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Page 1: DOMO NYLON & INTERMEDIATES · PDF fileDOMO NYLON & INTERMEDIATES Production ... PHENOL is produced by the oxidation of cumene using air to form cumene hydroperoxide,

DOMO NYLON & INTERMEDIATES

IN CHEMICALS WE TRUST.

Page 2: DOMO NYLON & INTERMEDIATES · PDF fileDOMO NYLON & INTERMEDIATES Production ... PHENOL is produced by the oxidation of cumene using air to form cumene hydroperoxide,

DOMO NYLON & INTERMEDIATESPreface

The Business Unit NYLON & INTERMEDIATES represents the core of DOMO Chemicals integratedNylon activities.

One of the main reasons for our success is the provision of high-quality products and a uniquelyhigh level of flexibility and dynamism in meeting the needs and wishes of our customers.

Our vertical integration and the use of cutting-edge technology ensure we keep pace with theglobal competition.

Thanks to continuous investments to improve process efficiency and product quality, our statusas an expert and high-performing partner is secured both now and in the future.

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Luc De Raedt

Business Unit Manager NYLON & INTERMEDIATESManaging Director DOMO Caproleuna GmbH

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DOMO NYLON & INTERMEDIATESProduction

BENZENE

SOLUTION OF AMMONIUM SULPHATE AND UREA

DOMAMID® VIRGIN GRADES

DOMAMON® L26

SULPHURIC ACID

CUMENE

PHENOL

ACETONE

CYCLOHEXANONE

CAPROLACTAM

DOMOGRAN® 45SPECIAL GRADE

INDUSTRIAL GRADE

SULPHUR

SULPHURIC ACID

HYDROXYLAMINE SULPHATE PHENOL

AMMONIA

CYCLOHEXANONE

CAPROLACTAM

AMMONIUM SULPHATE

UREA

POLYAMIDE 6

CUMENE

AMMONIUM SULPHATE

PROPYLENE

TECHNICAL GRADE

PHARMA GRADE

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DOMO Caproleuna GmbH (D) – Chemicals, FertiliserXentrys Leuna GmbH (D) – Nylon 6 basic resinsDOMO Engineering Plastics GmbH (D) – Nylon 6 basic resins, Nylon Compounds

growth = strength

DOMO NYLON & INTERMEDIATES is one of DOMO CHEMICALS’ business units. Throughout theworld the company represents values such as flexibility, speed and production at a high standardof reliability. DOMO NYLON & INTERMEDIATES is positioning itself dynamically within the marketfor nylon and nylon intermediates, and is actively expanding in the market for polymers andsynthetic materials.

history = motivation

In 1994 the DOMO Group, whose roots lie in the manufacture of carpets, integrated the entireproduction chain from raw materials through to polyamides within its production and operatingsystems. At the same time DOMO NYLON & INTERMEDIATES commenced its operations at sitesin Leuna and Premnitz. The successful history of the company, which is still quite recent, isbased upon the high level of motivation and many years of experience possessed by its em-ployees. Successful investments and successful business development have led to continiousgrowth of the company. DOMO NYLON & INTERMEDIATES is ready to face new targets.

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DOMO NYLON & INTERMEDIATESOne of DOMO CHEMICALS’ business units

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PremnitzLeuna

WarsawDresden

Berlin

Hamburg

Cologne

Frankfurt

Stuttgart

Brussels

Munich

ParisPrague

London

ViennaBerne

Milan

Rome

MadridLisbon

Budapest

ZagrebBucharest

Riga

Minsk

Kiev

St PetersburgHelsinki

Oslo

Stockholm

Copenhagen

Athens

Dublin

Rotterdam

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DOMO NYLON & INTERMEDIATESProduct group: ORGANIC INTERMEDIATES

DOMO NYLON & INTERMEDIATESService to the customer

In the ORGANICS group of products DOMO NYLON & INTERMEDIATES again offers its partnersand its customers the complete spectrum of traditional preliminary and intermediate productsfor the synthesis of caprolactam.

