+ All Categories
Home > Documents > United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of...

United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of...

Date post: 24-Aug-2020
Category:
Upload: others
View: 6 times
Download: 0 times
Share this document with a friend
202
Regional OftW Wester:n Region, Kendriy a-pdfyava ra n Bh ava n, United Phosphorus Limited 7461750, G.l.D;Q.,P. B. No. g, Jhagadia993 110, Dist. Bharuch, Gujarat. Phone: (02645) 226011-15 o Fax: (0A645) 2260:t7-18 .1 i .i'} $ Responsible Care" \'--,,i Ref. : UPL/Jhg/E Nv / 27 /2013/0 1 To, Dr. A.'Mehrotra, Dir:ector (S), Ministryof Envir nt & Forest, Dear Sir, Lin\fid No. 3, Ravi Shankar Nagar AL - 462 016 (M.P.) Sub. : Half Yearly Report Ref.: 1. Environmental clearance No. 1.130 tL/26/96-tA.II, Combined CycleCo. Generation power plant. 2. Environmenral Clearance No. J-1j.01I/42/gS-A.II (1), -Chlor-Alkali Plant. '3. Environmental Clearance No. J- j.101L/325/2006-iA II P rodu cts ' ..) Cc: (1) The Zonal CPCB, Baroda GPCB XGNID # 25353 February 25, 201.3 dtd. 24th. Dec., 1996 of 50 MW dtd. 17th. May, 1996 of t 00 TpD (I) dtd. 25th July 2007 for various r.a w-e tlerebysubmit half-yearly Report,, consisting ofthe following detailsfor thc period startingfrom July 2012 to Decembe( - 201.2 tor your evatuation & records. l1 stalus of compliancc of conditions mentioned in above three Environmental clea.rances. 2) Ambient Air Monitoring Report. 3) Stack Monitoring. Report. . 4) Noise Level Monitoring Report. 5) Waste WaterAnalysis Report. 6) Ground Water euality Report. 7) Soit Analysis rcport. 8) Solid Waste Analysis report. 9) Details of Green Bclt F)eveloDment. , f0) Dctails of Expenditure on various pollution Control Measure_s. Pl refer Environmentat ctoarance No.J-11011/325/2006_14 II (I) dtd. 25th )uly 2OO7 for various products . GPCB has issued Consent to Establish (NOC) form. NOC copyis attached in Annexure _1 for your ready ,' reference. out of the various.products mentioned in EC, wi -r" ;nu"riiitrri"g rvun."r"i ino We trust that thesc dct-ails arc in line with your requirements. Kindly acknowledge rcccipt of the same. Thanking You, Yours faithfully, for united Phosphorus Ltd, Unit Head, Encl.: a . a. Mumbal office : ruNrPHos" Houso, c.E.Marg, 11Jh Road, Khar (w), Mumbai. Phone : (OZ2l 26469000-111 r Fax: {0lZ2\ ZOoOOzOO. S. M Chakra=5ortY
Transcript
Page 1: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

Regional OftW Wester:n Region,Kendriy a-pdfyava ra n Bh ava n,

United Phosphorus Limited7461750, G.l.D;Q., P. B. No. g, Jhagadia 993 110, Dist. Bharuch, Gujarat.

Phone: (02645) 226011-15 o Fax: (0A645) 2260:t7-18 .1

i

.i'}

$Responsible Care"

\'--,,i

Ref. : UPL/Jhg/E Nv / 27 /2013/0 1

To,Dr. A . 'Mehro t ra ,Dir :ector (S),Ministry of Envir nt & Forest ,

Dear S i r ,

L in\ f id No. 3, Ravi Shankar NagarA L - 4 6 2 0 1 6 ( M . P . )

Sub. : Half Yearly ReportR e f . : 1 . E n v i r o n m e n t a l c l e a r a n c e N o . 1 . 1 3 0 t L / 2 6 / 9 6 - t A . I I ,

Combined Cyc le Co. Genera t ion power p lan t .2 . E n v i r o n m e n r a l C l e a r a n c e N o . J - 1 j . 0 1 I / 4 2 / g S - A . I I ( 1 ) ,

- C h l o r - A l k a l i P l a n t .' 3 . E n v i r o n m e n t a l C l e a r a n c e N o . J - j . 1 0 1 L / 3 2 5 / 2 0 0 6 - i A I IP rod u cts '

..)

C c : ( 1 ) T h e Z o n a lCPCB, Baroda

G P C B X G N I D # 2 5 3 5 3

February 25, 201.3

d t d . 2 4 t h . D e c . , 1 9 9 6 o f 5 0 M W

d t d . 1 7 t h . M a y , 1 9 9 6 o f t 0 0 T p D

( I ) d t d . 2 5 t h J u l y 2 0 0 7 f o r v a r i o u s

r.aw-e tlereby submit half-yearly Report,, consisting ofthe following details for thc period starting from July2012 to Decembe( - 201.2 tor your evatuation & records.

l1 stalus of compliancc of conditions mentioned in above three Environmental clea.rances.2) Ambient Ai r Moni tor ing Report .3) Stack Moni tor ing. Report .

. 4) Noise Level Monitoring Report.5) Waste Water Analysis Report.6) Ground Water eual i ty Report .7) Soit Analysis rcport.8) Solid Waste Analysis report.9) Deta i ls of Green Bcl t F)eveloDment .

, f0) Dcta i ls of Expendi ture on var ious pol lu t ion Contro l Measure_s.

Pl refer Envi ronmentat c toarance No. J-11011/325/2006_14 I I ( I ) d td. 25th )u ly 2OO7 for var ious products .GPCB has issued Consent to Establish (NOC) form. NOC copy is attached in Annexure _1 for your ready,' reference. out of the various.products mentioned in EC, wi -r" ;nu"riiitrri"g rvun."r"i ino

W e t r u s t t h a t t h e s c d c t - a i l s a r c i n l i n e w i t h y o u r r e q u i r e m e n t s . K i n d l y a c k n o w l e d g e r c c c i p t o f t h e s a m e .

Thank ing You,Yours fa i th fu l l y ,fo r un i ted Phosphorus L td ,

U n i t H e a d ,

E n c l . : a . a .

Mumbal office : ruNrPHos" Houso, c.E.Marg, 11Jh Road, Khar (w), Mumbai.Phone : (OZ2l 26469000-111 r Fax : {0lZ2\ ZOoOOzOO.

S. M Chakra=5ortY

Page 2: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

Ref.: UPL/Jhg/ENV/27/2013/01 February 21, 2013 To, Dr. A. Mehrotra,

Director (S), Ministry of Environment & Forest, Regional Office – Western Region, Kendriya Paryavaran Bhavan, Link Road No. 3, Ravi Shankar Nagar BHOPAL – 462 016 (M.P.)

Sub. : Half Yearly Report. Ref.: 1. Environmental Clearance No. J.13011/26/96-1A.II, dtd. 24th. Dec., 1996 of 50 MW

Combined Cycle Co. Generation Power Plant. 2. Environmental Clearance No. J-11011/42/95-A.II (1), dtd. 17th. May, 1996 of 100 TPD Chlor-Alkali Plant. 3. Environmental Clearance No. J-11011/325/2006-IA II (I) dtd. 25th July 2007 for various products.

Dear Sir, We hereby submit half-yearly Report, consisting of the following details for the period starting from July - 2012 to December - 2012 for your evaluation & records.

1) Status of Compliance of Conditions mentioned in above three Environmental Clearances.

2) Ambient Air Monitoring Report. 3) Stack Monitoring Report. 4) Noise Level Monitoring Report. 5) Waste Water Analysis Report. 6) Ground Water Quality Report. 7) Soil Analysis report. 8) Solid Waste Analysis report.

9) Details of Green Belt Development. 10) Details of Expenditure on various Pollution Control Measures.

Pl refer Environmental Clearance No. J-11011/325/2006-IA II (I) dtd. 25th July 2007 for various products . GPCB has issued Consent to Establish (NOC) form. NOC copy is attached in Annexure -1 for your ready reference. Out of the various products mentioned in EC, we are manufacturing Mancozeb and Pendimethylene, which have been included in our Consent. We are implementing CS2 Project.

We trust that these details are in line with your requirements. Kindly acknowledge receipt of the same. Thanking You, Yours faithfully, for United Phosphorus Ltd,

S. N. Chakraborty, Unit Head, Encl.: a. a.

Cc: (1) The Zonal Officer CPCB, Baroda (2) The Regional Officer GPCB XGN ID # 25353 GPCB – Ankleshwar

Page 3: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

DETAILS OF GREEN BELT DEVELOPMENT

For the period July – 12 to December - 12

1. No. of trees planted before July -12 inside the company premises = 39295

in 20.75 acre.

2. During the above mentioned period:

-No. of trees planted inside company premises = 247 in 1 acre area. -Total Trees survived inside company: 232 out of 247 for above period.

3. Total trees available inside company: 39527

4. Total area covered : 21.75 acre

5. Total trees per Ha: 4543

Page 4: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

EXPENDITURE ON POLUTION CONTROL MEASURES FOR THE PERIOD JULY – 12 TO DECEMBER – 12

A) Operating cost for Air Pollution Control Equipment's

Sr. No. Plant Pollution Control Equipment Expense

1 PCL3 Scrubbers 539568

2 POCL3 Scrubbers 70564

3 Caustic – Chlorine Hypo Scrubber 9825095

4 Caustic – Chlorine Caustic Scrubber 345846

5 White Phosphorus Venture Scrubber 0

6 PCl5 Scrubbers 2030827

7 Mancozeb Scrubbers 4892650

Total cost for operating Air Pollution Control equipment is Rs. 1,77,04,550

B) Operating cost for Water Pollution Control Equipment's

Sr. No. Plant Pollution Control Equipment Expense

1 Caustic – Chlorine ETP 732386

2 PCL3 & POCl3 Plant Scrubber Effluent 697565

3 Power Plant ETP 294353

4 White Phosphorus ETP 0

5 Central ETP ETP 130980

6 RO RO 1057160

7 1 MLD ETP (C-Tech) ETP 8824842

8 MEE MEE 3,35,40,228

Total cost for operating Water Pollution Control equipment is Rs. 4,52,77,514

C) Operational cost for solid waste disposal

Rs. 42,57,624 (This includes transferring cost from plant to our internal solid waste storage and

from our site to TSDF, BEIL, Ankleshwar)

Page 5: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

Summary of Stack Monitoring Parameters:

Stacks Pollutants Limit Average Maximum Minimum

Power Plant HRSG Stack NOX 50 ppm 26.8 32.8 21.6

Caustic Scrubber WAD 100-TPD Plant Cl2 9 mg/Nm3

1.7 2.7 0.7

HCl 20 mg/Nm3 5.5 8.6 3.4

Caustic Scrubber of HCl Furness 100-TPD Plant HCl 20 mg/Nm3 14.8 17.8 11.6

Caustic Scrubber of Phosphorus Oxy-Chloride Plant Distillation Column

HCl 20 mg/Nm3

7.5 9.4 4.5

Caustic Scrubber of Distillation Section of PCl3 Plant

HCl 20 mg/Nm3 8.5 10.8 6.2

PCl3 9 mg/Nm3 0.9 1.6 0.5

Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant

HCl 20 mg/Nm3 6.5 9.8 4.0

PCl3 9 mg/Nm3 0.5 0.9 0.2

Water Scrubber + Alkali Scrubber of Reactor PCl5 Plant

Cl2 9 mg/Nm3 0.8 1.2 0.5

HCl 20 mg/Nm3 12.2 15.1 8.7

Alkali Scrubber of Mancozeb Plant Reactor D-14 New EDA Scrubber

H2S 45 mg/Nm3 12.1 22.4 2.9

CS2 180 mg/Nm3 102.5 125.0 83.1

Water Scrubber of Wet Spray Dryer of Mancozeb Plant

PM 20 mg/Nm3

16.5 19.2 13.4

Bag Filter of RVDF of Mancozeb Plant PM 20 mg/Nm3 13.0 15.4 9.9

TPPI - Thermic Fluid Heater

PM 150 mg/Nm3 59.8 72.5 45.6

SO2 100 ppm 13.1 16.1 9.7

NOX 50 ppm 19.0 24.3 15.2

TPPI -Water Scrubber + Ventury Scrubber of Tri-Phenyl Phosphite Plant Rector(C-2102)

HCl 20 mg/Nm3

12.2 14.3 9.2

TPPI -Water Scrubber + Ventury Scrubber of Tri-Phenyl Phosphite Plant Rector(C-2002A)

HCl 20 mg/Nm3

9.5 12.5 6.7

TPPI -Water Scrubber + Ventury Scrubber of Tri-Phenyl Phosphite Plant Rector(C-2020)

HCl 20 mg/Nm3

9.8 9.8 9.8

Page 6: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

Summary of Ambient Monitoring Parameters:

Pollutants Limit Average Maximum Minimum

PM10 100 µg/m3 77.3 83.5 68.3

PM2.5 60 µg/m3 39.9 45.2 34.2

SOX 80 µg/m3 20.3 24.9 11.9

NOX 80 µg/m3 28.9 36.1 21.6

HCl 200 µg/m3 5.1 8.5 2.5

Cl2 100 µg/m3 BDL BDL BDL

NH3 400 µg/m3 BDL BDL BDL

HF 160 µg/m3 BDL BDL BDL

H2S 500 µg/m3 BDL BDL BDL

CS2 2000 µg/m3 84.7 120.2 62.7

HC 160 µg/m3 BDL BDL BDL

P2O5 70 µg/m3 BDL BDL BDL

Summary of Effluent Parameters:

Parameters Limits 3rd Party Results NCTL Results

Average Maximum Minimum Average Maximum Minimum

pH 6.5-8.5 -- -- 7.47 6.89 -- 8.04 7.17

COD (mg/L) 100 mg/L 107 136 93 143 272 63

SS (mg/L) 100 mg/L 76 92 54 45 102 20

Ammonical Nitrogen (mg/L)

50 mg/L 12 14 BDL 14 29 BDL

Page 7: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +
Page 8: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

UNITED PHOSPHORUS LTD., UNIT NO. 5

JHAGADIA

STATUS CUM COMPLIANCE REPORT FOR 100 TPD CCP ENV. CLEARANCE

Sr.

No.

Condition Status

1 To adhere GPCB and state Govt. stipulation Complied as per CCA No.

10067 Dated 25th February

2008 valid up to 18.12.2012,

Applied for CC&A renewal 0n

02.11.2012.

2 To intimate MoEF about any project coming up in the

premises

Complied. As and when new

projects are coming up, we will

intimate MOEF

3 Gaseous (CL2, SO2, Nox, HC ) and particulate emission

from the various process vents and storage tanks should

conform to the standards.

Complied.

We have internal and external

Monitoring & all Parameters

are within limits.

4 Three AAQ to install

Stack emission to monitor regularly

To submit AAQ + Stack report to MoEF once in six

month with statistical analysis and interpretation

3 AAQ installed for

monitoring of SPM, PM10,

PM2.5, SO2,NOX & CL2.

CL2,HCL Monitored in

Hypo & Hcl stacks

Results are being

submitted in half yearly

reports. It is well within

stipulated norms.

5 Fugitive emission monitoring and data recorded

Chlorine sensor is to be installed in the chlorine storage

area at lower level between the tanks

Complied.

16 Cl2 sensors at strategic

locations & monitored on DCS.

6 Liquid effluents coming out of the plants should be

confirmed to the standard prescribed by the GPCB

Recycling and reuse of the treated waste water

should be maximized

Complied

Steam condensate of

Caustic Evaporation reused

in Brine make up & Cooling

tower make up

Page 9: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

7 Adequate measures for the control noise levels

below 85dB.

Employees to be provided with PPE.

Engineering Control measures to reduce noise

Monitoring done monthly.

Range is from 70 to 75dB

Ear muffs & ear plugs are

provided to the person

working in high noise area

like H2 compressor, & air

compressor

Acoustic enclosures

provided

8 Occupational health surveillance program with respect to

exposure to chlorine, thermal stresses and noise

pollution.

Complied.

We are doing half yearly

medical check up. We are

also doing full body

medical check up by

external expert agency

once in two years. All

records are maintained

9 Green belt of adequate width & density covering 25

acres of land should be developed

Treated effluent to be used for green belt development

Complied

Presently we have about

39106 trees

Sewage water is used for

gardening

Page 10: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

10 Educate the neighboring people for accidental release

of chlorine

To install wind sock

Necessary approval from CCE & Chief Inspector of

Factories

Complied.

Disclosure of Information

on CL2 to general public is

given in book let thrice and

also conducted awareness

program in the year 1999 &

2005

We have installed 14 wind

socks inside the factory

Obtained CCE approval for

CL2 Storage, filling in

toners, hydro testing. Also

for H2 filling & storage.

Maps of plant approved &

inspected by Chief Inspector

of Factories (Director –

Industrial Safety & Health,

Gujarat State)

11 Hazardous waste handling as per rules 1989 Complied

Yearly return submission is

done for solid waste

generation & disposal to

GPCB

12 To follow hazardous chemicals Mfg./Storage/Handling /

import Rules1989-1994

Complied.

MSIHC guidelines followed for

e.g On site emergency

plan, MSDS etc.

13 To set up laboratory for collection & analysis of sample Complied

Laboratory is in operation &

regular analysis is being

done for waste water,

stacks & ambient air,

ground water etc.

