-

ETC FIELD PARAMETER FORM (CC2) Form 0002Sampla Management

08/M

ETC JOB # .Sample Point

(LA &w.i i I

FIELD PROCEDURES

WATER VOL. IN CASINOI li<e\

SAMPLING METHOD: ___________________

I V/ I A-Submartlbla Pump D-Dlppar/BottlaSampler Type | A/f J B-ISCO E-Baiiar

" T' C-Bladdar Pump F£coop/Snoval

Sampler Material

Tubing Material

Sample Composited IJCN I

A-TttlonB-Tygon

C-PVCD-Pla»tlcC-Polyathylana0-Sillcon

X-Othar

X-Othar

X-Otnai

Well Elevation (tt/msl)Depth to Ground water (ft)Groundwater Elevation (ft msl)

FIELD MEASUREMENTSI I I i I I Well Depth (ft)I |2|S~1 I 101 sample Depth (non-well)(ft) I_LI I I i I I

1 I I

1st I \Ll&\\\»™ i i n 2nd I I f^J^-^ I

3rd I l/«j£3lSl I«TDI 3rd I I /I•*

Jj »T" 4th I I / I

I I I I I I

J LJJ

I I i lZi 31FIELD COMMENTS

Sample Appear»nce:_C4£filWeather Conditions:. r; zllP

FILTERING: Us* Chiln o( Custody (CC1) to Indlctt* which botttot w»r» lllt»r»d

Sampler: Employer

I certity that sampling procedures were in accordance with applicable EPA state and corporate protocols.

24T

The OBIQINAL

ENVIRONMENTAL TESTING »nt) CERTIFICATION ' Seal No.

CHAIN OF CUSTODY FORM (CC1) ORIGINM Date sealed.ETC Job*

89/08/01 .By:.

Company: PELfl Attn.: DAN GREEN

c: „ ,„. CITY DISPOSALFacility/Site: —c-'O HOLIDAY I MM HAD ISO

Address: I90//EXIT 12 AND 18 EAST, MADISON, UI 53704


Facility: I f P ? I IFMilitylS'1*

I I I I I I

Sample Point: ll»/l-l I•MIC! COM

I Itour Se W *wnt ID

\Q>tf\rh(A I l l t f lSlirl DH* ' Slwt TbM

Iliom Miowt dttt luilify) (VYflriMfDD) IMOO hr. cMOfe) s ': • fRMVMlIM

Sourct Cod*t: .. <yW*)ll (W) OulUII .,, ...(0) Bottom $exJimt)nt... ,(B) SurfMt) Impoundment... .(I) L*ach«MCoH«JCtlon.)yB.....(C| -JNMr -Soil <S| RivfWSlrMm (H) Q»n«r it ton Point . .|Ql Trwmtnt Pettlllly . . . . . , (T> UMPCMn ............. ..flj "ipJCIIV


No

2

1

2

2

1

/1

I

I

/

j

TypeUQf

TB

EX1

EX1

MET

V

Sin

4(

40

100C

1000

1000

560

-âs'J**"

I7.T

'US'

Praeere.

NONE

oc/ns

none

none

HN03

(U.d,

>««

^^

A*n«

3t,,WCB

ANALYSIS

UOLATILES

TRIP BLANK

EXTRB/nS

PST/-PCB

I1ETALS

cyw-iprpfc^»«^

"/tL

ClvL^p

T=>c.

SAMPLERnumw

^

tf

<Jfj

r/vA/fj/v

Obnrvitlora

./

*/ a iei

ss./I/""sS

IS

LAB. ObeenatioiM

>/

' L/I/I-/

I/,tXI//^/u/^/


1.

2.

3.

4.

Shuttle OpenerffBy: (pri

Signature: Mf— ""$7" ~£>K» <S«jc«J Date: g-S-S'\ Time: t(o'-00^^^ Seal*: oj\<s~li>t-V Intact: ^/

I nave received these materials in good condition from the above person. O^ /^*7Name: -»- C/u / T^> Signature: dtdffs^^^ ' *^^

y V —Dale: Z'I?-5<«pSel Time: A^3/fc Remarks: «ri-

I have received these materials in good condition from the above person.Name: Signature: ^ f ^

Date : Time: Remarks:

Shuttle Sealed By: (prinSignature. x< ,f5^£ \

t) - .e <£Hj£c*s/E> Date: 7-9- SA»S«I Tlm* n i ~|^z_____^' Seal*: lO^-VZ" Intact: M,

LAB USE ONLY O^SHUTTLE* .TEMP. "C . .SEAL* . .COND. .

FIELD PARAMETER FORM (CC2) Form 0002Sample Management

08/98

ETC JOB «Sample Point li_ l| lfacAg.ll itl Bgl

Sourct CoOt aamBM Point I.D

STAUT nmotI3MO Hr Clock)

FIELD PROCEDURESI iu6l I i I I

SAMPLING METHOD:

Sampler Material

Tubing Material

Sample Composited

I \f\f I *--SubmSampler Type \ML\ B-ISCO

^f — ' osiadd

|/( J ^Me'

|/rfc| £T*

A-Submtrilblt Pump O-Olpptr/BottlaB-ISCO E-BalltrC-BladOar Pump F-Seoap»ltavtl

C-PVCD-PlaallcC-PolytlnylanaD-Sllicon

X-Otlw

x-otnat

x-Otnai

ISMCIPY OTHIHI


FIELD MEASUREMENTSI I I I 1 I I Well Depth (ft) II I I 2.I3J51T I Sample Depth (non-well) (ft) II I I I 1 I I

I I 1

1st

3rd

Ithl

1st

2nd

3rd

I I I I |__I

I8I3I3I

B 4th I I jgl3l-?l an?e

l"/l/ lulled I Tl I I INTU

FIELD COMMENTSSample Appearance:.Weather Conditions:. g-eT«"/»A <:S" P

FILTEBINQ: Us« Chain oi Custody (CC1) to Indlcitt which bottlo w«r«) fllltr»d

Sampler: fAj£-f Employer:

I certify that sampling procedures were in accord

Th. I

,witn applicable EPA state and corporate protocols.

248OfiiOiNAL

^^^^^ CNVIRONMCNTAl TCSTINO IIXI CERTIFICATION ' Saal No 4jQ • *A4i ETC Job « (LA l3fj

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Date Sealed _&ir/2___ By:.

Company:. Attn.: .»„


Facility:

Sample Point:

I I I IF«:lMta.u (Cod*

i ^H LU Bi 1 1*2 1 1? i

\4\e\f\ (*£_IglHIdli<fl 2,14-

lODtiWW S»nml« Potnl WWnplioni,

Soure* COM tout MmpM Pant(torn o*M*! iwn |u*ii(yi

Sourci Codti.W*ll . .(W) OulUH. ... .10) Bottom Stdlmtnt... .<B) Surl«e*lmpoundnwnl.,

i iua

Soil . <S1 «ivtr/Slf«tn IR> OtfWIIion Point .. ,<Qt Tr«tm«m Facility . . . . . . <T> LlMIOcwn ............. ,.|U SpteHy

BOTTLENo

,

/

1.

2.

3.

4.

Type

V

-r°

Sin

3£L-

'\ :•':,.. '"' '

Prexn.

^

jLs&L

SHUTTLE CONTENTS

ANALYSIS

^>^^W,AA / y>^>»//

^tUple TAC

A/A TV//

SAMPLERFlit ft INI

/I/

li/

Observation*

^

^

LASObMnillem

J..{fs fl/.*d

6\/

CHAIN OF CUSTODY CHRONICLEShuttle Opened/fly: (priSignature: JJ._

?* "b/f/x G«»J Date; 8-1 -»1 Time; OT--'S-^ _ Seal#:oo*« * *« Intact: ^^

I have received these materials in good condition from the above person. . j \ /"XName: -r- _ . f^ Signature: />^^ s(^2**t. • »*C^

JeTW= K*>6-LA-iu\\ fff ' ——., ff f/ ( 1

Date: Z *-i«pi8fl Time: Aft-dcl Remarks: ' «fe \^

1 have received these materials In good condition from the above person.Name: Signature:


Shuttle Sealed By: (print) ^f^s- ^f=rjsG.&/f~S~-£) Date: 29-5'vdT ^"^''IÔfSignature: /jfe^ ^>r

LAB USE ONLY O^MtSHUTTLE •

~--a^-^_£_--' Seal*: fl)rf^L*?'7 Intact:^ '

^T^^fl^y JfJi"*- ————— Date: f-Jf-ff —————— Time: Phi ———— ___ —TEUP -r ^' SEAL • ^X* coNn. ^/niHff- —— 4^Z —

FIELD PARAMETER FORM (CC2)

ETC JOB ».Sample Point ImJ I' iÛiiBi\ iZig

Source COM Simp* *oini i.D.

