United States Environmental Protection AgencyRegion 7

901 N. 5th StreetKansas City, KS 66101

2007Date:

Subject: Transmittal of Sample Analysis Results for ASR #: 3565

Project ID: BZA72ZRO

Project Description: Garvey Elevator site - Removal Oversight

A/ / 7^>From:°rDaksha Dalai, Acting Director (—^/ J ,, -Regional Laboratory, Environmental Services Division

To: Brian ZurbuchenSUPR/IANE

Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.

Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.

If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.

Enclosures

cc: Analytical Data File.

Page 1 of 10

ASR Number: 3565 Summary of Project Information 09/10/2007

Project Manager: Brian Zurbuchen Org: SUPR/IANE Phone:913-551-7101

Project ID: BZA72ZRO

Project Desc: Garvey Elevator site - Removal Oversight

Location: Hastings State: Nebraska Program: Superfund

Site Name: GARVEY ELEVATOR - SITEWIDE Site ID: A72Z Site OU: 00

Purpose: Site Characterization GPRA PRC: 302DD2C

This ASR is for sampling being conducted as oversight of a PRP contractor.

Explanation of Codes, Units and Qualifiers used on this report

Sample QC Codes: QC Codes identify the type of Units: Specific units in which results aresample for quality control purpose. reported.

= Field Sample % = PercentFB = Field Blank ug/kg = Micrograms per KilogramFD = Field Duplicate

Data Qualifiers: Specific codes used in conjunction with data values to provide additional informationon the quality of reported results, or used to explain the absence of a specific value.

(Blank)= Values have been reviewed and found acceptable for use.U = The analyte was not detected at or above the reporting limit.

UJ = The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.

Page 2 of 10

ASR Number: 3565

Project ID: BZA72ZRO

Sample Information Summary

Project Desc: Garvey Elevator site - Removal Oversight

09/10/2007

Sample QCNo Code Matrix Location Description

ExternalSample No

StartDate

StartTime

EndDate

EndTime

ReceiptDate

2 - __ Solid DPT-7, 80-81' bgs

3-_ Solid DPT-7, 90-91.5'bgs

3 - FD Solid DPT-7/Field Duplicate of sample 3

4-_ Solid DPT-7, 100-1021 bgs

5-_ Solid DPT-7, 110-110.5'bgs

6 - Solid DPT-4, 19.5-20' bgs

7 - _ Solid DPT-4, 39.5-40' bgs

8 - _ Solid DPT-4, 59.5-60' bgs

9 - Solid DPT-4, 79.5-80' bgs

10 - _ Solid S014D100SA

11 -_ Solid SO14D085SA

13 - FB Solid 5035 soil VOA Trip Blank sample

08/08/200708/09/200708/09/200708/09/200708/09/200708/09/200708/09/200708/09/200708/10/200708/15/200708/14/2007

18:0309:5109:5112:0014:5416:0216:2417:0908:3608:5515:15

08/08/200708/09/200708/09/200708/09/200708/09/200708/09/200708/09/200708/09/200708/10/200708/15/200708/14/2007

18:0509:5309:5312:0214:5516:0316:2517:1008:3709:0015:20

08/10/200708/10/200708/10/200708/10/200708/10/200708/10/200708/10/200708/10/200708/10/200708/16/200708/16/200708/10/2007

Page 3 of 10

ASR Number:3565 RLAB Approved Analysis Comments 09/10/2007

Project ID:BZA72ZRO Project DescGarvey Elevator site - Removal Oversight

Analysis Comments About Results For This Analysis

1 Percent SolidLab: Region 7 EPA Laboratory - Kansas City, Ks.

Method: EPA Region 7 RLAB Method 3142.9E

Samples: 2-_ 3-_ 3-FD 4-_ 5-_ 6-_ 7-_8- 9- 10- 11- 13-FB

Comments:(N/A)

1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-TrapLab: Region 7 EPA Laboratory - Kansas City, Ks.

Method: EPA Region 7 RLAB Method 3230.16C

Samples: 2- 3- 3-FD 4- 5- 6- 7-8- 9- 10- 11- 13-FB

Comments:Bromomethane was UJ-coded in samples 2, 3, 3-fd, 4, 5, 6, 7, 8, 9, 10, 11, and 13-fb. Thisanalyte was not found in the samples at or above the reporting limit, however, the reportinglimit is an estimate (UJ-coded) due to the initial instrument calibration curve not meetinglinearity specifications. The actual reporting limit may be higher than the reported value.