Page 11: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

14 Set up Environment management cell Internal Environment

management cell

comprising of Unit Head,

plant head, SHE Head &

Corporate Environment

head is in operation for

close monitoring. The

environment cell verifies

environmental performance

and involves in

environmental audit

15 Funds earmarked during project for Env. protection

Year wise expenditure to be submitted to MoEF

Complied.

Project has been

commissioned since 1997

with compliance of all

environment related

protection

Statement of expenditure

submitted half yearly.

16 Six monthly - Half yearly report submission to MoEF Being submitted regularly

Date: 20th February 2013

Page 12: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

UNITED PHOSPHORUS LTD., UNIT NO. 5

JHAGADIA

STATUS CUM COMPLIANCE REPORT FOR 50 MW PP ENV. CLEARANCE

Sr.

No.

Condition Status

1 All the conditions stipulated in the GPCB NOC No.

PC/NOC/-BRCH-1611/9518 should be

implemented

Complied for effluent quantity &

quality norms

2 An area of 103 acres only to be acquired for power

plant including green belt development

Complied. Power plant is included in

the area of 103 acres

3 Three stack of height 30m, 35m, 7m for Gas Turbine,

HRSG, DG sets should be installed

Complied

Installed & commissioned

4 Ambient air quality should be regularly monitored

and results should be submitted to the MoEF

every six months

Complied.

We have internal and external

monitoring and all results are well

within the limit. As per new

standard started monitoring

parameters PM10 and PM 2.5

We are submitting results half yearly

to MOEF.

5 Sulfur content in Naphtha should not exceed 0.15% Condition is not applicable now as

we have switched over from

Naphtha to Natural Gas from

June 2002 and consent has been

obtained

6 Nox control system should be installed to ensure that

Nox emission should not exceed 50 ppm

Complied

Nox is well within norms.

7 To use effluent for green belt development Complied

It is being used

8 Water used for plant should be restricted to 6480

KL/Day

Complied.

It ranges from 1200 to 1500 KL/Day

9 Adequate measured for Noise control below - 85

dB

To give PPE to employees

Complied.

Enclosures provided to control

noise

People use ear muffs & ear plugs

10 Green belt development @ 1500-2000 trees /

hectares

Complied.

Presently we have about 39106 trees

Page 13: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

11 Land fill site provided No solid waste generation from

power plant

12 To build thermal proof wall between Naphtha tanks

and switch yard

Complied

Not applicable as we have switched

over from Naphtha to Natural

Gas.

13 Sludge from common sludge tank to be incinerated

and disposed in the land fill site

No such sludge is generated which

requires incinerator

14 Full cooperation should be extended to the statutory

authority during their visit

Noted the point

15 Funds earmarked for Env. protection during project Pr Project has been commissioned since

1997 with compliance of all

environment related protection

16 Environment monitoring committee should be

constituted

As our plant is commissioned since

long Internal Environment

management cell comprising of

Unit Head, plant head, SHE Head

& Corporate Environment head

is in operation for close

monitoring.

After implementation of the project,

we have constituted a

monitoring committee and the

last meeting was conducted in

September - 2002

We have carried out a meeting

involving various stakeholders

including the monitoring

members in September 2005 in

connection with information on

the change over of fuel from

naphtha to natural gas as we are

working on CDM project.

17 Any deviation or alternation in project need fresh

reference to the ministry

There was no deviation during

project. However subsequently

raw material change from

Naphtha to Natural Gas in 2002

Page 14: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

Date: 20th February 2013

Page 15: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

UNITED PHOSPHORUS LTD., UNIT NO. 5, JHAGADIA

STATUS CUM COMPLIANCE REPORT FOR ENV. CLEARANCE NO. J –

11011/325/2006 – IA II (I)

Sr. No. Condition Status

1 The ministry of Environment & forest has examined the

proposal. It is noted that the proposal is for expansion of

Unit – V at Jhagadia Gujarat. The expansion project

comprise of addition of new units for producing Pesticide

Intermediate & Technical Products and expansion of

existing Chlor-alkali & Captive Power Plants. Company

proposes to produce the following Pesticides Intermediate

Products, Technical Grade Pesticide Products along with

their By – Products

Noted and complied.

Company has obtained consent to

establishment (NOC) for other

products and copy is attached.

Company has started manufacturing

of Mancozeb and Pendimethyline .

CS2 Plant is under construction

Sr.

No.

Products By Products

Quantity in MT/Month Quantity in MT/Month

Items Existing

Capacity

Additional

Capacity

Overall

capacity

after

expansio

n

Items Existing

capacity

Additional

capacity

Overall

capacity after

expansion

1 Triphenyl

Phosphite

300 - 300 HCl

(30%)

353 - 353

2 Phosphor

us

Trichloride

2250 - 2250 - - - -

3 2,4Di

Chlorophe

nol

166 - 166 Mix

Chloro

phenol

15 - 15

HCl

(30%)

250 - 250

4 Phosphor

us

Oxychlori

de

150 - 150 - - - -

5 Phosphor

us

900 - 900 Ferrou

s

150 - 150

Page 16: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

Phosp

horus

Calciu

m

Silicate

6000 - 6000

6 Phosphor

us Acid

150 - 150 HCl(30

%)

600 - 600

7 Trinonyl

Phenyl

Phosphite

100 - 100

8 Phenyl Di

Iso Decyl

Phosphite

100 - 100

9 Amino Tri

Methylene

Phosphori

c Acid

200 - 200

10 Ethylene

Diamine

Tetra

Phosphori

c Acid

100 - 100

11 Phosphor

us Penta

Chloride

150 150

DVACl

Plant

12 DVACl - 300 300 Spent

Sulphu

ric

Acid

- 900 900

POCl3 - 400 400

HCL

(28%)

- 490 490

Sodiu

m

Sulphit

e

(20%)

- 1200 1200

Page 17: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

Pesticides

Intermedi

ate

Products

– Multi

Product

Plant

13 N –

Alkylated

Xyledene

- 300 300 Pera

Toluen

e

Sulpho

nic

Acid

(PTSA)

- 94 94

OR

HRT

Ketone

- 200 200

OR

2 – Ethyl

6 –

Methyl –

n – n

Aniline

- 300 300

OR

MPBAL - 300 300

Caustic

Chlorine

Plant

14 Caustic

Soda Lye

48% (On

100 %

Basis)

4680 10500 15180 Sodiu

m

Hypoc

hlorite

225 525 750

15 Chlorine 3972 8537 12509 - - - -

16 Hydrogen 225 263 488 - - - -

17 Hydrochlo

ric Acid

(30%)

1200 2625 3825 - - - -

Power

Page 18: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

Plant

18 Electrical

Power

50

MW/Hrs

37.6

MW/Hrs.

87.6

MW/Hrs.

Steam 30 MT /

Hrs.

- 30 MT/Hrs

Pesticides

Technical

Products

19 Glyphosat

e

- 1000 1000

20 Pendimet

hylene

- 200 200

21 Tebucona

zole

- 200 200

22 Metalochl

or

- 200 200

23 Aceflorfen - 500 500 Acetic

Acid

(80%)

- 1185 1185

24 Mancozeb - 4000 4000 Sodiu

m

Sulpha

te 96%

/

Sodiu

m

Sulpha

te

Solutio

n

- 4092/

15680

4092/ 15680

25 Acephate - 800 800 Ammo

nium

Acetat

e

- 464 464

26 Cypermet

hrin

- 500 500

27 Permethri

n

- 300 300 HCl

(30%)

- 94.8 94.8

Pesticides

Formulati

on

Page 19: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

28 Isopropyl

Amine

Salt of

Glyphosat

e (liq) –

Formulati

on

(Kl/Month

)

- 2600 2600

29 Ammoniu

m Salt of

Glyphosat

e (liq) –

Formulati

on

(Kl/Month

)

- 2600 2600

30 Sodium

Salt of

Aceflorofe

n –

Formulati

on

- 1500 1500

CS2

(Carbon

Disulfide)

Plant

31 Carbon

Disulfide

- 3000 3000

MnSO4

(Mangane

se Sulfate)

Plant

32 MnSO4

(31%)

- 10000 10000

Page 20: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

2 The unit already has 50 MW CPP and additional 37.5 MW CPP is proposal

to be added. Cooling Towers/ N2 Plant, Compressor, chilling unit,

Biological ET, DM plant, Fire Fighting System etc. shall be added. Total

cost of the expansion is Rs. 473.74 Crores and recurring cost will be Rs.

07.00 Crores. The company has total 8,85,601 sq m (218 acres) of land and

the proposed expansion project will be in the existing premises. Out of

this, about 91,655 sq m is covered as green belt and greenery and an

additional agricultural or forest land is involved in the project site and no

eco-sensitive zone is involved in 7 km area of the project site. However,

about 21 Reserve Forests exist with 10 to 24 km from the site.

Noted.

Company has

obtained consent to

establishment (NOC)

and copy is attached

3 The project activities are listed at 4(c) and 5(b) in the schedule of the EIA

Notification, 2006 and are of „A‟ category. The project is submitted under

the EIA Notification, 2006 for evaluation of the completeness of Draft

EIA/EMP and for additional TORs, if any, as per Para 2.2.1(b) of the

Ministry. The Interim Operational Guidelines dated 13th October 2006

issued by the Ministry, The additional information as desired by the

committee were submitted by the proponent, since the proposed project

is industrial area, it would not need Public Consultation as per Para 7(i) III,

Stage (3) (b) – public construction of EIA Notification 2006.

-

4 Based on the information provided, the Ministry of Environment and

Forests hereby accords environmental clearance to above project under

the provisions of EIA Notification dated 14th September 2006 subject to

the compliance of the following specific and General conditions:

-

5 SPECIFIC CONDITIONS:

I The gaseous emissions (SO2, NOx, HCl, Cl2, CH4, P2O5, DMS, H2S, HC,

PCl3, NH4, CS2 AND CO, HC and RSPM from various process units shall

conform to the standards prescribed by the concerned authorities from

time to time. At no time, the emission levels shall go beyond the stipulated

standards. In the event of failure of pollution control system(s) adopted by

the unit, the respective unit shall not be restarted until the control

measures are rectified to achieve the desired efficiency.

Noted and complied.

We have regular

monitoring internally

and externally .All

parameters are well

within the limit

II New standards for pesticides unit, as proposed by the CPCB under the E(P)

A, 1986 shall be followed by the Unit.

Noted and complied.

III Three new boilers shall be based on Imported Coal/Lignite/ RDF (pellets or

fluff). Fuel for other boilers and D.G. Sets will be Natural Gas, HSD and FO.

Noted

Page 21: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

IV Natural Gas, H2 and Cl2 shall be transported through pipelines. Present

transportation mode of hazardous Chemicals by road shall be switched

over to railway line as soon as it is laid down. All Transportation of

Hazardous Chemicals shall be as per the MVA, 1989

Noted

V 23 additional Stacks shall be provided for dispersion of gaseous emissions.

The height of these shall be as per the Prescribed Stack Height rules and

CPCB guidelines. For process emissions like HCl, Cl2, SO2, PCl3, CS2 etc.

Scrubbers shall be provided with each reactor for quenching. Waste air de-

chlorination system shall be provided in the Caustic chlorine Plant, Vent

gases from 2, 4-Dichloro Phenol shall be subjected to two-stage absorption

consisting of DM water and caustic jet. For Chlorine, 2 stages Scrubber with

recovery of Sodium Hypo shall be provided.

Noted and complied.

Scrubbers provided for

Mancozeb plant to

control process

emissions.

VI Water/ Alkali Two stage Scrubber systems, Mist Eliminator with Koch filter

and Vet Scrubber with Mist Eliminator shall be installed for the boilers.

Thermic Fluid heater, D.G.Sets, The scrubbed water shall be sent to ETP for

further treatment.

Complied

VII Flare system shall be provided for burning of contaminated H2 and Fume

incinerator shall be provided for decomposition of contaminated air/gas

from the plant.

Noted, will be

incorporated in the

proposed project

VIII For CPP, ESP will be provided which will meet SPM limits with in 50

mg/nm3.

Noted, will be

incorporated in

the proposed

project

IX All liquid raw material shall be stored in storage Tanks and Drums Complied

X Regular monitoring for SO2, NOx, HCl, Cl2,, CH4, P2O5, DMS, H2S, HC,

PCl3, NH3, CS2 and VOC along with SPM and RSPM in the ambient air at

carious probable locations in the plant shall be carried out.

Complied. Company

have regular

monitoring internally

and externally . All

parameters are well

within limits.

XI The location if ambient air quality monitoring station shall be reviewed in

consultation with the State Pollution Control Board (SPCB) and additional

stations shall be installed, if required in the downwind direction as well as

where maximum ground level concentration are anticipated.

Noted and complied.

XII Use if toxic solvent like Methylene Chloride (MC) etc. shall be minimized to

the extent possible. Benzene shall not be used as solvent and no odorous

compounds/ gas like Mercaptans or Hydrogen Sulfide shall be used or

formed in any of reactions at the site.

Noted

XIII Bioassay test and toxicity index shall be carried out regularly. Complied

Page 22: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

XIV All the storage tanks shall be under negative pressure to avoid any

leakages. Breathers, N2 blanketing and condensers will be provided for all

the storage tanks. Closed handling systems for chemicals and solvents will

be provided. Magnetic seals will be provided for pumps/agitators for

reactors for reduction of fugitive emission, Chilled Brine based condensers

shall be used to prevent VOC emission. Solvent traps shall be installed

wherever necessary.

Complied

XV All venting equipment shall have vapour recovery system. All the pumps

and other equipment‟s where there is a likelihood of HC leakages shall be

provided with Leak Detection and Repair (LDAR) system and LEL indicators

and Hydrocarbon detectors. Provision for immediate isolation of such

equipment, in case of a leakage will also be made. The company shall

provide a well defined Leak Detection and Repair (LDAR) programme for

quantification and control of fugitive emissions. The detectors sensitivity

will be in ppm levels.

Complied

XVI Spent solvents shall be recovered as possible & solvent recovery shall be

further increased from the present 95% to at least 98% percent. Solvent

vapours emitted during purification process from purification tanks as

fugitive emissions shall be reduced as far as possible.

Noted and complied.

XVII Portable monitoring instruments for all relevant gases like Chlorine and

Ammonia shall be provided.

Complied. Chlorine

sensors are provided.

XVIII Fugitive emissions in the work zone environment, product, raw materials

storage area shall be regularly monitored for all relevant parameters. The

emissions shall conform to the limits imposed by the State Pollution

Boards/Central Pollution Control Board.

Complied.

Online sensors are

provided for

monitoring Fugitive

emissions like

Chlorine, H2S etc.

XIX No ground water shall be used for the project. Water requirement will not

exceed 10,000 m3/day, which will be met through GIDC Water supply.

Complied. Our water

consumption is well

within the limit.

Page 23: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

XX Daily waste water generation will not exceed to 4,575 m3/day. The whole

waste water shall be treated in the proposed two ETPs. One Effluent

Treatment Plant shall consist of primary, secondary and tertiary treatment

units for the proposed Pesticide, CS2 and MnSO4 Plants. The inorganic

stream shall be sent to CETP after the primary treatment. The

Biodegradable stream shall be treated up to tertiary treatment. High TDS

and low COD stream shall taken to MEE System and High Organic (high

COD) stream will be incinerated. The final treated effluent will be collected

in collection sump and discharged through GIDC drainage line. The effluent

generated from the proposed 350 TPD Caustic Chlorine and enhanced CPP

which will be modified. The effluent generated from the proposed

pesticides in the proposed ETP. The treated effluent shall be sent to CETP

of BEAIL for final discharge into the deep sea through closed pipeline. No

free solvent shall go to the ETP.

Complied.

Effluent treatment

plant consisting

primary, Secondary

and tertiary treatment.

Augmented the

treatment system with

Hypo treatment to

Ammonical Nitrogen

within limit

XXI Hazardous / Solid Waste generated shall be as per the list and quantities

submitted to this Ministry as per the letter no. UJH/PRO/17/2007 dated 14th

May 2007. On-site Incinerator shall be installed to incinerate incinerable

waste. Otherwise the waste shall de sent to the Common Incinerator of

BEIL. Land fillable waste shall be sent to BEIL-TSDF.

Complied.

We have taken

membership of BEIL

and sending material

to BEIL regularly.

XXII Emissions from the incinerator shall be the prescribed norms for the

incinerators. Monitoring Protocol as prescribed in these standard shall be

followed.

Noted

XXIII Fly ash generated from the CPP will be utilized for Brick manufacturing and

for Cement manufacturing as per the Fly Ash Utilisation Notification.

Noted

XXIV All safety measures suggested in the letter no. UJH/PRO/17/2007 dated 14th

May 2007 for the solvent and reactants storage shall be implemented

Noted & complied

XV The company shall undertake following Waste Minimization measures.

A Metering and control of quantities of active ingredients to minimize waste. Noted and complied

B Reuse of by-products from the process as raw materials or as raw material

substitutes in other processes.

Complied

C Use of automated filling to minimize spillage. Complied

D Use of “Close Feed” system into batch reactors. Complied

E Venting equipment through vapour recovery system. Complied

F Use of high pressure hoses for equipment clearing to reduce wastewater

generation.

