1204.22
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
December 16, 2011
Prepared Under USEPA Brownfields Grant # 2B-00T18101-0
For:
City of Oakland
250 Frank H. Ogawa Plaza, 4th Floor
Oakland, California 94612
Prepared By:
Northgate Environmental Management, Inc.
300 Frank H. Ogawa Plaza, Suite 510
Oakland, California 94612
Dennis Laduzinsky, C.E.G., R.E.A.
Principal
Anya Starovoytov
Staff Environmental Scientist
Phase II Environmental Site Assessment ii December 16, 2011
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APN 004-049-001
Oakland, California
TABLE OF CONTENTS
ACRONYMS AND ABBREVIATIONS .................................................................................... iii
1.0 INTRODUCTION AND SCOPE OF SERVICES ......................................................... 1
2.0 BACKGROUND ............................................................................................................... 3
2.1 SITE DESCRIPTION ........................................................................................................... 3 2.2 PREVIOUS INVESTIGATIONS ............................................................................................. 3
3.0 SOIL AND GROUNDWATER INVESTIGATION ...................................................... 6
3.1 INVESTIGATION METHODS ............................................................................................... 6 3.1.1 Sampling and Analysis ............................................................................................... 6
3.1.2 Groundwater Monitoring Well Re-Development and Sampling ................................ 8
3.1.3 Data Evaluation ........................................................................................................... 9 3.2 INVESTIGATION RESULTS ............................................................................................... 10
3.2.1 Scanning for Underground Utilities .......................................................................... 10 3.2.2 Subsurface Conditions .............................................................................................. 10 3.2.3 Soil Quality ............................................................................................................... 10
3.2.4 Grab-Groundwater Quality ....................................................................................... 13 3.3 QUALITY ASSURANCE/QUALITY CONTROL (QA/QC) .................................................... 15
4.0 CONCLUSIONS AND RECOMMENDATIONS ........................................................ 17
5.0 LIMITATIONS ............................................................................................................... 19
6.0 REFERENCES ................................................................................................................ 20
TABLES
1 Soil Sample Analytical Results – TPH, VOCs, SVOCs, Pesticides, and PCBs
2 Soil Sample Analytical Results – Metals
3 Soil Sample Analytical Results – Soluble Lead
4 Grab Groundwater Sample Analytical Results – TPH and VOCs
5 Grab Groundwater Sample Analytical Results - Metals
6 Groundwater Monitoring Well Sample Analytical Results – TPH and VOCs
7 Groundwater Monitoring Well Sample Analytical Results – Metals
8 Quality Control Sample Assessment – Soil
9 Quality Control Sample Assessment – Groundwater
FIGURES
1 Site Location Map
2 Site Plan
APPENDICES
A Boring Permits
B Boring Logs
C Laboratory Analytical Reports
Phase II Environmental Site Assessment iii December 16, 2011
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APN 004-049-001
Oakland, California
ACRONYMS AND ABBREVIATIONS
APN Assessor’s Parcel Number
BART Bay Area Rapid Transit
bgs Below Ground Surface
BTEX Benzene, toluene, ethylbenzene, and xylenes
Caltrans California Department of Transportation
CHHSL California Human Health Screening Level
DCA Dichloroethane
DCB Dichlorobenzene
DCE Dichloroethylene
DTSC Department of Toxic Substances Control
EPA United States Environmental Protection Agency
ESI Environmental Solutions, Inc.
ESL Environmental Screening Levels
LCS/LCSD Laboratory Control Spike/Laboratory Control Spike Duplicate
LUST Leaking Underground Storage Tank
MCL Maximum Contaminant Level
µg/kg Microgram per kilogram
µg/L Microgram per liter
mg/kg Milligram per kilogram
mg/L Milligram per liter
MRL Method Reporting Limit
MS/MSD Matrix Spike/Matrix Spike Duplicate
MTBE Methyl tert-Butyl Ether
ORP Oxygen Reducing Potential
PCB Polychlorinated Biphenyls
PCE Tetrachloroethylene
PID Photoionization Detector
PRG Preliminary Remedial Goals
PSI Professional Service Industries, Inc.
PVC Polyvinyl Chloride
QA/QC Quality Assurance/Quality Control
ROW Right Of Way
RPD Relative Percent Difference
RSL Regional Screening Levels (U.S. EPA)
RWQCB Regional Water Quality Control Board
SAP Sampling and Analysis Plan
STLC Soluble Threshold Limit Concentration
SVOC Semi-volatile Organic Compounds
TCA Trichloroethane
TCE Trichloroethylene
TCLP Toxicity Characteristic Leaching Procedure
TPH-d Total Petroleum Hydrocarbons as Diesel
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TPH-g Total Petroleum Hydrocarbons as Gasoline
TPH-o Total Petroleum Hydrocarbons as Motor Oil
TTLC Total Threshold Limit Concentration
USCS Unified Soils Classification System
UST Underground Storage Tank
VCA Voluntary Cleanup Agreement
VOC Volatile Organic Compounds
WET Waste Extraction Test
Phase II Environmental Site Assessment 1 December 16, 2011
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1.0 INTRODUCTION AND SCOPE OF SERVICES
This report presents the results of a Phase II Environmental Site Assessment performed by
Northgate Environmental Management, Inc. (Northgate) for the City of Oakland at 500 Kirkham
Street (Assessor’s Parcel Number (APN) 004-049-001) in Oakland, Alameda County, California
(the Site). The Site consists of an approximate 2.76-acre (500 feet by 250 feet) parcel of land
primarily occupied by an asphalt-paved lot utilized as a construction staging area and storage
yard. The Site is currently owned by the California Department of Transportation (Caltrans). A
Site Location Map is shown on Figure 1 and a Site Plan is shown on Figure 2.
The purpose of the investigation has been to evaluate soil and groundwater quality conditions at
the Site to evaluate possible impacts to potential redevelopment, including impacts to future
commercial or residential occupants and potential worker exposure to contaminants during
construction. A specific redevelopment plan has not been determined at this time. However, for
the purpose of this report we have assumed that redevelopment will include both residential and
commercial uses. This investigation was performed under the United States Environmental
Protection Agency (EPA) Brownfield Assessment Grant # 2B-00T18101-0 for both hazardous
substances and petroleum hydrocarbons. The work was performed in accordance with the
following documents:
Quality Assurance Project Plan, West Oakland Development Area, Oakland, California,
Northgate, September 8, 2009 (the QAPP), and
Sampling and Analysis Plan, Phase II Soil and Groundwater Investigation, 500 Kirkham
Street, APN 004-049-001, Oakland, California, Northgate, August 8, 2011 (the SAP).
According to the Phase I Environmental Site Assessment, 500 Kirkham Street, APN 004-049-
001, Oakland, California dated June 6, 2011, prepared by Northgate, the Site was occupied by
residences and commercial/industrial development (including a variety of commercial/industrial
warehouse and manufacturing operations such as clothing, canned goods, paper products, and
others) from before the 1930s through the mid-1950s. From the mid-1950s through the early
1990s, the entire Site, with the exception of the southwest quarter, was covered by an elevated
section of the Interstate 880 freeway. During this time, the southwest portion of the Site was
occupied by a chemical repackaging operation and an automotive and truck repair businesses.
The freeway was removed from the Site in the early 1990s at which time the entire Site reverted
back to commercial and industrial land use.
The Site is listed as Smilo Chemical Company on the VCP, Envirostor, CERC-NFRAP, RCRA-
SQG, and FINDS databases. The Site is also listed as J & A Truck Repair on the RCRA-SQG,
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APN 004-049-001
Oakland, California
FINDS, HIST CORTESE, LUST, Alameda County CS, and HAZNET databases. These listings
are related to historic use, storage, and release of hazardous materials on the southwest portion of
the Site. Available information indicates that 4,700 cubic yards of contaminated soil was
excavated and removed from the southwest portion of the Site in the 1990s. Groundwater
beneath this portion of the Site reportedly contained a variety of contaminants, including
petroleum hydrocarbons and volatile organic compounds (VOCs). The Site is currently listed as
an open clean-up project undergoing site assessment on the Geotracker website maintained by
the Regional Water Quality Control Board (RWQCB) as of December 30, 1995. The
Department of Toxic Substance Control (DTSC) is listed as the lead agency for oversight.
Within the DTSC Envirostor database, the Site status is listed as inactive and requiring
evaluation as of September 3, 2010. It is understood that the City of Oakland is assisting the
current property owner, Caltrans, in assessing environmental conditions at the Site to evaluate
potential redevelopment options.
The scope of work for this investigation included the following services:
Scanning the property with a metal detecting device to evaluate the Site for the possible
presence of underground utilities;
Collecting soil samples from 16 soil borings advanced to depths of 10 to 15 feet below
ground surface (bgs) across the Site;
Collecting grab groundwater samples from nine of the boring locations;
Re-developing four on-Site groundwater monitoring wells and collecting groundwater
samples;
Selectively analyzing soil and groundwater samples for total petroleum hydrocarbons
(TPH), VOCs, semi-volatile organic compounds (SVOCs), organochlorine pesticides,
polychlorinated biphenyls (PCBs), and metals; and
Preparing this report.
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2.0 BACKGROUND
2.1 Site Description
The Site is located at 500 Kirkham Street in Oakland, California. The Site consists of an
approximate 2.76 acre (500 feet by 250 feet) parcel of land bounded by 7th
Street on the north, 5th
Street on the south, Union Street on the east, and Kirkham Street on the west. The Site consists
of a paved lot currently used as a storage yard and staging area for a construction company. A
paved, inclined roadway previously used for truck driver training is present on the northern
portion of the Site and an office trailer is located along the western property boundary. A Bay
Area Rapid Transit (BART) right-of-way (ROW) easement transects the southwest corner of the
Site. The southwest portion of the Site situated between the BART easement and Kirkham and
5th
Streets consists of vacant land.
The Site originally consisted of bay-margin wetlands that were partially filled in between 1866
and 1890. In 1902, the Site was bisected between 7th
and 5th
Streets by Poplar Street. Land use
at that time consisted of a mix of residences and commercial/industrial activities. A railroad spur
track entered the southwestern portion of the Site from 5th
Street to serve commercial and
industrial operations that were present on the Site between 1912 and the mid-1950s. Between
the mid-1950s and 1990, the majority of the Site was covered diagonally from northwest to
southeast by an elevated section of the Nimitz (Eastshore) Freeway. The freeway was removed
and relocated about 300 feet south of the Site in the mid-1990s.
Between 1954 and 1984, the southwestern portion of the Site was occupied by Smilo Chemical
Company, a chemical repackaging business. Between 1984 and 1994, this portion of the Site
was occupied by J&A Truck Repair. The Site is currently owned and managed by Caltrans who
acquired the Site in 1994.
2.2 Previous Investigations
A soil sampling program performed in 1981 by the Alameda County Department of Health and
Safety indicated the presence of heavy metals and pesticides in shallow soil at the Site.
However, the actual sampling depths and locations were not reported. In 1992, GeoResource
Consultants collected soil samples from depths of 1 and 3 feet bgs at one location along the
southwestern corner of the Site. Organochlorine pesticides and metals were not detected above
the laboratory method reporting limits (MRLs) in either sample with the exception of lead, which
was detected in the 1-foot sample at 81 milligrams per kilogram (mg/kg). Results from a
California Waste Extraction Test (WET) analysis indicated that soluble lead concentrations did
not exceed the Soluble Threshold Limit Concentration (STLC) for lead.
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APN 004-049-001
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In 1994, Environmental Solutions, Inc. (ESI) performed an investigation that included collecting
six wipe samples from interior walls and floors of the on-Site warehouse and collecting soil and
groundwater samples from 12 locations in the vicinity of an underground storage tank (UST)
present along the western Site boundary (north of the BART ROW) at that time. Borings were
drilled to depths of 4 to 13 feet bgs, with soil samples collected at 1, 5, and 8 feet bgs submitted
for chemical analysis. Analytical results indicated that soils in the vicinity of the UST were
impacted by gasoline, oil and grease, lead, acetone, BTEX (benzene, toluene, ethylbenzene, and
xylenes), and SVOCs. A WET test performed on samples near the UST, former sumps, and an
on-Site railroad spur indicated soluble lead concentrations above the STLC. Six boring locations
were drilled to approximately 10 to 13 feet bgs for collecting groundwater samples. According
to ESI, groundwater beneath the Site was impacted by petroleum hydrocarbons, metals, VOCs
and unknown compounds in the diesel and motor oil range. Heavy metals and VOCs detected in
groundwater exceeded their respective maximum contaminant levels (MCLs, the State primary
drinking water standard), established under Title 22 of the California Code of Regulations.
In 1994, Caltrans entered into a Voluntary Cleanup Agreement (VCA) with the DTSC for the
Cypress Freeway Relocation Project and East Bay Municipal Utility District Sewer Line
Realignment in Oakland and Emeryville, California. The reconstruction project covered 34
separate properties, including the 500 Kirkham Street property. The VCA was subsequently
amended twice in 1996, and once in each 1997, 1999, and 2002.
According to a Site investigation report prepared by Professional Service Industries, Inc. (PSI),
all on-Site structures were demolished in April 1995 and one approximately 2,000-gallon UST
was removed from the Site on August 30, 1995. Petroleum hydrocarbons were detected in soil
and groundwater samples collected from the UST excavation pit. Heavy metals were detected in
a composite sample collected from the excavated soil stockpile. In November 1995, the
southwest portion of the Site was over-excavated and a total of 92 confirmation samples were
collected from the excavation pit. Twenty-five chemicals were detected in the soil samples,
including PCBs, which were found at concentrations exceeding the Region 9 Preliminary
Remedial Goals (PRGs), established by the EPA. The Envirostor database record for the Site,
maintained by the DTSC, notes the completion of soil excavation to 6 feet bgs. However, it
should be noted that a formal report describing the details of this remediation work could not be
located for review. In 2000, PSI installed four monitoring wells at the Site and collected soil
samples from depths of 6.5 and 7 feet bgs. Low levels of VOCs, SVOCs, and heavy metals were
detected in the soil samples. Low levels of TPH as gasoline and diesel, VOCs, SVOCs, and
heavy metals were detected in groundwater beneath the Site. The report concluded that
groundwater monitoring should continue at the Site on a quarterly basis. However, groundwater
Phase II Environmental Site Assessment 5 December 16, 2011
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monitoring data for 2001 and beyond could not be located and it is unclear whether quarterly
groundwater monitoring ever occurred at the Site.
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3.0 SOIL AND GROUNDWATER INVESTIGATION
3.1 Investigation Methods
3.1.1 Sampling and Analysis
Northgate performed soil and groundwater sampling at the subject Site on August 10 and 11,
2011. Field work included scanning the property with remote sensing equipment to evaluate the
Site for the possible presence of underground utilities. Subsequent to scanning, nine borings
were advanced to depths of 10 to 15 feet bgs for collecting soil and groundwater samples. Seven
additional borings were advanced to a depth of 10 feet bgs for collecting soil samples.
Approximate boring locations are shown on Figure 2. Permits for the borings were obtained
from the Alameda County Public Works Department and are presented in Appendix A.
The borings were advanced using a truck-mounted direct push GeoProbe sampling rig. During
sampling, continuous cores of subsurface materials were collected in clear acetate liners. Upon
removing the sampler from the borehole, the acetate liner containing the soil core was opened at
various intervals, and the soils were visually inspected and screened using a photoionization
detector (PID) for the possible presence of contamination. Borings were logged in the field in
accordance with the Unified Soils Classification System (USCS). Copies of the boring logs are
attached in Appendix B.
Soil samples were collected for chemical analysis at approximate depths of 1, 5, and 7-13 feet
bgs from borings B-1 through B-16. Sample intervals selected for chemical analysis were cut
from the liners, sealed with Teflon tape and plastic caps, labeled, and stored on ice in a cooler for
transport to the testing laboratory under appropriate chain-of-custody control. Soil samples
selected for VOC analysis were collected directly from a cut liner using a TerraCore™ sampler
and were immediately transferred to a pre-weighed laboratory-supplied glass vial preserved with
sodium bisulfate.
Duplicate soil samples were collected at 5 feet bgs from boring B-5 and at 1 foot bgs from
borings B-7 and B-12. Duplicate soil samples were collected immediately adjacent to the
primary sample. The laboratory was instructed to perform analysis on adjoining ends of the two
core samples.
Soil samples collected from depths of approximately 1 and 5 feet bgs were analyzed for the
following constituents:
TPH as diesel and oil (TPH-d, TPH-o) using EPA Method 8015;
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TPH as gasoline (TPH-g) using EPA Method 8260;
VOCs using EPA Method 8260;
PCBs using EPA Method 8082;
SVOCs using EPA Method 8270; and
17 Metals using EPA 6000/7000 series.
Soil samples collected from a depth of 1 foot bgs were additionally analyzed for:
Organochlorine pesticides using EPA Method 8081.
Soil samples collected from 7-10 feet bgs were initially held pending the results of the 1 foot and
5 foot bgs samples. The following deeper samples were analyzed following receipt of the
shallow soil sample results:
The 10-foot sample from boring B-11 analyzed for TPH-g and VOCs; and
The 9-foot sample from boring B-2 and 8-foot sample from boring B-8 analyzed for
TPH-o and total lead.
Grab groundwater samples were collected at nine borings by lowering a perforated PVC casing
into the borehole and collecting groundwater samples from the casing using a peristaltic pump
with dedicated tubing. A duplicate groundwater sample was collected from boring B-12.
Groundwater samples were placed in laboratory-supplied glassware, labeled, and stored on ice in
a cooler for transport to the testing laboratory under appropriate chain-of-custody control.
Groundwater samples were analyzed for:
TPH-d and TPH-o using EPA Method 8015;
TPH-g using EPA Method 8260;
VOCs using EPA Method 8260; and
17 Metals (dissolved) using EPA 6000/7000 series.
Soil and groundwater samples were analyzed at Torrent Laboratory of Milpitas, California. All
drilling equipment was steam-cleaned or washed and rinsed prior to use at each boring location.
After completion of sampling activities, all borings were backfilled with neat cement in
accordance with the Alameda County Public Works Agency, Water Resources Section
requirements. All soil cuttings generated during this investigation were stored on the Site in a
sealed 55-gallon drum.
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3.1.2 Groundwater Monitoring Well Re-Development and Sampling
Four groundwater monitoring wells are located on the Site. Well JA-1 is located along the
western property boundary (adjacent to Kirkham Street) and wells JA-2 through JA-4 are located
on the southern portion of the Site (immediately north of the BART ROW). An additional
unmarked well, MW-X, was also observed adjacent to well JA-4. Northgate was unable to
access well JA-1 due to a large storage container which was staged on top of the well box. The
remaining wells were assessed in the field and well construction specifications including depth,
casing diameter and material, surface completion, well security, and installed sampling
equipment were recorded. The wells were re-developed on August 10 and 11, 2011 by gentle
surging and pumping using a disposable bailer and a peristaltic pump with dedicated tubing.
Groundwater field parameters of temperature, pH, electrical conductance, dissolved oxygen, and
oxygen reducing potential (ORP) were recorded at regular intervals during re-development.
Well re-development continued until the water was relatively free of sand, silt, and turbidity and
the field parameters had stabilized to within 10 percent of previous readings. A minimum of 10
casing volumes were purged from each well during re-development. Purge water was stored on-
Site in sealed and labeled 55-gallon drums.
Wells JA-2, JA-3, and JA-4 were sampled on August 15, 2011 using a peristaltic pump with
dedicated tubing. The tubing was positioned at the approximate middle of the water column of
each well. The pumping rate was maintained to control drawdown to less than 0.3 feet. The
pumping rate was maintained below 100 milliliters per minute when collecting samples for
volatile constituent analysis. A duplicate groundwater sample was collected from well JA-4.
All samples were placed in laboratory supplied containers, labeled, and stored on ice in a cooler
for transport to the laboratory under appropriate chain-of-custody control. Samples were
analyzed at Torrent Laboratory of Milpitas, California. Each monitoring well groundwater
sample was analyzed for:
TPH-d and TPH-o using EPA Method 8015;
TPH-g using EPA Method 8260;
VOCs using EPA Method 8260; and
17 Metals using EPA 6000/7000 series.
All non-dedicated sampling equipment was decontaminated by washing with Alconox (a
laboratory-grade detergent) and rinsing with deionized water before use at each well.
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3.1.3 Data Evaluation
Chemical test results from soil samples collected during this investigation were evaluated using
Environmental Screening Levels (ESLs) established by the California RWQCB (Screening for
Environmental Concerns at Sites with Contaminated Soil and Groundwater, Interim Final,
November 2005, Revised May 2008) and the Total Threshold Limit Concentrations (TTLCs)
established by the State of California (Title 22, California Code of Regulations).
The ESLs were developed to address environmental protection goals presented in the Water
Quality Control Plan for the San Francisco Bay Basin (Basin Plan; RWQCB, 2006), including
protection of groundwater and surface water resources, protection of human health, protection
against vapor intrusion into buildings, and other concerns. The ESLs are developed using a
tiered approach to environmental risk assessment. For site characterization studies such as the
present investigation, Tier 1 ESLs are used as a general screening guide to determine whether
additional investigation, remedial actions, or risk assessment may be required. The Tier 1 ESLs
are not regulatory cleanup standards, and the presence of a chemical at a concentration above the
Tier 1 ESL does not necessarily indicate that adverse impacts to human health or the
environment are occurring, but rather, indicate that a potential for adverse risk may exist and that
additional evaluation may be warranted. The Tier 1 ESLs are conservative, and are generally
based on an assumption of future residential land use, and the potential use of groundwater as
drinking water; assumptions that may not necessarily be applicable to a particular site.
According to the RWQCB Basin Plan, groundwater in the vicinity of the subject Site is classified
as a potential drinking water supply. This report also considers RWQCB ESLs for commercial /
industrial land use and ESLs for evaluating direct human exposure to soil for construction
workers. Based on a reduction in blood lead level benchmarks for children, the DTSC in
September 2009 lowered the established California Human Health Screening Level (CHHSL) for
lead in residential land use to 80 parts per million (ppm) and in commercial/industrial land use to
320 ppm. Those screening levels are used in place of the RWQCB ESLs for lead in soil in this
report. The TTLCs are used to define a waste as a hazardous or non-hazardous waste for landfill
disposal purposes, and do not necessarily have any relation to health risk evaluation.
Groundwater chemical test results were compared to the MCLs (the State Primary Drinking
Water Standards) established under Title 22 of the California Code of Regulations and the ESLs
for evaluating potential vapor intrusion into buildings. Where ESLs were not established, the US
EPA Regional Screening Levels (RSLs) for tap water are provided.
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3.2 Investigation Results
3.2.1 Scanning for Underground Utilities
Scanning the boring locations with remote sensing equipment (e.g., metal detecting devices) did
not indicate the presence of underground utilities in the vicinity of the borings.
3.2.2 Subsurface Conditions
The majority of the Site is paved with an approximate 4-inch asphaltic concrete that was drilled
through prior to soil sampling each boring, with the exception of borings B-3 and B-16. Boring
B-3 was advanced along the inclined roadway in an unpaved area and boring B-16 was advanced
in the southwest corner of the Site, within a small vacant unpaved lot. Subsurface soils
encountered at the Site consisted primarily of well graded sand. Well graded sand with clay and
clayey sand were encountered in several borings at depths typically ranging from 5 to 10 feet
bgs. Groundwater was encountered in nine of the 16 borings at depths between 6.5 to 8.5 feet
bgs in borings B-1, B-4, B-8, B-11, and B-12 and at depths of 3.5 to 5.5 feet bgs in borings B-5,
B-13, and B-16.
3.2.3 Soil Quality
Soil sample analytical results are presented in Tables 1 and 2, and the laboratory analytical
reports are presented in Appendix C. As shown in Table 1, TPH-g was not detected above the
laboratory MRL in any of the soil samples collected at the Site, with the exception of the 5-foot
sample collected from boring B-3 (0.11 mg/kg) and the 6-foot sample collected from boring B-
11 (150 mg/kg). These borings were advanced at the top of the inclined roadway (B-3) and
immediately west of the office trailer, in close proximity to the location of the former on-Site
UST (B-11), respectively. The measured concentration of TPH-g from boring B-11 (150 mg/kg)
exceeds the Tier 1 and Commercial/Industrial ESLs of 83 mg/kg but does not exceed the
construction worker exposure ESL of 4,200 mg/kg for TPH-g. The 10-foot sample from boring
B-11 was analyzed for TPH-g to evaluate the vertical extent of elevated TPH-g concentrations.
The 10-foot sample did not contain TPH-g above the laboratory MRL of 0.1 mg/kg.
TPH-d was reported in five soil samples collected from the 5-6 foot depth in borings B-3, B-5,
B-11, B-12, and B-15. TPH-d concentrations range from 2.0 to 8.1 mg/kg and do not exceed
ESLs for residential or commercial land use.
TPH-o was detected above the laboratory MRLs in all but five of the samples analyzed, at
concentrations ranging from 4 to 960 mg/kg. Concentrations of TPH-o in three soil samples, the
5-foot sample from B-8 (550 mg/kg), the 1-foot sample from B-9 (720 mg/kg), and the 1-foot
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sample from B-13 (960 mg/kg), exceed the Tier 1 ESL of 370 mg/kg for TPH-o. The elevated
concentrations of TPH-o do not exceed the commercial/industrial land use ESL of 2,500 mg/kg
or the construction worker exposure ESL of 12,000 mg/kg. As shown on Table 1, deeper soil
samples from all three borings (B-8, B-9, and B-13) did not exceed any of the regulatory
standards considered in this investigation.
VOCs were not detected above the laboratory MRLs in any of the soil samples collected at the
Site, with the exception of the 6-foot sample from B-11 which contained 1,500 micrograms per
kilogram (µg/kg) of ethylbenzene, 5,470 µg/kg of xylenes, 1,600 µg/kg of 1,3,5-
trimethylbenzene, and 4,800 µg/kg of 1,2,4-trimethylbenzene and the 1-foot sample from boring
B-14 which contained 7.7 µg/kg of xylenes and 8.9 µg/kg of 1,2,4-trimethylbenzene
The concentration of xylenes in the sample from B-11 (5,470 µg/kg) exceeds the Tier 1 and
commercial/industrial ESLs of 2,300 µg/kg but does not exceed the construction worker
exposure ESL of 420,000 µg/kg. It should be noted that, the high concentration of hydrocarbons
in the 6-foot sample from boring B-11 required dilution, which increased the MRLs for benzene
and MTBE above their respective Tier 1 and commercial/industrial land use ESLs. VOCs were
not detected above the laboratory MRLs in the 10-foot sample from boring B-11.
SVOCs, organochlorine pesticides, and PCBs were not detected above the laboratory MRLs in
any soil samples analyzed for these constituents.
Test results for metals are shown in Table 2. Antimony, beryllium, molybdenum, selenium,
silver, and thallium were not detected above the laboratory MRLs in any soil samples collected
at the Site. Cadmium was not detected above the laboratory MRLs in any soil samples with the
exception of the 1-foot sample from boring B-11, which contained 1.1 mg/kg of cadmium. The
measured concentration of cadmium does not exceed any of the regulatory standards considered
in this investigation. Barium (27 to 430 mg/kg), chromium (8.5 to 49 mg/kg), nickel (9.2 to 37
mg/kg), and zinc (9 to 130 mg/kg) were detected above the laboratory MRLs in every soil
sample analyzed, but at concentrations below their respective regulatory standards. Cobalt was
measured in 21 soil samples at concentrations ranging from 5.1 to 17 mg/kg. Copper was
measured in 23 soil samples at concentrations ranging from 5.5 to 58 mg/kg. Mercury was
measured in nine soil samples at concentrations ranging from 0.1 to 0.38 mg/kg. None of the
reported concentrations of cobalt, copper, or mercury exceed their respective regulatory
standards.
Arsenic was reported in nearly all soil samples analyzed, at concentrations ranging from 1.7 to
16 mg/kg. All measured concentrations exceed the Tier 1 and commercial/industrial ESLs of
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0.39 mg/kg and 1.6 mg/kg, respectively. One reported concentration, 16 mg/kg measured in the
1-foot sample from boring B-11, exceeds the construction worker exposure ESL of 15 mg/kg.
Vanadium was reported in all of the soil samples analyzed at concentrations ranging from 15 to
41 mg/kg. With the exception of two soil samples, all of the measured concentrations exceed the
Tier 1 ESL of 16 mg/kg for vanadium. However, none of the reported concentrations exceed the
commercial/industrial land use or construction worker exposure ESLs of 200 mg/kg and 770
mg/kg, respectively. It should be noted that most soils throughout the San Francisco Bay Area
contain arsenic and vanadium at naturally occurring levels that are above the Tier 1 ESLs. In our
opinion, the arsenic and vanadium measured in the samples are generally representative of
naturally occurring background levels and do not represent a significant environmental concern.
Lead was reported in every sample analyzed at concentrations ranging from 2 to 130 mg/kg.
Five of the highest concentrations reported exceed the residential land use CHHSL of 80 mg/kg:
87 mg/kg (1-foot sample from B-9), 98 mg/kg (1-foot sample from B-8), 100 mg/kg (1-foot
sample from B-3), 120 mg/kg (1-foot sample from B-2), and 130 mg/kg (5-foot sample from B-
2). However, none of the reported concentrations exceed the commercial/industrial land use
CHHSL of 320 mg/kg or the construction worker ESL of 750 mg/kg. Given the increasing lead
concentration with depth in boring B-2, the 9-foot soil sample was additionally analyzed for total
lead. This sample contained 2.1 mg/kg, which is below the regulatory screening standards.