Slight Acetone contamination was found in the laboratory method blank. Only samplescontaining this analyte at a level greater than ten times the contamination level of the blank arereported without being qualified. All samples that contained this analyte but at a level less thanten times the contamination in the blank have the result U-coded indicating that the reportinglimit has been raised to the level found in the sample. Samples affected were: 13-fb.

Dichlorodifluoromethane was UJ-coded in samples 4, 8, 9, 10, 11, and 13-fb. This analyte wasnot found in the samples at or above the reporting limit, however, the reporting limit is anestimate (UJ-coded) due to low recovery of this analyte in the laboratory control sample. Theactual reporting limit for this analyte may be higher than the reported value.

Page 4 of 10

ASR Number: 3565

Project ID: BZA72ZRO

Analysis/ Analyte

RLAB Approved Sample Analysis Results

Project Desc: Garvey Elevator site - Removal Oversight

09/10/2007

Units 2-

1 Percent SolidSolids, percent

1 VOC's in Soil at Low LevelsAcetone

Benzene

Bromodichloromethane

Bromoform

Bromomethane

2-ButanoneCarbon DisulfideCarbon Tetrachloride

ChlorobenzeneChloroethane

Chloroform

Chloromethane

Cyclohexanel,2-Dibromo-3-Chloropropane

Dibromochloromethane

1,2-Dibromoethane

1,2-Dichlorobenzene1,3-Dichlorobenzene

1,4-Dichlorobenzene

Dichlorodifluoromethane1,1-Dichloroethane

1,2-Dichloroethane

1,1-Dichloroethenecis-l,2-Dichloroethene

trans-l,2-Dichloroethene

1,2-Dichloropropane

cis-l,3-Dichloropropenetrans- 1,3-Dichloropropene

Ethyl Benzene

2-HexanoneIsopropylbenzene

Methyl AcetateMethyl tert-butyl ether

Methyl cyclohexane

Methylene Chloride4- Methyl- 2-Pentanone

NaphthaleneStyrene

1,1/2,2-Tetrachloroethane

Tetrachloroethene

Toluene

1,2,3-Trichlorobenzene

1,2,4-Trichlorobenzene

%

by GC/MS Closed-Systemug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kgug/kg

ug/kgug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kgug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kgug/kg

ug/kg

ug/kgug/kg

ug/kgug/kg

ug/kg

ug/kgug/kg

ug/kgug/kg

ug/kgug/kg

ug/kg

ug/kg

ug/kg

96.7

Purge-and-Trap10 U

5.2 U

5.2 U

5.2 U

5.2 UJ

10 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

10 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

3-

95.8

10 U

5.0 U

5.0U

5.0 U

5.0 UJ

10 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

. 5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

10 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

3-FD

97.7

11 U

5.5 U

5.5 U

5.5 U

5.5 UJ

11 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

11 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

4-

97.7

13 U

6.3 U

6.3 U

6.3 U

6.3 UJ

13 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 UJ

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

13 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

Page 5 of 10

ASR Number: 3565

Project ID: BZA72ZRO

Analysis/ Analyte

RLAB Approved Sample Analysis Results

Project Desc: Garvey Elevator site - Removal Oversight

09/10/2007

Units 2- 3- 3-FD 4-

1,1,1-Trichloroethane

1,1,2-Trichloroethane

Trichloroethene

Trichlorofluoromethane

1,1,2-Trichlorotrifluoroethane

Vinyl Chloride

m and/or p-Xylene

o-Xylene

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.0 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