By bundling the capacities at the Leuna site we have become a successful major producer ofintermediate and final products in both the European and global markets for chemicals. You canrely on professional standards of service, and high-quality, environmentally friendly products –all from the same source.

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integrated = fast

By the use of complete integrated value creation chains we can serve the wishes of our customerswith flexibility throughout the world. Our strict orientation to the needs of our customers overrecent decades has also ensured that we have a strong position within emerging markets ona global basis. In particular DOMO NYLON & INTERMEDIATES excels by making decisions fast,efficiently and promptly in all divisions of the company.

trust = profit

Trust is of primary importance in our relationships with our customers, our partners and ourstaff. Our business relationships are firmly founded on conducting our business at all levelswith integrity and in a proper manner. Everyone can rely on the professionalism of the otherparty. We at DOMO NYLON & INTERMEDIATES aim to meet these high standards every day andto fully merit this description of our services.

quality = reliability

The continual improvement in our standards of technology takes place within the context ofDOMO’s health, safety and environmental policies. We undertake to carry out the manufactureof our products in safety and to treat natural resources with consideration. In doing this we adherestrictly to local environmental standards and have a proactive approach to any legal requirements.From environmental considerations DOMO NYLON & INTERMEDIATES is again a reliable partnerfor the future.

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Acetone

Ammoniumsulphate

+

Cumene

Phenol

Cyclohexanone

Hydroxylamine sulphate

Caprolactam

Polyamide 6

Sulphuric acid

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DOMO NYLON & INTERMEDIATESProducts: Phenol, acetone

DOMO NYLON & INTERMEDIATESProduct: Cumene

PHENOL is produced by the oxidation of cumene using air to form cumene hydroperoxide,which is decomposed catalytically to produce phenol and acetone.

Use

PHENOL is used in the production of: phenolic resins, bisphenol A, adipic acid, plasticisers,antioxidants and aniline as preliminary product in the manufacture of caprolactam.

ACETONE is a by-product of the synthesis of phenol.

Use

ACETONE TECHNICAL GRADE is used as a solvent and as a starting material in the productionof methyl methacrylate, acetone condensation products and bisphenol.ACETONE PHARMA GRADE is used in pharmaceutical industry with highest requirements onquality. A Major part is used as solvent and for syntheses of pharmaceutical products.

CUMENE is produced by the liquid phase alkylation of benzene using propylene. The planterected in 1998 for the manufacture of cumene uses the most modern methods employed withinthe field of chemical engineering, and guarantees a final product that corresponds to the higheststandards of quality.

Use

CUMENE is mainly used for the manufacture of phenol, acetone and organic peroxides.

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DOMO NYLON & INTERMEDIATESProduct: Caprolactam

DOMO NYLON & INTERMEDIATESProduct: Cyclohexanone

CYCLOHEXANONE is produced by the selective gas-phase hydrogenation of phenol. A speciallydeveloped palladium-based catalyst, coupled with highly developed process technology, makeit possible to achieve the manufacture of a product of outstandingly high quality.

Use

CYCLOHEXANONE is the immediate precursor to caprolactam and is used as a solvent in theadhesives and sealants industry. It is also used as a solvent in the paint and dye industry, andis used in organic syntheses and in the manufacture of pesticides.

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The synthesis of CAPROLACTAM forms the core of chemical production and manufacture atLeuna. In the traditional process this is achieved by the oximation of cyclohexanone withhydroxylamine sulphate to form cyclohexanoxime, which is changed into caprolactam usingoleum by means of the Beckmann rearrangement.

High-quality CAPROLACTAM is the raw material for our Domamid® products. Integration into thenylon manufacturing chain permits DOMO to have not only continuous access to high-qualitycaprolactam, but also to organic and inorganic preliminary products. A comprehensive systemof quality control and quality assurance throughout all stages of production up to and includingthe final product is an important requirement for all Domamid® products.

