+ All Categories
Home > Documents > WEBSTER STREET BRIDGE PID 90794 DAYTON, OHIO

WEBSTER STREET BRIDGE PID 90794 DAYTON, OHIO

Date post: 25-Oct-2021
Category:
Upload: others
View: 2 times
Download: 0 times
Share this document with a friend
148
Planning, Engineering, Construction Management, Technology 6350 Presidential Gateway Columbus, Ohio 43231 P 614-823-4949 F 614-823-4990 WEBSTER STREET BRIDGE PID 90794 DAYTON, OHIO Phase II Environmental Site Assessment Prepared For: Evans, Mechwart, Hambleton, and Tilton, Inc. 5500 New Albany Road Columbus, Ohio 43054 Prepared By: Resource International, Inc. 6350 Presidential Gateway Columbus, Ohio 43231 Rii Project No. W-11-138 May 2014
Transcript

Planning, Engineering, Construction Management, Technology

6350 Presidential Gateway Columbus, Ohio 43231

P 614-823-4949 F 614-823-4990

WEBSTER STREET BRIDGE

PID 90794

DAYTON, OHIO

Phase II Environmental

Site Assessment

Prepared For:

Evans, Mechwart, Hambleton, and Tilton, Inc.

5500 New Albany Road

Columbus, Ohio 43054

Prepared By:

Resource International, Inc.

6350 Presidential Gateway

Columbus, Ohio 43231

Rii Project No. W-11-138

May 2014

RESOURCE INTERNATIONAL, INC.

Columbus Office

6350 Presidential Gateway

Columbus, Ohio 43231

Phone: 614.823.4949

Fax: 614.823.4990

Columbus, Cleveland, Cincinnati, Newark, Ohio Indianapolis, Indiana Pittsburgh, Pennsylvania

May 7, 2014 Mr. Chris Selvaggio EMH&T 5500 New Albany Road Columbus, Ohio 43054

Re: Phase II Environmental Site Assessment (ESA) Webster Street Bridge PID 90794

Dayton, Ohio Rii Project #W-11-138

Dear Mr. Selvaggio Resource International, Inc. (Rii) is submitting this Phase II Environmental Site Assessment (ESA) report for the Webster Street Bridge located in Dayton, Ohio. We sincerely appreciate this opportunity to provide our environmental services. If you have any questions concerning this report, please do not hesitate to contact us at 614-823-4949. Sincerely, RESOURCE INTERNATIONAL, INC.

Steve Sawyer Environmental Specialist

Michelle L. Eckels, CPG, LEED Green Assoc. Director – Environmental Services Enclosure: Phase II ESA Report

Planning

Engineering

Construction

Management

Technology

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants i

TABLE OF CONTENTS

EXECUTIVE SUMMARY ........................................................................................................... 1

1.0 INTRODUCTION .......................................................................................................... 2

1.1 GENERAL ................................................................................................................................ 2 1.2 PROJECT SUMMARY .................................................................................................................. 2

2.0 SUBSURFACE SAMPLING FIELD PROCEDURES .............................................................. 4

2.1 HAND AUGER SAMPLING ........................................................................................................... 4 2.2 SOIL BORINGS.......................................................................................................................... 4

3.0 SAMPLE AND CHEMICAL ANALYSIS ............................................................................. 7

3.1 SOIL ...................................................................................................................................... 7 3.2 GROUNDWATER ....................................................................................................................... 7

4.0 SUBSURFACE PROFILE................................................................................................. 9

5.0 ANALYTICAL RESULTS ............................................................................................... 11

6.0 CONCLUSIONS AND RECOMMENDATIONS ................................................................ 12

6.1 CONCLUSIONS ....................................................................................................................... 12 6.2 RECOMMENDATIONS .............................................................................................................. 13

7.0 RELIABILITY OF REPORT - DISCLAIMER ...................................................................... 14

8.0 SIGNATURE OF ENVIRONMENTAL PROFESSIONAL(S) ................................................ 15

TABLES

TABLE 1 SOIL ANALYTICAL RESULTS

TABLE 2 GROUNDWATER ANALYTICAL RESULTS

LIST OF APPENDICES

APPENDIX I SITE MAP APPENDIX II BORING LOCATIONS APPENDIX III BORING LOGS APPENDIX IV ANALYTICAL RESULTS AND CHAIN OF CUSTODY

APPENDIX V PHOTOGRAPHS

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

1

EXECUTIVE SUMMARY Resource International, Inc. (Rii) was retained by Evans, Mechwart, Hambleton, and Tilton, Inc. (EMH&T) to conduct a Phase II Environmental Site Assessment (ESA) of the Webster Street Bridge over Mad River located in Dayton, Montgomery County, Ohio, in accordance with the scope provided by the Ohio Department of Transportation (ODOT). The following is a summary of the findings and recommendations. Rii obtained soil samples from eight (8) soil borings and groundwater samples from two (2) monitoring wells, and provided the samples to an independent laboratory for analyses. The groundwater samples (MW-1 and MW-2) were obtained from Borings SB-8 and SB-7, respectively. The soil sample results were compared to the BUSTR Soil Re-Use Action Levels in accordance with OAC 1301: 7-9-13 and Ohio EPA Voluntary Action Plan (VAP) for Construction and Excavation Direct Contact standards, in accordance with OAC 3745-300-08. The groundwater sample results were compared to the BUSTR Groundwater Ingestion Action Levels in accordance with OAC 1301: 7-9-13 and the Ohio EPA VAP Generic Unrestricted Potable Water Use standards, in accordance with OAC 3745-300-08. See Appendix IV for the complete laboratory analysis results.

Volatile Organic Compounds (VOCs)

o Soil - Trace levels of naphthalene and xylenes were detected in the soils of SB-1; however, the levels did not exceed Ohio EPA Voluntary Action Plan (VAP) for Construction and Excavation or the BUSTR Soil Re-Use Action Levels. No levels of VOCs were detected in the other seven (7) borings.

o Groundwater - Trace levels of naphthalene and xylenes were detected in the soils of SB-1. Trace levels of n-propylbenzene, isopropylbenzene, and sec-butylbenzene were detected in the groundwater of MW-1 and MW-2; however, the levels did not exceed the VAP Generic Unrestricted Potable Water standards or BUSTR Groundwater Ingestion Action Levels.

Semi-Volatile Organic Compounds (SVOCs)

o Soil - Small detections of SVOCs were identified in SB-1, SB-2, SB-3, SB-7 and SB-8. The low levels of SVOCs included: benzo (a) anthracene, benzo (k) fluoranthene, benzo (a) pyrene, benzo (b) fluoranthene, chrysene, fluoranthene, naphthalene, phenanthrene, and pyrene. The detected levels did not exceed the Voluntary Action Plan (VAP) for Construction and Excavation Direct Contact standards or the BUSTR Soil Re-Use Action Levels.

o Groundwater - No levels of SVOCs were detected in the two (2) groundwater samples.

8 RCRA Metals

o Soil - Low levels of barium, chromium, lead, mercury, arsenic, and cadmium were detected in SB-1, SB-2, SB-3, SB-4, SB-5, SB-6, SB-7, and SB-8; however, the levels did not exceed the VAP for Construction and Excavation or the BUSTR Soil Re-Use Action Levels. The lead levels in SB-7 and SB-8, from 503 mg/kg (4 to 8 feet) and 352 mg/kg (0 to 4 feet), respectively, were above typical Ohio background levels. The remaining detected levels of metals within the soil samples were consistent with industrial land use.

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

2

o Groundwater - Trace levels of barium were detected in both groundwater samples, but were below Ohio EPA Voluntary Action Plan (VAP) for Generic Unrestricted Potable Water standards and BUSTR Groundwater Ingestion Action Levels.

Based on the above identified findings, the following is a summary of our recommendations:

Site 13 and Mad River Sediment - Based on the findings, Rii does not recommend any additional environmental investigation of the Site 13 and Mad River sediment. Due to the area’s historical industrial land use, if soils in the project area are to be excavated, stockpiled, and/or removed from the site, plan notes should be prepared detailing the additional testing that should be conducted to characterize the soil for proper landfill disposal (construction/demolition landfill, solid waste landfill, or hazardous waste landfill).

Site 14 - Based on the findings of the visible fill material and petroliferous odors from sample locations SB-7 and SB-8, and high lead levels, Rii recommends any excavated materials be stockpiled, and/or removed from the site, plan notes should be prepared detailing the additional testing that should be conducted to characterize the soil for proper landfill disposal (construction/demolition landfill, solid waste landfill, or hazardous waste landfill). Rii does not recommend any additional environmental investigation for Site 14.

The entire report should be read to obtain a full understanding of the information provided, in order to make an informed business decision about the property.

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

2

1.0 INTRODUCTION

1.1 General Pursuant to the agreement with Evans, Mechwart, Hambleton, and Tilton, Inc. (EMH&T) (“the user”), Resource International, Inc. (Rii) was retained to perform a Phase II Environmental Site Assessment (ESA) for the Webster Street Bridge (PID 90794) roadway project located in Dayton, Ohio in accordance with the scope provided by the Ohio Department of Transportation (ODOT). Refer to the Site Location Map in Appendix I. The purpose of the Phase II ESA was to identify the presence of soil and/or groundwater contamination within the project area.

The Phase II ESA was conducted in general conformance with the American Society of Testing Materials (ASTM), Standard Guide for Environmental Site Assessments: Phase II Environmental Site Assessment Process, E1903-11 and the ODOT Environmental Site Assessment Guidelines.

1.2 Project Summary The purpose of the Webster Street Bridge project (PID 90794) is to correct the structural deficiency of the Webster Street Bridge over the Mad River, improve the geometrics and functionality of the bridge, and increase the capacity of the Webster Street corridor to accommodate anticipated future traffic loads. EMH&T conducted a Phase I ESA in September 2013. Based on the information obtained from the previous Phase I ESA, recognized environmental conditions were associated with six (6) of the eleven (11) properties located within the project area. The project area is situated within a former industrial location. The Ohio Department of Transportation (ODOT), Office of Environmental Services reviewed the Phase I ESA and recommended further environmental investigation. A Phase II ESA was recommended for Site 13, Miami Conservancy District Levee; Site 14, Webster Street, LLC; and Miami River sediments. Site specific recommendations are listed below; boring locations are shown in Appendix II.

Property No. 13, Miami Conservancy District Levee – Two (2) near surface samples analyzed for Volatile Organic Compounds (VOCs) by 8260, semi-VOCs by 8270, total Resource Conservation and Recovery Act (RCRA) metals and Total Petroleum Hydrocarbons (TPH) – Gasoline Range Organics, Diesel Range Organics, and Oil Range Organics (GRO/DRO/ORO).

Property No. 14, Webster Street LLC – Two (2) soil borings to a depth of 20 feet each boring converted to temporary groundwater wells. One (1) sample from each boring analyzed for VOCs by 8260, semi-VOCs by 8270, total RCRA metals and

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

3

TPH GRO/DRO/ORO. Groundwater analyzed for VOCs by 8260, semi-VOCs by 8270, and total RCRA metals (filtered).

Miami River sediments – Four (4) sediment samples collected and analyzed for VOCs by 8260, semi-VOCs by 8270, total RCRA metals, and TPH GRO/DRO/ORO.

The Phase I ESA concluded or reasonably implied that further environmental investigation was warranted for the subject property.

1.3 Phase I ESA Summary EMH&T completed a Phase I ESA report in September 2013. The following is a brief summary of the site findings associated with the two (2) property locations identified by ODOT above as recommending further environmental investigation. Site 13, a grassy embankment, is adjacent to the northern bank of the Mad River. The property is owned by the Miami Conservancy District. There does not appear to have been historical development with any permanent structures. The proposed activities for this property are to include moving of the existing sidewalk, bike path, and installation of a storm sewer and inlets. The proposed depth of excavation for these activities is approximately 2 feet for sidewalk and bike path, approximately 2 to 15 feet for storm sewer and inlets, and approximately 2 to 3 feet for pavement. Site 14 is a mowed grassy parcel located at the southeast corner of Webster Street and State Route 4 Exit 54C/Detrick Street. The property is owned by Webster Street LLC. There is no documented contamination on the property; however review of previous reports suggests the potential presence of undocumented fill materials. There is an environmental concern associated with the disposal of undocumented fill material. The proposed activities for this property are to include replacement and moving of the existing sidewalk and bike path, the installation of a storm sewer and inlets, and pavement replacement and expansion. The proposed depth of excavation for these activities is approximately 2 feet for sidewalk and bike path, approximately 4 to 15 feet for storm sewer and inlets, and approximately 2 to 3 feet for pavement.

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

4

2.0 SUBSURFACE SAMPLING FIELD PROCEDURES On April 17, 2014, Rii conducted sampling at eight (8) boring locations within the project area. The boring locations were determined by ODOT and provided to Rii to field locate. Refer to the boring plan provided in Appendix II. Rii contracted with EnviroCore Limited to provide the Geoprobe sampling rig. Rii characterized the soil types, screened samples, containerized the soil and groundwater samples, and transported the samples to the independent laboratory. The following is a summary of the sampling procedures: A total of eight (8) soil sample locations were completed within the project area, identified on the boring plan provided in Appendix II as SB-1 through SB-8. Borings SB-1 through SB-6 were sampled to shallow depths due to the requested shallow depth of the sampling and the restrictive access under the bridge and within the Mad River. Borings SB-7 and SB-8 were drilled to a maximum depth of 22 feet. SB-1 and SB-2 were sampled within the Mad River in proximity to the proposed new bridge pier locations. SB-3 and SB-4 were sampled along the north side of the Mad River floodplain at the proposed pier location. SB-5 through SB-6 were sampled on the north embankment of the Mad River for Site 13. SB-7 and SB-8 were drilled adjacent to Webster Street within Site 14. Temporary wells were installed in borings SB-7 and SB-8 for obtaining groundwater samples. The following is a summary of the field procedures.

2.1 Hand Auger Sampling A standard clean hand auger was utilized in collecting samples from locations SB-1 through SB-6 which were located under the bridge. Rii removed sediment using the auger and placed sediment on clean poly sheeting. Sediment was examined, characterized, and placed in a container. The Mad River samples, SB-1 and SB-2 were able to be completed to a depth of 1.0 foot before encountering refusal on cobbles. The samples SB-3 through SB-6 were able to be completed to depths between 2.0 and 2.6 feet, before encountering refusal on rock and/or concrete.

2.2 Soil Borings 1. Two (2) soil borings, SB-7 and SB-8, were sampled continuously to a depth of 22

and 20 feet, respectively. A Geoprobe® Model 6620DT, using the direct-push method of sampling, was utilized to advance a 48-inch long by 2-inch diameter soil sampler. Soil samples were retained at continuous 4-foot intervals. A new sample tube was dedicated for each continuous soil sample to minimize cross-contamination of samples and eliminate the need for decontamination of sample tubes.

