W.C. REED PLAYFIELD CLEVELAND, CUYAHOGA COUNTY, OHIO

DATA VALIDATION REPORT Date: December 12, 2013 Laboratory: ALS Environmental (ALS), Holland, Michigan Laboratory Project #: 1312188 Data Validation Performed By: Lisa Graczyk, Weston Solutions, Inc. (WESTON®) Superfund Technical Assessment and Response Team (START) Weston Work Order #: 20405.012.001.2102.00 This data validation report has been prepared by WESTON START under the START III Region V contract. This report documents the data validation for 21 soil samples collected for the W.C. Reed Playfield Site that were analyzed for the following parameters and U.S. Environmental Protection Agency methods:

Polynuclear Aromatic Hydrocarbons (PAH) by SW-846 Method 8270

A level II data package was requested from ALS. The data validation was conducted in general accordance with the EPA “Contract Laboratory Program National Functional Guidance for Superfund Organic Methods Data Review” dated June 2008 and “Contract Laboratory Program National Functional Guidelines for Inorganic Superfund Data Review” dated January 2010. The Attachment contains the results summary sheets with any hand-written qualifiers applied during data validation.

Data Validation Report W.C. Reed Playfield Site ALS Environmental Laboratory Project #: 1312188 PAHs by SW-846 METHOD 8270C 1. Samples

The following table summarizes the samples for which this data validation is being conducted.

Samples Lab ID Matrix Date Collected

Date Analyzed

WCR-008-27-062-FY6 1312188-01 Soil 12/3/2013 12/6/2013 WCR-008-27-062-FY24 1312188-02 Soil 12/3/2013 12/6/2013 WCR-008-27-062-BY6 1312188-03 Soil 12/3/2013 12/6/2013 WCR-008-27-062-BY24 1312188-04 Soil 12/3/2013 12/6/2013 WCR-008-27-060-BY6 1312188-05 Soil 12/3/2013 12/6/2013 WCR-008-27-060-BY24 1312188-06 Soil 12/3/2013 12/6/2013 WCR-008-27-059-SY6 1312188-07 Soil 12/3/2013 12/6/2013 WCR-008-27-059-SY24 1312188-08 Soil 12/3/2013 12/6/2013 WCR-008-27-059-BY6 1312188-09 Soil 12/3/2013 12/6/2013 WCR-008-27-059-BY24 1312188-10 Soil 12/3/2013 12/6/2013 WCR-008-26-058-BY6 1312188-11 Soil 12/3/2013 12/6/2013 WCR-008-26-058-BY24 1312188-12 Soil 12/3/2013 12/6/2013 WCR-008-26-057-6 1312188-13 Soil 12/3/2013 12/6/2013 WCR-008-26-057-24 1312188-14 Soil 12/3/2013 12/9/2013 WCR-008-26-062-6 1312188-15 Soil 12/3/2013 12/6/2013 WCR-008-26-062-FD6 1312188-16 Soil 12/3/2013 12/10/2013 WCR-008-26-062-24 1312188-17 Soil 12/3/2013 12/9/2013 WCR-008-26-034-BY6 1312188-18 Soil 12/3/2013 12/9/2013 WCR-008-26-034-BY24 1312188-19 Soil 12/3/2013 12/9/2013 WCR-008-26-032-BY6 1312188-20 Soil 12/3/2013 12/10/2013 WCR-008-26-032-BY24 1312188-21 Soil 12/3/2013 12/10/2013

2. Holding Times

The samples were analyzed within the required holding time limit of 14 days from sample collection to extraction and 40 days from extraction to analysis.

3. Blanks

Method blanks were analyzed with the PAH analyses. The method blanks contained no detections of target compound above the reporting limits.

Data Validation Report W.C. Reed Playfield Site ALS Environmental Laboratory Project #: 1312188 4. Surrogate Results

The surrogate recovery results were within the laboratory-established quality control (QC) limits except for as follows. In a few instances, one of the three surrogates was outside QC limits. No qualifications are required for one surrogate being outside QC limits.

5. Laboratory Control Sample (LCS) Results

The LCS recoveries were within laboratory QC limits.

6. Matrix Spike (MS) and Matrix Spike Duplicate (MSD) Results

A site-specific MS and MSD were not analyzed with this work order for SVOCs; therefore, matrix interferences could not be evaluated using MS/MSDs. For the MS and MSDs that were analyzed, the percent recoveries and relative percent differences (RPD) were with QC limits.

7. Field Duplicate Results

Sample WCR-008-26-062-FD6 is a field duplicate of sample WCR-008-26-062-6. RPDs were calculated for detected PAHs. RPDs ranged from 9 to 67 percent. Three of the RPDs exceeded a standard QC limit of 50 RPD indicating some minor heterogeneity.

8. Overall Assessment

The PAH data are acceptable for use based on the information received.

Data Validation Report W.C. Reed Playfield Site ALS Environmental Laboratory Project #: 1312188

ATTACHMENT

ALS ENVIRONMENTAL RESULTS SUMMARY WITH QUALIFIERS

10-Dec-2013

Environmental Quality Management, Inc.Angye Dragotta

Dear Angye,

Re: WC Reed Playfield (030281.0129) Work Order: 1312188

1800 Carillon BlvdCincinnati, OH 45240

ALS Environmental received 21 samples on 04-Dec-2013 10:00 AM for the analyses presented in the following report.

Senior Project ManagerTom Beamish

Electronically approved by: Tom Beamish

Certificate No: OH: CL 103

The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested.

Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in fullunless written approval has been obtained from ALS Environmental. Samples will be disposed in 30 daysunless storage arrangements are made.

The total number of pages in this report is ZZ.

If you have any questions regarding this report, please feel free to contact me.

Sincerely,

ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 | PHONE (616) 399-6070 | FAX (616) 399-6185

Report of Laboratory Analysis

Date: 10-Dec-13ALS Group USA, Corp

Project: WC Reed Playfield (030281.0129)Client: Environmental Quality Management, Inc.

Work Order: 1312188Work Order Sample Summary

Lab Samp ID Client Sample ID Collection DateTag Number Date ReceivedMatrix Hold1312188-01 WCR-008-27-062-FY6 Soil 12/03/13 09:10 12/04/13 10:001312188-02 WCR-008-27-062-FY24 Soil 12/03/13 09:15 12/04/13 10:001312188-03 WCR-008-27-062-BY6 Soil 12/03/13 09:10 12/04/13 10:001312188-04 WCR-008-27-062-BY24 Soil 12/03/13 09:15 12/04/13 10:001312188-05 WCR-008-27-060-BY6 Soil 12/03/13 10:30 12/04/13 10:001312188-06 WCR-008-27-060-BY24 Soil 12/03/13 10:30 12/04/13 10:001312188-07 WCR-008-27-059-SY6 Soil 12/03/13 11:15 12/04/13 10:001312188-08 WCR-008-27-059-SY24 Soil 12/03/13 11:20 12/04/13 10:001312188-09 WCR-008-27-059-BY6 Soil 12/03/13 11:15 12/04/13 10:001312188-10 WCR-008-27-059-BY24 Soil 12/03/13 11:20 12/04/13 10:001312188-11 WCR-008-26-058-BY6 Soil 12/03/13 12:55 12/04/13 10:001312188-12 WCR-008-26-058-BY24 Soil 12/03/13 12:55 12/04/13 10:001312188-13 WCR-008-26-057-6 Soil 12/03/13 13:35 12/04/13 10:001312188-14 WCR-008-26-057-24 Soil 12/03/13 13:30 12/04/13 10:001312188-15 WCR-008-26-062-6 Soil 12/03/13 14:20 12/04/13 10:001312188-16 WCR-008-26-062-FD6 Soil 12/03/13 14:20 12/04/13 10:001312188-17 WCR-008-26-062-24 Soil 12/03/13 14:25 12/04/13 10:001312188-18 WCR-008-26-034-BY6 Soil 12/03/13 15:05 12/04/13 10:001312188-19 WCR-008-26-034-BY24 Soil 12/03/13 15:00 12/04/13 10:001312188-20 WCR-008-26-032-BY6 Soil 12/03/13 15:35 12/04/13 10:001312188-21 WCR-008-26-032-BY24 Soil 12/03/13 15:33 12/04/13 10:00

Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 10-Dec-13

QUALIFIERS, ACRONYMS, UNITSProject: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.

WorkOrder: 1312188

Units Reported Description

Qualifier Description

Acronym Description

Percent of Sample% of sampleMilligrams per Kilogram Dry Weightmg/Kg-dry

Value exceeds Regulatory Limit*Not accreditedaAnalyte detected in the associated Method Blank above the Reporting LimitBValue above quantitation rangeEAnalyzed outside of Holding TimeHAnalyte is present at an estimated concentration between the MDL and Report LimitJNot offered for accreditationnNot Detected at the Reporting LimitNDSample amount is > 4 times amount spikedODual Column results percent difference > 40%PRPD above laboratory control limitRSpike Recovery outside laboratory control limitsSAnalyzed but not detected above the MDLU

Method DuplicateDUP

Laboratory Control SampleLCS

Laboratory Control Sample DuplicateLCSD

Limit of Detection (see MDL)LOD

Limit of Quantitation (see PQL)LOQ

Method BlankMBLK

Method Detection LimitMDL

Matrix SpikeMS

Matrix Spike DuplicateMSD

Practical Quantitation LimitPQL

Relative Percent DifferenceRPD

Target Detection LimitTDL

APHA Standard MethodsA

ASTMD

EPAE

SW-846 Update IIISW

QF Page 1 of 1

Date: 10-Dec-13ALS Group USA, Corp

Project: WC Reed Playfield (030281.0129)Client: Environmental Quality Management, Inc.

Work Order: 1312188Case Narrative

Analytical Comments:

Batch 53888, Method SVO_8270C_S, Sample 1312188-15A: One or more SVOC surrogate recoveries are unavailable due to sample matrix interference. Target analytes were not affected by the interference. No qualification is necessary.

Batch 53888, Method SVO_8270C_S, Sample 1312188-16A: One or more SVOC surrogate recoveries are unavailable due to sample matrix interference. Target analytes were not affected by the interference. No qualification is necessary.

