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UNIT
III
MANUFACTURING OF ADVANCED
COMPOSITES
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CONTENTSMANUFACTURINGOFCOMPOSITES
Preparation of moulding compounds
Prepregs
Hand lay up methodAutoclave method
Filament winding method
Compression moulding
Reaction Injection moulding
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PREPARATIONOFMOULDINGCOMPOUNDS
High polymer material is mixed with 4 to 10
ingredients each of which discharges a useful
function during moulding or impart some usefulproperty to the finished artifact
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TYPESOFMOULDINGCOMPOUNDING
INGREDIENTS
1.Resin
2.Plasticizer
3.Fillers 4.Lubricants
5.Catalyst Or Accelerators
6.Stabilizers 7.Colouring Materials
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TYPESOFMOULDINGCOMPOUNDINGINGREDIENTS-
1.RESIN
It is a binder which holds different constituents together
Resin in the most specific use of the term is ahydrocarbon secretion of many plants, particularlyconiferous trees.
Resins are valued for their chemical properties andassociated uses, such as the production of varnishes,adhesives and food glazing agents
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1.RESIN
Synthetic resins are viscous liquids that are
capable of hardening permanently.
Otherwise, chemically they are very different from
the various resinous compounds secreted by
plants
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1.RESIN-EXAMPLES
Acrylate Resin
Acrylic
Acrylic Resin
Polyethylene
Phenolic, Phenolic Resin
Phenoplast
Epoxy Glue
Epoxy Resin
Melamine Resin
Polyvinyl Resin
Vinyl Polymer
Vinyl Resin
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1.RESIN
Some are thermosetting plastics in which the term
"resin" is loosely applied to the reactant or product,
or both. "Resin" may be applied to one of two
monomers in a copolymer (the other being called a
"hardener", as in epoxy resins).
For those thermosetting plastics which require only
one monomer, the monomer compound is the
"resin.
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1.RESIN
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TYPESOFMOULDINGCOMPOUNDINGINGREDIENTS
2.PLASTICIZERS
Plasticizers are materials that are added to resinsto increase their plasticity and flexibility
They neutralise the part of the intermolecular forces
of attraction between macromolecules of resins
They impart a greater freedom of movementbetween the polymeric macro molecules of resin
there by increasing the flexibility and plasticity of
the compound material.
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2.PLASTICIZERS
Phthalate esters areplasticizers used in polyvinyl chloride(PVC) to soften the hard PVC by
lubricating the areas between
polymer strands so that it can be
used in consumer products like
inflatable pools and food packaging.
Almost 90% of the market for plasticizer is for PVC, giving this
material improved flexibility and durability.
Plasticizers work by embedding themselves between the chains of
polymers, spacing them apart (increasing the "free volume"), and
thus significantly lowering the glass transition temperature for the
plastic and making it softer.
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2.PLASTICIZERS
Plasticizers evaporate and tend to concentrate in
an enclosed space; the "new car smell" is caused
mostly by plasticizers evaporating from the car
interior.
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3.FILLERS
Fillers are added to give the final plastic better
hardness , tensile strength , finish and workability.
Advantages :
Reduces cost
Reduces shrinkage
Reduces brittleness
Examples :
Carborundum,Quartz,Mica to provide extra hardness
Barium salts to make plastic impervious to X-rays
Addition of asbestos provides heat and corrosion
resistance .
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4.LUBRICANTS
Added to make moulding of plastic easier.
To impart a flawless , glossy finish to the products .
Prevents plastic material from sticking to the
fabricating equipment. Eg: Waxes , Oils , soaps etc
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5.CATALYSTSORACCELERATORS
Are added only in case of thermosetting plastics.
Accelerates the polymerization of fusible resin
during moulding operation into crosslinked infusibleform .
Eg: Hydrogen peroxide
Acetyle sulphuric acidBenzoyl peroxide
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6. STABILIZERS
Improve thermal stability during processing
Eg :
Vinyl chloride
UV light stabilizers are used frequently in plastics,
including cosmetics and films.
The primary function is to protect the substancefrom the long-term degradation effects from light,
most frequently ultraviolet light.