Although none of the measured concentrations of metals exceed their respective TTLCs, soil
samples with the nine highest reported concentrations of lead could potentially contain soluble
lead above the STLC of 5 milligrams per liter (mg/L) which could classify a waste as hazardous
waste based on its soluble lead content. To evaluate this potential, four soil samples (B-7-1.0
with lead at 50 mg/kg, B-8-1.0 with lead at 98 mg/kg, B-3-1.0 with lead at 100 mg/kg, and B-2-
5.0 with lead at 130 mg/kg) were additionally analyzed for soluble lead using the WET. One of
the samples (B-2-5.0) was also analyzed for soluble lead using the Toxicity Characteristic
Leaching Procedure (TCLP). Soluble lead test results are presented in Table 3. As shown in the
table, soluble lead was reported at concentrations ranging from 4.1 to 11 mg/L using the WET
and below the MRL of 0.10 mg/L using the TCLP. Lead solubility varied between soil samples
collected from the elevated roadway on the northern boundary of the Site, compared to samples
collected on the eastern half of the Site. As shown on the associated solubility graph on Table 3,
soils from the elevated roadway could potentially contain soluble lead above the STLC of 5
mg/L if the total lead concentration is 170 mg/kg or above. Alternatively, soils from the eastern
half of the Site could potentially contain soluble lead above the STLC when total lead
concentrations are 50 mg/kg or above. Soluble lead content in soil samples B-7-1.0 and B-8-1.0,
located on the eastern corner of the Site, exceed the STLC of 5.0 mg/L for lead and would be
Phase II Environmental Site Assessment 13 December 16, 2011
500 Kirkham Street
APN 004-049-001
Oakland, California
classified as a California hazardous waste for landfill disposal purposes if removed from the Site.
Although soils in the elevated roadway contain higher concentrations of total lead it appears to
be in a less leachable form than lead reported in Site-wide soil.
3.2.4 Grab-Groundwater Quality
Groundwater samples were collected from borings B-1, B-4, B-5, B-8, B-9, B-11, B-12, B-13,
and B-16. Chemical test results are presented in Table 4 and 5, and laboratory analytical reports
are presented in Appendix C. As shown in Table 4, TPH-o was not detected above the
laboratory MRL in any of the groundwater samples analyzed. TPH-g was not detected in any
samples, with the exception of groundwater collected at boring B-11 (1,300 µg/L) and B-13 (51
µg/L). The laboratory report notes that the TPH-g results from B-11 do not match the reference
gasoline standard and may be due to contributions from heavy end hydrocarbons (possibly aged
gasoline) and non-fuel hydrocarbons. The 51 µg/L of TPH-g reported at B-13 is between the
laboratory method detection limit (MDL) and the method reporting limit (the MRL, or the
practical quantitation limit – PQL) and is considered “estimated” (J flagged) by the laboratory.
The measured concentration at B-11 exceeds the drinking water ESL of 100 µg/L but does not
exceed the non-drinking water ESL of 5,000 µg/L.
TPH-d was measured only in the groundwater sample from boring B-11, at a concentration of
350 µg/L. The laboratory report noted that the results for TPH-d did not match the reference
diesel pattern and may be fuel lighter than diesel. The reported concentration of TPH-d exceeds
the drinking water MCL of 100 µg/L but does not exceed the non-drinking water MCL of 2,500
µg/L.
VOCs were detected above laboratory MRLs in the groundwater samples collected from five
borings locations. Chloromethane was reported at 0.88 µg/L in groundwater from boring B-4.
Groundwater from boring B-8 contained 4.9 µg/L of chloroform and 0.35 µg/L of methylene
chloride. However, the measured concentration of methylene chloride fell between the MDL
and the PQL and is considered “estimated” (J flagged) by the laboratory. Methyl tert-butyl ether
(MTBE) was reported at 0.69 µg/L in groundwater from boring B-9. The largest suite of VOCs
were reported in groundwater collected at boring B-11 including ethylbenzene (45 µg/L),
xylenes (127 µg/L), isopropyl benzene (6.1 µg/L), n-propylbenzene (21 µg/L), 1,3,5-
trimentylbenzene (26 µg/L), 1,2,4-trimethylbenzene (52 µg/L), n-butylbenzene (4.6 µg/L), and
naphthalene (12 µg/L). The reported concentrations of chloroform, 1,2,4-trimethylbenzene, and
naphthalene exceed the RSLs of 0.19, 15, and 0.14 µg/L, respectively. None of the other
measured concentrations of VOCs in groundwater from borings B-4, B-8, B-9, or B11 exceed
their respective regulatory standards.
Phase II Environmental Site Assessment 14 December 16, 2011
500 Kirkham Street
APN 004-049-001
Oakland, California
Groundwater from boring B-13 contained several chlorinated VOCs including: 48 µg/L of
tetrachloroethylene (PCE), 49 µg/L of trichloroethylene (TCE), 1.1 µg/L of vinyl chloride, 9.6
µg/L of cis-1,2-DCE, 1.5 µg/L of trans-1,2-DCE, and 0.61 µg/L of chloroform. The reported
concentrations of PCE, TCE, vinyl chloride, and cis-1,2-DCE exceed the MCLs (the State
Primary Drinking Water Standards) established under Title 22 of the California Code of
Regulations of 5, 5, 0.5, and 6 µg/L, respectively. The reported concentration of chloroform
exceeds the RSL of 0.19 µg/L. All of the detected concentrations of VOCs are well below their
respective ESLs for evaluating potential vapor intrusion into buildings established by the
RWQCB.
As shown in Table 5, with the exception of arsenic, barium, cobalt, molybdenum, nickel, and
silver, metals were not detected above the laboratory MRLs in any grab-groundwater sample
analyzed. Barium (0.022-0.19 mg/L), cobalt (0.0052-0.023 mg/L), molybdenum (0.015-0.043
mg/L), nickel (0.012-0.059 mg/L), and silver (0.0054 and 0.0056 mg/L) were reported at
concentrations below their respective MCLs, where established. Arsenic was measured above
the laboratory MRL in groundwater from two boring locations: B-9 (at 0.02 mg/L) and B 16 (at
0.01 mg/L). The reported concentration of arsenic from boring B-9 exceeds the MCL of 0.01
mg/L for arsenic.
3.2.5 Monitoring Well Groundwater Quality
Groundwater samples were collected from on-Site monitoring wells JA-2, JA-3, and JA-4 on
August 15, 2011. Chemical test results are presented in Tables 6 and 7, and laboratory analytical
results are presented in Appendix C. As shown in Table 6, TPH-d and TPH-o were not detected
above the laboratory MRLs in any of the wells. TPH-g was reported in the primary and
duplicate groundwater samples collected from well JA-4 at concentrations of 180 µg/L and 190
µg/L, respectively. The laboratory report notes that results for both the primary and duplicate
samples did not match the reference gasoline standard and the results are due to discrete peaks of
non-fuel compounds (VOCs). Both measured concentrations of TPH-g exceed the drinking
water ESL of 100 µg/L but do not exceed the non-drinking water ESL of 5,000 µg/L.
Phase II Environmental Site Assessment 15 December 16, 2011
500 Kirkham Street
APN 004-049-001
Oakland, California
VOCs were not detected in groundwater sample from the monitoring wells, with the exception of
the primary and duplicate samples from well JA-4. Benzene (0.53 µg/L), 1,1-dichloroethene
(1,1-DCE – 5.2 µg/L in both samples), trans-1,2-DCE (2.6 and 2.7 µg/L), chloroform (0.53
µg/L), and 1,1,2-TCA (0.91 and 0.85 µg/L) were reported at concentrations below their
respective regulatory standards. PCE (36 and 34 µg/L), TCE (140 and 150 µg/L), cis-1,2-DCE
(160 and 170 µg/L), 1,1-DCA (46 and 45 µg/L), and vinyl chloride (2.5 µg/L in both samples)
were measured in the primary and duplicate samples at concentrations that exceed their
respective MCLs, but below their respective ESLs for vapor intrusion. The reported
concentration of chloroform in the primary sample exceeds the RSL of 0.19 µg/L. As previously
discussed, a suite of VOCs were also reported in the grab groundwater sample from boring B-13,
located upgradient of well JA-4. However, the grab groundwater sample collected from boring
B-5, located upgradient of B-13 did not contain VOCs above the laboratory MRLs. The
potential source or the full extent of VOCs in groundwater beneath the Site remains undefined.
As shown in Table 7, with the exception of barium, chromium, cobalt, and nickel, dissolved
metals were not detected above the laboratory MRLs in any monitoring well samples analyzed.
Barium was measured in all four monitoring well samples, at concentrations ranging from 0.074
to 0.17 mg/L. Chromium was only measured in the primary and duplicate samples from well
JA-4, at concentrations of 0.007 and 0.0067 mg/L, respectively. Cobalt was only measured in
the primary and duplicate samples from well JA-4, at concentrations of 0.008 and 0.0079 mg/L,
respectively. Nickel was measured in three of the four groundwater samples, from wells JA-3
and JA-4 (primary and duplicate), at concentrations of 0.036, 0.3, and 0.29 mg/L, respectively.
The reported concentrations of nickel in groundwater from well JA-4 exceed the MCL of 0.1
mg/L for nickel. None of the other measured concentrations of dissolved metals exceed their
respective MCLs.
3.3 Quality Assurance/Quality Control (QA/QC)
Soil and groundwater samples were collected following sampling protocols and QA/QC
procedures outlined in the SAP, prepared by Northgate on August 8, 2011. Chain-of-custody
forms were completed for all samples and samples were preserved according to the analytical
method requirements.
Sampling QA/QC procedures were followed with respect to equipment, field procedures, sample
containers, decontamination, storage, holding times, and field QC sampling outlined in the SAP.
All analyses were performed according to standard methods by Torrent Laboratory in Milpitas,
California. All sample holding times and preservation requirements were met. The laboratory
report noted that high concentrations of hydrocarbons in the 6-foot sample from boring B-11
Phase II Environmental Site Assessment 16 December 16, 2011
500 Kirkham Street
APN 004-049-001
Oakland, California
necessitated a methanol extraction for VOCs, as opposed to analyzing from the pre-tared 5035
vials. In this case, the soil sample for methanol extraction was collected directly from the soil
liner.
Method blanks were analyzed for each analytical method performed to assess the level of
contamination introduced by the laboratory. Results of the method blank analysis were all non-
detect, with the exception of TPH-d, TPH-o, methylene chloride, and several metals that were
reported at very low-level concentrations.
Surrogate recoveries were performed by spiking selected samples with a known concentration of
a contaminant (laboratory control spike [LCS] and laboratory control spike duplicate [LCSD])
and the percent recovery was calculated to assess the accuracy of the analytical method.
Surrogate recoveries and the relative percent different (RPD) between duplicate results –
calculated to assess the precision of the data – were all within the acceptable range.
Northgate collected three duplicate soil samples: at the 5-foot depth from boring B-5, the 1-foot
depth from boring B-7, and the 1-foot depth from boring B-12. One grab groundwater duplicate
sample was collected from boring B-12. One duplicate groundwater monitoring well sample was
collected from well JA-4. Comparison of primary and duplicate sample results is shown in
Tables 8 and 9. All duplicate samples contained the same detected compounds at generally
similar concentrations. RPD values for soil duplicates were below 50% and RPD values for
groundwater duplicates were below 30%, indicating the results are acceptable.
Northgate collected equipment blanks for VOCs and metals and a field blank for VOCs in
accordance with procedures outlines in the SAP. Contaminants were not measured above the
laboratory MRLs in any of the equipment and field blanks.
Matrix spike/matrix spike duplicate (MS/MSD) analyses were performed by the laboratory on
one of the samples submitted from this investigation. The percent recoveries for several metals,
1,4-DCB, and TPH-d were outside of laboratory control limits but were within RPD limits. The
associated LCS/LCSD percentage recoveries and RPD were within limits and corrective actions
were not required.
Phase II Environmental Site Assessment 17 December 16, 2011
500 Kirkham Street
APN 004-049-001
Oakland, California
4.0 CONCLUSIONS AND RECOMMENDATIONS
Soil in the vicinity of boring B-11, located along the western property boundary, appears
to be locally impacted by TPH-g. The concentration of TPH-g at 6-feet bgs exceeds both
the Tier 1 (residential) and commercial/industrial land use ESLs. Soil in this area should
be excavated and removed off-Site or isolated beneath an engineered cap prior to
redevelopment.
Shallow soil in several locations throughout the Site (borings B-8, B-9, and B-13)
contains concentrations of TPH-o above the Tier 1 (residential land use) ESL. Shallow
soil in these areas should be excavated and removed off-Site or isolated beneath an
engineered cap prior to any residential development. Given the long industrial use of the
Site, localized areas of hydrocarbon impacted soil could be encountered elsewhere. We
recommend additional evaluation of impacted soil if encountered during Site grading
activities to evaluate appropriate management options.
Elevated concentrations of total lead were measured in soil samples collected from the
elevated roadway, located along the northern Site boundary. Although lead in these
samples from the roadway does not appear to be readily soluble, total lead concentrations
exceed the CHHSL for residential land use. The measured concentrations of lead do not
exceed the CHHSL for commercial/industrial land use. If a mixed
residential/commercial redevelopment is proposed for the Site, soil with lead above 80
mg/kg should be excavated and removed off-Site, selectively relocated to commercial
development areas of the Site or isolated beneath an engineered cap prior to any
residential development.
Soluble lead test results indicate that any soil from the main body of the Site containing
total lead greater than 50 mg/kg could potentially contain soluble lead above the STLC of
5 milligrams per liter (mg/L), which would classify the soil as a hazardous waste for off-
Site landfill disposal purposes. Any soil that will be removed from the Site should be
tested for total and soluble lead prior to off-Site disposal.
Petroleum-related VOCs are present in groundwater beneath the southwestern portion of
the Site, in close proximity to the location of a former on-Site UST. Although UST
excavation and soil remediation activities were documented, the results suggest that some
residual contamination may be present in groundwater beneath this portion of the Site.
However, the reported concentrations of petroleum-related VOCs do not exceed their
respective ESLs for vapor intrusion or the MCLs. It is our opinion that petroleum-related
Phase II Environmental Site Assessment 18 December 16, 2011
500 Kirkham Street
APN 004-049-001
Oakland, California
VOCs in groundwater appear to be limited in extent and do not represent a significant
concern for potential Site redevelopment.
Chlorinated VOCs are present in groundwater beneath the southern portion of the Site, at
boring B-13 and in well JA-4, located downgradient of boring B-13. PCE, TCE, and
several breakdown products were reported at concentrations above their respective MCLs
but did not exceed their respective ESLs for vapor intrusion. In our opinion, VOCs in
groundwater are unlikely to represent a significant environmental concern, as shallow
groundwater in this area is not expected to be used for drinking water. However, the
source area and full extent of VOCs in groundwater beneath the Site have not been fully
defined, and additional investigation may be warranted. Any construction dewatering
performed at the Site will need to account for VOCs in groundwater.
Phase II Environmental Site Assessment 19 December 16, 2011
500 Kirkham Street
APN 004-049-001
Oakland, California
5.0 LIMITATIONS
The purpose of a soil and groundwater quality investigation is to reasonably characterize existing
Site conditions based on the results of a limited target subsurface investigation. In performing
such a study, it is understood that a balance must be struck between a reasonable inquiry into the
Site conditions and an exhaustive analysis of each conceivable environmental characteristic. The
following paragraphs discuss the assumptions and parameters under which such an opinion is
rendered.
No investigation is thorough enough to describe all environmental conditions of interest at a
given Site. If conditions have not been identified during the study, such a finding should not
therefore be construed as a guarantee of the absence of such conditions at the Site, but rather as
the result of the services performed within the scope, limitations, and cost of the work
performed.
We are unable to report on or accurately predict events that may change the Site conditions after
the described services are performed, whether occurring naturally or caused by external forces.
We assume no responsibility for conditions we were not authorized to evaluate, or conditions not
generally recognized as predictable when services were performed.
Environmental conditions may exist at the Site that cannot be identified solely by visual
observation. Where subsurface exploratory work was performed, our professional opinions are
based in part on interpretation of data from discrete sampling locations that may not represent
actual conditions at unsampled locations.
Phase II Environmental Site Assessment 20 December 16, 2011
500 Kirkham Street
APN 004-049-001
Oakland, California
6.0 REFERENCES
EPA, 1983. Interim Guidelines and Specifications for Preparing Quality Assurance Project
Plans, 1983.
EPA. 1986. Test Methods for Evaluating Solid Waste, Physical and Chemical Methods (SW-
846). Third Edition of SW-846 with Update I (pages dated September 1992), Update IIA
(pages dated August 1993), Update II (pages dated September 1994), Update IIB (pages
dated January 1995), and Update III (pages dated December 1996).
EPA, 1991. Office of Emergency and Remedial Response (OERR) Directive 9345.3-02, 1991.
Geo/Resource Consultants, Inc. 1992. Site Investigation Report – Area 8, Department of
Transportation, T.O. Number: 04-192201-01, Highway 880, Cypress Reconstruction,
Oakland, California, August 28.
Jonas & Associates, Inc. 1995. Remedial Design and Implementation Plan, Cypress Freeway
Re-Alignment, Oakland, California, September 12, 1995.
Northgate Environmental Management, Inc. 2009. Draft Quality Assurance Project Plan, West
Oakland Development Area, Oakland, California, September 8, 2009.
Northgate Environmental Management, Inc. 2011. Phase I Environmental Site Assessment, 500
Kirkham Street, APN 004-049-001, Oakland, California, June 6, 2011.
Northgate Environmental Management, Inc. 2011. Sampling and Analysis Plan, Phase II Soil
and Groundwater Investigation, 500 Kirkham Street, APN 004-049-001, Oakland,
California, August 8, 2011.
Office of the Federal Register National Archives and Records Administration, 1994. 40 Code of
Federal Regulations (CFR) Part 136, Appendix B, 1994.
Professional Service Industries, Inc. 2000. Site Investigation Report, Task Order Number 04-
192203-RJ, Contract Number 43A0012, Former J & A Truck Repair & Container
Freight Sites, Oakland, California, September 2000.
Regional Water Quality Control Board. 2008. Screening for Environmental Concerns at Sites
with Contaminated Soil and Groundwater, May 2008.
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
TABLES
TABLE 1
Soil Sample Analytical Results - TPH, VOCs, SVOCs, Pesticides, and PCBs
SVOCs PCBs
TP
H a
s G
aso
lin
e
TP
H a
s D
iese
l
TP
H a
s O
il
Ben
zen
e
To
luen
e
Eth
ylb
enze
ne
Xy
len
es
MT
BE
1,3
,5-T
rim
eth
ylb
enze
ne
1,2
,4-T
rim
eth
ylb
enze
ne
Oth
er V
OC
s
SV
OC
s
4,4
'-D
DE
4,4
'-D
DD
4,4
'-D
DT
Oth
er P
esti
cid
es
PC
Bs
mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg mg/kg µg/kg µg/kg µg/kg µg/kg mg/kg
B-1-1.0 1.0 <0.089 <10 160 <8.9 <8.9 <8.9 <13.4 <8.9 <8.9 <8.9 ND ND <9.5 <9.4 <16 ND ND
B-1-5.0 5.0 <0.081 <2 <4 <8.1 <8.1 <8.1 <12.2 <8.1 <8.1 <8.1 ND ND -- -- -- -- ND
B-2-1.0 1.0 <0.092 <4.8 120 <9.2 <9.2 <9.2 <13.8 <9.2 <9.2 <9.2 ND ND <20 <20 <20 ND ND
B-2-5.0 5.0 <0.093 <4.8 160 <9.3 <9.3 <9.3 <14 <9.3 <9.3 <9.3 ND ND -- -- -- -- ND
B-2-9.0 9.0 -- -- <4 -- -- -- -- -- -- -- -- -- -- -- -- -- --
B-3-1.0 1.0 <0.084 <10 130 <8.4 <8.4 <8.4 <12.6 <8.4 <8.4 <8.4 ND ND <9.5 <9.4 <16 ND ND
B-3-5.0 5.0 0.110 1
2 2
6.8 <8.7 <8.7 <8.7 <13.1 <8.7 <8.7 <8.7 ND ND -- -- -- -- ND
B-4-1.0 1.0 <0.089 <2 12 <8.9 <8.9 <8.9 <13.4 <8.9 <8.9 <8.9 ND ND <2 <2 <2 ND ND
B-4-5.0 5.0 <0.087 <2 <4 <8.7 <8.7 <8.7 <13.1 <8.7 <8.7 <8.7 ND ND -- -- -- -- ND
B-5-1.0 1.0 <0.086 <2 12 <8.6 <8.6 <8.6 <12.9 <8.6 <8.6 <8.6 ND ND <2 <2 <2 ND ND
B-5-5.0 5.0 <0.076 2.4 2
4.8 <7.6 <7.6 <7.6 <11.4 <7.6 <7.6 <7.6 ND ND -- -- -- -- ND
B-5-5.0D 5.0 <0.073 <2 <4 <7.3 <7.3 <7.3 <11.0 <7.3 <7.3 <7.3 ND ND -- -- -- -- ND
B-6-1.0 1.0 <0.094 <2 4 <9.4 <9.4 <9.4 <14.1 <9.4 <9.4 <9.4 ND ND <2 <2 <2 ND ND
B-6-5.0 5.0 <0.079 <2 5.5 <7.9 <7.9 <7.9 <11.9 <7.9 <7.9 <7.9 ND ND -- -- -- -- ND
B-7-1.0 1.0 <0.100 <2 9.2 <10 <10 <10 <15.2 <10 <10 <10 ND ND <2 <2 <2 ND ND
B-7-1.0D 1.0 <0.093 <2 8.9 <9.3 <9.3 <9.3 <14.0 <9.3 <9.3 <9.3 ND -- -- -- -- -- --
B-7-5.0 5.0 <0.077 <2 5.2 <7.7 <7.7 <7.7 <11.6 <7.7 <7.7 <7.7 ND ND -- -- -- -- ND
B-8-1.0 1.0 <0.087 <2 13 <8.7 <8.7 <8.7 <13.1 <8.7 <8.7 <8.7 ND ND <2 <2 <2 ND ND
B-8-5.0 5.0 <0.078 <19 550 <7.8 <7.8 <7.8 <11.7 <7.8 <7.8 <7.8 ND ND -- -- -- -- ND
B-8-8.0 8.0 -- -- <4 -- -- -- -- -- -- -- -- -- -- -- -- -- --
B-9-1.0 1.0 <0.110 <20 720 <11 <11 <11 <16.5 <11 <11 <11 ND ND <19 <19 <32 ND ND
B-9-3.0 3.0 <0.085 <10 270 <8.5 <8.5 <8.5 <12.8 <8.5 <8.5 <8.5 ND ND -- -- -- -- ND
B-10-1.0 1.0 <0.087 <4 88 <8.7 <8.7 <87 <13.1 <8.7 <8.7 <8.7 ND ND <20 <20 <20 ND ND
B-10-5.0 5.0 <0.080 <2 6.3 <8.1 <8.1 <8.1 <12.2 <8.1 <8.1 <8.1 ND ND -- -- -- -- ND
B-11-1.0 1.0 <0.082 <10 130 <8.2 <8.2 <8.2 <12.3 <8.2 <8.2 <8.2 ND ND <20 <20 <20 ND ND
B-11-6.0 6.0 150 1
8.1 2
5.2 <1,000 <1,000 1,500 5,470 <1,000 1,600 4,800 ND ND -- -- -- -- ND
B-11-10.0 10.0 <0.1 -- -- <10 <10 <10 <15 <10 <10 <10 ND -- -- -- -- -- --
B-12-1.0 1.0 <0.091 <2 29 <9.1 <9.1 <9.1 <13.7 <9.1 <9.1 <9.1 ND ND <8 <8 <8 ND ND
B-12-1.0D 1.0 <0.076 -- -- <7.6 <7.6 <7.6 <11.4 <7.6 <7.6 <7.6 ND ND -- -- -- -- --
B-12-5.0 5.0 <0.072 2.2 2
<4 <7.2 <7.2 <7.2 <10.8 <7.2 <7.2 <7.2 ND ND -- -- -- -- ND
B-13-1.0 1.0 <0.081 <20 960 <8.1 <8.1 <8.1 <12.2 <8.1 <8.1 <8.1 ND ND <19 <19 <32 ND ND
B-13-5.0 5.0 <0.076 <2 <4 <7.6 <7.6 <7.6 <11.4 <7.6 <7.6 <7.6 ND ND -- -- -- -- ND
Soil Sample ID Sample Depth
ANALYTE
Total Petroleum Hydrocarbons Volatile Organic Compounds Organochlorine Pesticides
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
1 of 2 December 16, 2011
TABLE 1
Soil Sample Analytical Results - TPH, VOCs, SVOCs, Pesticides, and PCBs
SVOCs PCBs
TP
H a
s G
aso
lin
e
TP
H a
s D
iese
l
TP
H a
s O
il
Ben
zen
e
To
luen
e
Eth
ylb
enze
ne
Xy
len
es
MT
BE
1,3
,5-T
rim
eth
ylb
enze
ne
1,2
,4-T
rim
eth
ylb
enze
ne
Oth
er V
OC
s
SV
OC
s
4,4
'-D
DE
4,4
'-D
DD
4,4
'-D
DT
Oth
er P
esti
cid
es
PC
Bs
mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg mg/kg µg/kg µg/kg µg/kg µg/kg mg/kgSoil Sample ID Sample Depth
ANALYTE
Total Petroleum Hydrocarbons Volatile Organic Compounds Organochlorine Pesticides
B-14-1.0 1.0 <0.077 <10 280 <7.7 <7.7 <7.7 7.7 <7.7 <7.7 8.9 ND ND <19 <19 <32 ND ND
B-14-5.0 5.0 <0.071 <2 14 <10 <10 <10 <15 <10 <10 <10 ND ND -- -- -- -- ND
B-15-1.0 1.0 <0.085 <10 150 <8.5 <8.5 <8.5 <12.8 <8.5 <8.5 <8.5 ND ND <20 <20 <20 ND ND
B-15-5.0 5.0 <0.077 2.6 2
6 <7.7 <7.7 <7.7 <11.6 <7.7 <7.7 <7.7 ND ND -- -- -- -- ND
B-16-1.0 1.0 <0.075 <4.8 270 <7.5 <7.5 <7.5 <11.3 <7.5 <7.5 <7.5 ND ND <9.5 <9.4 <16 ND ND
B-16-5.0 5.0 <0.092 <2 <4 <9.2 <9.2 <9.2 <13.8 <9.2 <9.2 <9.2 ND ND -- -- -- -- ND
RWQCB ESL - Tier 1 83 83 370 44 2,900 2,300 2,300 23 ne ne na na 1,700 2,400 1,700 na 0.22
RWQCB ESL - Commercial/Industrial 83 83 2,500 44 2,900 3,300 2,300 23 ne ne na na 4,000 10,000 4,000 na 0.74
RWQCB ESL - Construction Worker 4,200 4,200 12,000 12,000 650,000 210,000 420,000 2,800,000 ne ne na na 87,000 120,000 87,000 na 6.7
TTLC ne ne ne ne ne ne ne ne ne ne na na 1,000 1,000 1,000 na ne
NOTES
mg/kg: milligrams per kilogram (parts per million)
g/kg: micrograms per kilogram (parts per billion)TPH: Total Petroleum Hydrocarbons
SVOC: Semi-Volatile Organic Compound
<: Not detected at or above the indicated laboratory method reporting limit
--: Not tested
ND: Not detected above the laboratory method reporting limit; limits vary by compound
ne: Not established
na: Not applicable
ESL: Tier 1 - Environmental Screening Level for shallow soil = <10 feet deep in residential land use (RWQCB, 2008 Table A-1)
Commercial/Industrial - soil screening level for shallow soil = <10 feet deep in commercial/industrial land use (RWQCB, 2008 Table A-2)
Construction Worker - soil screening level for direct exposure of construction/trench worker (RWQCB, 2008 Table K-3)
TTLC: Total Threshold Limit Concentration for defining a waste as a hazardous waste
(1) = Does not match pattern of reference Gasoline standard.