Noted

Page 24: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

G The project authorities shall strictly comply with the provisions made in

Manufacture, Storage and Import of Hazardous Chemicals Rules, 1989 as

amended in 2000 for handling of hazardous chemicals. Necessary approvals

from Chief Controller of Explosives must be obtained before commissioning

of the expansion project. Requisite On-Site and Off-Site Disaster

Management Plans will be prepared and implemented. Regular mock drills

shall be carried out for both On-Site and Off-Sit plans.

Noted

H The company shall develop rain water harvesting structures to harvest the

run off water for recharge of ground water.

Noted

I Minimum 25% of the total area shall be developed as green belt as per the

CPCB guidelines. Additional 1,12,091 sq.m shall be developed as green belt.

Noted

J Occupational health surveillance of the workers shall be done on a regular

basis and records maintained as per the Factories Act.

Complied

K Training shall be impaired to all employees on safety and health aspects of

chemicals handling. As informed to the Ministry. OHSAS 18001 shall be

continued. Pre employment and routine periodical medical examinations for

all employees shall be undertaken on regular basis. Training to all

employees on handling of chemicals shall be imported.

Complied

L Usage of PPEs by all employees/ workers shall be ensured. Complied

M The company shall strictly follow all the recommendations mentioned in the

Charter on Corporate Responsibility for Environmental Protection (CREP).

Complied

N The company shall harvest surface as well as rainwater from the rooftops of

the buildings proposed in the expansion project and storm water drains to

recharge the ground water and use the same water for various activities of

the project to conserve fresh water.

Noted

O All the recommendations made by the consultants in respect of

environmental management and risk mitigation measures relating to the

project shall be implemented.

Complied

P The company shall undertake all relevant measures as indicated during the

Public Hearing for improving the Socio-economic conditions of the

surrounding area. CSR activities will be undertaken by involving local

villages and administration.

Complied

Q The company shall undertake eco-developmental measures including

community welfare measures in the project area for the overall

improvement of the environment. The eco-development plan should be

submitted to the SPCB within three months of receipt of this letter for

approval.

Noted

GENERAL CONDITIONS

Page 25: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

I The project authorities shall strictly adhere to the stipulations made by the

State Pollution Control Board.

Complied

II No further expansion or modifications in the plant shall be carried out

without prior approval of the Ministry of Environment and Forests. In case

of deviations or alterations in the project proposal from those submitted to

this Ministry for clearance, a fresh reference shall be made to the Ministry

to assess the adequacy of conditions imposed and to odd additional

environmental protection measures required, if any.

Noted and complied.

III At no time, the emissions shall exceed the prescribed limits. In the event of

failure of any pollution control system adopted by the unit, the unit shall

be immediately put out of operation and shall not be restarted until the

desired efficiency has been achieved.

Noted and Complied.

IV The project authorities shall strictly comply with the rules and regulations

under Manufacture, Storage and Import of Hazardous Chemicals Rules,

1989 as amended in October, 1994 and January, 2000. Authorization from

the SPCB shall be obtained for collection, treatment, storage, and disposal

of hazardous wastes.

Complied

V The over all noise levels in and around the plant area shall be kept well

within the standards by providing noise control measures including acoustic

hoods, silencers, enclosures etc. on all sources of noise generation. The

ambient noise levels shall conform to the standards prescribed under

Environment (protection) Act,1986 Rules, 1989 viz. 75 dBA (day time) and

70 dBA (night time).

Complied

VI The project proponent shall also comply with all the environmental

protection measures and safeguards recommended in the EIA/EMP report.

Complied

VII A separate Environmental Management Cell equipped with full fledged

laboratory facilities shall be set up to carry out the Environmental

Management and Monitoring functions.

Complied

VIII The project authorities shall earmark separate funds of Rs. 43.09 Crores to

implement the conditions stipulated by the Ministry of Environment and

Forests as well as the State Government along with the implementation

schedule for all the conditions stipulated herein. Rs. 07.00 crores will be the

annual recurring expenditure for environmental protection measures. The

funds so provided shall not be diverted for any other purpose.

Noted and being

complied

IX The implementation of the project vis-à-vis environmental action plans shall

be monitored by the concerned Regional Office of the Ministry / SPCB /

CPCB. A six monthly compliance status report shall be submitted to

monitoring agencies.

Complied

Page 26: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

X The project proponent shall inform the public that the project has been

accorded environmental clearance by the Ministry and copies of the

clearance letter are available with the SPCB/Committee and may also be

advertised within seven days from the date of issue of the clearance letter

at least in two local newspapers that are widely circulated in the region of

which one shall be in the vernacular language of the locality concerned and

a copy of the same shall be forwarded to the concerned Regional Office of

the Ministry.

Complied

XI The project authorities shall inform the Regional Office as well as the

Ministry, the date of financial closure and final approval of the project by

the concerned authorities and the date of start of the project.

Complied

XII The Ministry may revoke the right to stipulated additional conditions, if

found necessary. The company in a time bound manner will implement

these conditions.

Noted

XIII The above conditions will be enforced, inter-alia under the provisions of

the Water (Prevention & Control of Pollution) Act, 1981, the Environment

(Protection) Act, 1986 Hazardous Waste (Management and Handling)

Rules, 2003 and the Public Liability Insurance Act, 1991 along with their

amendments rules.

Noted

Date: 20th February 2013

Page 27: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT

Test Report No.: EP/UPL-5/2012/1 Issue Date: 17 / 07 / 12

Customer’s Name & Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch. Description of Sample

: ETP Outlet (Treated Effluent)

Quantity/No. of Sample : 5 L / 1 No

Sampling By : ENPRO Team Packing/Seal : Sealed Date of Sampling : 10 / 07 / 12 Sample Received Date

: 11 / 07 / 12 Protocol (purpose) : Waste Water Analysis (Monthly Monitoring)

Date of Starting of Test

: 11 / 07 / 12 Date of Completion : 17 / 07 / 12

Sampling Method : IS 3025 Part-1 Sample ID : EP / WW / 0712 / 1 Test Method : IS 3025 & APHA Type of Sampling : Grab

RESULT TABLE

SR. NO. TEST PARAMETER UNIT RESULTS GPCB LIMIT

1. pH (at 270 C) - 7.47 5.5-8.5 2. Temperature 0C 30 40 3. Colour Pt. Co. 28 100 4. Total Residual Chlorine mg/L BDL 1.0 5. Total Suspended Solids mg/L 66 100

6. Total Dissolved Solids (at 1800 C) mg/L 11072 2100

7. Oil & Grease mg/L 2.8 10

8. Phenolic Compound ( as C6H5OH ) mg/L BDL 1.0

9. Ammonical Nitrogen mg/L 10.0 50 10. Boron as B mg/L BDL 2.0 11. COD mg/L 136 100 12. BOD ( 3 days at 270C ) mg/L 38.2 30 13. Chloride (as Cl) mg/L 5726 600 14. Sulphate (as So4

-2) mg/L 3939 1000 15. Fluoride ( as F) mg/L 0.2 1.5

16. Sulphide mg/L BDL 0.5

17. Cyanides ( as CN ) mg/L BDL 0.2 18. Selenium ( as Se ) mg/L BDL 0.05 19. Zinc mg/L BDL 5.0 20. Lead ( as Pb ) mg/L BDL 0.1

…contd

Page 28: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

SR. NO. TEST PARAMETER UNIT RESULTS GPCB LIMIT

21. Nickel mg/L 0.24 3.0

22. Copper mg/L BDL 2.0

23. Total Chromium mg/L 0.11 2.0

24. Hexavalent Chromium mg/L BDL 0.1

25. Mercury (as Hg ) mg/L BDL 0.01

26. Arsenic ( as As) mg/L BDL 0.2

27. Cadmium ( as Cd ) mg/L BDL 2.0

28. Total Heavy Metal mg/L <1 7.0

29. Percentage Sodium (% Na) % 58.9 60

30. Bioassay Test % 80% 90% Survival of Fish after 96 Hrs. in 100%

Effluent Note: BDL: - Below Detectable Limit

ANALYSED BY CHECKED BY

Page 29: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 17 / 07 / 12

REF. NO. EP/UPL-5/2012/2

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 09 / 07 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/2

Description of Source

: Stack attached to Gas Turbine ( Power Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Natural Gas

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 119 - 3 Avg. Velocity m/s 12.1 - 4 Avg.flow rate m3/hr. 217948 - 5 Stack Dia. m 3.0 - 6 Particulate Matter (PM) mg/NM3 BDL 150 7 Sulphur Oxides (SOx) ppm BDL 100 8 Nitrogen Oxides (NOx) ppm 21.6 50

Page 30: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 17 / 07 / 12

REF. NO. EP/UPL-5/2012/3

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 09 / 07 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/3

Description of Source

: Stack attached to Thermic Fluid Heater (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : HSD

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 33.0 - 2 Flue Gas Temp. 0 C 199 - 3 Avg. Velocity m/s 11.0 - 4 Avg.flow rate m3/hr. 7101 - 5 Stack Dia. m 0.6 - 6 Particulate Matter (PM) mg/NM3

58.1 150 7 Sulphur Oxides (SOx) ppm 9.7 100 8 Nitrogen Oxides (NOx) ppm 16.6 50

Page 31: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 17 / 07 / 12

REF. NO. EP/UPL-5/2012/4

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 09 / 07 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/4

Description of Source

: Stack attached to Water Scrubber of Wet Spray Dryer (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 69 - 3 Avg. Velocity m/s 12.8 - 4 Avg.flow rate m3/hr. 117199 - 5 Stack Dia. m 1.8 - 6 Particulate Matter (PM) mg/NM3

19.2 20

Page 32: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 17 / 07 / 12

REF. NO. EP/UPL-5/2012/5

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 09 / 07 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/5

Description of Source

: Stack attached to Bag Filter of RVDF (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 56 - 3 Avg. Velocity m/s 8.5 - 4 Avg.flow rate m3/hr. 961 - 5 Stack Dia. m 0.2 - 6 Particulate Matter (PM) mg/NM3

15.4 20

Page 33: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 17 / 07 / 12

REF. NO. EP/UPL-5/2012/6

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 09 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/6

Description of Source

: Stack attached to Alkali Scrubber of-D-14 New EDA Reactor (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (34) - 3 Stack Dia. m 0.1 - 4 Hydrogen Sulphide (H2S) mg/NM3

22.4 45 5 Carbon Di-Sulphide (CS2) mg/NM3

125 180

Page 34: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 17 / 07 / 12

REF. NO. EP/UPL-5/2012/7

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 09 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/7

Description of Source

: Stack attached to Caustic Scrubber of Distillation Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (34) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

6.2 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 1.0 9

Page 35: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 17 / 07 / 12

REF. NO. EP/UPL-5/2012/8

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 09 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/8

Description of Source

: Stack attached to Caustic Scrubber of Storage Tank & Drum Filling Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Storage Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (34) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

4.4 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.6 9

Page 36: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 17 / 07 / 12

REF. NO. EP/UPL-5/2012/9

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 09 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/9

Description of Source

: Stack attached to Water Scrubber + Alkali Scrubber of Reactor (PCl5 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (34) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

0.9 9 5 Hydro Chloride Vapours (HCl) mg/NM3

15.1 20

Page 37: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 17 / 07 / 12

REF. NO. EP/UPL-5/2012/10

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 09 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/10

Description of Source

: Stack attached to Caustic Scrubber of Distillation Column (POCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (34) - 3 Stack Dia. m 0.2 - 4 Hydro Chloride Vapours (HCl) mg/NM3

9.1 20

Page 38: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 17 / 07 / 12

REF. NO. EP/UPL-5/2012/11

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 09 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/11

Description of Source

: Stack attached to Caustic Scrubber WAD 100 (TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (34) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

2.7 9 5 Hydro Chloride Vapours (HCl) mg/NM3

4.1 20

Page 39: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 17 / 07 / 12

REF. NO. EP/UPL-5/2012/12

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 09 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/12

Description of Source

: Stack attached to Caustic Scrubber HCl Furnace 100(TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 49 - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

17.8 20

Page 40: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 17 / 07 / 12

REF. NO. EP/UPL-5/2012/13

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 09 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/13

Description of Source

: Stack attached to Water Scrubber + Ventury Scrubber (C-2102) (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (34) - 3 Stack Dia. m 0.15 - 4 Hydro Chloride Vapours (HCl) mg/NM3

13.5 20

Page 41: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 17 / 07 / 12

REF. NO. EP/UPL-5/2012/14

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 09 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/14

Description of Source

: Stack attached to Water Scrubber + Ventury Scrubber (C-2002A) (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (34) - 3 Stack Dia. m 0.15 - 4 Hydro Chloride Vapours (HCl) mg/NM3

10.6 20

Page 42: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch. Description of Sample : Gaseous sample of

Ambient Air Sampling Procedure : As per IS method

Date of Sampling : 09 / 07 / 12 Duration of Sampling (Hrs)

: 24 Hrs.

Sample Collected by : EN-PRO Team Packing / Seal : Seal Description of Location : Nr Pump House Lab ID Code : EP/AA/0712/15

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS: 5182

Meteorological Data / Environmental Condition Avg. Wind velocity

km/hr Prominent Wind

Direction Relative Humidity (%) Temperature (0C)

Max. Min. Max. Min. 3.4 SW - NE 72 40 39 24

RESULT TABLE Sr. No.

Parameters Unit Result GPCB Limit

1 Respirable Suspended Particulate Matter (PM10) μg/m3 68.3 100

2 Suspended Particulate Matter (PM2.5) μg/m3 34.2 60

3 Sulphur Dioxide (SO2) μg/m3 11.9 80

4 Nitrogen Oxides (NOx) μg/m3 36.1 80

5 Hydro Chloride Vapour (HCl) μg/m3 2.5 200

6 Chlorine (Cl2) μg/m3 BDL 100

7 Ammonia (NH3) μg/m3 BDL 400

8 Hydrogen Flouride (HF) μg/m3 BDL 60

9 Hydrogen Sulphide (H2S) μg/m3 BDL 500

10 Carbon Di-Sulphide (CS2) μg/m3 62.7 2000

ISSUE DATE 17 / 07 / 12 REF. NO. EP/UPL-5/2012/15

Page 43: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

11 Hydrocarbon (HC) μg/m3 BDL 160

12 Phosphorus Pent-oxide Fumes (P2O5) μg/m3 BDL 70

Note: BDL: - Below Detectable Limit ANALYSED BY CHECKED BY Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

Description of Monitoring

: Noise Monitoring Test Method : Instrumental method (SL/Lutron – 4010)

Date of Monitoring

: 09 / 07 / 12 Lab ID Code : EP/N/0712/16

Sample Collected by

: ENPRO Team Duration of Sampling

: 10 Min/Location

Description of Location

: As per Table Protocol (Purpose) : Monthly Monitoring

Type of Test : On Site Testing RESULT TABLE

Sr. No. Location Noise Level dB(A)

Leq Day Time Night

Time 1. Primary Brine 66.5 63.4 2. Secondary Brine 68.3 63.2 3. H2 Compressor 87.7 85.3 4. Cl2 Compressor 88.3 81.2 5. Utility Block - Mechanical 78.4 71.5 6. WP-CO Pump 68.2 61.1 7. Power Plant GT 86.1 78.6 8. Utility - MNZ 79.5 72.6 9. D-14 Tank MNZ 80.2 75.3

10. SPD - Panel Room - MNZ 76.7 73.4 11. Security Gate 70.5 66.2 12. 1 MLD ETP 65.1 62.5

ISSUE DATE 17 / 07 / 12 REF. NO. EP/UPL-5/2012/16

Page 44: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

13. Belt Filter Vacuum Pump - MNZ 73.9 67.8 Norms db(A) Leq TLV - 90 ANALYSED BY CHECKED BY Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

Description of Monitoring

: Noise Monitoring Test Method : Instrumental method (SL/Lutron – 4010)

Date of Monitoring

: 09 / 07 / 12 Lab ID Code : EP/N/0712/17

Sample Collected by

: ENPRO Team Duration of Sampling

: 10 Min/Location

Description of Location

: As per Table Protocol (Purpose) : Monthly Monitoring

Type of Test : On Site Testing

RESULT TABLE

Sr. No.