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7.COLOURINGMATERIAL
Used in high polymer artifacts
Eg: Organic dystuffs
Opaque inorganic pigments
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Carbon fiber epoxy
rein prepreg
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PREPREGS
Prepreg is the industry term for high quality
reinforced fibers , which are preimpregnated with aresin system and partially cured to B-stage.
B-stage is an intermediate cure stage of a thermosetting
resin that lies between the completely uncured stageand a completely cured stage.
Ready to mold or cure material in sheet form which
may be tow , tape , cloth or mat impregnated withresin.
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ADVANTAGES
Consistent quality and consistent resin to
reinforcement ratio
Few rejections
Less variance in mechanical properties .
Finest quality material.
Reduce the handling damage to dry fibers. Increased curing pressure reduces voids and
improves fiber wetting
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PREPREGS
A prepreg consists of a reinforcement material
preimpregnated with a resin matrix in controlled
quantities.
The resin is partially cured to a B-stage, and in this
form is supplied to the fabricator, who lays up the
finished part and completes the cure with heat and
pressure.
The required heat and pressure will vary with the
resin system and the intended application.
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PREPREGS
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METHODSOFPRODUCINGPREPREG
1.Solvent Solution Pre-impregnation Process orSolution Coating
2.Hot Melt Pre Impregnation Procedure.
Solution coating saturates the reinforcement with resindissolved in carrier solvent.
Hot melt coating uses heat and pressure to impregnatethe fibers with resin.
The prepreg is typically laid against the paper orpolyethylene film separator called interleaf so that thepreperg dont stick on to itself and is wound around acore.
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1.SOLVENT SOLUTION PRE-IMPREGNATION
PROCESS
Woven fabric or fiber yarn is passed through a resin
rich solution .
Prepreg is then dried to remove the solvent
Excess resin is then removed via doctor blade ormetering rolls
Then the product is staged to the cold stable
prepreg form (B-Stage )
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1.SOLVENT SOLUTION PRE-IMPREGNATION PROCESS
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HOT MELT PREIMPREGNATION PROCEDURE
It replaces solvent method because of
environmental concerns and a need to exert bettercontrol over the amount of resin on the fiber .
Issues with Solvent method :
Stringent Air emission control regulations and liabilities .
High cost of maintaining solution ovens .
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HOT MELT PREIMPREGNATION PROCEDURE
In this process woven fabric or fiber yarn is passed
over a series of rollers .
The molten polymeric resin wets the fibers and then
the resin impregnated sheet of fibers is compacted
over a sheet of release paper and subsequently
wrapped on rolls for storage .
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HOT MELT PREIMPREGNATION PROCEDURE
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HOT MELT PREIMPREGNATION PROCEDURE
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HOT MELT PREIMPREGNATION PROCEDURE
At the hot melting machine , the fibers go through a
metered comb to maintain their parallel integrity for evenspreading , and are laid on a release film containing a
controlled amount of resin .
Another role of release film , either dry or film coated , ispositioned above the fibers.
The fibers sandwiched between the films are pulled along
the tape line with pull rollers as pressure is applied fromsets of heated compaction rolls metered to the prepreg
thickness
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HOT MELT PREIMPREGNATION PROCEDURE
The compaction ensures that the fibers are evenly spreadapart and wet out .
Once through the heated compaction area , the sandwichtypically passes through cooling rolls before the carrierpaper is removed.
Great care is taken to control the temperature
Trimming is done at both sides of the prepreg to exact
width is down just before rewinding
At the end of the tapeline , windup rolls remove one layerof carrier film and reroll it for disposal.
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PREPREGCLASSIFICATION
1.Bleed System
2.No Bleed or Net Resin Content System
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BLEEDSYSTEM
The bleed system Prepregs are those, which
contain excess matrix that is bled off during the
cure cycle by the use ofBLEEDER PILES.
Bleeder piles are the layers of fiber glass cloth or other
highly absorbent material
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NOBLEEDSYSTEM
Curing of prepreg takes place underheat and
pressure
Bleeder piles are generally not required for no
bleeding system
P
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DISADVANTAGESOF PREPREGS
Shelf Life Since the epoxy is in a B-stage, it is required to be
stored either refrigerated or frozen prior to use.