FIELD PROCEDURESi i f iâ I i i i/u5t

SAMPLING METHOD:

i ., i i A-SubmrallM Pump D-DlppwflSampler Type IXM B-ISOO E-B.I*Lt l_c êirt pump F-scoopf!

Sampler Material I ftfC\ B-M*.'U" D^MIIC xotiwr

Tubing Material \A/t\ trJg'S; MaK!"'"* »-otf«

Sample Composited |

FIELD MEASUREMENTSWell Elevation (ft/msl) I I I I i I I Well Depth (tt) IDepth to Ground water (It) I I I2l^l5li-/l Sample Depth (non-well) (ft) I I I 1 I IGroundwater Elevation (ft msl) I I I I 1 I I

2ndl_lMLZl ""• 2nd I I Jfj3l8l -R I _ I I I I I I I LJ

3rd I lyi^lTO 3rd I I I0I3I3I

4th I I **l ' l&l WW 4th I__L

FIELD COMMENTSSample Appearance:.Weather Conditions:_Jnih«r U"lll (-*-•

FILTERING: Us* Chain oi Custody (CC1) to lndlc*t* which bottl*s w*r* »lt*r«d

Sampler 3 GPF- £^6 <-Gir£\~*>______ Employer

I certify that samplingj>rocedofes were in accorjlan^V with applicable EPA etate and corporate protocols.

250The ImtrannMittel t«cvto»« Compeny ORIGINAL

^^^^k ENVIRONMENTAL TESTING imt CERTIFICATION ' Seal No. O'l^>~7' £>?

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Date Sealed __!!££12i

Company:.

Facility/Site:.

PELS Ann.: DAN GREEN

CITY DISPOSALPhone: (414) 631 - 3150

Ad(Jreas. 190XXEXIT 12 AND IB EAST, MADISON, UI 53704


Facility: I I* P ? J. J,, J.J ' '

Sample Point: Ifej-l I |6|W| ft 1

I

Sou'clIIXMll Miew) Illll |u*l>lyl

SoufCf Coou:

Sotl .(SI RivcrfSlrtam .IRI OvncnltonPoint .

I ISi*UI2l?t

..IS) SurtMCImoouiidnMnt.. .(!> L«M»wl«Co««otlontyt...:.|Q O101 Tft»tn>«nl raclllty . . . . . .{D LahwOcMft.,'..,....,.... .flj r.Sl


No Type Slie ANALYSISSAMPLER

ObstrvttlonsLAB

UOf 40 NONE UOLftTILES

TB 40 GCxns TRIP BLANK

EXT 1000 EXTRBXMS

EXT 1000 PSTXPCB yME! 100C HN03 METALS J.

A'

A/ y/

A/ VCHAIN OF CUSTODY CHRONICLE

Shuttle Opened,Signature:

Date: 8 . . Time:" Intact:

have received these materials in good condition from the above person.Name: * Sisnatura:




Shuttle Sealed By: (pnnt)

Signature:

LAB USE ONLYSHUTTLE I

ETC FIELD PARAMETER FORM (CC2)

ETC JOB*.Sample Point LJ II i&iuli&l

SnTStog. low,

FIELD PROCEDURES

SAMPLING METHOD:

Sampler TypeC-BI«ddtf Pump F-8coop/Shov«i arton

Tubing Material

Sample Composited ItTNJ

FIELD MEASUREMENTSWell Elevation (ft/msl) I I I I 1 I I Well Depth (ft) I______|

Depth to Ground water (ft) I I I I gl l'gl Sample Depth (non-well) (ft) I I I i I IGroundwater-Elevatlon (ft m»l) I I I I 1 I I

,nJ l?-|5-tOl -TO, 2no I I m^l .73K |______________| I I I I I I |___|

i i i£i.3i&i .nrs l____I i i i i i i i_iw I I / I / I /Iro I I I I I i™

FIELD COMMENTSSample App»ar.nca- ft.-\trw*Weather Condition.- 5""" M

FILTERING: U»« Chain of Custody (CC1) to Indleata which bottlM w»r» flltorad

Sampler:

I certify that sampling procedures were Irvaeee/dance with applicable EPA atate and corporate protocola.

The IiKfcommntal »«cvto«. Company

^^^^L ENWflONMENMt TtSIINB tl\lt CCRTIFICWON ' Seal No 4AQ- 440 ETC Job » f AI3f3

CHAIN OF CUSTODY FORM (CC1) ORIGINAL D.,.SMi.d P-J-/9 By fas

Company: ——

Facility/Site: _^_

UlfTlT p>l///


Facility: L

Sample Point:

1 1 1 1 1 1I I IFMimysn* c

B i l i ? i t t j R i i I \\ \f[p\*\ I 12.15!low Swnplt Poini 10 slarl 0«» Sun TWM

llromMlowt (l«(1 lutnlyl (YYMWOD) 12400 W.CMOM

Source Coder ,.Wttl..(W1 Outlall.... ..(01 •oltofflS«d(tn«nl.. ,.(B) Surttci Impoundment.... (I) LMCluttCollMtloaSy».....(G) Otfw ...Soil .<S> Rivef/8trMm..fHl Gentrttion Point . . . . (01 Tretlmenl Ficlttty . . . . . . m LaktrfOcwn ............... .(U Sg«el«y _


No

/

/

Type

V

1°

SIM

flSQ

-sffl?

•

Pmtn.

(

riaU)<L

ANALYSIS

dtt/Jaji Tt^f

tJlla TXtJ

SAMPLEDfnit jvmt

/^

/^

ObMmtlom

^

^^

LABObeeiyatloni

j6///. f T)^

N ^

CHAIN OF CUSTODY CHRONICLEShuttle Opened^y: (print)Signature: AL ^4/L "

Date:

Seal »: oaf 3Time:

" Intact:

I have received these' materials in good condition from the above person.Si»n'tur':

Date: Time: RemarK,:

1 have received these materials In good condition from the above person.Name: Signature:

Date: Time: RemarKs:

Shuttle Sealed By: (print) JfVf Date: -4

Seal ft'Timt:

Intact: ««fe

SHUTTLE I TE«IP -C 4*

.Date: _l_SEAL«

.Time:CON" t


ETC JOB »Sample Point liLJ II iSil~ti liO4<3<3 i I

SowrMCod* Umptt MM 1.0.

SAMPLING METHOD:

Sampler Type

Sampler Material [ftW

Tubing Materlai

Sample Composited

FIELD PROCEDURESI iZi5t I i i i la

A-SubnmlbU Pump D-Dlppw/BottttB-ISCO E-B«ll«rC-BI«dO«f Pump F'Scoop/Shonl

X-Otlw

XOttwr .

X-Otn«i

Well Elevation (tt/msl)Depth to Ground water (ft)GroundwatSr Elevation (ft msl)

FIELD MEASUREMENTSI I I I 1 I I Well Depth (ft) II I I Ifii" KT Sample Depth (non-well) (ft) I I I 1 I

1st

3rd I

1st

2nd

3rd I I I I I I I | __ |

l I 5161^0, 4th I I Ifel3l&l

FIELD COMMENTSSample Appaarancn-

Weather Conditions:Olhar gi^y f***k

^M^

tvl'llP *.,~tr~ v+f*LI* * *** *P

FILTERING: Us* Chain of Custody (CC1) to Indicate which bottl.s w»r» tlltarad

Sampler: 3fPF Employer P&LA _

I certify that sampling procedures/rare

X^-in accordance witn applicable EPA state and corporate protocols.

—— 25A.Tlw Envlc Company

^^^^L ENVIRONMENTAL TESriNS lia CERTlflCtTION , Seal No. /S"^7/ £<3 ETC Job «

CHAIN OF CUSTODY FORM (CC7) ORIGINAL Date Sealed __!! ! L_By: .

Company. , Attn.: DON GREEN

Facility,*..: C' fgn,,

Address: I90/XEXIT 12XPI30H 9HITM CMT Phone: (414) 631 - 3190

18 EAST, MADISON, UI 97704


Facility:

Sample Point:

f P ?'•Olllyflllit* Coo*

ifrlkJlftl

I I I I I Ii

Smj'C* COM YOU' S*mpl« *wn| ID(from MIOwl (UN |U*1>'y) (YVfMHfODl

Source Codes:Weti . (W) Outfall.. ... 10) Bottom Sediment,.. ,(B) Surface ImpoundmentSoil CS} RlverfSlream .(H) Generation Point ,...|G) Treaiment Faeiflly ...