Case Narrative Page 1 of 1

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-27-062-FY6Collection Date: 12/03/13 09:10 AM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-01

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: RMPrep Date: 12/05/132-Chloronaphthalene 12/06/13 07:03 PM0.0079 mg/Kg-dry 1ND2-Methylnaphthalene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.19Acenaphthene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.043Acenaphthylene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.063Anthracene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.17Benzo(a)anthracene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.63Benzo(a)pyrene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.64Benzo(b)fluoranthene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.95Benzo(g,h,i)perylene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.43Benzo(k)fluoranthene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.33Chrysene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.75Dibenzo(a,h)anthracene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.12Fluoranthene 12/06/13 07:03 PM0.0079 mg/Kg-dry 11.3Fluorene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.050Indeno(1,2,3-cd)pyrene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.47Naphthalene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.14Phenanthrene 12/06/13 07:03 PM0.0079 mg/Kg-dry 10.73Pyrene 12/06/13 07:03 PM0.0079 mg/Kg-dry 11.1 Surr: 2-Fluorobiphenyl 12/06/13 07:03 PM12-100 %REC 181.6 Surr: 4-Terphenyl-d14 12/06/13 07:03 PM25-137 %REC 199.8 Surr: Nitrobenzene-d5 12/06/13 07:03 PM37-107 %REC 167.1

MOISTURE A2540 G Analyst: MEBMoisture 12/05/13 06:00 PM0.050 % of sample 118

Analytical Results Page 1 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-27-062-FY24Collection Date: 12/03/13 09:15 AM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-02

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: RMPrep Date: 12/05/132-Chloronaphthalene 12/06/13 07:23 PM0.0075 mg/Kg-dry 1ND2-Methylnaphthalene 12/06/13 07:23 PM0.0075 mg/Kg-dry 10.088Acenaphthene 12/06/13 07:23 PM0.0075 mg/Kg-dry 1NDAcenaphthylene 12/06/13 07:23 PM0.0075 mg/Kg-dry 1NDAnthracene 12/06/13 07:23 PM0.0075 mg/Kg-dry 10.075Benzo(a)anthracene 12/06/13 07:23 PM0.0075 mg/Kg-dry 10.23Benzo(a)pyrene 12/06/13 07:23 PM0.0075 mg/Kg-dry 10.22Benzo(b)fluoranthene 12/06/13 07:23 PM0.0075 mg/Kg-dry 10.29Benzo(g,h,i)perylene 12/06/13 07:23 PM0.0075 mg/Kg-dry 10.15Benzo(k)fluoranthene 12/06/13 07:23 PM0.0075 mg/Kg-dry 10.11Chrysene 12/06/13 07:23 PM0.0075 mg/Kg-dry 10.24Dibenzo(a,h)anthracene 12/06/13 07:23 PM0.0075 mg/Kg-dry 10.046Fluoranthene 12/06/13 07:23 PM0.0075 mg/Kg-dry 10.46Fluorene 12/06/13 07:23 PM0.0075 mg/Kg-dry 1NDIndeno(1,2,3-cd)pyrene 12/06/13 07:23 PM0.0075 mg/Kg-dry 10.16Naphthalene 12/06/13 07:23 PM0.0075 mg/Kg-dry 10.067Phenanthrene 12/06/13 07:23 PM0.0075 mg/Kg-dry 10.32Pyrene 12/06/13 07:23 PM0.0075 mg/Kg-dry 10.41 Surr: 2-Fluorobiphenyl 12/06/13 07:23 PM12-100 %REC 177.3 Surr: 4-Terphenyl-d14 12/06/13 07:23 PM25-137 %REC 197.6 Surr: Nitrobenzene-d5 12/06/13 07:23 PM37-107 %REC 166.3

MOISTURE A2540 G Analyst: MEBMoisture 12/05/13 06:00 PM0.050 % of sample 114

Analytical Results Page 2 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-27-062-BY6Collection Date: 12/03/13 09:10 AM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-03

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: RMPrep Date: 12/05/132-Chloronaphthalene 12/06/13 07:43 PM0.0082 mg/Kg-dry 1ND2-Methylnaphthalene 12/06/13 07:43 PM0.0082 mg/Kg-dry 10.21Acenaphthene 12/06/13 07:43 PM0.0082 mg/Kg-dry 10.24Acenaphthylene 12/06/13 07:43 PM0.0082 mg/Kg-dry 10.31Anthracene 12/06/13 07:43 PM0.0082 mg/Kg-dry 11.0Benzo(a)anthracene 12/09/13 11:34 PM0.041 mg/Kg-dry 53.5Benzo(a)pyrene 12/09/13 11:34 PM0.041 mg/Kg-dry 53.4Benzo(b)fluoranthene 12/09/13 11:34 PM0.041 mg/Kg-dry 55.0Benzo(g,h,i)perylene 12/06/13 07:43 PM0.0082 mg/Kg-dry 12.1Benzo(k)fluoranthene 12/06/13 07:43 PM0.0082 mg/Kg-dry 11.5Chrysene 12/09/13 11:34 PM0.041 mg/Kg-dry 53.6Dibenzo(a,h)anthracene 12/06/13 07:43 PM0.0082 mg/Kg-dry 10.58Fluoranthene 12/09/13 11:34 PM0.041 mg/Kg-dry 57.2Fluorene 12/06/13 07:43 PM0.0082 mg/Kg-dry 10.30Indeno(1,2,3-cd)pyrene 12/06/13 07:43 PM0.0082 mg/Kg-dry 12.3Naphthalene 12/06/13 07:43 PM0.0082 mg/Kg-dry 10.21Phenanthrene 12/09/13 11:34 PM0.041 mg/Kg-dry 53.8Pyrene 12/09/13 11:34 PM0.041 mg/Kg-dry 56.2 Surr: 2-Fluorobiphenyl 12/06/13 07:43 PM12-100 %REC 181.5 Surr: 4-Terphenyl-d14 12/06/13 07:43 PM25-137 %REC 192.5 Surr: Nitrobenzene-d5 12/06/13 07:43 PM37-107 %REC 168.6

MOISTURE A2540 G Analyst: MEBMoisture 12/05/13 06:00 PM0.050 % of sample 120

Analytical Results Page 3 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-27-062-BY24Collection Date: 12/03/13 09:15 AM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-04

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: RMPrep Date: 12/05/132-Chloronaphthalene 12/06/13 08:03 PM0.0076 mg/Kg-dry 1ND2-Methylnaphthalene 12/06/13 08:03 PM0.0076 mg/Kg-dry 10.26Acenaphthene 12/06/13 08:03 PM0.0076 mg/Kg-dry 10.31Acenaphthylene 12/06/13 08:03 PM0.0076 mg/Kg-dry 10.18Anthracene 12/06/13 08:03 PM0.0076 mg/Kg-dry 11.0Benzo(a)anthracene 12/09/13 11:54 PM0.038 mg/Kg-dry 53.1Benzo(a)pyrene 12/09/13 11:54 PM0.038 mg/Kg-dry 52.8Benzo(b)fluoranthene 12/09/13 11:54 PM0.038 mg/Kg-dry 54.0Benzo(g,h,i)perylene 12/06/13 08:03 PM0.0076 mg/Kg-dry 11.5Benzo(k)fluoranthene 12/06/13 08:03 PM0.0076 mg/Kg-dry 11.2Chrysene 12/09/13 11:54 PM0.038 mg/Kg-dry 53.0Dibenzo(a,h)anthracene 12/06/13 08:03 PM0.0076 mg/Kg-dry 10.40Fluoranthene 12/09/13 11:54 PM0.038 mg/Kg-dry 56.9Fluorene 12/06/13 08:03 PM0.0076 mg/Kg-dry 10.38Indeno(1,2,3-cd)pyrene 12/06/13 08:03 PM0.0076 mg/Kg-dry 11.7Naphthalene 12/06/13 08:03 PM0.0076 mg/Kg-dry 10.46Phenanthrene 12/09/13 11:54 PM0.038 mg/Kg-dry 54.4Pyrene 12/09/13 11:54 PM0.038 mg/Kg-dry 56.0 Surr: 2-Fluorobiphenyl 12/06/13 08:03 PM12-100 %REC 175.7 Surr: 4-Terphenyl-d14 12/06/13 08:03 PM25-137 %REC 198.3 Surr: Nitrobenzene-d5 12/06/13 08:03 PM37-107 %REC 162.6

MOISTURE A2540 G Analyst: MEBMoisture 12/05/13 06:00 PM0.050 % of sample 115

Analytical Results Page 4 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-27-060-BY6Collection Date: 12/03/13 10:30 AM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-05

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: RMPrep Date: 12/05/132-Chloronaphthalene 12/06/13 08:23 PM0.0081 mg/Kg-dry 1ND2-Methylnaphthalene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.065Acenaphthene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.051Acenaphthylene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.050Anthracene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.16Benzo(a)anthracene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.52Benzo(a)pyrene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.54Benzo(b)fluoranthene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.77Benzo(g,h,i)perylene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.35Benzo(k)fluoranthene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.24Chrysene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.58Dibenzo(a,h)anthracene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.096Fluoranthene 12/06/13 08:23 PM0.0081 mg/Kg-dry 11.1Fluorene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.050Indeno(1,2,3-cd)pyrene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.40Naphthalene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.060Phenanthrene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.70Pyrene 12/06/13 08:23 PM0.0081 mg/Kg-dry 10.93 Surr: 2-Fluorobiphenyl 12/06/13 08:23 PM12-100 %REC 174.7 Surr: 4-Terphenyl-d14 12/06/13 08:23 PM25-137 %REC 196.6 Surr: Nitrobenzene-d5 12/06/13 08:23 PM37-107 %REC 160.9

MOISTURE A2540 G Analyst: MEBMoisture 12/05/13 06:00 PM0.050 % of sample 119

Analytical Results Page 5 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-27-060-BY24Collection Date: 12/03/13 10:30 AM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-06