Additionally, the overall shelf life can be low.
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DISADVANTAGESOF PREPREGS
Cost Prohibitive
When manufacturing composites through a process
such as vacuum infusion, the raw fiber and resin are
combined on site.
However, when using prepregs, the raw material mustfirst be prepregged. This is most often done off-site at a
specialized company that focuses on prepregs. This
added step in the manufacturing chain can add
increased cost, and in some instances close to double
the material cost.
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3.HAND LAYUP METHOD
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WET/HANDLAYUPMETHOD
Hand Lay-Up is well suited for low volume
production of product.
This method can be used for both corrosion barrier
and the structural portion.
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WET/HANDLAYUPMETHOD
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WET/HANDLAYUPMETHOD
A mold must be used for hand lay-up parts unless
the composite is to be joined directly to another
structure.
The mold can be as simple as a flat sheet or have
infinite curves and edges.
For some shapes, molds must be joined in
sections so they can be taken apart for part
removal after curing.
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WET/HANDLAYUPMETHOD
Reinforcement fibers can be cut and laid in the
mold.
It is up to the designer to organize the type, amount and
direction of the fibers being used.
Resin must then be catalyzed and added to thefibers.
A brush or roller can be used to impregnate the
fibers with the resin.
The lay-up technician is responsible for controlling theamount of resin and the quality of saturation.
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MATERIALSUSEDFORHANDLAYUP
Resins:
Any, e.g. epoxy, polyester, vinylester,
phenolic.
Fibres:
Any, although heavy aramid fabrics can
be hard to wet-out by hand.
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HAND LAYUPMETHOD ADVANTAGES
Advantages:
i) Widely used for many years.
ii) Simple principles to teach.
iii) Low cost tooling, if room-temperature cure resins
are used.
iv) Wide choice of suppliers and material types.
v) Higher fibre contents, and longer fibers than with
spray lay-up.
Hand Lay Up Method
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Figure 15.4 Hand lay-up : (1) mold is treated with mold release agent; (2) thin gel coat
(resin) is applied, to the outside surface of molding; (3) when gel coat has partially
set, layers of resin and fiber are applied, the fiber is in the form of mat or cloth;
each layer is rolled to impregnate the fiber with resin and remove air; (4) part is
cured; (5) fully hardened part is removed from mold.
Hand Lay-Up Method
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HAND LAY-UP METHOD
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HANDLAYUP METHOD - DISADVANTAGES
Resin mixing, laminate resin contents, and laminate
quality are very Dependent On The Skills of laminators.
Low resin content laminates cannot usually be achieved
without the incorporation of excessive quantities of
voids.
ii) Health and safety considerations of resins. The lower
molecular weights of hand lay-up resins generally
means that they have the potential to be more harmful
than higher molecular weight products. The lowerviscosity of the resins also means that they have an
increased tendency to penetrate clothing etc.
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HANDLAYUP METHOD - DISADVANTAGES
iii) Resins need to be low in viscosity to be
workable by hand. This generally compromises
their mechanical/thermal properties due to the need
for high diluents levels.
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TYPICAL APPLICATIONS
Standard wind-turbine blades
Production boats,
Architectural moldings
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PRODUCTS MADEBY HAND LAY-UP
Generally large in size but low in productionquantity - not economical for high production
Applications:
Boat hulls
Swimming pools Large container tanks
Movie and stage props
Other formed sheets
The largest molding ever made was ship hulls forthe British Royal Navy: 85 m (280 ft) long
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FILAMENTWINDINGPROCESS
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Filament winding is automated processes for
creating parts of simple geometry wherein
continuous resin impregnated fibres are wound
over a rotating male tool called mandrel.
Filament winding process
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FILAMENT WINDING
Resin impregnated continuous fibers are wrapped around arotating mandrel that has the internal shape of the desired
FRP product; the resin is then cured and the mandrel
removed.
The fiber rovings are pulled through a resin bathimmediately before being wound in a helical pattern onto
the mandrel.
The operation is repeated to form additional layers, each
having a criss-cross pattern with the previous, until thedesired part thickness has been obtained.