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

5

2. Soil samples collected were vertically split into two (2) representative portions. Each portion was visually inspected by the field geologist and analyzed in the field using a photoionization detector (PID) to determine the presence of volatile organic compounds. One portion was placed in an analytical jar provided and prepared by the environmental laboratory for potential analyses. The other portion was used to fill a sealable plastic bag with ample air space to accumulate vapors. The plastic bags were placed in a warm environment for approximately fifteen (15) minutes. The PID was then inserted through the seal and the maximum meter response was recorded as the headspace reading.

3. Samples obtained from each boring were handled wearing disposable latex gloves

to minimize cross-contamination of samples. Immediately upon collection, samples to be analyzed were stored in air-tight, screw type glass jars with Teflon lids and preserved on ice in coolers.

4. Each glass jar was labeled with the project number, site number, boring number,

sample number, and depth at which the sample was retained. 5. All non-dedicated sampling equipment was steam cleaned before probing as a

means of decontamination. The probe (cutting shoe) was decontaminated after each use with a non-phosphate detergent (Alconox) and potable wash water, and rinsed with distilled water.

6. Samples selected for further laboratory analysis were placed in an ice filled cooler

for storage. The samples were transported to Advanced Analytics Laboratories, Inc. accompanied by a chain-of-custody. A copy of the laboratory analytical results and chain-of-custody are provided in Appendix IV. The samples were transported in such a way as to keep the samples as undisturbed as possible.

7. Since the Geoprobe utilizes the direct push method, no soil cuttings were generated

during sampling. Upon completion, the borings were filled with bentonite pellets. 8. Groundwater samples were collected from SB-7 and SB-8 by the installation of a 1-

inch PVC temporary monitoring well with a 5.0-foot screen. A peristaltic pump was used to collect the groundwater into the proper containers. Water samples were “in-line” filtered in the field at the time of collection using a Geotech dispos-a-filter with a 0.45 micron filter. A new packaged filter and tubing were utilized for each groundwater sample. Once the water sample was collected, the 1-inch PVC temporary monitoring well was removed and the boring was sealed utilizing bentonite chips.

The field geologist, Steve Sawyer, maintained field logs documenting the interpretive soil description, sample depths, field screening levels, and sample selected for analyses, in accordance with ASTM D 5434, Standard Guide for Field Logging of Subsurface

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

6

Explorations of Soil and Rock. Visual examination of all collected samples was performed in accordance with ASTM D 2488, Standard Practice for Description and Identification of Soil (Visual-Manual Procedure). Refer to Appendix III for the Boring Logs.

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

7

3.0 SAMPLE AND CHEMICAL ANALYSIS

3.1 Soil A Mini-Rae 3000 Photoionization detector (PID) was used to obtain field readings and headspace screening of the soil samples. The screenings provide a qualitative indication of VOCs in the soil. The PID was calibrated with isobutylene prior to commencement of the fieldwork. The criteria for selecting the soil samples that were submitted for chemical analyses from each boring were as follows:

1. The sample exhibiting the highest headspace reading. 2. If the readings were not significant, the sample exhibiting visual or odorous

contamination. 3. If no visual or odorous contamination was present, the sample at the bottom of

the boring. 4. The discretion of the field geologist.

One (1) soil sample from each of borings SB-1 through SB-6 was selected for laboratory analysis and two (2) samples each from SB-7 and SB-8 were selected for laboratory based on locations. The selected soil samples were analyzed for the following:

1. Volatile Organic Compounds (VOC) EPA Method 8260C 2. Semi-Volatile Organic Compounds (SVOC) EPA Method 8270 3. Eight (8) RCRA Metals EPA Method 6010C 4. Total Petroleum Hydrocarbons (TPHs) EPA Method 8015

Advanced Analytics Laboratories, Inc., located at 1025 Concord Avenue, Columbus, Ohio 43212 conducted the laboratory analyses of the soil samples. The applicable EPA Analytical Method Numbers are referenced from the United States EPA Document SW-846, Test Methods for Evaluating Solid Wastes.

3.2 Groundwater Borings SB-7 and SB-8 were converted to temporary monitoring wells labeled MW-2 and MW-1, respectively. Monitoring wells were installed with 5 feet of slotted screen within the saturated zone. Water samples were “in-line” filtered, and no restrictions were observed. One (1) groundwater sample from each monitoring well was selected for laboratory analysis based on locations. The selected groundwater samples were analyzed for the following:

1. Volatile Organic Compounds (VOC) EPA Method 8260C

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

8

2. Semi-Volatile Organic Compounds (SVOC) EPA Method 8270 3. Eight (8) RCRA Metals EPA Method 6010C

Advanced Analytics Laboratories, Inc., located at 1025 Concord Avenue, Columbus, Ohio 43212 conducted the laboratory analyses of the soil samples. The applicable EPA Analytical Method Numbers are referenced from the United States EPA Document SW-846, Test Methods for Evaluating Solid Wastes.

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

9

4.0 SUBSURFACE PROFILE

Soil borings SB-1 through SB-8 were sampled below the ground surface and/or Mad River water level. The following information describes the subsurface material that was encountered in the drilling or hand auguring process of each boring. Refer to the boring location plan provided in Appendix II. Soil Boring SB-1 (Mad River Sediment Sample) Boring SB-1 was sampled in the Mad River to a depth of 1 foot; soil within the boring was gray, poorly graded sand with gravel. Auger refusal occurred at 1 foot due to cobbles. Soil Boring SB-2 (Mad River Sediment Sample) Boring SB-2 was sampled in the Mad River to a depth of 1 foot; soil within the boring was gray, poorly graded sand and gravel. Auger refusal occurred at 1 foot due to cobbles. Soil Boring SB-3 (Mad River Sediment Sample) Boring SB-3 was sampled at the surface to a depth of 2 feet; soil within the boring was gray, poorly graded sand and gravel. Auger refusal occurred at 2 feet due to cobbles. Soil Boring SB-4 (Mad River Sediment Sample) Boring SB-4 was sampled at the surface to a depth of 2.6 feet; soil within the boring was gray, poorly graded sand and gravel with glass fragments present throughout. Auger refusal occurred at 2.6 feet due to cobbles. Soil Boring SB-5 (Site 13 Miami Conservancy District Levee Sample) Boring SB-5 was sampled at the surface to a depth of 2.0 feet; soil within the boring was brown and gray, poorly graded sand with gravel with shells and cobbles present throughout. Auger refusal occurred at 2.0 feet due to concrete. Soil Boring SB-6 (Site 13 Miami Conservancy District Levee Sample) Boring SB-6 was sampled at the surface to a depth of 2.4 feet; soil within the boring was gray, poorly graded sand and gravel with glass fragments and cobbles present throughout. Auger refusal occurred at 2.4 feet due to cobbles. Soil Boring SB-7 (Site 14, Webster Street, LLC Sample) Boring SB-7 was sampled below 6 inches of topsoil to a depth of 22 feet bgs. Soil within the boring consisted of black to tan and brown cinders and gravel transitioning to black to brown lean clay at approximately 8 feet. At approximately 13 feet the soil changed to gray poorly graded sand with gravel with petroleum odors present from 16 to 20 feet. Groundwater was initially encountered at 17 feet. A 1-inch temporary monitoring well was installed to a depth of 22 feet with a 5-foot screen in order to collect a groundwater sample. The temporary monitoring well was removed and the boring was grouted with bentonite after ground water samples were collected.

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

10

Soil Boring SB-8 (Site 14, Webster Street, LLC Sample) Boring SB-8 was sampled below 3 inches of topsoil to a depth of 20 feet bgs. Soil within the boring consisted of black cinders to 1.7 feet, with brown lean clay with gravel separating another layer of black cinders starting at 4.4 feet. At 8.0 feet the soil transitioned to brown and red lean clay before changing to gray, well graded sand at 10.9 feet. Poorly graded gray gravel separated the brown poorly graded sand at the bottom of the boring. Groundwater was initially encountered at 17 feet. A 1-inch temporary monitoring well was installed to a depth of 20 feet with a 5 foot screen in order to collect a groundwater sample. The temporary monitoring well was removed and the boring was grouted with bentonite after ground water samples were collected. Definitions of the soil terms used in this report are presented in Appendix III. A complete description of subsurface materials encountered in each boring can be found on the borings logs provided in Appendix III.

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

11

5.0 ANALYTICAL RESULTS The selected soil and groundwater samples were sent to Advanced Analytics Laboratories for analyses. The soil sample results were compared to the BUSTR Re-Use Action Levels

in accordance with OAC 1301: 7-9-13 and Ohio EPA Voluntary Action Plan (VAP) for Construction and Excavation Direct Contact standards, in accordance with OAC 3745-300-

08. No levels of VOCs, SVOCs, 8 RCRA Metals or TPHs exceeded the BUSTR Soil Re-

Use Action Levels or Ohio EPA Voluntary Action Plan (VAP) for Construction and

Excavation Direct Contact standards. Refer to Table 1 in the Appendix for the soil analytical results with detectable levels. The complete laboratory analyses are provided in Appendix IV.

The groundwater sample results were compared to the BUSTR Groundwater Ingestion Action Levels in accordance with OAC 1301: 7-9-13 and the Ohio EPA VAP Generic

Unrestricted Potable Water Use standards, in accordance with OAC 3745-300-08. No

levels of VOCs, SVOCs or 8 RCRA Metals exceeded the BUSTR Groundwater

Ingestion Action Levels or the Ohio EPA VAP Generic Unrestricted Potable Water

Use standards. Refer to Table 2 in the Appendix for groundwater analytical results with detectable levels. See Appendix IV for the complete laboratory analysis.

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

12

6.0 CONCLUSIONS AND RECOMMENDATIONS

6.1 Conclusions Rii obtained soil samples from eight (8) soil borings and groundwater samples from two (2) monitoring wells, and provided the samples to an independent laboratory for analyses. The groundwater samples (MW-1 and MW-2) were obtained from Borings SB-8, SB-7, respectively.

The soil sample results were compared to the BUSTR Soil Re-Use Action Levels in accordance with OAC 1301: 7-9-13 and Ohio EPA Voluntary Action Plan (VAP) for Construction and Excavation activities standards, in accordance with OAC 3745-300-08. The groundwater sample results were compared to the BUSTR Groundwater Ingestion Action Levels in accordance with OAC 1301: 7-9-13 and the Ohio EPA VAP Generic Unrestricted Potable Water Use standards, in accordance with OAC 3745-300-08. See Appendix IV for the complete laboratory analysis results.

Volatile Organic Compounds (VOCs)

o Soil - Trace levels of naphthalene and xylenes were detected in the soils of SB-1; however, the levels did not exceed Ohio EPA Voluntary Action Plan (VAP) for Construction and Excavation or the BUSTR Soil Re-Use Action Levels. No levels of VOCs were detected in the other seven (7) borings.

o Groundwater - Trace levels of naphthalene and xylenes were detected in the soils of SB-1. Trace levels of n-propylbenzene, isopropylbenzene, and sec-butylbenzene were detected in the groundwater of MW-1 and MW-2; however, the levels did not exceed the VAP Generic Unrestricted Potable Water standards or BUSTR Groundwater Ingestion Action Levels.

Semi-Volatile Organic Compounds (SVOCs)

o Soil - Small detections of SVOCs were identified in SB-1, SB-2, SB-3, SB-7 and SB-8. The low levels of SVOCs included: benzo (a) anthracene, benzo (k) fluoranthene, benzo (a) pyrene, benzo (b) fluoranthene, chrysene, fluoranthene, naphthalene, phenanthrene, and pyrene. The detected levels did not exceed the Voluntary Action Plan (VAP) for Construction and Excavation Direct Contact standards or the BUSTR Soil Re-Use Action Levels.

o Groundwater - No levels of SVOCs were detected in the two (2) groundwater samples.

8 RCRA Metals

o Soil - Low levels of barium, chromium, lead, mercury, arsenic, and cadmium were detected in SB-1, SB-2, SB-3, SB-4, SB-5, SB-6, SB-7, and SB-8; however, the levels did not exceed the VAP for Construction and Excavation

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

13

or the BUSTR Soil Re-Use Action Levels. The lead levels in SB-7 and SB-8, from 503 mg/kg (4 to 8 feet) and 352 mg/kg (0 to 4 feet), respectively, were above typical Ohio background levels. The remaining detected levels of metals within the soil samples were consistent with industrial land use.

o Groundwater - Trace levels of barium were detected in both groundwater samples, but were below Ohio EPA Voluntary Action Plan (VAP) for Generic Unrestricted Potable Water standards and BUSTR Groundwater Ingestion Action Levels.

6.2 Recommendations Based on the above identified findings, the following is a summary of our recommendations:

Site 13 and Mad River Sediment - Based on the findings, Rii does not recommend any additional environmental investigation of the Site 13 and Mad River sediment. Due to the area’s historical industrial land use, if soils in the project area are to be excavated, stockpiled, and/or removed from the site, plan notes should be prepared detailing the additional testing that should be conducted to characterize the soil for proper landfill disposal (construction/demolition landfill, solid waste landfill, or hazardous waste landfill).

Site 14 - Based on the findings of the visible fill material and petroliferous odors from sample locations SB-7 and SB-8, and high lead levels, Rii recommends any excavated materials be stockpiled, and/or removed from the site, plan notes should be prepared detailing the additional testing that should be conducted to characterize the soil for proper landfill disposal (construction/demolition landfill, solid waste landfill, or hazardous waste landfill). Rii does not recommend any additional environmental investigation for Site 14.

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

14

7.0 RELIABILITY OF REPORT - DISCLAIMER Results and conclusions presented in this investigation were developed utilizing the soil and/or groundwater information and subsequent laboratory analyses obtained from the borings that were made on the site. The borings only depict the soil and/or groundwater conditions at the specific locations and the times at which they were made. Since subsurface conditions are known to vary both in space and time, there is inherent risk in the extrapolation of data. Furthermore, this investigation included soil sampling and aquifer testing, for the specific parameters identified in this report. Conclusions reached in this report are based upon the objective data available to Rii at the time of forming our opinions and as presented in this report. The accuracy of this report depends upon the accuracy of the data. Every effort is made to evaluate the information by the methods that are generally recognized to constitute the State of the Art at the time of rendering the report and conclusions, and the conclusions reached herein represent our opinions. Rii is not responsible for actual conditions proved to be materially at variance with the data that was available to us and upon which we relied, as presented in this report. Rii is not responsible for actual conditions proved to be materially at variance with the data that were available to them and upon which they relied, as presented in this report. The opinions, conclusions and recommendations presented in this report are put forth for a specific and proposed purpose and for the specific site discussed. Rii is not responsible for any other application, whether of purpose or location, of our opinions, conclusions and recommendations other than as specifically indicated in this report. Following sections of this report include comment on issues related to groundwater conditions. Prospective contractors for the project must evaluate potential construction problems on the basis of their review of the contract documents, and their own knowledge of and experience in the local area, and on the basis of similar project in other localities, taking into account their own proposed methods and procedures. Rii is not assuming responsibility for control or charge of construction means, methods, techniques, sequences, procedures or scheduling used by the contractors to comply with their obligations under their contracts for the project or for safety precautions and programs in connection with other contractor’s work on the project or for any failure of any other contractor to comply with Laws and regulations applicable to its furnishing and/or performing of its work.

