InfraLum FT - 02InfraLum FT - 02
FT (Mid)IR SpectrometerFT (Mid)IR Spectrometer
CERTIFICATIONCERTIFICATION
FOURIER TRANSFORM SPECTROPHOTOMETERFOURIER TRANSFORM SPECTROPHOTOMETER
DEVICE LAYOUTDEVICE LAYOUT
LightSource
Interferometer Focusing Optics
Sample Compartment
Detector
PRINCIPLE OF PRINCIPLE OF OPERATIONOPERATION
Permanently aligned “Double Cats Eye” interferometer ensures stability and durability.
1 – Light source2 – Heat shield3-4 – Focusing spherical mirrors 5 – Diaphragm6 – “Double Cats Eye” interferometer 7 – Flat mirror8, 9,11 – Toric mirrors10 – Sample Compartment12 – Detector
ADVANTAGEADVANTAGESS
high throughput
high photometric accuracy
high selectivity
simultaneous analysis of several components
variability of accessories
ROUTINE MEASUREMENTROUTINE MEASUREMENT
Take a Sample
Fill a Cell
Placethe Cell
Measure
Complete a Report
Condition the Sample
ROUTINE MEASUREMENTROUTINE MEASUREMENT
Take a Sample
Fill a Cell
Placethe Cell
Measure
Complete a Report
Condition the Sample
ROUTINE MEASUREMENTROUTINE MEASUREMENT
Take a Sample
Fill a Cell
Placethe Cell
Measure
Complete a Report
Condition the Sample
ROUTINE MEASUREMENTROUTINE MEASUREMENT
Take a Sample
Fill a Cell
Placethe Cell
Measure
Complete a Report
Condition the Sample
Calcium gluconate transmission spectrum
ROUTINE MEASUREMENTROUTINE MEASUREMENT
Take a Sample
Fill a Cell
Placethe Cell
Measure
Complete a Report
Condition the Sample
Comparison with the standard spectrum
MAIN APPLICATIONSMAIN APPLICATIONS
Functional group analysis Unknown substance identification Pharmaceuticals identification (RF
Pharmacopoeia) Oil content in water and in soil (DIN) Oil-in-water pollutant source identification
MAIN APPLICATIONSMAIN APPLICATIONS
Environmental Monitoring Air and emission measurement Determination of water oil polluters Detection of the presence of
ozone-destructing substance Concentration of oil in water
measurement Petrochemistry Fractional composition of oils Oil-type analysis Benzene content in gasoline Octane number, cetane number
Determination of gas composition Testing the composition of polymer
films and coatings
Industry
Pharmacology Determination of the authenticity of
medicine preparations using IR reference standards
Quality control of medicine preparations using IR reference standards
Quality assurance of organic raw materials
Forensic investigations At expert laboratories for
qualitative analysis: drugs, medicine, pigments, gas and etc. sample identification
AIR POLLUTANTS CONTROLAIR POLLUTANTS CONTROL
Pollutant Detection limit, mg/m3
Carbon monoxide 0,11
Carbon dioxide 0,034
Water 0,18
Hydrogen chloride 0,11
Ammonia 0,033
Sulfur dioxide 0,25
Multi-component analysis of typical industrial air pollutants.
Multi-pass gas cell, L = 2,1 m.
OIL CONTENT IN WATER AND IN SOILOIL CONTENT IN WATER AND IN SOIL
DIN 38409 H18
and Certificate of validation M 01-39-2000
Measured content range: from 0.025 to 50 mg/l
Automatic calculation based on absorption peaks
2925. 2960, 3055 cm-1
Quartz cell, L = 4 cm
OIL POLLUTANT IDENTIFICATIONOIL POLLUTANT IDENTIFICATION
Identification of oil-in-water pollution source by Department of Ecology rule No 241
Automatic calculation based on 12 absorption peaks (1600, 1375, 1310, 1170, 1030, 970, 870, 810, 770, 750, 720, 695 cm-1).
Sealed Cell, NaCl, L=0.04-0.10 mm
HHC IDENTIFICATIONHHC IDENTIFICATION
Comparison of the measured spectrum with the prohibited halogenated hydrocarbons database using Euclidian distance.
Sample: C2F4Br2
Gas cell, KBr, L=10 cm
PHARMACEUTICALS PHARMACEUTICALS IDENTIFICATIONIDENTIFICATION
Comparison of the measured spectrum with the RF Pharmacopoeia database using Euclidian distance.
Sample: Calcium Gluconate
Demountable cell,
Nujol Suspension.
PERFUME RAW MATERIALS QCPERFUME RAW MATERIALS QC
4000 3000 2000 1000
100
80
60
40
20
0
Волн. число
ПропусканиеDetermination of contaminant in perfume raw materials.
Sample: CH3-(CH2)10-(CH2-CH2O)2-OSO3Na
Demountable cell, CaF2, L=0.05 cm.
Black - a standard sample
Red - a contaminated sample.
HARDWEARHARDWEAR
Parameter Specification
Optical System Single Beam Optics
Interferometer Proprietary “Double Cats Eye” interferometer, Sealed and Desiccated
Beam Splitter Multi-layer Coated KBr plate
Light Source High Temperature Ceramic
Detector Pyroelectric (LiTaO3 or DTGS)
Scanning speed 1.6; 2; 3.2; 5 mm/sec
HARDWEARHARDWEAR
Parameter Specification
Size 580х515х295 mm
Weight 37 kg
Power Requirements ~ 110/220 V, 50/60 Hz
Operating ConditionsTemperature: 10oC to 35oC, Humidity: Below 80%
Typical analysis time 60 sec
Data acquisition and processing
PC data station, Laptop
SPECIFICATIONSSPECIFICATIONS
Parameter Specification
Spectral resolution 0.5, 1, 2, 4, 8, 16 cm-1
Spectral range 6 500 350 cm-1
Wavenumber accuracy ± 0.02 cm-1
Noise level of 100% transmission line (spectral range: 200050 cm-1; resolution: 4 cm-1)
< 0.08 %