(2) = Not typical of Diesel standard pattern (unknown hydrocarbons present)
Regulatory Standards
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
2 of 2 December 16, 2011
TABLE 2
Soil Sample Analytical Results - Metals
An
tim
on
y
Ars
enic
Ba
riu
m
Ber
yll
ium
Ca
dm
ium
Ch
rom
ium
Co
ba
lt
Co
pp
er
Lea
d
Mer
cury
Mo
lyb
den
um
Nic
kel
Sel
eniu
m
Sil
ver
Th
all
ium
Va
na
diu
m
Zin
c
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
B-1-1.0 1.0 <5 2.3 72 <2 <1 22 <5 12 55 <0.1 <5 9.9 <5 <1 <5 23 23
B-1-5.0 5.0 <5 2 27 <2 <1 26 6.1 <5 2.0 <0.1 <5 19 <5 <1 <5 20 11
B-2-1.0 1.0 <5 5.3 100 <2 <1 31 6.9 44 120 0.31 <5 26 <5 <1 <5 30 120
B-2-5.0 5.0 <5 6.6 190 <2 <1 21 12 40 130 0.24 <5 21 <5 <1 <5 37 130
B-2-9.0 9.0 -- -- -- -- -- -- -- -- 2.1 -- -- -- -- -- -- -- --
B-3-1.0 1.0 <5 4.2 140 <2 <1 36 8.0 29 100 0.19 <5 24 <5 <1 <5 30 99
B-3-5.0 5.0 <5 <1.7 69 <2 <1 23 <5 <5 3.0 <0.1 <5 14 <5 <1 <5 18 16
B-4-1.0 1.0 <5 2.4 67 <2 <1 31 <5 6.5 34 <0.1 <5 19 <5 <1 <5 23 35
B-4-5.0 5.0 <5 1.9 65 <2 <1 25 <5 5.6 12 <0.1 <5 12 <5 <1 <5 20 19
B-5-1.0 1.0 <5 <1.7 37 <2 <1 23 6 <5 2.1 <0.1 <5 14 <5 <1 <5 17 12
B-5-5.0 5.0 <5 1.8 28 <2 <1 45 5.4 5.5 3 <0.1 <5 31 <5 <1 <5 30 19
B-5-5.0D 5.0 <5 2.5 43 <2 <1 30 6.2 <5 2.4 <0.1 <5 29 <5 <1 <5 22 16
B-6-1.0 1.0 <5 <1.7 42 <2 <1 21 <5 <5 2.7 <0.1 <5 13 <5 <1 <5 15 14
B-6-5.0 5.0 <5 <1.7 50 <2 <1 22 <5 <5 1.9 <0.1 <5 9.2 <5 <1 <5 18 9.0
B-7-1.0 1.0 <5 <1.7 53 <2 <1 29 <5 6.8 50 0.12 <5 14 <5 <1 <5 21 130
B-7-1.0D 1.0 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --
B-7-5.0 5.0 <5 <1.7 58 <2 <1 25 <5 <5 4.2 <0.1 <5 12 <5 <1 <5 16 13
B-8-1.0 1.0 <5 2.9 76 <2 <1 29 6.3 55 98 0.17 <5 19 <5 <1 <5 24 130
B-8-5.0 5.0 <5 1.8 89 <2 <1 26 <5 6.1 13 <0.1 <5 16 <5 <1 <5 19 22
B-8-8.0 8.0 -- -- -- -- -- -- -- -- 3.8 -- -- -- -- -- -- -- --
B-9-1.0 1.0 <5 4 86 <2 <1 22 6.1 22 87 0.23 <5 20 <5 <1 <5 22 73
B-9-3.0 3.0 <5 3.8 78 <2 <1 38 17 19 44 0.25 <5 24 <5 <1 <5 41 41
B-10-1.0 1.0 <5 1.7 42 <2 <1 23 <5 <5 3.5 <0.1 <5 14 <5 <1 <5 17 13
B-10-5.0 5.0 <5 2.1 47 <2 <1 37 6.7 5.9 3.1 <0.1 <5 31 <5 <1 <5 29 20
B-11-1.0 1.0 <5 16 430 <2 1.1 8.5 9.2 58 18 0.38 <5 16 <5 <1 <5 39 77
B-11-6.0 6.0 <5 4.8 42 <2 <1 30 5.3 5.7 4.3 <0.1 <5 31 <5 <1 <5 29 17
B-12-1.0 1.0 <5 1.7 42 <2 <1 24 <5 <5 2 <0.1 <5 15 <5 <1 <5 17 12
B-12-1.0D 1.0 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --
B-12-5.0 5.0 <5 2.5 46 <2 <1 44 11 6.1 3.2 <0.1 <5 33 <5 <1 <5 29 20
B-13-1.0 1.0 <5 4.3 94 <2 <1 30 7 19 53 <0.1 <5 33 <5 <1 <5 29 58
B-13-5.0 5.0 <5 2.5 55 <2 <1 49 6.2 6.7 3.5 <0.1 <5 37 <5 <1 <5 37 21
Soil Sample ID Sample Depth
ANALYTE
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
1 of 2 December 16, 2011
TABLE 2
Soil Sample Analytical Results - Metals
An
tim
on
y
Ars
enic
Ba
riu
m
Ber
yll
ium
Ca
dm
ium
Ch
rom
ium
Co
ba
lt
Co
pp
er
Lea
d
Mer
cury
Mo
lyb
den
um
Nic
kel
Sel
eniu
m
Sil
ver
Th
all
ium
Va
na
diu
m
Zin
c
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kgSoil Sample ID Sample Depth
ANALYTE
B-14-1.0 1.0 <5 2.7 77 <2 <1 28 5.7 13 46 <0.1 <5 26 <5 <1 <5 22 47
B-14-5.0 5.0 <5 3.4 75 <2 <1 36 6.6 11 7.2 <0.1 <5 30 <5 <1 <5 31 25
B-15-1.0 1.0 <5 3.9 82 <2 <1 25 6.4 18 53 0.1 <5 24 <5 <1 <5 24 56
B-15-5.0 5.0 <5 2.2 31 <2 <1 34 <5 <5 2.4 <0.1 <5 19 <5 <1 <5 23 13
B-16-1.0 1.0 <5 2.5 58 <2 <1 24 5.1 12 41 <0.1 <5 19 <5 <1 <5 21 45
B-16-5.0 5.0 <5 2 50 <2 <1 38 6.9 5.6 3.2 <0.1 <5 29 <5 <1 <5 27 18
RWQCB ESL - Tier 1 6.3 0.39 750 4.0 1.7 750 40 230 80* 1.3 40 150 10 20 1.3 16 600
RWQCB ESL - Commercial/Industrial 40 1.6 1,500 8.0 7.4 750 80 230 320* 10 40 150 10 40 16 200 600
RWQCB ESL - Construction Worker 310 15 2,600 98 39 1,200,000 94 310,000 750 58 3,900 260 3,900 3,900 62 770 230,000
TTLC 500 500 10,000 75 100 2,500 8,000 2,500 1,000 20 3,500 2,000 100 500 700 2,400 5,000
NOTES
mg/kg: milligrams per kilogram (parts per million) ESL: Tier 1 - Environmental Screening Level for soil <10 feet deep in residential land use (RWQCB, 2008 Table A-1)
<: Not detected at or above the indicated laboratory method reporting limit * - California Human Health Screening Level for residential land use established by California EPA (September 2009)
--: Not tested Commercial/Industrial - soil screening level for soil <10 feet deep in commercial/industrial land use (RWQCB, 2008 Table A-2)
TTLC: Total Threshold Limit Concentration for defining a waste as a hazardous waste Construction Worker - soil screening level for direct exposure of construction/trench worker (RWQCB, 2008 Table K-3)
Regulatory Standards
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
2 of 2 December 16, 2011
TABLE 3
Soil Sample Analytical Results - Soluble Lead
WET TCLP
Location Sample ID mg/kg mg/L mg/L
B-2-5.0 130 4.6 < 0.1
B-3-1.0 100 4.1 --
B-7-1.0 50 5.7 --
B-8-1.0 98 11 --
TTLC 1,000
STLC 5
NOTES
mg/kg: milligrams per kilogram (parts per million)
mg/L: Milligrams per liter (parts per million)
<: Not detected at or above the indicated laboratory method reporting limit
--: Not analyzed
TTLC/STLC: Total and Soluble Threshold Limit Concentration for defining a waste as a hazardous waste
WET: California Waste Extraction Test for defining waste as a California hazardous waste
TCLP: Toxicity Characteristic Leaching Procedure for defining waste as federal hazardous waste
Total LeadSoluble Lead
Elevated Roadway
Site-wide
4.6 4.1
5.7
11
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
0 20 40 60 80 100 120 140 160 180
Solu
ble
Le
ad (
mg/
L)
Total Lead (mg/kg)
Stockpile Samples
Site-Wide Samples
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
1 of 1 December 16, 2011
TABLE 4
Grab Groundwater Sample Analytical Results - TPH and VOCs
RWQCB ESL
Vapor Intrusion
TPH as Gasoline µg/L <50 <50 <50 <26 <50 1,300 1
<50 <50 51 J <50 ne 100/5,000 a
TPH as Diesel µg/L <100 <100 <100 <100 <100 350 2
<100 <100 <100 <100 10,000 a
100/2,500 a
TPH as Oil µg/L <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 10,000 a
100/2,500 a
Benzene µg/L <0.5 <0.5 <0.5 <0.41 <0.5 <0.5 <0.5 <0.5 <0.60 <0.5 1,800 1
Toluene µg/L <0.5 <0.5 <0.5 <0.23 <0.5 <0.5 <0.50 <0.5 <0.60 <0.5 530,000 150
Ethylbenzene µg/L <0.5 <0.5 <0.5 <0.19 <0.5 45 <0.50 <0.5 <0.60 <0.5 170,000 300
Xylenes µg/L <1.5 <1.5 <1.50 <0.4 <1.5 127 <1.5 <1.5 <1.80 <1.5 160,000 1,750
MTBE µg/L <0.5 <0.5 <0.5 <0.46 0.69 <0.5 <0.50 <0.5 <0.60 <0.5 80,000 13
Isopropyl Benzene µg/L <0.5 <0.5 <0.5 <0.34 <0.5 6.1 <0.50 <0.5 <0.60 <0.5 ne 680 b
n-Propylbenzene µg/L <0.5 <0.5 <0.5 <0.36 <0.5 21 <0.50 <0.5 <0.60 <0.5 ne 1,300 b
1,3,5-Trimethylbenzene µg/L <0.5 <0.5 <0.5 <0.24 <0.5 26 <0.50 <0.5 <0.60 <0.5 ne 370 b
1,2,4-Trimethylbenzene µg/L <0.5 <0.5 <0.5 <0.4 <0.5 52 <0.50 <0.5 <0.60 <0.5 ne 15 b
n-Butylbenzene µg/L <0.5 <0.5 <0.5 <0.39 <0.5 4.6 <0.50 <0.5 <0.60 <0.5 ne ne
Naphthalene µg/L <1 <1 <1 <0.7 <1 12 <1 <1 <1.2 <1 11,000 0.14 b
PCE µg/L <0.5 <0.5 <0.5 <0.18 <0.5 <0.5 <0.5 <0.5 48 <0.5 420 5
TCE µg/L <0.5 <0.5 <0.5 <0.46 <0.5 <0.5 <0.5 <0.5 49 <0.5 1,800 5
Vinyl Chloride µg/L <0.5 <0.5 <0.5 <0.45 <0.5 <0.5 <0.5 <0.5 1.1 <0.5 13 0.5
cis-1,2-DCE µg/L <0.5 <0.5 <0.5 <0.4 <0.5 <0.5 <0.5 <0.5 9.6 <0.5 17,000 6
trans-1,2-DCE µg/L <0.5 <0.5 <0.5 <0.38 <0.5 <0.5 <0.5 <0.5 1.5 <0.5 19,000 10
Chloroform µg/L <0.5 <0.5 <0.5 4.9 <0.5 <0.5 <0.5 <0.5 0.61 <0.5 1,100 0.19 b
Chloromethane µg/L <0.5 0.88 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.6 <0.5 140 190 b
Methylene Chloride µg/L <5 <5 <5 0.36 J <5 <5 <5 <5 <6 <5 8,100 5
Other VOCs µg/L ND ND ND ND ND ND ND ND ND ND na na
NOTES
mg/l: Micrograms per liter (parts per billion) (1) Does not match pattern of reference Gasoline standard.
TPH: Total Petroleum Hydrocarbons (2) Not typical of Disel standard pattern (possibly fuel lighter than diesel).
<: Not detected at or above the indicated laboratory method reporting limit ESL: Vapor Intrusion - Environmental Screening Level for potential vapor intrusion into buildings
ND: Not detected above the laboratory method reporting limit; limits vary by compound (RWQCB, 2008 Table E-1)
ne: Not established MCL: Maximum contaminant level for drinking water, California Department of Public Health (October 2008)
na: Not applicable a: MCL not established. ESL for drinking water / non-drinking water shown instead (RWQCB, 2008)
J = Indicates an estimated value b: MCL not established, value provided is the Regional Screening Level for tapwater, established by the U.S. EPA
Volatile Organic Compounds
Regulatory Standards
B-5-GW MCLAnalyte
B-8-GW B-9-GW B-11-GW B-12-GW
Sample ID
B-16-GWB-13-GWB-4-GWUnits
B-1-GW B-12-GWD
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
1 of 1 December 16, 2011
TABLE 5
Grab Groundwater Sample Analytical Results - Metals
Regulatory
Standards
Antimony mg/L <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 0.006
Arsenic mg/L <0.009 <0.009 <0.009 <0.009 0.020 <0.009 <0.009 <0.009 0.010 0.010
Barium mg/L 0.035 0.044 0.030 0.091 0.19 0.047 0.022 0.091 0.12 1
Beryllium mg/L <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.004
Cadmium mg/L <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.005
Chromium mg/L <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.05
Cobalt mg/L <0.005 <0.005 0.023 0.0052 <0.005 0.0060 0.012 0.0095 0.0057 0.011 a
Copper mg/L <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 1.3
Lead mg/L <0.014 <0.014 <0.014 <0.014 <0.014 <0.014 <0.014 <0.014 <0.014 0.015
Mercury mg/L <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 0.002
Molybdenum mg/L 0.027 <0.009 0.023 0.015 0.016 0.030 0.040 0.043 0.022 0.18 a
Nickel mg/L 0.012 <0.009 0.033 <0.009 <0.009 <0.009 0.019 0.020 0.059 0.1
Selenium mg/L <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 0.05
Silver mg/L <0.005 <0.005 0.0054 <0.005 <0.005 <0.005 <0.005 0.0056 <0.005 0.18 a
Thallium mg/L <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 0.002
Vanadium mg/L <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 0.18 a
Zinc mg/L <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 ne
NOTES
mg/L: Milligrams per liter (parts per million)
<: Not detected at or above the indicated laboratory method reporting limit
ne: Not established
--: Not tested
MCL: Maximum contaminant level for drinking water, California Department of Public Health (October 2008)
a: MCL not established, value provided is the Regional Screening Level for tapwater, established by the U.S. EPA
MCLB-11-GW B-12-GW B-16-GW
Dissolved Metals
B-13-GW
Analyte Units
Sample ID
B-1-GW B-4-GW B-5-GW B-8-GW B-9-GW
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
1 of 1 December 16, 2011
TABLE 6
Groundwater Monitoring Well Sample Analytical Results - TPH and VOCs
RWQCB ESL
Vapor Intrusion
TPH as Gasoline µg/L <50 <50 180 1
190 1 ne 100/5,000
a
TPH as Diesel µg/L <100 <100 <100 <100 ne 100/2,500a
TPH as Oil µg/L <200 <200 <200 <200 ne 100/2,500a
Benzene µg/L <0.50 <0.50 0.53 <0.50 1,800 1
Toluene µg/L <0.50 <0.50 <0.50 <0.50 530,000 150
Ethylbenzene µg/L <1.50 <1.50 <0.50 <1.50 170,000 300
Xylenes µg/L <0.50 <0.50 <1.50 <0.50 160,000 1,750
MTBE µg/L <0.50 <0.50 <0.50 <0.50 80,000 13
PCE µg/L <0.50 <0.50 36 34 420 5
TCE µg/L <0.50 <0.50 140 150 1,800 5
1,1-DCE µg/L <0.50 <0.50 5.2 5.2 18,000 6
cis-1,2-DCE µg/L <0.50 <0.50 160 170 17,000 6
trans-1,2-DCE µg/L <0.50 <0.50 2.6 2.7 19,000 10
1,1-DCA µg/L <0.50 <0.50 46 45 3,400 5
Vinyl Chloride µg/L <0.50 <0.50 2.5 2.5 13 0.5
Chloroform µg/L <0.50 <0.50 0.53 <0.50 1,100 0.19 b
1,1,2-TCA µg/L <0.50 <0.50 0.91 0.85 1,200 5
Other VOCs µg/L ND ND ND ND na na
NOTES
g/L: Micrograms per liter (parts per billion)TPH: Total Petroleum Hydrocarbons
<: Not detected at or above the indicated laboratory method reporting limit
ND: Not detected above the laboratory method reporting limit; limits vary by compound
na: Not applicable
ESL: Vapor Intrusion - Environmental Screening Level for potential vapor intrusion into buildings
(RWQCB, 2008 Table E-1)
(1) Not typical of Gasoline standard pattern.
MCL: Maximum contaminant level for drinking water, California Department of Public Health (October 2008)
a: MCL not established. ESL for drinking water / non-drinking water shown instead (RWQCB, 2008)
b: MCL not established, value provided is the Regional Screening Level for tapwater, established by the U.S. EPA
MCL
Volatile Organic Compounds
JA-3 JA-4 JA-4DAnalyte Units
Sample ID Regulatory Standards
JA-2
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
1 of 1 December 16, 2011
TABLE 7
Groundwater Monitoring Well Sample Analytical Results - Metals
Regulatory
Standards
Antimony mg/L <0.009 <0.009 <0.009 <0.009 0.006
Arsenic mg/L <0.009 <0.009 <0.009 <0.009 0.010
Barium mg/L 0.13 0.074 0.17 0.16 1
Beryllium mg/L <0.005 <0.005 <0.005 <0.005 0.004
Cadmium mg/L <0.005 <0.005 <0.005 <0.005 0.005
Chromium mg/L <0.005 <0.005 0.0070 0.0067 0.05
Cobalt mg/L <0.005 <0.005 0.0080 0.0079 0.011 a
Copper mg/L <0.009 <0.009 <0.009 <0.009 1.3
Lead mg/L <0.014 <0.014 <0.014 <0.014 0.015
Mercury mg/L <0.0002 <0.0002 <0.0002 <0.0002 0.002
Molybdenum mg/L <0.009 <0.009 <0.009 <0.009 0.18 a
Nickel mg/L <0.009 0.036 0.30 0.29 0.1
Selenium mg/L <0.02 <0.02 <0.02 <0.02 0.05
Silver mg/L <0.005 <0.005 <0.005 <0.005 0.18 a
Thallium mg/L <0.009 <0.009 <0.009 <0.009 0.002
Vanadium mg/L <0.009 <0.009 <0.009 <0.009 0.18 a
Zinc mg/L <0.009 <0.009 <0.009 <0.009 ne
NOTES
mg/L: Milligrams per liter (parts per million)
<: Not detected at or above the indicated laboratory method reporting limit
ne: Not established
MCL: Maximum contaminant level for drinking water, California Department of Public Health (October 2008)
a: MCL not established, value provided is the Regional Screening Level for tapwater, established by the U.S. EPA
Dissolved Metals
JA-3 JA-4 JA-4D MCL
Analyte Units
Sample ID
JA-2
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
1 of 1 December 16, 2011
TABLE 8
Quality Control Sample Assessment - Soil
AnalyteB-5-5.0
(mg/kg)
B-5-5.0D
(mg/kg)RPD
B-7-1.0
(mg/kg)
B-7-1.0D
(mg/kg)RPD
B-12-1.0
(mg/kg)
B-12-1.0D
(mg/kg)RPD
TPH-gasoline < 0.076 < 0.073 NA < 0.1 < 0.093 NA < 0.091 < 0.076 NA
TPH-diesel 2.4 < 2 18.2% < 2 < 2 NA -- -- NA
TPH-oil 4.8 < 4 18.2% 9.2 8.9 3.3% -- -- NA
VOCs ND ND NA ND ND NA ND ND NA
SVOCs ND ND NA -- -- NA ND ND NA
PCBs ND ND NA -- -- NA -- -- NA
Arsenic 1.8 2.5 32.6% -- -- NA -- -- NA
Barium 28 43 42.3% -- -- NA -- -- NA
Chromium 45 30 40.0% -- -- NA -- -- NA
Cobalt 5.4 6.2 13.8% -- -- NA -- -- NA
Copper 5.5 < 5 9.5% -- -- NA -- -- NA
Lead 3 2.4 22.2% -- -- NA -- -- NA
Nickel 31 29 6.7% -- -- NA -- -- NA
Vanadium 30 22 30.8% -- -- NA -- -- NA
Zinc 19 16 17.1% -- -- NA -- -- NA
Other Metals ND ND NA -- -- NA -- -- NA
NOTES:
RPD: Relative Percent Difference
mg/kg: milligrams per kilogram
NA: not applicable
ND: Not detected above the laboratory method reporting limit; limits vary by compound
<: Not detected at or above the indicated laboratory method reporting limit
--: Sample pairs not analyzed
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
1 of 1 Decmber 16, 2011
TABLE 9
Quality Control Sample Assessment - Groundwater
AnalyteB-12-GW
(µg/L)
B-12-GWD
(µg/L)RPD
JA-4
(µg/L)
JA-4D
(µg/L)RPD
TPH-gasoline < 50 < 50 NA 180 190 5.4%
TPH-diesel < 100 < 100 NA < 100 < 100 NA
TPH-oil < 200 < 200 NA < 200 < 200 NA
Benzene < 0.5 < 0.5 NA 0.53 < 0.5 5.8%
PCE < 0.5 < 0.5 NA 36 34 5.7%
TCE < 0.5 < 0.5 NA 140 150 6.9%
1,1-DCE < 0.5 < 0.5 NA 5.2 5.2 0.0%
cis-1,2-DCE < 0.5 < 0.5 NA 160 170 6.1%
trans-1,2-DCE < 0.5 < 0.5 NA 2.6 2.7 3.8%
1,1-DCA < 0.5 < 0.5 NA 46 45 2.2%
Vinyl Chloride < 0.5 < 0.5 NA 2.5 2.5 0.0%
Chloroform < 0.5 < 0.5 NA 0.53 < 0.5 5.8%
1,1,2-TCA < 0.5 < 0.5 NA 0.91 0.85 6.8%
Other VOCs ND ND NA ND ND NA
Barium -- -- NA 0.17 0.16 6.1%
Chromium -- -- NA 0.007 0.0067 4.4%
Cobalt -- -- NA 0.008 0.0079 1.3%
Nickel -- -- NA 0.3 0.29 3.4%
Other Metals ND ND NA ND ND NA
NOTES:
RPD: Relative Percent Difference
µg/L: micrograms per liter
NA: not applicable
ND: Not detected above the laboratory method reporting limit; limits vary by compound
<: Not detected at or above the indicated laboratory method reporting limit
--: Sample pairs not analyzed
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
1 of 1 December 16, 2011
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
FIGURES
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
APPENDIX A
BORING PERMITS
Alameda County Public Works Agency - Water Resources Well Permit
399 Elmhurst StreetHayward, CA 94544-1395
Telephone: (510)670-6633 Fax:(510)782-1939
Application Approved on: 08/04/2011 By jamesy Permit Numbers: W2011-0515Permits Valid from 08/10/2011 to 08/11/2011
Application Id: 1312327539477 City of Project Site:OaklandSite Location: 500 Kirkham St, Oakland, CAProject Start Date: 08/10/2011 Completion Date:08/11/2011Assigned Inspector: Contact Steve Miller at (510) 670-5517 or [email protected]
Applicant: Northgate Envt. Mgmt. Inc. - Anya Starovoytov Phone: 510-839-0688 x227300 F H Ogawa Plaza, Ste 510, Oakland, CA 94612
Property Owner: State of CA, Dept. of Transportation Phone: 510-286-5322111 Grand Ave, PO Box 23440, Oakland, CA 94623
Client: City of Oakland, Gopakumar Nair Phone: 510-238-6361250 F. H Ogawa Plaza, Ste 5301, Oakland, CA 94612
Total Due: $265.00Receipt Number: WR2011-0240 Total Amount Paid: $265.00
Payer Name : Northgate Paid By: CHECK PAID IN FULL
Works Requesting Permits:
Borehole(s) for Investigation-Environmental/Monitorinig Study - 16 Boreholes
Driller: Penecore - Lic #: 906899 - Method: other Work Total: $265.00
Specifications
Permit
Number
Issued Dt Expire Dt #
Boreholes
Hole Diam Max Depth
W2011-
0515
08/04/2011 11/08/2011 16 2.25 in. 20.00 ft
Specific Work Permit Conditions1. Backfill bore hole by tremie with cement grout or cement grout/sand mixture. Upper two-three feet replaced in kind or
with compacted cuttings. All cuttings remaining or unused shall be containerized and hauled off site. The containers shall
be clearly labeled to the ownership of the container and labeled hazardous or non-hazardous.
2. Boreholes shall not be left open for a period of more than 24 hours. All boreholes left open more than 24 hours will
need approval from Alameda County Public Works Agency, Water Resources Section. All boreholes shall be backfilled
according to permit destruction requirements and all concrete material and asphalt material shall be to Caltrans Spec or
County/City Codes. No borehole(s) shall be left in a manner to act as a conduit at any time.
3. Permittee shall assume entire responsibility for all activities and uses under this permit and shall indemnify, defend
and save the Alameda County Public Works Agency, its officers, agents, and employees free and harmless from any and
all expense, cost, liability in connection with or resulting from the exercise of this Permit including, but not limited to,
properly damage, personal injury and wrongful death.
4. Applicant shall contact Steve Miller for an inspection time at (510) 670-5517 or email to [email protected] at least
five (5) working days prior to starting, once the permit has been approved. Confirm the scheduled date(s) at least 24
hours prior to drilling.
5. Copy of approved drilling permit must be on site at all times. Failure to present or show proof of the approved permit
application on site shall result in a fine of $500.00.
6. Prior to any drilling activities onto any public right-of-ways, it shall be the applicants responsibilities to contact and
Alameda County Public Works Agency - Water Resources Well Permit
coordinate a Underground Service Alert (USA), obtain encroachment permit(s), excavation permit(s) or any other permits
required for that City or to the County and follow all City or County Ordinances. It shall also be the applicants
responsibilities to provide to the Cities or to Alameda County a Traffic Safety Plan for any lane closures or detours
planned. No work shall begin until all the permits and requirements have been approved or obtained.
7. Permit is valid only for the purpose specified herein. No changes in construction procedures, as described on this
permit application. Boreholes shall not be converted to monitoring wells, without a permit application process.