Location Day Time Noise Level dB(A) Leq

Night Time Noise Level dB(A) Leq

1. Fencing Wall East Side (Nr. C-Tech ETP) 64.8 61.4 2. Fencing Wall North Side (Nr. Rais Plant) 61.7 58.4 3. Fencing Wall South Side (Nr. Secondary Brine 65.2 63.3 4. Fencing Wall West Side (Nr. Salt Yard) 63.4 54.6

Norms db(A) Leq 75 70 Note: Day Time: 06:00 AM to 10:00 PM & Night Time: 10:00 PM to 06:00 AM ANALYSED BY CHECKED BY

ISSUE DATE 17 / 07 / 12 REF. NO. EP/UPL-5/2012/17

Page 45: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit

ISSUE DATE 25 / 07 / 12

REF. NO. EP/UPL-5/2012/2

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 20 / 07 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/18

Description of Source

: Stack attached to Gas Turbine ( Power Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Natural Gas

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 138 - 3 Avg. Velocity m/s 14.2 - 4 Avg.flow rate m3/hr. 255775 - 5 Stack Dia. m 3.0 - 6 Particulate Matter (PM) mg/NM3 BDL 150 7 Sulphur Oxides (SOx) ppm BDL 100 8 Nitrogen Oxides (NOx) ppm 24.3 50

Page 46: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

ANALYSED BY CHECKED BY Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ISSUE DATE 25 / 07 / 12

REF. NO. EP/UPL-5/2012/3

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 20 / 07 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/19

Description of Source

: Stack attached to Thermic Fluid Heater (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : HSD

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 33.0 - 2 Flue Gas Temp. 0 C 210 - 3 Avg. Velocity m/s 14.0 - 4 Avg.flow rate m3/hr. 9038 - 5 Stack Dia. m 0.6 - 6 Particulate Matter (PM) mg/NM3 72.5 150

Page 47: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

ANALYSED BY CHECKED BY Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

7 Sulphur Oxides (SOx) ppm 15.6 100 8 Nitrogen Oxides (NOx) ppm 20.3 50

ISSUE DATE 25 / 07 / 12

REF. NO. EP/UPL-5/2012/4

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 20 / 07 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/20

Description of Source

: Stack attached to Water Scrubber of Wet Spray Dryer (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 70 - 3 Avg. Velocity m/s 13.2 - 4 Avg.flow rate m3/hr. 120861 - 5 Stack Dia. m 1.8 -

Page 48: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

ANALYSED BY CHECKED BY Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

6 Particulate Matter (PM) mg/NM3 15.1 20

ISSUE DATE 25 / 07 / 12

REF. NO. EP/UPL-5/2012/5

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 20 / 07 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/21

Description of Source

: Stack attached to Bag Filter of RVDF (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 64 - 3 Avg. Velocity m/s 11.6 - 4 Avg.flow rate m3/hr. 1311 - 5 Stack Dia. m 0.2 -

Page 49: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

ANALYSED BY CHECKED BY Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

6 Particulate Matter (PM) mg/NM3 11.8 20

ISSUE DATE 25 / 07 / 12

REF. NO. EP/UPL-5/2012/6

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 20 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/22

Description of Source

: Stack attached to Alkali Scrubber of-D-14 New EDA Reactor (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (33) - 3 Stack Dia. m 0.1 -

Page 50: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

ANALYSED BY CHECKED BY Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

4 Hydrogen Sulphide (H2S) mg/NM3 20.0 45 5 Carbon Di-Sulphide (CS2) mg/NM3 99.5 180

ISSUE DATE 25 / 07 / 12

REF. NO. EP/UPL-5/2012/7

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 20 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/23

Description of Source

: Stack attached to Caustic Scrubber of Distillation Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (33) -

Page 51: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 7.9 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.8 9

ISSUE DATE 25 / 07 / 12

REF. NO. EP/UPL-5/2012/8

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 20 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/24

Description of Source

: Stack attached to Caustic Scrubber of Storage Tank & Drum Filling Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Storage Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 -

Page 52: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

2 Flue Gas Temp. 0 C Ambient (33) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 7.0 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.2 9

ISSUE DATE 25 / 07 / 12

REF. NO. EP/UPL-5/2012/9

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 20 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/25

Description of Source

: Stack attached to Water Scrubber + Alkali Scrubber of Reactor (PCl5 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 9.0 -

Page 53: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

ANALYSED BY CHECKED BY Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

2 Flue Gas Temp. 0 C Ambient (33) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3 0.5 9 5 Hydro Chloride Vapours (HCl) mg/NM3 12.6 20

ISSUE DATE 25 / 07 / 12

REF. NO. EP/UPL-5/2012/10

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 20 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/26

Description of Source

: Stack attached to Caustic Scrubber of Distillation Column (POCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

Page 54: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

ANALYSED BY CHECKED BY Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (33) - 3 Stack Dia. m 0.2 - 4 Hydro Chloride Vapours (HCl) mg/NM3 7.6 20

ISSUE DATE 25 / 07 / 12

REF. NO. EP/UPL-5/2012/11

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 20 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/27

Description of Source

: Stack attached to Caustic Scrubber WAD 100 (TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

Page 55: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (33) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3 2.2 9 5 Hydro Chloride Vapours (HCl) mg/NM3 5.8 20

ISSUE DATE 25 / 07 / 12

REF. NO. EP/UPL-5/2012/12

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 20 / 07 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0712/28

Description of Source

: Stack attached to Caustic Scrubber HCl Furnace 100(TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

Page 56: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 58 - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 14.2 20

Page 57: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT

Test Report No.: EP/UPL-5/2012/1 Issue Date: 23 / 08 / 12

Customer’s Name & Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch. Description of Sample

: ETP Outlet (Treated Effluent)

Quantity/No. of Sample : 5 L / 1 No

Sampling By : ENPRO Team Packing/Seal : Sealed Date of Sampling : 16 / 08 / 12 Sample Received Date

: 17 / 08 / 12 Protocol (purpose) : Waste Water Analysis (Monthly Monitoring)

Date of Starting of Test

: 17 / 08 / 12 Date of Completion : 23 / 08 / 12

Sampling Method : IS 3025 Part-1 Sample ID : EP / WW / 0812 / 1 Test Method : IS 3025 & APHA Type of Sampling : Grab

RESULT TABLE

SR. NO. TEST PARAMETER UNIT RESULTS GPCB LIMIT

1. pH (at 270 C) - 7.11 5.5-8.5 2. Temperature 0C 31 40 3. Colour Pt. Co. 35 100 4. Total Residual Chlorine mg/L BDL 1.0 5. Total Suspended Solids mg/L 54 100

6. Total Dissolved Solids (at 1800 C) mg/L 12912 2100

7. Oil & Grease mg/L 2.0 10

8. Phenolic Compound ( as C6H5OH ) mg/L BDL 1.0

9. Ammonical Nitrogen mg/L 13.6 50 10. Boron as B mg/L BDL 2.0 11. COD mg/L 115 100 12. BOD ( 3 days at 270C ) mg/L 33.0 30 13. Chloride (as Cl) mg/L 4602 600 14. Sulphate (as So4

-2) mg/L 6089 1000 15. Fluoride ( as F) mg/L 0.32 1.5

16. Sulphide mg/L BDL 0.5

17. Cyanides ( as CN ) mg/L BDL 0.2 18. Selenium ( as Se ) mg/L BDL 0.05 19. Zinc mg/L BDL 5.0 20. Lead ( as Pb ) mg/L BDL 0.1

…contd

Page 58: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

SR. NO. TEST PARAMETER UNIT RESULTS GPCB LIMIT

21. Nickel mg/L 0.20 3.0

22. Copper mg/L BDL 2.0

23. Total Chromium mg/L 0.19 2.0

24. Hexavalent Chromium mg/L BDL 0.1

25. Mercury (as Hg ) mg/L BDL 0.01

26. Arsenic ( as As) mg/L BDL 0.2

27. Cadmium ( as Cd ) mg/L BDL 2.0

28. Total Heavy Metal mg/L <1 7.0

29. Percentage Sodium (% Na) % 72.5 60

30. Bioassay Test % 90% 90% Survival of Fish after 96 Hrs. in 100%

Effluent Note: BDL: - Below Detectable Limit

ANALYSED BY CHECKED BY

Page 59: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 13 / 08 / 12

REF. NO. EP/UPL-5/2012/2

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 06 / 08 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/2

Description of Source

: Stack attached to Gas Turbine ( Power Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Natural Gas

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 146 - 3 Avg. Velocity m/s 13.1 - 4 Avg.flow rate m3/hr. 235961 - 5 Stack Dia. m 3.0 - 6 Particulate Matter (PM) mg/NM3 BDL 150 7 Sulphur Oxides (SOx) ppm BDL 100 8 Nitrogen Oxides (NOx) ppm 30.2 50

Page 60: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 13 / 08 / 12

REF. NO. EP/UPL-5/2012/4

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 06 / 08 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/3

Description of Source

: Stack attached to Water Scrubber of Wet Spray Dryer (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 76 - 3 Avg. Velocity m/s 14.3 - 4 Avg.flow rate m3/hr. 130933 - 5 Stack Dia. m 1.8 - 6 Particulate Matter (PM) mg/NM3

17.9 20

Page 61: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 13 / 08 / 12

REF. NO. EP/UPL-5/2012/5

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 06 / 08 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/4

Description of Source

: Stack attached to Bag Filter of RVDF (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 52 - 3 Avg. Velocity m/s 9.3 - 4 Avg.flow rate m3/hr. 1051 - 5 Stack Dia. m 0.2 - 6 Particulate Matter (PM) mg/NM3

14.1 20

Page 62: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 13 / 08 / 12

REF. NO. EP/UPL-5/2012/6

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 06 / 08 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/5

Description of Source

: Stack attached to Alkali Scrubber of-D-14 New EDA Reactor (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.1 - 4 Hydrogen Sulphide (H2S) mg/NM3

16.6 45 5 Carbon Di-Sulphide (CS2) mg/NM3

110 180

Page 63: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 13 / 08 / 12

REF. NO. EP/UPL-5/2012/7

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 06 / 08 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/6

Description of Source

: Stack attached to Caustic Scrubber of Distillation Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

9.3 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 1.1 9

Page 64: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 13 / 08 / 12

REF. NO. EP/UPL-5/2012/8

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 06 / 08 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/7

Description of Source

: Stack attached to Caustic Scrubber of Storage Tank & Drum Filling Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Storage Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

5.7 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.7 9

Page 65: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 13 / 08 / 12

REF. NO. EP/UPL-5/2012/9

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 06 / 08 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/8

Description of Source

: Stack attached to Water Scrubber + Alkali Scrubber of Reactor (PCl5 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

1.0 9 5 Hydro Chloride Vapours (HCl) mg/NM3

14.2 20

Page 66: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 13 / 08 / 12

REF. NO. EP/UPL-5/2012/10

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 06 / 08 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/9

Description of Source

: Stack attached to Caustic Scrubber of Distillation Column (POCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.2 - 4 Hydro Chloride Vapours (HCl) mg/NM3

8.8 20

Page 67: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 13 / 08 / 12

REF. NO. EP/UPL-5/2012/11

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 06 / 08 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/10

Description of Source

: Stack attached to Caustic Scrubber WAD 100 (TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

1.3 9 5 Hydro Chloride Vapours (HCl) mg/NM3

8.0 20

Page 68: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 13 / 08 / 12

REF. NO. EP/UPL-5/2012/12

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 06 / 08 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/11

Description of Source

: Stack attached to Caustic Scrubber HCl Furnace 100(TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 52 - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

12.5 20

Page 69: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch. Description of Sample : Gaseous sample of

Ambient Air Sampling Procedure : As per IS method

Date of Sampling : 06 / 08 / 12 Duration of Sampling (Hrs)

: 24 Hrs.

Sample Collected by : EN-PRO Team Packing / Seal : Seal Description of Location : Nr PCL3 PLANT Lab ID Code : EP/AA/0812/12

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS: 5182

Meteorological Data / Environmental Condition Avg. Wind velocity

km/hr Prominent Wind

Direction Relative Humidity (%) Temperature (0C)

Max. Min. Max. Min. 4.8 SW - NE 78 48 34 23

RESULT TABLE Sr. No.

Parameters Unit Result GPCB Limit

1 Respirable Suspended Particulate Matter (PM10) μg/m3 74.8 100

2 Suspended Particulate Matter (PM2.5) μg/m3 36.2 60

3 Sulphur Dioxide (SO2) μg/m3 23.1 80

4 Nitrogen Oxides (NOx) μg/m3 29.8 80

5 Hydro Chloride Vapour (HCl) μg/m3 5.3 200

6 Chlorine (Cl2) μg/m3 BDL 100

7 Ammonia (NH3) μg/m3 BDL 400

8 Hydrogen Flouride (HF) μg/m3 BDL 60

9 Hydrogen Sulphide (H2S) μg/m3 BDL 500

10 Carbon Di-Sulphide (CS2) μg/m3 72.5 2000

11 Hydrocarbon (HC) μg/m3 BDL 160

12 Phosphorus Pent-oxide Fumes (P2O5) μg/m3 BDL 70

Note: BDL: - Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 13 / 08 / 12 REF. NO. EP/UPL-5/2012/15

Page 70: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

Description of Monitoring

: Noise Monitoring Test Method : Instrumental method (SL/Lutron – 4010)

Date of Monitoring

: 06 / 08 / 12 Lab ID Code : EP/N/0812/13

Sample Collected by

: ENPRO Team Duration of Sampling

: 10 Min/Location

Description of Location

: As per Table Protocol (Purpose) : Monthly Monitoring

Type of Test : On Site Testing RESULT TABLE

Sr. No. Location Noise Level dB(A)

Leq Day Time Night

Time 1. Primary Brine 68.5 65.7 2. Secondary Brine 67.3 64.3 3. H2 Compressor 85.4 83.1 4. Cl2 Compressor 89.1 81.4 5. Utility Block - Mechanical 80.2 76.9 6. WP-CO Pump 70.5 66.2 7. Power Plant GT 87.4 82.2 8. Utility - MNZ 81.2 75.4 9. D-14 Tank MNZ 83.1 72.3

10. SPD - Panel Room - MNZ 78.1 68.9 11. Security Gate 68.2 63.7 12. 1 MLD ETP 67.7 65.4 13. Belt Filter Vacuum Pump - MNZ 87.5 85.6

Norms db(A) Leq TLV - 90 ANALYSED BY CHECKED BY

ISSUE DATE 13 / 08 / 12 REF. NO. EP/UPL-5/2012/16

Page 71: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

Description of Monitoring

: Noise Monitoring Test Method : Instrumental method (SL/Lutron – 4010)

Date of Monitoring

: 06 / 08 / 12 Lab ID Code : EP/N/0812/14

Sample Collected by

: ENPRO Team Duration of Sampling

: 10 Min/Location

Description of Location

: As per Table Protocol (Purpose) : Monthly Monitoring

Type of Test : On Site Testing

RESULT TABLE

Sr. No.

Location Day Time Noise Level dB(A) Leq

Night Time Noise Level dB(A) Leq

1. Fencing Wall East Side (Nr. C-Tech ETP) 67.9 62.5 2. Fencing Wall North Side (Nr. Rais Plant) 64.3 62.2 3. Fencing Wall South Side (Nr. Secondary Brine 67.5 63.1 4. Fencing Wall West Side (Nr. Salt Yard) 62.8 58.7

Norms db(A) Leq 75 70 Note: Day Time: 06:00 AM to 10:00 PM & Night Time: 10:00 PM to 06:00 AM ANALYSED BY CHECKED BY

ISSUE DATE 13 / 08 / 12 REF. NO. EP/UPL-5/2012/17

Page 72: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 23 / 08 / 12

REF. NO. EP/UPL-5/2012/2

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 16 / 08 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/15

Description of Source

: Stack attached to Gas Turbine ( Power Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Natural Gas

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 140 - 3 Avg. Velocity m/s 13.2 - 4 Avg.flow rate m3/hr. 237762 - 5 Stack Dia. m 3.0 - 6 Particulate Matter (PM) mg/NM3 BDL 150 7 Sulphur Oxides (SOx) ppm BDL 100 8 Nitrogen Oxides (NOx) ppm 22.5 50

Page 73: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 23 / 08 / 12

REF. NO. EP/UPL-5/2012/3

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 16 / 08 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/16

Description of Source

: Stack attached to Thermic Fluid Heater (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : HSD

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 33.0 - 2 Flue Gas Temp. 0 C 216 - 3 Avg. Velocity m/s 9.6 -

4 Avg.flow rate m3/hr. 6585 - 5 Stack Dia. m 0.6 - 6 Particulate Matter (PM) mg/NM3 46.3 150 7 Sulphur Oxides (SOx) ppm 12.5 100 8 Nitrogen Oxides (NOx) ppm 18.0 50

Page 74: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 23 / 08 / 12

REF. NO. EP/UPL-5/2012/4

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 16 / 08 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/17

Description of Source

: Stack attached to Water Scrubber of Wet Spray Dryer (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 72 - 3 Avg. Velocity m/s 13.1 - 4 Avg.flow rate m3/hr. 119946 - 5 Stack Dia. m 1.8 - 6 Particulate Matter (PM) mg/NM3 14.2 20

Page 75: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 23 / 08 / 12

REF. NO. EP/UPL-5/2012/5

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 16 / 08 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/18

Description of Source

: Stack attached to Bag Filter of RVDF (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 64 - 3 Avg. Velocity m/s 10.3 - 4 Avg.flow rate m3/hr. 1164 - 5 Stack Dia. m 0.2 - 6 Particulate Matter (PM) mg/NM3 12.3 20

Page 76: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 23 / 08 / 12

REF. NO. EP/UPL-5/2012/6

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 16 / 08 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/19

Description of Source

: Stack attached to Alkali Scrubber of-D-14 New EDA Reactor (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.1 - 4 Hydrogen Sulphide (H2S) mg/NM3 21.8 45 5 Carbon Di-Sulphide (CS2) mg/NM3 122 180

Page 77: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 23 / 08 / 12

REF. NO. EP/UPL-5/2012/7

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 16 / 08 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/20

Description of Source

: Stack attached to Caustic Scrubber of Distillation Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 10.8 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.6 9

Page 78: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 23 / 08 / 12

REF. NO. EP/UPL-5/2012/8

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 16 / 08 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/20

Description of Source

: Stack attached to Caustic Scrubber of Storage Tank & Drum Filling Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Storage Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 6.8 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.4 9

Page 79: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 23 / 08 / 12

REF. NO. EP/UPL-5/2012/9

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 16 / 08 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/22

Description of Source

: Stack attached to Water Scrubber + Alkali Scrubber of Reactor (PCl5 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 9.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3 0.8 9 5 Hydro Chloride Vapours (HCl) mg/NM3 10.7 20