5.5 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3 U

6.3U

6.3 U

6.3 U

Page 6 of 10

ASR Number: 3565

Project ID: BZA72ZRO

Analysis/ Analyte

RLAB Approved Sample Analysis Results

Project Desc: Garvey Elevator site - Removal Oversight

09/10/2007

Units 5-

1 Percent SolidSolids, percent

1 VOC's in Soil at Low LevelsAcetone

BenzeneBromodichloromethaneBromoform

Bromomethane2-Butanone

Carbon Disulfide

Carbon Tetrachloride

ChlorobenzeneChloroethane

Chloroform

Chloromethane

Cyclohexanel,2-Dibromo-3-Chloropropane

Dibromochloromethane1,2-Dibromoethane

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Dichlorodifluoromethane

1,1-Dichloroethane1,2-Dichloroethane

1,1-Dichloroethene

cis-l,2-Dichloroethene

trans-l,2-Dichloroethene

1,2-Dichloropropane

cis-l,3-Dichloropropenetrans- 1,3-Dichloropropene

Ethyl Benzene2-Hexanone

Isopropylbenzene

Methyl Acetate

Methyl tert-butyl ether

Methylcyclohexane

Methylene Chloride4-Methyl-2-PentanoneNaphthalene

Styrene

1,1,2,2-TetrachloroethaneTetrachloroethene

Toluene1,2,3-Trichlorobenzene

1,2,4-Trichlorobenzene

%

by GC/MS Closed-Systemug/kg

ug/kgug/kg

ug/kg

ug/kgug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kgug/kg

ug/kgug/kg

ug/kgug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kgug/kg

ug/kgug/kgug/kg

ug/kg

ug/kgug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kgug/kg

ug/kg

ug/kg

ug/kgug/kg

ug/kg

ug/kg

ug/kg

94.3

Purge-and-Trap13

5.1 U

5.1 U

5.1 U

5.1 UJ

10 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

10 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

5.1 U

6-

81.7

12 U

5.8 U

5.8 U

5.8 U

5.8 UJ

12 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5,8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

12 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

5.8 U

7- 8-

85.1

11 U

5.4 U

5.4 U

5.4 U

5.4 UJ

11 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

' 5.4 U

5.4 U

5.4 U

5.4 U

5.4 U5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

11 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

5.4 U

90.3

9.3 U

4.7 U

4.7 U

4.7 U

4.7 UJ

9.3 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 UJ

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

9.3 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

Page 7 of 10

ASR Number: 3565

Project ID: BZA72ZRO

Analysis/ Analyte

RLAB Approved Sample Analysis Results

Project Desc: Garvey Elevator site - Removal Oversight

09/10/2007

Units 5- 6- 7- 8-

1,1,1-Trichloroethane1,1,2-Trichloroethane

Trichloroethene

Trichlorofluoromethane1,1,2-Trichlorotrifluoroethane

Vinyl Chloride

m and/or p-Xylene

o-Xylene

ug/kgug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

5.1

5.1

5.1

5.1

5.1

5.1

5.1

5.1

U

U

U

U

U

U

U

U

5.8

5

5

5

5

5

5

5

.8

.8

.8

.8

.8

.8

.8

U

U

U

U

U

U

U

U

5.

5.

5,

5,

5,

5

5,

5

.4

4

A

A

A

A

A

A

U

U

U

U

U

U

U

U

4.

4.

4.

4.

4.

4.

4.

4.

7

7

7

7

7

7

7

.7

U

U

U

U

U

U

U

U

Page 8 of 10

ASR Number: 3565

Project ID: BZA72ZRO

Analysis/ Analyte

RLAB Approved Sample Analysis Results

Project Desc: Garvey Elevator site - Removal Oversight

09/10/2007

Units 9-

1 Percent SolidSolids, percent % 95.6

1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-TrapAcetoneBenzeneBromodichloromethane

Bromoform

Bromomethane

2-Butanone

Carbon Disulfide

Carbon Tetrachloride

Chlorobenzene

Chloroethane

Chloroform

Chloromethane

Cyclohexane

l,2-Dibromo-3-Chloropropane

Dibromochloromethane

1,2-Dibromoethane

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Dichlorodifluoromethane

1,1-Dichloroethane

1,2-Dichloroethane

1,1-Dichloroethene

cis-l,2-Dichloroethene

trans-l,2-Dichloroethene

1,2-Dichloropropane

cis-l,3-Dichloropropenetrans-l,3-Dichloropropene

Ethyl Benzene2-Hexanone

Isopropylbenzene

Methyl Acetate

Methyl tert-butyl ether

Methylcyclohexane

Methylene Chloride4-Methyl-2-Pentanone

Naphthalene

Styrene

1,1,2,2-Tetrachloroethane

Tetrachloroethene

Toluene

1,2,3-Trichlorobenzene

1,2,4-Trichlorobenzene

10-

93.5

11-

97.4

13-FB

99.3

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

11 U5.6 U5.6 U5.6 U5.6 UJ

11 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 UJ

5.6 U

5.6 U

5.6 U

5. 61)