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
APPENDIX B
BORING LOGS
B-1-1.0
B-1-5.0
B-1-7.0
0.1
0.0
0.0
70
90
AS
SW
SW
SC
ASPHALT (4")WELL GRADED SAND WITH GRAVEL (SW); dark yellow-brown (10YR 3/4), ~20% fine tomedium gravels, ~5% clay, ~75% fine sand, damp to moist, loose, no odorWELL GRADED SAND (SW); dark yellow-brown (10YR 4/4), trace gravels and clay, damp tomoist, loose, no odor
Same as above, clay content increases to ~10%
CLAYEY SAND (SC); dark yellow-brown (10YR 4/4), ~40% clay, ~60% fine sand, moist, mediumdense, no odor
Same as above, moisture content increases (moist to wet)
Bottom of borehole at 10.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING 8.50 ft
Ground ELEVATION
SURFACE CONDITIONS: Asphalt
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/10/11DATE STARTED 8/10/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-1
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
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BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-10-1.0
B-10-5.0
B-10-9.0
0.1
0.0
0.0
50
97
AS
SW
SC
Asphalt (4")WELL GRADED SAND (SW); dark yellow-brown (10YR 3/4), moist, loose, no odor
Same as above, color changes to yellow-brown (10YR 5/4), clay content increases with depth(~10%)CLAYEY SAND (SC); dark yellow-brown (10YR 4/6), ~60% fine sand, ~40% clay, moist to wet,occasional saturated pores, dense, no odor
Same as above, moisture content increases (wet)
Sand fraction increases to ~70%, clay ~30%
Bottom of borehole at 10.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING ---
Ground ELEVATION
SURFACE CONDITIONS: Asphalt
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/10/11DATE STARTED 8/10/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-10
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-11-1.0
B-11-6.0
B-11-10.0
0.1
0.0
308
275
28.6
4.9
3.3
7.3
70
100
100
100
AS
SW
CL
SW
Asphalt (4")WELL GRADED SAND WITH GRAVEL (SW); dark brown (10YR 3/3), ~70% fine sand, ~30% fineto coarse gravel (angular), damp, loose, no odor
SANDY CLAY WITH GRAVEL (CL); dark brown (10YR 3/3), ~60% clay (low plasticity), ~15% finesand, ~25% fine to medium angular gravels, damp no odor
WELL GRADED SAND (SW); olive (5Y 4/4), trace clay, moist, loose, strong hydrocarbon odorbetween 6' and 8.5' bgs
Same as above, moisture content increases (wet)
Same as above, occasional mottling with gray
Same as above, color changes to dark yellow-brown (10YR 4/4) with large patches of gray (2.5Y6/1), moist
Same as above, moisture increases (saturated)
Bottom of borehole at 15.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING 6.90 ft
Ground ELEVATION
SURFACE CONDITIONS: Asphalt
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/10/11DATE STARTED 8/10/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-11
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-12-1.0
B-12-5.0
B-12-10.0
0.1
0.0
0.0
0.0
90
100
100
100
AS
SW
SW
SC
SW-SC
Asphalt (4")WELL GRADED SAND WITH GRAVEL (SW); dark brown (10YR 3/3), ~80% fine sand, ~20% fineto medium gravel, trace clay, damp, loose, no odor
WELL GRADED SAND (SW); dark yellow brown (10YR 4/6), trace clay, moist to wet, mediumdense, no odor
Same as above, clay fraction increases to 15-20%CLAYEY SAND (SC); dark yellow-brown (10YR 4/6), ~60% fine sand, ~40% clay, wet, mediumdense, no odor
Same as above, moisture increases with depth
WELL GRADED SAND WITH CLAY (SW-SC); dark yellow brown (10YR 4/6), ~80-85% fine sand,~15-20% clay, occasional mottling, saturated, medium dense
Bottom of borehole at 12.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING 6.80 ft
Ground ELEVATION
SURFACE CONDITIONS: Asphalt
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/10/11DATE STARTED 8/10/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
11
12
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-12
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-13-1.0
B-13-5.0
B-13-8.0
7.3
6.8
7.0
6.8
6.4
6.0
30
100
96
100
AS
SW
SC
Asphalt (4")WELL GRADED SAND WITH GRAVEL (SW); very dark gray (10YR 3/1), ~80% fine sand, ~20%fine to medium gravel, damp, medium dense, no odor
CLAYEY SAND (SC); yellowish brown (10YR 5/6), ~60% fine sand, ~40-45% clay, damp, dense,no odor
Same as above, moisture content increases (wet)
Same as above, clay content decreases (~20%)
Same as above, clay content decreases (~15%), saturated
Same as above, color changes to light yellow brown (2.5Y 6/3), zones of gray mottling
Bottom of borehole at 15.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING 3.60 ft
Ground ELEVATION
SURFACE CONDITIONS: Asphalt
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/10/11DATE STARTED 8/10/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-13
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-14-1.0
B-14-5.0
B-14-7.0
1.2
0.7
0.5
90
100
AS
SC
CL
SW-SC
Asphalt (4")CLAYEY SAND (SC); dark yellow-brown (10YR 3/4), ~20% clay, ~10-15% fine to medium angulargravels, ~65% fine sand, moist, loose, no odorSANDY CLAY WITH GRAVEL (CL); dark yellow brown (10YR 4/4), ~20% fine to medium gravel(angular), ~20% fine sand, ~60% clay, damp, medium stiffness, no odor
WELL GRADED SAND WITH CLAY (SW-SC); dark yellow-brown (10YR 4/6), ~85% fine sand,~15% clay, moist to wet, loose, no odor
Bottom of borehole at 10.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING ---
Ground ELEVATION
SURFACE CONDITIONS: Asphalt
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/10/11DATE STARTED 8/10/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-14
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-15-1.0
B-15-5.0
B-15-9.0
0.7
0.5
0.0
90
100
AS
SW
CL
SC
Asphalt (4")WELL GRADED SAND (SW); dark brown (10YR 3/3), ~90% fine sand, ~5-10% fine to mediumgravels, trace clay, damp, medium dense, no odor
SANDY CLAY WITH GRAVEL (CL); dark yellow-brown (10YR 4/4), ~20% fine to coarse gravels(angular), ~15% fine sand, ~65% clay, damp, medium stiffness, no odor
CLAYEY SAND (SC); dark yellow brown (10YR 4/4), ~60% fine sand, ~40% clay, moist, mediumdense, no odor
Same as above, clay content decreases (~20%), moisture increases (wet)
Bottom of borehole at 10.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING ---
Ground ELEVATION
SURFACE CONDITIONS: Asphalt
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/10/11DATE STARTED 8/10/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-15
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-16-1.0
B-16-5.0
B-16-10.0
0.0
0.0
0.0
0.0
0.0
0.0
80
100
100
100
100
SW
SC
SW-SC
WELL GRADED SAND (SW); dark yellow-brown (10YR 3/4), very fine, trace gravels (fine tomedium angular), damp, loose, no odor
Same as above, moisture content increases (moist)
Same as above, moisture content increases (wet), trace wood fragments, clay fraction increasesto ~10%CLAYEY SAND (SC); yellow-brown (10YR 5/6), ~80% fine sand, ~20% clay, moist to wet,medium dense, no odor
Same as above, moisture content increases to ~40%
Same as above, occasional gray mottles, moisture content decreases with depth (moist)
Same as above, moisture increases (wet), clay content decreases (20%)
WELL GRADED SAND WITH CLAY (SW-SC); dark yellow brown (10YR 4/4), ~85-90% fine sand,~10-15% clay, wet, no odorSame as above, moisture increases with depth (wet to saturated)
Same as above, color changes to light olive brown (10YR 5/4)
Bottom of borehole at 15.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING 5.40 ft
Ground ELEVATION
SURFACE CONDITIONS: Asphalt
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/11/11DATE STARTED 8/11/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-16
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-2-1.0
B-2-5.0
B-2-9.0
0.0
0.0
0.0
0.0
70
90
AS
SW
SW
Asphalt (4")WELL GRADED SAND WITH GRAVEL (SW); dark olive brown (2.5Y 3/3), ~80% fine sand, ~20%fine to medium angular gravels, damp, loose, no odorConcrete fragments
3" zone with charred wood fragments and discolored soil, no odor
WELL GRADED SAND (SW); dark brown (10YR 3/3), damp, loose, no odor
Charred wood fragments @6' bgs
Same as above, moisture content increases (moist)
Bottom of borehole at 10.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING ---
Ground ELEVATION
SURFACE CONDITIONS: Bare soil
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/11/11DATE STARTED 8/11/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-2
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-3-1.0
B-3-5.0
B-3-9.0
0.0
0.0
0.0
50
90
SW
WELL GRADED SAND (SW); dark olive-brown (2.5Y 3/3), ~10% fine to medium gravel, rootletspresent, damp, loose, no odor
3" zone of coarse gravel (concrete fragments)
2" zone of increased clay (~10%)
Same as above, color change to very dark brown (10YR 2/2)
Same as above, color changes to dark yellow brown (10YR 4/4), damp to moist
Same as above, clay content increases (~10%)
Bottom of borehole at 10.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING ---
Ground ELEVATION
SURFACE CONDITIONS: Bare soil
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/10/11DATE STARTED 8/10/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-3
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-4-1.0
B-4-5.0
B-4-10.0
6.3
5.6
4.5
4.8
0.0
0.0
0.0
70
70
AS
SW
CL
SW-SC
Asphalt (4")WELL GRADED SAND (SW); brown (10YR 4/3), ~5% fine to medium angular gravels, damp,loose, no odor
Same as above, large pieces of charred wood debris (slight chemical odor) and coarse gravels (6"layer) and red brick fragments moisture content increases to moist
Same as above, color changes to very dark gray-brown (10YR 3/2), moist, loose, fine grainedsand, no odor
Same as above, moisture content increases (saturated), color changes to brown (10YR 4/3), noodor
Same as above, clay content increases (~10%)
LEAN CLAY WITH SAND (CL); greenish-gray (Gley1 6/5G), ~80% clay, ~20% fine sand, stiff,trace rootlets, mottling with orange, no odor
Same as above, sand fraction increases to ~25%
WELL GRADED SAND WITH CLAY (SW-SC); dark yellow brown (10YR 4/4), medium dense,wet, no odor
Same as above, occasional zones of gray mottles
Bottom of borehole at 15.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING 8.50 ft
Ground ELEVATION
SURFACE CONDITIONS: Asphalt
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/11/11DATE STARTED 8/11/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-4
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-5-1.0
B-5-5.0
B-5-10.0
5.3
7.7
7.5
6.6
8.1
90
AS
SW
Asphalt (4")WELL GRADED SAND (SW); dark yellow brown (10YR 3/4), ~90% fine sand, ~10% fine tomedium angular gravels, trace clay, damp, loose, no odor
Same as above, clay fraction increases to ~15%
Same as above, content increases (wet to saturated)
Same as above, occasional mottling with light gray, soil becoming more dense with depth, clay at15-20%
Bottom of borehole at 15.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING 4.70 ft
Ground ELEVATION
SURFACE CONDITIONS: Asphalt
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/10/11DATE STARTED 8/10/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-5
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-6-1.0
B-6-5.0
B-6-9.0
0.0
0.0
0.0
0.0
0.0
80
100
AS
SW
Asphalt (4")WELL GRADED SAND (SW); very dark gray-brown (10YR 3/2), ~5-10% fine to medium angulargravel, damp, slight chemical odor (possibly hydraulic fluid)
Same as above, slight hydrocarbon odor from 2.5' to 4' bgs, color changes to black (10YR 2/1)
Same as above, strong hydrocarbon odor, moisture content increases (wet to saturated)
Same as above, saturated conditions, slight organic/hydrocarbon (?) odor
Same as above, color changes to dark yellow brown (10YR 4/4)
Bottom of borehole at 10.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING ---
Ground ELEVATION
SURFACE CONDITIONS: Asphalt
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/11/11DATE STARTED 8/11/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-6
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-7-1.0
B-7-5.0
B-7-7.0
0.0
0.0
0.0
50
50
AS
SW
Asphalt (4")WELL GRADED SAND (SW); dark yellow brown (10YR 4/4), trace gravel, moist, loose, no odorVery dark soil (possibly charcoal) for ~2"
Same as above, color changes to dark brown (10YR 3/3), glass and charcoal or charred woodfragments throughout
Same as above color changes to dark yellow-brown (10YR 4/4), moisture content increases(saturated)
Bottom of borehole at 10.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING ---
Ground ELEVATION
SURFACE CONDITIONS: Asphalt
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/11/11DATE STARTED 8/11/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-7
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-8-1.0
B-8-5.0
B-8-8.0
1.7
1.2
0.0
0.7
0.0
0.0
50
70
100
100
AS
SW
CL
SW-SC
Asphalt (4")WELL GRADED SAND (SW); brown (10YR 4/3), trace fine gravels, damp, loose, no odor
3-4" zone of gravel and debris (crashed brick, concrete, charred wood, white rock (?), tilefragments
Large piece of concrete (~2" dia.)
Same as above, moisture content increases (saturated), color changes to dark yellow-brown(10YR 4/4)
Same as above, clay content increases (~10-15%)LEAN CLAY WITH SAND (CL); yellow-brown (10YR 5/6) with heavy gray mottles, ~75% clay,~25% fine sand, trace rootlets, wet, no odor
WELL GRADED SAND WITH CLAY (SW-SC); dark yellow-brown (10YR 4/6), ~90% fine sand,~10% clay, wet, medium dense, no odor
Same as above, clay fraction decreases (~5%)
Same as above, moisture content increases (saturated)
Bottom of borehole at 15.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING 7.90 ft
Ground ELEVATION
SURFACE CONDITIONS: Asphalt
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/11/11DATE STARTED 8/11/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-8
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
B-9-1.0
B-9-3.0
B-9-13.0
15.7
9.9
7.5
70
33
100
AS
SW
SW
Asphalt (4")WELL GRADED SAND WITH GRAVEL (SW); very dark brown (10YR 2/2), ~80% fine sand,~20% fine to coarse gravels, trace clay, damp, loose, slight chemical odor
Same as above, concrete fragments/coarse gravel at 3.8'
No recovery. Driller reports feeling a void between 5' and 10' bgs. Some coarse gravel recovered(possibly concrete)
WELL GRADED SAND (SW); dark gray-brown (2.5Y 4/2), ~90-95% fine sand, ~5-10% clay,saturated, loose, organic odor
Bottom of borehole at 15.0 feet bgs.
DRILLING METHOD Geoprobe
HOLE SIZE 2.25
DRILLING CONTRACTOR PeneCore
NOTES:
AFTER DRILLING ---
AT TIME OF DRILLING ---
AT END OF DRILLING 4.60 ft
Ground ELEVATION
SURFACE CONDITIONS: Asphalt
GROUNDWATER LEVELS:
LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky
COMPLETED 8/10/11DATE STARTED 8/10/11
SA
MP
LE T
YP
EN
UM
BE
R
DE
PT
H(f
t)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
MATERIAL DESCRIPTION
PAGE 1 OF 1BORING NUMBER B-9
PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA
BORING LOCATIONPROJECT NAME 500 Kirkham
GE
NE
RA
L N
OR
TH
GA
TE
EN
VIR
ON
ME
NT
AL
- O
S 1
204
.22_
BO
RIN
G_L
OG
S.G
PJ
9/13
/11
300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688
PID
(pp
m)
RE
CO
VE
RY
%
U.S
.C.S
.
GR
AP
HIC
LOG
Phase II Environmental Site Assessment
500 Kirkham Street
APN 004-049-001
Oakland, California
APPENDIX C
LABORATORY ANALYTICAL REPORTS
Northgate Environmental Management Inc.300 Frank H. Ogawa Plaza, Suite 510Oakland, California 94612Tel: 5108390688Fax: (510) 839-4350RE: 500 Kirkham
Torrent Laboratory, Inc. received 40 sample(s) on August 23, 2011 for the analyses presented in the following Report.
Dear Dennis Laduzinsky:
Work Order No.: 1108073 Rev: 1
All data for associated QC met EPA or laboratory specification(s) except where noted in the case narrative.
Torrent Laboratory, Inc. is certified by the State of California, ELAP #1991. If you have any questions regarding these test results, please feel free to contact the Project Management Team at (408)263-5258; ext 204.
DateAugust 18, 2011
Patti Sandrock
Page 1 of 260Total Page Count: 260
Date: 8/18/2011
Client: Northgate Environmental Management Inc.
Project: 500 Kirkham
Work Order: 1108073
CASE NARRATIVE
No issues encountered with the receiving, preparation, analysis or reporting of the results associated with this work order.
Note for 8260B/GCMS-GRO: Final result & PQL (Reporting limit) has been corrected for actual mass from pre-tarred 5035 VOAs for all samples except 1108073-014A. Due to high concentration of hydrocarbons, methanol extraction was performed. Sample was analyzed from liner.
Analytical Comments for method S_6010B, 1108073-002 MS/MSD, QC Analytical Batch ID 406266, Note:The % recoveries for Barium, Copper and Nickel are outside of laboratory control limits but are within % RPD limits. The associated LCS/LCSD % recoveries and % RPD are within limits. No corrective action required.
Analytical Comments for method S_8270C, 1108073-002 MS/MSD, QC Analytical Batch ID 406315, Note:The % recoveries for 1,4-DCB are outside of laboratory control limits but are within % RPD limits. The associated LCS/LCSD % recoveries and % RPD are within limits. No corrective action required.
Analytical Comments for method S_TPHDO, 1108073-002 MS/MSD, QC Analytical Batch ID 406315, Note:The % recoveries for TPH as Diesel are outside of laboratory control limits but are within % RPD limits. The associated LCS/LCSD % recoveries and % RPD are within limits. No corrective action required.
Analytical Comment for Method S_8081, 1108073-002 MS/MSD, although an MS/MSD was extracted it is not reported due to the high concentration of compounds found in the parent sample (reported at a 20X dilution).
REVISIONS:
Per client request, STLC extraction and analysis for Lead was performed on sample -004A.
Note: Extraction of 50 g sample / 500g 0.2M Sodium Citrate Solution was performed according to wet extraction procedure (WET) which was rotated in a rotary shaker for 48 hours.
STLC:Extraction started on 8/23/11 @4.30 PM and ended on 8/25/[email protected] PM. Rev 1 (8/26/11)
Page 2 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-001B-1-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg2.31.70.28SW6010B 1
Barium mg/Kg725.01SW6010B 1Chromium mg/Kg225.00.0590SW6010B 1
Copper mg/Kg125.00.0900SW6010B 1
Lead mg/Kg551.00.043SW6010B 1Nickel mg/Kg9.95.00.0590SW6010B 1
Vanadium mg/Kg235.00.12SW6010B 1
Zinc mg/Kg235.00.59SW6010B 1
TPH as Motor Oil mg/Kg160208.33SW8015B(M) 1
1108073-002B-1-5.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg2.01.70.28SW6010B 1
Barium mg/Kg275.01SW6010B 1Chromium mg/Kg265.00.0590SW6010B 1
Cobalt mg/Kg6.15.00.14SW6010B 1
Lead mg/Kg2.01.00.043SW6010B 1Nickel mg/Kg195.00.0590SW6010B 1
Vanadium mg/Kg205.00.12SW6010B 1
Zinc mg/Kg115.00.59SW6010B 1
Page 3 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-004B-3-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg4.21.70.28SW6010B 1
Barium mg/Kg1405.01SW6010B 1Chromium mg/Kg365.00.0590SW6010B 1
Cobalt mg/Kg8.05.00.14SW6010B 1
Copper mg/Kg295.00.0900SW6010B 1Lead mg/Kg1001.00.043SW6010B 1
Nickel mg/Kg245.00.0590SW6010B 1
Vanadium mg/Kg305.00.12SW6010B 1Zinc mg/Kg995.00.59SW6010B 1
Mercury mg/Kg0.190.100.01SW7471A 1
TPH as Motor Oil mg/Kg130208.33SW8015B(M) 1
Lead (STLC) mg/L4.10.100.0500SW6010B 1
Page 4 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-005B-3-5.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Barium mg/Kg695.01SW6010B 1
Chromium mg/Kg235.00.0590SW6010B 1Lead mg/Kg3.01.00.043SW6010B 1
Nickel mg/Kg145.00.0590SW6010B 1
Vanadium mg/Kg185.00.12SW6010B 1Zinc mg/Kg165.00.59SW6010B 1
TPH(Gasoline) ug/Kg11087158260TPH 1
TPH as Diesel mg/Kg2.02.00.759SW8015B(M) 1TPH as Motor Oil mg/Kg6.84.01.65SW8015B(M) 1
1108073-007B-10-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg1.71.70.28SW6010B 1
Barium mg/Kg425.01SW6010B 1
Chromium mg/Kg235.00.0590SW6010B 1Lead mg/Kg3.51.00.043SW6010B 1
Nickel mg/Kg145.00.0590SW6010B 1
Vanadium mg/Kg175.00.12SW6010B 1Zinc mg/Kg135.00.59SW6010B 1
TPH as Motor Oil mg/Kg888.03.33SW8015B(M) 1
Page 5 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-008B-10-5.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg2.11.70.28SW6010B 1
Barium mg/Kg475.01SW6010B 1Chromium mg/Kg375.00.0590SW6010B 1
Cobalt mg/Kg6.75.00.14SW6010B 1
Copper mg/Kg5.95.00.0900SW6010B 1Lead mg/Kg3.11.00.043SW6010B 1
Nickel mg/Kg315.00.0590SW6010B 1
Vanadium mg/Kg295.00.12SW6010B 1Zinc mg/Kg205.00.59SW6010B 1
TPH as Motor Oil mg/Kg6.34.01.65SW8015B(M) 1
1108073-010B-12-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg1.71.70.28SW6010B 1
Barium mg/Kg425.01SW6010B 1Chromium mg/Kg245.00.0590SW6010B 1
Lead mg/Kg2.01.00.043SW6010B 1
Nickel mg/Kg155.00.0590SW6010B 1Vanadium mg/Kg175.00.12SW6010B 1
Zinc mg/Kg125.00.59SW6010B 1
TPH as Motor Oil mg/Kg294.01.65SW8015B(M) 1
Page 6 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-011B-12-5.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg2.51.70.28SW6010B 1
Barium mg/Kg465.01SW6010B 1Chromium mg/Kg445.00.0590SW6010B 1
Cobalt mg/Kg115.00.14SW6010B 1
Copper mg/Kg6.15.00.0900SW6010B 1Lead mg/Kg3.21.00.043SW6010B 1
Nickel mg/Kg335.00.0590SW6010B 1
Vanadium mg/Kg295.00.12SW6010B 1Zinc mg/Kg205.00.59SW6010B 1
TPH as Diesel mg/Kg2.22.00.759SW8015B(M) 1
Page 7 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-013B-11-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg161.70.28SW6010B 1
Barium mg/Kg4305.01SW6010B 1Cadmium mg/Kg1.11.00.0590SW6010B 1
Chromium mg/Kg8.55.00.0590SW6010B 1
Cobalt mg/Kg9.25.00.14SW6010B 1Copper mg/Kg585.00.0900SW6010B 1
Lead mg/Kg181.00.043SW6010B 1
Nickel mg/Kg165.00.0590SW6010B 1Vanadium mg/Kg395.00.12SW6010B 1
Zinc mg/Kg775.00.59SW6010B 1
Mercury mg/Kg0.380.100.01SW7471A 1
TPH as Motor Oil mg/Kg130208.33SW8015B(M) 1
Page 8 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-014B-11-6.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg4.81.70.28SW6010B 1
Barium mg/Kg425.01SW6010B 1Chromium mg/Kg305.00.0590SW6010B 1
Cobalt mg/Kg5.35.00.14SW6010B 1
Copper mg/Kg5.75.00.0900SW6010B 1Lead mg/Kg4.31.00.043SW6010B 1
Nickel mg/Kg315.00.0590SW6010B 1
Vanadium mg/Kg295.00.12SW6010B 1Zinc mg/Kg175.00.59SW6010B 1
Ethyl Benzene ug/Kg1500100086SW8260B 100m,p-Xylene ug/Kg48001000190SW8260B 100
o-Xylene ug/Kg67050066SW8260B 100
1,3,5-Trimethylbenzene ug/Kg16001000110SW8260B 1001,2,4-Trimethylbenzene ug/Kg48001000110SW8260B 100
TPH(Gasoline) ug/Kg1500001000017008260TPH 100
TPH as Diesel mg/Kg8.12.00.759SW8015B(M) 1
TPH as Motor Oil mg/Kg5.24.01.65SW8015B(M) 1
1108073-015B-11-10.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
All compounds were non-detectable for this sample.
Page 9 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-016B-14-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg2.71.70.28SW6010B 1
Barium mg/Kg775.01SW6010B 1Chromium mg/Kg285.00.0590SW6010B 1
Cobalt mg/Kg5.75.00.14SW6010B 1
Copper mg/Kg135.00.0900SW6010B 1Lead mg/Kg461.00.043SW6010B 1
Nickel mg/Kg265.00.0590SW6010B 1
Vanadium mg/Kg225.00.12SW6010B 1Zinc mg/Kg475.00.59SW6010B 1
m,p-Xylene ug/Kg7.77.71.4SW8260B 11,2,4-Trimethylbenzene ug/Kg8.97.70.84SW8260B 1
TPH as Motor Oil mg/Kg280208.33SW8015B(M) 1
Page 10 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-017B-14-5.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg3.41.70.28SW6010B 1
Barium mg/Kg755.01SW6010B 1Chromium mg/Kg365.00.0590SW6010B 1
Cobalt mg/Kg6.65.00.14SW6010B 1
Copper mg/Kg115.00.0900SW6010B 1Lead mg/Kg7.21.00.043SW6010B 1
Nickel mg/Kg305.00.0590SW6010B 1
Vanadium mg/Kg315.00.12SW6010B 1Zinc mg/Kg255.00.59SW6010B 1
TPH as Motor Oil mg/Kg144.01.65SW8015B(M) 1
Page 11 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-019B-15-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg3.91.70.28SW6010B 1
Barium mg/Kg825.01SW6010B 1Chromium mg/Kg255.00.0590SW6010B 1
Cobalt mg/Kg6.45.00.14SW6010B 1
Copper mg/Kg185.00.0900SW6010B 1Lead mg/Kg531.00.043SW6010B 1
Nickel mg/Kg245.00.0590SW6010B 1
Vanadium mg/Kg245.00.12SW6010B 1Zinc mg/Kg565.00.59SW6010B 1
Mercury mg/Kg0.100.100.01SW7471A 1
TPH as Motor Oil mg/Kg150208.33SW8015B(M) 1
1108073-020B-15-5.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg2.21.70.28SW6010B 1
Barium mg/Kg315.01SW6010B 1
Chromium mg/Kg345.00.0590SW6010B 1Lead mg/Kg2.41.00.043SW6010B 1
Nickel mg/Kg195.00.0590SW6010B 1
Vanadium mg/Kg235.00.12SW6010B 1Zinc mg/Kg135.00.59SW6010B 1
TPH as Diesel mg/Kg2.62.00.759SW8015B(M) 1
TPH as Motor Oil mg/Kg6.04.01.65SW8015B(M) 1
Page 12 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-022B-9-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg4.01.70.28SW6010B 1
Barium mg/Kg865.01SW6010B 1Chromium mg/Kg225.00.0590SW6010B 1
Cobalt mg/Kg6.15.00.14SW6010B 1
Copper mg/Kg225.00.0900SW6010B 1Lead mg/Kg871.00.043SW6010B 1
Nickel mg/Kg205.00.0590SW6010B 1
Vanadium mg/Kg225.00.12SW6010B 1Zinc mg/Kg735.00.59SW6010B 1
Mercury mg/Kg0.230.100.01SW7471A 1
TPH as Motor Oil mg/Kg7204016.7SW8015B(M) 1
Page 13 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-023B-9-3.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg3.81.70.28SW6010B 1
Barium mg/Kg785.01SW6010B 1Chromium mg/Kg385.00.0590SW6010B 1
Cobalt mg/Kg175.00.14SW6010B 1
Copper mg/Kg195.00.0900SW6010B 1Lead mg/Kg441.00.043SW6010B 1
Nickel mg/Kg245.00.0590SW6010B 1
Vanadium mg/Kg415.00.12SW6010B 1Zinc mg/Kg415.00.59SW6010B 1
Mercury mg/Kg0.250.100.01SW7471A 1
TPH as Motor Oil mg/Kg270208.33SW8015B(M) 1
1108073-025B-5-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Barium mg/Kg375.01SW6010B 1Chromium mg/Kg235.00.0590SW6010B 1
Cobalt mg/Kg6.05.00.14SW6010B 1
Lead mg/Kg2.11.00.043SW6010B 1Nickel mg/Kg145.00.0590SW6010B 1
Vanadium mg/Kg175.00.12SW6010B 1
Zinc mg/Kg125.00.59SW6010B 1
TPH as Motor Oil mg/Kg124.01.65SW8015B(M) 1
Page 14 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-026B-5-5.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg1.81.70.28SW6010B 1
Barium mg/Kg285.01SW6010B 1Chromium mg/Kg455.00.0590SW6010B 1
Cobalt mg/Kg5.45.00.14SW6010B 1
Copper mg/Kg5.55.00.0900SW6010B 1Lead mg/Kg3.01.00.043SW6010B 1
Nickel mg/Kg315.00.0590SW6010B 1
Vanadium mg/Kg305.00.12SW6010B 1Zinc mg/Kg195.00.59SW6010B 1
TPH as Diesel mg/Kg2.42.00.759SW8015B(M) 1
TPH as Motor Oil mg/Kg4.84.01.65SW8015B(M) 1
Page 15 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-028B-13-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg4.31.70.28SW6010B 1
Barium mg/Kg945.01SW6010B 1Chromium mg/Kg305.00.0590SW6010B 1
Cobalt mg/Kg7.05.00.14SW6010B 1
Copper mg/Kg195.00.0900SW6010B 1Lead mg/Kg531.00.043SW6010B 1
Nickel mg/Kg335.00.0590SW6010B 1
Vanadium mg/Kg295.00.12SW6010B 1Zinc mg/Kg585.00.59SW6010B 1
TPH as Motor Oil mg/Kg9604016.5SW8015B(M) 1
1108073-029B-13-5.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg2.51.70.28SW6010B 1Barium mg/Kg555.01SW6010B 1
Chromium mg/Kg495.00.0590SW6010B 1
Cobalt mg/Kg6.25.00.14SW6010B 1Copper mg/Kg6.75.00.0900SW6010B 1
Lead mg/Kg3.51.00.043SW6010B 1
Nickel mg/Kg375.00.0590SW6010B 1Vanadium mg/Kg375.00.12SW6010B 1
Zinc mg/Kg215.00.59SW6010B 1
Page 16 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-031B-12-1.0 D
Parameters: PQLMDL UnitResultsDFAnalysisMethod
All compounds were non-detectable for this sample.
1108073-032B-5-5.0 D
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg2.51.70.28SW6010B 1
Barium mg/Kg435.01SW6010B 1Chromium mg/Kg305.00.0590SW6010B 1
Cobalt mg/Kg6.25.00.14SW6010B 1
Lead mg/Kg2.41.00.043SW6010B 1Nickel mg/Kg295.00.0590SW6010B 1
Vanadium mg/Kg225.00.12SW6010B 1
Zinc mg/Kg165.00.59SW6010B 1
1108073-033B-1-GW
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Barium (Dissolved) mg/L0.0350.0090.002SW6010B 1Molybdenum (Dissolved) mg/L0.0270.0090.002SW6010B 1
Nickel (Dissolved) mg/L0.0120.0090.002SW6010B 1
Page 17 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-034B-12-GW
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Barium (Dissolved) mg/L0.0220.0090.002SW6010B 1
Cobalt (Dissolved) mg/L0.0120.0050.002SW6010B 1Molybdenum (Dissolved) mg/L0.0400.0090.002SW6010B 1
Nickel (Dissolved) mg/L0.0190.0090.002SW6010B 1
1108073-035B-12-GWD
Parameters: PQLMDL UnitResultsDFAnalysisMethod
All compounds were non-detectable for this sample.
Page 18 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-036B-11-GW
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Ethyl Benzene ug/L450.500.15SW8260B 1
m,p-Xylene ug/L1101.00.20SW8260B 1o-Xylene ug/L170.500.13SW8260B 1
Isopropyl Benzene ug/L6.10.500.28SW8260B 1
n-Propylbenzene ug/L210.500.30SW8260B 11,3,5-Trimethylbenzene ug/L260.500.20SW8260B 1
1,2,4-Trimethylbenzene ug/L520.500.33SW8260B 1
n-Butylbenzene ug/L4.60.500.32SW8260B 1Naphthalene ug/L121.00.57SW8260B 1
TPH(Gasoline) ug/L130050228260TPH 1
TPH as Diesel (SG) mg/L0.350.100.0400SW8015B(M) 1
Barium (Dissolved) mg/L0.0470.0090.002SW6010B 1
Cobalt (Dissolved) mg/L0.00600.0050.002SW6010B 1
Molybdenum (Dissolved) mg/L0.0300.0090.002SW6010B 1
1108073-037B-9-GW
Parameters: PQLMDL UnitResultsDFAnalysisMethod
MTBE ug/L0.690.500.38SW8260B 1
Arsenic (Dissolved) mg/L0.0200.0090.005SW6010B 1
Barium (Dissolved) mg/L0.190.0090.002SW6010B 1Molybdenum (Dissolved) mg/L0.0160.0090.002SW6010B 1
Page 19 of 260Total Page Count: 260
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/18/11
Sample Result Summary
1108073-038B-13-GW
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Vinyl Chloride ug/L1.10.600.44SW8260B 1.19
trans-1,2-Dichloroethene ug/L1.50.600.37SW8260B 1.19cis-1,2-Dichloroethene ug/L9.60.600.39SW8260B 1.19
Chloroform ug/L0.610.600.35SW8260B 1.19
Trichloroethylene ug/L490.600.45SW8260B 1.19Tetrachloroethylene ug/L480.600.18SW8260B 1.19
TPH(Gasoline) ug/L5160268260TPH 1.19
Barium (Dissolved) mg/L0.0910.0090.002SW6010B 1Cobalt (Dissolved) mg/L0.00950.0050.002SW6010B 1
Molybdenum (Dissolved) mg/L0.0430.0090.002SW6010B 1
Nickel (Dissolved) mg/L0.0200.0090.002SW6010B 1Silver (Dissolved) mg/L0.00560.0050.002SW6010B 1
1108073-039B-5-GW
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Barium (Dissolved) mg/L0.0300.0090.002SW6010B 1
Cobalt (Dissolved) mg/L0.0230.0050.002SW6010B 1Molybdenum (Dissolved) mg/L0.0230.0090.002SW6010B 1
Nickel (Dissolved) mg/L0.0330.0090.002SW6010B 1
Silver (Dissolved) mg/L0.00540.0050.002SW6010B 1
1108073-040Equip BLANK
Parameters: PQLMDL UnitResultsDFAnalysisMethod
All compounds were non-detectable for this sample.
Page 20 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 8:301204.22500 KirkhamB-1-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg2.3Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg72Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg22Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDCobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg12Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg55Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg9.9Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg23Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg23Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921
Page 21 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 8:301204.22500 KirkhamB-1-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 8.8 40 340120SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 7.9 40 340120SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 7.3 40 340120SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 9.8 40 340120SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 22 40 340120SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 8.8 40 340120SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 6.3 40 340120SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 8.4 40 340120SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 7.2 40 340120SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 12 40 340120SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 9.5 40 340120SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 8.5 40 340120SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 11 40 340120SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 9.4 40 340120SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 31 40 340120SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 16 40 340120SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 21 40 340120SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 9.8 40 340120SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 12 100 340120SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 8.0 40 340120SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 200 400 340120SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 200 2000 340120SW8081A 8/16/11 406314%121TCMX (S) 08/16/11 52.5 139 340120SW8081A 8/16/11 406314S %142DCBP (S) 08/16/11 50.2 139 340120
Reporting limits increased due to the nature of the sample matrix (dark color extract). Surrogate recovery of DCBP is bias high possibly due to the dilution made on the sample; recovery of second surrogate supports data quality.