Specification for Caprolactam

Characteristic Limit Method of testing

Permanganate absorption number max. 5 ISO 8660

Free bases max. 0.5 meq/kg ISO 8661

UV extinction at 290 nm max. 0.05 ISO 7059

Melting point min. 69°C ISO 7060

Water max. 0.05% ISO 760

Color max. 5 Hazen ISO 8112Alkalinity or acidity max. 0.05 meq/kg 83-076

In addition to the continuous monitoring of the process and a final examination of additionalparameters concerning the quality of the product, a gas chromatographic analysis, specificallyfor the manufacture of caprolactam, is used to monitor any trends arising during production.This process of inspection makes it possible to identify the nature and the amount of any traceimpurities.

Use

CAPROLACTAM is the starting material for polyamide 6 granulates, for staple fibres, textileyarns, films, compounds, cast polyamides and N-methylcaprolactam.

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DOMO NYLON & INTERMEDIATES

Product group: DOMAMID® Polyamide 6 basic resins

DOMO NYLON & INTERMEDIATESProduct group: DOMAMID® Polyamide 6 basic resins

DOMAMID® is an engineering plastic with an outstanding list of properties. The ease of workabilitypermits an extraordinary freedom of design. Polyamide 6 is the ideal material for use insideengine compartments, because of its exceptional mechanical properties, its high thermalresistance and to its very good chemical resistance. Increasing standards of safety combinedwith the demands for reductions in weight offer the possibilities for further innovative appli-cations of the product.

Typical applications in which DOMAMID® is used are the automobile, electrical, constructionand furniture industries, in sport and leisure clothing, and in textile floor coverings.

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DOMO NYLON & INTERMEDIATES offer high-quality polyamide 6 granulates under the brandname DOMAMID®. The product range includes grades for technical use and film production aswell as special spinning chips for use in the manufacture of fibres and yarns.

DOMAMID® granulates are manufactured in modern polymerisation plants situated in Germanyat Leuna and Premnitz. We directly supply our customers throughout the world and offer themflexibility together with a rapid service.

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Acetone

Ammoniumsulphate

+

Cumene

Phenol

Cyclohexanone

Hydroxylamine sulphate

Caprolactam

Polyamide 6

Sulphuric acid

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DOMO NYLON & INTERMEDIATES

Product group: DOMAMID® Polyamide 6 for use in spinning

Because of its very good mechanical properties, its resistance to temperature and its verygood abrasion characteristics, DOMAMID® is a multi-purpose synthetic material for use ininjection moulding.

DOMAMID® basic resins are high-quality raw materials for the manufacture of customizedcompounds. Due to the large range of possible ways in which it can be modified, DOMAMID®

possesses all the best attributes for use in innovative product development.

The DOMAMID® range of products contains basic resins of various viscosities. These granulatesare characterised by their natural white colour and by their low moisture content.

All DOMAMID® products are supplied in bulk in silo cars or packed into octabins or big bags.

Viscosity1

DOMAMID® 24 Low viscosity basic resin 2,45 ± 0,05for the production of compounds with very good flow properties

DOMAMID® 27 Medium viscosity basic resin; 2,70 ± 0,05standard quality for the production of compounds

DOMAMID® 28 Medium viscosity basic resin; 2,82 ± 0,06standard quality for the production of compounds

DOMAMID® 32 High viscosity basic resin 3,20 ± 0,05

1 relative solution viscosity: method of determination 1% solution in H2SO4 96% at 20 °C

DOMO NYLON & INTERMEDIATESProduct group: DOMAMID® Polyamide 6 for Engineering plastics

DOMAMID®Polyamide 6 granulates for spinning extrusion are the result of both our own productdevelopment and many years of experience in manufacturing and processing. The granulatesare characterised by a high degree of uniformity and permit a stable operation of the spinningprocess. The yarns and carpets manufactured demonstrate uniform characteristics when dyed.

The DOMAMID® range of products includes raw materials for the manufacture of both monofila-ments and multifilaments, BCF yarns, and highly stabilised polyamide 6 chips for the manufactureof textile yarns using the high-speed process.