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Figure 15.8 Filament winding.
Filament Winding
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FILAMENTWINDINGPROCESS
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TYPESOF FILAMENTWINDINGPROCESS
(i) The Polar Or Planer Method
(ii) The High Helical Pattern Winding.
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THEPOLARORPLANERMETHOD
A winding in which the filament path passes tangentto the polar opening at one end of the chamber andtangent to the opposite side of the polar opening atthe other end.
The polar or planer method of winding utilizes afixed mandrel and a shuttle that revolves aroundthe longitudinal axis of the part to form longitudinalwinding patterns.
This type of winding is used if the longitudinal fibresare required with angle less than 25 to the mandrelaxis.
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THEPOLARORPLANERMETHOD
HELICAL WINDING PROCESS
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HELICALWINDING PROCESS
A winding in which the filament or band advances
along a helical path, not necessarily at a constant
angle except in the case of a cylindrical article.Inthe high helical pattern winding, the mandrel rotates
while the shuttle transverses back and forth. Both
the mandrel rotation and shuttle movement are in
the horizontal plane. By controlling the mandrel
rotation and shuttle speed, the fibre angle can be
controlled.
.
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HELICALWINDINGPROCESS
Angles of 25-85 to the mandrel rotation axis are
possible
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HELICALWINDINGPROCESS
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HELICALWINDINGPROCESS
After completion of the winding, the filament wound
structure is cured at room temperature or in an
oven.
The mandrel is removed after the curing. The
mandrel, which determines accurate internal
geometry for the component, is generally the only
major tool.
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FILAMENTWINDINGPROCESS
Low cost mandrel materials such as cardboard orwood can be used for winding low cost routine
parts. For critical parts requiring close tolerances,
expensive mandrels designed for long term use
may be required.
For high temperature cure 315C (600F), graphite
mandrels with low thermal expansion may be
advantageous. However, attention should be paidfor potential difficulties for mandrel removal.
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TYPESOFMANDRELS
Mandrels are eitherREMOVABLE or NON-REMOVABLE.
Removable mandrels are classified according to
the removal techniques as:
Entirely removed.
Collapsible.
Breakable or soluble.
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THESELECTIONOFMANDREL
1. Part size and complexity
2. Size of openings
3. Resin system and its curing
4. The number of components to be
fabricated.
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THEREQUIREMENTSFORAMANDREL
It must be stiff and strong enough to support
its own weight and the weight of the applied
composite while resisting the fibre tension
pressure from winding and curing.
It must be dimensionally stable and should
have thermal coefficient of expansion greater
than the transverse coefficient of thecomposite structure.
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MATERIALSUSEDFORCONSTRUCTIONOF
MANDREL.
Low melting temperature alloys used for smalldiameter applications.
Sand, soluble plaster and eutectic salts used for
irregular shapes.
Inflatable material used in applications where
sometimes the mandrel remains a part of the structure.
Segmented metal used for high production rates, and
where the mandrel can be withdrawn through a small
hole in the part.
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This process utilises large tonnage presses whereinthe part is cured between two matched steel dies
under pressure and high temperature. The moving
platen is heated either by steam or electricity to
promote thermal curing.
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Curing of the part is affected by the followingfactors:
Size of platen, which determines the length and width of
the part, which can be cured.
Total tonnage of the press, which determines the
pressure to be exerted on the projected surface area of
the part.
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After placing the laminate to be cured called the'charge' in the core of the mold, the cavity is then
closed at a rate of usually 4-12 mm/sec.
In most cases the mold is heated to 150C (302F),which causes the charge viscosity to be reduced.
With increasing mold pressure as the mold is
closed, the charge flows towards the cavityextremities, forcing air out of the cavity.
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The molding pressure based on projected part arearanges from 0.7 to 9 MPa (100 to 1200 psi).
Higher molding pressure causes sink marks, while
lower pressure cause scumming of the mold andporosity.
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The curing time is usually between 25sec to 3 minutes depending on several
factors including
resin-initiator-inhibitor reactivity
part thickness
component complexity
mold temperature.