5.6 U

5.6 U

5.6U

5.6 U

5.6U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

11 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

9.4 U

4.7 U

4.7 U

4.7 U

4.7 UJ

9.4 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 UJ

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

9.4 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

11 U

5.3 U

5.3 U

5.3 U

5.3 UJ

11 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 UJ

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

11 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

12 U

5.2 U

5.2 U

5.2 U

5.2 UJ

10 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 UJ

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

10 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

Page 9 of 10

ASR Number: 3565

Project ID: BZA72ZRO

Analysis/ Analyte

RLAB Approved Sample Analysis Results

Project Desc: Garvey Elevator site - Removal Oversight

09/10/2007

Units 9- 10- 11- 13-FB

1,1,1-Trichloroethane

1,1,2-Trichloroethane

TrichloroetheneTrichlorofluoromethane

1,1,2-Trichlorotrifluoroethane

Vinyl Chloride

m and/or p-Xyleneo-Xylene

ug/kg

ug/kg

ug/kgug/kg

ug/kg

ug/kg

ug/kgug/kg

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

4.7 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.3 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

5.2 U

Page 10 of 10

CHAIN OF CUSTODY RECORDENVIRONMENTAL PROTECTION AGENCY REGION VII

ACTIVITY LEADER(Print) NAME OF SURVEY OR ACTIVITY £34 JZZ&O DATE OF COLLECTION

DAY MONTH YEAR

SHEET

CONTENTS OF SHIPMENT

SAMPLENUMBER

TYPE OF CONTAINERS

BOHLE BOTTLE BOHLEVOA SET

iQIVIALS EA)

y(<iUMBERS Or CONTAINERS PER SAMPLE NUMBER

SAMPLED MEDIA RECEIVING LABORATORYREMARKS'OTHER INFORMATION

(condition ol samples upon receipiolhe' sample numbers, etc )

»feS>vsjL_£<*

X^

KA1

/I

VV

DESCRIPTION OF SHIPMENT MODE OF SHIPMENT \

i CONSISTING OF.

. ICECHEST(S): OTHER

. BOX(ES)

•S

-COMMERCIAL CARRIER:.

SAMPLER CONVEYED (SHIPPING DOCUMENT NUMBER)

PERSONNEL CUSTODY RECORD

") SEALED

BY (SAMPLER)

UNSEALED

DATE TIME

n

RECEIVED BY

EALED UNSEALED

REASON FOR ORANGE OF CUSTODY

RELINQUISHED BY / DATE TIME

~1 SEALED UNSEALED [~

RECEIVED BY

~| SEALED

REASON FOR CHANGE OF CUSTODY

UNSEALED [""

RELINQUISHED BY DATE TIME RECEIVED BY REASON FOR CHANGE OF CUSTODY

ISEALED UNSEALED^ ~~ JSFALED UNSEALED^

7-EPA-9262(Revised 5/85)

CHAIN OF CUSTODY RECORDNVIRONMENTAL PROTECTION AGENCY REGION VII

ACTIVITY LEADER(Print)\ V v > TT^-

NAME OF SURVEY OR ACTIVITY t

"- tlArV

CONTENTS OF SHIPMENT

SAMPLENUMBER

35Co5-X/l

35U»5-\0V

\\

r" 1 V/'X'VCiT"

DATE OF COLLECTION SHEET"•11^ •* 0 4- L" o(l

DAY MONTH YEAR \ | \

TYPE OF CONTAINERS

CUBITAINER BOTTLE BOTTLE BOTTLE

NUMBERS OF CONTAINERS PER SAMPLE

*A

\

Xx^

NV /

\/

/\

/

i

\\

VOA SET(2 VIALS EA|

NUMBER

^s^

/

/

/

/

N! jN

^^^^

DESCRIPTION OF SHIPMENT

piFrF(^) r.(

\ ICE CHEST!

)NSISTING OF

SV OTHFR

n r\y / r c \

PERSONNEL CUSTODY RECORDFIELINQUISHED BY (SAMPLER) DATE TIME

/W%40/.Ax/t:/ ' %-IUrOl I'lOOvVsEALEo] UNSEALED (~

RELINQUISHED BY DATE TIME

~1 SEALED UNSEALED f~~

RELINQUISHED BY DATE TIME

~1 SEALED UNSEALED[~~

" ^

)

/

^O//?,x///x/ x

\

SAMPLED MEDIA

f

s,

1

I.