\8rf\j\4\l\8\ l^lfljlfl I |4| llStirt Call tUfl Thnt j llflll a Hogf»

.(I) Leache.teCo»tetlanSyt.....<C) OtMr .(T) L«h«yQcMn .............. .(U tpkVlfy

SHUTTLE CONTENTS•OTTLI

No Typt Preaen. ANALYSISSAMPLEB LAS

ObwrvalioiMHOP 40 NONE UOLflTILES

TB 40 CC/MS TRIP BLANK A* 3— X

~&EXT 1000 EXTRB^MS

EXT 1000 PST/PCBMET 1000 HNQJ METftLS I/

$00

Mlf:

TOcCHAIN OF CUSTODY CHRONICLE

SHuttle OSignature:

Date: g-S~fl"\ Time: 11-.' Seal#: eatg-nH--S ln'»ct:

1 have received these materials in good condition from the above person.Name: Slgnature:

Date: Tim«: Remarks: t

1 nave received these materials in good condition from the above person.Name: Signature:

i Date: Time: Remarks: 255

Shuttle Sealed By: (print)

Signature: /idz' ~1 ^2-

Date:Seal»:

Time: ,3,f' Intact: e^>

LAB USE ONLYSHUTTLE* _£ .TEMP. *C .

.Time:

Form 0002ETC FIELD PARAMETER FORM (CC2)"o»/M

ETC JOB * .Sample Point Liil \\ 161 tO|8i I 1^1 g.Ri i-' I

SAMPLING METHOD:

FIELD PROCEDURESifteaiVi i i < / t i i u__

STAB^PUWI IIAPSED HM WATM VOL IN CASINO

I \f /-I A-SubmemlBle Pump D-Olpper/BottleSampler Type |A/Cl B-ISCO E-Baiier X-otner

r I™ c-BlaOder Pump F-ScoOD/ShovelC-Bladdar Pump F-Scoop/Shovel nfKtn OTHIN>

Sampler Material l H tiMta? r>p7aiticTnhinn UatAritti \*af \ *"'**'®n C-PolyethyleneTubing Material 1/ v j B-Tygon D-SlliCPn

Sample Composited I ft<N I _______________

FIELD MEASUREMENTSWell Elevation (fUmsl) I I I I i I I Well Depth (ft) I I Zlfell ^ IDepth to Ground water (ft) I I I I 51(ol(p| Sample Depth (non-well) (ft) I I I i I IGroundwater Elevation (ft msl) I I I I i I I

1st I l^ l t l6) ! »™> 1lt I I l-^felfal ^Tc I ______I I I I I I I

«"» 2nd I I l^felfil SR |__

3rd I I JSI »™> 3rd I I

4th I I l"fl?t ll S

I TPl I I.

FIELD COMMENTSSample Appearance:_£i£24____A.JO aao<t-______________Weatherrnnnltlnn.- Si.. ^^ •?r»/>j»U A... .*,!.. Ar*t.1J£ ^ l-ti'c.

oth«r i^<I/ t^^.-^fJ L' rve - l.ê j,H ' 4^^,-e.k. ' t

- 3 35"^*iv<«FILTERING: Us* Chain of Custody (CC1) to Indlcat* which bottloi w»r» »lt«r«d

Sampler: J<TB*»- f^f^^/^f_________ Employer[*M»I

I certify that sampling procdures were in accordance with applicable EPA state and corporate protocols.

25(TlwEi

^^^^^ ENVIRONMENTAL TESTING mi CERTIFICATION ' Seal No V.39-440 ETC Job II

CHAIN OF CUSTODY FORM (CC1) ORIGINAL DatBSMiBd S-A-M By .

Company: _______

Facility/Site: liLLnn

Address: _______

Attn.: ^'fflSI 6>AA tin

(•!*£} Phone:.


Facility: I I I I I I I iVl * l-l 1-3*_______'•GHily'SiU COM

Sample Point: lU-H ifeiUJiBil iSlRiRj I I I8lÎ<t\tI 2|gj I l4l1 I

Souret Codes:Wt« . (W) OutUnSoil .IS)

.. (O) Bottom SMImtnt ....(•) Surface Impounamtnl . . . . (I) U«hti« CMlMlKm Syi. . . . -C) ''•ttwr . . ,) Qtnettiion Point . . . ,(Q) TftaifTum Facility . . . . . .(T) L»ht/Oc«n . . , .... , . . .... ,(U Specify .


Ho

,

,

1.

2.

3.

4.

Type

f

1°

Site

Sffft

35*

?

Prtscfv.

d

//»?/%/

ANALYSIS

JVf/>jA*n»tt fatJÂ*

rfjj/imfa Vi r

t^H& , *TTflJ

SAMPLERnu (YiNi

^

fJ

ObHnttlont

<^

^

LABObMnallom

l jU pflAJ

<Ll>

CHAIN OF CUSTODY CHRONICLEShuttle Opened/fly: (priSignature: Afr v<

"^ Zi/**' GeeoJ Date: 3-1- S4* Time; ot-/r..,_ Seal #: oofK 4 Vti Intact: —

I nave received these materials In good condition from the above person. .. xnN8me: Jff/' GVOt-Jvr) Signature: ^/^ L^-^^J/

Date: ZBsapa*? Tim«: AlV'f Remarks: ' ^^-Î nave received these materials in good condition from the above person.Name: Signature: o r *?£ J /Date: Time: Remarks:

Snuttle Sealed B> (punSignature: ^^^

« ,Jê^ Â£&«*I'> o»<«: 2«i_oS<? Tlme: /8d0

LABUSEONL'SHUTTLE* .TEMP.'C

.Date:_SEAL*

.Time: 10: i.COND. .

ETC FIELD PARAMETER FORM (CC2) Form 0002SampM Man«g«mtnt

oe/w

ETC JOB » .Sample Point LJ II ifauJiQi \iMilZjej

S*mol* Point i.D.

FIELD PROCEDURESI ill 11 I i I I

VOLUMC PUNOfD

SAMPLING METHOD:

Sampler Type | MflA-SutuiwtlUU Pump P-OlpptrlBottlt

Sampler Material

Tubing Material

Sample Composited I >N I

B-ISCOC-BIUdw PumpA-TlflonB-M.l.lA-TttlonB-Tygon

E-BillwF-ScoopfShcnwlC-PVCC-PlutlcC-Poly<thyltn«D-Sillcon

X-Otlw

X-Oimr

X-Otnn

IWtCIFY OTHIHI

FIELD MEASUREMENTS

Well Elevation (ft/msl) I I I I i I I Well Depth (ft) [Depth to Ground water (ft) I I I IfSlfelCol Sample Depth (non-well) (ft) I I I i I IGroundwatec Elevation (ft msl) I I I I 1 I I

1st

2nd i3rd |

I I I I ____|

3rdL

4,hl I1H51/I..TB, 4th | |

Sample Appearance:_i l£2_&.FIELD COMMENTS

Weather Conditions:_5±&£m• V\

- TfcU «•? (&.$":? / - '3.3*?FILTERING: U«« Chain of Cmtody (CC1) to Indlcit* which bottlM w«r« lllt«r«d

Sampler: ~T>=f^. gM&.L<a.<^_______ Employer

I certify that sampling procedures were in accordance with applicable EPA state and corporate protocc^ Q

L^Thelnoln

ENVIRONMENTAL TESTING 9fttt CERTIFICATION Seal No. 2/SZZS2-ETC Job» Cftl?BO

CHAIN OF

Company:

Address:

CUSTODY

PELA

CITY DISPI

I90/VEXIT

FORM(CC1) ORIGINAL Da.eSaalad 89/U8/01 ^ . 0

. .. DAN GREENAttn.:

3SAL (414) 631 - 3190

12 AND 18 EAST, MADISON, UI 53704


Facility: L f P ? 1 1 1 1 1 1 1 I III Sample"Point Description*)

Sample Point: Ikil-l 1 ifrlUll B I Ife I Rigj I I 18^101312.181 Ulbl^ll I I I liSISOW'CI COW Vmif SMTIPI* tanl ID Sllrt 0>l« Sun THM IKMM *MHra

Sourer CoflM. '\Wtll..(W) OulUII.. ,IO) Bottom Stdimcnl. ...(B) Sufttci lmpoundm»nl... .(I) LMChal«CollMtl«nSy».....,|9Soil .|S1 Hivar/Stftitn (HI Qtntfitton Point ... .101 TrMtmtm Ficttlly .., . (Tl LahfOcttn ...............flj

SHUHLE CONTENTSBOULE

Type ANALYSISSAMPLER

ObeenietiailBUOP NONE UOLAT1LES A/TB 40 SOUS TRIP BLANK

EXT 1000 EXTRBXMS

EXT 1000 PST/PCB sMET 1000 HN03 METALS

/tt*

A/CHAIN OF CUSTODY CHRONICLE

Shuttle OpeneflBy (pnyt)Signature:

Date:Seal *: 6 1 «• -i -i

Time:" Intact:

Ifa-.-sn

I have received these materials in good condition Irom the above person.Name: T _,. .. Signature:

Jfff-Date: Time: ^"7-^3 Remarks:

I have received these materials in good condition Irom the above person.Name: Signature:


Shuttle Sealed ByMprinSignature: 4^J7

LAB USE ONLYSHUTTLE*

ETC FIELD PARAMETER FORM (CC2) Form 0002mpu Miugtmmt

ETC JOB # __Sample Point iC. i

FIELD PROCEDURES

Iu3i2.il I I i lid I iVOLUMI FUNQEO

SAMPLING METHOD:

Sampler Type [X/ol

Sampler Materl/BfM

Tubing Material \H/C\

Sample Composited I frN I

A-SuDffwraibU Pump D-Dlpptr/BottltB-ISCO E-BllKrC-Blwldw Pump F-Scoop/SKovM

0-PVCD-PlutlcC-PolyMhyKMD-Slllcon

XOtMr

X-Otlw

XOIhx

FIELD MEASUREMENTSi I I Well Depth (ft) |ZI31Z-|2-IWell Elevation (ft/msl)

Depth to Ground water (ft) I I I 1 1 V 15131 Sample Depth (non-well) (ft) I I I 1 I IGroundwater Elevation (ft msl) 1 I I I i I I

I I 1 I I I I

2nd I 1 I I I

3rd LLLISlll »TDI 3rd I I»

ith I \*%4\p\m» 4th Ll

I l I I li

I I I I I

FIELD COMMENTSSample App«.ranc.:

Weather Conmiionii;nth»r t Lj&Jj i*

7 -^ .7.7 _~ /FILTERING: Us* Chain of Custody (CC1) to IndlciU which bottl** w*r* fllt»r«d

Sampler: -J fpf^ &UC. M-»?T>>_____ Employer

I certify that sampling proceODles were In aeoaf3anceywlth applicable EPA Mate and corporate protocols.

TThe E< ORIGINAL 260

ENVIRONMENTAL TESTING tun CERTIFICATION ' Saal No. ^9' 44l> ETC Job »

CHAIN OF CUSTODY FORM (CC1) ORIGINAL P.I.S..I.H f-J-M ay

Company: _______

Facility/Site: /) /y^n

Address: _______

,: JW£

Phone:i- f/l/tf} aUtS - 4/SI

SAMPLE IDENTIFICATIONI i_l jFacility:

Sample Point: U1-I lifa u>Qil"ili ftft I II l3lZ-lll 'l I /jffl

Soure* CodM:Well .(W) OulUll. .Soil (Si HiwfSlf

... .(0) iottom Sediment .. . (B) Surtaet imooondmtnt . . ..(I) LeKhat* CoilMtton Syi. . .. .(0) '-m ,<R) Gene n lion Pot ni , , . .jO) Treaimeflt FeKiHty ......fT) Lihe/Ocetn .............. .)U ' g


No

f

!

1.

2.

3

iyp»

V

^

Slie

fi2_

4&L-

• •

Prater*.

$

Ms&L

JÂtJ^nh fasA+v**,A./Ja^r -T^vc

A///JJ TVA/

SAMPLERFHirr/N)

AJ

AJ

Obienitlont

^

LABObeeneHera

/"ff' ^^

N/

CHAIN OF CUSTODY CHRONICLEShuttle Opened/6V: (pri

// __ySignature: /d^^J.j" Â>J S/ZtfWJ D"*: ff-")-8«; Tim<: O~I: iT^ __ Seal*: <yo*-?« * 1O Intact: — »

I have received these materials in good condition from the above person. r / JNa™ -32^ FAJUA/& Signalura: M<y^^Date: ZSie^fl*? H"i*'-tf>&fM) Remarks: v&c^J

1 have received these materials in good condition from the above person.N ime: Signature:


Shuttle Sealed By: (pnijt)

Signature:Date: 2g,j<ylOT Tlm*:

Seal*: Prf »V/ ' Intact:'

SHUTTLE*.Time: //•'/*

TEMP -r sum .CONO. _&


ETC JOB #_Sample Point l!td II igiulfe li£igi(?i i I

Souica Coot Sample *wni 1.0.

FIELD PROCEDURESI/ 1? rei 1 1 I 1 1 id I i

SAMPLING METHOD: __

I »/ j A-SubmwslbU Pump D-DlpP*r'Bottl«Sampler Type \AIQ B-ISCO E-B«M.r

I C-8l«dd«r Pump F-ScoopfShov«l

Sampler Material | /ftq B'M*«I«" SPIMIIC

Tubing Material

.Sample Composited

FIELD MEASUREMENTSWell Elevation (ft/msl) I I I I i I I Well Depth (ft)Depth to Ground water (ft) I I I ll*/!?^! Sample Depth (non-well) (ft) I I I i I IGroundwater Elevation (ft msl)

1.1 1 rc-Lfl¥l <•"> 1$l I I I <7l I I-TI

...I \1\tij\ "TO, 2n(J I I I8I*?IÎ SR I ______ 1 I I I I i |_J•• -

3rd I llCl^lfl «™ 3rd I I

4th »"» 4th

FIELD COMMENTSSample Appearance:.WeatherOther:_L

23.12. -FILTERING: Uc* Chain ol Custody (CC1) to Indicate which bottla* war* tllterad

Sampler: ^/"f'f*- <gvUycyf/^'j/)_______ Employer. .

I certify that sampling procedures were in accordance with applicable ERA atata and corporate protocols.

262

\

CNViaOHUeNTAL TeSTINO tn<t CERTIFICATION Seal No CV S~77 5"ETC J Ob « CA1381

CHA/N OF CUSTODY FOBM (CC1) ORIGINAL Date Sealed By:

Company:. PELA Attn.: DAN GREEN

F»eiNty'Si.e: L'eYHOL?pSvftn<H napisou SMITH BUSTAddress:.

Phone:190^/EXIT 12 AND IB EAST, MADISON, UI 55704

(414) 631 - 3190


Facility: I f P ? I I I I I I I I 3fc_________•Fie-ltty/iit* COM ~~ ~ * IOOIWXWI Simp4f7Pwfll Des

Sample Point: IfcfUWir0! i i I i i i I \9\1\9\1\Zft\ I/|3|Z|/I

Sogrct Cofl«;Wtll . .(W Outfall. . . . . ,(O) BotiomS**m»ni... (B) SurtactImpoundment.,..())Soit . (S) Hlvcf/Strtim, .(B) Q«ntr»1 ten Point ... <O> TfMtmtnl Ftciltty . . . . . ,(T)


No Type Sli» ANALYSIS SAMPLER

40 NONE UOLftTILES AJTB 40 CCxtlS TRIP BLANK

EXT 1000 EXTRBXMS

EXT 1000 PST/PCB A*tlEI 100C HN03 METALS Y

300

I1"XfcOl V

itsCHAIN OF CUSTODY CHRONICLE

Shuttle Opened Iff: (priSignature: j

Date:' Seal»: *

Time:Intact:"

1 have received these materials in good condition from the above person.Name: Sl°n«tu":

Remarks:D»t«: -2Sa&oe'&*l Time:

1 nave received these materials in good condition from the above person.Name: Signature:


Shuttle Sealed By: (prin D*'*:*: **/**/&Seal*: 'ttJif^ttC. Intact:

i». i .«c nM. YSHUTTLE* .TEMP. 'C

Date:

FIELD PARAMETER FORM (CC2) Form 0002Sample Management

oe/si

ETC JOB*

Sample PolntX1£}" I i I i i t I

SAMPLING METHOD:

FIELD PROCEDURESI i/i,8| 1 i ,/ttel I i i \2A\-

Sampler TypeA-SuoneralbJe Pump D-Dlpper/BottleB-ISCO E-BallaiC-Bladdar Pump F-ScoopfShovel

Sampler Material

Tubing Material \% \ ti!

Sample Composited

C-PVCD-PlaatleC-PolyathyUnaD-Slllcon

X-Other

x-ottw

X-Othei


FIELD MEASUREMENTS

—I—LJ—I Well Depth (It) I

:nd I I \8\^\ f.2nd

3rd

sample Depth (non-well) (ft) I I I 1 I I

I I I

I I I I II |__|

ith 4th I I

/ l /Lip» t»«»

L?|rq JMTU

FIELD COMMENTSSample Appearance:.Weather Conditions:.