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ADVANTAGEOFTHECOMPRESSIONMOLDING
The primary advantage of the compression moldingis its ability of producing large number of parts with
little dimensional variations
A wide variety of shapes, sizes and complexity can
be produced by compression molding.
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DRAWBACKS
High tooling cost
Need for large heated presses.
Thus, this method is not practical for low volume
production.
TYPES OF COMPRESSION MOULDING
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TYPES OF COMPRESSION MOULDING
PROCESSES
1.Sheet Moulding Compound. (SMC)
2.Bulk Moulding Compound. (BMC)
3.Wet system Compression Moulding.
4.Reinforced Thermoplastic Sheet Compression
Moulding.
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Sheet moulding compound (SMC) or sheet
moulding composite is a ready to mould fibre-
reinforced polyester material primarily used in
compression moulding.
The sheet is provided in rolls weighing up to
1000 kg.
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SHEET MOULDING COMPOUND(SMC)
It refers to both material and process for producingglass fiber reinforced polyester resin items .
SMC is a totally integrated compound in sheet form
that incorporates all reinforcements resin , chemicalthickness , fillers , mould release agents and other
ingredients .
Also includes pigments and shrink control agents
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SHEET MOULDING COMPOUND(SMC
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SHEET MOULDING COMPOUND(SMC
A SMC processing machine produces molding
compound in sheet form.
The glass fibre is added to a resin mixture that is
carried onto a plastic carrier film.
After partial cure, the carrier films are removed.
The sheet molding material is cut into lengths and
placed onto matched metal dies under heat and
pressure
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SHEET MOULDING COMPOUND(SMC
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ADVANTAGESOF SMC MOLDINGPROCESS
High volume production.
Excellent part reproducibility.
Minimum material scrap.
Excellent design flexibility.
Parts consolidation.
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BMC is a combination of chopped glass strands and Resin
in the form of a bulk pre-preg.
BMC is suitable for either compression or injection
molding.
Injection molding of BMC is used to produce complex
components such as electrical equipment, car
components, housings for electrical appliances and tools,
in large industrial volumes.
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BULKMOULDINGCOMPOUND
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Unlike SMC, it is not necessary to include amaturation stage. Consequently, BMC pre-preg
formulations contain higher filler contents.
The chopped glass strands vary in lengthdepending on the level of performance required.
Reinforcement content generally ranges between
15 and 20 percent; however, it may reach 25
percent for the highest performance. BMC uses a lower reinforcement content than SMC
and permits higher filler loadings with lower costs.
BULKMOULDINGCOMPOUND
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APPLICATIONSOFBULKMOLDINGCOMPOUND
Pump housing
A/C components
Circuit Breakers
Computer components
Power Tools
Gear cases
Electrical insulators
WETSYSTEMCOMPRESSIONMOULDING
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Matrix ( Liquid Resin ) is pumped to dryreinforcement in press mounted and heated
matched metal moulds
Hydraulic pressure forces the liquid resin to flowthrough the reinforcement and hold the material in
place until cure is completed at the cure
temperature of 120C to 180C
WETSYSTEMCOMPRESSIONMOULDING
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The equipment used for WCM is same as the BMC.
Matrix material is thermosetting polyester vinylester
and epoxy , resins filled with inert materials such as
clay , calcium carbonate and alumina , catalyst andpigment to form a complete liquid system which
require only the addition of heat for curing
Reinforcement is chopped strand mats andcontinuous strand mats
REINFORCED THERMOPLASTIC SHEET
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REINFORCEDTHERMOPLASTICSHEET
COMPRESSIONMOULDING
Utilizes precombined sheet of thermoplastic resinand glass fiber reinforcement
These sheets are cut into blanks which are
preheated to a specified temperature and loded into
matched metal compression mould. Under pressure , heat softened blanks flow and fill
the mould.
The mould is maintained at a temperature which
causes the sheet to solidify and allows demouldingof the part
REINFORCED THERMOPLASTIC SHEET
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Matrix :
Thermoplastic Resin , Polypropylene ,
thermoplastic polyester , polycarbonate and
nylon.