\

± — '

•3.

XX

\

^

sx

sedi

men

t

\

^^

V

^

r>

\

/

\

oitief

\\

1

/

/

\j

RECEIVING LABORATORYREMARKS/OTHER INFORMATION

(condition of samples upon icceipi.otner sampie numbeis. etc )

^CL r ^J £*»Y>L- HyJo4//.#t^ *i i ^/Cf -f- i /j, f ~ t>U -0'Cj f ' 1

^MrtLU+J iSli$rk#**-~

ftp <4jLf*J>fj

tSfC^ ' WWn^ ^c-(fit] H t u, ux^^ ^

' . .y

& ' t (• /j

fj/r.t^rd &£<U/

\ h^>~. o -i °,\\

\\

MODE OF SHIPMENT

nnMMFrniiRiE

RCIAL CARRIER3

— ^-SAMPLER CONVEYED (SHIPPING DOCUMENT NUMBER)

RECEIVED BY

^2] SEALED ^ UNSEALED [~

RECEIVED BY

ISEALED UNSEALED PRECEIVED BY

^SEALED UNSEALED^

REASON FOR CHANGE OF CUSTODY

ycjtt^ tJL tjL\ l<zJoREASON FOR CHANGE OF CUSTODY

REASON FOR CHANGE OF CUSTODY

7-EPA-9262(Revised 5/85)

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 3565 Sample Number: V" QC Code: _ Matrix: Solid Tag ID: 3565

Project ID: BZA72ZRO Project Manager: Brian ZurbuchenProject Desc: Garvey Elevator site - Removal Oversight

City: Hastings State: NebraskaProgram: Superfund

Site Name: GARVEY ELEVATOR - ON-SITE SOILS AND Site ID: A72Z Site OU: 01GROUNDWATER

Location Desc:

External Sample Number:

Expected Cone: (or Circle One: -ov> Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End: £^yO*/£7

Laboratory Analyses:Container Preservative Holding Time Analysis

2 - 40mL VOA vial 4 Deg C, H2O + sodium 14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System(preserved/tared) bisulfate (in vial) Purge-and-Trap

Sample Comments:

(N/A)

Sample Collected By: AR

1 of 1

Sample Collection Field SheetUS EPA Region 7Kansas^Gity, KS

(JASR Number: 3565 Sample Number: V QC Code: _ Matrix: Solid Tag ID: 3565-ft

Project ID: BZA72ZRO Project Manager: Brian ZurbuchenProject Desc: Garvey Elevator site - Removal Oversight

City: Hastings State: NebraskaProgram: Superfund

Site Name: GARVEY ELEVATOR - ON-SITE SOILS AND Site ID: A72Z Site OU: 01GROUNDWATER

Location Desc: t>PT 7 t>Lf>Tj *)C - ?/.

External Sample Number:

Expected Cone: (or Circle One: Q-ow\ Medium High) Date Time(24 hr)

Latitude: ___ Sample Collection: Start:.

Longitude: ___ E

Laboratory Analyses: ,£nContainer Preservative Holding Time Analysis ^f U&^&L-6t~

2 - 40mL VOA vial 4 Deg C, H2O + sodium 14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System(preserved/tared) bisulfate (in vial) Purge-and-Trap

Sample Comments:

(N/A)

Sample Collected By: AR

1 of 1

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 3565 Sample Number: QCCode:^* Matrix: Solid Tag ID:

Project ID: BZA72ZRO Project Manager: Brian ZurbuchenProject Desc: Garvey Elevator site - Removal Oversight

City: Hastings State: NebraskaProgram: Superfund

Site Name: GARVEY ELEVATOR - ON-SITE SOILS AND _Site ID: A72Z Site OU: 01GROUNDWATER

Location Desc:

Expected Cone:

Latitude:

Longitude:

(or Circle One: Medium

External Sample-Number:

Date

Sample Collection: Start:" \

EndK^&

Time(24 hr)

Laboratory Analyses:Container

2 - 40mL VGA vial(preserved/tared)

Preservative

4 Deg C, H2O + sodiumbisulfate (in vial)

Holding Time

14 Days

Analysis ~

1 VOC's in Soil at Low Levels by GC/MS Closed-SystemPurge-and-Trap

Sample Comments:

(N/A)

Sample Collected By: AR

1 of 1

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 3565 Sample Number: QC Code: Matrix: Solid Tag ID:

Project ID: BZA72ZRO Project Manager: Brian ZurbuchenProject Desc: Garvey Elevator site - Removal Oversight

City: Hastings State: NebraskaProgram: Superfund

Site Name: GARVEY ELEVATOR - ON-SITE SOILS AND Site ID: A72Z Site OU: 01GROUNDWATER

Location Desc:

Expected Cone:

Latitude:

Longitude:

f / ? <

External Sample Number:

(or Circle One: Low Medium High)

Sample Collection: Start:

Date

End:

Time(24 hr)

\»/.

Laboratory Analyses:Container Preservative

- 40mL VGA vial(preserved/tared)

4 Deg C, H2O + sodiumbisulfate (in vial)

Holding Time

14 Days

Analysis

1 VOC's in Soil at Low Levels by GC/MS Closed-SystemPurge-and-Trap

Sample Coirupeatst

(N/A)

Sample Collected By: AR

1 of 1

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 3565 Sample Number QC Code: Matrix: Solid Tag ID: 3565-V-

Project ID: BZA72ZRO Project Manager: Brian ZurbuchenProject Desc: Garvey Elevator site - Removal Oversight

City: Hastings State: NebraskaProgram: Superfund

Site Name: GARVEY ELEVATOR - ON-SITE SOILS AND Site ID: A72Z Site OU: 01GROUNDWATER

Location Desc:

Expected Cone:

Latitude:

Longitude:

-//a, <"

External Sample Number:

(or Circle One: Low Medium High)

Sample Collection: Start:

Date Time(24 hr)

En

Laboratory Analyses:Container

2 - 40mL VGA vial(preserved/tared)

Preservative

4 Deg C, H20 + sodiumbisulfate (in vial)

Holding Time

14 Days

Analysis -

1 VOC's in Soil at Low Levels by GC/MS Closed-SystemPurge-and-Trap

Sample Comments:

(N/A)

Sample Collected By: AR

1 of 1

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 3565 Sample Number: QC Code: Matrix: Solid Tag ID: 3565-;B-

Project ID: BZA72ZRO Project Manager: Brian ZurbuchenProject Desc: Garvey Elevator site - Removal Oversight

City: Hastings State: NebraskaProgram: Superfund

Site Name: GARVEY ELEVATOR - ON-SITE SOILS AND Site ID: A72Z Site OU: 01GROUNDWATER

Location Desc:

Expected Cone:

Latitude:

Longitude:

f-r

External Sample Number:

(or Circle One: //Cow) Medium High)

Sample Collection: Start:

End: '

Date Time(24 hr)

Laboratory Analyses:Container

2 - 40mL VGA vial(preserved/tared)

Preservative

4 Deg C, H2O + sodiumbisulfate (in vial)

Holding Time

14 Days

Analysis

1 VOC's in Soil at Low Levels by GC/MS Closed-SystemPurge-and-Trap

Sample Comments:

(N/A)

Sample Collected By: AR

1 of 1

Sample Collection Field SheetUS EPA Region 7Kansars City, KS

ASR Number: 3565 Sample Number: QC Code: Matrix: Solid Tag ID: 3565-

Project ID: BZA72ZRO Project Manager: Brian ZurbuchenProject Desc: Garvey Elevator site - Removal Oversight

City: Hastings State: NebraskaProgram: Superfund

Site Name: GARVEY ELEVATOR - ON-SITE SOILS AND Site ID: A72Z Site OU: 01GROUNDWATER

Location Desc:

Expected Cone:

Latitude:

Longitude:

Dpr4(£>??.<External Sample Number:

(or Circle One: /Cow) Medium High)

Sample Collection: Start:

Date Time(24 hr)

End

Laboratory Analyses:Container

2 - 40mL VOA vial(preserved/tared)

Preservative

4 Deg C, H2O + sodiumbisulfate (in vial)

Holding Time

14 DaysAnalysis

I VOC's in Soil at Low Levels by GC/MS Closed-SystemPurge-and-Trap

Sample Comments:

(N/A)

Sample Collected By: AR

1 of 1

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 3565 Sample Number: QC Code: _ Matrix: Solid Tag ID: 3565-^-