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: RMPrep Date: 12/05/132-Chloronaphthalene 12/06/13 08:43 PM0.0076 mg/Kg-dry 1ND2-Methylnaphthalene 12/06/13 08:43 PM0.0076 mg/Kg-dry 1NDAcenaphthene 12/06/13 08:43 PM0.0076 mg/Kg-dry 1NDAcenaphthylene 12/06/13 08:43 PM0.0076 mg/Kg-dry 1NDAnthracene 12/06/13 08:43 PM0.0076 mg/Kg-dry 10.057Benzo(a)anthracene 12/06/13 08:43 PM0.0076 mg/Kg-dry 10.19Benzo(a)pyrene 12/06/13 08:43 PM0.0076 mg/Kg-dry 10.18Benzo(b)fluoranthene 12/06/13 08:43 PM0.0076 mg/Kg-dry 10.26Benzo(g,h,i)perylene 12/06/13 08:43 PM0.0076 mg/Kg-dry 10.12Benzo(k)fluoranthene 12/06/13 08:43 PM0.0076 mg/Kg-dry 10.084Chrysene 12/06/13 08:43 PM0.0076 mg/Kg-dry 10.20Dibenzo(a,h)anthracene 12/06/13 08:43 PM0.0076 mg/Kg-dry 1NDFluoranthene 12/06/13 08:43 PM0.0076 mg/Kg-dry 10.39Fluorene 12/06/13 08:43 PM0.0076 mg/Kg-dry 1NDIndeno(1,2,3-cd)pyrene 12/06/13 08:43 PM0.0076 mg/Kg-dry 10.13Naphthalene 12/06/13 08:43 PM0.0076 mg/Kg-dry 1NDPhenanthrene 12/06/13 08:43 PM0.0076 mg/Kg-dry 10.22Pyrene 12/06/13 08:43 PM0.0076 mg/Kg-dry 10.32 Surr: 2-Fluorobiphenyl 12/06/13 08:43 PM12-100 %REC 174.5 Surr: 4-Terphenyl-d14 12/06/13 08:43 PM25-137 %REC 199.1 Surr: Nitrobenzene-d5 12/06/13 08:43 PM37-107 %REC 166.8

MOISTURE A2540 G Analyst: MEBMoisture 12/05/13 06:00 PM0.050 % of sample 114

Analytical Results Page 6 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-27-059-SY6Collection Date: 12/03/13 11:15 AM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-07

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: RMPrep Date: 12/05/132-Chloronaphthalene 12/06/13 09:03 PM0.0085 mg/Kg-dry 1ND2-Methylnaphthalene 12/06/13 09:03 PM0.0085 mg/Kg-dry 10.11Acenaphthene 12/06/13 09:03 PM0.0085 mg/Kg-dry 10.38Acenaphthylene 12/06/13 09:03 PM0.0085 mg/Kg-dry 10.079Anthracene 12/06/13 09:03 PM0.0085 mg/Kg-dry 10.96Benzo(a)anthracene 12/10/13 12:14 PM0.043 mg/Kg-dry 52.8Benzo(a)pyrene 12/06/13 09:03 PM0.0085 mg/Kg-dry 12.5Benzo(b)fluoranthene 12/10/13 12:14 PM0.043 mg/Kg-dry 53.9Benzo(g,h,i)perylene 12/06/13 09:03 PM0.0085 mg/Kg-dry 11.5Benzo(k)fluoranthene 12/06/13 09:03 PM0.0085 mg/Kg-dry 11.0Chrysene 12/10/13 12:14 PM0.043 mg/Kg-dry 52.8Dibenzo(a,h)anthracene 12/06/13 09:03 PM0.0085 mg/Kg-dry 10.37Fluoranthene 12/10/13 12:14 PM0.043 mg/Kg-dry 56.7Fluorene 12/06/13 09:03 PM0.0085 mg/Kg-dry 10.30Indeno(1,2,3-cd)pyrene 12/06/13 09:03 PM0.0085 mg/Kg-dry 11.7Naphthalene 12/06/13 09:03 PM0.0085 mg/Kg-dry 10.12Phenanthrene 12/10/13 12:14 PM0.043 mg/Kg-dry 54.4Pyrene 12/10/13 12:14 PM0.043 mg/Kg-dry 55.7 Surr: 2-Fluorobiphenyl 12/06/13 09:03 PM12-100 %REC 179.1 Surr: 4-Terphenyl-d14 12/06/13 09:03 PM25-137 %REC 197.0 Surr: Nitrobenzene-d5 12/06/13 09:03 PM37-107 %REC 162.7

MOISTURE A2540 G Analyst: MEBMoisture 12/05/13 06:00 PM0.050 % of sample 123

Analytical Results Page 7 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-27-059-SY24Collection Date: 12/03/13 11:20 AM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-08

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: RMPrep Date: 12/05/132-Chloronaphthalene 12/06/13 09:23 PM0.0078 mg/Kg-dry 1ND2-Methylnaphthalene 12/06/13 09:23 PM0.0078 mg/Kg-dry 10.078Acenaphthene 12/06/13 09:23 PM0.0078 mg/Kg-dry 1NDAcenaphthylene 12/06/13 09:23 PM0.0078 mg/Kg-dry 1NDAnthracene 12/06/13 09:23 PM0.0078 mg/Kg-dry 10.10Benzo(a)anthracene 12/06/13 09:23 PM0.0078 mg/Kg-dry 10.40Benzo(a)pyrene 12/06/13 09:23 PM0.0078 mg/Kg-dry 10.41Benzo(b)fluoranthene 12/06/13 09:23 PM0.0078 mg/Kg-dry 10.59Benzo(g,h,i)perylene 12/06/13 09:23 PM0.0078 mg/Kg-dry 10.27Benzo(k)fluoranthene 12/06/13 09:23 PM0.0078 mg/Kg-dry 10.17Chrysene 12/06/13 09:23 PM0.0078 mg/Kg-dry 10.44Dibenzo(a,h)anthracene 12/06/13 09:23 PM0.0078 mg/Kg-dry 10.076Fluoranthene 12/06/13 09:23 PM0.0078 mg/Kg-dry 10.81Fluorene 12/06/13 09:23 PM0.0078 mg/Kg-dry 1NDIndeno(1,2,3-cd)pyrene 12/06/13 09:23 PM0.0078 mg/Kg-dry 10.30Naphthalene 12/06/13 09:23 PM0.0078 mg/Kg-dry 10.060Phenanthrene 12/06/13 09:23 PM0.0078 mg/Kg-dry 10.42Pyrene 12/06/13 09:23 PM0.0078 mg/Kg-dry 10.66 Surr: 2-Fluorobiphenyl 12/06/13 09:23 PM12-100 %REC 177.3 Surr: 4-Terphenyl-d14 12/06/13 09:23 PM25-137 %REC 1103 Surr: Nitrobenzene-d5 12/06/13 09:23 PM37-107 %REC 165.6

MOISTURE A2540 G Analyst: MEBMoisture 12/05/13 06:00 PM0.050 % of sample 116

Analytical Results Page 8 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-27-059-BY6Collection Date: 12/03/13 11:15 AM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-09

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: RMPrep Date: 12/05/132-Chloronaphthalene 12/06/13 09:42 PM0.0090 mg/Kg-dry 1ND2-Methylnaphthalene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.16Acenaphthene 12/06/13 09:42 PM0.0090 mg/Kg-dry 1NDAcenaphthylene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.062Anthracene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.096Benzo(a)anthracene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.41Benzo(a)pyrene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.46Benzo(b)fluoranthene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.69Benzo(g,h,i)perylene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.33Benzo(k)fluoranthene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.20Chrysene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.49Dibenzo(a,h)anthracene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.088Fluoranthene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.82Fluorene 12/06/13 09:42 PM0.0090 mg/Kg-dry 1NDIndeno(1,2,3-cd)pyrene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.35Naphthalene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.11Phenanthrene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.44Pyrene 12/06/13 09:42 PM0.0090 mg/Kg-dry 10.64 Surr: 2-Fluorobiphenyl 12/06/13 09:42 PM12-100 %REC 171.6 Surr: 4-Terphenyl-d14 12/06/13 09:42 PM25-137 %REC 194.4 Surr: Nitrobenzene-d5 12/06/13 09:42 PM37-107 %REC 154.4

MOISTURE A2540 G Analyst: MEBMoisture 12/05/13 06:00 PM0.050 % of sample 127

Analytical Results Page 9 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-27-059-BY24Collection Date: 12/03/13 11:20 AM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-10

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: RMPrep Date: 12/05/132-Chloronaphthalene 12/06/13 10:02 PM0.0075 mg/Kg-dry 1ND2-Methylnaphthalene 12/06/13 10:02 PM0.0075 mg/Kg-dry 1NDAcenaphthene 12/06/13 10:02 PM0.0075 mg/Kg-dry 10.12Acenaphthylene 12/06/13 10:02 PM0.0075 mg/Kg-dry 1NDAnthracene 12/06/13 10:02 PM0.0075 mg/Kg-dry 10.24Benzo(a)anthracene 12/06/13 10:02 PM0.0075 mg/Kg-dry 10.68Benzo(a)pyrene 12/06/13 10:02 PM0.0075 mg/Kg-dry 10.68Benzo(b)fluoranthene 12/06/13 10:02 PM0.0075 mg/Kg-dry 10.87Benzo(g,h,i)perylene 12/06/13 10:02 PM0.0075 mg/Kg-dry 10.41Benzo(k)fluoranthene 12/06/13 10:02 PM0.0075 mg/Kg-dry 10.29Chrysene 12/06/13 10:02 PM0.0075 mg/Kg-dry 10.68Dibenzo(a,h)anthracene 12/06/13 10:02 PM0.0075 mg/Kg-dry 10.11Fluoranthene 12/06/13 10:02 PM0.0075 mg/Kg-dry 11.5Fluorene 12/06/13 10:02 PM0.0075 mg/Kg-dry 10.082Indeno(1,2,3-cd)pyrene 12/06/13 10:02 PM0.0075 mg/Kg-dry 10.46Naphthalene 12/06/13 10:02 PM0.0075 mg/Kg-dry 1NDPhenanthrene 12/06/13 10:02 PM0.0075 mg/Kg-dry 11.1Pyrene 12/06/13 10:02 PM0.0075 mg/Kg-dry 11.3 Surr: 2-Fluorobiphenyl 12/06/13 10:02 PM12-100 %REC 176.4 Surr: 4-Terphenyl-d14 12/06/13 10:02 PM25-137 %REC 1103 Surr: Nitrobenzene-d5 12/06/13 10:02 PM37-107 %REC 171.3