NOTE:
Page 22 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 8:301204.22500 KirkhamB-1-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%102TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324S %117DCBP (S) 08/17/11 55.1 113 34001
Surrogate recovery of DCPB is bias high; recovery of second surrogate supports data quality. Sample is ND.NOTE:
Page 23 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 8:301204.22500 KirkhamB-1-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDDichlorodifluoromethane 08/15/11 3.9 8.9 NA1SW8260B NA 406301ug/KgNDChloromethane 08/15/11 4.1 8.9 NA1SW8260B NA 406301ug/KgNDVinyl Chloride 08/15/11 2.4 8.9 NA1SW8260B NA 406301ug/KgNDBromomethane 08/15/11 4.2 8.9 NA1SW8260B NA 406301ug/KgNDTrichlorofluoromethane 08/15/11 2.6 8.9 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethene 08/15/11 1.4 8.9 NA1SW8260B NA 406301ug/KgNDFreon 113 08/15/11 3.3 8.9 NA1SW8260B NA 406301ug/KgNDMethylene Chloride 08/15/11 1.8 45 NA1SW8260B NA 406301ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.99 8.9 NA1SW8260B NA 406301ug/KgNDMTBE 08/15/11 2.3 8.9 NA1SW8260B NA 406301ug/KgNDtert-Butanol 08/15/11 18 45 NA1SW8260B NA 406301ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.9 8.9 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethane 08/15/11 1.1 8.9 NA1SW8260B NA 406301ug/KgNDETBE 08/15/11 2.1 8.9 NA1SW8260B NA 406301ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.6 8.9 NA1SW8260B NA 406301ug/KgND2,2-Dichloropropane 08/15/11 1.1 8.9 NA1SW8260B NA 406301ug/KgNDBromochloromethane 08/15/11 2.0 8.9 NA1SW8260B NA 406301ug/KgNDChloroform 08/15/11 1.1 8.9 NA1SW8260B NA 406301ug/KgNDCarbon Tetrachloride 08/15/11 1.4 8.9 NA1SW8260B NA 406301ug/KgND1,1,1-Trichloroethane 08/15/11 1.1 8.9 NA1SW8260B NA 406301ug/KgND1,1-Dichloropropene 08/15/11 1.3 8.9 NA1SW8260B NA 406301ug/KgNDBenzene 08/15/11 1.3 8.9 NA1SW8260B NA 406301ug/KgNDTAME 08/15/11 1.8 8.9 NA1SW8260B NA 406301ug/KgND1,2-Dichloroethane 08/15/11 1.7 8.9 NA1SW8260B NA 406301ug/KgNDTrichloroethylene 08/15/11 3.5 8.9 NA1SW8260B NA 406301ug/KgNDDibromomethane 08/15/11 2.0 8.9 NA1SW8260B NA 406301ug/KgND1,2-Dichloropropane 08/15/11 1.2 8.9 NA1SW8260B NA 406301ug/KgNDBromodichloromethane 08/15/11 0.99 8.9 NA1SW8260B NA 406301ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.3 8.9 NA1SW8260B NA 406301ug/KgNDToluene 08/15/11 0.87 8.9 NA1SW8260B NA 406301ug/KgNDTetrachloroethylene 08/15/11 1.6 8.9 NA1SW8260B NA 406301ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.0 8.9 NA1SW8260B NA 406301ug/KgND1,1,2-Trichloroethane 08/15/11 1.6 8.9 NA1SW8260B NA 406301ug/KgNDDibromochloromethane 08/15/11 1.0 8.9 NA1SW8260B NA 406301ug/KgND1,3-Dichloropropane 08/15/11 1.8 8.9 NA1SW8260B NA 406301ug/KgND1,2-Dibromoethane 08/15/11 1.6 8.9 NA1
Page 24 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 8:301204.22500 KirkhamB-1-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDEthyl Benzene 08/15/11 0.77 8.9 NA1SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 3.7 8.9 NA1SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.76 8.9 NA1SW8260B NA 406301ug/KgNDm,p-Xylene 08/15/11 1.6 8.9 NA1SW8260B NA 406301ug/KgNDo-Xylene 08/15/11 0.59 4.5 NA1SW8260B NA 406301ug/KgNDStyrene 08/15/11 0.68 8.9 NA1SW8260B NA 406301ug/KgNDBromoform 08/15/11 1.7 8.9 NA1SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 1.1 8.9 NA1SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 1.3 8.9 NA1SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 1.1 8.9 NA1SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.7 8.9 NA1SW8260B NA 406301ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.0 8.9 NA1SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 3.0 8.9 NA1SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 1.4 8.9 NA1SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 1.4 8.9 NA1SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 1.3 8.9 NA1SW8260B NA 406301ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.97 8.9 NA1SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 1.5 8.9 NA1SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 1.3 8.9 NA1SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 1.6 8.9 NA1SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 1.3 8.9 NA1SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 1.9 8.9 NA1SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 1.2 8.9 NA1SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.8 8.9 NA1SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 2.3 8.9 NA1SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.9 8.9 NA1SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 2.5 8.9 NA1SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.6 8.9 NA1SW8260B NA 406301%95.0(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406301%93.8(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406301%117(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 25 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 8:301204.22500 KirkhamB-1-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 200 198 337420SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 33.3 100 337420SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 37.2 100 337420SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 39.0 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 20.7 100 337420SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 39.0 100 337420SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 22.2 100 337420SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 20.1 2000 337420SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 31.5 100 337420SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 21.6 100 337420SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 35.1 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 20.7 100 337420SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 42.0 100 337420SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 28.2 100 337420SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 14.1 100 337420SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 16.0 100 337420SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 17.4 198 337420SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 15.9 198 337420SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 40.2 2000 337420SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 1700 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 17.7 100 337420SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 31.5 100 337420SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 22.2 100 337420SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 31.5 100 337420SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 27.3 100 337420SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 30.0 100 337420SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 19.8 100 337420SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 30.9 100 337420SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 24.0 100 337420SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 24.0 100 337420SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 8.40 100 337420SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 28.8 100 337420SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 36.6 100 337420SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 18.0 990 337420SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 21.0 100 337420
Page 26 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 8:301204.22500 KirkhamB-1-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 35.7 100 337420SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 32.0 100 337420SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 25.8 100 337420SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 8.10 100 337420SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 26.0 100 337420SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 21.0 100 337420SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 29.1 100 337420SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 9.00 990 337420SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 20.1 100 337420SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 23.7 100 337420SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 8.10 100 337420SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 36.0 100 337420SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 36.0 100 337420SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 35.4 100 337420SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 30.0 100 337420SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 24.3 100 337420SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 24.3 100 337420SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 20.1 100 337420SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 20.1 100 337420SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 33.0 100 337420SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 24.6 990 337420SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 30.6 100 337420SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 30.9 990 337420SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 42.9 100 337420SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 40.1 100 337420SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 40.1 100 337420SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 32.7 510 337420SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 40.1 198 337420SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 113 990 337420SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 44.5 100 337420SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 27.0 100 337420SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 45.3 100 337420SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 46.2 100 337420SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 53.4 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 25.2 100 337420
Page 27 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 8:301204.22500 KirkhamB-1-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 41.7 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 40.2 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 51.3 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 40.8 100 337420SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 39.6 100 337420SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 45.9 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 45.6 100 337420SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 45.6 100 337420SW8270C 8/14/11 406315S,D %0.0002,4,6-Tribromophenol (S) 08/15/11 19 122 337420SW8270C 8/14/11 406315S,D %0.0002-Fluorobiphenyl (S) 08/15/11 30 115 337420SW8270C 8/14/11 406315S,D %0.0002-Fluorophenol (S) 08/15/11 25 121 337420SW8270C 8/14/11 406315S,D %0.000Nitrobenzene-d5 (S) 08/15/11 23 120 337420SW8270C 8/14/11 406315S,D %0.000Phenol-d6 (S) 08/15/11 24 113 337420SW8270C 8/14/11 406315S,D %0.000p-Terphenyl-d14 (S) 08/15/11 18 137 337420
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406301ug/KgNDTPH(Gasoline) 08/15/11 15 89 NA18260TPH NA 406301%45.0(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 3.83 10 33981SW8015B(M) 8/16/11 406319mg/Kg160TPH as Motor Oil 08/17/11 8.33 20 33981SW8015B(M) 8/16/11 406319mg/Kg79.8Pentacosane (S) 08/17/11 59.7 129 33981
Page 28 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 8:351204.22500 KirkhamB-1-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg2.0Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg27Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg26Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg6.1Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/KgNDCopper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg2.0Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg19Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg20Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg11Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%82.2TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%81.2DCBP (S) 08/17/11 55.1 113 34001
Page 29 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 8:351204.22500 KirkhamB-1-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDDichlorodifluoromethane 08/15/11 3.5 8.1 NA1SW8260B NA 406328ug/KgNDChloromethane 08/15/11 3.7 8.1 NA1SW8260B NA 406328ug/KgNDVinyl Chloride 08/15/11 2.1 8.1 NA1SW8260B NA 406328ug/KgNDBromomethane 08/15/11 3.8 8.1 NA1SW8260B NA 406328ug/KgNDTrichlorofluoromethane 08/15/11 2.3 8.1 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethene 08/15/11 1.3 8.1 NA1SW8260B NA 406328ug/KgNDFreon 113 08/15/11 3.0 8.1 NA1SW8260B NA 406328ug/KgNDMethylene Chloride 08/15/11 1.6 41 NA1SW8260B NA 406328ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.90 8.1 NA1SW8260B NA 406328ug/KgNDMTBE 08/15/11 2.1 8.1 NA1SW8260B NA 406328ug/KgNDtert-Butanol 08/15/11 17 41 NA1SW8260B NA 406328ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.8 8.1 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethane 08/15/11 1.0 8.1 NA1SW8260B NA 406328ug/KgNDETBE 08/15/11 2.0 8.1 NA1SW8260B NA 406328ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.4 8.1 NA1SW8260B NA 406328ug/KgND2,2-Dichloropropane 08/15/11 1.0 8.1 NA1SW8260B NA 406328ug/KgNDBromochloromethane 08/15/11 1.9 8.1 NA1SW8260B NA 406328ug/KgNDChloroform 08/15/11 0.99 8.1 NA1SW8260B NA 406328ug/KgNDCarbon Tetrachloride 08/15/11 1.3 8.1 NA1SW8260B NA 406328ug/KgND1,1,1-Trichloroethane 08/15/11 0.98 8.1 NA1SW8260B NA 406328ug/KgND1,1-Dichloropropene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgNDBenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgNDTAME 08/15/11 1.7 8.1 NA1SW8260B NA 406328ug/KgND1,2-Dichloroethane 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgNDTrichloroethylene 08/15/11 3.1 8.1 NA1SW8260B NA 406328ug/KgNDDibromomethane 08/15/11 1.8 8.1 NA1SW8260B NA 406328ug/KgND1,2-Dichloropropane 08/15/11 1.1 8.1 NA1SW8260B NA 406328ug/KgNDBromodichloromethane 08/15/11 0.90 8.1 NA1SW8260B NA 406328ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.1 8.1 NA1SW8260B NA 406328ug/KgNDToluene 08/15/11 0.80 8.1 NA1SW8260B NA 406328ug/KgNDTetrachloroethylene 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.93 8.1 NA1SW8260B NA 406328ug/KgND1,1,2-Trichloroethane 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgNDDibromochloromethane 08/15/11 0.91 8.1 NA1SW8260B NA 406328ug/KgND1,3-Dichloropropane 08/15/11 1.7 8.1 NA1SW8260B NA 406328ug/KgND1,2-Dibromoethane 08/15/11 1.4 8.1 NA1
Page 30 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 8:351204.22500 KirkhamB-1-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.70 8.1 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 3.4 8.1 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.69 8.1 NA1SW8260B NA 406328ug/KgNDm,p-Xylene 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.54 4.1 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.62 8.1 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 1.0 8.1 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 0.96 8.1 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.4 8.1 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.91 8.1 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 2.7 8.1 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.3 8.1 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.3 8.1 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.88 8.1 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.3 8.1 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 1.8 8.1 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 1.1 8.1 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.4 8.1 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 2.1 8.1 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.7 8.1 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.3 8.1 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.3 8.1 NA1SW8260B NA 406328%76.5(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%90.9(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%92.6(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 31 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 8:351204.22500 KirkhamB-1-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 0.660 0.653 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 0.110 0.330 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 0.123 0.330 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 0.0663 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 0.0713 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 0.116 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 0.139 0.330 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 0.0931 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.0465 0.330 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.0528 0.330 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.0574 0.653 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.0525 0.653 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 0.133 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 5.59 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.0584 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 0.0901 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.0653 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 0.102 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.0277 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 0.0950 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 0.121 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.0594 3.27 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 0.118 0.330 33741
Page 32 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 8:351204.22500 KirkhamB-1-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 0.106 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 0.0851 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 0.0858 0.330 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 0.0960 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.0297 3.27 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 0.0782 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 0.117 0.330 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 0.109 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 0.0812 3.27 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 0.101 0.330 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 0.102 3.27 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 0.142 0.330 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 0.108 1.68 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 0.132 0.653 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 0.374 3.27 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 0.147 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 0.0891 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 0.149 0.330 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 0.152 0.330 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 0.176 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 0.0832 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 0.138 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 0.133 0.330 33741
Page 33 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 8:351204.22500 KirkhamB-1-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 0.169 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 0.135 0.330 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 0.131 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 0.151 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315%57.22,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%69.72-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%59.12-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%65.8Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%68.2Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315%66.1p-Terphenyl-d14 (S) 08/15/11 18 137 33741
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/15/11 406328ug/KgNDTPH(Gasoline) 08/15/11 14 81 342518260TPH 8/15/11 406328%82.7(S) 4-Bromofluorobenzene 08/15/11 43.9 127 34251
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/KgNDTPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg110Pentacosane (S) 08/17/11 59.7 129 33981
Page 34 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:151204.22500 KirkhamB-3-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/25/11 406447mg/L4.1Lead (STLC) 08/26/11 0.0500 0.10 34961
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg4.2Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg140Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg36Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg8.0Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg29Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg100Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg24Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg30Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg99Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/Kg0.19Mercury 08/16/11 0.01 0.10 33921
Page 35 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:151204.22500 KirkhamB-3-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 8.8 40 340120SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 7.9 40 340120SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 7.3 40 340120SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 9.8 40 340120SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 22 40 340120SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 8.8 40 340120SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 6.3 40 340120SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 8.4 40 340120SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 7.2 40 340120SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 12 40 340120SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 9.5 40 340120SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 8.5 40 340120SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 11 40 340120SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 9.4 40 340120SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 31 40 340120SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 16 40 340120SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 21 40 340120SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 9.8 40 340120SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 12 100 340120SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 8.0 40 340120SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 200 400 340120SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 200 2000 340120SW8081A 8/16/11 406314%90.1TCMX (S) 08/16/11 52.5 139 340120SW8081A 8/16/11 406314%92.0DCBP (S) 08/16/11 50.2 139 340120
Reporting limits increased due to the nature of the sample matrix (dark color extract).NOTE:
Page 36 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:151204.22500 KirkhamB-3-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%91.3TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%105DCBP (S) 08/17/11 55.1 113 34001
Page 37 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:151204.22500 KirkhamB-3-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDDichlorodifluoromethane 08/15/11 3.7 8.4 NA1SW8260B NA 406328ug/KgNDChloromethane 08/15/11 3.9 8.4 NA1SW8260B NA 406328ug/KgNDVinyl Chloride 08/15/11 2.2 8.4 NA1SW8260B NA 406328ug/KgNDBromomethane 08/15/11 3.9 8.4 NA1SW8260B NA 406328ug/KgNDTrichlorofluoromethane 08/15/11 2.4 8.4 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethene 08/15/11 1.3 8.4 NA1SW8260B NA 406328ug/KgNDFreon 113 08/15/11 3.1 8.4 NA1SW8260B NA 406328ug/KgNDMethylene Chloride 08/15/11 1.7 42 NA1SW8260B NA 406328ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.93 8.4 NA1SW8260B NA 406328ug/KgNDMTBE 08/15/11 2.2 8.4 NA1SW8260B NA 406328ug/KgNDtert-Butanol 08/15/11 17 42 NA1SW8260B NA 406328ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.8 8.4 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethane 08/15/11 1.1 8.4 NA1SW8260B NA 406328ug/KgNDETBE 08/15/11 2.0 8.4 NA1SW8260B NA 406328ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.5 8.4 NA1SW8260B NA 406328ug/KgND2,2-Dichloropropane 08/15/11 1.0 8.4 NA1SW8260B NA 406328ug/KgNDBromochloromethane 08/15/11 1.9 8.4 NA1SW8260B NA 406328ug/KgNDChloroform 08/15/11 1.0 8.4 NA1SW8260B NA 406328ug/KgNDCarbon Tetrachloride 08/15/11 1.4 8.4 NA1SW8260B NA 406328ug/KgND1,1,1-Trichloroethane 08/15/11 1.0 8.4 NA1SW8260B NA 406328ug/KgND1,1-Dichloropropene 08/15/11 1.2 8.4 NA1SW8260B NA 406328ug/KgNDBenzene 08/15/11 1.3 8.4 NA1SW8260B NA 406328ug/KgNDTAME 08/15/11 1.7 8.4 NA1SW8260B NA 406328ug/KgND1,2-Dichloroethane 08/15/11 1.6 8.4 NA1SW8260B NA 406328ug/KgNDTrichloroethylene 08/15/11 3.3 8.4 NA1SW8260B NA 406328ug/KgNDDibromomethane 08/15/11 1.8 8.4 NA1SW8260B NA 406328ug/KgND1,2-Dichloropropane 08/15/11 1.1 8.4 NA1SW8260B NA 406328ug/KgNDBromodichloromethane 08/15/11 0.94 8.4 NA1SW8260B NA 406328ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.2 8.4 NA1SW8260B NA 406328ug/KgNDToluene 08/15/11 0.82 8.4 NA1SW8260B NA 406328ug/KgNDTetrachloroethylene 08/15/11 1.5 8.4 NA1SW8260B NA 406328ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.97 8.4 NA1SW8260B NA 406328ug/KgND1,1,2-Trichloroethane 08/15/11 1.5 8.4 NA1SW8260B NA 406328ug/KgNDDibromochloromethane 08/15/11 0.94 8.4 NA1SW8260B NA 406328ug/KgND1,3-Dichloropropane 08/15/11 1.7 8.4 NA1SW8260B NA 406328ug/KgND1,2-Dibromoethane 08/15/11 1.5 8.4 NA1
Page 38 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:151204.22500 KirkhamB-3-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.72 8.4 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 3.5 8.4 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.72 8.4 NA1SW8260B NA 406328ug/KgNDm,p-Xylene 08/15/11 1.6 8.4 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.56 4.2 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.64 8.4 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.6 8.4 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 1.0 8.4 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.2 8.4 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 1.0 8.4 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.5 8.4 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.95 8.4 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 2.8 8.4 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.3 8.4 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.3 8.4 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.2 8.4 NA1SW8260B NA 406328ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.91 8.4 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.4 8.4 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.2 8.4 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.5 8.4 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.3 8.4 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 1.8 8.4 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 1.1 8.4 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.6 8.4 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 2.1 8.4 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.8 8.4 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.4 8.4 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.4 8.4 NA1SW8260B NA 406328%86.1(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%92.0(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%80.6(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 39 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:151204.22500 KirkhamB-3-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 200 198 337420SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 33.3 100 337420SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 37.2 100 337420SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 39.0 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 20.7 100 337420SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 39.0 100 337420SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 22.2 100 337420SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 20.1 2000 337420SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 31.5 100 337420SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 21.6 100 337420SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 35.1 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 20.7 100 337420SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 42.0 100 337420SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 28.2 100 337420SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 14.1 100 337420SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 16.0 100 337420SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 17.4 198 337420SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 15.9 198 337420SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 40.2 2000 337420SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 1700 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 17.7 100 337420SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 31.5 100 337420SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 22.2 100 337420SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 31.5 100 337420SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 27.3 100 337420SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 30.0 100 337420SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 19.8 100 337420SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 30.9 100 337420SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 24.0 100 337420SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 24.0 100 337420SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 8.40 100 337420SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 28.8 100 337420SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 36.6 100 337420SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 18.0 990 337420SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 21.0 100 337420
Page 40 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:151204.22500 KirkhamB-3-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 35.7 100 337420SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 32.0 100 337420SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 25.8 100 337420SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 8.10 100 337420SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 26.0 100 337420SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 21.0 100 337420SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 29.1 100 337420SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 9.00 990 337420SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 20.1 100 337420SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 23.7 100 337420SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 8.10 100 337420SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 36.0 100 337420SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 36.0 100 337420SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 35.4 100 337420SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 30.0 100 337420SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 24.3 100 337420SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 24.3 100 337420SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 20.1 100 337420SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 20.1 100 337420SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 33.0 100 337420SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 24.6 990 337420SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 30.6 100 337420SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 30.9 990 337420SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 42.9 100 337420SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 40.1 100 337420SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 40.1 100 337420SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 32.7 510 337420SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 40.1 198 337420SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 113 990 337420SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 44.5 100 337420SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 27.0 100 337420SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 45.3 100 337420SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 46.2 100 337420SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 53.4 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 25.2 100 337420
Page 41 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:151204.22500 KirkhamB-3-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 41.7 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 40.2 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 51.3 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 40.8 100 337420SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 39.6 100 337420SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 45.9 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 45.6 100 337420SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 45.6 100 337420SW8270C 8/14/11 406315S,D %0.0002,4,6-Tribromophenol (S) 08/15/11 19 122 337420SW8270C 8/14/11 406315S,D %0.0002-Fluorobiphenyl (S) 08/15/11 30 115 337420SW8270C 8/14/11 406315S,D %0.0002-Fluorophenol (S) 08/15/11 25 121 337420SW8270C 8/14/11 406315S,D %0.000Nitrobenzene-d5 (S) 08/15/11 23 120 337420SW8270C 8/14/11 406315S,D %0.000Phenol-d6 (S) 08/15/11 24 113 337420SW8270C 8/14/11 406315S,D %0.000p-Terphenyl-d14 (S) 08/15/11 18 137 337420
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/15/11 406328ug/KgNDTPH(Gasoline) 08/15/11 14 84 342518260TPH 8/15/11 406328%48.0(S) 4-Bromofluorobenzene 08/15/11 43.9 127 34251
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 3.83 10 33981SW8015B(M) 8/16/11 406319mg/Kg130TPH as Motor Oil 08/17/11 8.33 20 33981SW8015B(M) 8/16/11 406319mg/Kg76.8Pentacosane (S) 08/17/11 59.7 129 33981
Page 42 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:201204.22500 KirkhamB-3-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/KgNDArsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg69Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg23Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDCobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/KgNDCopper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg3.0Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg14Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg18Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg16Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%91.4TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%93.9DCBP (S) 08/17/11 55.1 113 34001
Page 43 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:201204.22500 KirkhamB-3-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDDichlorodifluoromethane 08/15/11 3.8 8.7 NA1SW8260B NA 406328ug/KgNDChloromethane 08/15/11 4.0 8.7 NA1SW8260B NA 406328ug/KgNDVinyl Chloride 08/15/11 2.3 8.7 NA1SW8260B NA 406328ug/KgNDBromomethane 08/15/11 4.1 8.7 NA1SW8260B NA 406328ug/KgNDTrichlorofluoromethane 08/15/11 2.5 8.7 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethene 08/15/11 1.3 8.7 NA1SW8260B NA 406328ug/KgNDFreon 113 08/15/11 3.2 8.7 NA1SW8260B NA 406328ug/KgNDMethylene Chloride 08/15/11 1.7 44 NA1SW8260B NA 406328ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.97 8.7 NA1SW8260B NA 406328ug/KgNDMTBE 08/15/11 2.2 8.7 NA1SW8260B NA 406328ug/KgNDtert-Butanol 08/15/11 18 44 NA1SW8260B NA 406328ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.9 8.7 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethane 08/15/11 1.1 8.7 NA1SW8260B NA 406328ug/KgNDETBE 08/15/11 2.1 8.7 NA1SW8260B NA 406328ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.5 8.7 NA1SW8260B NA 406328ug/KgND2,2-Dichloropropane 08/15/11 1.1 8.7 NA1SW8260B NA 406328ug/KgNDBromochloromethane 08/15/11 2.0 8.7 NA1SW8260B NA 406328ug/KgNDChloroform 08/15/11 1.1 8.7 NA1SW8260B NA 406328ug/KgNDCarbon Tetrachloride 08/15/11 1.4 8.7 NA1SW8260B NA 406328ug/KgND1,1,1-Trichloroethane 08/15/11 1.1 8.7 NA1SW8260B NA 406328ug/KgND1,1-Dichloropropene 08/15/11 1.3 8.7 NA1SW8260B NA 406328ug/KgNDBenzene 08/15/11 1.3 8.7 NA1SW8260B NA 406328ug/KgNDTAME 08/15/11 1.8 8.7 NA1SW8260B NA 406328ug/KgND1,2-Dichloroethane 08/15/11 1.7 8.7 NA1SW8260B NA 406328ug/KgNDTrichloroethylene 08/15/11 3.4 8.7 NA1SW8260B NA 406328ug/KgNDDibromomethane 08/15/11 1.9 8.7 NA1SW8260B NA 406328ug/KgND1,2-Dichloropropane 08/15/11 1.1 8.7 NA1SW8260B NA 406328ug/KgNDBromodichloromethane 08/15/11 0.97 8.7 NA1SW8260B NA 406328ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.2 8.7 NA1SW8260B NA 406328ug/KgNDToluene 08/15/11 0.85 8.7 NA1SW8260B NA 406328ug/KgNDTetrachloroethylene 08/15/11 1.6 8.7 NA1SW8260B NA 406328ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.0 8.7 NA1SW8260B NA 406328ug/KgND1,1,2-Trichloroethane 08/15/11 1.6 8.7 NA1SW8260B NA 406328ug/KgNDDibromochloromethane 08/15/11 0.98 8.7 NA1SW8260B NA 406328ug/KgND1,3-Dichloropropane 08/15/11 1.8 8.7 NA1SW8260B NA 406328ug/KgND1,2-Dibromoethane 08/15/11 1.5 8.7 NA1
Page 44 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:201204.22500 KirkhamB-3-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.75 8.7 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 3.7 8.7 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.75 8.7 NA1SW8260B NA 406328ug/KgNDm,p-Xylene 08/15/11 1.6 8.7 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.58 4.4 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.67 8.7 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.7 8.7 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 1.1 8.7 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.2 8.7 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 1.0 8.7 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.6 8.7 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.98 8.7 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 2.9 8.7 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.4 8.7 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.4 8.7 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.2 8.7 NA1SW8260B NA 406328ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.94 8.7 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.4 8.7 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.3 8.7 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.6 8.7 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.3 8.7 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 1.9 8.7 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 1.1 8.7 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.7 8.7 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 2.2 8.7 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.9 8.7 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.5 8.7 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.5 8.7 NA1SW8260B NA 406328%76.9(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%94.4(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%80.1(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 45 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:201204.22500 KirkhamB-3-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 0.660 0.653 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 0.110 0.330 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 0.123 0.330 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 0.0663 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 0.0713 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 0.116 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 0.139 0.330 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 0.0931 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.0465 0.330 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.0528 0.330 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.0574 0.653 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.0525 0.653 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 0.133 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 5.59 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.0584 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 0.0901 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.0653 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 0.102 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.0277 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 0.0950 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 0.121 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.0594 3.27 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 0.118 0.330 33741
Page 46 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:201204.22500 KirkhamB-3-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 0.106 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 0.0851 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 0.0858 0.330 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 0.0960 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.0297 3.27 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 0.0782 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 0.117 0.330 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 0.109 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 0.0812 3.27 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 0.101 0.330 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 0.102 3.27 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 0.142 0.330 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 0.108 1.68 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 0.132 0.653 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 0.374 3.27 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 0.147 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 0.0891 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 0.149 0.330 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 0.152 0.330 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 0.176 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 0.0832 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 0.138 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 0.133 0.330 33741
Page 47 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:201204.22500 KirkhamB-3-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 0.169 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 0.135 0.330 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 0.131 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 0.151 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315%58.22,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%73.72-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%72.72-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%71.7Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%84.0Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315%61.9p-Terphenyl-d14 (S) 08/15/11 18 137 33741
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/15/11 406328x ug/Kg110TPH(Gasoline) 08/15/11 15 87 342518260TPH 8/15/11 406328%125(S) 4-Bromofluorobenzene 08/15/11 43.9 127 34251
x - Does not match pattern of reference Gasoline standard. Hydrocarbons in the range of C5-C12 quantified as Gasoline.NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319x mg/Kg2.0TPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/Kg6.8TPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg121Pentacosane (S) 08/17/11 59.7 129 33981
x-Not typical of Diesel standard pattern (unknown hydrocarbons present).NOTE:
Page 48 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:501204.22500 KirkhamB-10-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg1.7Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg42Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg23Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDCobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/KgNDCopper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg3.5Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg14Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg17Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg13Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921
Page 49 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:501204.22500 KirkhamB-10-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 4.4 20 340110SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 4.0 20 340110SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 3.6 20 340110SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 4.9 20 340110SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 11 20 340110SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 4.4 20 340110SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 3.2 20 340110SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 4.2 20 340110SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 3.6 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 5.9 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 4.8 20 340110SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 4.3 20 340110SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 5.7 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 4.7 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 15 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 8.1 20 340110SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 10 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 4.9 20 340110SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 6.2 50 340110SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 4.0 20 340110SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 100 200 340110SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 100 100 340110SW8081A 8/16/11 406314%107TCMX (S) 08/16/11 52.5 139 340110SW8081A 8/16/11 406314%109DCBP (S) 08/16/11 50.2 139 340110
Reporting limits increased due to the nature of the sample matrix (dark color extract). Toxaphene reported to the MDL.NOTE:
Page 50 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:501204.22500 KirkhamB-10-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%90.7TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%104DCBP (S) 08/17/11 55.1 113 34001
Page 51 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:501204.22500 KirkhamB-10-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDDichlorodifluoromethane 08/15/11 3.8 8.7 NA1SW8260B NA 406328ug/KgNDChloromethane 08/15/11 4.0 8.7 NA1SW8260B NA 406328ug/KgNDVinyl Chloride 08/15/11 2.3 8.7 NA1SW8260B NA 406328ug/KgNDBromomethane 08/15/11 4.1 8.7 NA1SW8260B NA 406328ug/KgNDTrichlorofluoromethane 08/15/11 2.5 8.7 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethene 08/15/11 1.3 8.7 NA1SW8260B NA 406328ug/KgNDFreon 113 08/15/11 3.2 8.7 NA1SW8260B NA 406328ug/KgNDMethylene Chloride 08/15/11 1.7 44 NA1SW8260B NA 406328ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.97 8.7 NA1SW8260B NA 406328ug/KgNDMTBE 08/15/11 2.2 8.7 NA1SW8260B NA 406328ug/KgNDtert-Butanol 08/15/11 18 44 NA1SW8260B NA 406328ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.9 8.7 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethane 08/15/11 1.1 8.7 NA1SW8260B NA 406328ug/KgNDETBE 08/15/11 2.1 8.7 NA1SW8260B NA 406328ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.5 8.7 NA1SW8260B NA 406328ug/KgND2,2-Dichloropropane 08/15/11 1.1 8.7 NA1SW8260B NA 406328ug/KgNDBromochloromethane 08/15/11 2.0 8.7 NA1SW8260B NA 406328ug/KgNDChloroform 08/15/11 1.1 8.7 NA1SW8260B NA 406328ug/KgNDCarbon Tetrachloride 08/15/11 1.4 8.7 NA1SW8260B NA 406328ug/KgND1,1,1-Trichloroethane 08/15/11 1.1 8.7 NA1SW8260B NA 406328ug/KgND1,1-Dichloropropene 08/15/11 1.3 8.7 NA1SW8260B NA 406328ug/KgNDBenzene 08/15/11 1.3 8.7 NA1SW8260B NA 406328ug/KgNDTAME 08/15/11 1.8 8.7 NA1SW8260B NA 406328ug/KgND1,2-Dichloroethane 08/15/11 1.7 8.7 NA1SW8260B NA 406328ug/KgNDTrichloroethylene 08/15/11 3.4 8.7 NA1SW8260B NA 406328ug/KgNDDibromomethane 08/15/11 1.9 8.7 NA1SW8260B NA 406328ug/KgND1,2-Dichloropropane 08/15/11 1.1 8.7 NA1SW8260B NA 406328ug/KgNDBromodichloromethane 08/15/11 0.97 8.7 NA1SW8260B NA 406328ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.2 8.7 NA1SW8260B NA 406328ug/KgNDToluene 08/15/11 0.85 8.7 NA1SW8260B NA 406328ug/KgNDTetrachloroethylene 08/15/11 1.6 8.7 NA1SW8260B NA 406328ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.0 8.7 NA1SW8260B NA 406328ug/KgND1,1,2-Trichloroethane 08/15/11 1.6 8.7 NA1SW8260B NA 406328ug/KgNDDibromochloromethane 08/15/11 0.98 8.7 NA1SW8260B NA 406328ug/KgND1,3-Dichloropropane 08/15/11 1.8 8.7 NA1SW8260B NA 406328ug/KgND1,2-Dibromoethane 08/15/11 1.5 8.7 NA1
Page 52 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:501204.22500 KirkhamB-10-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.75 8.7 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 3.7 8.7 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.75 8.7 NA1SW8260B NA 406328ug/KgNDm,p-Xylene 08/15/11 1.6 8.7 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.58 4.4 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.67 8.7 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.7 8.7 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 1.1 8.7 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.2 8.7 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 1.0 8.7 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.6 8.7 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.98 8.7 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 2.9 8.7 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.4 8.7 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.4 8.7 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.2 8.7 NA1SW8260B NA 406328ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.94 8.7 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.4 8.7 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.3 8.7 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.6 8.7 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.3 8.7 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 1.9 8.7 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 1.1 8.7 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.7 8.7 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 2.2 8.7 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.9 8.7 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.5 8.7 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.5 8.7 NA1SW8260B NA 406328%78.9(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%89.8(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%90.0(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 53 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:501204.22500 KirkhamB-10-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 10.0 9.90 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 1.67 5.00 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 1.86 5.00 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 1.95 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 1.04 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 1.95 5.00 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 1.11 5.00 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 1.01 99.9 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 1.58 5.00 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 1.08 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 1.76 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 1.04 5.00 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 2.10 5.00 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 1.41 5.00 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.705 5.00 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.800 5.00 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.870 9.90 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.795 9.90 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 2.01 99.9 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 84.8 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.885 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 1.58 5.00 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 1.11 5.00 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 1.58 5.00 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 1.37 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 1.50 5.00 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.990 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 1.55 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 1.20 5.00 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 1.20 5.00 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.420 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 1.44 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 1.83 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.900 49.5 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 1.05 5.00 33741
Page 54 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:501204.22500 KirkhamB-10-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 1.79 5.00 33741SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 1.60 5.00 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 1.29 5.00 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.405 5.00 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 1.30 5.00 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 1.05 5.00 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 1.46 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.450 49.5 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 1.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 1.19 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.405 5.00 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 1.80 5.00 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 1.80 5.00 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 1.77 5.00 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 1.50 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 1.22 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 1.22 5.00 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 1.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 1.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 1.65 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 1.23 49.5 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 1.53 5.00 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 1.55 49.5 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 2.15 5.00 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 2.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 2.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 1.64 25.5 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 2.01 9.90 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 5.67 49.5 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 2.23 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 1.35 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 2.27 5.00 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 2.31 5.00 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 2.67 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 1.26 5.00 33741
Page 55 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:501204.22500 KirkhamB-10-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 2.09 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 2.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 2.57 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 2.04 5.00 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 1.98 5.00 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 2.30 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 2.28 5.00 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 2.28 5.00 33741SW8270C 8/14/11 406315S %1062,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%1062-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%82.82-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%93.4Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%82.1Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315S,D %0.000p-Terphenyl-d14 (S) 08/15/11 18 137 33741
D - Surrogates not recoverable due to prep of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/15/11 406328ug/KgNDTPH(Gasoline) 08/15/11 15 87 342518260TPH 8/15/11 406328%80.5(S) 4-Bromofluorobenzene 08/15/11 43.9 127 34251
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 1.53 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg88TPH as Motor Oil 08/17/11 3.33 8.0 33981SW8015B(M) 8/16/11 406319mg/Kg84.5Pentacosane (S) 08/17/11 59.7 129 33981
Page 56 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:551204.22500 KirkhamB-10-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-008A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg2.1Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg47Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg37Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg6.7Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg5.9Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg3.1Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg31Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg29Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg20Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%95.6TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%104DCBP (S) 08/17/11 55.1 113 34001
Page 57 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:551204.22500 KirkhamB-10-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-008A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDDichlorodifluoromethane 08/15/11 3.5 8.1 NA1SW8260B NA 406328ug/KgNDChloromethane 08/15/11 3.7 8.1 NA1SW8260B NA 406328ug/KgNDVinyl Chloride 08/15/11 2.1 8.1 NA1SW8260B NA 406328ug/KgNDBromomethane 08/15/11 3.8 8.1 NA1SW8260B NA 406328ug/KgNDTrichlorofluoromethane 08/15/11 2.3 8.1 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethene 08/15/11 1.3 8.1 NA1SW8260B NA 406328ug/KgNDFreon 113 08/15/11 3.0 8.1 NA1SW8260B NA 406328ug/KgNDMethylene Chloride 08/15/11 1.6 41 NA1SW8260B NA 406328ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.90 8.1 NA1SW8260B NA 406328ug/KgNDMTBE 08/15/11 2.1 8.1 NA1SW8260B NA 406328ug/KgNDtert-Butanol 08/15/11 17 41 NA1SW8260B NA 406328ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.8 8.1 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethane 08/15/11 1.0 8.1 NA1SW8260B NA 406328ug/KgNDETBE 08/15/11 2.0 8.1 NA1SW8260B NA 406328ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.4 8.1 NA1SW8260B NA 406328ug/KgND2,2-Dichloropropane 08/15/11 1.0 8.1 NA1SW8260B NA 406328ug/KgNDBromochloromethane 08/15/11 1.9 8.1 NA1SW8260B NA 406328ug/KgNDChloroform 08/15/11 0.99 8.1 NA1SW8260B NA 406328ug/KgNDCarbon Tetrachloride 08/15/11 1.3 8.1 NA1SW8260B NA 406328ug/KgND1,1,1-Trichloroethane 08/15/11 0.98 8.1 NA1SW8260B NA 406328ug/KgND1,1-Dichloropropene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgNDBenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgNDTAME 08/15/11 1.7 8.1 NA1SW8260B NA 406328ug/KgND1,2-Dichloroethane 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgNDTrichloroethylene 08/15/11 3.1 8.1 NA1SW8260B NA 406328ug/KgNDDibromomethane 08/15/11 1.8 8.1 NA1SW8260B NA 406328ug/KgND1,2-Dichloropropane 08/15/11 1.1 8.1 NA1SW8260B NA 406328ug/KgNDBromodichloromethane 08/15/11 0.90 8.1 NA1SW8260B NA 406328ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.1 8.1 NA1SW8260B NA 406328ug/KgNDToluene 08/15/11 0.80 8.1 NA1SW8260B NA 406328ug/KgNDTetrachloroethylene 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.93 8.1 NA1SW8260B NA 406328ug/KgND1,1,2-Trichloroethane 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgNDDibromochloromethane 08/15/11 0.91 8.1 NA1SW8260B NA 406328ug/KgND1,3-Dichloropropane 08/15/11 1.7 8.1 NA1SW8260B NA 406328ug/KgND1,2-Dibromoethane 08/15/11 1.4 8.1 NA1
Page 58 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:551204.22500 KirkhamB-10-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-008A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.70 8.1 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 3.4 8.1 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.69 8.1 NA1SW8260B NA 406328ug/KgNDm,p-Xylene 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.54 4.1 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.62 8.1 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 1.0 8.1 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 0.96 8.1 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.4 8.1 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.91 8.1 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 2.7 8.1 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.3 8.1 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.3 8.1 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.88 8.1 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.3 8.1 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 1.8 8.1 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 1.1 8.1 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.4 8.1 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 2.1 8.1 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.7 8.1 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.3 8.1 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.3 8.1 NA1SW8260B NA 406328%97.6(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%81.1(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%98.5(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 59 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:551204.22500 KirkhamB-10-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-008A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 0.660 0.653 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 0.110 0.330 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 0.123 0.330 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 0.0663 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 0.0713 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 0.116 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 0.139 0.330 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 0.0931 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.0465 0.330 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.0528 0.330 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.0574 0.653 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.0525 0.653 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 0.133 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 5.59 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.0584 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 0.0901 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.0653 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 0.102 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.0277 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 0.0950 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 0.121 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.0594 3.27 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 0.118 0.330 33741
Page 60 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:551204.22500 KirkhamB-10-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-008A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 0.106 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 0.0851 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 0.0858 0.330 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 0.0960 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.0297 3.27 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 0.0782 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 0.117 0.330 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 0.109 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 0.0812 3.27 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 0.101 0.330 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 0.102 3.27 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 0.142 0.330 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 0.108 1.68 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 0.132 0.653 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 0.374 3.27 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 0.147 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 0.0891 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 0.149 0.330 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 0.152 0.330 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 0.176 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 0.0832 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 0.138 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 0.133 0.330 33741
Page 61 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:551204.22500 KirkhamB-10-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-008A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 0.169 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 0.135 0.330 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 0.131 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 0.151 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315%47.82,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%58.02-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%60.82-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%57.9Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%67.1Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315%56.8p-Terphenyl-d14 (S) 08/15/11 18 137 33741
D - Surrogates not recoverable due to prep of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/15/11 406330ug/KgNDTPH(Gasoline) 08/18/11 14 80 342518260TPH 8/15/11 406330%80.3(S) 4-Bromofluorobenzene 08/18/11 43.9 127 34251
Final results and PQL (Reporting Limit) have been corrected for actual mass from pre-tarred 5035 VOAs.NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/Kg6.3TPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg123Pentacosane (S) 08/17/11 59.7 129 33981
Page 62 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:401204.22500 KirkhamB-12-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg1.7Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg42Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg24Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDCobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/KgNDCopper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg2.0Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg15Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg17Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg12Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921
Page 63 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:401204.22500 KirkhamB-12-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 1.8 8.0 34014SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 1.6 8.0 34014SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 1.5 8.0 34014SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 2.0 8.0 34014SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 4.4 8.0 34014SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 1.8 8.0 34014SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 1.3 8.0 34014SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 1.7 8.0 34014SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 1.4 8.0 34014SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 2.4 8.0 34014SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 1.9 8.0 34014SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 1.7 8.0 34014SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 2.3 8.0 34014SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 1.9 8.0 34014SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 6.1 8.0 34014SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 3.2 8.0 34014SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 4.1 8.0 34014SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 2.0 8.0 34014SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 2.5 20 34014SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 1.6 8.0 34014SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 40 80 34014SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 40 400 34014SW8081A 8/16/11 406314%107TCMX (S) 08/16/11 52.5 139 34014SW8081A 8/16/11 406314%105DCBP (S) 08/16/11 50.2 139 34014
Reporting limits increased due to the nature of the sample matrix (dark color extract).NOTE:
Page 64 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:401204.22500 KirkhamB-12-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%94.3TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%107DCBP (S) 08/17/11 55.1 113 34001
Page 65 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:401204.22500 KirkhamB-12-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDDichlorodifluoromethane 08/15/11 4.0 9.1 NA1SW8260B NA 406328ug/KgNDChloromethane 08/15/11 4.2 9.1 NA1SW8260B NA 406328ug/KgNDVinyl Chloride 08/15/11 2.4 9.1 NA1SW8260B NA 406328ug/KgNDBromomethane 08/15/11 4.2 9.1 NA1SW8260B NA 406328ug/KgNDTrichlorofluoromethane 08/15/11 2.6 9.1 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethene 08/15/11 1.4 9.1 NA1SW8260B NA 406328ug/KgNDFreon 113 08/15/11 3.4 9.1 NA1SW8260B NA 406328ug/KgNDMethylene Chloride 08/15/11 1.8 46 NA1SW8260B NA 406328ug/KgNDtrans-1,2-Dichloroethene 08/15/11 1.0 9.1 NA1SW8260B NA 406328ug/KgNDMTBE 08/15/11 2.4 9.1 NA1SW8260B NA 406328ug/KgNDtert-Butanol 08/15/11 19 46 NA1SW8260B NA 406328ug/KgNDDiisopropyl ether (DIPE) 08/15/11 2.0 9.1 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethane 08/15/11 1.2 9.1 NA1SW8260B NA 406328ug/KgNDETBE 08/15/11 2.2 9.1 NA1SW8260B NA 406328ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.6 9.1 NA1SW8260B NA 406328ug/KgND2,2-Dichloropropane 08/15/11 1.1 9.1 NA1SW8260B NA 406328ug/KgNDBromochloromethane 08/15/11 2.1 9.1 NA1SW8260B NA 406328ug/KgNDChloroform 08/15/11 1.1 9.1 NA1SW8260B NA 406328ug/KgNDCarbon Tetrachloride 08/15/11 1.5 9.1 NA1SW8260B NA 406328ug/KgND1,1,1-Trichloroethane 08/15/11 1.1 9.1 NA1SW8260B NA 406328ug/KgND1,1-Dichloropropene 08/15/11 1.3 9.1 NA1SW8260B NA 406328ug/KgNDBenzene 08/15/11 1.4 9.1 NA1SW8260B NA 406328ug/KgNDTAME 08/15/11 1.9 9.1 NA1SW8260B NA 406328ug/KgND1,2-Dichloroethane 08/15/11 1.7 9.1 NA1SW8260B NA 406328ug/KgNDTrichloroethylene 08/15/11 3.5 9.1 NA1SW8260B NA 406328ug/KgNDDibromomethane 08/15/11 2.0 9.1 NA1SW8260B NA 406328ug/KgND1,2-Dichloropropane 08/15/11 1.2 9.1 NA1SW8260B NA 406328ug/KgNDBromodichloromethane 08/15/11 1.0 9.1 NA1SW8260B NA 406328ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.3 9.1 NA1SW8260B NA 406328ug/KgNDToluene 08/15/11 0.89 9.1 NA1SW8260B NA 406328ug/KgNDTetrachloroethylene 08/15/11 1.6 9.1 NA1SW8260B NA 406328ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.1 9.1 NA1SW8260B NA 406328ug/KgND1,1,2-Trichloroethane 08/15/11 1.7 9.1 NA1SW8260B NA 406328ug/KgNDDibromochloromethane 08/15/11 1.0 9.1 NA1SW8260B NA 406328ug/KgND1,3-Dichloropropane 08/15/11 1.9 9.1 NA1SW8260B NA 406328ug/KgND1,2-Dibromoethane 08/15/11 1.6 9.1 NA1
Page 66 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:401204.22500 KirkhamB-12-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.78 9.1 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 3.8 9.1 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.78 9.1 NA1SW8260B NA 406328ug/KgNDm,p-Xylene 08/15/11 1.7 9.1 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.60 4.6 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.70 9.1 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.7 9.1 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 1.1 9.1 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.3 9.1 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 1.1 9.1 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.7 9.1 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.0 9.1 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 3.0 9.1 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.4 9.1 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.4 9.1 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.3 9.1 NA1SW8260B NA 406328ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.99 9.1 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.5 9.1 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.3 9.1 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.6 9.1 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.4 9.1 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 2.0 9.1 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 1.2 9.1 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.9 9.1 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 2.3 9.1 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.9 9.1 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.6 9.1 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.6 9.1 NA1SW8260B NA 406328%78.2(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%89.9(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%92.0(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 67 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:401204.22500 KirkhamB-12-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 10.0 9.90 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 1.67 5.00 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 1.86 5.00 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 1.95 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 1.04 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 1.95 5.00 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 1.11 5.00 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 1.01 99.9 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 1.58 5.00 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 1.08 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 1.76 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 1.04 5.00 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 2.10 5.00 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 1.41 5.00 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.705 5.00 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.800 5.00 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.870 9.90 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.795 9.90 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 2.01 99.9 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 84.8 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.885 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 1.58 5.00 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 1.11 5.00 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 1.58 5.00 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 1.37 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 1.50 5.00 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.990 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 1.55 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 1.20 5.00 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 1.20 5.00 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.420 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 1.44 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 1.83 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.900 49.5 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 1.05 5.00 33741
Page 68 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:401204.22500 KirkhamB-12-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 1.79 5.00 33741SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 1.60 5.00 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 1.29 5.00 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.405 5.00 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 1.30 5.00 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 1.05 5.00 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 1.46 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.450 49.5 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 1.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 1.19 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.405 5.00 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 1.80 5.00 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 1.80 5.00 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 1.77 5.00 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 1.50 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 1.22 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 1.22 5.00 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 1.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 1.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 1.65 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 1.23 49.5 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 1.53 5.00 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 1.55 49.5 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 2.15 5.00 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 2.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 2.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 1.64 25.5 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 2.01 9.90 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 5.67 49.5 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 2.23 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 1.35 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 2.27 5.00 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 2.31 5.00 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 2.67 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 1.26 5.00 33741
Page 69 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:401204.22500 KirkhamB-12-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 2.09 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 2.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 2.57 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 2.04 5.00 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 1.98 5.00 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 2.30 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 2.28 5.00 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 2.28 5.00 33741SW8270C 8/14/11 406315%1002,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%1022-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%79.92-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%89.1Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%75.3Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315S,D %-29.9p-Terphenyl-d14 (S) 08/15/11 18 137 33741
D - Surrogates not recoverable due to prep of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/15/11 406328ug/KgNDTPH(Gasoline) 08/15/11 15 91 342518260TPH 8/15/11 406328%83.3(S) 4-Bromofluorobenzene 08/15/11 43.9 127 34251
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/Kg29TPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg86.6Pentacosane (S) 08/17/11 59.7 129 33981
Page 70 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:501204.22500 KirkhamB-12-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-011A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg2.5Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg46Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg44Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg11Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg6.1Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg3.2Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg33Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg29Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg20Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%77.1TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%87.6DCBP (S) 08/17/11 55.1 113 34001
Page 71 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:501204.22500 KirkhamB-12-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-011A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDDichlorodifluoromethane 08/15/11 3.1 7.2 NA1SW8260B NA 406328ug/KgNDChloromethane 08/15/11 3.3 7.2 NA1SW8260B NA 406328ug/KgNDVinyl Chloride 08/15/11 1.9 7.2 NA1SW8260B NA 406328ug/KgNDBromomethane 08/15/11 3.4 7.2 NA1SW8260B NA 406328ug/KgNDTrichlorofluoromethane 08/15/11 2.1 7.2 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethene 08/15/11 1.1 7.2 NA1SW8260B NA 406328ug/KgNDFreon 113 08/15/11 2.7 7.2 NA1SW8260B NA 406328ug/KgNDMethylene Chloride 08/15/11 1.4 36 NA1SW8260B NA 406328ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.80 7.2 NA1SW8260B NA 406328ug/KgNDMTBE 08/15/11 1.9 7.2 NA1SW8260B NA 406328ug/KgNDtert-Butanol 08/15/11 15 36 NA1SW8260B NA 406328ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.6 7.2 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethane 08/15/11 0.92 7.2 NA1SW8260B NA 406328ug/KgNDETBE 08/15/11 1.7 7.2 NA1SW8260B NA 406328ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.3 7.2 NA1SW8260B NA 406328ug/KgND2,2-Dichloropropane 08/15/11 0.89 7.2 NA1SW8260B NA 406328ug/KgNDBromochloromethane 08/15/11 1.6 7.2 NA1SW8260B NA 406328ug/KgNDChloroform 08/15/11 0.88 7.2 NA1SW8260B NA 406328ug/KgNDCarbon Tetrachloride 08/15/11 1.2 7.2 NA1SW8260B NA 406328ug/KgND1,1,1-Trichloroethane 08/15/11 0.88 7.2 NA1SW8260B NA 406328ug/KgND1,1-Dichloropropene 08/15/11 1.0 7.2 NA1SW8260B NA 406328ug/KgNDBenzene 08/15/11 1.1 7.2 NA1SW8260B NA 406328ug/KgNDTAME 08/15/11 1.5 7.2 NA1SW8260B NA 406328ug/KgND1,2-Dichloroethane 08/15/11 1.4 7.2 NA1SW8260B NA 406328ug/KgNDTrichloroethylene 08/15/11 2.8 7.2 NA1SW8260B NA 406328ug/KgNDDibromomethane 08/15/11 1.6 7.2 NA1SW8260B NA 406328ug/KgND1,2-Dichloropropane 08/15/11 0.94 7.2 NA1SW8260B NA 406328ug/KgNDBromodichloromethane 08/15/11 0.80 7.2 NA1SW8260B NA 406328ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.0 7.2 NA1SW8260B NA 406328ug/KgNDToluene 08/15/11 0.71 7.2 NA1SW8260B NA 406328ug/KgNDTetrachloroethylene 08/15/11 1.3 7.2 NA1SW8260B NA 406328ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.83 7.2 NA1SW8260B NA 406328ug/KgND1,1,2-Trichloroethane 08/15/11 1.3 7.2 NA1SW8260B NA 406328ug/KgNDDibromochloromethane 08/15/11 0.81 7.2 NA1SW8260B NA 406328ug/KgND1,3-Dichloropropane 08/15/11 1.5 7.2 NA1SW8260B NA 406328ug/KgND1,2-Dibromoethane 08/15/11 1.3 7.2 NA1
Page 72 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:501204.22500 KirkhamB-12-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-011A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.62 7.2 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 3.0 7.2 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.62 7.2 NA1SW8260B NA 406328ug/KgNDm,p-Xylene 08/15/11 1.3 7.2 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.48 3.6 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.55 7.2 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.4 7.2 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 0.89 7.2 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.0 7.2 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 0.86 7.2 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.2 7.2 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.81 7.2 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 2.4 7.2 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.1 7.2 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.1 7.2 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.0 7.2 NA1SW8260B NA 406328ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.78 7.2 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.2 7.2 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.1 7.2 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.3 7.2 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.1 7.2 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 1.6 7.2 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 0.94 7.2 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.0 7.2 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 1.8 7.2 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.5 7.2 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.0 7.2 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.1 7.2 NA1SW8260B NA 406328%95.6(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%81.6(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%96.7(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 73 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:501204.22500 KirkhamB-12-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-011A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 0.660 0.653 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 0.110 0.330 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 0.123 0.330 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 0.0663 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 0.0713 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 0.116 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 0.139 0.330 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 0.0931 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.0465 0.330 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.0528 0.330 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.0574 0.653 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.0525 0.653 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 0.133 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 5.59 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.0584 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 0.0901 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.0653 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 0.102 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.0277 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 0.0950 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 0.121 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.0594 3.27 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 0.118 0.330 33741
Page 74 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:501204.22500 KirkhamB-12-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-011A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 0.106 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 0.0851 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 0.0858 0.330 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 0.0960 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.0297 3.27 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 0.0782 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 0.117 0.330 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 0.109 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 0.0812 3.27 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 0.101 0.330 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 0.102 3.27 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 0.142 0.330 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 0.108 1.68 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 0.132 0.653 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 0.374 3.27 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 0.147 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 0.0891 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 0.149 0.330 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 0.152 0.330 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 0.176 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 0.0832 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 0.138 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 0.133 0.330 33741