Project ID: BZA72ZRO Project Manager: Brian ZurbuchenProject Desc: Garvey Elevator site - Removal Oversight

City: Hastings State: NebraskaProgram: Superfund

Site Name: GARVEY ELEVATOR - ON-SITE SOILS AND Site ID: A72Z Site OU: 01GROUNDWATER

Location Desc:

Expected Cone:

Latitude:

Longitude:

External Sample Number:

(or Circle One: Low Medium High)

Sample Collection:

Date Time(24 hr)

17 :d

Laboratory Analyses:Container

2 - 40mL VGA vial(preserved/tared)

Preservative

4 Deg C, H2O + sodiumbisulfate (in vial)

Holding Time

14 Days

Analysis °

1 VOC's in Soil at Low Levels by GC/MS Closed-SystemPurge-and-Trap

Sample Comments:

(N/A)

Sample Collected By: AR

1 of 1

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 3565 Sample Number: QC Code: Matrix: Solid Tag ID: 3565-

Project ID: BZA72ZRO Project Manager: Brian ZurbuchenProject Desc: Garvey Elevator site - Removal Oversight

City: Hastings State: NebraskaProgram: Superfund

Site Name: GARVEY ELEVATOR - ON-SITE SOILS AND Site ID: A72Z Site OU: 01GROUNDWATER

Location Desc:

Expected Cone:

Latitude:

Longitude:

- 9*0

External Sample Number:

(or Circle One: Low Medium High) Date

Sample Collection: StarV^/JO

Time(24 hr)

45 J_£

Laboratory Analyses:Container Preservative

2 - 40mL VOA vial(preserved/tared)

4 Deg C, H20 + sodiumbisulfate (in vial)

Holding Time Analysis -

14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-SystemPurge-and-Trap

Sample Comments:

(N/A)

Sample Collected By: AR

1 of 1

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

10ASR Number: 3565 Sample Number: &•&- QC Code: Matrix: Solid Tag ID:

Project ID: BZA72ZRO Project Manager: Brian ZurbuchenProject Desc: Garvey Elevator site - Removal Oversight

City: Hastings State: NebraskaProgram: Superfund

Site Name: GARVEY ELEVATOR - ON-SITE SOILS AND Site ID: A72Z Site OU: 01GROUNDWATER

Location Desc:

External Sample Number:

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End:

Laboratory Analyses:Container Preservative Holding Time Analysis

2 - 40mL VOA vial 4 Deg C, H2O + sodium 14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System(preserved/tared) bisulfate (in vial) Purge-and-Trap

Sample Comments:

(N/A)

ByWVR-

1 of 1

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 3565 Sample Number:^ QC Code: _ Matrix: Solid Tag ID:

Project ID: BZA72ZRO Project Manager: Brian ZurbuchenProject Desc: Garvey Elevator site - Removal Oversight

City: Hastings State: NebraskaProgram: Superfund

Site Name: GARVEY ELEVATOR - ON-SITE SOILS AND Site ID: A72Z Site OU: 01GROUNDWATER

Location Desc:

External Sample Number:

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End:

Laboratory Analyses:Container Preservative Holding Time Analysis

2 - 40mL VOA vial 4 Deg C, H2O + sodium 14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System(preserved/tared) bisulfate (in vial) Purge-and-Trap

Sample Comments:

(N/A)

-Sample-Gel teGt-ed-Byi-AR-

1 of 1

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 3565 Sample Number: QC Code: Matrix: Solid Tag ID; 3 U

Project ID: BZA72ZRO Project Manager: Brian ZurbuchenProject Desc: Garvey Elevator site - Removal Oversight

City: Hastings State: NebraskaProgram: Superfund

Site Name: GARVEY ELEVATOR - ON-SITE SOILS AND Site ID: A72Z Site OU: 01GROUNDWATER

Location Desc:

Expected Cone:

Latitude:

Longitude:

External Sample Number:

(or Circle One:^tovv^Medium High)

Sample Collection: Start:

End:

Date Time(24 hr)

Laboratory Analyses:Container

2 - 40mL VGA vial(preserved/tared)

Preservative

4 Deg C, H2O + sodiumbisulfate (in vial)

Holding Time Analysis ^ ffi^l C. /,1 ,14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System

Purge-and-Trap

Sample Comments:

(N/A)

Sample Collected By: AR

1 of 1