MOISTURE A2540 G Analyst: MEBMoisture 12/05/13 06:00 PM0.050 % of sample 113

Analytical Results Page 10 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-26-058-BY6Collection Date: 12/03/13 12:55 PM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-11

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: RMPrep Date: 12/05/132-Chloronaphthalene 12/06/13 10:22 PM0.0087 mg/Kg-dry 1ND2-Methylnaphthalene 12/06/13 10:22 PM0.0087 mg/Kg-dry 10.065Acenaphthene 12/06/13 10:22 PM0.0087 mg/Kg-dry 10.11Acenaphthylene 12/06/13 10:22 PM0.0087 mg/Kg-dry 10.058Anthracene 12/06/13 10:22 PM0.0087 mg/Kg-dry 10.42Benzo(a)anthracene 12/06/13 10:22 PM0.0087 mg/Kg-dry 11.2Benzo(a)pyrene 12/06/13 10:22 PM0.0087 mg/Kg-dry 11.2Benzo(b)fluoranthene 12/06/13 10:22 PM0.0087 mg/Kg-dry 11.7Benzo(g,h,i)perylene 12/06/13 10:22 PM0.0087 mg/Kg-dry 10.73Benzo(k)fluoranthene 12/06/13 10:22 PM0.0087 mg/Kg-dry 10.53Chrysene 12/06/13 10:22 PM0.0087 mg/Kg-dry 11.3Dibenzo(a,h)anthracene 12/06/13 10:22 PM0.0087 mg/Kg-dry 10.20Fluoranthene 12/06/13 10:22 PM0.0087 mg/Kg-dry 12.6Fluorene 12/06/13 10:22 PM0.0087 mg/Kg-dry 10.14Indeno(1,2,3-cd)pyrene 12/06/13 10:22 PM0.0087 mg/Kg-dry 10.81Naphthalene 12/06/13 10:22 PM0.0087 mg/Kg-dry 10.056Phenanthrene 12/06/13 10:22 PM0.0087 mg/Kg-dry 11.5Pyrene 12/06/13 10:22 PM0.0087 mg/Kg-dry 12.1 Surr: 2-Fluorobiphenyl 12/06/13 10:22 PM12-100 %REC 176.6 Surr: 4-Terphenyl-d14 12/06/13 10:22 PM25-137 %REC 196.0 Surr: Nitrobenzene-d5 12/06/13 10:22 PM37-107 %REC 159.2

MOISTURE A2540 G Analyst: MEBMoisture 12/05/13 06:00 PM0.050 % of sample 124

Analytical Results Page 11 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-26-058-BY24Collection Date: 12/03/13 12:55 PM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-12

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: RMPrep Date: 12/05/132-Chloronaphthalene 12/06/13 10:42 PM0.0079 mg/Kg-dry 1ND2-Methylnaphthalene 12/06/13 10:42 PM0.0079 mg/Kg-dry 1NDAcenaphthene 12/06/13 10:42 PM0.0079 mg/Kg-dry 10.058Acenaphthylene 12/06/13 10:42 PM0.0079 mg/Kg-dry 1NDAnthracene 12/06/13 10:42 PM0.0079 mg/Kg-dry 10.27Benzo(a)anthracene 12/06/13 10:42 PM0.0079 mg/Kg-dry 10.52Benzo(a)pyrene 12/06/13 10:42 PM0.0079 mg/Kg-dry 10.44Benzo(b)fluoranthene 12/06/13 10:42 PM0.0079 mg/Kg-dry 10.58Benzo(g,h,i)perylene 12/06/13 10:42 PM0.0079 mg/Kg-dry 10.24Benzo(k)fluoranthene 12/06/13 10:42 PM0.0079 mg/Kg-dry 10.23Chrysene 12/06/13 10:42 PM0.0079 mg/Kg-dry 10.50Dibenzo(a,h)anthracene 12/06/13 10:42 PM0.0079 mg/Kg-dry 10.073Fluoranthene 12/06/13 10:42 PM0.0079 mg/Kg-dry 11.2Fluorene 12/06/13 10:42 PM0.0079 mg/Kg-dry 10.087Indeno(1,2,3-cd)pyrene 12/06/13 10:42 PM0.0079 mg/Kg-dry 10.28Naphthalene 12/06/13 10:42 PM0.0079 mg/Kg-dry 1NDPhenanthrene 12/06/13 10:42 PM0.0079 mg/Kg-dry 10.83Pyrene 12/06/13 10:42 PM0.0079 mg/Kg-dry 10.90 Surr: 2-Fluorobiphenyl 12/06/13 10:42 PM12-100 %REC 170.5 Surr: 4-Terphenyl-d14 12/06/13 10:42 PM25-137 %REC 189.3 Surr: Nitrobenzene-d5 12/06/13 10:42 PM37-107 %REC 167.3

MOISTURE A2540 G Analyst: MEBMoisture 12/06/13 10:40 AM0.050 % of sample 118

Analytical Results Page 12 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-26-057-6Collection Date: 12/03/13 01:35 PM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-13

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: HLPrep Date: 12/06/132-Chloronaphthalene 12/06/13 08:12 PM0.0079 mg/Kg-dry 1ND2-Methylnaphthalene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.066Acenaphthene 12/06/13 08:12 PM0.0079 mg/Kg-dry 1NDAcenaphthylene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.013Anthracene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.031Benzo(a)anthracene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.17Benzo(a)pyrene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.19Benzo(b)fluoranthene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.29Benzo(g,h,i)perylene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.098Benzo(k)fluoranthene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.080Chrysene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.21Dibenzo(a,h)anthracene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.029Fluoranthene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.39Fluorene 12/06/13 08:12 PM0.0079 mg/Kg-dry 1NDIndeno(1,2,3-cd)pyrene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.097Naphthalene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.044Phenanthrene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.16Pyrene 12/06/13 08:12 PM0.0079 mg/Kg-dry 10.33 Surr: 2-Fluorobiphenyl 12/06/13 08:12 PM12-100 %REC 166.8 Surr: 4-Terphenyl-d14 12/06/13 08:12 PM25-137 %REC 192.5 Surr: Nitrobenzene-d5 12/06/13 08:12 PM37-107 %REC 163.2

MOISTURE A2540 G Analyst: MEBMoisture 12/06/13 10:40 AM0.050 % of sample 118

Analytical Results Page 13 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-26-057-24Collection Date: 12/03/13 01:30 PM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-14

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: HLPrep Date: 12/06/132-Chloronaphthalene 12/09/13 06:34 PM0.085 mg/Kg-dry 10ND2-Methylnaphthalene 12/09/13 06:34 PM0.085 mg/Kg-dry 10NDAcenaphthene 12/09/13 06:34 PM0.085 mg/Kg-dry 10NDAcenaphthylene 12/09/13 06:34 PM0.085 mg/Kg-dry 10NDAnthracene 12/09/13 06:34 PM0.085 mg/Kg-dry 100.22Benzo(a)anthracene 12/09/13 06:34 PM0.085 mg/Kg-dry 101.1Benzo(a)pyrene 12/09/13 06:34 PM0.085 mg/Kg-dry 101.1Benzo(b)fluoranthene 12/09/13 06:34 PM0.085 mg/Kg-dry 101.5Benzo(g,h,i)perylene 12/09/13 06:34 PM0.085 mg/Kg-dry 100.63Benzo(k)fluoranthene 12/09/13 06:34 PM0.085 mg/Kg-dry 100.55Chrysene 12/09/13 06:34 PM0.085 mg/Kg-dry 100.92Dibenzo(a,h)anthracene 12/09/13 06:34 PM0.085 mg/Kg-dry 100.25Fluoranthene 12/09/13 06:34 PM0.085 mg/Kg-dry 101.9Fluorene 12/09/13 06:34 PM0.085 mg/Kg-dry 10NDIndeno(1,2,3-cd)pyrene 12/09/13 06:34 PM0.085 mg/Kg-dry 100.70Naphthalene 12/09/13 06:34 PM0.085 mg/Kg-dry 10NDPhenanthrene 12/09/13 06:34 PM0.085 mg/Kg-dry 100.84Pyrene 12/09/13 06:34 PM0.085 mg/Kg-dry 101.5 Surr: 2-Fluorobiphenyl 12/09/13 06:34 PM12-100 %REC 1071.8 Surr: 4-Terphenyl-d14 12/09/13 06:34 PM25-137 %REC 1088.0 Surr: Nitrobenzene-d5 12/09/13 06:34 PM37-107 %REC 1057.8

MOISTURE A2540 G Analyst: MEBMoisture 12/06/13 10:40 AM0.050 % of sample 123

Analytical Results Page 14 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-26-062-6Collection Date: 12/03/13 02:20 PM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-15