73. Z2'- /V.FILTERING: Use Chain of Custody (CC1) to indicate which bottles were filtered

Sampler: Employer

I certify that sampling procedure} were in ac with applicable EPA state and corporate protocols.

264

fNWflONMErVML TESTING «M CERTIFICATION Saal No " -44t ETCJObO f.O I3i 'I

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Date Sealed _£i£iZi By:

Company:

Facility/Site: J\u

Address:

^> '^Jff


Facility: I I I I I

Sample Point:

Souret Cod«:Well ..(W) Outfall...... ,|0) Bottom SMImtnt... .(6) Surface Impoundnwni,.. .(I) InchiM Co.Me.lon Sya.... .(Q -Otter . . . . . . .


No

f

1

Type

i>

*P

Site

Jf/>

lff>

1 " •

f

Preten.

(

lllS&L

ANALYSIS

JlJfAtAâf, fltnAA***.

JjjLfo* T2VS

Htu-njl

SAMPLERFlit (V/N)

A^

^

ObMnttlont

.X

^

LABObunatleiw

//// fl/LAjT)

0 '

^


1.

2.

3.

4.

Shuttle OpenedAy: (pri

Signature: fyL^ "^p/) * >|uj <~,e£Bij.e .

Date: a-T-6e\. Tim»: O~l: tSSeal*: ooY-Jf ito Intact: -^

I have received these materials in good condition from the above person. _. __Name: -r — ,. — ~ Sianature: /L^^z^T^' ^S*^

)ffV*' ftff-t-fl&JT} /JBfjff I

Date: y)~^*vS7 T|rn«; /3lijZS Remarks: <# .



Shuttle Sealed By: (prin

Signature: dLJ/sfZ-

LAB USE ONLY Ope*BHlfTTlC.

11 T.Vw.sn^c.JC.iA.Afo D*'*: ^9.4a-ft<? Time: [&(1><1>-*• w»J>< Seal*: 0ft* <? / Intact: ©fcr

TECp T. /* SEAL • <W/ CONH ~JfrfAJ-±

ETC FIELD PARAMETER FOhM (CCZ) Simple Management

ETC JOB #_

Sample Point

. ,/,V«7 FIELD PROCEDURES' l l i 3 i z i | I I ihSl l_i_ i i

VOUUMC PUMEO

SAMPLING METHOD:

Sampler TypeA'SubmwtlbM Pump D-DlpparfBottUB-ISCO E-BallatC-Bladdtr Pump F-ScoopfShovel

Sampler Material [ J tlT.'Ja"

Tubing Material \f^(_\ £J*

Sample Composited I >/N I

C-PVCD-Plaitlc

C-PolytlhyKmD-Slllcon

X-Otnar .

X-OtMr .

X-Otnti


"i 2ndH*

3rd L_Lkl±LU »TD1 3rdith I l^l^lBTD, 4th

I ill/ Jko

FIELD MEASUREMENTS

I I I I 1 I I Well Depth (ft) I_________I I III l.Sl.3 I Sample Depth (non-well) (ft) I I I 1 I II I I I 1 I I

I I

J I I I I I I |__|

L_LLJ_LJ«™

Sample Appearance:.Weather Conditions:."'"*'• inifvM Lat

FIELD COMMENTS

(.96*

r-a o^ prc. • 1 2" D,A

FILTERING: Us* Chain of Custody (CC1) to Indicate which bottlo w*f» filtered

Sampler: J fpP =AJ6-Cfrr T}_______ Employer


•206

^B *B* CNViaONUfNTAL TESTINB ma CERTIFICATION ' S»«l kfifcj.

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Date Seal

Company:

Facility/Site: _

Address: _

PELS

CITY DISPOSALerO MBLIPftV 1HHI90X/-EX1T 12 AND

I1BPI9BH SH1TH BUST ——18 EAST, MADISON, UI

tf ^?^W FTC.inh. CA1381

ad By /V. ( •

Ann, WN GREEN

_. (414) 631 - 3150

53704


Facility: L

Sample Point:

f P 7 1 1 1 1 1'•cii<iy<$itt COM

i 1 1 3e.i , , 1 I*3|fl f|2i8|"

1

i/iîVi "i \/ASou>e« Coot Togr tempi* FOMI IDllrom o*Kiw| (KM full if y) (VVfMMfDO) UNO hr. «M«K)

Score* Codti;W«ll . . (W) OulOll . . . . . . . 10) Bottom Stdtmtnt . . . . (B) Surlcc* t mpoundmtnt ... (I) LMcnal* Coiltetlon ftyt. . , .'.(Soil .|S) Rlw/Sirwn (H) G«n«f«lon Point . ..(0) Trwmtm FKcllliy . . ...,(T) L>htJOct«n ........... ...d

w


No

2

2

2

1

TypeUOP

EXT

EXT

MET

Size

40

1000

1000

1000

$>;;V '. '

Present.

NONE

none

none

HN03

ANALYSIS

UOLAT I LES

EXTRBXHS

PST/PCB

HETALS

SAMPLEDFIII rrm)

/s/

If

/vr

Obtenallent

,/

yy_/

LASObservations

u— - —^^— ~

l>~~~. . ^^_-

<_^—


1.

2.

3.

4.

Shuttle Opened Bf (pri

Signature: MJttm, '"V >>An ateevJ Date: fi.-s-a* Time: la-.os^_^ Seal#:ov«-nTjT !"<»=<: ^

I have received these materials In good condition from the above person. /^ f* ^-^Name: — ^^ Signature: /L^/ A*" — *" — '~

Date: 6l/2*/t^ Time: I7ftth Remarks: ^fA_S —



Shuttle Sealed By. (print) -Jff.m gjj A-fjnSignature: ^ . \*~&

Date: SH/ftl** Tima: itlS""T, 1^" X5 Seal* (B'/^-^-5^lntact: ip^n

LAB USE ONLY 6p«nidVSHUTTLE! ru. -r

_TUne:SEAL 267

ETC FIELD PARAMETER FORM (CC2) Form 0002Sampto M«nigMntnt

08/M

ETC JOB «Sample Point L l \D<(J\P\

BouruCa* I

FIELD PROCEDURES

Tff&fStSAMPLING METHOD:

SXKESL ILAntO MM WATI VOLUMI PUMf D

Sampler TypeA-SubmmlbU Pump D-DlppMBottMB-ISCOC-SI«dd«f Pump

Sampler Materlal

Tubing Material

Sample Composited ^/N

A-TXlon •B-M.i.l

C-PVCD-PlullcC-Poly«thylan«D-Sllicon

X-Othw

X-Otlwr

XOUw

Well Elevation (ft/msl)Depth to Ground water (tt)Groundwater Elevation (tt msl)

,.,

2nd

3rd

FIELD MEASUREMENTS . .

I I 1 I I Well Depth (ft) I I I !Sample Depth (non-well) (ft) I I I 1

J I I I I I

3rd I \W\9\ I J I

4m i iI \l\1tf\™

FIELD COMMENTSSample Appearance:.Weather Conditions:r..h., 6J0J 4~ >8Mjp AfrtCfM* #s*SX±rcr*»S

FILTERING: Us* Chain ot Custody (CC1) to Indicate which boHUt w»r«Vllt»r«d

Sampi.r Employer

I certify that sampling procedures were in accerOIpca with applicable EPA state and corporal* protocols.

4M

ENWBONMENMl TESTING ina CERTIFICATION Seal No

CHX/N OF CUSTODY FOflM (CC1) ORIGINAL Date Sealed.

.ETCJob* Cfll3B1

89/08/01 _By:.

Company:.

Facility/Site:.

PELA Attn.: DAN GREEN

CITY DISPOSAL9MITM CA9T . Phone: 631 - 3190

I90//EXIT 12 AND IB EAST, MADISON, UI 93704

SAMPLE IDENTIFICATIONf P V i . .

FK'l'lyJSH* CI3c

I I I I ISample Point:

Sourc* CodM:Wtll . .(W OutUii ... .(0) Bottom S«4im*nt... ,(B) Surfac* Impoundment... .|l)Soil (81 Biv«rJSlrtim .(«) Q«ntfitipn Point ..,.|Q) Treatment Pftclllly . . . . . .(T)


No

2

1

2

2

1

Type

uo<TB

EXT

EX1

HE!

.

Sin

40

40

1000

1000

1000

ivy*."^ S

•• t <i~»-.',j

•.-:..

PrMtrv.

NONE

sc/nsnone

none

HNOJ

V

1

UOLATILES

TRIP BLANK

EXTRB/nS

PST/PCB

METALS

e)

SAMPLERFHlfYfN)

fjM

/VA/y

ObMrvatloni

^

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^^fc*44&~ *»V-TT5

L*-^-

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wCHAIN OF CUSTODY CHRONICLE

1.