Page 75 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:501204.22500 KirkhamB-12-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-011A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 0.169 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 0.135 0.330 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 0.131 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 0.151 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315%50.52,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%68.22-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%67.42-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%64.1Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%75.0Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315%64.4p-Terphenyl-d14 (S) 08/15/11 18 137 33741
D - Surrogates not recoverable due to prep of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/15/11 406330ug/KgNDTPH(Gasoline) 08/18/11 12 72 342518260TPH 8/15/11 406330%78.5(S) 4-Bromofluorobenzene 08/18/11 43.9 127 34251
Final results and PQL (Reporting Limit) have been corrected for actual mass from pre-tarred 5035 VOAs.NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319x mg/Kg2.2TPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/KgNDTPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg97.4Pentacosane (S) 08/17/11 59.7 129 33981
x-Not typical of Diesel standard pattern (unknown hydrocarbons present).NOTE:
Page 76 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:501204.22500 KirkhamB-11-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg16Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg430Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/Kg1.1Cadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg8.5Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg9.2Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg58Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg18Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg16Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg39Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg77Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/Kg0.38Mercury 08/16/11 0.01 0.10 33921
Page 77 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:501204.22500 KirkhamB-11-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 4.4 20 340110SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 4.0 20 340110SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 3.6 20 340110SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 4.9 20 340110SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 11 20 340110SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 4.4 20 340110SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 3.2 20 340110SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 4.2 20 340110SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 3.6 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 5.9 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 4.8 20 340110SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 4.3 20 340110SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 5.7 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 4.7 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 15 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 8.1 20 340110SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 10 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 4.9 20 340110SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 6.2 50 340110SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 4.0 20 340110SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 100 200 340110SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 100 100 340110SW8081A 8/16/11 406314%93.9TCMX (S) 08/16/11 52.5 139 340110SW8081A 8/16/11 406314%87.1DCBP (S) 08/16/11 50.2 139 340110
Reporting limits increased due to the nature of the sample matrix (dark color extract). Toxaphene reported to the MDL.NOTE:
Page 78 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:501204.22500 KirkhamB-11-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%74.4TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%84.6DCBP (S) 08/17/11 55.1 113 34001
Page 79 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:501204.22500 KirkhamB-11-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDDichlorodifluoromethane 08/15/11 3.6 8.2 NA1SW8260B NA 406328ug/KgNDChloromethane 08/15/11 3.8 8.2 NA1SW8260B NA 406328ug/KgNDVinyl Chloride 08/15/11 2.2 8.2 NA1SW8260B NA 406328ug/KgNDBromomethane 08/15/11 3.8 8.2 NA1SW8260B NA 406328ug/KgNDTrichlorofluoromethane 08/15/11 2.4 8.2 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethene 08/15/11 1.3 8.2 NA1SW8260B NA 406328ug/KgNDFreon 113 08/15/11 3.0 8.2 NA1SW8260B NA 406328ug/KgNDMethylene Chloride 08/15/11 1.6 41 NA1SW8260B NA 406328ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.91 8.2 NA1SW8260B NA 406328ug/KgNDMTBE 08/15/11 2.1 8.2 NA1SW8260B NA 406328ug/KgNDtert-Butanol 08/15/11 17 41 NA1SW8260B NA 406328ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.8 8.2 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethane 08/15/11 1.0 8.2 NA1SW8260B NA 406328ug/KgNDETBE 08/15/11 2.0 8.2 NA1SW8260B NA 406328ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.4 8.2 NA1SW8260B NA 406328ug/KgND2,2-Dichloropropane 08/15/11 1.0 8.2 NA1SW8260B NA 406328ug/KgNDBromochloromethane 08/15/11 1.9 8.2 NA1SW8260B NA 406328ug/KgNDChloroform 08/15/11 1.0 8.2 NA1SW8260B NA 406328ug/KgNDCarbon Tetrachloride 08/15/11 1.3 8.2 NA1SW8260B NA 406328ug/KgND1,1,1-Trichloroethane 08/15/11 1.0 8.2 NA1SW8260B NA 406328ug/KgND1,1-Dichloropropene 08/15/11 1.2 8.2 NA1SW8260B NA 406328ug/KgNDBenzene 08/15/11 1.2 8.2 NA1SW8260B NA 406328ug/KgNDTAME 08/15/11 1.7 8.2 NA1SW8260B NA 406328ug/KgND1,2-Dichloroethane 08/15/11 1.6 8.2 NA1SW8260B NA 406328ug/KgNDTrichloroethylene 08/15/11 3.2 8.2 NA1SW8260B NA 406328ug/KgNDDibromomethane 08/15/11 1.8 8.2 NA1SW8260B NA 406328ug/KgND1,2-Dichloropropane 08/15/11 1.1 8.2 NA1SW8260B NA 406328ug/KgNDBromodichloromethane 08/15/11 0.92 8.2 NA1SW8260B NA 406328ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.2 8.2 NA1SW8260B NA 406328ug/KgNDToluene 08/15/11 0.81 8.2 NA1SW8260B NA 406328ug/KgNDTetrachloroethylene 08/15/11 1.5 8.2 NA1SW8260B NA 406328ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.95 8.2 NA1SW8260B NA 406328ug/KgND1,1,2-Trichloroethane 08/15/11 1.5 8.2 NA1SW8260B NA 406328ug/KgNDDibromochloromethane 08/15/11 0.92 8.2 NA1SW8260B NA 406328ug/KgND1,3-Dichloropropane 08/15/11 1.7 8.2 NA1SW8260B NA 406328ug/KgND1,2-Dibromoethane 08/15/11 1.4 8.2 NA1
Page 80 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:501204.22500 KirkhamB-11-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.71 8.2 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 3.5 8.2 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.70 8.2 NA1SW8260B NA 406328ug/KgNDm,p-Xylene 08/15/11 1.5 8.2 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.54 4.1 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.63 8.2 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.6 8.2 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 1.0 8.2 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.2 8.2 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 0.97 8.2 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.5 8.2 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.92 8.2 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 2.7 8.2 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.3 8.2 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.3 8.2 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.2 8.2 NA1SW8260B NA 406328ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.89 8.2 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.3 8.2 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.2 8.2 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.5 8.2 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.2 8.2 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 1.8 8.2 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 1.1 8.2 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.5 8.2 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 2.1 8.2 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.7 8.2 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.3 8.2 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.4 8.2 NA1SW8260B NA 406328%94.8(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%89.8(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%89.5(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 81 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:501204.22500 KirkhamB-11-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 100 99.0 337410SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 16.7 50.0 337410SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 18.6 50.0 337410SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 19.5 50.0 337410SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 10.4 50.0 337410SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 19.5 50.0 337410SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 11.1 50.0 337410SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 10.1 999 337410SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 15.8 50.0 337410SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 10.8 50.0 337410SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 17.6 50.0 337410SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 10.4 50.0 337410SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 21.0 50.0 337410SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 14.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 7.05 50.0 337410SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 8.00 50.0 337410SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 8.70 99.0 337410SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 7.95 99.0 337410SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 20.1 999 337410SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 848 50.0 337410SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 8.85 50.0 337410SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 15.8 50.0 337410SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 11.1 50.0 337410SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 15.8 50.0 337410SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 13.7 50.0 337410SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 15.0 50.0 337410SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 9.90 50.0 337410SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 15.5 50.0 337410SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 12.0 50.0 337410SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 12.0 50.0 337410SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 4.20 50.0 337410SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 14.4 50.0 337410SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 18.3 50.0 337410SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 9.00 495 337410SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 10.5 50.0 337410
Page 82 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:501204.22500 KirkhamB-11-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 17.9 50.0 337410SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 16.0 50.0 337410SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 12.9 50.0 337410SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 4.05 50.0 337410SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 13.0 50.0 337410SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 10.5 50.0 337410SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 14.6 50.0 337410SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 4.50 495 337410SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 10.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 11.9 50.0 337410SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 4.05 50.0 337410SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 18.0 50.0 337410SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 18.0 50.0 337410SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 17.7 50.0 337410SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 15.0 50.0 337410SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 12.2 50.0 337410SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 12.2 50.0 337410SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 10.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 10.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 16.5 50.0 337410SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 12.3 495 337410SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 15.3 50.0 337410SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 15.5 495 337410SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 21.5 50.0 337410SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 20.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 20.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 16.4 255 337410SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 20.1 99.0 337410SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 56.7 495 337410SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 22.3 50.0 337410SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 13.5 50.0 337410SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 22.7 50.0 337410SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 23.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 26.7 50.0 337410SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 12.6 50.0 337410
Page 83 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:501204.22500 KirkhamB-11-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 20.9 50.0 337410SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 20.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 25.7 50.0 337410SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 20.4 50.0 337410SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 19.8 50.0 337410SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 23.0 50.0 337410SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 22.8 50.0 337410SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 22.8 50.0 337410SW8270C 8/14/11 406315S,D %0.0002,4,6-Tribromophenol (S) 08/15/11 19 122 337410SW8270C 8/14/11 406315S,D %0.0002-Fluorobiphenyl (S) 08/15/11 30 115 337410SW8270C 8/14/11 406315S,D %0.0002-Fluorophenol (S) 08/15/11 25 121 337410SW8270C 8/14/11 406315S,D %0.000Nitrobenzene-d5 (S) 08/15/11 23 120 337410SW8270C 8/14/11 406315S,D %0.000Phenol-d6 (S) 08/15/11 24 113 337410SW8270C 8/14/11 406315S,D %0.000p-Terphenyl-d14 (S) 08/15/11 18 137 337410
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/15/11 406328ug/KgNDTPH(Gasoline) 08/15/11 14 82 342518260TPH 8/15/11 406328S %43.4(S) 4-Bromofluorobenzene 08/15/11 43.9 127 34251
S-Surrogate recovery out of limit.Matrix effect suspected. Sample analyzed twice with similar results.NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 3.83 10 33981SW8015B(M) 8/16/11 406319mg/Kg130TPH as Motor Oil 08/17/11 8.33 20 33981SW8015B(M) 8/16/11 406319mg/Kg69.6Pentacosane (S) 08/17/11 59.7 129 33981
Page 84 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:551204.22500 KirkhamB-11-6.0
SoilSample Matrix:
Lab Sample ID: 1108073-014A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg4.8Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg42Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg30Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg5.3Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg5.7Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg4.3Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg31Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg29Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg17Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%88.5TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%95.0DCBP (S) 08/17/11 55.1 113 34001
Page 85 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:551204.22500 KirkhamB-11-6.0
SoilSample Matrix:
Lab Sample ID: 1108073-014A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDDichlorodifluoromethane 08/15/11 440 1000 NA100SW8260B NA 406301ug/KgNDChloromethane 08/15/11 460 1000 NA100SW8260B NA 406301ug/KgNDVinyl Chloride 08/15/11 260 1000 NA100SW8260B NA 406301ug/KgNDBromomethane 08/15/11 470 1000 NA100SW8260B NA 406301ug/KgNDTrichlorofluoromethane 08/15/11 290 1000 NA100SW8260B NA 406301ug/KgND1,1-Dichloroethene 08/15/11 150 1000 NA100SW8260B NA 406301ug/KgNDFreon 113 08/15/11 370 1000 NA100SW8260B NA 406301ug/KgNDMethylene Chloride 08/15/11 200 5000 NA100SW8260B NA 406301ug/KgNDtrans-1,2-Dichloroethene 08/15/11 110 1000 NA100SW8260B NA 406301ug/KgNDMTBE 08/15/11 260 1000 NA100SW8260B NA 406301ug/KgNDtert-Butanol 08/15/11 2100 5000 NA100SW8260B NA 406301ug/KgNDDiisopropyl ether (DIPE) 08/15/11 220 1000 NA100SW8260B NA 406301ug/KgND1,1-Dichloroethane 08/15/11 130 1000 NA100SW8260B NA 406301ug/KgNDETBE 08/15/11 240 1000 NA100SW8260B NA 406301ug/KgNDcis-1,2-Dichloroethene 08/15/11 180 1000 NA100SW8260B NA 406301ug/KgND2,2-Dichloropropane 08/15/11 120 1000 NA100SW8260B NA 406301ug/KgNDBromochloromethane 08/15/11 230 1000 NA100SW8260B NA 406301ug/KgNDChloroform 08/15/11 120 1000 NA100SW8260B NA 406301ug/KgNDCarbon Tetrachloride 08/15/11 160 1000 NA100SW8260B NA 406301ug/KgND1,1,1-Trichloroethane 08/15/11 120 1000 NA100SW8260B NA 406301ug/KgND1,1-Dichloropropene 08/15/11 140 1000 NA100SW8260B NA 406301ug/KgNDBenzene 08/15/11 150 1000 NA100SW8260B NA 406301ug/KgNDTAME 08/15/11 210 1000 NA100SW8260B NA 406301ug/KgND1,2-Dichloroethane 08/15/11 190 1000 NA100SW8260B NA 406301ug/KgNDTrichloroethylene 08/15/11 390 1000 NA100SW8260B NA 406301ug/KgNDDibromomethane 08/15/11 220 1000 NA100SW8260B NA 406301ug/KgND1,2-Dichloropropane 08/15/11 130 1000 NA100SW8260B NA 406301ug/KgNDBromodichloromethane 08/15/11 110 1000 NA100SW8260B NA 406301ug/KgNDcis-1,3-Dichloropropene 08/15/11 140 1000 NA100SW8260B NA 406301ug/KgNDToluene 08/15/11 98 1000 NA100SW8260B NA 406301ug/KgNDTetrachloroethylene 08/15/11 180 1000 NA100SW8260B NA 406301ug/KgNDtrans-1,3-Dichloropropene 08/15/11 120 1000 NA100SW8260B NA 406301ug/KgND1,1,2-Trichloroethane 08/15/11 180 1000 NA100SW8260B NA 406301ug/KgNDDibromochloromethane 08/15/11 110 1000 NA100SW8260B NA 406301ug/KgND1,3-Dichloropropane 08/15/11 210 1000 NA100SW8260B NA 406301ug/KgND1,2-Dibromoethane 08/15/11 170 1000 NA100
Page 86 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:551204.22500 KirkhamB-11-6.0
SoilSample Matrix:
Lab Sample ID: 1108073-014A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/Kg1500Ethyl Benzene 08/15/11 86 1000 NA100SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 420 1000 NA100SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 86 1000 NA100SW8260B NA 406301ug/Kg4800m,p-Xylene 08/15/11 190 1000 NA100SW8260B NA 406301ug/Kg670o-Xylene 08/15/11 66 500 NA100SW8260B NA 406301ug/KgNDStyrene 08/15/11 77 1000 NA100SW8260B NA 406301ug/KgNDBromoform 08/15/11 190 1000 NA100SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 120 1000 NA100SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 140 1000 NA100SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 120 1000 NA100SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 300 1000 NA100SW8260B NA 406301ug/Kg16001,3,5-Trimethylbenzene 08/15/11 110 1000 NA100SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 330 1000 NA100SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 160 1000 NA100SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 160 1000 NA100SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 140 1000 NA100SW8260B NA 406301ug/Kg48001,2,4-Trimethylbenzene 08/15/11 110 1000 NA100SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 160 1000 NA100SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 150 1000 NA100SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 180 1000 NA100SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 150 1000 NA100SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 220 1000 NA100SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 130 1000 NA100SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 420 1000 NA100SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 260 1000 NA100SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 210 1000 NA100SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 280 1000 NA100SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 290 1000 NA100SW8260B NA 406301%103(S) Dibromofluoromethane 08/15/11 59.8 148 NA100SW8260B NA 406301%72.8(S) Toluene-d8 08/15/11 55.2 133 NA100SW8260B NA 406301%89.1(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA100
Page 87 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:551204.22500 KirkhamB-11-6.0
SoilSample Matrix:
Lab Sample ID: 1108073-014A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 0.660 0.653 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 0.110 0.330 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 0.123 0.330 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 0.0663 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 0.0713 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 0.116 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 0.139 0.330 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 0.0931 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.0465 0.330 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.0528 0.330 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.0574 0.653 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.0525 0.653 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 0.133 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 5.59 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.0584 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 0.0901 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.0653 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 0.102 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.0277 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 0.0950 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 0.121 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.0594 3.27 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 0.118 0.330 33741
Page 88 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:551204.22500 KirkhamB-11-6.0
SoilSample Matrix:
Lab Sample ID: 1108073-014A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 0.106 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 0.0851 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 0.0858 0.330 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 0.0960 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.0297 3.27 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 0.0782 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 0.117 0.330 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 0.109 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 0.0812 3.27 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 0.101 0.330 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 0.102 3.27 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 0.142 0.330 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 0.108 1.68 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 0.132 0.653 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 0.374 3.27 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 0.147 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 0.0891 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 0.149 0.330 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 0.152 0.330 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 0.176 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 0.0832 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 0.138 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 0.133 0.330 33741
Page 89 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:551204.22500 KirkhamB-11-6.0
SoilSample Matrix:
Lab Sample ID: 1108073-014A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 0.169 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 0.135 0.330 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 0.131 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 0.151 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315%59.22,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%67.32-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%75.42-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%64.2Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%78.9Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315%67.6p-Terphenyl-d14 (S) 08/15/11 18 137 33741
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406301x ug/Kg150000TPH(Gasoline) 08/15/11 1700 10000 NA1008260TPH NA 406301%82.7(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA100
x - Does not match pattern of reference Gasoline standard. Result is elevated due to contribution from heavy end hydrocarbons (possibly aged gasoline) and non-fuel light hydrocarbons to the C5-C12 range quantified as Gasoline.
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319x mg/Kg8.1TPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/Kg5.2TPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg113Pentacosane (S) 08/17/11 59.7 129 33981
x-Not typical of Diesel standard pattern (unknown hydrocarbons present).NOTE:
Page 90 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:001204.22500 KirkhamB-11-10.0
SoilSample Matrix:
Lab Sample ID: 1108073-015A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406411ug/KgNDDichlorodifluoromethane 08/24/11 4.4 10 NA1SW8260B NA 406411ug/KgNDChloromethane 08/24/11 4.6 10 NA1SW8260B NA 406411ug/KgNDVinyl Chloride 08/24/11 2.6 10 NA1SW8260B NA 406411ug/KgNDBromomethane 08/24/11 4.7 10 NA1SW8260B NA 406411ug/KgNDTrichlorofluoromethane 08/24/11 2.9 10 NA1SW8260B NA 406411ug/KgND1,1-Dichloroethene 08/24/11 1.5 10 NA1SW8260B NA 406411ug/KgNDFreon 113 08/24/11 3.7 10 NA1SW8260B NA 406411ug/KgNDMethylene Chloride 08/24/11 2.0 50 NA1SW8260B NA 406411ug/KgNDtrans-1,2-Dichloroethene 08/24/11 1.1 10 NA1SW8260B NA 406411ug/KgNDMTBE 08/24/11 2.6 10 NA1SW8260B NA 406411ug/KgNDtert-Butanol 08/24/11 21 50 NA1SW8260B NA 406411ug/KgNDDiisopropyl ether (DIPE) 08/24/11 2.2 10 NA1SW8260B NA 406411ug/KgND1,1-Dichloroethane 08/24/11 1.3 10 NA1SW8260B NA 406411ug/KgNDETBE 08/24/11 2.4 10 NA1SW8260B NA 406411ug/KgNDcis-1,2-Dichloroethene 08/24/11 1.8 10 NA1SW8260B NA 406411ug/KgND2,2-Dichloropropane 08/24/11 1.2 10 NA1SW8260B NA 406411ug/KgNDBromochloromethane 08/24/11 2.3 10 NA1SW8260B NA 406411ug/KgNDChloroform 08/24/11 1.2 10 NA1SW8260B NA 406411ug/KgNDCarbon Tetrachloride 08/24/11 1.6 10 NA1SW8260B NA 406411ug/KgND1,1,1-Trichloroethane 08/24/11 1.2 10 NA1SW8260B NA 406411ug/KgND1,1-Dichloropropene 08/24/11 1.4 10 NA1SW8260B NA 406411ug/KgNDBenzene 08/24/11 1.5 10 NA1SW8260B NA 406411ug/KgNDTAME 08/24/11 2.1 10 NA1SW8260B NA 406411ug/KgND1,2-Dichloroethane 08/24/11 1.9 10 NA1SW8260B NA 406411ug/KgNDTrichloroethylene 08/24/11 3.9 10 NA1SW8260B NA 406411ug/KgNDDibromomethane 08/24/11 2.2 10 NA1SW8260B NA 406411ug/KgND1,2-Dichloropropane 08/24/11 1.3 10 NA1SW8260B NA 406411ug/KgNDBromodichloromethane 08/24/11 1.1 10 NA1SW8260B NA 406411ug/KgNDcis-1,3-Dichloropropene 08/24/11 1.4 10 NA1SW8260B NA 406411ug/KgNDToluene 08/24/11 0.98 10 NA1SW8260B NA 406411ug/KgNDTetrachloroethylene 08/24/11 1.8 10 NA1SW8260B NA 406411ug/KgNDtrans-1,3-Dichloropropene 08/24/11 1.2 10 NA1SW8260B NA 406411ug/KgND1,1,2-Trichloroethane 08/24/11 1.8 10 NA1SW8260B NA 406411ug/KgNDDibromochloromethane 08/24/11 1.1 10 NA1SW8260B NA 406411ug/KgND1,3-Dichloropropane 08/24/11 2.1 10 NA1SW8260B NA 406411ug/KgND1,2-Dibromoethane 08/24/11 1.7 10 NA1
Page 91 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:001204.22500 KirkhamB-11-10.0
SoilSample Matrix:
Lab Sample ID: 1108073-015A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406411ug/KgNDEthyl Benzene 08/24/11 0.86 10 NA1SW8260B NA 406411ug/KgNDChlorobenzene 08/24/11 4.2 10 NA1SW8260B NA 406411ug/KgND1,1,1,2-Tetrachloroethane 08/24/11 0.86 10 NA1SW8260B NA 406411ug/KgNDm,p-Xylene 08/24/11 1.9 10 NA1SW8260B NA 406411ug/KgNDo-Xylene 08/24/11 0.66 5.0 NA1SW8260B NA 406411ug/KgNDStyrene 08/24/11 0.77 10 NA1SW8260B NA 406411ug/KgNDBromoform 08/24/11 1.9 10 NA1SW8260B NA 406411ug/KgNDIsopropyl Benzene 08/24/11 1.2 10 NA1SW8260B NA 406411ug/KgNDn-Propylbenzene 08/24/11 1.4 10 NA1SW8260B NA 406411ug/KgNDBromobenzene 08/24/11 1.2 10 NA1SW8260B NA 406411ug/KgND1,1,2,2-Tetrachloroethane 08/24/11 3.0 10 NA1SW8260B NA 406411ug/KgND1,3,5-Trimethylbenzene 08/24/11 1.1 10 NA1SW8260B NA 406411ug/KgND1,2,3-Trichloropropane 08/24/11 3.3 10 NA1SW8260B NA 406411ug/KgND4-Chlorotoluene 08/24/11 1.6 10 NA1SW8260B NA 406411ug/KgND2-Chlorotoluene 08/24/11 1.6 10 NA1SW8260B NA 406411ug/KgNDtert-Butylbenzene 08/24/11 1.4 10 NA1SW8260B NA 406411ug/KgND1,2,4-Trimethylbenzene 08/24/11 1.1 10 NA1SW8260B NA 406411ug/KgNDsec-Butyl Benzene 08/24/11 1.6 10 NA1SW8260B NA 406411ug/KgNDp-Isopropyltoluene 08/24/11 1.5 10 NA1SW8260B NA 406411ug/KgND1,3-Dichlorobenzene 08/24/11 1.8 10 NA1SW8260B NA 406411ug/KgND1,4-Dichlorobenzene 08/24/11 1.5 10 NA1SW8260B NA 406411ug/KgNDn-Butylbenzene 08/24/11 2.2 10 NA1SW8260B NA 406411ug/KgND1,2-Dichlorobenzene 08/24/11 1.3 10 NA1SW8260B NA 406411ug/KgND1,2-Dibromo-3-Chloropropane 08/24/11 4.2 10 NA1SW8260B NA 406411ug/KgNDHexachlorobutadiene 08/24/11 2.6 10 NA1SW8260B NA 406411ug/KgND1,2,4-Trichlorobenzene 08/24/11 2.1 10 NA1SW8260B NA 406411ug/KgNDNaphthalene 08/24/11 2.8 10 NA1SW8260B NA 406411ug/KgND1,2,3-Trichlorobenzene 08/24/11 2.9 10 NA1SW8260B NA 406411%87.9(S) Dibromofluoromethane 08/24/11 59.8 148 NA1SW8260B NA 406411%90.4(S) Toluene-d8 08/24/11 55.2 133 NA1SW8260B NA 406411%94.1(S) 4-Bromofluorobenzene 08/24/11 55.8 141 NA1
Page 92 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:001204.22500 KirkhamB-11-10.0
SoilSample Matrix:
Lab Sample ID: 1108073-015A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/24/11 406411ug/KgNDTPH(Gasoline) 08/24/11 17 100 348018260TPH 8/24/11 406411%72.5(S) 4-Bromofluorobenzene 08/24/11 43.9 127 34801
Page 93 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:501204.22500 KirkhamB-14-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg2.7Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg77Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg28Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg5.7Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg13Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg46Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg26Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg22Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg47Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921
Page 94 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:501204.22500 KirkhamB-14-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 18 80 340140SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 16 80 340140SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 15 80 340140SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 20 80 340140SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 44 80 340140SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 18 80 340140SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 13 80 340140SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 17 80 340140SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 14 80 340140SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 24 80 340140SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 19 80 340140SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 17 80 340140SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 23 80 340140SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 19 80 340140SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 61 80 340140SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 32 80 340140SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 41 80 340140SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 20 80 340140SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 25 200 340140SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 16 80 340140SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 400 800 340140SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 400 4000 340140SW8081A 8/16/11 406314S,D %0.000TCMX (S) 08/16/11 52.5 139 340140SW8081A 8/16/11 406314S,D %0.000DCBP (S) 08/16/11 50.2 139 340140
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (dark color extract).NOTE:
Page 95 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:501204.22500 KirkhamB-14-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%92.0TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%101DCBP (S) 08/17/11 55.1 113 34001
Page 96 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:501204.22500 KirkhamB-14-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDDichlorodifluoromethane 08/15/11 3.4 7.7 NA1SW8260B NA 406328ug/KgNDChloromethane 08/15/11 3.5 7.7 NA1SW8260B NA 406328ug/KgNDVinyl Chloride 08/15/11 2.0 7.7 NA1SW8260B NA 406328ug/KgNDBromomethane 08/15/11 3.6 7.7 NA1SW8260B NA 406328ug/KgNDTrichlorofluoromethane 08/15/11 2.2 7.7 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethene 08/15/11 1.2 7.7 NA1SW8260B NA 406328ug/KgNDFreon 113 08/15/11 2.9 7.7 NA1SW8260B NA 406328ug/KgNDMethylene Chloride 08/15/11 1.5 39 NA1SW8260B NA 406328ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.86 7.7 NA1SW8260B NA 406328ug/KgNDMTBE 08/15/11 2.0 7.7 NA1SW8260B NA 406328ug/KgNDtert-Butanol 08/15/11 16 39 NA1SW8260B NA 406328ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.7 7.7 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethane 08/15/11 0.98 7.7 NA1SW8260B NA 406328ug/KgNDETBE 08/15/11 1.9 7.7 NA1SW8260B NA 406328ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.4 7.7 NA1SW8260B NA 406328ug/KgND2,2-Dichloropropane 08/15/11 0.95 7.7 NA1SW8260B NA 406328ug/KgNDBromochloromethane 08/15/11 1.8 7.7 NA1SW8260B NA 406328ug/KgNDChloroform 08/15/11 0.94 7.7 NA1SW8260B NA 406328ug/KgNDCarbon Tetrachloride 08/15/11 1.2 7.7 NA1SW8260B NA 406328ug/KgND1,1,1-Trichloroethane 08/15/11 0.94 7.7 NA1SW8260B NA 406328ug/KgND1,1-Dichloropropene 08/15/11 1.1 7.7 NA1SW8260B NA 406328ug/KgNDBenzene 08/15/11 1.2 7.7 NA1SW8260B NA 406328ug/KgNDTAME 08/15/11 1.6 7.7 NA1SW8260B NA 406328ug/KgND1,2-Dichloroethane 08/15/11 1.5 7.7 NA1SW8260B NA 406328ug/KgNDTrichloroethylene 08/15/11 3.0 7.7 NA1SW8260B NA 406328ug/KgNDDibromomethane 08/15/11 1.7 7.7 NA1SW8260B NA 406328ug/KgND1,2-Dichloropropane 08/15/11 1.0 7.7 NA1SW8260B NA 406328ug/KgNDBromodichloromethane 08/15/11 0.86 7.7 NA1SW8260B NA 406328ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.1 7.7 NA1SW8260B NA 406328ug/KgNDToluene 08/15/11 0.76 7.7 NA1SW8260B NA 406328ug/KgNDTetrachloroethylene 08/15/11 1.4 7.7 NA1SW8260B NA 406328ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.89 7.7 NA1SW8260B NA 406328ug/KgND1,1,2-Trichloroethane 08/15/11 1.4 7.7 NA1SW8260B NA 406328ug/KgNDDibromochloromethane 08/15/11 0.86 7.7 NA1SW8260B NA 406328ug/KgND1,3-Dichloropropane 08/15/11 1.6 7.7 NA1SW8260B NA 406328ug/KgND1,2-Dibromoethane 08/15/11 1.3 7.7 NA1
Page 97 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:501204.22500 KirkhamB-14-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.66 7.7 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 3.2 7.7 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.66 7.7 NA1SW8260B NA 406328ug/Kg7.7m,p-Xylene 08/15/11 1.4 7.7 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.51 3.9 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.59 7.7 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.5 7.7 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 0.95 7.7 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.1 7.7 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 0.91 7.7 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.3 7.7 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.87 7.7 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 2.6 7.7 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.2 7.7 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.2 7.7 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.1 7.7 NA1SW8260B NA 406328ug/Kg8.91,2,4-Trimethylbenzene 08/15/11 0.84 7.7 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.3 7.7 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.1 7.7 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.4 7.7 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.2 7.7 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 1.7 7.7 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 1.0 7.7 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.3 7.7 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 2.0 7.7 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.6 7.7 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.2 7.7 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.2 7.7 NA1SW8260B NA 406328%86.3(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%99.6(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%76.2(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 98 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:501204.22500 KirkhamB-14-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 200 198 337420SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 33.3 100 337420SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 37.2 100 337420SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 39.0 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 20.7 100 337420SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 39.0 100 337420SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 22.2 100 337420SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 20.1 2000 337420SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 31.5 100 337420SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 21.6 100 337420SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 35.1 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 20.7 100 337420SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 42.0 100 337420SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 28.2 100 337420SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 14.1 100 337420SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 16.0 100 337420SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 17.4 198 337420SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 15.9 198 337420SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 40.2 2000 337420SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 1700 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 17.7 100 337420SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 31.5 100 337420SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 22.2 100 337420SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 31.5 100 337420SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 27.3 100 337420SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 30.0 100 337420SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 19.8 100 337420SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 30.9 100 337420SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 24.0 100 337420SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 24.0 100 337420SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 8.40 100 337420SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 28.8 100 337420SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 36.6 100 337420SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 18.0 990 337420SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 21.0 100 337420
Page 99 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:501204.22500 KirkhamB-14-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 35.7 100 337420SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 32.0 100 337420SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 25.8 100 337420SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 8.10 100 337420SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 26.0 100 337420SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 21.0 100 337420SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 29.1 100 337420SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 9.00 990 337420SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 20.1 100 337420SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 23.7 100 337420SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 8.10 100 337420SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 36.0 100 337420SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 36.0 100 337420SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 35.4 100 337420SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 30.0 100 337420SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 24.3 100 337420SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 24.3 100 337420SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 20.1 100 337420SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 20.1 100 337420SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 33.0 100 337420SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 24.6 990 337420SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 30.6 100 337420SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 30.9 990 337420SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 42.9 100 337420SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 40.1 100 337420SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 40.1 100 337420SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 32.7 510 337420SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 40.1 198 337420SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 113 990 337420SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 44.5 100 337420SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 27.0 100 337420SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 45.3 100 337420SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 46.2 100 337420SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 53.4 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 25.2 100 337420
Page 100 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:501204.22500 KirkhamB-14-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 41.7 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 40.2 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 51.3 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 40.8 100 337420SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 39.6 100 337420SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 45.9 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 45.6 100 337420SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 45.6 100 337420SW8270C 8/14/11 406315S,D %0.0002,4,6-Tribromophenol (S) 08/15/11 19 122 337420SW8270C 8/14/11 406315S,D %0.0002-Fluorobiphenyl (S) 08/15/11 30 115 337420SW8270C 8/14/11 406315S,D %0.0002-Fluorophenol (S) 08/15/11 25 121 337420SW8270C 8/14/11 406315S,D %0.000Nitrobenzene-d5 (S) 08/15/11 23 120 337420SW8270C 8/14/11 406315S,D %0.000Phenol-d6 (S) 08/15/11 24 113 337420SW8270C 8/14/11 406315S,D %0.000p-Terphenyl-d14 (S) 08/15/11 18 137 337420
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/15/11 406328ug/KgNDTPH(Gasoline) 08/15/11 13 77 342518260TPH 8/15/11 406328%45.7(S) 4-Bromofluorobenzene 08/15/11 43.9 127 34251
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 3.83 10 33981SW8015B(M) 8/16/11 406319mg/Kg280TPH as Motor Oil 08/17/11 8.33 20 33981SW8015B(M) 8/16/11 406319mg/Kg71.8Pentacosane (S) 08/17/11 59.7 129 33981