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: HLPrep Date: 12/06/132-Chloronaphthalene 12/06/13 08:43 PM0.16 mg/Kg-dry 20ND2-Methylnaphthalene 12/06/13 08:43 PM0.16 mg/Kg-dry 201.2Acenaphthene 12/06/13 08:43 PM0.16 mg/Kg-dry 204.8Acenaphthylene 12/06/13 08:43 PM0.16 mg/Kg-dry 203.1Anthracene 12/06/13 08:43 PM0.16 mg/Kg-dry 2011Benzo(a)anthracene 12/06/13 08:43 PM0.16 mg/Kg-dry 2040Benzo(a)pyrene 12/06/13 08:43 PM0.16 mg/Kg-dry 2034Benzo(b)fluoranthene 12/06/13 08:43 PM0.16 mg/Kg-dry 2045Benzo(g,h,i)perylene 12/06/13 08:43 PM0.16 mg/Kg-dry 2015Benzo(k)fluoranthene 12/06/13 08:43 PM0.16 mg/Kg-dry 2015Chrysene 12/06/13 08:43 PM0.16 mg/Kg-dry 2033Dibenzo(a,h)anthracene 12/06/13 08:43 PM0.16 mg/Kg-dry 205.5Fluoranthene 12/09/13 06:56 PM0.41 mg/Kg-dry 5078Fluorene 12/06/13 08:43 PM0.16 mg/Kg-dry 205.7Indeno(1,2,3-cd)pyrene 12/06/13 08:43 PM0.16 mg/Kg-dry 2015Naphthalene 12/06/13 08:43 PM0.16 mg/Kg-dry 201.1Phenanthrene 12/09/13 06:56 PM0.41 mg/Kg-dry 5064Pyrene 12/09/13 06:56 PM0.41 mg/Kg-dry 5085 Surr: 2-Fluorobiphenyl 12/06/13 08:43 PM12-100 %REC 2060.8 Surr: 2-Fluorobiphenyl 12/09/13 06:56 PM12-100 %REC 5060.0 Surr: 4-Terphenyl-d14 12/06/13 08:43 PM25-137 %REC 2072.4 Surr: 4-Terphenyl-d14 12/09/13 06:56 PM25-137 %REC 50124 Surr: Nitrobenzene-d5 12/09/13 06:56 PM37-107 %REC 5066.0 Surr: Nitrobenzene-d5 S 12/06/13 08:43 PM37-107 %REC 2036.0

MOISTURE A2540 G Analyst: MEBMoisture 12/06/13 10:40 AM0.050 % of sample 119

Analytical Results Page 15 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-26-062-FD6Collection Date: 12/03/13 02:20 PM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-16

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: HLPrep Date: 12/06/132-Chloronaphthalene 12/06/13 09:14 PM0.17 mg/Kg-dry 20ND2-Methylnaphthalene 12/06/13 09:14 PM0.17 mg/Kg-dry 201.7Acenaphthene 12/06/13 09:14 PM0.17 mg/Kg-dry 207.7Acenaphthylene 12/06/13 09:14 PM0.17 mg/Kg-dry 205.4Anthracene 12/06/13 09:14 PM0.17 mg/Kg-dry 2018Benzo(a)anthracene 12/09/13 07:19 PM0.42 mg/Kg-dry 5052Benzo(a)pyrene 12/06/13 09:14 PM0.17 mg/Kg-dry 2050Benzo(b)fluoranthene 12/09/13 07:19 PM0.42 mg/Kg-dry 5074Benzo(g,h,i)perylene 12/06/13 09:14 PM0.17 mg/Kg-dry 2019Benzo(k)fluoranthene 12/09/13 07:19 PM0.42 mg/Kg-dry 5027Chrysene 12/06/13 09:14 PM0.17 mg/Kg-dry 2048Dibenzo(a,h)anthracene 12/06/13 09:14 PM0.17 mg/Kg-dry 207.7Fluoranthene 12/10/13 11:38 AM0.84 mg/Kg-dry 10071Fluorene 12/06/13 09:14 PM0.17 mg/Kg-dry 208.9Indeno(1,2,3-cd)pyrene 12/06/13 09:14 PM0.17 mg/Kg-dry 2021Naphthalene 12/06/13 09:14 PM0.17 mg/Kg-dry 202.2Phenanthrene 12/09/13 07:19 PM0.42 mg/Kg-dry 5090Pyrene 12/09/13 07:19 PM0.42 mg/Kg-dry 50110 Surr: 2-Fluorobiphenyl 12/06/13 09:14 PM12-100 %REC 2062.8 Surr: 2-Fluorobiphenyl 12/09/13 07:19 PM12-100 %REC 5058.0 Surr: 4-Terphenyl-d14 12/06/13 09:14 PM25-137 %REC 2091.2 Surr: 4-Terphenyl-d14 12/09/13 07:19 PM25-137 %REC 50113 Surr: Nitrobenzene-d5 12/09/13 07:19 PM37-107 %REC 5070.0 Surr: Nitrobenzene-d5 S 12/06/13 09:14 PM37-107 %REC 2035.2

MOISTURE A2540 G Analyst: MEBMoisture 12/06/13 10:40 AM0.050 % of sample 121

Analytical Results Page 16 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-26-062-24Collection Date: 12/03/13 02:25 PM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-17

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: HLPrep Date: 12/06/132-Chloronaphthalene 12/09/13 09:31 PM0.0075 mg/Kg-dry 1ND2-Methylnaphthalene 12/09/13 09:31 PM0.0075 mg/Kg-dry 1NDAcenaphthene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.030Acenaphthylene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.046Anthracene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.10Benzo(a)anthracene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.47Benzo(a)pyrene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.56Benzo(b)fluoranthene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.83Benzo(g,h,i)perylene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.36Benzo(k)fluoranthene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.28Chrysene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.45Dibenzo(a,h)anthracene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.092Fluoranthene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.74Fluorene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.029Indeno(1,2,3-cd)pyrene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.43Naphthalene 12/09/13 09:31 PM0.0075 mg/Kg-dry 1NDPhenanthrene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.40Pyrene 12/09/13 09:31 PM0.0075 mg/Kg-dry 10.82 Surr: 2-Fluorobiphenyl 12/09/13 09:31 PM12-100 %REC 153.5 Surr: 4-Terphenyl-d14 12/09/13 09:31 PM25-137 %REC 177.5 Surr: Nitrobenzene-d5 12/09/13 09:31 PM37-107 %REC 144.8

MOISTURE A2540 G Analyst: MEBMoisture 12/06/13 12:00 PM0.050 % of sample 112

Analytical Results Page 17 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-26-034-BY6Collection Date: 12/03/13 03:05 PM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-18

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: HLPrep Date: 12/06/132-Chloronaphthalene 12/09/13 09:53 PM0.0084 mg/Kg-dry 1ND2-Methylnaphthalene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.027Acenaphthene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.041Acenaphthylene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.052Anthracene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.11Benzo(a)anthracene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.39Benzo(a)pyrene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.41Benzo(b)fluoranthene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.61Benzo(g,h,i)perylene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.22Benzo(k)fluoranthene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.20Chrysene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.40Dibenzo(a,h)anthracene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.061Fluoranthene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.77Fluorene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.035Indeno(1,2,3-cd)pyrene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.26Naphthalene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.021Phenanthrene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.45Pyrene 12/09/13 09:53 PM0.0084 mg/Kg-dry 10.81 Surr: 2-Fluorobiphenyl 12/09/13 09:53 PM12-100 %REC 168.8 Surr: 4-Terphenyl-d14 12/09/13 09:53 PM25-137 %REC 199.9 Surr: Nitrobenzene-d5 12/09/13 09:53 PM37-107 %REC 155.2

MOISTURE A2540 G Analyst: MEBMoisture 12/06/13 12:00 PM0.050 % of sample 122

Analytical Results Page 18 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-26-034-BY24Collection Date: 12/03/13 03:00 PM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-19

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: HLPrep Date: 12/06/132-Chloronaphthalene 12/09/13 10:15 PM0.0082 mg/Kg-dry 1ND2-Methylnaphthalene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.025Acenaphthene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.025Acenaphthylene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.11Anthracene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.12Benzo(a)anthracene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.42Benzo(a)pyrene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.44Benzo(b)fluoranthene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.62Benzo(g,h,i)perylene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.23Benzo(k)fluoranthene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.24Chrysene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.44Dibenzo(a,h)anthracene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.071Fluoranthene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.81Fluorene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.033Indeno(1,2,3-cd)pyrene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.29Naphthalene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.024Phenanthrene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.42Pyrene 12/09/13 10:15 PM0.0082 mg/Kg-dry 10.76 Surr: 2-Fluorobiphenyl 12/09/13 10:15 PM12-100 %REC 165.6 Surr: 4-Terphenyl-d14 12/09/13 10:15 PM25-137 %REC 185.3 Surr: Nitrobenzene-d5 12/09/13 10:15 PM37-107 %REC 156.2

MOISTURE A2540 G Analyst: MEBMoisture 12/06/13 12:00 PM0.050 % of sample 119

Analytical Results Page 19 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-26-032-BY6Collection Date: 12/03/13 03:35 PM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-20

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: RMPrep Date: 12/06/132-Chloronaphthalene 12/09/13 10:15 PM0.0087 mg/Kg-dry 1ND2-Methylnaphthalene 12/09/13 10:15 PM0.0087 mg/Kg-dry 10.27Acenaphthene 12/09/13 10:15 PM0.0087 mg/Kg-dry 10.16Acenaphthylene 12/09/13 10:15 PM0.0087 mg/Kg-dry 10.14Anthracene 12/09/13 10:15 PM0.0087 mg/Kg-dry 10.52Benzo(a)anthracene 12/09/13 10:15 PM0.0087 mg/Kg-dry 11.6Benzo(a)pyrene 12/09/13 10:15 PM0.0087 mg/Kg-dry 11.5Benzo(b)fluoranthene 12/09/13 10:15 PM0.0087 mg/Kg-dry 12.3Benzo(g,h,i)perylene 12/09/13 10:15 PM0.0087 mg/Kg-dry 10.87Benzo(k)fluoranthene 12/09/13 10:15 PM0.0087 mg/Kg-dry 10.86Chrysene 12/09/13 10:15 PM0.0087 mg/Kg-dry 11.7Dibenzo(a,h)anthracene 12/09/13 10:15 PM0.0087 mg/Kg-dry 10.26Fluoranthene 12/10/13 01:48 PM0.043 mg/Kg-dry 5NDFluorene 12/09/13 10:15 PM0.0087 mg/Kg-dry 10.16Indeno(1,2,3-cd)pyrene 12/09/13 10:15 PM0.0087 mg/Kg-dry 10.90Naphthalene 12/09/13 10:15 PM0.0087 mg/Kg-dry 10.22Phenanthrene 12/09/13 10:15 PM0.0087 mg/Kg-dry 11.8Pyrene 12/10/13 01:48 PM0.043 mg/Kg-dry 5ND Surr: 2-Fluorobiphenyl 12/09/13 10:15 PM12-100 %REC 172.3 Surr: 4-Terphenyl-d14 12/09/13 10:15 PM25-137 %REC 193.4 Surr: Nitrobenzene-d5 12/09/13 10:15 PM37-107 %REC 166.3