EMH&T Webster Street Bridge – Phase II ESA Resource International, Inc. Rii Project #W-11-138 – May 7, 2014 Engineering Consultants

15

8.0 SIGNATURE OF ENVIRONMENTAL PROFESSIONAL(S) The Rii environmental professional(s) responsible for the Environmental Subsurface Sampling is as follows:

Steven R. Sawyer Environmental Specialist

Michelle L. Eckels, CPG, LEED Green Assoc. Director – Environmental Services

TABLES 1 & 2

SOIL AND WATER ANALYSES

TABLE 1SOIL ANALYTICAL RESULTS

Page 1 of 1

SB-1 SB-2 SB-3 SB-4 SB-5 SB-6 SB-7 SB-7 SB-8 SB-8

BUSTR Soil Re-Use Action Levels

VAP Construction & Excavation

Activities

Sample Depth (ft) 0-1' 0-1' 0-2' 0-2' 0-2' 0-2' 4-8' 16-20' 0-4' 8-12'Sample Date 4/17/14 4/17/14 4/17/14 4/17/14 4/17/14 4/17/14 4/17/14 4/17/14 4/17/14 4/17/14

EPA Method PARAMETER (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg)Napthalene 0.007 ND ND ND ND ND ND ND ND ND NA 84Xylenes 0.006 ND ND ND ND ND ND 0.01 ND ND 15,700 370Isopropylbenzene ND ND ND ND ND ND ND ND ND ND NA NAsec-Butylbenzene ND ND ND ND ND ND ND ND ND ND NA NAn-Propylbenzene ND ND ND ND ND ND ND 0.006 ND ND NA NA1,2,4-Trimethylbenzene ND ND ND ND ND ND ND 0.01 ND ND NA 35

8015 ORO (C20-C34) 57.5 32.9 41 ND 15.4 19.3 36.7 ND 65.7 ND 5,000 NA

8015 DRO (C10-C20) ND ND ND ND ND ND ND 175 17 ND 2,000 NA

Benzo (a) anthracene 0.41 ND ND ND ND ND 0.39 ND ND ND 2,200 680Benzo (k) fluoranthene 0.34 ND ND ND ND ND ND ND ND ND 1,970 6,900

Benzo (a) pyrene 0.42 ND ND ND ND ND 0.41 ND ND ND 1,100 69.0

Benzo (b) fluoranthene 0.50 ND 0.36 ND ND ND 0.46 ND ND ND 5,530 690Chrysene 0.41 ND 0.33 ND ND ND 0.46 ND ND ND 1,270 69,000Fluoranthene 1.10 0.41 0.80 ND ND ND 1.16 ND ND ND NA 290,000Naphthalene ND ND ND ND ND ND ND ND 0.39 ND 3,980 84Phenanthrene 0.74 ND 0.59 ND ND ND 0.87 ND ND ND NA NAPyrene 0.96 0.34 0.66 ND ND ND 1.01 ND ND ND NA 220,000

Barium 16.9 21.7 77.1 78.2 71.1 92.3 128 146 265 147 NA 120,000Chromium 7.89 5.73 20.5 18.2 15.7 14 12.8 5.53 6.83 8.8 NA 13,000Lead 32.9 7.67 29.9 27.9 29.4 67.7 503 2.91 352 5.67 NA 750.0Mercury ND ND 0.118 0.12 0.0980 0.112 13.6 ND 0.114 ND NA 190.0Arsenic ND 2.39 3.26 3.42 3.21 3.43 11 ND 19.7 3.32 NA 420.0Cadmium ND ND 1.0 0.89 0.88 0.94 0.57 ND 0.66 ND NA 1,600.0

BOLD = Analyte DetectedND - Non Detect

NA - Not Applicable

SVOC Method 8270B

VOCSW-846 Method

8260B

Metals 6000/7000

Series Methods

Extractable Petroleum

Hydrocarbons

TABLE 2GROUNDWATER ANALYTICAL RESULTS

MW-1/SB-8 MW-2/SB-7BUSTRGroundwater Ingestion Action

UnrestrictedPotable Use Standards

Sample Date 4/17/2014 4/17/2014EPA Method PARAMETER (mg/L) (mg/L) (mg/L) (mg/L)

n-Propylbenzene 0.035 0.006 NA NAIsopropylbenzene 0.010 0.005 NA NAsec-Butylbenzene 0.003 0.005 NA NA

BOLD = Analyte DetectedNA = Not Applicable

0.146 NA 2,000Metals (Dissolved) 200 Series Method

VOCSW-846 Method 8260B

Barium 0.271

APPENDIX I

SITE MAP

Rii Project W-11-138

N Site Map

Webster Street Bridge Dayton, Ohio

steves
Callout
Webster Street Bridge PID 90794

APPENDIX II

BORING LOCATIONS

APPENDIX III

BORING LOGS

HS-1 100 Gray poorly graded SAND with GRAVEL.

-HS-1: Visual USCS SPAuger refusal @ 1.0' (due to cobble obstruction)

Bottom of Boring = 1.0 feet

1.0

RC - Rock Coring

SAMPLE TYPE GROUND WATER READING

DRILLING AND SAMPLING INFORMATION

MD - Mud Drilling

4/17/144/17/14Date Finished:S.S.

21.9' LT

SS - Split Spoon Sample

Station

Offset

Drilled By:

Hammer Weight

NAElevation

WD - Wash Drilling

NA

Date Started:

Hammer Drop

HSA - Hollow Stem Augers

SFA - Solid Flight AugersAS - Auger Sample

Hand Auger110+88.09

NA

Boring Method

NAInitial

Extended

BORING METHOD

GS - Geoprobe Sample

ST - Shelby Tube

RC - Rock Core

At Completion

NA

NOTES: Boring located in river

RECOVERYDEPTH SOIL DESCRIPTION

SAMPLE

NO Field Head Space

SAMPLE

TESTED

PERCENT PID READINGS (ppm)DCP

.

2.5

5.0

7.5

10.0

12.5

15.0

Webster Street Bridge

W-11-138

SB-1

1 1

1.0'

EMH&T

Project

Project Number

Boring Number

Sheet of

Completion Depth

RESOURCE INTERNATIONAL, INC.

REPORT OF SOIL EXPLORATION

Client

6350 PRESIDENTIAL GATEWAYCOLUMBUS, OHIO 43231

(614) 823-4949

RESOURCE INTERNATIONAL, INC.

CLEVELAND, OHIO 441259885 ROCKSIDE ROAD

(216) 573-0955

HS-1 100 Gray poorly graded SAND with GRAVEL.

-HS-1: Visual USCS SPAuger refusal @ 1.0' (due to cobble obstruction)

Bottom of Boring = 1.0 feet

1.0

RC - Rock Coring

SAMPLE TYPE GROUND WATER READING

DRILLING AND SAMPLING INFORMATION

MD - Mud Drilling

4/17/144/17/14Date Finished:S.S.

18.2' RT

SS - Split Spoon Sample

Station

Offset

Drilled By:

Hammer Weight

NAElevation

WD - Wash Drilling

NA

Date Started:

Hammer Drop

HSA - Hollow Stem Augers

SFA - Solid Flight AugersAS - Auger Sample

Hand Auger110+50.07

NA

Boring Method

NAInitial

Extended

BORING METHOD

GS - Geoprobe Sample

ST - Shelby Tube

RC - Rock Core

At Completion

NA

NOTES: Boring located in river

RECOVERYDEPTH SOIL DESCRIPTION

SAMPLE

NO Field Head Space

SAMPLE

TESTED

PERCENT PID READINGS (ppm)DCP

.

2.5

5.0

7.5

10.0

12.5

15.0

Webster Street Bridge

W-11-138

SB-2

1 1

1.0'

EMH&T

Project

Project Number

Boring Number

Sheet of

Completion Depth

RESOURCE INTERNATIONAL, INC.

REPORT OF SOIL EXPLORATION

Client

6350 PRESIDENTIAL GATEWAYCOLUMBUS, OHIO 43231

(614) 823-4949

RESOURCE INTERNATIONAL, INC.

CLEVELAND, OHIO 441259885 ROCKSIDE ROAD

(216) 573-0955

HS-1 100 Gray poorly graded SAND with GRAVEL.

-HS-1: Visual USCS SPAuger refusal @ 2.0' (due to cobble obstruction)

Bottom of Boring = 2.0 feet2.0

18.8

RC - Rock Coring

SAMPLE TYPE GROUND WATER READING

DRILLING AND SAMPLING INFORMATION

MD - Mud Drilling

4/17/144/17/14Date Finished:S.S.

21.8' LT

SS - Split Spoon Sample

Station

Offset

Drilled By:

Hammer Weight

NAElevation

WD - Wash Drilling

NA

Date Started:

Hammer Drop

HSA - Hollow Stem Augers

SFA - Solid Flight AugersAS - Auger Sample

Hand Auger112+29.69

NA

Boring Method

DryInitial

Extended

BORING METHOD

GS - Geoprobe Sample

ST - Shelby Tube

RC - Rock Core

At Completion

Dry

NOTES:

RECOVERYDEPTH SOIL DESCRIPTION

SAMPLE

NO Field Head Space

SAMPLE

TESTED

PERCENT PID READINGS (ppm)DCP

.

2.5

5.0

7.5

10.0

12.5

15.0

Webster Street Bridge

W-11-138

SB-3

1 1

2.0'

EMH&T

Project

Project Number

Boring Number

Sheet of

Completion Depth

RESOURCE INTERNATIONAL, INC.

REPORT OF SOIL EXPLORATION

Client

6350 PRESIDENTIAL GATEWAYCOLUMBUS, OHIO 43231

(614) 823-4949

RESOURCE INTERNATIONAL, INC.

CLEVELAND, OHIO 441259885 ROCKSIDE ROAD

(216) 573-0955

HS-1 100 Gray poorly graded SAND with GRAVEL.

HS-1: Visual USCS SP -glass fragments present throughout

Auger refusal @ 2.6' (due to cobble obstruction)

Bottom of Boring = 2.6 feet2.6

2.6

RC - Rock Coring

SAMPLE TYPE GROUND WATER READING

DRILLING AND SAMPLING INFORMATION

MD - Mud Drilling

4/17/144/17/14Date Finished:S.S.

18.2' RT

SS - Split Spoon Sample

Station

Offset

Drilled By:

Hammer Weight

NAElevation

WD - Wash Drilling

NA

Date Started:

Hammer Drop

HSA - Hollow Stem Augers

SFA - Solid Flight AugersAS - Auger Sample

Hand Auger112+29.67

NA

Boring Method

DryInitial

Extended

BORING METHOD

GS - Geoprobe Sample

ST - Shelby Tube

RC - Rock Core

At Completion

Dry

NOTES:

RECOVERYDEPTH SOIL DESCRIPTION

SAMPLE

NO Field Head Space

SAMPLE

TESTED

PERCENT PID READINGS (ppm)DCP

.

2.5

5.0

7.5

10.0

12.5

15.0

Webster Street Bridge

W-11-138

SB-4

1 1

2.6'

EMH&T

Project

Project Number

Boring Number

Sheet of

Completion Depth

RESOURCE INTERNATIONAL, INC.

REPORT OF SOIL EXPLORATION

Client

6350 PRESIDENTIAL GATEWAYCOLUMBUS, OHIO 43231

(614) 823-4949

RESOURCE INTERNATIONAL, INC.

CLEVELAND, OHIO 441259885 ROCKSIDE ROAD

(216) 573-0955

HS-1 100 Brown and gray poorly graded SAND withGRAVEL.

HS-1: Visual USCS SP -shells and cobbles present throughoutAuger refusal @ 2.0' (due to concrete obstruction)

Bottom of Boring = 2.0 feet

2.0

7.9

RC - Rock Coring

SAMPLE TYPE GROUND WATER READING

DRILLING AND SAMPLING INFORMATION

MD - Mud Drilling

4/17/144/17/14Date Finished:S.S.

40.6' LT

SS - Split Spoon Sample

Station

Offset

Drilled By:

Hammer Weight

NAElevation

WD - Wash Drilling

NA

Date Started:

Hammer Drop

HSA - Hollow Stem Augers

SFA - Solid Flight AugersAS - Auger Sample

Hand Auger113+02.80

NA

Boring Method

DryInitial

Extended

BORING METHOD

GS - Geoprobe Sample

ST - Shelby Tube

RC - Rock Core

At Completion

Dry

NOTES:

RECOVERYDEPTH SOIL DESCRIPTION

SAMPLE

NO Field Head Space

SAMPLE

TESTED

PERCENT PID READINGS (ppm)DCP

.

2.5

5.0

7.5

10.0

12.5

15.0

Webster Street Bridge

W-11-138

SB-5

1 1

2.0'

EMH&T

Project

Project Number

Boring Number

Sheet of

Completion Depth

RESOURCE INTERNATIONAL, INC.

REPORT OF SOIL EXPLORATION

Client

6350 PRESIDENTIAL GATEWAYCOLUMBUS, OHIO 43231

(614) 823-4949

RESOURCE INTERNATIONAL, INC.

CLEVELAND, OHIO 441259885 ROCKSIDE ROAD

(216) 573-0955

HS-1

HS-2

100

100

Gray POORLY GRADED SAND with GRAVEL.

HS-1: Visual USCS SP -glass fragments and cobbles present throughoutAuger refusal @ 2.4' (due to concrete obstruction)

Bottom of Boring = 2.4 feet2.4

0.4

0.3

RC - Rock Coring

SAMPLE TYPE GROUND WATER READING

DRILLING AND SAMPLING INFORMATION

MD - Mud Drilling

4/17/144/17/14Date Finished:S.S.