DOMAMID® is offered in bright or semidull. A further important characteristic, in terms of quality,is the very low moisture content which has a maximum value of 0.06%.

All DOMAMID® products are supplied in bulk in silo cars or packed into octabins or big bags.

Viscosity2

DOMAMID® 2403T-HS A semidull highly stabilised 2,47 ± 0,03polyamide for the manufacture of textile yarns

DOMAMID® 27 A bright polyamide for the 2,70 ± 0,05manufacture of multifilaments, BCF yarns or yarns for technical applications

DOMAMID® 28 A bright polyamide for the 2,82 ± 0,06manufacture of multifilaments, BCF yarns or yarns for technical applications

DOMAMID® 32 A bright polyamide for the 3,20 ± 0,05extrusion of monofilaments and mutifilaments, tyre cord, fish nets

2 relative solution viscosity: method of determination 1% solution in H2SO4 96% at 20 °C

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DOMO NYLON & INTERMEDIATESProduct group: Ammonium sulphate

DOMO NYLON & INTERMEDIATES

Product group: INORGANIC PRODUCTS

AMMONIUM SULPHATE is an important by-product in the manufacture of caprolactam. Theproduction process permits its manufacture in three different high-quality grades: ammoniumsulphate industrial grade (with an anti-caking agent), ammonium sulphate special grade (withoutan anti-caking agent) and the coarse crystalline product used as fertiliser DOMOGRAN® 45. For further information about DOMOGRAN® 45 please consult our fertiliser brochure or visitdomochemicals.com.

Specification for ammonium sulphate industrial grade

Parameter Unit Limiting value Method

ammonium sulphate content wt -% min. 99.00 84-512

NH4-nitrogen content wt -% min. 21.00 84-512

water content wt -% max. 0.2 84-503

Particle size 0.4 until 1.6 mm wt -% min. 90 84-539

content of conditioning wt -% max. 0.05 84-505

Use

AMMONIUM SULPHATE has many different uses: e.g. for making paper, wood and textilesbecome flame resistant; as an additive in the manufacture of fire extinguishing agents, as anadditive in the particle board and pulp industry, in the manufacture of special fertilisers andas a deliming agent in the leather industry.

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For several decades DOMO NYLON & INTERMEDIATES has integrated traditional inorganic productsinto its production chain. Large volumes of basic chemicals as well as purer products aremarketed to our customers and partners throughout the world. Among the high-quality basicchemicals included in our INORGANICS portfolio are ammonium sulphate for technical use,hydroxylamine sulphate and sulphuric acid. Throughout its portfolio DOMO NYLON & INTERME-DIATES is noted for its dependability and reliability. We provide optimum sales and logisticssolutions as part of the services that we offer to our customers throughout the world. Our per-sonalised and professional service is available to you at our various locations.

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Acetone

Ammoniumsulphate

+

Cumene

Phenol

Cyclohexanone

Hydroxylamine sulphate

Caprolactam

Polyamide 6

Sulphuric acid

Page 10: DOMO NYLON & INTERMEDIATES · PDF fileDOMO NYLON & INTERMEDIATES Production ... PHENOL is produced by the oxidation of cumene using air to form cumene hydroperoxide,

Notes

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Page 11: DOMO NYLON & INTERMEDIATES · PDF fileDOMO NYLON & INTERMEDIATES Production ... PHENOL is produced by the oxidation of cumene using air to form cumene hydroperoxide,

Premnitz site

DOMO Engineering Plastics GmbHPaul-Schlack-Straße 14727 PremnitzGermany

Phone +49 3386 24-2261Fax +49 3386 [email protected]

Leuna site

DOMO Caproleuna GmbHAm Haupttor – Bau 310106234 LeunaGermany

Phone +49 3461 43-2200Fax +49 3461 [email protected]

Date of issue: October 2013

DOMO NYLON & INTERMEDIATES

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