MOISTURE A2540 G Analyst: MEBMoisture 12/06/13 12:00 PM0.050 % of sample 124

Analytical Results Page 20 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Project: WC Reed Playfield (030281.0129)Sample ID: WCR-008-26-032-BY24Collection Date: 12/03/13 03:33 PM Matrix: SOIL

Analyses Result Qual Units Date AnalyzedReport Limit

Client: Environmental Quality Management, Inc.Work Order: 1312188

Dilution Factor

Lab ID: 1312188-21

ALS Group USA, Corp Date: 10-Dec-13

SEMI-VOLATILE ORGANIC COMPOUNDS SW8270C Analyst: RMPrep Date: 12/06/132-Chloronaphthalene 12/09/13 09:55 PM0.0076 mg/Kg-dry 1ND2-Methylnaphthalene 12/09/13 09:55 PM0.0076 mg/Kg-dry 10.47Acenaphthene 12/09/13 09:55 PM0.0076 mg/Kg-dry 10.29Acenaphthylene 12/09/13 09:55 PM0.0076 mg/Kg-dry 10.11Anthracene 12/09/13 09:55 PM0.0076 mg/Kg-dry 10.94Benzo(a)anthracene 12/10/13 02:08 PM0.038 mg/Kg-dry 5NDBenzo(a)pyrene 12/09/13 09:55 PM0.0076 mg/Kg-dry 12.1Benzo(b)fluoranthene 12/10/13 02:08 PM0.038 mg/Kg-dry 5NDBenzo(g,h,i)perylene 12/09/13 09:55 PM0.0076 mg/Kg-dry 10.76Benzo(k)fluoranthene 12/09/13 09:55 PM0.0076 mg/Kg-dry 11.2Chrysene 12/10/13 02:08 PM0.038 mg/Kg-dry 5NDDibenzo(a,h)anthracene 12/09/13 09:55 PM0.0076 mg/Kg-dry 10.32Fluoranthene 12/10/13 02:08 PM0.038 mg/Kg-dry 5NDFluorene 12/09/13 09:55 PM0.0076 mg/Kg-dry 10.29Indeno(1,2,3-cd)pyrene 12/09/13 09:55 PM0.0076 mg/Kg-dry 11.0Naphthalene 12/09/13 09:55 PM0.0076 mg/Kg-dry 10.37Phenanthrene 12/10/13 02:08 PM0.038 mg/Kg-dry 5NDPyrene 12/10/13 02:08 PM0.038 mg/Kg-dry 5ND Surr: 2-Fluorobiphenyl 12/09/13 09:55 PM12-100 %REC 179.5 Surr: 4-Terphenyl-d14 12/09/13 09:55 PM25-137 %REC 1100 Surr: Nitrobenzene-d5 12/09/13 09:55 PM37-107 %REC 170.8

MOISTURE A2540 G Analyst: MEBMoisture 12/06/13 12:00 PM0.050 % of sample 115

Analytical Results Page 21 of 21

Note: See Qualifiers page for a list of qualifiers and their definitions.

Date: 10-Dec-13ALS Group USA, Corp

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: 53871 Instrument ID SVMS8 Method: SW8270

QualRPD Limit

Analysis Date: 12/05/13 05:38 PM

Prep Date: 12/05/13

Analyte Result %REC %RPD

Units:µg/Kg

PQL

Client ID: SeqNo:2568207

MBLK

Run ID: SVMS8_131205A

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: SBLKS1-53871-53871

2-Chloronaphthalene 6.7ND

2-Methylnaphthalene 6.7ND

Acenaphthene 6.7ND

Acenaphthylene 6.7ND

Anthracene 6.7ND

Benzo(a)anthracene 6.7ND

Benzo(a)pyrene 6.7ND

Benzo(b)fluoranthene 6.7ND

Benzo(g,h,i)perylene 6.7ND

Benzo(k)fluoranthene 6.7ND

Chrysene 6.7ND

Dibenzo(a,h)anthracene 6.7ND

Fluoranthene 6.7ND

Fluorene 6.7ND

Indeno(1,2,3-cd)pyrene 6.7ND

Naphthalene 6.7ND

Phenanthrene 6.7ND

Pyrene 6.7ND

001667 Surr: 2-Fluorobiphenyl 74.5 12-10001242

001667 Surr: 4-Terphenyl-d14 99.1 25-13701651

001667 Surr: Nitrobenzene-d5 72 37-10701201

QC Page: 1 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: 53871 Instrument ID SVMS8 Method: SW8270

QualRPD Limit

Analysis Date: 12/05/13 05:58 PM

Prep Date: 12/05/13

Analyte Result %REC %RPD

Units:µg/Kg

PQL

Client ID: SeqNo:2568208

LCS

Run ID: SVMS8_131205A

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: SLCSS1-53871-53871

00666.72-Chloronaphthalene 82.8 45-1056.7552

00666.72-Methylnaphthalene 88.2 45-1056.7588

00666.7Acenaphthene 82.3 45-1106.7548.7

00666.7Acenaphthylene 87.5 45-1056.7583.3

00666.7Anthracene 88.4 55-1056.7589.7

00666.7Benzo(a)anthracene 89.8 50-1106.7599

00666.7Benzo(a)pyrene 91.7 50-1106.7611.7

00666.7Benzo(b)fluoranthene 91.8 45-1156.7612.3

00666.7Benzo(g,h,i)perylene 87.6 40-1256.7584.3

00666.7Benzo(k)fluoranthene 92.2 45-1156.7615

00666.7Chrysene 90.2 55-1106.7601.7

00666.7Dibenzo(a,h)anthracene 90.6 40-1256.7604.3

00666.7Fluoranthene 95.6 55-1156.7637.7

00666.7Fluorene 89.2 50-1106.7594.7

00666.7Indeno(1,2,3-cd)pyrene 88.2 40-1206.7588

00666.7Naphthalene 84.6 40-1056.7564.3

00666.7Phenanthrene 85.3 50-1106.7569

00666.7Pyrene 89 45-1256.7593.7

001667 Surr: 2-Fluorobiphenyl 77.6 12-10001294

001667 Surr: 4-Terphenyl-d14 97.4 25-13701623

001667 Surr: Nitrobenzene-d5 78.2 37-10701303

QC Page: 2 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: 53871 Instrument ID SVMS8 Method: SW8270

QualRPD Limit

Analysis Date: 12/05/13 08:38 PM

Prep Date: 12/05/13

Analyte Result %REC %RPD

Units:µg/Kg

PQL

Client ID: SeqNo:2568209

MS

Run ID: SVMS8_131205A

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: 13111398-01A MS

0012762-Chloronaphthalene 72.1 45-10513919.9

0012762-Methylnaphthalene 81.7 45-105131043

001276Acenaphthene 73.2 45-11013933.9

001276Acenaphthylene 79.6 45-105131016

001276Anthracene 92.1 55-105131176

048.81276Benzo(a)anthracene 92.7 50-110131232

046.181276Benzo(a)pyrene 93.3 50-110131236

067.471276Benzo(b)fluoranthene 98.7 45-115131326

040.291276Benzo(g,h,i)perylene 78 40-125131036

020.311276Benzo(k)fluoranthene 95.9 45-115131243

055.681276Chrysene 90.7 55-110131213

001276Dibenzo(a,h)anthracene 80.9 40-125131032

092.041276Fluoranthene 103 55-115131402

001276Fluorene 91 50-110131161

031.771276Indeno(1,2,3-cd)pyrene 79.7 40-120131049

001276Naphthalene 74.8 40-10513955

049.461276Phenanthrene 87 50-110131159

0103.51276Pyrene 91.6 45-125131272

003190 Surr: 2-Fluorobiphenyl 64.6 12-10002062

003190 Surr: 4-Terphenyl-d14 105 25-13703337

003190 Surr: Nitrobenzene-d5 66.9 37-10702133

QC Page: 3 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: 53871 Instrument ID SVMS8 Method: SW8270

QualRPD Limit

Analysis Date: 12/05/13 08:58 PM

Prep Date: 12/05/13

Analyte Result %REC %RPD

Units:µg/Kg

PQL

Client ID: SeqNo:2568210

MSD

Run ID: SVMS8_131205A

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: 13111398-01A MSD

919.9012592-Chloronaphthalene 74.8 45-105 3013 2.39942.2

1043012592-Methylnaphthalene 77.7 45-105 3013 6.43978

933.901259Acenaphthene 76.9 45-110 3013 3.58968

101601259Acenaphthylene 82 45-105 3013 1.621032

117601259Anthracene 96.1 55-105 3013 2.91210

123248.81259Benzo(a)anthracene 82.1 50-110 3013 131082

123646.181259Benzo(a)pyrene 102 50-110 3013 7.721336

132667.471259Benzo(b)fluoranthene 104 45-115 3013 3.351371

103640.291259Benzo(g,h,i)perylene 91.7 40-125 3013 14.21195

124320.311259Benzo(k)fluoranthene 101 45-115 3013 3.411286

121355.681259Chrysene 80.7 55-110 3013 12.41071

103201259Dibenzo(a,h)anthracene 91.2 40-125 3013 10.71149

140292.041259Fluoranthene 100 55-115 3013 3.371356

116101259Fluorene 91.3 50-110 3013 0.9661150

104931.771259Indeno(1,2,3-cd)pyrene 92.1 40-120 3013 12.71191

95501259Naphthalene 73.1 40-105 3013 3.71920.1

115949.461259Phenanthrene 91.8 50-110 3013 3.91205

1272103.51259Pyrene 99.2 45-125 3013 6.131353

206203147 Surr: 2-Fluorobiphenyl 66.6 12-100 400 1.72097

333703147 Surr: 4-Terphenyl-d14 109 25-137 400 2.73428

213303147 Surr: Nitrobenzene-d5 66.2 37-107 400 2.372083

The following samples were analyzed in this batch: 1312188-01A 1312188-02A 1312188-03A1312188-04A 1312188-05A 1312188-06A1312188-07A 1312188-08A 1312188-09A1312188-10A 1312188-11A 1312188-12A