36.5' RT

SS - Split Spoon Sample

Station

Offset

Drilled By:

Hammer Weight

NAElevation

WD - Wash Drilling

NA

Date Started:

Hammer Drop

HSA - Hollow Stem Augers

SFA - Solid Flight AugersAS - Auger Sample

Hand Auger113+04.27

NA

Boring Method

DryInitial

Extended

BORING METHOD

GS - Geoprobe Sample

ST - Shelby Tube

RC - Rock Core

At Completion

Dry

NOTES:

RECOVERYDEPTH SOIL DESCRIPTION

SAMPLE

NO Field Head Space

SAMPLE

TESTED

PERCENT PID READINGS (ppm)DCP

.

2.5

5.0

7.5

10.0

12.5

15.0

Webster Street Bridge

W-11-138

SB-6

1 1

2.4'

EMH&T

Project

Project Number

Boring Number

Sheet of

Completion Depth

RESOURCE INTERNATIONAL, INC.

REPORT OF SOIL EXPLORATION

Client

6350 PRESIDENTIAL GATEWAYCOLUMBUS, OHIO 43231

(614) 823-4949

RESOURCE INTERNATIONAL, INC.

CLEVELAND, OHIO 441259885 ROCKSIDE ROAD

(216) 573-0955

GS-1

GS-2

GS-3

GS-4

63

46

46

65

6.0" - TopsoilBlack CINDERS, and GRAVEL.

-GS-1: Visual USCS GW

-changing to black, tan and brown @ 4.0'

-GS-2: Visual USCS GW

-0.3' wet black sand present @ 8.0'

Black LEAN CLAY, some silt, little sand.

-GS-3: Visual USCS CL

-changing to brown @ 12.0'

Gray poorly graded SAND with GRAVEL.

-GS-4: Visual USCS SP

0.5

8.0

13.4

10.5

5.5

1.9

3.5

RC - Rock Coring

SAMPLE TYPE GROUND WATER READING

DRILLING AND SAMPLING INFORMATION

MD - Mud Drilling

4/17/144/17/14Date Finished:S.S.

36.3' RT

SS - Split Spoon Sample

Station

Offset

Drilled By:

Hammer Weight

NAElevation

WD - Wash Drilling

NA

Date Started:

Hammer Drop

HSA - Hollow Stem Augers

SFA - Solid Flight AugersAS - Auger Sample

Geoprobe115+69.06

NA

Boring Method

16.7Initial

Extended

BORING METHOD

GS - Geoprobe Sample

ST - Shelby Tube

RC - Rock Core

At Completion

17.0

NOTES:

RECOVERYDEPTH SOIL DESCRIPTION

SAMPLE

NO Field Head Space

SAMPLE

TESTED

PERCENT PID READINGS (ppm)DCP

.

2.5

5.0

7.5

10.0

12.5

15.0

Webster Street Bridge

W-11-138

SB-7

1 2

22.0'

EMH&T

Project

Project Number

Boring Number

Sheet of

Completion Depth

RESOURCE INTERNATIONAL, INC.

REPORT OF SOIL EXPLORATION

Client

6350 PRESIDENTIAL GATEWAYCOLUMBUS, OHIO 43231

(614) 823-4949

RESOURCE INTERNATIONAL, INC.

CLEVELAND, OHIO 441259885 ROCKSIDE ROAD

(216) 573-0955

GS-5 38 -petroleum odor present from 16.0' to 20.0'

-becoming wet @ from 17.0' to 17.8'

-GS-5: Visual USCS SP

Bottom of Boring = 22.0 feet

Set temporary well @ 22.0'

22.0

71.0

NOTES:

17.5

20.0

22.5

25.0

27.5

30.0

32.5

35.0

37.5

Webster Street Bridge

W-11-138

SB-7

2 2

22.0'

EMH&T

RECOVERYDEPTH SOIL DESCRIPTION

SAMPLE

NO Field Head Space

SAMPLE

TESTED

PERCENT PID READINGS (ppm)DCP

.

Project

Project Number

Boring Number

Sheet of

Completion Depth

RESOURCE INTERNATIONAL, INC.

REPORT OF SOIL EXPLORATION

Client

6350 PRESIDENTIAL GATEWAYCOLUMBUS, OHIO 43231

(614) 823-4949

RESOURCE INTERNATIONAL, INC.

CLEVELAND, OHIO 441259885 ROCKSIDE ROAD

(216) 573-0955

GS-1

GS-2

GS-3

GS-4

50

24

69

63

3.0" - TopsoilBlack CINDERS.

Brown LEAN CLAY with GRAVEL, trace sand.

-GS-1: Visual USCS CL

Black CINDERS, some gravel.

-GS-2: Visual USCS GP

Stiff, brown and red LEAN CLAY with GRAVEL,some silt.

-GS-3: Visual USCS CL

Gray well graded SAND.

-GS-4: Visual USCS SW

0.3

1.7

4.4

8.0

10.9

36.2

23.1

28.4

33.2

RC - Rock Coring

SAMPLE TYPE GROUND WATER READING

DRILLING AND SAMPLING INFORMATION

MD - Mud Drilling

4/17/144/17/14Date Finished:S.S.

37.3' RT

SS - Split Spoon Sample

Station

Offset

Drilled By:

Hammer Weight

NAElevation

WD - Wash Drilling

NA

Date Started:

Hammer Drop

HSA - Hollow Stem Augers

SFA - Solid Flight AugersAS - Auger Sample

Geoprobe115+95.22

na

Boring Method

15.4Initial

Extended

BORING METHOD

GS - Geoprobe Sample

ST - Shelby Tube

RC - Rock Core

At Completion

16.0

NOTES:

RECOVERYDEPTH SOIL DESCRIPTION

SAMPLE

NO Field Head Space

SAMPLE

TESTED

PERCENT PID READINGS (ppm)DCP

.

2.5

5.0

7.5

10.0

12.5

15.0

Webster Street Bridge

W-11-138

SB-8

1 2

20.0'

EMH&T

Project

Project Number

Boring Number

Sheet of

Completion Depth

RESOURCE INTERNATIONAL, INC.

REPORT OF SOIL EXPLORATION

Client

6350 PRESIDENTIAL GATEWAYCOLUMBUS, OHIO 43231

(614) 823-4949

RESOURCE INTERNATIONAL, INC.

CLEVELAND, OHIO 441259885 ROCKSIDE ROAD

(216) 573-0955

GS-5 56

-wet @ 16.0'

Gray poorly graded GRAVEL.

Brown, poorly graded SAND, wet.

-GS-5: Visual USCS SP

Bottom of Boring = 20.0'

Set temporary well (5.0' screen) at 15.0'

16.0

17.0

20.0

29.4

NOTES:

17.5

20.0

22.5

25.0

27.5

30.0

32.5

35.0

37.5

Webster Street Bridge

W-11-138

SB-8

2 2

20.0'

EMH&T

RECOVERYDEPTH SOIL DESCRIPTION

SAMPLE

NO Field Head Space

SAMPLE

TESTED

PERCENT PID READINGS (ppm)DCP

.

Project

Project Number

Boring Number

Sheet of

Completion Depth

RESOURCE INTERNATIONAL, INC.

REPORT OF SOIL EXPLORATION

Client

6350 PRESIDENTIAL GATEWAYCOLUMBUS, OHIO 43231

(614) 823-4949

RESOURCE INTERNATIONAL, INC.

CLEVELAND, OHIO 441259885 ROCKSIDE ROAD

(216) 573-0955

APPENDIX IV

ANALYTICAL RESULTS AND CHAIN OF CUSTODY

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-1 0-1'

1404090-01 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Volatile Organic Compounds by EPA Method 8260B

1,1,1,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,1-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromo-3-chloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromoethane (EDB) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,4-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acetone 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Benzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromodichloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromoform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 1 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-1 0-1'

1404090-01 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Ethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl ethyl ketone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methylene chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Naphthalene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/140.007 JWG

Styrene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

tert-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Tetrachloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Toluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,4-Dichloro-2-butene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichlorofluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Xylenes (total) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/140.006 JWG

2-Hexanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chloroethylvinyl ether 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon disulfide 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon tetrachloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 2 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-1 0-1'

1404090-01 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Chlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl acetate 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Methyl-2-pentanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrolein 0.01 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrylonitrile 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dichlorodifluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Iodomethane 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Isopropyl alcohol 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl tert-butyl ether 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Propylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 3 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-1 0-1'

1404090-01 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Isopropylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

sec-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,4-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3,5-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

p-Isopropyltoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Surrogate: 1,2-Dichloroethane-d4 70-130 4/23/14 4/23/14 EPA 8260B84.7 % JWG

Surrogate: Toluene-d8 70-130 4/23/14 4/23/14 EPA 8260B109 % JWG

Surrogate: 4-Bromofluorobenzene 70-130 4/23/14 4/23/14 EPA 8260B106 % JWG

Extractable Petroleum Hydrocarbons by 8015 GRO

GRO (C6-C12) 1.00 EPA 8015mg/kg 4/22/14 4/22/14ND JAW

Surrogate: a,a,a-Trifluorotoluene 70-130 4/22/14 4/22/14 EPA 8015118 % JAW

Extractable Petroleum Hydrocarbons by 8015 DRO

DRO (C10 - C20) 10.0 EPA 8015mg/kg 4/21/14 4/23/14ND ATS

Surrogate: 2-Fluorobiphenyl 40-120 4/21/14 4/23/14 EPA 801557.5 % ATS

Extractable Petroleum Hydrocarbons by 8015 ORO

ORO (C20 - C34) 10.0 EPA 8015mg/kg 4/21/14 4/23/1457.5 ATS

Semivolatile Organic Compounds by EPA Method 8270B

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 4 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-1 0-1'

1404090-01 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Phenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Chlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

3 & 4-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dimethylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,6-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Chloro-3-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4,5-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4,6-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,3,4,6-Tetrachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4,6-Dinitro-2-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Pentachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-sec-Butyl-4,6-dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Surrogate: 2-Fluorophenol 25-121 4/21/14 4/24/14 EPA 8270B57.4 % ATS

Surrogate: Phenol-d6 24-113 4/21/14 4/24/14 EPA 8270B76.9 % ATS

Surrogate: 2,4,6-Tribromophenol 19-122 4/21/14 4/24/14 EPA 8270B91.6 % ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 5 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-1 0-1'

1404090-01 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Acenaphthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Acenaphthylene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (a) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.41 ATS

Benzo (b) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.50 ATS

Benzo (k) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.34 ATS

Benzo (g,h,i) perylene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (a) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.42 ATS

Bis(2-chloroethoxy)methane 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroethyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroisopropyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-ethylhexyl)phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Bromophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Butyl benzyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Chloronaphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Chlorophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Chrysene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.41 ATS

Dibenz (a,h) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Di-n-butyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

N-Nitrosodimethylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 6 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-1 0-1'

1404090-01 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

1,3-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,4-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2-Diphenylhydrazine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

3,3´-Dichlorobenzidine 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzidine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Diethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Dimethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,6-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Di-n-octyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/141.10 ATS

Fluorene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorobutadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorocyclopentadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachloroethane 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Indeno (1,2,3-cd) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Isophorone 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Naphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Nitrobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

N-Nitrosodiphenylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 7 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-1 0-1'

1404090-01 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

N-Nitrosodi-n-propylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Phenanthrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.74 ATS

Pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.96 ATS

1,2,4-Trichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Surrogate: Nitrobenzene-d5 23-120 4/21/14 4/24/14 EPA 8270B69.3 % ATS

Surrogate: 2-Fluorobiphenyl 30-115 4/21/14 4/24/14 EPA 8270B66.2 % ATS

Surrogate: Terphenyl-d14 18-137 4/21/14 4/24/14 EPA 8270B95.7 % ATS

Metals by EPA 6000/7000 Series Methods

Silver 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Arsenic 2.00 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Barium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/1416.9 MWB

Cadmium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Chromium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/147.89 MWB

Mercury 0.0400 EPA 7471mg/kg 4/21/14 4/22/14ND MWB

Lead 2.00 EPA 6010Cmg/kg 4/21/14 4/22/1432.9 MWB

Selenium 2.00 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 8 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-2 0-1'

1404090-02 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Volatile Organic Compounds by EPA Method 8260B

1,1,1,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,1-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromo-3-chloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromoethane (EDB) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,4-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acetone 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Benzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromodichloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromoform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 9 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-2 0-1'

1404090-02 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Ethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl ethyl ketone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methylene chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Naphthalene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Styrene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

tert-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Tetrachloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Toluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,4-Dichloro-2-butene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichlorofluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Xylenes (total) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Hexanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chloroethylvinyl ether 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon disulfide 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon tetrachloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 10 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-2 0-1'

1404090-02 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Chlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl acetate 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Methyl-2-pentanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrolein 0.01 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrylonitrile 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dichlorodifluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Iodomethane 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Isopropyl alcohol 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl tert-butyl ether 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Propylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 11 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-2 0-1'

1404090-02 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Isopropylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

sec-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,4-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3,5-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

p-Isopropyltoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Surrogate: 1,2-Dichloroethane-d4 70-130 4/23/14 4/23/14 EPA 8260B86.5 % JWG

Surrogate: Toluene-d8 70-130 4/23/14 4/23/14 EPA 8260B103 % JWG

Surrogate: 4-Bromofluorobenzene 70-130 4/23/14 4/23/14 EPA 8260B109 % JWG

Extractable Petroleum Hydrocarbons by 8015 GRO

GRO (C6-C12) 1.00 EPA 8015mg/kg 4/22/14 4/22/14ND JAW

Surrogate: a,a,a-Trifluorotoluene 70-130 4/22/14 4/22/14 EPA 8015121 % JAW

Extractable Petroleum Hydrocarbons by 8015 DRO

DRO (C10 - C20) 10.0 EPA 8015mg/kg 4/21/14 4/23/14ND ATS

Surrogate: 2-Fluorobiphenyl 40-120 4/21/14 4/23/14 EPA 801565.4 % ATS

Extractable Petroleum Hydrocarbons by 8015 ORO

ORO (C20 - C34) 10.0 EPA 8015mg/kg 4/21/14 4/23/1432.9 ATS

Semivolatile Organic Compounds by EPA Method 8270B

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 12 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-2 0-1'

1404090-02 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Phenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Chlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

3 & 4-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dimethylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,6-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Chloro-3-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4,5-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4,6-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,3,4,6-Tetrachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4,6-Dinitro-2-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Pentachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-sec-Butyl-4,6-dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Surrogate: 2-Fluorophenol 25-121 4/21/14 4/24/14 EPA 8270B71.5 % ATS

Surrogate: Phenol-d6 24-113 4/21/14 4/24/14 EPA 8270B88.3 % ATS

Surrogate: 2,4,6-Tribromophenol 19-122 4/21/14 4/24/14 EPA 8270B92.7 % ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 13 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-2 0-1'