Reinfrocement :
Continous glass fiber mats
REINFORCEDTHERMOPLASTICSHEET
COMPRESSIONMOULDING
REINFORCEDTHERMOPLASTICSHEET
COMPRESSION MOULDING
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ADVANTAGES
Maximum design flexibility
Low capital cost
Tooling cost is low
Minimum material scrap
High volume production
COMPRESSIONMOULDING
REINFORCED THERMOPLASTIC SHEET
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DISADVANTAGES
DISADVANTAGES
Operater skill dependent
Lower impact resistance
Only one molded surface is obtained
Longer curig times required
REINFORCEDTHERMOPLASTICSHEET
COMPRESSIONMOULDING
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APLICATION
Helmets
Automotive bumper
Radiator supports
Battery trays
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INJECTIONMOULDING
INJECTION MOULDING
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Injection molding is a manufacturing process forproducing parts from both thermoplastic and
thermosettingplastic materials.
INJECTIONMOULDING
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Material is fed into a heated barrel,
mixed, and forced into a mold cavitywhere it cools and hardens to theconfiguration of the cavity.
INJECTIONMOULDING
INJECTION MOULDING
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INJECTIONMOULDING
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CLAMPING - the moving and
fixed platens of the injection
moulding machine holds the
mould tool together under
pressure.
INJECTION - the molten plastic
that has been melted from pellet
form in the barrel of the moulding
machine is injected under
pressure into the mould.
DWELLING - after the molten
plastic has been injected into the
mould pressure is applied toensure all cavities are filled.
COOLING - the plastic parts are
then allowed to solidify in the
mould.
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OPENING - the moving platen moves away from the fixed platen separating
the mould tool.
EJECTION - rods, a plate or air blast then aids ejection of the completed
plastic moulding from the injection mould tool.
The length of time from closing the mould to ejecting the finished plastic
moulding is the cycle
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PROCESS CHARACTERISTICS
Utilizes a ram or screw-type plunger to force molten
plastic material into a mold cavity .
Produces a solid or open-ended shape that hasconformed to the contour of the mold.
It is ideal for producing high volumes of the same
object
I
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wire spools, packaging, bottle caps, automotive dashboards,
pocket combs,
, one-piece chairs and small tables,
storage containers,
mechanical parts (including gears),
and most other plastic products available today.
Injection molding is the most common method of
part manufacturing..[4].
INJECTIONMOULDING
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ADVANTAGESOFINJECTIONMOLDING
high production rates
repeatable high tolerances
the ability to use a wide range of materials
low labor cost
minimal scrap losses
little need to finish parts after molding
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DISADVANTAGES
expensive equipment investment
potentially high running costs
the need to design moldable parts.
REACTIONINJECTIONMOLDING
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It is similar to injection moulding except thermosetting
polymers which requires a curing reaction to occur
within the mold.
The RIM Process involves a chemical reaction between
the two liquid components. Initially, the liquids are held
in separate, temperature-controlled feed tanks. The
chemicals are fed through supply lines to metering units
that precisely meter both chemicals, at high pressure, to
a mixhead device.
Reaction injection molding
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RIM parts are created through a process thatbegins when two liquid reactants - an Isocyanate
component and a Polyol resin mixture - are held in
separate tanks at an elevated temperature with
agitators.
These liquids are fed through supply lines at high
pressure to the mixhead.
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When the injection begins, valves open in themixhead and the liquids enter a chamber in the
mixhead at high pressures (usually between 1,500
and 3,000 psi) and high speeds.
Here they are mixed by high-velocityimpingement.
From the mix chamber, the mixed liquid flows into
the mold at atmospheric pressure and undergoes
an exothermic chemical reaction, forming a polymerin the mold.
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Reaction time is usually expressed in seconds. Forextremely large parts the reaction time can be
extended to allow for proper filling of the mold.
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ADVANTAGES
strong, flexible, lightweight parts which can easilybe painted.
The bi-component mixture injected into the mold
has a much lower viscosity than moltenthermoplastic polymers, therefore large, light-
weight, and thin-walled items can be successfully
RIM processed.
This thinner mixture also requires less clamping
forces, which leads to smaller equipment and
ultimately lowercapital expenditures.
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The disadvantages are slow cycle times, comparedto injection molding, and expensive raw materials.