Page 80: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 23 / 08 / 12

REF. NO. EP/UPL-5/2012/10

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 16 / 08 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/23

Description of Source

: Stack attached to Caustic Scrubber of Distillation Column (POCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.2 - 4 Hydro Chloride Vapours (HCl) mg/NM3 8.3 20

Page 81: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 23 / 08 / 12

REF. NO. EP/UPL-5/2012/11

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 16 / 08 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/24

Description of Source

: Stack attached to Caustic Scrubber WAD 100 (TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3 2.5 9 5 Hydro Chloride Vapours (HCl) mg/NM3 4.9 20

Page 82: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 23 / 08 / 12

REF. NO. EP/UPL-5/2012/12

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 16 / 08 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0812/25

Description of Source

: Stack attached to Caustic Scrubber HCl Furnace 100(TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 46 - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 15.8 20

Page 83: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT

Test Report No.: EP/UPL-5/2012/1 Issue Date: 10 / 09 / 12

Customer’s Name & Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch. Description of Sample

: ETP Outlet (Treated Effluent)

Quantity/No. of Sample : 5 L / 1 No

Sampling By : ENPRO Team Packing/Seal : Sealed Date of Sampling : 04 / 09 / 12 Sample Received Date

: 05 / 09 / 12 Protocol (purpose) : Waste Water Analysis (Monthly Monitoring)

Date of Starting of Test

: 05 / 09 / 12 Date of Completion : 10 / 09 / 12

Sampling Method : IS 3025 Part-1 Sample ID : EP / WW / 0912 / 1 Test Method : IS 3025 & APHA Type of Sampling : Grab

RESULT TABLE

SR. NO. TEST PARAMETER UNIT RESULTS GPCB LIMIT

1. pH (at 270 C) - 6.89 5.5-8.5 2. Temperature 0C 30 40 3. Colour Pt. Co. 32 100 4. Total Residual Chlorine mg/L BDL 1.0 5. Total Suspended Solids mg/L 68 100

6. Total Dissolved Solids (at 1800 C) mg/L 26788 2100

7. Oil & Grease mg/L 1.4 10

8. Phenolic Compound ( as C6H5OH ) mg/L BDL 1.0

9. Ammonical Nitrogen mg/L 14.3 50 10. Boron as B mg/L BDL 2.0 11. COD mg/L 204 100 12. BOD ( 3 days at 270C ) mg/L 49 30 13. Chloride (as Cl) mg/L 6163 600 14. Sulphate (as So4

-2) mg/L 4436 1000 15. Fluoride ( as F) mg/L 0.28 1.5

16. Sulphide mg/L 0.4 0.5

17. Cyanides ( as CN ) mg/L BDL 0.2 18. Selenium ( as Se ) mg/L BDL 0.05 19. Zinc mg/L BDL 5.0 20. Lead ( as Pb ) mg/L BDL 0.1

…contd

Page 84: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

SR. NO. TEST PARAMETER UNIT RESULTS GPCB LIMIT

21. Nickel mg/L 0.16 3.0

22. Copper mg/L BDL 2.0

23. Total Chromium mg/L 0.23 2.0

24. Hexavalent Chromium mg/L BDL 0.1

25. Mercury (as Hg ) mg/L BDL 0.01

26. Arsenic ( as As) mg/L BDL 0.2

27. Cadmium ( as Cd ) mg/L BDL 2.0

28. Total Heavy Metal mg/L <1 7.0

29. Percentage Sodium (% Na) % 58.4 60

30. Bioassay Test % 90 % 90% Survival of Fish after 96 Hrs. in 100%

Effluent Note: BDL: - Below Detectable Limit

ANALYSED BY CHECKED BY

Page 85: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12

REF. NO. EP/UPL-5/2012/2

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 03 / 09 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/2

Description of Source

: Stack attached to Gas Turbine ( Power Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Natural Gas

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 136 - 3 Avg. Velocity m/s 13.5 - 4 Avg.flow rate m3/hr. 246352 - 5 Stack Dia. m 3.0 - 6 Particulate Matter (PM) mg/NM3

BDL 150 7 Sulphur Oxides (SOx) ppm BDL 100 8 Nitrogen Oxides (NOx) ppm 24.1 50

Page 86: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12

REF. NO. EP/UPL-5/2012/4

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 03 / 09 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/3

Description of Source

: Stack attached to Water Scrubber of Wet Spray Dryer (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 78 - 3 Avg. Velocity m/s 14.3 - 4 Avg.flow rate m3/hr. 130936 - 5 Stack Dia. m 1.8 - 6 Particulate Matter (PM) mg/NM3

15.2 20

Page 87: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12

REF. NO. EP/UPL-5/2012/5

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 03 / 09 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/4

Description of Source

: Stack attached to Bag Filter of RVDF (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 68 - 3 Avg. Velocity m/s 11.2 - 4 Avg.flow rate m3/hr. 1050 - 5 Stack Dia. m 0.2 - 6 Particulate Matter (PM) mg/NM3

14.2 20

Page 88: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12TEST REPORT

Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12

REF. NO. EP/UPL-5/2012/3

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 03 / 09 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/5

Description of Source

: Stack attached to Thermic Fluid Heater (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : HSD

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 33.0 - 2 Flue Gas Temp. 0 C 196 - 3 Avg. Velocity m/s 10.9 - 4 Avg.flow rate m3/hr. 8422 - 5 Stack Dia. m 0.6 - 6 Particulate Matter (PM) mg/NM3 52.2 150 7 Sulphur Oxides (SOx) ppm 10.5 100 8 Nitrogen Oxides (NOx) ppm 16.8 50

Page 89: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12

REF. NO. EP/UPL-5/2012/6

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 03 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/6

Description of Source

: Stack attached to Alkali Scrubber of-D-14 New EDA Reactor (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.1 - 4 Hydrogen Sulphide (H2S) mg/NM3

19.3 45 5 Carbon Di-Sulphide (CS2) mg/NM3

101.2 180

Page 90: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12TEST REPORT

Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12

REF. NO. EP/UPL-5/2012/7

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 03 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/7

Description of Source

: Stack attached to Caustic Scrubber of Distillation Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

9.6 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 1.2 9

Page 91: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12TEST REPORT

Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12

REF. NO. EP/UPL-5/2012/8

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 03 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/8

Description of Source

: Stack attached to Caustic Scrubber of Storage Tank & Drum Filling Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Storage Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

6.2 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.6 9

Page 92: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12

REF. NO. EP/UPL-5/2012/9

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 03 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/9

Description of Source

: Stack attached to Water Scrubber + Alkali Scrubber of Reactor (PCl5 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

1.1 9 5 Hydro Chloride Vapours (HCl) mg/NM3

11.0 20

Page 93: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12

REF. NO. EP/UPL-5/2012/10

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 03 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/10

Description of Source

: Stack attached to Caustic Scrubber of Distillation Column (POCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.2 - 4 Hydro Chloride Vapours (HCl) mg/NM3

8.4 20

Page 94: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12

REF. NO. EP/UPL-5/2012/11

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 03 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/11

Description of Source

: Stack attached to Caustic Scrubber WAD 100 (TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

2.1 9 5 Hydro Chloride Vapours (HCl) mg/NM3

4.2 20

Page 95: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12

REF. NO. EP/UPL-5/2012/12

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 03 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/12

Description of Source

: Stack attached to Caustic Scrubber HCl Furnace 100(TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 41 - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

14.9 20

Page 96: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12

REF. NO. EP/UPL-5/2012/13

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 03 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/13

Description of Source

: Stack attached to Water Scrubber + Ventury Scrubber (C-2102) (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.15 - 4 Hydro Chloride Vapours (HCl) mg/NM3

12.5 20

Page 97: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12

REF. NO. EP/UPL-5/2012/14

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 03 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/14

Description of Source

: Stack attached to Water Scrubber + Ventury Scrubber (C-2002A) (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.15 - 4 Hydro Chloride Vapours (HCl) mg/NM3 9.2 20

Page 98: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch. Description of Sample : Gaseous sample of

Ambient Air Sampling Procedure : As per IS method

Date of Sampling : 03 / 09 / 12 Duration of Sampling (Hrs)

: 24 Hrs.

Sample Collected by : EN-PRO Team Packing / Seal : Seal Description of Location : Nr. Raise Plant

Toilet Block Lab ID Code : EP/AA/0912/15

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS: 5182

Meteorological Data / Environmental Condition Avg. Wind velocity

km/hr Prominent Wind

Direction Relative Humidity (%) Temperature (0C)

Max. Min. Max. Min. 4.2 SW - NE 72 44 35 25

RESULT TABLE Sr. No.

Parameters Unit Result GPCB Limit

1 Respirable Suspended Particulate Matter (PM10) μg/m3 77.2 100

2 Suspended Particulate Matter (PM2.5) μg/m3 44.3 60

3 Sulphur Dioxide (SO2) μg/m3 23.5 80

4 Nitrogen Oxides (NOx) μg/m3 31.1 80

5 Hydro Chloride Vapour (HCl) μg/m3 4.3 200

6 Chlorine (Cl2) μg/m3 BDL 100

7 Ammonia (NH3) μg/m3 BDL 400

8 Hydrogen Flouride (HF) μg/m3 BDL 60

9 Hydrogen Sulphide (H2S) μg/m3 BDL 500

10 Carbon Di-Sulphide (CS2) μg/m3 120.2 2000

11 Hydrocarbon (HC) μg/m3 BDL 160

12 Phosphorus Pent-oxide Fumes (P2O5) μg/m3 BDL 70

Note: BDL: - Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12 REF. NO. EP/UPL-5/2012/15

Page 99: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

Description of Monitoring

: Noise Monitoring Test Method : Instrumental method (SL/Lutron – 4010)

Date of Monitoring

: 03 / 09 / 12 Lab ID Code : EP/N/0912/16

Sample Collected by

: ENPRO Team Duration of Sampling

: 10 Min/Location

Description of Location

: As per Table Protocol (Purpose) : Monthly Monitoring

Type of Test : On Site Testing RESULT TABLE

Sr. No. Location Noise Level dB(A)

Leq Day Time Night

Time 1. Primary Brine 70.2 69.5 2. Secondary Brine 65.3 63.4 3. H2 Compressor 87.1 85.6 4. Cl2 Compressor 88.3 86.5 5. Utility Block - Mechanical 82.4 80.3 6. WP-CO Pump 71.8 63.3 7. Power Plant GT 88.6 83.4 8. Utility - MNZ 80.2 79.5 9. D-14 Tank MNZ 84.6 79.6

10. SPD - Panel Room - MNZ 76.7 75.0 11. Security Gate 64.3 60.2 12. 1 MLD ETP 68.4 66.5 13. Belt Filter Vacuum Pump - MNZ 83.7 76.3

Norms db(A) Leq TLV - 90 ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12 REF. NO. EP/UPL-5/2012/16

Page 100: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

Description of Monitoring

: Noise Monitoring Test Method : Instrumental method (SL/Lutron – 4010)

Date of Monitoring

: 03 / 09 / 12 Lab ID Code : EP/N/0912/17

Sample Collected by

: ENPRO Team Duration of Sampling

: 10 Min/Location

Description of Location

: As per Table Protocol (Purpose) : Monthly Monitoring

Type of Test : On Site Testing

RESULT TABLE

Sr. No.

Location Day Time Noise Level dB(A) Leq

Night Time Noise Level dB(A) Leq

1. Fencing Wall East Side (Nr. C-Tech ETP) 67.9 62.5 2. Fencing Wall North Side (Nr. Rais Plant) 64.3 62.2 3. Fencing Wall South Side (Nr. Secondary Brine 67.5 63.1 4. Fencing Wall West Side (Nr. Salt Yard) 62.8 58.7

Norms db(A) Leq 75 70 Note: Day Time: 06:00 AM to 10:00 PM & Night Time: 10:00 PM to 06:00 AM ANALYSED BY CHECKED BY

ISSUE DATE 10 / 09 / 12 REF. NO. EP/UPL-5/2012/17

Page 101: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 22 / 09 / 12

REF. NO. EP/UPL-5/2012/2

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 18 / 09 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/18

Description of Source

: Stack attached to Gas Turbine ( Power Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Natural Gas

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 136 - 3 Avg. Velocity m/s 13.5 - 4 Avg.flow rate m3/hr. 246352 - 5 Stack Dia. m 3.0 - 6 Particulate Matter (PM) mg/NM3 BDL 150 7 Sulphur Oxides (SOx) ppm BDL 100 8 Nitrogen Oxides (NOx) ppm 24.1 50

Page 102: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12TEST REPORT

Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 22 / 09 / 12

REF. NO. EP/UPL-5/2012/3

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 18 / 09 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/19

Description of Source

: Stack attached to Thermic Fluid Heater (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : HSD

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 33.0 - 2 Flue Gas Temp. 0 C 198 - 3 Avg. Velocity m/s 10.3 - 4 Avg.flow rate m3/hr. 7622 - 5 Stack Dia. m 0.6 - 6 Particulate Matter (PM) mg/NM3 45.6 150 7 Sulphur Oxides (SOx) ppm 10.6 100 8 Nitrogen Oxides (NOx) ppm 15.2 50

Page 103: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 22 / 09 / 12

REF. NO. EP/UPL-5/2012/4

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 18 / 09 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/20

Description of Source

: Stack attached to Water Scrubber of Wet Spray Dryer (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 75 - 3 Avg. Velocity m/s 13.2 - 4 Avg.flow rate m3/hr. 141296 - 5 Stack Dia. m 1.8 - 6 Particulate Matter (PM) mg/NM3 13.4 20

Page 104: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 22 / 09 / 12

REF. NO. EP/UPL-5/2012/5

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 18 / 09 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/21

Description of Source

: Stack attached to Bag Filter of RVDF (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 65 - 3 Avg. Velocity m/s 10.9 - 4 Avg.flow rate m3/hr. 1101 - 5 Stack Dia. m 0.2 - 6 Particulate Matter (PM) mg/NM3 15.1 20

Page 105: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 22 / 09 / 12

REF. NO. EP/UPL-5/2012/6

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 18 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/22

Description of Source

: Stack attached to Alkali Scrubber of-D-14 New EDA Reactor (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.1 - 4 Hydrogen Sulphide (H2S) mg/NM3 18.6 45 5 Carbon Di-Sulphide (CS2) mg/NM3 99.4 180

Page 106: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12TEST REPORT

Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 22 / 09 / 12

REF. NO. EP/UPL-5/2012/7

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 18 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/23

Description of Source

: Stack attached to Caustic Scrubber of Distillation Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 9.2 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.9 9

Page 107: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 22 / 09 / 12

REF. NO. EP/UPL-5/2012/8

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 18 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/24

Description of Source

: Stack attached to Caustic Scrubber of Storage Tank & Drum Filling Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Storage Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 6.1 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.8 9

Page 108: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 22 / 09 / 12

REF. NO. EP/UPL-5/2012/9

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 18 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/25

Description of Source

: Stack attached to Water Scrubber + Alkali Scrubber of Reactor (PCl5 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3 0.5 9 5 Hydro Chloride Vapours (HCl) mg/NM3 9.9 20

Page 109: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 22 / 09 / 12

REF. NO. EP/UPL-5/2012/10

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 18 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/26

Description of Source

: Stack attached to Caustic Scrubber of Distillation Column (POCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.2 - 4 Hydro Chloride Vapours (HCl) mg/NM3

9.4 20

Page 110: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 22 / 09 / 12

REF. NO. EP/UPL-5/2012/11

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 18 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/27

Description of Source

: Stack attached to Caustic Scrubber WAD 100 (TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3 2.4 9 5 Hydro Chloride Vapours (HCl) mg/NM3 4.7 20

Page 111: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 22 / 09 / 12

REF. NO. EP/UPL-5/2012/12

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 18 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/28

Description of Source

: Stack attached to Caustic Scrubber HCl Furnace 100(TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 49 - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 15.9 20

Page 112: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 22 / 09 / 12

REF. NO. EP/UPL-5/2012/13

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 18 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/29

Description of Source

: Stack attached to Water Scrubber + Ventury Scrubber (C-2102) (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.15 - 4 Hydro Chloride Vapours (HCl) mg/NM3

9.8 20

Page 113: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 22 / 09 / 12

REF. NO. EP/UPL-5/2012/14

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 18 / 09 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/0912/30

Description of Source

: Stack attached to Water Scrubber + Ventury Scrubber (C-2002A) (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (30) - 3 Stack Dia. m 0.15 - 4 Hydro Chloride Vapours (HCl) mg/NM3

13.2 20

Page 114: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT

Test Report No.: EP/UPL-5/2012/1 Issue Date: 16 / 10 / 12

Customer’s Name & Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch. Description of Sample

: ETP Outlet (Treated Effluent)

Quantity/No. of Sample : 5 L / 1 No

Sampling By : ENPRO Team Packing/Seal : Sealed Date of Sampling : 09 / 10 / 12 Sample Received Date

: 10 / 10 / 12 Protocol (purpose) : Waste Water Analysis (Monthly Monitoring)

Date of Starting of Test

: 10 / 10 / 12 Date of Completion : 16 / 10 / 12

Sampling Method : IS 3025 Part-1 Sample ID : EP / WW / 1012 / 1 Test Method : IS 3025 & APHA Type of Sampling : Grab