QC Page: 4 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: 53888 Instrument ID SVMS8 Method: SW8270

QualRPD Limit

Analysis Date: 12/06/13 12:23 PM

Prep Date: 12/06/13

Analyte Result %REC %RPD

Units:µg/Kg

PQL

Client ID: SeqNo:2572028

MBLK

Run ID: SVMS8_131206A

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: SBLKS1-53888-53888

2-Chloronaphthalene 6.7ND

2-Methylnaphthalene 6.7ND

Acenaphthene 6.7ND

Acenaphthylene 6.7ND

Anthracene 6.7ND

Benzo(a)anthracene 6.7ND

Benzo(a)pyrene 6.7ND

Benzo(b)fluoranthene 6.7ND

Benzo(g,h,i)perylene 6.7ND

Benzo(k)fluoranthene 6.7ND

Chrysene 6.7ND

Dibenzo(a,h)anthracene 6.7ND

Fluoranthene 6.7ND

Fluorene 6.7ND

Indeno(1,2,3-cd)pyrene 6.7ND

Naphthalene 6.7ND

Phenanthrene 6.7ND

Pyrene 6.7ND

001667 Surr: 2-Fluorobiphenyl 77.4 12-10001290

001667 Surr: 4-Terphenyl-d14 108 25-13701804

001667 Surr: Nitrobenzene-d5 74.5 37-10701241

QC Page: 5 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: 53888 Instrument ID SVMS8 Method: SW8270

QualRPD Limit

Analysis Date: 12/06/13 12:43 PM

Prep Date: 12/06/13

Analyte Result %REC %RPD

Units:µg/Kg

PQL

Client ID: SeqNo:2572029

LCS

Run ID: SVMS8_131206A

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: SLCSS1-53888-53888

00666.72-Chloronaphthalene 87.7 45-1056.7584.7

00666.72-Methylnaphthalene 86.9 45-1056.7579.7

00666.7Acenaphthene 83.5 45-1106.7557

00666.7Acenaphthylene 89.4 45-1056.7596.3

00666.7Anthracene 92.5 55-1056.7617

00666.7Benzo(a)anthracene 96.8 50-1106.7645.3

00666.7Benzo(a)pyrene 98.9 50-1106.7659.3

00666.7Benzo(b)fluoranthene 102 45-1156.7682.3

00666.7Benzo(g,h,i)perylene 92.5 40-1256.7616.7

00666.7Benzo(k)fluoranthene 102 45-1156.7678.3

00666.7Chrysene 96.8 55-1106.7645.3

00666.7Dibenzo(a,h)anthracene 91.4 40-1256.7609.7

00666.7Fluoranthene 94.8 55-1156.7632

00666.7Fluorene 89.3 50-1106.7595.7

00666.7Indeno(1,2,3-cd)pyrene 91 40-1206.7606.7

00666.7Naphthalene 85.6 40-1056.7570.7

00666.7Phenanthrene 89.4 50-1106.7596.3

00666.7Pyrene 105 45-1256.7698.7

001667 Surr: 2-Fluorobiphenyl 79.7 12-10001329

001667 Surr: 4-Terphenyl-d14 112 25-13701859

001667 Surr: Nitrobenzene-d5 78.9 37-10701316

QC Page: 6 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: 53888 Instrument ID SVMS8 Method: SW8270

QualRPD Limit

Analysis Date: 12/06/13 01:03 PM

Prep Date: 12/06/13

Analyte Result %REC %RPD

Units:µg/Kg

PQL

Client ID: SeqNo:2572030

MS

Run ID: SVMS8_131206A

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: 1312139-03B MS

0019552-Chloronaphthalene 74.2 45-105201451

0019552-Methylnaphthalene 70.8 45-105201384

001955Acenaphthene 74.9 45-110201464

001955Acenaphthylene 77.6 45-105201518

001955Anthracene 82.7 55-105201618

001955Benzo(a)anthracene 85.4 50-110201670

001955Benzo(a)pyrene 87.1 50-110201704

001955Benzo(b)fluoranthene 89.1 45-115201743

001955Benzo(g,h,i)perylene 90.6 40-125201771

001955Benzo(k)fluoranthene 85.3 45-115201669

001955Chrysene 85.6 55-110201674

001955Dibenzo(a,h)anthracene 87.2 40-125201705

001955Fluoranthene 82.3 55-115201610

001955Fluorene 80 50-110201564

001955Indeno(1,2,3-cd)pyrene 88.9 40-120201739

001955Naphthalene 67.5 40-105201320

001955Phenanthrene 82.1 50-110201605

001955Pyrene 96.1 45-125201879

004888 Surr: 2-Fluorobiphenyl 68.3 12-10003336

004888 Surr: 4-Terphenyl-d14 105 25-13705119

004888 Surr: Nitrobenzene-d5 63 37-10703079

QC Page: 7 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: 53888 Instrument ID SVMS8 Method: SW8270

QualRPD Limit

Analysis Date: 12/06/13 01:23 PM

Prep Date: 12/06/13

Analyte Result %REC %RPD

Units:µg/Kg

PQL

Client ID: SeqNo:2572031

MSD

Run ID: SVMS8_131206A

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: 1312139-03B MSD

1451018922-Chloronaphthalene 74.2 45-105 3019 3.31404

1384018922-Methylnaphthalene 70.8 45-105 3019 3.31339

146401892Acenaphthene 74.3 45-110 3019 4.031406

151801892Acenaphthylene 78 45-105 3019 2.781476

161801892Anthracene 81.6 55-105 3019 4.71544

167001892Benzo(a)anthracene 85.2 50-110 3019 3.471613

170401892Benzo(a)pyrene 86.4 50-110 3019 4.161634

174301892Benzo(b)fluoranthene 87 45-115 3019 5.741646

177101892Benzo(g,h,i)perylene 87.5 40-125 3019 6.721656

166901892Benzo(k)fluoranthene 85 45-115 3019 3.711608

167401892Chrysene 84.8 55-110 3019 4.241604

170501892Dibenzo(a,h)anthracene 85.3 40-125 3019 5.441614

161001892Fluoranthene 79.8 55-115 3019 6.441510

156401892Fluorene 79.5 50-110 3019 3.921504

173901892Indeno(1,2,3-cd)pyrene 86.4 40-120 3019 6.21634

132001892Naphthalene 67.9 40-105 3019 2.631285

160501892Phenanthrene 80.8 50-110 3019 4.831529

187901892Pyrene 90.2 45-125 3019 9.571707

333604729 Surr: 2-Fluorobiphenyl 69.3 12-100 400 1.793277

511904729 Surr: 4-Terphenyl-d14 98 25-137 400 9.984633

307904729 Surr: Nitrobenzene-d5 64.1 37-107 400 1.53033

The following samples were analyzed in this batch: 1312188-13A 1312188-14A 1312188-15A1312188-16A 1312188-17A 1312188-18A1312188-19A

QC Page: 8 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: 53901 Instrument ID SVMS8 Method: SW8270

QualRPD Limit

Analysis Date: 12/09/13 11:34 AM

Prep Date: 12/06/13

Analyte Result %REC %RPD

Units:µg/Kg

PQL

Client ID: SeqNo:2572181

MBLK

Run ID: SVMS8_131209A

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: SBLKS1-53901-53901

2-Chloronaphthalene 6.7ND

2-Methylnaphthalene 6.7ND

Acenaphthene 6.7ND

Acenaphthylene 6.7ND

Anthracene 6.7ND

Benzo(a)anthracene 6.7ND

Benzo(a)pyrene 6.7ND

Benzo(b)fluoranthene 6.7ND

Benzo(g,h,i)perylene 6.7ND

Benzo(k)fluoranthene 6.7ND

Chrysene 6.7ND

Dibenzo(a,h)anthracene 6.7ND

Fluoranthene 6.7ND

Fluorene 6.7ND

Indeno(1,2,3-cd)pyrene 6.7ND

Naphthalene 6.7ND

Phenanthrene 6.7ND

Pyrene 6.7ND

001667 Surr: 2-Fluorobiphenyl 80.4 12-10001340

001667 Surr: 4-Terphenyl-d14 111 25-13701847

001667 Surr: Nitrobenzene-d5 80.9 37-10701349

QC Page: 9 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: 53901 Instrument ID SVMS8 Method: SW8270

QualRPD Limit

Analysis Date: 12/09/13 11:54 AM

Prep Date: 12/06/13

Analyte Result %REC %RPD

Units:µg/Kg

PQL

Client ID: SeqNo:2572183

LCS

Run ID: SVMS8_131209A

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: SLCSS1-53901-53901

00666.72-Chloronaphthalene 83.9 45-1056.7559.7

00666.72-Methylnaphthalene 85.1 45-1056.7567.3

00666.7Acenaphthene 81.1 45-1106.7540.7

00666.7Acenaphthylene 85.9 45-1056.7573

00666.7Anthracene 90 55-1056.7600.3

00666.7Benzo(a)anthracene 96.9 50-1106.7646.3

00666.7Benzo(a)pyrene 100 50-1106.7668.3

00666.7Benzo(b)fluoranthene 103 45-1156.7689.3

00666.7Benzo(g,h,i)perylene 93.2 40-1256.7621.3

00666.7Benzo(k)fluoranthene 100 45-1156.7667

00666.7Chrysene 96.6 55-1106.7644

00666.7Dibenzo(a,h)anthracene 92.1 40-1256.7614

00666.7Fluoranthene 95.1 55-1156.7634.3

00666.7Fluorene 84.4 50-1106.7563

00666.7Indeno(1,2,3-cd)pyrene 92.4 40-1206.7616

00666.7Naphthalene 84 40-1056.7560

00666.7Phenanthrene 88.5 50-1106.7590.3

00666.7Pyrene 106 45-1256.7708.3

001667 Surr: 2-Fluorobiphenyl 78.2 12-10001303

001667 Surr: 4-Terphenyl-d14 111 25-13701843

001667 Surr: Nitrobenzene-d5 81.7 37-10701361

QC Page: 10 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: 53901 Instrument ID SVMS8 Method: SW8270