1404090-02 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Acenaphthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Acenaphthylene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (a) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (b) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (k) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (g,h,i) perylene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (a) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroethoxy)methane 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroethyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroisopropyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-ethylhexyl)phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Bromophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Butyl benzyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Chloronaphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Chlorophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Chrysene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Dibenz (a,h) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Di-n-butyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

N-Nitrosodimethylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 14 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-2 0-1'

1404090-02 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

1,3-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,4-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

3,3´-Dichlorobenzidine 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2-Diphenylhydrazine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzidine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Diethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Dimethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,6-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Di-n-octyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.41 ATS

Fluorene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorobutadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorocyclopentadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachloroethane 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Indeno (1,2,3-cd) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Isophorone 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Naphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Nitrobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

N-Nitrosodiphenylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 15 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-2 0-1'

1404090-02 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

N-Nitrosodi-n-propylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Phenanthrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.34 ATS

1,2,4-Trichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Surrogate: Nitrobenzene-d5 23-120 4/21/14 4/24/14 EPA 8270B83.3 % ATS

Surrogate: 2-Fluorobiphenyl 30-115 4/21/14 4/24/14 EPA 8270B74.8 % ATS

Surrogate: Terphenyl-d14 18-137 4/21/14 4/24/14 EPA 8270B103 % ATS

Metals by EPA 6000/7000 Series Methods

Silver 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Arsenic 2.00 EPA 6010Cmg/kg 4/21/14 4/22/142.39 MWB

Barium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/1421.7 MWB

Cadmium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Chromium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/145.73 MWB

Mercury 0.0400 EPA 7471mg/kg 4/21/14 4/22/14ND MWB

Lead 2.00 EPA 6010Cmg/kg 4/21/14 4/22/147.67 MWB

Selenium 2.00 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 16 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-3 0-2'

1404090-03 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Volatile Organic Compounds by EPA Method 8260B

1,1,1,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,1-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromo-3-chloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromoethane (EDB) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,4-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acetone 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Benzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromodichloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromoform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 17 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-3 0-2'

1404090-03 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Ethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl ethyl ketone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methylene chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Naphthalene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Styrene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

tert-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Tetrachloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Toluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,4-Dichloro-2-butene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichlorofluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Xylenes (total) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Hexanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chloroethylvinyl ether 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon disulfide 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon tetrachloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 18 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-3 0-2'

1404090-03 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Chlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl acetate 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Methyl-2-pentanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrolein 0.01 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrylonitrile 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dichlorodifluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Iodomethane 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Isopropyl alcohol 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl tert-butyl ether 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Propylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 19 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-3 0-2'

1404090-03 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Isopropylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

sec-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,4-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3,5-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

p-Isopropyltoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Surrogate: 1,2-Dichloroethane-d4 70-130 4/23/14 4/23/14 EPA 8260B86.1 % JWG

Surrogate: Toluene-d8 70-130 4/23/14 4/23/14 EPA 8260B117 % JWG

Surrogate: 4-Bromofluorobenzene 70-130 4/23/14 4/23/14 EPA 8260B126 % JWG

Extractable Petroleum Hydrocarbons by 8015 GRO

GRO (C6-C12) 1.00 EPA 8015mg/kg 4/22/14 4/22/14ND JAW

Surrogate: a,a,a-Trifluorotoluene 70-130 4/22/14 4/22/14 EPA 8015123 % JAW

Extractable Petroleum Hydrocarbons by 8015 DRO

DRO (C10 - C20) 10.0 EPA 8015mg/kg 4/21/14 4/23/14ND ATS

Surrogate: 2-Fluorobiphenyl 40-120 4/21/14 4/23/14 EPA 801562.1 % ATS

Extractable Petroleum Hydrocarbons by 8015 ORO

ORO (C20 - C34) 10.0 EPA 8015mg/kg 4/21/14 4/23/1441.0 ATS

Semivolatile Organic Compounds by EPA Method 8270B

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 20 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-3 0-2'

1404090-03 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Phenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Chlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

3 & 4-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dimethylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,6-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Chloro-3-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4,5-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4,6-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,3,4,6-Tetrachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4,6-Dinitro-2-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Pentachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-sec-Butyl-4,6-dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Surrogate: 2-Fluorophenol 25-121 4/21/14 4/24/14 EPA 8270B56.4 % ATS

Surrogate: Phenol-d6 24-113 4/21/14 4/24/14 EPA 8270B77.9 % ATS

Surrogate: 2,4,6-Tribromophenol 19-122 4/21/14 4/24/14 EPA 8270B84.2 % ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 21 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-3 0-2'

1404090-03 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Acenaphthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Acenaphthylene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (a) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (b) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.36 ATS

Benzo (k) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (g,h,i) perylene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (a) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroethoxy)methane 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroethyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroisopropyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-ethylhexyl)phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Bromophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Butyl benzyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Chloronaphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Chlorophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Chrysene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.33 ATS

Dibenz (a,h) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Di-n-butyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

N-Nitrosodimethylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 22 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-3 0-2'

1404090-03 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

1,3-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,4-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2-Diphenylhydrazine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzidine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

3,3´-Dichlorobenzidine 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Diethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Dimethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,6-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Di-n-octyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.80 ATS

Fluorene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorobutadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorocyclopentadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachloroethane 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Indeno (1,2,3-cd) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Isophorone 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Naphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Nitrobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

N-Nitrosodiphenylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 23 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-3 0-2'

1404090-03 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

N-Nitrosodi-n-propylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Phenanthrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.59 ATS

Pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.66 ATS

1,2,4-Trichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Surrogate: Nitrobenzene-d5 23-120 4/21/14 4/24/14 EPA 8270B74.6 % ATS

Surrogate: 2-Fluorobiphenyl 30-115 4/21/14 4/24/14 EPA 8270B68.5 % ATS

Surrogate: Terphenyl-d14 18-137 4/21/14 4/24/14 EPA 8270B96.6 % ATS

Metals by EPA 6000/7000 Series Methods

Silver 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Arsenic 2.00 EPA 6010Cmg/kg 4/21/14 4/22/143.26 MWB

Barium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/1477.1 MWB

Cadmium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/141.00 MWB

Chromium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/1420.5 MWB

Mercury 0.0400 EPA 7471mg/kg 4/21/14 4/22/140.118 MWB

Lead 2.00 EPA 6010Cmg/kg 4/21/14 4/22/1429.9 MWB

Selenium 2.00 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 24 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-4 0-2'

1404090-04 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Volatile Organic Compounds by EPA Method 8260B

1,1,1,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,1-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromo-3-chloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromoethane (EDB) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,4-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acetone 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Benzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromodichloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromoform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 25 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-4 0-2'

1404090-04 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Ethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl ethyl ketone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methylene chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Naphthalene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Styrene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

tert-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Tetrachloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Toluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,4-Dichloro-2-butene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichlorofluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Xylenes (total) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Hexanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chloroethylvinyl ether 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon disulfide 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon tetrachloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 26 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-4 0-2'

1404090-04 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Chlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl acetate 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Methyl-2-pentanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrolein 0.01 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrylonitrile 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dichlorodifluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Iodomethane 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Isopropyl alcohol 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl tert-butyl ether 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Propylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 27 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-4 0-2'

1404090-04 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Isopropylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

sec-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,4-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3,5-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

p-Isopropyltoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Surrogate: 1,2-Dichloroethane-d4 70-130 4/23/14 4/23/14 EPA 8260B81.6 % JWG

Surrogate: Toluene-d8 70-130 4/23/14 4/23/14 EPA 8260B123 % JWG

Surrogate: 4-Bromofluorobenzene 70-130 4/23/14 4/23/14 EPA 8260B128 % JWG

Extractable Petroleum Hydrocarbons by 8015 GRO

GRO (C6-C12) 1.00 EPA 8015mg/kg 4/22/14 4/22/14ND JAW

Surrogate: a,a,a-Trifluorotoluene 70-130 4/22/14 4/22/14 EPA 8015130 % JAW

Extractable Petroleum Hydrocarbons by 8015 DRO

DRO (C10 - C20) 10.0 EPA 8015mg/kg 4/21/14 4/23/14ND ATS

Surrogate: 2-Fluorobiphenyl 40-120 4/21/14 4/23/14 EPA 801559.0 % ATS

Extractable Petroleum Hydrocarbons by 8015 ORO

ORO (C20 - C34) 10.0 EPA 8015mg/kg 4/21/14 4/23/14ND ATS

Semivolatile Organic Compounds by EPA Method 8270B

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 28 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-4 0-2'

1404090-04 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Phenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-Chlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

3 & 4-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4-Dimethylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,6-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4-Chloro-3-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4,5-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4,6-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4-Dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,3,4,6-Tetrachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4,6-Dinitro-2-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Pentachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-sec-Butyl-4,6-dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Surrogate: 2-Fluorophenol 25-121 4/21/14 4/23/14 EPA 8270B41.1 % ATS

Surrogate: Phenol-d6 24-113 4/21/14 4/23/14 EPA 8270B63.0 % ATS

Surrogate: 2,4,6-Tribromophenol 19-122 4/21/14 4/23/14 EPA 8270B74.2 % ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 29 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-4 0-2'

1404090-04 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Acenaphthene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Acenaphthylene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (a) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (b) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (k) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (g,h,i) perylene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (a) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Bis(2-chloroethoxy)methane 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Bis(2-chloroethyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Bis(2-chloroisopropyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Bis(2-ethylhexyl)phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4-Bromophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Butyl benzyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-Chloronaphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4-Chlorophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Chrysene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Dibenz (a,h) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Di-n-butyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

1,2-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

N-Nitrosodimethylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 30 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-4 0-2'

1404090-04 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

1,3-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

1,4-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

3,3´-Dichlorobenzidine 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

1,2-Diphenylhydrazine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzidine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Diethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Dimethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,6-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Di-n-octyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Fluorene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Hexachlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Hexachlorobutadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Hexachlorocyclopentadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Hexachloroethane 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Indeno (1,2,3-cd) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Isophorone 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Naphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Nitrobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

N-Nitrosodiphenylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 31 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-4 0-2'

1404090-04 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

N-Nitrosodi-n-propylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Phenanthrene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

1,2,4-Trichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Surrogate: Nitrobenzene-d5 23-120 4/21/14 4/23/14 EPA 8270B62.8 % ATS

Surrogate: 2-Fluorobiphenyl 30-115 4/21/14 4/23/14 EPA 8270B58.1 % ATS

Surrogate: Terphenyl-d14 18-137 4/21/14 4/23/14 EPA 8270B71.1 % ATS

Metals by EPA 6000/7000 Series Methods

Silver 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Arsenic 2.00 EPA 6010Cmg/kg 4/21/14 4/22/143.42 MWB

Barium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/1478.2 MWB

Cadmium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/140.89 MWB

Chromium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/1418.2 MWB

Mercury 0.0400 EPA 7471mg/kg 4/21/14 4/22/140.120 MWB

Lead 2.00 EPA 6010Cmg/kg 4/21/14 4/22/1427.9 MWB

Selenium 2.00 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 32 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-5 0-2'

1404090-05 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Volatile Organic Compounds by EPA Method 8260B

1,1,1,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,1-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromo-3-chloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromoethane (EDB) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,4-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acetone 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Benzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromodichloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromoform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 33 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-5 0-2'

1404090-05 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Ethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl ethyl ketone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methylene chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Naphthalene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Styrene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

tert-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Tetrachloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Toluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,4-Dichloro-2-butene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichlorofluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Xylenes (total) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Hexanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chloroethylvinyl ether 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon disulfide 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon tetrachloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 34 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-5 0-2'

1404090-05 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Chlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl acetate 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Methyl-2-pentanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrolein 0.01 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrylonitrile 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dichlorodifluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Iodomethane 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Isopropyl alcohol 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl tert-butyl ether 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Propylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 35 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-5 0-2'

1404090-05 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Isopropylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

sec-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,4-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3,5-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

p-Isopropyltoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Surrogate: 1,2-Dichloroethane-d4 70-130 4/23/14 4/23/14 EPA 8260B92.2 % JWG

Surrogate: Toluene-d8 70-130 4/23/14 4/23/14 EPA 8260B124 % JWG

Surrogate: 4-Bromofluorobenzene 70-130 4/23/14 4/23/14 EPA 8260B120 % JWG

Extractable Petroleum Hydrocarbons by 8015 GRO

GRO (C6-C12) 1.00 EPA 8015mg/kg 4/22/14 4/22/14ND JAW

Surrogate: a,a,a-Trifluorotoluene 70-130 4/22/14 4/22/14 EPA 8015118 % JAW

Extractable Petroleum Hydrocarbons by 8015 DRO

DRO (C10 - C20) 10.0 EPA 8015mg/kg 4/21/14 4/23/14ND ATS

Surrogate: 2-Fluorobiphenyl 40-120 4/21/14 4/23/14 EPA 801562.4 % ATS

Extractable Petroleum Hydrocarbons by 8015 ORO

ORO (C20 - C34) 10.0 EPA 8015mg/kg 4/21/14 4/23/1415.4 ATS

Semivolatile Organic Compounds by EPA Method 8270B

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 36 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-5 0-2'

1404090-05 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Phenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Chlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

3 & 4-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dimethylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,6-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Chloro-3-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4,5-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4,6-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,3,4,6-Tetrachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4,6-Dinitro-2-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Pentachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-sec-Butyl-4,6-dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Surrogate: 2-Fluorophenol 25-121 4/21/14 4/24/14 EPA 8270B67.4 % ATS

Surrogate: Phenol-d6 24-113 4/21/14 4/24/14 EPA 8270B94.8 % ATS

Surrogate: 2,4,6-Tribromophenol 19-122 4/21/14 4/24/14 EPA 8270B84.3 % ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 37 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-5 0-2'

1404090-05 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Acenaphthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Acenaphthylene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (a) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (b) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (k) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (g,h,i) perylene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (a) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroethoxy)methane 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroethyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroisopropyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-ethylhexyl)phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Bromophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Butyl benzyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Chloronaphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Chlorophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Chrysene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Dibenz (a,h) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Di-n-butyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

N-Nitrosodimethylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 38 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-5 0-2'

1404090-05 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

1,3-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,4-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2-Diphenylhydrazine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

3,3´-Dichlorobenzidine 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzidine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Diethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Dimethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,6-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Di-n-octyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Fluorene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorobutadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorocyclopentadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachloroethane 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Indeno (1,2,3-cd) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Isophorone 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Naphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Nitrobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

N-Nitrosodiphenylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 39 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-5 0-2'

1404090-05 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

N-Nitrosodi-n-propylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Phenanthrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2,4-Trichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Surrogate: Nitrobenzene-d5 23-120 4/21/14 4/24/14 EPA 8270B84.3 % ATS