2.

3.

Shuttle Opened B^! (printy foAM &U&J

Signature: xir v2.»— -°»<* 8-s-4<\Seal »: <j »<T "n T \

Time: . -^ . ^QIntact: */

I nave received these rrtatenals in good condition from the above person. ^ f^> s^JName: tn/iL/ uur* Signature: S±^^7\ — "iP-i -^ (^

Date: o9/2fl/59 Time: J^ffd Remarks: ' £%^



Shuttle SealedSinature

SHUTTLE • . ffttfv. °

ETC FIELD PARAMETER FORM (CC2) FormOOOa^Mgwrwit

ETC JOB *Sample Point Ufl l£iKifl

•eurnCMta

W1WS?SAMPLING METHOD:

I'frVlSoil's!

FIELD PROCEDURES

VOLUMJJJ

Sampler Type

Sampler Material

Tubing Material \*/K,\

Sample Composited

/ A-Subnwilbto Pump O-Dlpw/Boltl.IC.\ B-isco E-atitot

C-Bi«M«r Pump F-Scoop/Shov.1

»n£tk>

<McrrOTH«~

*-T«flonB-Tyjon

FIELD MEASUREMENTS'I I I I 1 I I Well Depth (ft)I I i /itli <iti _ . _ . .

Well Elevation (fUmsl) i • i i * i i wen oeptn (ft)Depth to Ground water (ft) I I I /!*!*! 3|S| sample Depth (non-well) (ft)Groundwater. Elevation (ft msl) I I I I i I I

î*!2-!

1st 1M

,„, i iJ I I I I I I |_1

3rd I 3rd I

*th I II I I I I I.

I I I I I

FIELD COMMENTSSample App«»r«ne«r

Weather Conditions:n.h«,

FILTERING: Us* Chain of Custody (CC1) to Indlcat* which botttos w*r*1IU*r*d

Sampler:

licable EPA state and corporate protocols.

ORIGINAL 270

^^^^k ENVIRONMENT!!. TfSTINB tna CERTIFICATION Seal No lj/wU~>'7 ETC Job » CA1382

CHAIN OF CUSTODY FORM

Company:

Facility/Site:

Address:

PELA

CITY DISPOSAL

UCC1) OF"G1NAL D.,.a«.«. 89/09/25 By KC

Aim: CLAYTON LINOSEY

Phon.. (414) 431 - 3150C/0 HOLIDAY INN MADISON SMITH EASTI90//EXIT 12 AND 18 EAST. MADISON. UI 53704


Facility: L

Sample Point:

« 0 5 1 1 1 1 1

[XUF-iZ-iJiiBiLiA-iA1 1 1

xfci i 1 Brtldfl \i\1\ l/MicM 1 i i3l1

Sogrct CoM Vour $im»H) »oint ID(font Miowl ll*rt |u»Hly)

Sourct Codm:w»n .(W) Outfall...... .(0) Bottom Sediment.

BOTTLENo

?

3

1

1

1

1

1

1

1

1

iyp«Uflfl

EXT

MET

MET

COK

FL-

C»

con-» * *'coh

COK

Sin

40

1000

500

500

J 129

„•«?

sT'.W*i iif

i" "*5. - I2f

J 129

Prtttirv.

NONE

none

HN03

HN03

NONE

-NONE

H2S04

WS04

•H2S04

NONE

SHUTTLE CONTENTS

UOLATILES 1 MiA*aet>-t±.

exT/ns/ccMETALS

CYANIDE

CHLOR

FLUOR IDE

TOC

N03/N02

PHENOL

PH/SCONO

SAMPLERnit (mi

t*

fI1

fl

fJ

V

/

yj

fJ

J

Observations

S

^

S-

^

s^*sss

LABObeemMons

f^

£-"

L^^s/. L -

l "

l^

l^

(^


1.

2.

3.

4.

Shuttle Opened By: (print) £t/W'fi&/(J LJM&2?LfSignature: fÂ...^^.

Date: t&U&Jf^^™ 0?Z3T» l,-/,« ' Seal*: 6>/kdSTi Intact: ^jt

1 have received trMse Materials in gooAondltion from the above person. A / JName: r#j^ eus-t-**^ Siflnatura: 4M/<^~*-^Date: 2/7-SAtf £fl Time: / / "^S> Remarks: ' OG>—

1 nave received these materials in good condition trom the above person.Name: ' Signature:


Shuttle Sealed By: Iprtnt) J£rp, ^7 ^T^&C/tuJT )Signature: 'L/iAX^.

LAB USE ONLY pXvSHUTTLE t /4ote

Date: 2?5«i'5«? Tlme: ifdd^£~~*^^^r Seal*: j*|f, %-|rf ntact: erf. '

t<jft\P&r»,Lfaf>f^f<?r:«* AJ<7-C>f-3-f TUrr- 7'-'^^'

^-^ TEUP -C 7?" SEAL! 'n/tpn^&ClOHH jLSl&r J- K ~ -

FIELD PARAMETER FORM (CC2) Form 0002Sample McniMmwitoa/aa

ETC JOB* flA/^tJ

Sample Point U(J IFi UDifti^-iftifVi Vg 1 1SouitaCod* ftwnpM folnl 1.0.

FIELD PROCEDURES

lafigi r^ l/i'/iAidl 1 i i^l 1 i i i <p| 1 i i i (6\

SAMPLING METHOD:

l -"r"TP5ubm«filblt Pump D*Dlpp«rfBSampler Type r 1 nsco E-Biitor

C-Bladdar Pump F-ScoopfS

Sampler Material \**\ frMjii" £PIM«C

Tubing Material L±]*1 JS SffiT1

Sample Composited | Y/Nj

FIELD MlVUBll Elevation (tt/msl) 1 1 | | 1

Depth to Ground u/atar (ft) I ' l l !

Grounrtaatar Eluvation (M m«l) | ,..] 1 1 _, _

WIO HM WATIFI VOL. IN O*INO VQLUMt KJMCO<O«»oni) (OWienM

OttltX-OthW ,_., n,

1OV«I (WIClPY OTHIW

y.nth.rAHWvdTHi i

'•«rnoumiKoionlon

iASUREMENTS

. J w»"D»rth(«) 1 1 1 1 1 1__ 1 Sample Depth (non-WBll) (ft) 1 1 I 1 I I

u

1.1 1 1 1 1 1 <** 1lt I I I I I I SSfi, I I I I I I I I I IfH •*•«.«••«. (#**r*****l *MM VMM

Jnrtl I I I I -TO, .,„„ i i i i i i -- i I I i i i i M I*D •Wt.MHtL

M l l l l l m i M l l l l l l•« •**m«w-L

llhl I I I l»Tt» 4th I I I I I I

I I I I k« I I I I I

MhWMrMiMMt *MM wriM

ass. \ 1 1 1 1 1 1 1 1 1"™c ',«»»«-_, .«» ».»raa I I I II I I I 1 i

(•MWMTMMMO «MM uMto

I NTUSxnfM T«m. TlM«W«

FIELD COMMENTS

vv«alh«rCondltion«- ,>,„/«- &/V|lU. ftf«PT * iV^^ 5-^t ^^*

4 A*t \ r\ BD**/V -Pltlix

FILTERING: Us* Chain ol Custody (CC1) to Indicate which bottlM w«r» flltarsd

Samplar 3" ?^^ ^'/*&C'AfA& ttmnlnuar fffzL.rt

\ certify that sampling procedures were in accordance with applicable EPA atate and corporate protocols.

(Daw g ISfWuw

ThefmHn

^B^BW CNVIRONUCNTtL fSSriNQ ina CeariFICATIOH ' Seal NO. 4-3Q-44-0 ETC Job*

CHAIN OF CUSTODY FOflM (CC1) ORIGINAL Datesealed JL.

Company: __

Facility/Site: _A

Address:.

Attn.:.