RESULT TABLE

SR. NO. TEST PARAMETER UNIT RESULTS GPCB LIMIT

1. pH (at 270 C) - 6.89 5.5-8.5 2. Temperature 0C 32 40 3. Colour Pt. Co. 45 100 4. Total Residual Chlorine mg/L BDL 1.0 5. Total Suspended Solids mg/L 92 100

6. Total Dissolved Solids (at 1800 C) mg/L 16212 2100

7. Oil & Grease mg/L 3.2 10

8. Phenolic Compound ( as C6H5OH ) mg/L BDL 1.0

9. Ammonical Nitrogen mg/L 11.02 50 10. Boron as B mg/L BDL 2.0 11. COD mg/L 98.40 100 12. BOD ( 3 days at 270C ) mg/L 27.03 30 13. Chloride (as Cl) mg/L 5244 600 14. Sulphate (as So4

-2) mg/L 5333 1000 15. Fluoride ( as F) mg/L 0.16 1.5

16. Sulphide mg/L 0.08 0.5

17. Cyanides ( as CN ) mg/L BDL 0.2 18. Selenium ( as Se ) mg/L BDL 0.05 19. Zinc mg/L BDL 5.0 20. Lead ( as Pb ) mg/L BDL 0.1

…contd

Page 115: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

SR. NO. TEST PARAMETER UNIT RESULTS GPCB LIMIT

21. Nickel mg/L 0.22 3.0

22. Copper mg/L BDL 2.0

23. Total Chromium mg/L 0.32 2.0

24. Hexavalent Chromium mg/L 0.06 0.1

25. Mercury (as Hg ) mg/L BDL 0.01

26. Arsenic ( as As) mg/L BDL 0.2

27. Cadmium ( as Cd ) mg/L BDL 2.0

28. Total Heavy Metal mg/L <1.5 7.0

29. Percentage Sodium (% Na) % 49.8 60

30. Bioassay Test % 90 % 90% Survival of Fish after 96 Hrs. in 100%

Effluent Note: BDL: - Below Detectable Limit

ANALYSED BY CHECKED BY

Page 116: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12

REF. NO. EP/UPL-5/2012/2

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 08 / 10 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/2

Description of Source

: Stack attached to Gas Turbine ( Power Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Natural Gas

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 140 - 3 Avg. Velocity m/s 13.8 - 4 Avg.flow rate m3/hr. 251826 - 5 Stack Dia. m 3.0 - 6 Particulate Matter (PM) mg/NM3

BDL 150 7 Sulphur Oxides (SOx) ppm BDL 100 8 Nitrogen Oxides (NOx) ppm 31.8 50

Page 117: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12

REF. NO. EP/UPL-5/2012/4

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 08 / 10 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/3

Description of Source

: Stack attached to Water Scrubber of Wet Spray Dryer (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 68 - 3 Avg. Velocity m/s 14.2 - 4 Avg.flow rate m3/hr. 130017 - 5 Stack Dia. m 1.8 - 6 Particulate Matter (PM) mg/NM3

18.6 20

Page 118: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12

REF. NO. EP/UPL-5/2012/5

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 08 / 10 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/4

Description of Source

: Stack attached to Bag Filter of RVDF (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 68 - 3 Avg. Velocity m/s 11.2 - 4 Avg.flow rate m3/hr. 1050 - 5 Stack Dia. m 0.2 - 6 Particulate Matter (PM) mg/NM3

14.2 20

Page 119: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12

REF. NO. EP/UPL-5/2012/3

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 08 / 10 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/5

Description of Source

: Stack attached to Thermic Fluid Heater (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : HSD

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 33.0 - 2 Flue Gas Temp. 0 C 210 - 3 Avg. Velocity m/s 11.3 - 4 Avg.flow rate m3/hr. 8362 - 5 Stack Dia. m 0.6 - 6 Particulate Matter (PM) mg/NM3 62.9 150 7 Sulphur Oxides (SOx) ppm 16.1 100 8 Nitrogen Oxides (NOx) ppm 21.0 50

Page 120: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12

REF. NO. EP/UPL-5/2012/6

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 08 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/6

Description of Source

: Stack attached to Alkali Scrubber of-D-14 New EDA Reactor (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.1 - 4 Hydrogen Sulphide (H2S) mg/NM3

4.9 45 5 Carbon Di-Sulphide (CS2) mg/NM3

115 180

Page 121: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12

REF. NO. EP/UPL-5/2012/7

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 08 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/7

Description of Source

: Stack attached to Caustic Scrubber of Distillation Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

6.8 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.5 9

Page 122: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12

REF. NO. EP/UPL-5/2012/8

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 08 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/8

Description of Source

: Stack attached to Caustic Scrubber of Storage Tank & Drum Filling Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Storage Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

4.0 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.3 9

Page 123: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12

REF. NO. EP/UPL-5/2012/9

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 08 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/9

Description of Source

: Stack attached to Water Scrubber + Alkali Scrubber of Reactor (PCl5 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

1.2 9 5 Hydro Chloride Vapours (HCl) mg/NM3

13.9 20

Page 124: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12

REF. NO. EP/UPL-5/2012/10

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 08 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/10

Description of Source

: Stack attached to Caustic Scrubber of Distillation Column (POCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.2 - 4 Hydro Chloride Vapours (HCl) mg/NM3

5.4 20

Page 125: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12

REF. NO. EP/UPL-5/2012/11

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 08 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/11

Description of Source

: Stack attached to Caustic Scrubber WAD 100 (TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

0.9 9 5 Hydro Chloride Vapours (HCl) mg/NM3

7.1 20

Page 126: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12

REF. NO. EP/UPL-5/2012/12

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 08 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/12

Description of Source

: Stack attached to Caustic Scrubber HCl Furnace 100(TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 38 - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

17.3 20

Page 127: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12

REF. NO. EP/UPL-5/2012/13

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 08 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/13

Description of Source

: Stack attached to Water Scrubber + Ventury Scrubber (C-2102) (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.15 - 4 Hydro Chloride Vapours (HCl) mg/NM3 10.9 20

Page 128: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12TEST REPORT

Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12

REF. NO. EP/UPL-5/2012/14

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 08 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/14

Description of Source

: Stack attached to Water Scrubber + Ventury Scrubber (C-2002A) (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.15 - 4 Hydro Chloride Vapours (HCl) mg/NM3

10.9 20

Page 129: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch. Description of Sample : Gaseous sample of

Ambient Air Sampling Procedure : As per IS method

Date of Sampling : 08 / 10 / 12 Duration of Sampling (Hrs)

: 24 Hrs.

Sample Collected by : EN-PRO Team Packing / Seal : Seal Description of Location : Nr. Pump House Lab ID Code : EP/AA/1012/15

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS: 5182

Meteorological Data / Environmental Condition Avg. Wind velocity

km/hr Prominent Wind

Direction Relative Humidity (%) Temperature (0C)

Max. Min. Max. Min. 3.4 SW - NE 60 38 36 24

RESULT TABLE Sr. No.

Parameters Unit Result GPCB Limit

1 Respirable Suspended Particulate Matter (PM10) μg/m3 81.6 100

2 Suspended Particulate Matter (PM2.5) μg/m3 45.2 60

3 Sulphur Dioxide (SO2) μg/m3 24.9 80

4 Nitrogen Oxides (NOx) μg/m3 28.7 80

5 Hydro Chloride Vapour (HCl) μg/m3 6.1 200

6 Chlorine (Cl2) μg/m3 BDL 100

7 Ammonia (NH3) μg/m3 BDL 400

8 Hydrogen Flouride (HF) μg/m3 BDL 60

9 Hydrogen Sulphide (H2S) μg/m3 BDL 500

10 Carbon Di-Sulphide (CS2) μg/m3 99.8 2000

11 Hydrocarbon (HC) μg/m3 BDL 160

12 Phosphorus Pent-oxide Fumes (P2O5) μg/m3 BDL 70

Note: BDL: - Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12 REF. NO. EP/UPL-5/2012/15

Page 130: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12TEST REPORT

Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

Description of Monitoring

: Noise Monitoring Test Method : Instrumental method (SL/Lutron – 4010)

Date of Monitoring

: 08 / 10 / 12 Lab ID Code : EP/N/1012/16

Sample Collected by

: ENPRO Team Duration of Sampling

: 10 Min/Location

Description of Location

: As per Table Protocol (Purpose) : Monthly Monitoring

Type of Test : On Site Testing RESULT TABLE

Sr. No. Location Noise Level dB(A)

Leq Day Time Night

Time 1. Primary Brine 70.2 68.4 2. Secondary Brine 64.0 60.3 3. H2 Compressor 88.3 86.6 4. Cl2 Compressor 86.4 80.2 5. Utility Block - Mechanical 76.8 72.3 6. WP-CO Pump 68.1 64.9 7. Power Plant GT 89.5 86.7 8. Utility - MNZ 79.2 77.3 9. D-14 Tank MNZ 80.4 76.9

10. SPD - Panel Room - MNZ 75.1 70.2 11. Security Gate 62.7 60.4 12. 1 MLD ETP 65.3 64.2 13. Belt Filter Vacuum Pump - MNZ 84.2 82.5

Norms db(A) Leq TLV - 90 ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12 REF. NO. EP/UPL-5/2012/16

Page 131: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

Description of Monitoring

: Noise Monitoring Test Method : Instrumental method (SL/Lutron – 4010)

Date of Monitoring

: 08 / 10 / 12 Lab ID Code : EP/N/1012/17

Sample Collected by

: ENPRO Team Duration of Sampling

: 10 Min/Location

Description of Location

: As per Table Protocol (Purpose) : Monthly Monitoring

Type of Test : On Site Testing

RESULT TABLE

Sr. No.

Location Day Time Noise Level dB(A) Leq

Night Time Noise Level dB(A) Leq

1. Fencing Wall East Side (Nr. C-Tech ETP) 63.1 59.8 2. Fencing Wall North Side (Nr. Rais Plant) 60.7 57.3 3. Fencing Wall South Side (Nr. Secondary Brine 68.5 66.2 4. Fencing Wall West Side (Nr. Salt Yard) 59.4 57.1

Norms db(A) Leq 75 70 Note: Day Time: 06:00 AM to 10:00 PM & Night Time: 10:00 PM to 06:00 AM ANALYSED BY CHECKED BY

ISSUE DATE 16 / 10 / 12 REF. NO. EP/UPL-5/2012/17

Page 132: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12TEST REPORT

Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 27 / 10 / 12

REF. NO. EP/UPL-5/2012/2

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 23 / 10 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/18

Description of Source

: Stack attached to Gas Turbine ( Power Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Natural Gas

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 126 - 3 Avg. Velocity m/s 12.5 - 4 Avg.flow rate m3/hr. 228103 - 5 Stack Dia. m 3.0 - 6 Particulate Matter (PM) mg/NM3 BDL 150 7 Sulphur Oxides (SOx) ppm BDL 100 8 Nitrogen Oxides (NOx) ppm 28.7 50

Page 133: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 27 / 10 / 12

REF. NO. EP/UPL-5/2012/4

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 23 / 10 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/19

Description of Source

: Stack attached to Water Scrubber of Wet Spray Dryer (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 73 - 3 Avg. Velocity m/s 13.0 - 4 Avg.flow rate m3/hr. 119030 - 5 Stack Dia. m 1.8 - 6 Particulate Matter (PM) mg/NM3 16.1 20

Page 134: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 27 / 10 / 12

REF. NO. EP/UPL-5/2012/5

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 23 / 10 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/20

Description of Source

: Stack attached to Bag Filter of RVDF (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 50 - 3 Avg. Velocity m/s 7.8 - 4 Avg.flow rate m3/hr. 882 - 5 Stack Dia. m 0.2 - 6 Particulate Matter (PM) mg/NM3 13.3 20

Page 135: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 27 / 10 / 12

REF. NO. EP/UPL-5/2012/6

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 23 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/21

Description of Source

: Stack attached to Alkali Scrubber of-D-14 New EDA Reactor (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.1 - 4 Hydrogen Sulphide (H2S) mg/NM3 5.6 45 5 Carbon Di-Sulphide (CS2) mg/NM3 88.8 180

Page 136: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12TEST REPORT

Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 27 / 10 / 12

REF. NO. EP/UPL-5/2012/7

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 23 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/22

Description of Source

: Stack attached to Caustic Scrubber of Distillation Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 8.2 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 1.0 9

Page 137: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 27 / 10 / 12

REF. NO. EP/UPL-5/2012/8

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 23 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/23

Description of Source

: Stack attached to Caustic Scrubber of Storage Tank & Drum Filling Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Storage Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 7.2 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.5 9

Page 138: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 27 / 10 / 12

REF. NO. EP/UPL-5/2012/9

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 23 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/24

Description of Source

: Stack attached to Water Scrubber + Alkali Scrubber of Reactor (PCl5 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3 0.7 9 5 Hydro Chloride Vapours (HCl) mg/NM3 14.7 20

Page 139: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 27 / 10 / 12

REF. NO. EP/UPL-5/2012/10

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 23 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/25

Description of Source

: Stack attached to Caustic Scrubber of Distillation Column (POCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.2 - 4 Hydro Chloride Vapours (HCl) mg/NM3

7.9 20

Page 140: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 27 / 10 / 12

REF. NO. EP/UPL-5/2012/11

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 23 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/26

Description of Source

: Stack attached to Caustic Scrubber WAD 100 (TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (32) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3 1.8 9 5 Hydro Chloride Vapours (HCl) mg/NM3 5.0 20

Page 141: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 27 / 10 / 12

REF. NO. EP/UPL-5/2012/12

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 23 / 10 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1012/27

Description of Source

: Stack attached to Caustic Scrubber HCl Furnace 100(TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 45 - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 13.6 20

Page 142: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT

Test Report No.: EP/UPL-5/2012/1 Issue Date: 28 / 11 / 12

Customer’s Name & Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch. Description of Sample

: ETP Outlet (Treated Effluent)

Quantity/No. of Sample : 5 L / 1 No

Sampling By : ENPRO Team Packing/Seal : Sealed Date of Sampling : 23 / 11 / 12 Sample Received Date

: 24 / 11 / 12 Protocol (purpose) : Waste Water Analysis (Monthly Monitoring)

Date of Starting of Test

: 24 / 11 / 12 Date of Completion : 28 / 11 / 12

Sampling Method : IS 3025 Part-1 Sample ID : EP / WW / 1112 / 1 Test Method : IS 3025 & APHA Type of Sampling : Grab

RESULT TABLE

SR. NO. TEST PARAMETER UNIT RESULTS GPCB LIMIT

1. pH (at 270 C) - 7.32 5.5-8.5 2. Temperature 0C 29 40 3. Colour Pt. Co. 25 100 4. Total Residual Chlorine mg/L BDL 1.0 5. Total Suspended Solids mg/L 84 100

6. Total Dissolved Solids (at 1800 C) mg/L 14628 2100

7. Oil & Grease mg/L 1.8 10

8. Phenolic Compound ( as C6H5OH ) mg/L BDL 1.0

9. Ammonical Nitrogen mg/L 9.78 50 10. Boron as B mg/L BDL 2.0 11. COD mg/L 108.00 100 12. BOD ( 3 days at 270C ) mg/L 30.15 30 13. Chloride (as Cl) mg/L 4874 600 14. Sulphate (as So4

-2) mg/L 3718 1000 15. Fluoride ( as F) mg/L 0.22 1.5

16. Sulphide mg/L 0.32 0.5

17. Cyanides ( as CN ) mg/L BDL 0.2 18. Selenium ( as Se ) mg/L BDL 0.05 19. Zinc mg/L BDL 5.0 20. Lead ( as Pb ) mg/L BDL 0.1

…contd

Page 143: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

SR. NO. TEST PARAMETER UNIT RESULTS GPCB LIMIT

21. Nickel mg/L 0.34 3.0

22. Copper mg/L BDL 2.0

23. Total Chromium mg/L 0.46 2.0

24. Hexavalent Chromium mg/L 0.11 0.1

25. Mercury (as Hg ) mg/L BDL 0.01

26. Arsenic ( as As) mg/L BDL 0.2

27. Cadmium ( as Cd ) mg/L BDL 2.0

28. Total Heavy Metal mg/L <1.5 7.0

29. Percentage Sodium (% Na) % 55.2 60

30. Bioassay Test % 90% 90% Survival of Fish after 96 Hrs. in 100%

Effluent Note: BDL: - Below Detectable Limit

ANALYSED BY CHECKED BY

Page 144: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12

REF. NO. EP/UPL-5/2012/2

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 05 / 11 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/2

Description of Source

: Stack attached to Gas Turbine ( Power Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Natural Gas

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 132 - 3 Avg. Velocity m/s 13.1 - 4 Avg.flow rate m3/hr. 239052 - 5 Stack Dia. m 3.0 - 6 Particulate Matter (PM) mg/NM3

BDL 150 7 Sulphur Oxides (SOx) ppm BDL 100 8 Nitrogen Oxides (NOx) ppm 25.3 50

Page 145: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12

REF. NO. EP/UPL-5/2012/4

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 05 / 11 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/3

Description of Source

: Stack attached to Water Scrubber of Wet Spray Dryer (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 66 - 3 Avg. Velocity m/s 11.7 - 4 Avg.flow rate m3/hr. 107127 - 5 Stack Dia. m 1.8 - 6 Particulate Matter (PM) mg/NM3

19.0 20

Page 146: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12

REF. NO. EP/UPL-5/2012/5

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 05 / 11 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/4