Surrogate: 2-Fluorobiphenyl 30-115 4/21/14 4/24/14 EPA 8270B74.9 % ATS

Surrogate: Terphenyl-d14 18-137 4/21/14 4/24/14 EPA 8270B76.3 % ATS

Metals by EPA 6000/7000 Series Methods

Silver 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Arsenic 2.00 EPA 6010Cmg/kg 4/21/14 4/22/143.21 MWB

Barium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/1471.1 MWB

Cadmium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/140.88 MWB

Chromium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/1415.7 MWB

Mercury 0.0400 EPA 7471mg/kg 4/21/14 4/22/140.0980 MWB

Lead 2.00 EPA 6010Cmg/kg 4/21/14 4/22/1429.4 MWB

Selenium 2.00 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 40 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-6 0-2'

1404090-06 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Volatile Organic Compounds by EPA Method 8260B

1,1,1,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,1-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromo-3-chloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromoethane (EDB) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,4-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acetone 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Benzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromodichloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromoform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 41 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-6 0-2'

1404090-06 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Ethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl ethyl ketone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methylene chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Naphthalene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Styrene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

tert-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Tetrachloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Toluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,4-Dichloro-2-butene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichlorofluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Xylenes (total) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Hexanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chloroethylvinyl ether 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon disulfide 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon tetrachloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 42 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-6 0-2'

1404090-06 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Chlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl acetate 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Methyl-2-pentanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrolein 0.01 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrylonitrile 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dichlorodifluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Iodomethane 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Isopropyl alcohol 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl tert-butyl ether 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Propylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 43 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-6 0-2'

1404090-06 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Isopropylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

sec-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,4-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3,5-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

p-Isopropyltoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Surrogate: 1,2-Dichloroethane-d4 70-130 4/23/14 4/23/14 EPA 8260B93.1 % JWG

Surrogate: Toluene-d8 70-130 4/23/14 4/23/14 EPA 8260B111 % JWG

Surrogate: 4-Bromofluorobenzene 70-130 4/23/14 4/23/14 EPA 8260B126 % JWG

Extractable Petroleum Hydrocarbons by 8015 GRO

GRO (C6-C12) 1.00 EPA 8015mg/kg 4/22/14 4/22/14ND JAW

Surrogate: a,a,a-Trifluorotoluene 70-130 4/22/14 4/22/14 EPA 8015127 % JAW

Extractable Petroleum Hydrocarbons by 8015 DRO

DRO (C10 - C20) 10.0 EPA 8015mg/kg 4/21/14 4/23/14ND ATS

Surrogate: 2-Fluorobiphenyl 40-120 4/21/14 4/23/14 EPA 801565.2 % ATS

Extractable Petroleum Hydrocarbons by 8015 ORO

ORO (C20 - C34) 10.0 EPA 8015mg/kg 4/21/14 4/23/1419.3 ATS

Semivolatile Organic Compounds by EPA Method 8270B

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 44 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-6 0-2'

1404090-06 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Phenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Chlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

3 & 4-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dimethylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,6-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Chloro-3-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4,5-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4,6-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,3,4,6-Tetrachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4,6-Dinitro-2-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Pentachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-sec-Butyl-4,6-dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Surrogate: 2-Fluorophenol 25-121 4/21/14 4/24/14 EPA 8270B58.6 % ATS

Surrogate: Phenol-d6 24-113 4/21/14 4/24/14 EPA 8270B80.2 % ATS

Surrogate: 2,4,6-Tribromophenol 19-122 4/21/14 4/24/14 EPA 8270B84.7 % ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 45 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-6 0-2'

1404090-06 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Acenaphthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Acenaphthylene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (a) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (b) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (k) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (g,h,i) perylene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (a) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroethoxy)methane 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroethyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroisopropyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-ethylhexyl)phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Bromophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Butyl benzyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Chloronaphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Chlorophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Chrysene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Dibenz (a,h) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Di-n-butyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

N-Nitrosodimethylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 46 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-6 0-2'

1404090-06 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

1,3-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,4-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2-Diphenylhydrazine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzidine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

3,3´-Dichlorobenzidine 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Diethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Dimethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,6-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Di-n-octyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Fluorene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorobutadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorocyclopentadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachloroethane 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Indeno (1,2,3-cd) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Isophorone 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Naphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Nitrobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

N-Nitrosodiphenylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 47 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-6 0-2'

1404090-06 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

N-Nitrosodi-n-propylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Phenanthrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2,4-Trichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Surrogate: Nitrobenzene-d5 23-120 4/21/14 4/24/14 EPA 8270B78.4 % ATS

Surrogate: 2-Fluorobiphenyl 30-115 4/21/14 4/24/14 EPA 8270B72.7 % ATS

Surrogate: Terphenyl-d14 18-137 4/21/14 4/24/14 EPA 8270B88.0 % ATS

Metals by EPA 6000/7000 Series Methods

Silver 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Arsenic 2.00 EPA 6010Cmg/kg 4/21/14 4/22/143.43 MWB

Barium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/1492.3 MWB

Cadmium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/140.94 MWB

Chromium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/1414.0 MWB

Mercury 0.0400 EPA 7471mg/kg 4/21/14 4/22/140.112 MWB

Lead 2.00 EPA 6010Cmg/kg 4/21/14 4/22/1467.7 MWB

Selenium 2.00 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 48 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 4-8'

1404090-07 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Volatile Organic Compounds by EPA Method 8260B

1,1,1,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,1-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromo-3-chloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromoethane (EDB) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,4-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acetone 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Benzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromodichloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromoform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 49 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 4-8'

1404090-07 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Ethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl ethyl ketone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methylene chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Naphthalene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Styrene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

tert-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Tetrachloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Toluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,4-Dichloro-2-butene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichlorofluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Xylenes (total) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Hexanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chloroethylvinyl ether 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon disulfide 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon tetrachloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 50 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 4-8'

1404090-07 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Chlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl acetate 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Methyl-2-pentanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrolein 0.01 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrylonitrile 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dichlorodifluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Iodomethane 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Isopropyl alcohol 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl tert-butyl ether 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Propylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 51 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 4-8'

1404090-07 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Isopropylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

sec-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,4-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3,5-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

p-Isopropyltoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Surrogate: 1,2-Dichloroethane-d4 70-130 4/23/14 4/23/14 EPA 8260B93.4 % JWG

Surrogate: Toluene-d8 70-130 4/23/14 4/23/14 EPA 8260B129 % JWG

Surrogate: 4-Bromofluorobenzene 70-130 4/23/14 4/23/14 EPA 8260B128 % JWG

Extractable Petroleum Hydrocarbons by 8015 GRO

GRO (C6-C12) 1.00 EPA 8015mg/kg 4/22/14 4/22/14ND JAW

Surrogate: a,a,a-Trifluorotoluene 70-130 4/22/14 4/22/14 EPA 801591.8 % JAW

Extractable Petroleum Hydrocarbons by 8015 DRO

DRO (C10 - C20) 10.0 EPA 8015mg/kg 4/21/14 4/23/14ND ATS

Surrogate: 2-Fluorobiphenyl 40-120 4/21/14 4/23/14 EPA 801562.4 % ATS

Extractable Petroleum Hydrocarbons by 8015 ORO

ORO (C20 - C34) 10.0 EPA 8015mg/kg 4/21/14 4/23/1436.7 ATS

Semivolatile Organic Compounds by EPA Method 8270B

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 52 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 4-8'

1404090-07 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Phenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Chlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

3 & 4-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dimethylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,6-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Chloro-3-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4,5-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4,6-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,3,4,6-Tetrachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4,6-Dinitro-2-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Pentachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-sec-Butyl-4,6-dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Surrogate: 2-Fluorophenol 25-121 4/21/14 4/24/14 EPA 8270B45.9 % ATS

Surrogate: Phenol-d6 24-113 4/21/14 4/24/14 EPA 8270B70.7 % ATS

Surrogate: 2,4,6-Tribromophenol 19-122 4/21/14 4/24/14 EPA 8270B72.2 % ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 53 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 4-8'

1404090-07 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Acenaphthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Acenaphthylene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (a) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.39 ATS

Benzo (b) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.46 ATS

Benzo (k) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (g,h,i) perylene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (a) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.41 ATS

Bis(2-chloroethoxy)methane 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroethyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroisopropyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-ethylhexyl)phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Bromophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Butyl benzyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Chloronaphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Chlorophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Chrysene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.46 ATS

Dibenz (a,h) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Di-n-butyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

N-Nitrosodimethylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 54 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 4-8'

1404090-07 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

1,3-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,4-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2-Diphenylhydrazine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

3,3´-Dichlorobenzidine 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzidine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Diethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Dimethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,6-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Di-n-octyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/141.16 ATS

Fluorene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorobutadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorocyclopentadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachloroethane 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Indeno (1,2,3-cd) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Isophorone 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Naphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Nitrobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

N-Nitrosodiphenylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 55 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 4-8'

1404090-07 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

N-Nitrosodi-n-propylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Phenanthrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.87 ATS

Pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/141.01 ATS

1,2,4-Trichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Surrogate: Nitrobenzene-d5 23-120 4/21/14 4/24/14 EPA 8270B71.9 % ATS

Surrogate: 2-Fluorobiphenyl 30-115 4/21/14 4/24/14 EPA 8270B66.0 % ATS

Surrogate: Terphenyl-d14 18-137 4/21/14 4/24/14 EPA 8270B77.7 % ATS

Metals by EPA 6000/7000 Series Methods

Silver 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Arsenic 2.00 EPA 6010Cmg/kg 4/21/14 4/22/1411.0 MWB

Barium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14128 MWB

Cadmium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/140.57 MWB

Chromium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/1412.8 MWB

Mercury 0.800 EPA 7471mg/kg 4/23/14 4/24/1413.6 MWB

Lead 20.0 EPA 6010Cmg/kg 4/21/14 4/22/14503 MWB

Selenium 2.00 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 56 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 16-20'

1404090-08 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Volatile Organic Compounds by EPA Method 8260B

1,1,1,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,1-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1,2-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromo-3-chloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dibromoethane (EDB) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,3-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,4-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acetone 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Benzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromodichloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromoform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 57 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 16-20'

1404090-08 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloroform 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Chloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Ethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl ethyl ketone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methylene chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Naphthalene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Styrene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

tert-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Tetrachloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Toluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,4-Dichloro-2-butene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Trichlorofluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Xylenes (total) 0.005 EPA 8260Bmg/kg 4/23/14 4/23/140.01 JWG

2-Hexanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chloroethylvinyl ether 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon disulfide 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Carbon tetrachloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 58 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 16-20'

1404090-08 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Chlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

cis-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dibromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl acetate 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Vinyl chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

2-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

4-Methyl-2-pentanone 0.02 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrolein 0.01 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Acrylonitrile 0.05 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Dichlorodifluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Iodomethane 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Isopropyl alcohol 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Methyl tert-butyl ether 0.002 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

trans-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,1-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

n-Propylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/140.006 JWG

1,3-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 59 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 16-20'

1404090-08 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Isopropylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Bromobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

sec-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,3-Trichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

1,2,4-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/140.01 JWG

1,3,5-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

p-Isopropyltoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/23/14ND JWG

Surrogate: 1,2-Dichloroethane-d4 70-130 4/23/14 4/23/14 EPA 8260B102 % JWG

Surrogate: Toluene-d8 70-130 4/23/14 4/23/14 EPA 8260B106 % JWG

Surrogate: 4-Bromofluorobenzene 70-130 4/23/14 4/23/14 EPA 8260B106 % JWG

Extractable Petroleum Hydrocarbons by 8015 GRO

GRO (C6-C12) 1.00 EPA 8015mg/kg 4/22/14 4/22/14ND JAW

Surrogate: a,a,a-Trifluorotoluene 70-130 4/22/14 4/22/14 EPA 8015123 % JAW

Extractable Petroleum Hydrocarbons by 8015 DRO

DRO (C10 - C20) 10.0 EPA 8015mg/kg 4/21/14 4/22/14175 ATS

Surrogate: 2-Fluorobiphenyl 40-120 4/21/14 4/22/14 EPA 801567.0 % ATS

Extractable Petroleum Hydrocarbons by 8015 ORO

ORO (C20 - C34) 10.0 EPA 8015mg/kg 4/21/14 4/22/14ND ATS

Semivolatile Organic Compounds by EPA Method 8270B

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 60 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 16-20'

1404090-08 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Phenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-Chlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

3 & 4-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4-Dimethylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,6-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4-Chloro-3-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4,5-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4,6-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4-Dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,3,4,6-Tetrachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4,6-Dinitro-2-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Pentachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-sec-Butyl-4,6-dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Surrogate: 2-Fluorophenol 25-121 4/21/14 4/23/14 EPA 8270B39.8 % ATS

Surrogate: Phenol-d6 24-113 4/21/14 4/23/14 EPA 8270B59.5 % ATS

Surrogate: 2,4,6-Tribromophenol 19-122 4/21/14 4/23/14 EPA 8270B82.2 % ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 61 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 16-20'

1404090-08 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Acenaphthene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Acenaphthylene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (a) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (b) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (k) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (g,h,i) perylene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (a) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Bis(2-chloroethoxy)methane 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Bis(2-chloroethyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Bis(2-chloroisopropyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Bis(2-ethylhexyl)phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4-Bromophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Butyl benzyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-Chloronaphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4-Chlorophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Chrysene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Dibenz (a,h) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Di-n-butyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

1,2-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

N-Nitrosodimethylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 62 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 16-20'

1404090-08 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

1,3-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

1,4-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

1,2-Diphenylhydrazine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzidine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

3,3´-Dichlorobenzidine 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Diethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Dimethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,6-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Di-n-octyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Fluorene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Hexachlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Hexachlorobutadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Hexachlorocyclopentadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Hexachloroethane 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Indeno (1,2,3-cd) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Isophorone 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Naphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Nitrobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

N-Nitrosodiphenylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 63 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7 16-20'

1404090-08 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

N-Nitrosodi-n-propylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Phenanthrene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

1,2,4-Trichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Surrogate: Nitrobenzene-d5 23-120 4/21/14 4/23/14 EPA 8270B45.9 % ATS

Surrogate: 2-Fluorobiphenyl 30-115 4/21/14 4/23/14 EPA 8270B61.9 % ATS

Surrogate: Terphenyl-d14 18-137 4/21/14 4/23/14 EPA 8270B74.2 % ATS

Metals by EPA 6000/7000 Series Methods

Silver 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Arsenic 2.00 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Barium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14146 MWB