Phnn.-

^ ttJft


Facility: I i i i i i i

s.mpi.pnint-Soure* Cod* Youi StmDit *«ni ID . sUrl Dl»(Irom Mlowl (HH pHUly] (VV/HMfODI

Source Codes: " *W«)l .(W) Owltttt. . ... .10) Bottom Sediment . . . .<B) Swrtace Impoundment . . ID Le«en«teColleetlon3n.'..,.<C} J;Soil (Si Rivef/Slre«m |B| Qenoelion Poini . . . .(Q\ Tf«>tm«n) Picltity . . . . . .(T) LthefOceen ............. i .(U t-

I i i3l

SHUTTLE CONTENTS

W -gf Type SUe Preterv. ANALYSIS nn ivmi ObunatlaiMSAMPLER

iutL

CHAIN OF CUSTODY CHRONICLEShuttle OpeneSignature:

Date: g.-,.^ Time: ,' Se«l«:oo^3«i f <to Intact:"

I have received these' materials in good condition Irom the above person.Name: Siflnature:


1 have received these materials in good condition trom the above person.Name: Signature:


Shuttle SealedSignature:

Date:Seal*: m<*ct: Off

/ft/TEMP.'C

.Date: »•-_SEALt -*1

.Time: /*•».COND. _t

ENVfflONMCNMl TESTING trot CCRTIflCATIOH

FIELD PARAMETER FORM (CC2)ETC JOB*.Sample Point 1}£J I &<-& iBili/»i<m l<i

SouritCeM SwnpM *w« 1.0.

FIELD PROCEDURESI/if iî^ I I i i3l I i i i mlssKfst «L«IOHM «AT«V«..»C^W I I I I I

VOUJHf

SAMPLING METHOD:

Sampler Type \'\ B-ISCO'———' C-BI«M«Pgmp

Sampler Material | '\ &M*<uT

Tubing Material

Sample Composited I Y/N

D-Olpp«f/Bottl«E-BallwF-Scooprahov.1

C-PVCD-Plutlc

C-PolyilhylwitD-Sllicon

XOirxr

xotiw .

X-Olh4i

Well Elevation (tt/msl)Depth to Ground water (ft)

FIELD MEASUREMENTSI I I I 1 I I well Depth (ft) 1 I II I I I i I I Sample Depth (non-well) (ft) I I I 1 I I

Groundwater Elevation (ft mal) I I I I i I I

1st I_L

2ndU_

I"™1 1st I_L

3rd I I I I I

2nd

3rd L

4th L M «n» 4th M IM L _LJ

J M M I

FIELD COMMENTSSample Appearance:.Weather Conditions: j UnQth.r (?B^CT

FILTERING: Us* Chain ol Custody (CC1) to IndlcaU which boni*s w«m IllUrtd

Sampler:

lance with applicable EPA state and corporate protocols.I certify that sampling procedures were In

f*VIRONUENT*L TESTING ma CERTIFICATIONV

CHAIN OF CUSTODY FORM |

Facility/Site:

Address:

PELA

CITY DISPOSALr yn HOL r PAY I MM M190/X EXIT 12 AND

'CCD ,„.„,„. L n,,.R.al.ri 89XO<?/14 Bu. KC

4(tn. CLAYTON LIN.1SEY

(414) 631 - 3150001 SOU SMITH CftOT —— Phone: ——————————————————————

18 EAST, MADISON, UI 53704


Facility: 1

Sample Point:

1 1 1 1 1 1 1 1 1FlollWftil* Coot

lujUl ifriWifiîAi i. 1 1 1

<ODi'on»i &«mpi« poini DncnDtiontl

i i 1 ISi*?! 1 idlld i Z-1 liifiVi^ 1 i5uilSoufc* COM vmi( 9anw«llrem M<owl lift Jullllvl (VVfMI

Sourc* Codes:W*II..(W) OutUII . .. ..(O) Bottom SMInwI... .(SI Surtact Impoundnwnl... .(I) LMChtl* CoMclIwi Sy«.. ...(CtSoil . .ISt RivffJSIrum (fl) Q«n«ialionPoint ....|Qt

SHUTTLE CONTENTS

ANALYSISSAMPLER LAB

UOA 40 NONE: UOUATILES

TB 40 cc/ns TRIP BLftNK

EXT looo EXTXMS

CXT 1000 EXTxPSTxPCBMET 1000 HN07 METALS I/

yoo

JZ.-5 («•(*««>

JVf &B*IP°I, A/A/or A/ t/

CHAIN OF CUSTODY CHRONICLEShuttle Opened By: (print)Signature: /2L**^T *

Time:" Intact:

I have received the** maferials in go#d condition from the above person.Name: Siflnature:

Date: 2 Tirt<«: Remarks: ' alt. (

I have received these materials in good condition from the above person.Name: Signature:


Shuttle Sealed By: (print)Signature: /S/

Tlma:

LAB USE ONLY C,SHUTTLE• |/ " * SBALi COMB.

ENVIRONMENTAL TESTING •»« CfRTIflCtTION

FIELD PARAMETER FORM (CC2)ETC JOB ».Sample Point JjjIJl Pi3iA i i i I

njMt DATErrt MuooiSAMPLING METHOD:

FIELD PROCEDURESI \sit&

WATER VOL. IN CASINO

Sampler Type |^j

Sampler Material I ffid

Tubing Material \A{C]

Sample Composited

A-SubnwilDIt Pump D-Dlppw/BotttoB-ISCO E-BtJMjr XOttwrC-BI«KlwPump F-ScooprenovW

C-PVOD-PlMlle X-OWnxC*PolyrthyMjfwD-Slllcon X-Ottw

Well Elevation (ft/msl)Depth to Ground water (ft)Qroundwater Elevation (ft msl)

FIELD MEASUREMENTS

I 1 I I Well Depth (ft)I I I /If 1^ I5"1 Sample Depth (non-well) (ft) I I II I I I i I I

1 I I

ut«• 2nd I I ISVf 13 I

3rd I IÎVITH «• 3rd I I

B, 4lh I I

I 1 / l l . f T T - e .l^l..ii

I IHTU

J IJ I I I I I I

Sample Appearance:.WeatheOther_

FIELD COMMENTS

-**.«.XV - Si.FILTERING: Us* Chain of Custody (CC1) to Indicate which botttes w*r* HlUrad

Sampler __ Ttff- ff)f%-J-A*l£}________ Employer

with applicable EPA state and corporate protocols.

ORIGINAL

^^^^^ CNVIRONUCNTAL TCSTINO lad CERTIFICATION ' Seal No 431-440 ETC Job II

CHAIN OF CUSTODY FORM (CC1) ORIGINAL DateSM|Bd /-J-/9 Ry..

Company:. LJffUL Attn.: J

Facility/Site: -(\it_nn

Address: _______

- Q/JI


I I I I I IFacility:

Sample Point: lu/l-l I ifrild Pk3i ftii(«CoM

1 I iSourct Codt vour tomtM »oini ID Sun 0*tt Sun TIMlirom MIO»I (i«tt m.rityt (YV'MM/00) (1«00 Mêtoeki

Sowrc* Codtt:W»tl . .(Wl Ouldll.. ... .(0) •otlofnSMimtnl,.. .(B)Soil .|Sl *iw>Slftim..<H) Qtntr»t*oo Point .. .(0) Tr«nm»nt Fictllly ......|T) Lak«0emn .

I ivfi^SlJliPMdMdun


Ne

,

1

'

1.

2.

3.

4.

Type

V

•f

Sue

stxn

ISO

*

: •

Preserv.

0

dtSfu

ANALYSIS

^//•ÂÂ /^Â^,^^

*L,/Jto* Tt>S0 '

SAMPLERFIII <vm^

/J

Observations

^

^

LABObservations

/y/y /I/^T)^

x /

CHAIN OF CUSTODY CHRONICLEShuttle Opened/By: (pri

Signature: JUt^ffcj,W "T\«..j f^rfftH Date: e-T-41 Tlme; CO.'cSn_ _ " Seal*: oot-Vk t *o Intact: ^

\ nave received these materials in good condition from the above person. /- ! ,_Name. ^- j&ijfj -t/*> Signature: / . ^ r' " ^^^

Date: 2«lTfl Time: C0V^" Remarks: 6r&K?**~'



Shuttle Sealed By: (print) "fffac- &^6-L.A-t,fo_Signature: rld!n Jr*

Date: loo-en Tlmr /7-3^^_J^ Seal* 0/f.rAn intact: «t '

LAB USE ONLY Op/ne^^xSHUTTLE* -r

.Date: _J_SEAL* .

Time:conn

ETC FIELD PARAMETER FORM (CC2) Form 0002 'Strnpl* Mimgwmnt

OS/tl

ETC JOB «

Sample Point lid 11SoutctCoM SwnpM mot 1.0.