QualRPD Limit

Analysis Date: 12/09/13 12:54 PM

Prep Date: 12/06/13

Analyte Result %REC %RPD

Units:µg/Kg

PQL

Client ID: SeqNo:2572184

MS

Run ID: SVMS8_131209A

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: 1312196-02A MS

0012772-Chloronaphthalene 89.6 45-105131145

0012772-Methylnaphthalene 90.9 45-105131161

001277Acenaphthene 86.3 45-110131102

001277Acenaphthylene 92.5 45-105131181

001277Anthracene 92.1 55-105131177

001277Benzo(a)anthracene 98.1 50-110131253

001277Benzo(a)pyrene 101 50-110131288

001277Benzo(b)fluoranthene 105 45-115131338

001277Benzo(g,h,i)perylene 93.6 40-125131195

001277Benzo(k)fluoranthene 104 45-115131332

001277Chrysene 99.1 55-110131266

001277Dibenzo(a,h)anthracene 94.1 40-125131202

001277Fluoranthene 93.2 55-115131190

001277Fluorene 89.7 50-110131146

001277Indeno(1,2,3-cd)pyrene 94 40-120131200

001277Naphthalene 90.1 40-105131151

001277Phenanthrene 90.6 50-110131157

001277Pyrene 110 45-125131400

003193 Surr: 2-Fluorobiphenyl 82.3 12-10002627

003193 Surr: 4-Terphenyl-d14 116 25-13703692

003193 Surr: Nitrobenzene-d5 86.5 37-10702761

QC Page: 11 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: 53901 Instrument ID SVMS8 Method: SW8270

QualRPD Limit

Analysis Date: 12/09/13 01:14 PM

Prep Date: 12/06/13

Analyte Result %REC %RPD

Units:µg/Kg

PQL

Client ID: SeqNo:2572186

MSD

Run ID: SVMS8_131209A

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: 1312196-02A MSD

1145013002-Chloronaphthalene 84.6 45-105 3013 3.981100

1161013002-Methylnaphthalene 85.5 45-105 3013 4.31112

110201300Acenaphthene 81.7 45-110 3013 3.61063

118101300Acenaphthylene 87.8 45-105 3013 3.41142

117701300Anthracene 89.5 55-105 3013 1.11164

125301300Benzo(a)anthracene 94 50-110 3013 2.51222

128801300Benzo(a)pyrene 96.7 50-110 3013 2.391257

133801300Benzo(b)fluoranthene 99.4 45-115 3013 3.431293

119501300Benzo(g,h,i)perylene 89.8 40-125 3013 2.271168

133201300Benzo(k)fluoranthene 98.7 45-115 3013 3.651284

126601300Chrysene 95.4 55-110 3013 1.991241

120201300Dibenzo(a,h)anthracene 90.2 40-125 3013 2.421173

119001300Fluoranthene 91.3 55-115 3013 0.2431187

114601300Fluorene 85.8 50-110 3013 2.631116

120001300Indeno(1,2,3-cd)pyrene 90 40-120 3013 2.481171

115101300Naphthalene 85 40-105 3013 3.951106

115701300Phenanthrene 87.9 50-110 3013 1.211143

140001300Pyrene 103 45-125 3013 41345

262703251 Surr: 2-Fluorobiphenyl 79.2 12-100 400 1.972576

369203251 Surr: 4-Terphenyl-d14 112 25-137 400 1.763627

276103251 Surr: Nitrobenzene-d5 83.2 37-107 400 2.122704

The following samples were analyzed in this batch: 1312188-20A 1312188-21A

QC Page: 12 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: R131909 Instrument ID MOIST Method: A2540 G

QualRPD Limit

Analysis Date: 12/05/13 06:00 PM

Prep Date:

Analyte Result %REC %RPD

Units:% of sample

PQL

Client ID: SeqNo:2568478

MBLK

Run ID: MOIST_131205D

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: WBLKS-R131909

Moisture 0.050ND

QualRPD Limit

Analysis Date: 12/05/13 06:00 PM

Prep Date:

Analyte Result %REC %RPD

Units:% of sample

PQL

Client ID: SeqNo:2568468

LCS

Run ID: MOIST_131205D

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: LCS-R131909

00100Moisture 100 99.5-100.50.050100

QualRPD Limit

Analysis Date: 12/05/13 06:00 PM

Prep Date:

Analyte Result %REC %RPD

Units:% of sample

PQL

Client ID: WCR-008-27-062-FY24 SeqNo:2568439

DUP

Run ID: MOIST_131205D

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: 1312188-02A DUP

13.7500Moisture 0 0-0 200.050 6.0712.94

QualRPD Limit

Analysis Date: 12/05/13 06:00 PM

Prep Date:

Analyte Result %REC %RPD

Units:% of sample

PQL

Client ID: SeqNo:2568457

DUP

Run ID: MOIST_131205D

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: 1312213-01B DUP

7600Moisture 0 0-0 200.050 0.42275.68

The following samples were analyzed in this batch: 1312188-01A 1312188-02A 1312188-03A1312188-04A 1312188-05A 1312188-06A1312188-07A 1312188-08A 1312188-09A1312188-10A 1312188-11A

QC Page: 13 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: R131965 Instrument ID MOIST Method: A2540 G

QualRPD Limit

Analysis Date: 12/06/13 10:40 AM

Prep Date:

Analyte Result %REC %RPD

Units:% of sample

PQL

Client ID: SeqNo:2569925

MBLK

Run ID: MOIST_131206C

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: WBLKS-R131965

Moisture 0.050ND

QualRPD Limit

Analysis Date: 12/06/13 10:40 AM

Prep Date:

Analyte Result %REC %RPD

Units:% of sample

PQL

Client ID: SeqNo:2569921

LCS

Run ID: MOIST_131206C

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: LCS-R131965

00100Moisture 100 99.5-100.50.050100

QualRPD Limit

Analysis Date: 12/06/13 10:40 AM

Prep Date:

Analyte Result %REC %RPD

Units:% of sample

PQL

Client ID: SeqNo:2569898

DUP

Run ID: MOIST_131206C

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: 1312196-09B DUP

5.7200Moisture 0 0-0 200.050 10.95.13

QualRPD Limit

Analysis Date: 12/06/13 10:40 AM

Prep Date:

Analyte Result %REC %RPD

Units:% of sample

PQL

Client ID: SeqNo:2569914

DUP

Run ID: MOIST_131206C

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: 1312304-10B DUP

42.4800Moisture 0 0-0 200.050 9.8546.88

The following samples were analyzed in this batch: 1312188-12A 1312188-13A 1312188-14A1312188-15A 1312188-16A

QC Page: 14 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

Project: WC Reed Playfield (030281.0129)

Client: Environmental Quality Management, Inc.Work Order: 1312188

QC BATCH REPORT

Batch ID: R131971 Instrument ID MOIST Method: A2540 G

QualRPD Limit

Analysis Date: 12/06/13 12:00 PM

Prep Date:

Analyte Result %REC %RPD

Units:% of sample

PQL

Client ID: SeqNo:2570224

MBLK

Run ID: MOIST_131206D

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: WBLKS-R131971

Moisture 0.050ND

QualRPD Limit

Analysis Date: 12/06/13 12:00 PM

Prep Date:

Analyte Result %REC %RPD

Units:% of sample

PQL

Client ID: SeqNo:2570220

LCS

Run ID: MOIST_131206D

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: LCS-R131971

00100Moisture 100 99.5-100.50.050100

QualRPD Limit

Analysis Date: 12/06/13 12:00 PM

Prep Date:

Analyte Result %REC %RPD

Units:% of sample

PQL

Client ID: SeqNo:2570203

DUP

Run ID: MOIST_131206D

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: 1312196-12B DUP

11.6100Moisture 0 0-0 200.050 211.38

QualRPD Limit

Analysis Date: 12/06/13 12:00 PM

Prep Date:

Analyte Result %REC %RPD

Units:% of sample

PQL

Client ID: SeqNo:2570209

DUP

Run ID: MOIST_131206D

SPK ValSPK Ref

ValueRPD Ref

ValueControl

Limit

DF: 1

Sample ID: 1312215-04A DUP

55.1200Moisture 0 0-0 200.050 1.7856.11

The following samples were analyzed in this batch: 1312188-17A 1312188-18A 1312188-19A1312188-20A 1312188-21A

QC Page: 15 of 15Note: See Qualifiers Page for a list of Qualifiers and their explanation.

ALS Group USA, Corp

Sample Receipt Checklist

Client Name: EQM - CINCINNATI

Work Order: 1312188

Date/Time Received: 04-Dec-13 10:00

Received by: DS

Checklist completed byeSignature Date

Reviewed by:DateeSignature

Matrices: SoilCarrier name: FedEx

Shipping container/cooler in good condition? Yes No Not Present

Custody seals intact on shipping container/cooler? Yes No Not Present

Custody seals intact on sample bottles? Yes No Not Present

Chain of custody present? Yes No

Chain of custody signed when relinquished and received? Yes No

Chain of custody agrees with sample labels? Yes No

Samples in proper container/bottle? Yes No

Sample containers intact? Yes No

Sufficient sample volume for indicated test? Yes No

All samples received within holding time? Yes No

Container/Temp Blank temperature in compliance? Yes No

Yes No No VOA vials submittedWater - VOA vials have zero headspace?

Water - pH acceptable upon receipt? Yes No N/A

Temperature(s)/Thermometer(s): 4.0 c

Login Notes:

Cooler(s)/Kit(s):

04-Dec-13 04-Dec-13 Diane Shaw Tom Beamish

pH adjusted? Yes No N/ApH adjusted by:

Date/Time sample(s) sent to storage: 12/4/2013 3:45:42 PM

Sample(s) received on ice? Yes No

CorrectiveAction:

Comments:

Client Contacted: Date Contacted: Person Contacted:

Contacted By: Regarding:

SRC Page 1 of 1