Cadmium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Chromium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/145.53 MWB

Mercury 0.0400 EPA 7471mg/kg 4/21/14 4/22/14ND MWB

Lead 2.00 EPA 6010Cmg/kg 4/21/14 4/22/142.91 MWB

Selenium 2.00 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 64 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 0-4'

1404090-09 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Volatile Organic Compounds by EPA Method 8260B

1,1,1,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,1,1-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,1,2,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,1,2-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,1-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,1-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2,3-Trichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2-Dibromo-3-chloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2-Dibromoethane (EDB) 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,3-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,4-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Acetone 0.05 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Benzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Bromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Bromodichloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Bromoform 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 65 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 0-4'

1404090-09 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Chloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Chloroform 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Chloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Ethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Methyl ethyl ketone 0.02 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Methylene chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Naphthalene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Styrene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

tert-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Tetrachloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Toluene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

trans-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

trans-1,4-Dichloro-2-butene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Trichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Trichlorofluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Xylenes (total) 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

2-Hexanone 0.02 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

2-Chloroethylvinyl ether 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Carbon disulfide 0.002 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Carbon tetrachloride 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 66 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 0-4'

1404090-09 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Chlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

cis-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

cis-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Dibromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Dibromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Vinyl acetate 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Vinyl chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

2-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

4-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

4-Methyl-2-pentanone 0.02 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Acrolein 0.01 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Acrylonitrile 0.05 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Dichlorodifluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Iodomethane 0.002 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Isopropyl alcohol 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Methyl tert-butyl ether 0.002 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

n-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

trans-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,1-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

n-Propylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,3-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 67 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 0-4'

1404090-09 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Isopropylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Bromobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

sec-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2,3-Trichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2,4-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,3,5-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

p-Isopropyltoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Surrogate: 1,2-Dichloroethane-d4 70-130 4/23/14 4/24/14 EPA 8260B92.4 % JWG

Surrogate: Toluene-d8 70-130 4/23/14 4/24/14 EPA 8260B122 % JWG

Surrogate: 4-Bromofluorobenzene 70-130 4/23/14 4/24/14 Sr-VEPA 8260B143 % JWG

Extractable Petroleum Hydrocarbons by 8015 GRO

GRO (C6-C12) 1.00 EPA 8015mg/kg 4/22/14 4/22/14ND JAW

Surrogate: a,a,a-Trifluorotoluene 70-130 4/22/14 4/22/14 EPA 8015122 % JAW

Extractable Petroleum Hydrocarbons by 8015 DRO

DRO (C10 - C20) 10.0 EPA 8015mg/kg 4/21/14 4/23/1417.0 ATS

Surrogate: 2-Fluorobiphenyl 40-120 4/21/14 4/23/14 EPA 801572.6 % ATS

Extractable Petroleum Hydrocarbons by 8015 ORO

ORO (C20 - C34) 10.0 EPA 8015mg/kg 4/21/14 4/23/1465.7 ATS

Semivolatile Organic Compounds by EPA Method 8270B

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 68 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 0-4'

1404090-09 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Phenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Chlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

3 & 4-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dimethylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,6-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Chloro-3-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4,5-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4,6-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,3,4,6-Tetrachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4,6-Dinitro-2-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Pentachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-sec-Butyl-4,6-dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Surrogate: 2-Fluorophenol 25-121 4/21/14 4/24/14 EPA 8270B54.6 % ATS

Surrogate: Phenol-d6 24-113 4/21/14 4/24/14 EPA 8270B75.4 % ATS

Surrogate: 2,4,6-Tribromophenol 19-122 4/21/14 4/24/14 EPA 8270B70.7 % ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 69 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 0-4'

1404090-09 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Acenaphthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Acenaphthylene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (a) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (b) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (k) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (g,h,i) perylene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzo (a) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroethoxy)methane 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroethyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-chloroisopropyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Bis(2-ethylhexyl)phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Bromophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Butyl benzyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2-Chloronaphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

4-Chlorophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Chrysene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Dibenz (a,h) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Di-n-butyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

N-Nitrosodimethylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 70 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 0-4'

1404090-09 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

1,3-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,4-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

3,3´-Dichlorobenzidine 0.66 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2-Diphenylhydrazine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Benzidine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Diethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Dimethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,4-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

2,6-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Di-n-octyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Fluorene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorobutadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachlorocyclopentadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Hexachloroethane 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Indeno (1,2,3-cd) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Isophorone 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Naphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/140.39 ATS

Nitrobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

N-Nitrosodiphenylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 71 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 0-4'

1404090-09 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

N-Nitrosodi-n-propylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Phenanthrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

1,2,4-Trichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/24/14ND ATS

Surrogate: Nitrobenzene-d5 23-120 4/21/14 4/24/14 EPA 8270B82.4 % ATS

Surrogate: 2-Fluorobiphenyl 30-115 4/21/14 4/24/14 EPA 8270B75.1 % ATS

Surrogate: Terphenyl-d14 18-137 4/21/14 4/24/14 EPA 8270B87.8 % ATS

Metals by EPA 6000/7000 Series Methods

Silver 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Arsenic 2.00 EPA 6010Cmg/kg 4/21/14 4/22/1419.7 MWB

Barium 5.00 EPA 6010Cmg/kg 4/21/14 4/22/14265 MWB

Cadmium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/140.66 MWB

Chromium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/146.83 MWB

Mercury 0.0400 EPA 7471mg/kg 4/21/14 4/22/140.114 MWB

Lead 20.0 EPA 6010Cmg/kg 4/21/14 4/22/14352 MWB

Selenium 2.00 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 72 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 8-12'

1404090-10 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Volatile Organic Compounds by EPA Method 8260B

1,1,1,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,1,1-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,1,2,2-Tetrachloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,1,2-Trichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,1-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,1-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2,3-Trichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2-Dibromo-3-chloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2-Dibromoethane (EDB) 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2-Dichloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,3-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,4-Dichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Acetone 0.05 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Benzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Bromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Bromodichloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Bromoform 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 73 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 8-12'

1404090-10 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Chloroethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Chloroform 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Chloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Ethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Methyl ethyl ketone 0.02 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Methylene chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Naphthalene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Styrene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

tert-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Tetrachloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Toluene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

trans-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

trans-1,4-Dichloro-2-butene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Trichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Trichlorofluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Xylenes (total) 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

2-Hexanone 0.02 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

2-Chloroethylvinyl ether 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Carbon disulfide 0.002 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Carbon tetrachloride 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 74 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 8-12'

1404090-10 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Chlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

cis-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

cis-1,3-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Dibromochloromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Dibromomethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Vinyl acetate 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Vinyl chloride 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

2-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

4-Chlorotoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

4-Methyl-2-pentanone 0.02 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Acrolein 0.01 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Acrylonitrile 0.05 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Dichlorodifluoromethane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Iodomethane 0.002 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Isopropyl alcohol 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Methyl tert-butyl ether 0.002 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

n-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

trans-1,2-Dichloroethene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,1-Dichloropropene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

n-Propylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,3-Dichloropropane 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 75 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 8-12'

1404090-10 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Isopropylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Bromobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

sec-Butylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2,3-Trichlorobenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,2,4-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

1,3,5-Trimethylbenzene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

p-Isopropyltoluene 0.005 EPA 8260Bmg/kg 4/23/14 4/24/14ND JWG

Surrogate: 1,2-Dichloroethane-d4 70-130 4/23/14 4/24/14 EPA 8260B91.1 % JWG

Surrogate: Toluene-d8 70-130 4/23/14 4/24/14 EPA 8260B109 % JWG

Surrogate: 4-Bromofluorobenzene 70-130 4/23/14 4/24/14 EPA 8260B110 % JWG

Extractable Petroleum Hydrocarbons by 8015 GRO

GRO (C6-C12) 1.00 EPA 8015mg/kg 4/22/14 4/22/14ND JAW

Surrogate: a,a,a-Trifluorotoluene 70-130 4/22/14 4/22/14 EPA 8015122 % JAW

Extractable Petroleum Hydrocarbons by 8015 DRO

DRO (C10 - C20) 10.0 EPA 8015mg/kg 4/21/14 4/22/14ND ATS

Surrogate: 2-Fluorobiphenyl 40-120 4/21/14 4/22/14 EPA 801559.5 % ATS

Extractable Petroleum Hydrocarbons by 8015 ORO

ORO (C20 - C34) 10.0 EPA 8015mg/kg 4/21/14 4/22/14ND ATS

Semivolatile Organic Compounds by EPA Method 8270B

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 76 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 8-12'

1404090-10 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Phenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-Chlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

3 & 4-Methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4-Dimethylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,6-Dichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4-Chloro-3-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4,5-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4,6-Trichlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4-Dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4-Nitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,3,4,6-Tetrachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4,6-Dinitro-2-methylphenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Pentachlorophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-sec-Butyl-4,6-dinitrophenol 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Surrogate: 2-Fluorophenol 25-121 4/21/14 4/23/14 EPA 8270B53.1 % ATS

Surrogate: Phenol-d6 24-113 4/21/14 4/23/14 EPA 8270B78.4 % ATS

Surrogate: 2,4,6-Tribromophenol 19-122 4/21/14 4/23/14 EPA 8270B70.5 % ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 77 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 8-12'

1404090-10 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Acenaphthene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Acenaphthylene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (a) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (b) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (k) fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (g,h,i) perylene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzo (a) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Bis(2-chloroethoxy)methane 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Bis(2-chloroethyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Bis(2-chloroisopropyl)ether 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Bis(2-ethylhexyl)phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4-Bromophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Butyl benzyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2-Chloronaphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

4-Chlorophenyl phenyl ether 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Chrysene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Dibenz (a,h) anthracene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Di-n-butyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

1,2-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

N-Nitrosodimethylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 78 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 8-12'

1404090-10 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

1,3-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

1,4-Dichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

3,3´-Dichlorobenzidine 0.66 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

1,2-Diphenylhydrazine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Benzidine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Diethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Dimethyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,4-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

2,6-Dinitrotoluene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Di-n-octyl phthalate 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Fluoranthene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Fluorene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Hexachlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Hexachlorobutadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Hexachlorocyclopentadiene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Hexachloroethane 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Indeno (1,2,3-cd) pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Isophorone 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Naphthalene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Nitrobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

N-Nitrosodiphenylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 79 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8 8-12'

1404090-10 (Soil)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

N-Nitrosodi-n-propylamine 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Phenanthrene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Pyrene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

1,2,4-Trichlorobenzene 0.33 EPA 8270Bmg/kg 4/21/14 4/23/14ND ATS

Surrogate: Nitrobenzene-d5 23-120 4/21/14 4/23/14 EPA 8270B70.4 % ATS

Surrogate: 2-Fluorobiphenyl 30-115 4/21/14 4/23/14 EPA 8270B64.9 % ATS

Surrogate: Terphenyl-d14 18-137 4/21/14 4/23/14 EPA 8270B90.6 % ATS

Metals by EPA 6000/7000 Series Methods

Silver 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Arsenic 2.00 EPA 6010Cmg/kg 4/21/14 4/22/143.32 MWB

Barium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14147 MWB

Cadmium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Chromium 0.50 EPA 6010Cmg/kg 4/21/14 4/22/148.80 MWB

Mercury 0.0400 EPA 7471mg/kg 4/21/14 4/22/14ND MWB

Lead 2.00 EPA 6010Cmg/kg 4/21/14 4/22/145.67 MWB

Selenium 2.00 EPA 6010Cmg/kg 4/21/14 4/22/14ND MWB

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 80 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7/MW-2

1404090-11 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Volatile Organic Compounds by EPA Method 8260

1,1,1,2-Tetrachloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1,1-Trichloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1,2,2-Tetrachloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1,2-Trichloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1-Dichloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1-Dichloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2,3-Trichloropropane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2,4-Trimethylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dibromo-3-chloropropane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dibromoethane (EDB) 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dichlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

trans-1,2-Dichloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dichloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dichloropropane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,3,5-Trimethylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,3-Dichlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,4-Dichlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Acetone 0.02 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Benzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 81 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7/MW-2

1404090-11 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bromochloromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Bromodichloromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Bromoform 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1-Dichloropropene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Bromomethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Chloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Chloroform 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Chloromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Ethylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Methyl ethyl ketone 0.01 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Methylene chloride 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Naphthalene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Styrene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

tert-Butylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Tetrachloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Toluene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

trans-1,3-Dichloropropene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

trans-1,4-Dichloro-2-butene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Trichloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Trichlorofluoromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Xylenes (total) 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 82 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7/MW-2

1404090-11 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

2-Hexanone 0.01 EPA 8260mg/L 4/23/14 4/24/14ND JWG

2-Chloroethylvinyl ether 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Carbon disulfide 0.001 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Carbon tetrachloride 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,3-Dichloropropane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Chlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

cis-1,2-Dichloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

cis-1,3-Dichloropropene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Dibromochloromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Dibromomethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Vinyl acetate 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Vinyl chloride 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

2-Chlorotoluene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

4-Chlorotoluene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

4-Methyl-2-pentanone 0.01 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Acrolein 0.10 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Bromobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Acrylonitrile 0.02 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Dichlorodifluoromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Iodomethane 0.001 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Isopropylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/140.005 JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 83 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7/MW-2

1404090-11 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Methyl tert-butyl ether 0.001 EPA 8260mg/L 4/23/14 4/24/14ND JWG

n-Butylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

n-Propylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/140.006 JWG

p-Isopropyltoluene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

sec-Butylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/140.005 JWG

1,2,3-Trichlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Surrogate: 1,2-Dichloroethane-d4 70-130 4/23/14 4/24/14 EPA 826081.7 % JWG

Surrogate: Toluene-d8 70-130 4/23/14 4/24/14 EPA 8260101 % JWG

Surrogate: 4-Bromofluorobenzene 70-130 4/23/14 4/24/14 EPA 8260102 % JWG

Semivolatile Organic Compounds by EPA Method 8270B

Phenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2-Chlorophenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2-Methylphenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

3 & 4-Methylphenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2-Nitrophenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,4-Dimethylphenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,4-Dichlorophenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,6-Dichlorophenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

4-Chloro-3-methylphenol 0.020 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,4,5-Trichlorophenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 84 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7/MW-2

1404090-11 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

2,4,6-Trichlorophenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,4-Dinitrophenol 0.050 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

4-Nitrophenol 0.050 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,3,4,6-Tetrachlorophenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

4,6-Dinitro-2-methylphenol 0.050 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Pentachlorophenol 0.050 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2-sec-Butyl-4,6-dinitrophenol 0.020 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Surrogate: 2-Fluorophenol 21-100 4/18/14 4/22/14 EPA 8270B43.1 % ATS