FIELD PROCEDURESI I / I

SAMPLING METHOD:

Sampler Type

Sampler Material

A-SubmwtlbM PumpB-ISCOC-Bliddw Pump»-T«llonB-M«t«l

Tubing Material

Sample Composited I i<N I

D-DIOM«BOItl«E-BHKrF-ScoolKShowl

OPVCD-PIMIIC

OPolytinylnwD-Slllcon

X-Ottw

X-Otlwr

X-Ottui

Well Elevation (fl/msl)Depth to Ground water (It)Groundwater Elevation (tt msl)

„,

2nd

3rd

FIELD MEASUREMENTSI I I I i I. I Well Depth (ft) L/JI I I / tf W \f\ Sample Depth (non-well) (ft) I I I 1

ZndUlllILJ

3rd I

I I.Tl </l Jl

J I I I I I I |__|

J I I I I I I |__|

J I I I I I I |__|

i.hl -flare, 4th I I

Sample Appearance:_ jfi£&_FIELD COMMENTS

Weather Conditions: _Sja*Oth.r- (**./! C

FILTERING: U»« philn of Cuttody (CC1) to Indicate which bottl«> w»r« filtered

Sampler: "TtTy-g/O^-A-A-lTs ________ Employer

I certify that sampling procedures were IP-accordance with applicable EPA state and corporate protocols.

• • fc ENVIRONMENTAL TESTINO IM CERTIFICATION

CHAIN OF CUSTODY FORM (CC7)Seal No.

ORIGINAL Date Sealed. 89/09X14 -By:. KC

Company:.PELS Attn.: CLAYTON L1NDSEYCITY DISPOSAL

Facility/Site: c.'O IIOL1DAV 1API90H SMITH gHST631 - 3150

Address: I90XX EXIT 12 AND IB EAST, MADISON, UI 53704


Facility: I I I I I I IFKll'lyttilt CM*

i i i I ISample Point: i ia<m zi i 171*1

SoufCt Codtt:WtM (Wt Outfall. ... ..(0) Bottom S*llmtnt..Soil . .181 RivtrtSKMni . |Bt Q«rw»non Polnj . ,

..<B| Surf «ct Impoundment . . . .(I) lMCh»ttColl«etion>yt....(0) Tftilmtni f icllrty . . . . . . (T) Ukt/OcMn ..............

.(C) Pttwr ..(U

SHUTTLE CONTENTS

w BOTTLiANALYSIS nil (vim Obwntitlont

SAMPLER

UOA 40 NONE UOLATILES

TB 40 SCXMS TRIP BLANK

EXT 1000 EXTXMS A/EXT 1000 EXTXPSTXPCS

MET loon HN03 METALS

IV

A7n,?it* /I/

CHAIN OF CUSTODY CHRONICLEShuttle Opened By: (print) fj^vlM Ull/Kev

Signature: '*#£.difhesi

Date:' Seal*:

Time: ^_ ^" Intact: a*

I have received *mese materials<m good condition from the above person.Signature:

Date: Time: Remarks:: » *

1 have received these materials in good condition from the above person.Name. Signature:


Shuttle Sealed By: (print)

Signature:

Date: Timt:

LAB USE ONLY O^d ISHUTTLE* °*H — SEAL* . .CONO. . ttubtS

ENVIRONMENTAL TEST/NO ,ni CERTIFICATION

FIELD PARAMETER FORM (CC2)ETC JOB #.Sample Point ]M If i6-i

Soviet Coo*

FIELD PROCEDURESI i2ii>l

YMMOD)

SAMPLING METHOD:

Sampler Type

""SSSf

A-Subm«r«lblt Pump D-Dlpptr/BottliB-ISCO E.B«lltrC-Bi.aa.r Pump rscooptti«Mi

Sampler Material

Tubing Material \JJC,\ £

Sample Composited I?/N I

C-PVCD-PliillcC.?oly«1hyl«n.0-Sllleon


FIELD MEASUREMENTS * - "

I I I I i I I Well Depth (ft) LI I I I I H*? Iff I Sample Depth (non-well) (ft) I I I !

i,t l_L2L2_l±l2ndl_L2i£iZd

3rd I

18t

2nd

i •smJT.rr,. i____apM.MML (•**» tunm**H

\TO 3rd i i jjnfifli SR L_______| I I I I I I |__|«»*»JI pOfKIHM MkM MlHf

«thl_J_2L£L/J»™ 4m I I l^jVlQl ZSR I ^ I I I II INTU

FIELD COMMENTSSample Appearance:.Weather Conditions: <<-nv;r f-f-f1 it-tat** ft~HT*-Olh«r

,* yy -FILTERING: Us* Chain of Custody (CC1) to Indicate which bottlaa war* tlltarad

Sampler Jfr-,c f*>6-Ut+J£>______ Employer

I certify that sampling procedures accordance with applicable EPA state and corporate protocols.

INVmONUENTAL TESTING tna CERTIFICATION ' Sul Mn

CHAIN OF CUSTODY FORM (CC1) ORIGINAL DateSealed

Company:.

Facility/Site:.

Address:.

Attn.:. r\J"- f/.nl?) 332 -


Facility:

Sample Point: IU-I | I fc-ifcJl PA l&l i i i \8ft\ i \&d\z\SourciCoM1

(YWMMfOO)

Source CM«»:Well . (W) OutUII... .(0| Sottom SMimtnt.. ..(B) Surfcc*lmoown<tmtnl. .(I) UKhticCoHMtlonSys... ..(Q- bttor .....Soil .|S> Riv«ffStft«m ,(R| jtjn«filion Poini .. . .(0) Tftiinwrt Ficlllty . . . . . . fT) LlktypcMn ...............flj •HClty

SHUTTLE CONTENTS

Type ANALYSISSAMPLER

ih/

CHAIN OF CUSTODY CHRONICLEShuttle Opened fly: (priiat)Signature: }]r

Date: Time:" Intact:

I nave received these materials in good condition from the above person.Name: T__. ^nix-,..i*. Signature:

Date. ZPC.T- S3 Time: Remarks:

I have received these materials In good condition from the above person.Name: Signature:

Date. Time: Remarks:

Shuttle Sealed By: (ptim)Signature:

Date:Seal #:

SHUTTLE• TEUP - BBAL II

Tlma;

.CONO. _

•ETC FIELD PARAMETER FORM (CC2) Form 0002Sample Mtmgtnwnt.

OVM

ETC JOB *Sample Point Lbd II itriUJi P\Z ifti i i i I

source Coda ftanwM »wni 1.0.

\Sf(FIELD PROCEDURES

I iELAPSED MRS WATER VOL. IN CASINO VOLUME HJMID

SAMPLING METHOD:

Sampler Type |//d

Sampler Material 1

Tubing Material

Sample Composited I Y<N I

A-SubfTttrelbl* Pump D-Dlpptr/BottltB-ISCO - - "C-BI«ttw PumpA-T.llon

E-gallwF-Scoop/ShowlC-PVCD-PlMtic

C-Poly«lhyl«n«D-Sillcon

X-Otlw

x-othw

X-Otlwi

Well Elevation (fUmsl)Depth to Ground water (ft)Groundwater Elevation (ft msl)

i*t L_L2iVi£J «TO,

FIELD MEASUREMENTS

I—I—I—I i I I Wel I Depth (ft)I—I—I / IT'itlyl Sample Depth (non-well) (ft) I I 1 I I

i i

3rd I

2nd

3rd I

I I

\4\5\<\*r» 4th i iI INTU

FIELD COMMENTSSample Appearance:.Weather Conditions: J*"AUf l-ffl IMiJft 8/wlC 6S~*rOthl»f - " " - * - & ^ * ' - — - »_ -/ _^m -f .'•*» ^,^/-fl

FILTERING: Usa Chain of Custody (CC1) to InJIcata which bottlaa wara tlltarad

Sampler: Employer

I certily that sampling proceduresêre in with applicable EPA state and corporate protocols.

282irioM CompanyTIM Envir

ETC

LOG LINK

LABORATORY CHRONICLE: Metals Department

SAMPLES

fAtW\_____________

Hg Prep

AAPrep

ICAP Prep

Boron Prep

CHEMIST DATE

Lab Supervisor

283

bill

LOG LINK /CO


SAMPLES

Hg Prep

AAPrep

ICAP Prep

Boron Prep

CHEMIST DATE

Lab Supervisor Date

284

ETC

LOG LINK


SAMPLES

/Ansi

Hg Prep

AA Prep

ICAP Prep

Boron Prep

CHEMIST

fa -

DATE

Lab Supervisor Daw

285

LOG LINK


SAMPLES

Hg Prep

AAPrep

ICAP Prep

Boron Prep

CHEMIST DATE

/0 //-/T

Lab Supervisor Date

286

ETC

LOG LINK


Hg Prep

AAPrep

ICAP Prep

Boron Prep

SAMPLES

CHEMIST

/W

DATE

/J//»'C/

/-//.'fV

Lab Supervisor Date

287

ETC

LOG LINK / AJJ) a "


SAMPLES

A /in

Hg Prep

AAPrep

ICAP Prep

Boron Prep

CHEMIST DATE

la-H-P?

Lab Supervisor Date

288

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