Description of Source

: Stack attached to Bag Filter of RVDF (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 58 - 3 Avg. Velocity m/s 9.0 - 4 Avg.flow rate m3/hr. 1018 - 5 Stack Dia. m 0.2 - 6 Particulate Matter (PM) mg/NM3

11.7 20

Page 147: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12

REF. NO. EP/UPL-5/2012/3

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 05 / 11 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/5

Description of Source

: Stack attached to Thermic Fluid Heater (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : HSD

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 33.0 - 2 Flue Gas Temp. 0 C 189 - 3 Avg. Velocity m/s 10.2 - 4 Avg.flow rate m3/hr. 7548 - 5 Stack Dia. m 0.6 - 6 Particulate Matter (PM) mg/NM3 41.8 150 7 Sulphur Oxides (SOx) ppm 9.2 100 8 Nitrogen Oxides (NOx) ppm 14.5 50

Page 148: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12

REF. NO. EP/UPL-5/2012/6

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 05 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/6

Description of Source

: Stack attached to Alkali Scrubber of-D-14 New EDA Reactor (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (31) - 3 Stack Dia. m 0.1 - 4 Hydrogen Sulphide (H2S) mg/NM3

3.2 45 5 Carbon Di-Sulphide (CS2) mg/NM3

106 180

Page 149: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12

REF. NO. EP/UPL-5/2012/7

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 05 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/7

Description of Source

: Stack attached to Caustic Scrubber of Distillation Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (31) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

10.5 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.7 9

Page 150: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12

REF. NO. EP/UPL-5/2012/8

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 05 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/8

Description of Source

: Stack attached to Caustic Scrubber of Storage Tank & Drum Filling Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Storage Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (31) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

9.8 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.2 9

Page 151: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12

REF. NO. EP/UPL-5/2012/10

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 05 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/09

Description of Source

: Stack attached to Caustic Scrubber of Distillation Column (POCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (31) - 3 Stack Dia. m 0.2 - 4 Hydro Chloride Vapours (HCl) mg/NM3

4.5 20

Page 152: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12

REF. NO. EP/UPL-5/2012/11

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 05 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/10

Description of Source

: Stack attached to Caustic Scrubber WAD 100 (TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (31) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

1.1 9 5 Hydro Chloride Vapours (HCl) mg/NM3

8.6 20

Page 153: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12

REF. NO. EP/UPL-5/2012/12

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 05 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/11

Description of Source

: Stack attached to Caustic Scrubber HCl Furnace 100(TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 40 - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

16.5 20

Page 154: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12

REF. NO. EP/UPL-5/2012/13

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 05 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/12

Description of Source

: Stack attached to Water Scrubber + Ventury Scrubber (C-2102) (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (31) - 3 Stack Dia. m 0.15 - 4 Hydro Chloride Vapours (HCl) mg/NM3 12.0 20

Page 155: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12TEST REPORT

Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12

REF. NO. EP/UPL-5/2012/14

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 05 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/13

Description of Source

: Stack attached to Water Scrubber + Ventury Scrubber (C-2002A) (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (31) - 3 Stack Dia. m 0.15 - 4 Hydro Chloride Vapours (HCl) mg/NM3

6.7 20

Page 156: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch. Description of Sample : Gaseous sample of

Ambient Air Sampling Procedure : As per IS method

Date of Sampling : 05 / 11 / 12 Duration of Sampling (Hrs)

: 24 Hrs.

Sample Collected by : EN-PRO Team Packing / Seal : Seal Description of Location : Nr. ETP Lab ID Code : EP/AA/1112/14

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS: 5182

Meteorological Data / Environmental Condition Avg. Wind velocity

km/hr Prominent Wind

Direction Relative Humidity (%) Temperature (0C)

Max. Min. Max. Min. 2.8 SW – NE 64 40 34 22

RESULT TABLE Sr. No.

Parameters Unit Result GPCB Limit

1 Respirable Suspended Particulate Matter (PM10) μg/m3 83.5 100

2 Suspended Particulate Matter (PM2.5) μg/m3 41.8 60

3 Sulphur Dioxide (SO2) μg/m3 20.4 80

4 Nitrogen Oxides (NOx) μg/m3 26.1 80

5 Hydro Chloride Vapour (HCl) μg/m3 3.8 200

6 Chlorine (Cl2) μg/m3 BDL 100

7 Ammonia (NH3) μg/m3 BDL 400

8 Hydrogen Flouride (HF) μg/m3 BDL 60

9 Hydrogen Sulphide (H2S) μg/m3 BDL 500

10 Carbon Di-Sulphide (CS2) μg/m3 78.4 2000

11 Hydrocarbon (HC) μg/m3 BDL 160

12 Phosphorus Pent-oxide Fumes (P2O5) μg/m3 BDL 70

Note: BDL: - Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12 REF. NO. EP/UPL-5/2012/15

Page 157: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

Description of Monitoring

: Noise Monitoring Test Method : Instrumental method (SL/Lutron – 4010)

Date of Monitoring

: 05 / 11 / 12 Lab ID Code : EP/N/1112/15

Sample Collected by

: ENPRO Team Duration of Sampling

: 10 Min/Location

Description of Location

: As per Table Protocol (Purpose) : Monthly Monitoring

Type of Test : On Site Testing RESULT TABLE

Sr. No. Location Noise Level dB(A)

Leq Day Time Night

Time 1. Primary Brine 66.7 61.9 2. Secondary Brine 68.9 62.8 3. H2 Compressor 86.3 81.2 4. Cl2 Compressor 84.2 82.4 5. Utility Block - Mechanical 75.2 73.3 6. WP-CO Pump 78.1 74.1 7. Power Plant GT 84.3 82.8 8. Utility - MNZ 81.8 79.0 9. D-14 Tank MNZ 83.3 80.8

10. SPD - Panel Room - MNZ 66.2 62.4 11. Security Gate 75.7 71.2 12. 1 MLD ETP 69.3 64.7 13. Belt Filter Vacuum Pump - MNZ 76.2 70.3

Norms db(A) Leq TLV - 90 ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12 REF. NO. EP/UPL-5/2012/16

Page 158: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

Description of Monitoring

: Noise Monitoring Test Method : Instrumental method (SL/Lutron – 4010)

Date of Monitoring

: 05 / 11 / 12 Lab ID Code : EP/N/1112/17

Sample Collected by

: ENPRO Team Duration of Sampling

: 10 Min/Location

Description of Location

: As per Table Protocol (Purpose) : Monthly Monitoring

Type of Test : On Site Testing

RESULT TABLE

Sr. No.

Location Day Time Noise Level dB(A) Leq

Night Time Noise Level dB(A) Leq

1. Fencing Wall East Side (Nr. C-Tech ETP) 69.6 63.1 2. Fencing Wall North Side (Nr. Rais Plant) 65.8 60.4 3. Fencing Wall South Side (Nr. Secondary Brine 66.5 63.8 4. Fencing Wall West Side (Nr. Salt Yard) 61.9 54.6

Norms db(A) Leq 75 70 Note: Day Time: 06:00 AM to 10:00 PM & Night Time: 10:00 PM to 06:00 AM ANALYSED BY CHECKED BY

ISSUE DATE 12 / 11 / 12 REF. NO. EP/UPL-5/2012/16

Page 159: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 11 / 12

REF. NO. EP/UPL-5/2012/2

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 23 / 11 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/17

Description of Source

: Stack attached to Gas Turbine ( Power Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Natural Gas

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 144 - 3 Avg. Velocity m/s 14.3 - 4 Avg.flow rate m3/hr. 260950 - 5 Stack Dia. m 3.0 - 6 Particulate Matter (PM) mg/NM3 BDL 150 7 Sulphur Oxides (SOx) ppm BDL 100 8 Nitrogen Oxides (NOx) ppm 30.1 50

Page 160: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 11 / 12

REF. NO. EP/UPL-5/2012/4

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 23 / 11 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/18

Description of Source

: Stack attached to Water Scrubber of Wet Spray Dryer (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 59 - 3 Avg. Velocity m/s 12.4 - 4 Avg.flow rate m3/hr. 113536 - 5 Stack Dia. m 1.8 - 6 Particulate Matter (PM) mg/NM3 14.3 20

Page 161: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12TEST REPORT

Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 11 / 12

REF. NO. EP/UPL-5/2012/5

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 23 / 11 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/19

Description of Source

: Stack attached to Bag Filter of RVDF (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 52 - 3 Avg. Velocity m/s 8.1 - 4 Avg.flow rate m3/hr. 916 - 5 Stack Dia. m 0.2 - 6 Particulate Matter (PM) mg/NM3 9.9 20

Page 162: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12TEST REPORT

Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 11 / 12

REF. NO. EP/UPL-5/2012/3

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 23 / 11 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/20

Description of Source

: Stack attached to Thermic Fluid Heater (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : HSD

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 33.0 - 2 Flue Gas Temp. 0 C 202 - 3 Avg. Velocity m/s 10.9 - 4 Avg.flow rate m3/hr. 8066 - 5 Stack Dia. m 0.6 - 6 Particulate Matter (PM) mg/NM3 69.3 150 7 Sulphur Oxides (SOx) ppm 13.8 100 8 Nitrogen Oxides (NOx) ppm 19.4 50

Page 163: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 11 / 12

REF. NO. EP/UPL-5/2012/6

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 23 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/21

Description of Source

: Stack attached to Alkali Scrubber of-D-14 New EDA Reactor (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (31) - 3 Stack Dia. m 0.1 - 4 Hydrogen Sulphide (H2S) mg/NM3 4.7 45 5 Carbon Di-Sulphide (CS2) mg/NM3 92.5 180

Page 164: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 11 / 12

REF. NO. EP/UPL-5/2012/7

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 23 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/22

Description of Source

: Stack attached to Caustic Scrubber of Distillation Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (31) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 7.2 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 1.1 9

Page 165: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 11 / 12

REF. NO. EP/UPL-5/2012/8

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 23 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/23

Description of Source

: Stack attached to Caustic Scrubber of Storage Tank & Drum Filling Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Storage Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (31) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 5.1 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.7 9

Page 166: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 11 / 12

REF. NO. EP/UPL-5/2012/9

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 23 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/24

Description of Source

: Stack attached to Water Scrubber + Alkali Scrubber of Reactor (PCl5 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (31) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3 1.0 9 5 Hydro Chloride Vapours (HCl) mg/NM3 12.1 20

Page 167: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 11 / 12

REF. NO. EP/UPL-5/2012/10

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 23 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/25

Description of Source

: Stack attached to Caustic Scrubber of Distillation Column (POCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (31) - 3 Stack Dia. m 0.2 - 4 Hydro Chloride Vapours (HCl) mg/NM3

6.8 20

Page 168: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 11 / 12

REF. NO. EP/UPL-5/2012/11

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 23 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/26

Description of Source

: Stack attached to Caustic Scrubber WAD 100 (TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C Ambient (31) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3 0.7 9 5 Hydro Chloride Vapours (HCl) mg/NM3 3.4 20

Page 169: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 11 / 12

REF. NO. EP/UPL-5/2012/12

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 23 / 11 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1112/27

Description of Source

: Stack attached to Caustic Scrubber HCl Furnace 100(TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30.0 - 2 Flue Gas Temp. 0 C 54 - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3 BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3 12.1 20

Page 170: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT

Test Report No.: EP/UPL-5/2012/1 Issue Date: 28 / 12 / 12

Customer’s Name & Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch. Description of Sample

: ETP Outlet (Treated Effluent)

Quantity/No. of Sample : 5 L / 1 No

Sampling By : ENPRO Team Packing/Seal : Sealed Date of Sampling : 19 / 12 / 12 Sample Received Date

: 20 / 12 / 12 Protocol (purpose) : Waste Water Analysis (Monthly Monitoring)

Date of Starting of Test

: 20 / 12 / 12 Date of Completion : 28 / 12 / 12

Sampling Method : IS 3025 Part-1 Sample ID : EP / WW / 1212 / 1 Test Method : IS 3025 & APHA Type of Sampling : Grab

RESULT TABLE

SR. NO. TEST PARAMETER UNIT RESULTS GPCB LIMIT

1. pH (at 270 C) - 7.04 5.5-8.5 2. Temperature 0C 27 40 3. Colour Pt. Co. 30 100 4. Total Residual Chlorine mg/L BDL 1.0 5. Total Suspended Solids mg/L 90 100

6. Total Dissolved Solids (at 1800 C) mg/L 15800 2100

7. Oil & Grease mg/L 2.6 10

8. Phenolic Compound ( as C6H5OH ) mg/L BDL 1.0

9. Ammonical Nitrogen mg/L 11.23 50 10. Boron as B mg/L BDL 2.0 11. COD mg/L 92.72 100 12. BOD ( 3 days at 270C ) mg/L 28.86 30 13. Chloride (as Cl) mg/L 6618 600 14. Sulphate (as So4

-2) mg/L 4258 1000 15. Fluoride ( as F) mg/L 0.31 1.5

16. Sulphide mg/L 0.56 0.5

17. Cyanides ( as CN ) mg/L BDL 0.2 18. Selenium ( as Se ) mg/L BDL 0.05 19. Zinc mg/L BDL 5.0 20. Lead ( as Pb ) mg/L BDL 0.1

…contd

Page 171: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

SR. NO. TEST PARAMETER UNIT RESULTS GPCB LIMIT

21. Nickel mg/L 0.41 3.0

22. Copper mg/L BDL 2.0

23. Total Chromium mg/L 0.52 2.0

24. Hexavalent Chromium mg/L 0.07 0.1

25. Mercury (as Hg ) mg/L BDL 0.01

26. Arsenic ( as As) mg/L BDL 0.2

27. Cadmium ( as Cd ) mg/L BDL 2.0

28. Total Heavy Metal mg/L <1 7.0

29. Percentage Sodium (% Na) % 58.8 60

30. Bioassay Test % 90% 90% Survival of Fish after 96 Hrs. in 100%

Effluent Note: BDL: - Below Detectable Limit

ANALYSED BY CHECKED BY

Page 172: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/2

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 05 / 12 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/2

Description of Source

: Stack attached to Gas Turbine ( Power Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Natural Gas

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35 - 2 Flue Gas Temp. 0 C 135 - 3 Avg. Velocity m/s 13.4 - 4 Avg.flow rate m3/hr. 244526 - 5 Stack Dia. m 3.0 - 6 Particulate Matter (PM) mg/NM3

BDL 150 7 Sulphur Oxides (SOx) ppm BDL 100 8 Nitrogen Oxides (NOx) ppm 26.3 50

Page 173: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/4

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 19 / 12 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/3

Description of Source

: Stack attached to Water Scrubber of Wet Spray Dryer (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C 65 - 3 Avg. Velocity m/s 13.7 - 4 Avg.flow rate m3/hr. 125439 - 5 Stack Dia. m 1.8 - 6 Particulate Matter (PM) mg/NM3

18.2 20

Page 174: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/5

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 19 / 12 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/4

Description of Source

: Stack attached to Bag Filter of RVDF (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35 - 2 Flue Gas Temp. 0 C 56 - 3 Avg. Velocity m/s 8.7 - 4 Avg.flow rate m3/hr. 983 - 5 Stack Dia. m 0.2 - 6 Particulate Matter (PM) mg/NM3

12.6 20

Page 175: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/6

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 05 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/5

Description of Source

: Stack attached to Alkali Scrubber of-D-14 New EDA Reactor (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.1 - 4 Hydrogen Sulphide (H2S) mg/NM3

2.9 45 5 Carbon Di-Sulphide (CS2) mg/NM3

83.1 180

Page 176: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/7

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 05 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/6

Description of Source

: Stack attached to Caustic Scrubber of Distillation Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

9.5 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 1.6 9

Page 177: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/8

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 05 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/7

Description of Source

: Stack attached to Caustic Scrubber of Storage Tank & Drum Filling Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Storage Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

8.5 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.9 9

Page 178: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/10

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 05 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/8

Description of Source

: Stack attached to Caustic Scrubber of Distillation Column (POCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.2 - 4 Hydro Chloride Vapours (HCl) mg/NM3

8.5 20

Page 179: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/9

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 05 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/9

Description of Source

: Stack attached to Water Scrubber + Alkali Scrubber of Reactor (PCl5 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

0.6 9 5 Hydro Chloride Vapours (HCl) mg/NM3

8.7 20

Page 180: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/9

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 05 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/10

Description of Source

: Stack attached to General Scrubber (PCl5 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

0.4 9 5 Hydro Chloride Vapours (HCl) mg/NM3

7.9 20

Page 181: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/11

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 05 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/11

Description of Source

: Stack attached to Caustic Scrubber WAD 100 (TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

1.9 9 5 Hydro Chloride Vapours (HCl) mg/NM3

6.2 20

Page 182: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/12

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 05 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/12

Description of Source

: Stack attached to Caustic Scrubber HCl Furnace 100(TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C 48 - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

15.3 20

Page 183: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch. Description of Sample : Gaseous sample of

Ambient Air Sampling Procedure : As per IS method

Date of Sampling : 05 / 12 / 12 Duration of Sampling (Hrs)

: 24 Hrs.

Sample Collected by : EN-PRO Team Packing / Seal : Seal Description of Location : Nr. ETP Lab ID Code : EP/AA/1212/13

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS: 5182

Meteorological Data / Environmental Condition Avg. Wind velocity

km/hr Prominent Wind

Direction Relative Humidity (%) Temperature (0C)

Max. Min. Max. Min. 3.1 NE-SW 68 47 33 18

RESULT TABLE Sr. No.