Surrogate: Phenol-d6 10-94 4/18/14 4/22/14 EPA 8270B32.3 % ATS

Surrogate: 2,4,6-Tribromophenol 10-123 4/18/14 4/22/14 EPA 8270B81.7 % ATS

Acenaphthene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Acenaphthylene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Anthracene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Benzo (a) anthracene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Benzo (b) fluoranthene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Benzo (k) fluoranthene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Benzo (g,h,i) perylene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Benzo (a) pyrene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Bis(2-chloroethoxy)methane 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Bis(2-chloroethyl)ether 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Bis(2-chloroisopropyl)ether 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 85 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7/MW-2

1404090-11 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bis(2-ethylhexyl)phthalate 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

4-Bromophenyl phenyl ether 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Butyl benzyl phthalate 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2-Chloronaphthalene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

4-Chlorophenyl phenyl ether 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Chrysene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Dibenz (a,h) anthracene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Di-n-butyl phthalate 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

1,2-Dichlorobenzene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

1,3-Dichlorobenzene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

1,4-Dichlorobenzene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

3,3´-Dichlorobenzidine 0.020 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Benzidine 0.050 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

N-Nitrosodimethylamine 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

1,2-Diphenylhydrazine 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Diethyl phthalate 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Dimethyl phthalate 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,4-Dinitrotoluene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,6-Dinitrotoluene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Di-n-octyl phthalate 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Fluoranthene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 86 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7/MW-2

1404090-11 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Fluorene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Hexachlorobenzene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Hexachlorobutadiene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Hexachlorocyclopentadiene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Hexachloroethane 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Indeno (1,2,3-cd) pyrene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Isophorone 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Naphthalene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Nitrobenzene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

N-Nitrosodiphenylamine 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

N-Nitrosodi-n-propylamine 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Phenanthrene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Pyrene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

1,2,4-Trichlorobenzene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Surrogate: Nitrobenzene-d5 35-114 4/18/14 4/22/14 EPA 8270B94.3 % ATS

Surrogate: 2-Fluorobiphenyl 43-116 4/18/14 4/22/14 EPA 8270B85.1 % ATS

Surrogate: Terphenyl-d14 33-141 4/18/14 4/22/14 EPA 8270B95.3 % ATS

Metals (Dissolved) by EPA 200 Series Methods

Silver 0.028 EPA 200.7mg/L 4/24/14 4/24/14ND MWB

Arsenic 0.100 EPA 200.7mg/L 4/23/14 4/24/14ND MWB

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 87 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-7/MW-2

1404090-11 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Barium 0.025 EPA 200.7mg/L 4/23/14 4/24/140.271 MWB

Cadmium 0.025 EPA 200.7mg/L 4/23/14 4/24/14ND MWB

Chromium 0.025 EPA 200.7mg/L 4/23/14 4/24/14ND MWB

Mercury 0.0002 EPA 245.1mg/L 4/23/14 4/24/14ND MWB

Lead 0.100 EPA 200.7mg/L 4/23/14 4/24/14ND MWB

Selenium 0.100 EPA 200.7mg/L 4/23/14 4/24/14ND MWB

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 88 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8/MW-1

1404090-12 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Volatile Organic Compounds by EPA Method 8260

1,1,1,2-Tetrachloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1,1-Trichloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1,2,2-Tetrachloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1,2-Trichloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1-Dichloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1-Dichloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2,3-Trichloropropane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2,4-Trimethylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dibromo-3-chloropropane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dibromoethane (EDB) 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dichlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

trans-1,2-Dichloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dichloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dichloropropane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,3,5-Trimethylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,3-Dichlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,4-Dichlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Acetone 0.02 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Benzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 89 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8/MW-1

1404090-12 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bromochloromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Bromodichloromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Bromoform 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1-Dichloropropene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Bromomethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Chloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Chloroform 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Chloromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Ethylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Methyl ethyl ketone 0.01 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Methylene chloride 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Naphthalene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Styrene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

tert-Butylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Tetrachloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Toluene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

trans-1,3-Dichloropropene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

trans-1,4-Dichloro-2-butene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Trichloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Trichlorofluoromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Xylenes (total) 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 90 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8/MW-1

1404090-12 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

2-Hexanone 0.01 EPA 8260mg/L 4/23/14 4/24/14ND JWG

2-Chloroethylvinyl ether 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Carbon disulfide 0.001 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Carbon tetrachloride 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,3-Dichloropropane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Chlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

cis-1,2-Dichloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

cis-1,3-Dichloropropene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Dibromochloromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Dibromomethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Vinyl acetate 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Vinyl chloride 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

2-Chlorotoluene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

4-Chlorotoluene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

4-Methyl-2-pentanone 0.01 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Acrolein 0.10 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Bromobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Acrylonitrile 0.02 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Dichlorodifluoromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Iodomethane 0.001 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Isopropylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 91 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8/MW-1

1404090-12 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Methyl tert-butyl ether 0.001 EPA 8260mg/L 4/23/14 4/24/14ND JWG

n-Butylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

n-Propylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

p-Isopropyltoluene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

sec-Butylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2,3-Trichlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Surrogate: 1,2-Dichloroethane-d4 70-130 4/23/14 4/24/14 EPA 826084.0 % JWG

Surrogate: Toluene-d8 70-130 4/23/14 4/24/14 EPA 8260110 % JWG

Surrogate: 4-Bromofluorobenzene 70-130 4/23/14 4/24/14 EPA 8260108 % JWG

Semivolatile Organic Compounds by EPA Method 8270B

Phenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2-Chlorophenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2-Methylphenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

3 & 4-Methylphenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2-Nitrophenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,4-Dimethylphenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,4-Dichlorophenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,6-Dichlorophenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

4-Chloro-3-methylphenol 0.020 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,4,5-Trichlorophenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 92 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8/MW-1

1404090-12 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

2,4,6-Trichlorophenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,4-Dinitrophenol 0.050 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

4-Nitrophenol 0.050 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,3,4,6-Tetrachlorophenol 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

4,6-Dinitro-2-methylphenol 0.050 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Pentachlorophenol 0.050 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2-sec-Butyl-4,6-dinitrophenol 0.020 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Surrogate: 2-Fluorophenol 21-100 4/18/14 4/22/14 EPA 8270B42.4 % ATS

Surrogate: Phenol-d6 10-94 4/18/14 4/22/14 EPA 8270B32.1 % ATS

Surrogate: 2,4,6-Tribromophenol 10-123 4/18/14 4/22/14 EPA 8270B80.0 % ATS

Acenaphthene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Acenaphthylene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Anthracene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Benzo (a) anthracene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Benzo (b) fluoranthene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Benzo (k) fluoranthene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Benzo (g,h,i) perylene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Benzo (a) pyrene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Bis(2-chloroethoxy)methane 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Bis(2-chloroethyl)ether 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Bis(2-chloroisopropyl)ether 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 93 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8/MW-1

1404090-12 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bis(2-ethylhexyl)phthalate 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

4-Bromophenyl phenyl ether 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Butyl benzyl phthalate 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2-Chloronaphthalene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

4-Chlorophenyl phenyl ether 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Chrysene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Dibenz (a,h) anthracene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Di-n-butyl phthalate 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

1,2-Dichlorobenzene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

1,3-Dichlorobenzene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

1,4-Dichlorobenzene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

3,3´-Dichlorobenzidine 0.020 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

N-Nitrosodimethylamine 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Benzidine 0.050 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

1,2-Diphenylhydrazine 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Diethyl phthalate 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Dimethyl phthalate 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,4-Dinitrotoluene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

2,6-Dinitrotoluene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Di-n-octyl phthalate 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Fluoranthene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 94 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8/MW-1

1404090-12 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Fluorene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Hexachlorobenzene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Hexachlorobutadiene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Hexachlorocyclopentadiene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Hexachloroethane 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Indeno (1,2,3-cd) pyrene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Isophorone 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Naphthalene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Nitrobenzene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

N-Nitrosodiphenylamine 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

N-Nitrosodi-n-propylamine 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Phenanthrene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Pyrene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

1,2,4-Trichlorobenzene 0.010 EPA 8270Bmg/L 4/18/14 4/22/14ND ATS

Surrogate: Nitrobenzene-d5 35-114 4/18/14 4/22/14 EPA 8270B90.2 % ATS

Surrogate: 2-Fluorobiphenyl 43-116 4/18/14 4/22/14 EPA 8270B83.0 % ATS

Surrogate: Terphenyl-d14 33-141 4/18/14 4/22/14 EPA 8270B91.3 % ATS

Metals (Dissolved) by EPA 200 Series Methods

Silver 0.028 EPA 200.7mg/L 4/24/14 4/24/14ND MWB

Arsenic 0.100 EPA 200.7mg/L 4/23/14 4/24/14ND MWB

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 95 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

SB-8/MW-1

1404090-12 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Barium 0.025 EPA 200.7mg/L 4/23/14 4/24/140.146 MWB

Cadmium 0.025 EPA 200.7mg/L 4/23/14 4/24/14ND MWB

Chromium 0.025 EPA 200.7mg/L 4/23/14 4/24/14ND MWB

Mercury 0.0002 EPA 245.1mg/L 4/23/14 4/24/14ND MWB

Lead 0.100 EPA 200.7mg/L 4/23/14 4/24/14ND MWB

Selenium 0.100 EPA 200.7mg/L 4/23/14 4/24/14ND MWB

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 96 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

TRIP BLANK

1404090-13 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Volatile Organic Compounds by EPA Method 8260

1,1,1,2-Tetrachloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1,1-Trichloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1,2,2-Tetrachloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1,2-Trichloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1-Dichloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1-Dichloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2,3-Trichloropropane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2,4-Trimethylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dibromo-3-chloropropane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dibromoethane (EDB) 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dichlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

trans-1,2-Dichloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dichloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2-Dichloropropane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,3,5-Trimethylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,3-Dichlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,4-Dichlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Acetone 0.02 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Benzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 97 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

TRIP BLANK

1404090-13 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Bromochloromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Bromodichloromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Bromoform 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,1-Dichloropropene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Bromomethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Chloroethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Chloroform 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Chloromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Ethylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Methyl ethyl ketone 0.01 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Methylene chloride 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Naphthalene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Styrene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

tert-Butylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Tetrachloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Toluene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

trans-1,3-Dichloropropene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

trans-1,4-Dichloro-2-butene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Trichloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Trichlorofluoromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Xylenes (total) 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 98 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

TRIP BLANK

1404090-13 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

2-Hexanone 0.01 EPA 8260mg/L 4/23/14 4/24/14ND JWG

2-Chloroethylvinyl ether 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Carbon disulfide 0.001 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Carbon tetrachloride 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,3-Dichloropropane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Chlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

cis-1,2-Dichloroethene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

cis-1,3-Dichloropropene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Dibromochloromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Dibromomethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Vinyl acetate 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Vinyl chloride 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

2-Chlorotoluene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

4-Chlorotoluene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

4-Methyl-2-pentanone 0.01 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Acrolein 0.10 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Bromobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Acrylonitrile 0.02 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Dichlorodifluoromethane 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Iodomethane 0.001 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Isopropylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 99 of 100

Project:

P.O. Number:

Project Manager:

Resource International

6350 Presidential Gateway

[none]

Steven Sawyer

W-11-138

Columbus, OH 43231

Date Reported: 5/1/14

TRIP BLANK

1404090-13 (Water)

Client Sample I.D.:

AALI Sample I.D.:

ANALYTICAL RESULTS

Date Received:

Date Collected: 4/17/14

4/18/14

Analyte

Reporting

Notes AnalystMethodAnalyzedPreparedLimitUnitsResult

Methyl tert-butyl ether 0.001 EPA 8260mg/L 4/23/14 4/24/14ND JWG

n-Butylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

n-Propylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

p-Isopropyltoluene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

sec-Butylbenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

1,2,3-Trichlorobenzene 0.002 EPA 8260mg/L 4/23/14 4/24/14ND JWG

Surrogate: 1,2-Dichloroethane-d4 70-130 4/23/14 4/24/14 EPA 8260102 % JWG

Surrogate: Toluene-d8 70-130 4/23/14 4/24/14 EPA 8260110 % JWG

Surrogate: 4-Bromofluorobenzene 70-130 4/23/14 4/24/14 EPA 8260104 % JWG

Notes and Definitions

Sr-V This surrogate was outside the QC limits, but the data was accepted because the other 2 surrogates were within QC limits.

Analyte NOT DETECTED at or above the reporting limitND

Analyte DETECTEDDET

Advanced Analytics Laboratories, Inc.

L. Eve Karnitis, President Page 100 of 100

APPENDIX V

PHOTOGRAPHS

PHOTO LOG

Project Name: EMH&T

Location: Webster Street Bridge

Project No.: W-11-138

Photo No. 1

Date: 4-17-14

Sample No. SB-8/MW-1

Description: Soil boring SB-8 and monitoring well MW-1.

Project Name: EMH&T

Location: Webster Street Bridge

Project No.: W-11-138

Photo No. 2

Date: 4-17-14

Sample No. SB-7/MW-2

Description: Soil boring SB-7 and monitoring well MW-2.

PHOTO LOG

Project Name: EMH&T

Location: Webster Street Bridge

Project No.: W-11-138

Photo No. 3

Date: 4-17-14

Sample No. Soil boring SB-8

Description: Cinders observed in the 0-5 feet depths.

Project Name: EMH&T

Location: Webster Street Bridge

Project No.: W-11-138

Photo No. 4

Date: 4-17-14

Sample No. SB-6

Description: Hand auguring borings underneath the Webster Street Bridge.

PHOTO LOG

Project Name: EMH&T

Location: Webster Street Bridge

Project No.: W-11-138

Photo No. 5

Date: 4-17-14

Sample No. SB-1, SB-3 and SB-5

Description: Soil boring locations under the Webster Street Bridge.

Project Name: EMH&T

Location: Webster Street Bridge

Project No.: W-11-138

Photo No. 6

Date: 4-17-14

Sample No. SB-1

Description: Soil boring SB-1 being hand augured under the Mad River.

]

PHOTO LOG

Project Name: EMH&T

Location: Webster Street Bridge

Project No.: W-11-138

Photo No. 7

Date: 4-17-14

Sample No. SB-2

Description: Sand and gravel being collected from the hand auger.

Project Name: EMH&T

Location: Webster Street Bridge

Project No.: W-11-138

Photo No. 8

Date: 4-17-14

Sample No. SB-8

Description: Developing and collecting groundwater samples from monitoring well MW-1.


Recommended