Parameters Unit Result GPCB Limit

1 Respirable Suspended Particulate Matter (PM10) μg/m3 78.4 100

2 Suspended Particulate Matter (PM2.5) μg/m3 37.5 60

3 Sulphur Dioxide (SO2) μg/m3 17.8 80

4 Nitrogen Oxides (NOx) μg/m3 21.6 80

5 Hydro Chloride Vapour (HCl) μg/m3 8.5 200

6 Chlorine (Cl2) μg/m3 BDL 100

7 Ammonia (NH3) μg/m3 BDL 400

8 Hydrogen Flouride (HF) μg/m3 BDL 60

9 Hydrogen Sulphide (H2S) μg/m3 BDL 500

10 Carbon Di-Sulphide (CS2) μg/m3 74.7 2000

11 Hydrocarbon (HC) μg/m3 BDL 160

12 Phosphorus Pent-oxide Fumes (P2O5) μg/m3 BDL 70

Note: BDL: - Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12 REF. NO. EP/UPL-5/2012/15

Page 184: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

Description of Monitoring

: Noise Monitoring Test Method : Instrumental method (SL/Lutron – 4010)

Date of Monitoring

: 05 / 12 / 12 Lab ID Code : EP/N/1212/14

Sample Collected by

: ENPRO Team Duration of Sampling

: 10 Min/Location

Description of Location

: As per Table Protocol (Purpose) : Monthly Monitoring

Type of Test : On Site Testing RESULT TABLE

Sr. No. Location Noise Level dB(A)

Leq Day Time Night

Time 1. Primary Brine 63.5 58.2 2. Secondary Brine 66.4 59.5 3. H2 Compressor 83.5 79.8 4. Cl2 Compressor 80.6 78.7 5. Utility Block - Mechanical 73.5 69.6 6. WP-CO Pump 75.2 70.2 7. Power Plant GT 81.3 78.6 8. Utility - MNZ 78.4 75.2 9. D-14 Tank MNZ 79.5 74.1

10. SPD - Panel Room - MNZ 64.9 60.5 11. Security Gate 72.7 68.4 12. 1 MLD ETP 65.2 59.3 13. Belt Filter Vacuum Pump - MNZ 72.8 65.6

Norms db(A) Leq TLV - 90 ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12 REF. NO. EP/UPL-5/2012/16

Page 185: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

Description of Monitoring

: Noise Monitoring Test Method : Instrumental method (SL/Lutron – 4010)

Date of Monitoring

: 05 / 12 / 12 Lab ID Code : EP/N/1212/15

Sample Collected by

: ENPRO Team Duration of Sampling

: 10 Min/Location

Description of Location

: As per Table Protocol (Purpose) : Monthly Monitoring

Type of Test : On Site Testing

RESULT TABLE

Sr. No.

Location Day Time Noise Level dB(A) Leq

Night Time Noise Level dB(A) Leq

1. Fencing Wall East Side (Nr. C-Tech ETP) 66.5 59.4 2. Fencing Wall North Side (Nr. Rais Plant) 61.8 56.5 3. Fencing Wall South Side (Nr. Secondary Brine 62.7 58.9 4. Fencing Wall West Side (Nr. Salt Yard) 56.2 50.2

Norms db(A) Leq 75 70 Note: Day Time: 06:00 AM to 10:00 PM & Night Time: 10:00 PM to 06:00 AM ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12 REF. NO. EP/UPL-5/2012/16

Page 186: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/2

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 19 / 12 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/16

Description of Source

: Stack attached to Gas Turbine ( Power Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Natural Gas

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35 - 2 Flue Gas Temp. 0 C 141 - 3 Avg. Velocity m/s 14.0 - 4 Avg.flow rate m3/hr. 255475 - 5 Stack Dia. m 3.0 - 6 Particulate Matter (PM) mg/NM3

BDL 150 7 Sulphur Oxides (SOx) ppm BDL 100 8 Nitrogen Oxides (NOx) ppm 32.8 50

Page 187: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/4

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 24 / 12 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/17

Description of Source

: Stack attached to Water Scrubber of Wet Spray Dryer (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C 74 - 3 Avg. Velocity m/s 15.6 - 4 Avg.flow rate m3/hr. 142835 - 5 Stack Dia. m 1.8 - 6 Particulate Matter (PM) mg/NM3

16.7 20

Page 188: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/5

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 24 / 12 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/18

Description of Source

: Stack attached to Bag Filter of RVDF (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Stack

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 35.0 - 2 Flue Gas Temp. 0 C 61 - 3 Avg. Velocity m/s 9.5 - 4 Avg.flow rate m3/hr. 1073 - 5 Stack Dia. m 0.2 - 6 Particulate Matter (PM) mg/NM3

14.9 20

Page 189: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/3

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 19 / 12 / 12 Duration of Sampling (min.)

: 30 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/19

Description of Source

: Stack attached to Thermic Fluid Heater (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : HSD

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 33 - 2 Flue Gas Temp. 0 C 214 - 3 Avg. Velocity m/s 11.6 - 4 Avg.flow rate m3/hr. 8584 - 5 Stack Dia. m 0.6 - 6 Particulate Matter (PM) mg/NM3

61.8 150 7 Sulphur Oxides (SOx) ppm 14.9 100 8 Nitrogen Oxides (NOx) ppm 24.3 50

Page 190: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/6

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 24 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/20

Description of Source

: Stack attached to Alkali Scrubber of-D-14 New EDA Reactor (Mancozeb Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.1 - 4 Hydrogen Sulphide (H2S) mg/NM3

3.5 45 5 Carbon Di-Sulphide (CS2) mg/NM3

87.9 180

Page 191: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/7

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 19 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/21

Description of Source

: Stack attached to Caustic Scrubber of Distillation Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

6.4 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.8 9

Page 192: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/8

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 19 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/22

Description of Source

: Stack attached to Caustic Scrubber of Storage Tank & Drum Filling Section (PCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Storage Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

6.7 20 6 Phosphorus Tri- Chloride

Vapours (PCl3) mg/NM3 0.4 9

Page 193: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/9

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 19 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/23

Description of Source

: Stack attached to Water Scrubber + Alkali Scrubber of Reactor (PCl5 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

0.9 9 5 Hydro Chloride Vapours (HCl) mg/NM3

11.5 20

Page 194: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12TEST REPORT

Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/9

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 19 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/24

Description of Source

: Stack attached to General Scrubber (PCl5 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

0.8 9 5 Hydro Chloride Vapours (HCl) mg/NM3

12.7 20

Page 195: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/10

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 19 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/25

Description of Source

: Stack attached to Caustic Scrubber of Distillation Column (POCl3 Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.2 - 4 Hydro Chloride Vapours (HCl) mg/NM3

5.2 20

Page 196: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/11

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 19 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/26

Description of Source

: Stack attached to Caustic Scrubber WAD 100 (TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.15 - 4 Chlorine (Cl2) mg/NM3

1.0 9 5 Hydro Chloride Vapours (HCl) mg/NM3

4.5 20

Page 197: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/12

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 19 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/27

Description of Source

: Stack attached to Caustic Scrubber HCl Furnace 100(TPD Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C 40 - 3 Stack Dia. m 0.2 - 4 Chlorine (Cl2) mg/NM3

BDL 9 5 Hydro Chloride Vapours (HCl) mg/NM3

11.6 20

Page 198: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/13

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 19 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/28

Description of Source

: Stack attached to Water Scrubber + Ventury Scrubber (C-2102) (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.15 - 4 Hydro Chloride Vapours (HCl) mg/NM3 14.3 20

Page 199: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/14

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per E.P.A / Standard method

Date of Sampling : 19 / 12 / 12 Duration of Sampling (min.)

: 15 min.

Sample Colleted by

: ENPRO Team Lab ID Code : EP/ST/1212/29

Description of Source

: Stack attached to Water Scrubber + Ventury Scrubber (C-2020) (TPPI Plant)

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : As per E.P.A / Standard method

Fuel : Process Scrubber

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 30 - 2 Flue Gas Temp. 0 C Ambient(33) - 3 Stack Dia. m 0.15 - 4 Hydro Chloride Vapours (HCl) mg/NM3 9.8 20

Page 200: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT

Test Report No.: EP/UPL-5/2012/1 Issue Date: 28 / 12 / 12

Customer’s Name & Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch. Description of Sample

: Ground water (Nr.Pieziometricwell)/Grabe

Quantity/No. of Sample : 5 L / 1 No PVC CAN

Sampling By : ENPRO Team Packing/Seal : Sealed Date of Sampling : 19 / 12 / 12 Sample Received Date

: 20 / 12 / 12 Protocol (purpose) : Waste Water Analysis (Monthly Monitoring)

Date of Starting of Test

: 20 / 12 / 12 Date of Completion : 27 / 12 / 12

Sampling Method : IS 3025 Part-1 Sample ID : EP / W / 1212 / 30 Test Method : IS 3025 1987 RA 2003 Type of Sampling : Grab

RESULTS TABLE

Sr. No.  Parameters  Unit  Results BIS Desirable Standard (IS 10500:1991) 

Method Reference 

1.  pH  ‐  7.43  6.5 to 8.5  APHA, 21st  Ed., 2005, 4500 ‐ H+ 

2.  Colour  Hazen  15  5 Max  APHA, 21st  Ed., 2005, 2120 ‐ B 

3.  Suspended Solids  mg/L  44  100  IS 3025, Part 17:1984, RA 2006,Amds.1 

4.  Total Dissolved Solids (TDS)  mg/L  780  500 Max  APHA, 21st  Ed., 2005, 2540 ‐ C 

5.  Biological Oxygen Demand (BOD 3 Days 27oC)  mg/L  22.02  30  IS 3025 Part 44:1993, RA 2003, Eds.1(2000‐10) 

6.  Chemical Oxygen Demand (COD)  mg/L  73.82  100  APHA, 21st  Ed., 2005, 5220 ‐ B 

7.  Oil and Grease  mg/L  0.4  10  APHA, 21st   Ed., 2005, 5520 ‐ B 

8.  Alkalinity Total as CaCO3  mg/L  370  200 Max  IS 3025, Part 23:1986, RA 1998 

9.  Total Hardness as CaCO3  mg/L  340  300 Max  APHA,  21st  Ed., 2005, 2340 ‐ C 

10.  Calcium Hardness as CaCO3  mg/L  130  300 Max  APHA,  21st  Ed., 2005, 2340 – C,2‐37 

11.  Magnesium Hardness as CaCO3  mg/L  210  300 Max  APHA,  21st  Ed., 2005, 2340 – C,2‐37 

12.  Calcium as Ca+2  mg/L 54.4  75 Max  APHA, 21st  Ed., 2005, 3500‐Ca ‐ B 

13.  Magnesium as Mg+2  mg/L 26.1  30 Max  APHA, 21st  Ed., 2005, 3500‐Mg ‐ B 

14.  Iron as Fe  mg/L  0.64 0.3 Max  APHA, 21st  Ed., 2005, 3500‐Fe ‐ B 

15.  Zinc as Zn  mg/L  0.30  5 Max  APHA, 21st  Ed., 2005, 3111 ‐ B 

16.  Chloride as Cl‐  mg/L  44.4  250 Max  APHA, 21st  Ed., 2005, 4500‐Cl ‐ B 

17.  Sulphate as SO4‐2  mg/L  17.9  200 Max  APHA, 21st  Ed., 2005,4500‐ SO4 ‐ E 

18.  Fluoride as F‐  mg/L  0.033  1.0 Max  APHA, 21st  Ed., 2005, 4500‐F ‐ B&D 

19.  Total Phosphate as  P  mg/L  0.26  5 Max  APHA, 21st  Ed., 2005, , 4500‐P,E,4 153 

20.  Silica as SiO2  mg/L  0.52 0.3 Max  APHA, 21st  Ed., 2005, 4500‐SiO2,D,4‐167 

21.  Nitrate as NO3  mg/L  N.D.  45 Max  APHA, 21st  Ed., 2005, 4500‐NO3,B,4‐120 

Remarks:  N.D. – Not Detectable 

ANALYSED BY CHECKED BY

Page 201: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Test Report No.: EP/UPL-5/2012/202-31 Issue Date: 28 / 12 / 12

Customer’s Name & Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch. Description of Sample / Type

: Soil (Near Pieziometric Well) / Grab

Quantity/No. of Sample : 1kg / 1No. Polyethylene Bag

Sampling By : ENPRO Team Packing/Seal : Packing Date of Sampling : 19 / 12 / 12 Sample Received Date

: 20 / 12 / 12 Date of Completion : 26 / 12 / 12

Date of Starting of Test

: 20 / 12 / 12 Sample ID : EP / SW / 1212 / 31

Sampling Method : Laboratory manual for Environmental Quality Testing, EPRF (Environmental Protection Research Foundation)

RESULT TABLE

SR. NO. TEST PARAMETER UNIT RESULTS Method Reference

1. pH (at 270 C) (1:2.5) suspension - 7.34 Laboratory manual for Env. Analysis, EPRF

2. Moisture Content % 6.18 IS 2720, P - II:2002

3. Total Alkalinity as CaCO3 mg/L 15 IS 3025 (Part23) :1986 (RA 1998)

4. Total Hardness as CaCO3 mg/L 370 APHA, 22nd Ed.,2012, 2340-C

5. COD mg/L 13712 IS 3025 (Part58) :2006

6. Organic Carbon % 5.18 Laboratory manual for Env. Analysis

7. Available Phosphorus as P2O5 Kg/ha 3276 Laboratory manual for Env. Analysis

8. Available Calcium as Ca ppm 86.3 Laboratory manual for Env. Analysis

9. Available Magnesium as Mg ppm 22.8 Laboratory manual for Env. Analysis

10. Sulphate (as So4-2) mg/Kg 72.1 IS 2720, P - II : 1977, RA - 1995

11. Chloride (as Cl) mg/Kg 36.6 Methods of Soil Analysis, American Society of Agronomy

12. Copper as Cu mg/Kg 30.2 APHA, 22nd Ed.,2012, 3030D & 3111

13. Iron as Fe mg/Kg 25892 APHA, 22nd Ed.,2012, 3030D & 3112

14. Zinc as Zn mg/Kg 32.9 APHA, 22nd Ed.,2012, 3030D & 3113

15. Nickel as Ni mg/Kg 45.5 APHA, 22nd Ed.,2012, 3030D & 3116

16. Chromium as Cr mg/Kg 28.2 APHA, 22nd Ed.,2012, 3030D & 3119

17. Lead ( as Pb ) mg/Kg 12.8 APHA, 22nd Ed.,2012, 3030D & 3122 ANALYSED BY CHECKED BY

Page 202: United Phosphorus Limited - UPL-LTD · Caustic Scrubber of Storage Tank & Drum Filling Section of PCl3 Plant HCl 20 6.5mg/Nm3 9.8 4.0 PCl 3 9 mg/Nm 3 0.5 0.9 0.2 Water Scrubber +

 

ENPRO Enviro Tech and Engineers Pvt Ltd. Design, Engineering, Environmental Consulting, Monitoring & Testing Service Provider. Manufacturing & Supply of Pollution Control Devices.

Office: 306, Royal Park, Nr. Deepa Complex, Adajan Road, Surat – 395 009, Gujarat, INDIA. Ph. :+91-261-3295244 Fax : +91-261-2786129 E-Mail : [email protected] Web : www.enpro.co.in Factory: Plot no. D/29/16, Hojiwala Industrial Estate, Gate no. 3, Sachin Palsana Road,Sachin, Surat – 324230 Ph. : +91-261-3195244

Branch Offices: Ankleshwar : Shop No. F/2, 1st Floor, Suryadeep Complex, Asian Paint Chowkdi, GIDC Estate, Ankleshwar – 393002 Gandhidham : Office No. 10, 2nd Floor, Madhav Chamber, Plot no. 326, Ward 12B Tagor Rd., Gandhidham, Kutch (M) 93769 84790 ISO 9001:2008 Certified by

Work Order No : 4510063953 Dated: 19 / 04 / 12

TEST REPORT Customer’s Name and Address: United Phosphorus Ltd. (Unit-5) Plot No.-750, P.O Box No.-9, G.I.D.C., Jhagadia - 393110, Dist.-Bharuch.

RESULT TABLE

NOTE: BDL = Below Detectable Limit ANALYSED BY CHECKED BY

ISSUE DATE 28 / 12 / 12

REF. NO. EP/UPL-5/2012/202-32

Description of Sample

: Emission from Stationary Sources. (Stack/Vent)

Sampling Procedure : As per IS method

Date of Sampling : 19 / 12 / 12 Duration of Sampling (min.)

: 30 min.

Sample Collected by

: ENPRO Team Lab ID Code : EP/ST/1212/32

Description of Source

: Stack attached to Boiler-1

Packing/Seal : Seal

Quantity/No. of Sample

: Abs. soln 30ml/Parameter

Protocol (Purpose) : Monthly Monitoring

Test Method : IS:11255 Fuel : Natural Gas

Sr. No. Parameters Unit Result GPCB Limit

1 Stack Height m 45 - 2 Flue Gas Temp. 0 C 212 - 3 Avg. Velocity m/s 10.3 - 4 Avg.flow rate m3/hr. 14388 - 5 Stack Dia. m 1.23 - 6 Particulate Matter (PM) mg/Nm3

BDL 150 7 Sulphur Oxides (SOx) ppm BDL 100 8 Nitrogen Oxides (NOx) ppm 17.4 50


Recommended