Page 101 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:551204.22500 KirkhamB-14-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-017A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg3.4Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg75Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg36Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg6.6Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg11Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg7.2Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg30Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg31Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg25Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%64.2TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%86.7DCBP (S) 08/17/11 55.1 113 34001
Page 102 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:551204.22500 KirkhamB-14-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-017A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDDichlorodifluoromethane 08/15/11 4.4 10 NA1SW8260B NA 406328ug/KgNDChloromethane 08/15/11 4.6 10 NA1SW8260B NA 406328ug/KgNDVinyl Chloride 08/15/11 2.6 10 NA1SW8260B NA 406328ug/KgNDBromomethane 08/15/11 4.7 10 NA1SW8260B NA 406328ug/KgNDTrichlorofluoromethane 08/15/11 2.9 10 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethene 08/15/11 1.5 10 NA1SW8260B NA 406328ug/KgNDFreon 113 08/15/11 3.7 10 NA1SW8260B NA 406328ug/KgNDMethylene Chloride 08/15/11 2.0 50 NA1SW8260B NA 406328ug/KgNDtrans-1,2-Dichloroethene 08/15/11 1.1 10 NA1SW8260B NA 406328ug/KgNDMTBE 08/15/11 2.6 10 NA1SW8260B NA 406328ug/KgNDtert-Butanol 08/15/11 21 50 NA1SW8260B NA 406328ug/KgNDDiisopropyl ether (DIPE) 08/15/11 2.2 10 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethane 08/15/11 1.3 10 NA1SW8260B NA 406328ug/KgNDETBE 08/15/11 2.4 10 NA1SW8260B NA 406328ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.8 10 NA1SW8260B NA 406328ug/KgND2,2-Dichloropropane 08/15/11 1.2 10 NA1SW8260B NA 406328ug/KgNDBromochloromethane 08/15/11 2.3 10 NA1SW8260B NA 406328ug/KgNDChloroform 08/15/11 1.2 10 NA1SW8260B NA 406328ug/KgNDCarbon Tetrachloride 08/15/11 1.6 10 NA1SW8260B NA 406328ug/KgND1,1,1-Trichloroethane 08/15/11 1.2 10 NA1SW8260B NA 406328ug/KgND1,1-Dichloropropene 08/15/11 1.4 10 NA1SW8260B NA 406328ug/KgNDBenzene 08/15/11 1.5 10 NA1SW8260B NA 406328ug/KgNDTAME 08/15/11 2.1 10 NA1SW8260B NA 406328ug/KgND1,2-Dichloroethane 08/15/11 1.9 10 NA1SW8260B NA 406328ug/KgNDTrichloroethylene 08/15/11 3.9 10 NA1SW8260B NA 406328ug/KgNDDibromomethane 08/15/11 2.2 10 NA1SW8260B NA 406328ug/KgND1,2-Dichloropropane 08/15/11 1.3 10 NA1SW8260B NA 406328ug/KgNDBromodichloromethane 08/15/11 1.1 10 NA1SW8260B NA 406328ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.4 10 NA1SW8260B NA 406328ug/KgNDToluene 08/15/11 0.98 10 NA1SW8260B NA 406328ug/KgNDTetrachloroethylene 08/15/11 1.8 10 NA1SW8260B NA 406328ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.2 10 NA1SW8260B NA 406328ug/KgND1,1,2-Trichloroethane 08/15/11 1.8 10 NA1SW8260B NA 406328ug/KgNDDibromochloromethane 08/15/11 1.1 10 NA1SW8260B NA 406328ug/KgND1,3-Dichloropropane 08/15/11 2.1 10 NA1SW8260B NA 406328ug/KgND1,2-Dibromoethane 08/15/11 1.7 10 NA1
Page 103 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:551204.22500 KirkhamB-14-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-017A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.86 10 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 4.2 10 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.86 10 NA1SW8260B NA 406328ug/KgNDm,p-Xylene 08/15/11 1.9 10 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.66 5.0 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.77 10 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.9 10 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 1.2 10 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.4 10 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 1.2 10 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 3.0 10 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.1 10 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 3.3 10 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.6 10 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.6 10 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.4 10 NA1SW8260B NA 406328ug/KgND1,2,4-Trimethylbenzene 08/15/11 1.1 10 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.6 10 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.5 10 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.8 10 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.5 10 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 2.2 10 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 1.3 10 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 4.2 10 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 2.6 10 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 2.1 10 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.8 10 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.9 10 NA1SW8260B NA 406328%78.8(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%88.3(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%91.1(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 104 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:551204.22500 KirkhamB-14-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-017A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 0.660 0.653 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 0.110 0.330 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 0.123 0.330 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 0.0663 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 0.0713 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 0.116 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 0.139 0.330 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 0.0931 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.0465 0.330 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.0528 0.330 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.0574 0.653 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.0525 0.653 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 0.133 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 5.59 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.0584 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 0.0901 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.0653 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 0.102 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.0277 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 0.0950 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 0.121 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.0594 3.27 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 0.118 0.330 33741
Page 105 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:551204.22500 KirkhamB-14-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-017A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 0.106 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 0.0851 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 0.0858 0.330 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 0.0960 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.0297 3.27 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 0.0782 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 0.117 0.330 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 0.109 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 0.0812 3.27 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 0.101 0.330 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 0.102 3.27 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 0.142 0.330 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 0.108 1.68 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 0.132 0.653 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 0.374 3.27 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 0.147 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 0.0891 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 0.149 0.330 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 0.152 0.330 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 0.176 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 0.0832 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 0.138 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 0.133 0.330 33741
Page 106 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:551204.22500 KirkhamB-14-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-017A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 0.169 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 0.135 0.330 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 0.131 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 0.151 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315%41.22,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%53.52-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%60.22-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%53.0Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%68.4Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315%62.7p-Terphenyl-d14 (S) 08/15/11 18 137 33741
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/15/11 406328ug/KgNDTPH(Gasoline) 08/15/11 12 71 342518260TPH 8/15/11 406328%51.5(S) 4-Bromofluorobenzene 08/15/11 43.9 127 34251
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/Kg14TPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg105Pentacosane (S) 08/17/11 59.7 129 33981
Page 107 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 13:401204.22500 KirkhamB-15-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-019A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg3.9Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg82Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg25Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg6.4Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg18Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg53Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg24Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg24Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg56Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/Kg0.10Mercury 08/16/11 0.01 0.10 33921
Page 108 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 13:401204.22500 KirkhamB-15-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-019A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 4.4 20 340110SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 4.0 20 340110SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 3.6 20 340110SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 4.9 20 340110SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 11 20 340110SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 4.4 20 340110SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 3.2 20 340110SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 4.2 20 340110SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 3.6 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 5.9 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 4.8 20 340110SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 4.3 20 340110SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 5.7 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 4.7 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 15 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 8.1 20 340110SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 10 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 4.9 20 340110SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 6.2 50 340110SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 4.0 20 340110SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 100 200 340110SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 100 100 340110SW8081A 8/16/11 406314%100TCMX (S) 08/16/11 52.5 139 340110SW8081A 8/16/11 406314%96.5DCBP (S) 08/16/11 50.2 139 340110
Reporting limits increased due to the nature of the sample matrix (dark color extract). Toxaphene reported to the MDL.NOTE:
Page 109 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 13:401204.22500 KirkhamB-15-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-019A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%88.7TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%99.3DCBP (S) 08/17/11 55.1 113 34001
Page 110 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 13:401204.22500 KirkhamB-15-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-019A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDDichlorodifluoromethane 08/15/11 3.7 8.5 NA1SW8260B NA 406328ug/KgNDChloromethane 08/15/11 3.9 8.5 NA1SW8260B NA 406328ug/KgNDVinyl Chloride 08/15/11 2.2 8.5 NA1SW8260B NA 406328ug/KgNDBromomethane 08/15/11 4.0 8.5 NA1SW8260B NA 406328ug/KgNDTrichlorofluoromethane 08/15/11 2.4 8.5 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethene 08/15/11 1.3 8.5 NA1SW8260B NA 406328ug/KgNDFreon 113 08/15/11 3.2 8.5 NA1SW8260B NA 406328ug/KgNDMethylene Chloride 08/15/11 1.7 43 NA1SW8260B NA 406328ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.95 8.5 NA1SW8260B NA 406328ug/KgNDMTBE 08/15/11 2.2 8.5 NA1SW8260B NA 406328ug/KgNDtert-Butanol 08/15/11 18 43 NA1SW8260B NA 406328ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.9 8.5 NA1SW8260B NA 406328ug/KgND1,1-Dichloroethane 08/15/11 1.1 8.5 NA1SW8260B NA 406328ug/KgNDETBE 08/15/11 2.1 8.5 NA1SW8260B NA 406328ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.5 8.5 NA1SW8260B NA 406328ug/KgND2,2-Dichloropropane 08/15/11 1.1 8.5 NA1SW8260B NA 406328ug/KgNDBromochloromethane 08/15/11 1.9 8.5 NA1SW8260B NA 406328ug/KgNDChloroform 08/15/11 1.0 8.5 NA1SW8260B NA 406328ug/KgNDCarbon Tetrachloride 08/15/11 1.4 8.5 NA1SW8260B NA 406328ug/KgND1,1,1-Trichloroethane 08/15/11 1.0 8.5 NA1SW8260B NA 406328ug/KgND1,1-Dichloropropene 08/15/11 1.2 8.5 NA1SW8260B NA 406328ug/KgNDBenzene 08/15/11 1.3 8.5 NA1SW8260B NA 406328ug/KgNDTAME 08/15/11 1.7 8.5 NA1SW8260B NA 406328ug/KgND1,2-Dichloroethane 08/15/11 1.6 8.5 NA1SW8260B NA 406328ug/KgNDTrichloroethylene 08/15/11 3.3 8.5 NA1SW8260B NA 406328ug/KgNDDibromomethane 08/15/11 1.9 8.5 NA1SW8260B NA 406328ug/KgND1,2-Dichloropropane 08/15/11 1.1 8.5 NA1SW8260B NA 406328ug/KgNDBromodichloromethane 08/15/11 0.95 8.5 NA1SW8260B NA 406328ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.2 8.5 NA1SW8260B NA 406328ug/KgNDToluene 08/15/11 0.83 8.5 NA1SW8260B NA 406328ug/KgNDTetrachloroethylene 08/15/11 1.5 8.5 NA1SW8260B NA 406328ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.98 8.5 NA1SW8260B NA 406328ug/KgND1,1,2-Trichloroethane 08/15/11 1.6 8.5 NA1SW8260B NA 406328ug/KgNDDibromochloromethane 08/15/11 0.95 8.5 NA1SW8260B NA 406328ug/KgND1,3-Dichloropropane 08/15/11 1.8 8.5 NA1SW8260B NA 406328ug/KgND1,2-Dibromoethane 08/15/11 1.5 8.5 NA1
Page 111 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 13:401204.22500 KirkhamB-15-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-019A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.73 8.5 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 3.6 8.5 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.73 8.5 NA1SW8260B NA 406328ug/KgNDm,p-Xylene 08/15/11 1.6 8.5 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.56 4.3 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.65 8.5 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.6 8.5 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 1.1 8.5 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.2 8.5 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 1.0 8.5 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.6 8.5 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.96 8.5 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 2.8 8.5 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.4 8.5 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.4 8.5 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.2 8.5 NA1SW8260B NA 406328ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.92 8.5 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.4 8.5 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.2 8.5 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.5 8.5 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.3 8.5 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 1.9 8.5 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 1.1 8.5 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.6 8.5 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 2.2 8.5 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.8 8.5 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.4 8.5 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.4 8.5 NA1SW8260B NA 406328%83.3(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%102(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%72.9(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 112 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 13:401204.22500 KirkhamB-15-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-019A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406316mg/KgNDPyridine 08/16/11 200 198 337420SW8270C 8/14/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 33.3 100 337420SW8270C 8/14/11 406316mg/KgNDAniline 08/16/11 37.2 100 337420SW8270C 8/14/11 406316mg/KgNDPhenol 08/16/11 39.0 100 337420SW8270C 8/14/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 20.7 100 337420SW8270C 8/14/11 406316mg/KgND2-Chlorophenol 08/16/11 39.0 100 337420SW8270C 8/14/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 22.2 100 337420SW8270C 8/14/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 20.1 2000 337420SW8270C 8/14/11 406316mg/KgNDBenzyl Alcohol 08/16/11 31.5 100 337420SW8270C 8/14/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 21.6 100 337420SW8270C 8/14/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 35.1 100 337420SW8270C 8/14/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 20.7 100 337420SW8270C 8/14/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 42.0 100 337420SW8270C 8/14/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 28.2 100 337420SW8270C 8/14/11 406316mg/KgNDHexachloroethane 08/16/11 14.1 100 337420SW8270C 8/14/11 406316mg/KgNDNitrobenzene 08/16/11 16.0 100 337420SW8270C 8/14/11 406316mg/KgNDIsophorone 08/16/11 17.4 198 337420SW8270C 8/14/11 406316mg/KgND2-Nitrophenol 08/16/11 15.9 198 337420SW8270C 8/14/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 40.2 2000 337420SW8270C 8/14/11 406316mg/KgNDBenzoic Acid 08/16/11 1700 100 337420SW8270C 8/14/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 17.7 100 337420SW8270C 8/14/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 31.5 100 337420SW8270C 8/14/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 22.2 100 337420SW8270C 8/14/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 31.5 100 337420SW8270C 8/14/11 406316mg/KgNDNaphthalene 08/16/11 27.3 100 337420SW8270C 8/14/11 406316mg/KgND4-Chloroaniline 08/16/11 30.0 100 337420SW8270C 8/14/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 19.8 100 337420SW8270C 8/14/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 30.9 100 337420SW8270C 8/14/11 406316mg/KgND2-Methylnaphthalene 08/16/11 24.0 100 337420SW8270C 8/14/11 406316mg/KgND1-Methylnaphthalene 08/16/11 24.0 100 337420SW8270C 8/14/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 8.40 100 337420SW8270C 8/14/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 28.8 100 337420SW8270C 8/14/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 36.6 100 337420SW8270C 8/14/11 406316mg/KgND2-Chloronaphthalene 08/16/11 18.0 990 337420SW8270C 8/14/11 406316mg/KgND2-Nitroaniline 08/16/11 21.0 100 337420
Page 113 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 13:401204.22500 KirkhamB-15-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-019A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406316mg/KgNDDimethyl phthalate 08/16/11 35.7 100 337420SW8270C 8/14/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 32.0 100 337420SW8270C 8/14/11 406316mg/KgNDAcenaphthylene 08/16/11 25.8 100 337420SW8270C 8/14/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 8.10 100 337420SW8270C 8/14/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 26.0 100 337420SW8270C 8/14/11 406316mg/KgND3-Nitroaniline 08/16/11 21.0 100 337420SW8270C 8/14/11 406316mg/KgNDAcenaphthene 08/16/11 29.1 100 337420SW8270C 8/14/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 9.00 990 337420SW8270C 8/14/11 406316mg/KgND4-Nitrophenol 08/16/11 20.1 100 337420SW8270C 8/14/11 406316mg/KgNDDibenzofuran 08/16/11 23.7 100 337420SW8270C 8/14/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 8.10 100 337420SW8270C 8/14/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 36.0 100 337420SW8270C 8/14/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 36.0 100 337420SW8270C 8/14/11 406316mg/KgNDDiethylphthalate 08/16/11 35.4 100 337420SW8270C 8/14/11 406316mg/KgNDFluorene 08/16/11 30.0 100 337420SW8270C 8/14/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 24.3 100 337420SW8270C 8/14/11 406316mg/KgND4-Nitroaniline 08/16/11 24.3 100 337420SW8270C 8/14/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 20.1 100 337420SW8270C 8/14/11 406316mg/KgNDDiphenylamine 08/16/11 20.1 100 337420SW8270C 8/14/11 406316mg/KgNDAzobenzene 08/16/11 33.0 100 337420SW8270C 8/14/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 24.6 990 337420SW8270C 8/14/11 406316mg/KgNDHexachlorobenzene 08/16/11 30.6 100 337420SW8270C 8/14/11 406316mg/KgNDPentachlorophenol 08/16/11 30.9 990 337420SW8270C 8/14/11 406316mg/KgNDPhenanthrene 08/16/11 42.9 100 337420SW8270C 8/14/11 406316mg/KgNDAnthracene 08/16/11 40.1 100 337420SW8270C 8/14/11 406316mg/KgNDCarbazole 08/16/11 40.1 100 337420SW8270C 8/14/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 32.7 510 337420SW8270C 8/14/11 406316mg/KgNDFluoranthene 08/16/11 40.1 198 337420SW8270C 8/14/11 406316mg/KgNDBenzidine 08/16/11 113 990 337420SW8270C 8/14/11 406316mg/KgNDPyrene 08/16/11 44.5 100 337420SW8270C 8/14/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 27.0 100 337420SW8270C 8/14/11 406316mg/KgNDBenz[a]anthracene 08/16/11 45.3 100 337420SW8270C 8/14/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 46.2 100 337420SW8270C 8/14/11 406316mg/KgNDChrysene 08/16/11 53.4 100 337420SW8270C 8/14/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 25.2 100 337420
Page 114 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 13:401204.22500 KirkhamB-15-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-019A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 41.7 100 337420SW8270C 8/14/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 40.2 100 337420SW8270C 8/14/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 51.3 100 337420SW8270C 8/14/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 40.8 100 337420SW8270C 8/14/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 39.6 100 337420SW8270C 8/14/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 45.9 100 337420SW8270C 8/14/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 45.6 100 337420SW8270C 8/14/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 45.6 100 337420SW8270C 8/14/11 406316S,D %0.0002,4,6-Tribromophenol (S) 08/16/11 19 122 337420SW8270C 8/14/11 406316S,D %0.0002-Fluorobiphenyl (S) 08/16/11 30 115 337420SW8270C 8/14/11 406316S,D %0.0002-Fluorophenol (S) 08/16/11 25 121 337420SW8270C 8/14/11 406316S,D %0.000Nitrobenzene-d5 (S) 08/16/11 23 120 337420SW8270C 8/14/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 337420SW8270C 8/14/11 406316S,D %0.000p-Terphenyl-d14 (S) 08/16/11 18 137 337420
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/15/11 406328ug/KgNDTPH(Gasoline) 08/15/11 14 85 342518260TPH 8/15/11 406328%50.4(S) 4-Bromofluorobenzene 08/15/11 43.9 127 34251
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 3.83 10 33981SW8015B(M) 8/16/11 406319mg/Kg150TPH as Motor Oil 08/17/11 8.33 20 33981SW8015B(M) 8/16/11 406319mg/Kg76.2Pentacosane (S) 08/17/11 59.7 129 33981
Page 115 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 13:451204.22500 KirkhamB-15-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-020A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg2.2Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg31Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg34Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDCobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/KgNDCopper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg2.4Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg19Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg23Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg13Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%81.1TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%94.5DCBP (S) 08/17/11 55.1 113 34001
Page 116 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 13:451204.22500 KirkhamB-15-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-020A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDDichlorodifluoromethane 08/15/11 3.4 7.7 NA1SW8260B NA 406301ug/KgNDChloromethane 08/15/11 3.5 7.7 NA1SW8260B NA 406301ug/KgNDVinyl Chloride 08/15/11 2.0 7.7 NA1SW8260B NA 406301ug/KgNDBromomethane 08/15/11 3.6 7.7 NA1SW8260B NA 406301ug/KgNDTrichlorofluoromethane 08/15/11 2.2 7.7 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethene 08/15/11 1.2 7.7 NA1SW8260B NA 406301ug/KgNDFreon 113 08/15/11 2.9 7.7 NA1SW8260B NA 406301ug/KgNDMethylene Chloride 08/15/11 1.5 39 NA1SW8260B NA 406301ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.86 7.7 NA1SW8260B NA 406301ug/KgNDMTBE 08/15/11 2.0 7.7 NA1SW8260B NA 406301ug/KgNDtert-Butanol 08/15/11 16 39 NA1SW8260B NA 406301ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.7 7.7 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethane 08/15/11 0.98 7.7 NA1SW8260B NA 406301ug/KgNDETBE 08/15/11 1.9 7.7 NA1SW8260B NA 406301ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.4 7.7 NA1SW8260B NA 406301ug/KgND2,2-Dichloropropane 08/15/11 0.95 7.7 NA1SW8260B NA 406301ug/KgNDBromochloromethane 08/15/11 1.8 7.7 NA1SW8260B NA 406301ug/KgNDChloroform 08/15/11 0.94 7.7 NA1SW8260B NA 406301ug/KgNDCarbon Tetrachloride 08/15/11 1.2 7.7 NA1SW8260B NA 406301ug/KgND1,1,1-Trichloroethane 08/15/11 0.94 7.7 NA1SW8260B NA 406301ug/KgND1,1-Dichloropropene 08/15/11 1.1 7.7 NA1SW8260B NA 406301ug/KgNDBenzene 08/15/11 1.2 7.7 NA1SW8260B NA 406301ug/KgNDTAME 08/15/11 1.6 7.7 NA1SW8260B NA 406301ug/KgND1,2-Dichloroethane 08/15/11 1.5 7.7 NA1SW8260B NA 406301ug/KgNDTrichloroethylene 08/15/11 3.0 7.7 NA1SW8260B NA 406301ug/KgNDDibromomethane 08/15/11 1.7 7.7 NA1SW8260B NA 406301ug/KgND1,2-Dichloropropane 08/15/11 1.0 7.7 NA1SW8260B NA 406301ug/KgNDBromodichloromethane 08/15/11 0.86 7.7 NA1SW8260B NA 406301ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.1 7.7 NA1SW8260B NA 406301ug/KgNDToluene 08/15/11 0.76 7.7 NA1SW8260B NA 406301ug/KgNDTetrachloroethylene 08/15/11 1.4 7.7 NA1SW8260B NA 406301ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.89 7.7 NA1SW8260B NA 406301ug/KgND1,1,2-Trichloroethane 08/15/11 1.4 7.7 NA1SW8260B NA 406301ug/KgNDDibromochloromethane 08/15/11 0.86 7.7 NA1SW8260B NA 406301ug/KgND1,3-Dichloropropane 08/15/11 1.6 7.7 NA1SW8260B NA 406301ug/KgND1,2-Dibromoethane 08/15/11 1.3 7.7 NA1
Page 117 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 13:451204.22500 KirkhamB-15-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-020A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDEthyl Benzene 08/15/11 0.66 7.7 NA1SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 3.2 7.7 NA1SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.66 7.7 NA1SW8260B NA 406301ug/KgNDm,p-Xylene 08/15/11 1.4 7.7 NA1SW8260B NA 406301ug/KgNDo-Xylene 08/15/11 0.51 3.9 NA1SW8260B NA 406301ug/KgNDStyrene 08/15/11 0.59 7.7 NA1SW8260B NA 406301ug/KgNDBromoform 08/15/11 1.5 7.7 NA1SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 0.95 7.7 NA1SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 1.1 7.7 NA1SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 0.91 7.7 NA1SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.3 7.7 NA1SW8260B NA 406301ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.87 7.7 NA1SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 2.6 7.7 NA1SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 1.2 7.7 NA1SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 1.2 7.7 NA1SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 1.1 7.7 NA1SW8260B NA 406301ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.84 7.7 NA1SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 1.3 7.7 NA1SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 1.1 7.7 NA1SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 1.4 7.7 NA1SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 1.2 7.7 NA1SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 1.7 7.7 NA1SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 1.0 7.7 NA1SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.3 7.7 NA1SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 2.0 7.7 NA1SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.6 7.7 NA1SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 2.2 7.7 NA1SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.2 7.7 NA1SW8260B NA 406301%101(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406301%87.3(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406301%102(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 118 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 13:451204.22500 KirkhamB-15-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-020A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 0.660 0.653 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 0.110 0.330 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 0.123 0.330 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 0.0663 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 0.0713 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 0.116 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 0.139 0.330 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 0.0931 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.0465 0.330 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.0528 0.330 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.0574 0.653 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.0525 0.653 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 0.133 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 5.59 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.0584 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 0.0901 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.0653 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 0.102 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.0277 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 0.0950 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 0.121 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.0594 3.27 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 0.118 0.330 33741
Page 119 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 13:451204.22500 KirkhamB-15-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-020A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 0.106 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 0.0851 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 0.0858 0.330 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 0.0960 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.0297 3.27 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 0.0782 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 0.117 0.330 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 0.109 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 0.0812 3.27 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 0.101 0.330 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 0.102 3.27 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 0.142 0.330 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 0.108 1.68 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 0.132 0.653 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 0.374 3.27 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 0.147 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 0.0891 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 0.149 0.330 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 0.152 0.330 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 0.176 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 0.0832 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 0.138 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 0.133 0.330 33741
Page 120 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 13:451204.22500 KirkhamB-15-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-020A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 0.169 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 0.135 0.330 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 0.131 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 0.151 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315%51.92,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%64.52-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%65.52-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%63.2Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%72.8Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315%59.6p-Terphenyl-d14 (S) 08/15/11 18 137 33741
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406301ug/KgNDTPH(Gasoline) 08/15/11 13 77 NA18260TPH NA 406301%75.8(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319x mg/Kg2.6TPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/Kg6.0TPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg108Pentacosane (S) 08/17/11 59.7 129 33981
x-Not typical of Diesel standard pattern (unknown hydrocarbons present).NOTE:
Page 121 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 15:101204.22500 KirkhamB-9-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-022A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg4.0Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg86Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg22Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg6.1Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg22Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg87Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg20Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg22Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg73Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/Kg0.23Mercury 08/16/11 0.01 0.10 33921
Page 122 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 15:101204.22500 KirkhamB-9-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-022A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 18 80 340140SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 16 80 340140SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 15 80 340140SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 20 80 340140SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 44 80 340140SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 18 80 340140SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 13 80 340140SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 17 80 340140SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 14 80 340140SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 24 80 340140SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 19 80 340140SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 17 80 340140SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 23 80 340140SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 19 80 340140SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 61 80 340140SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 32 80 340140SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 41 80 340140SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 20 80 340140SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 25 200 340140SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 16 80 340140SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 400 800 340140SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 400 4000 340140SW8081A 8/16/11 406314S,D %0.000TCMX (S) 08/16/11 52.5 139 340140SW8081A 8/16/11 406314S,D %0.000DCBP (S) 08/16/11 50.2 139 340140
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (dark color extract).NOTE:
Page 123 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 15:101204.22500 KirkhamB-9-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-022A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0690 0.30 34003SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.276 0.60 34003SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.138 0.30 34003SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.129 0.30 34003SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.108 0.30 34003SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0720 0.30 34003SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0810 0.30 34003SW8082 8/16/11 406324%93.0TCMX (S) 08/17/11 50.4 136 34003SW8082 8/16/11 406324%106DCBP (S) 08/17/11 55.1 113 34003
Reporting limits increased due to the nature of the sample matrix (dark color extract).NOTE:
Page 124 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 15:101204.22500 KirkhamB-9-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-022A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDDichlorodifluoromethane 08/15/11 4.8 11 NA1SW8260B NA 406301ug/KgNDChloromethane 08/15/11 5.1 11 NA1SW8260B NA 406301ug/KgNDVinyl Chloride 08/15/11 2.9 11 NA1SW8260B NA 406301ug/KgNDBromomethane 08/15/11 5.1 11 NA1SW8260B NA 406301ug/KgNDTrichlorofluoromethane 08/15/11 3.2 11 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethene 08/15/11 1.7 11 NA1SW8260B NA 406301ug/KgNDFreon 113 08/15/11 4.1 11 NA1SW8260B NA 406301ug/KgNDMethylene Chloride 08/15/11 2.2 55 NA1SW8260B NA 406301ug/KgNDtrans-1,2-Dichloroethene 08/15/11 1.2 11 NA1SW8260B NA 406301ug/KgNDMTBE 08/15/11 2.8 11 NA1SW8260B NA 406301ug/KgNDtert-Butanol 08/15/11 23 55 NA1SW8260B NA 406301ug/KgNDDiisopropyl ether (DIPE) 08/15/11 2.4 11 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethane 08/15/11 1.4 11 NA1SW8260B NA 406301ug/KgNDETBE 08/15/11 2.7 11 NA1SW8260B NA 406301ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.9 11 NA1SW8260B NA 406301ug/KgND2,2-Dichloropropane 08/15/11 1.4 11 NA1SW8260B NA 406301ug/KgNDBromochloromethane 08/15/11 2.5 11 NA1SW8260B NA 406301ug/KgNDChloroform 08/15/11 1.3 11 NA1SW8260B NA 406301ug/KgNDCarbon Tetrachloride 08/15/11 1.8 11 NA1SW8260B NA 406301ug/KgND1,1,1-Trichloroethane 08/15/11 1.3 11 NA1SW8260B NA 406301ug/KgND1,1-Dichloropropene 08/15/11 1.6 11 NA1SW8260B NA 406301ug/KgNDBenzene 08/15/11 1.7 11 NA1SW8260B NA 406301ug/KgNDTAME 08/15/11 2.3 11 NA1SW8260B NA 406301ug/KgND1,2-Dichloroethane 08/15/11 2.1 11 NA1SW8260B NA 406301ug/KgNDTrichloroethylene 08/15/11 4.3 11 NA1SW8260B NA 406301ug/KgNDDibromomethane 08/15/11 2.4 11 NA1SW8260B NA 406301ug/KgND1,2-Dichloropropane 08/15/11 1.4 11 NA1SW8260B NA 406301ug/KgNDBromodichloromethane 08/15/11 1.2 11 NA1SW8260B NA 406301ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.6 11 NA1SW8260B NA 406301ug/KgNDToluene 08/15/11 1.1 11 NA1SW8260B NA 406301ug/KgNDTetrachloroethylene 08/15/11 2.0 11 NA1SW8260B NA 406301ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.3 11 NA1SW8260B NA 406301ug/KgND1,1,2-Trichloroethane 08/15/11 2.0 11 NA1SW8260B NA 406301ug/KgNDDibromochloromethane 08/15/11 1.2 11 NA1SW8260B NA 406301ug/KgND1,3-Dichloropropane 08/15/11 2.3 11 NA1SW8260B NA 406301ug/KgND1,2-Dibromoethane 08/15/11 1.9 11 NA1
Page 125 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 15:101204.22500 KirkhamB-9-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-022A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDEthyl Benzene 08/15/11 0.95 11 NA1SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 4.6 11 NA1SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.94 11 NA1SW8260B NA 406301ug/KgNDm,p-Xylene 08/15/11 2.0 11 NA1SW8260B NA 406301ug/KgNDo-Xylene 08/15/11 0.73 5.5 NA1SW8260B NA 406301ug/KgNDStyrene 08/15/11 0.84 11 NA1SW8260B NA 406301ug/KgNDBromoform 08/15/11 2.1 11 NA1SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 1.4 11 NA1SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 1.6 11 NA1SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 1.3 11 NA1SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 3.3 11 NA1SW8260B NA 406301ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.2 11 NA1SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 3.7 11 NA1SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 1.7 11 NA1SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 1.7 11 NA1SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 1.6 11 NA1SW8260B NA 406301ug/KgND1,2,4-Trimethylbenzene 08/15/11 1.2 11 NA1SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 1.8 11 NA1SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 1.6 11 NA1SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 2.0 11 NA1SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 1.6 11 NA1SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 2.4 11 NA1SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 1.4 11 NA1SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 4.7 11 NA1SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 2.8 11 NA1SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 2.3 11 NA1SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 3.1 11 NA1SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 3.2 11 NA1SW8260B NA 406301%95.4(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406301%96.7(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406301%129(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 126 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 15:101204.22500 KirkhamB-9-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-022A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406316mg/KgNDPyridine 08/16/11 250 248 337425SW8270C 8/14/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 41.6 125 337425SW8270C 8/14/11 406316mg/KgNDAniline 08/16/11 46.5 125 337425SW8270C 8/14/11 406316mg/KgNDPhenol 08/16/11 48.8 125 337425SW8270C 8/14/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 25.9 125 337425SW8270C 8/14/11 406316mg/KgND2-Chlorophenol 08/16/11 48.8 125 337425SW8270C 8/14/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 27.8 125 337425SW8270C 8/14/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 25.1 2500 337425SW8270C 8/14/11 406316mg/KgNDBenzyl Alcohol 08/16/11 39.4 125 337425SW8270C 8/14/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 27.0 125 337425SW8270C 8/14/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 43.9 125 337425SW8270C 8/14/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 25.9 125 337425SW8270C 8/14/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 52.5 125 337425SW8270C 8/14/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 35.3 125 337425SW8270C 8/14/11 406316mg/KgNDHexachloroethane 08/16/11 17.6 125 337425SW8270C 8/14/11 406316mg/KgNDNitrobenzene 08/16/11 20.0 125 337425SW8270C 8/14/11 406316mg/KgNDIsophorone 08/16/11 21.8 248 337425SW8270C 8/14/11 406316mg/KgND2-Nitrophenol 08/16/11 19.9 248 337425SW8270C 8/14/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 50.3 2500 337425SW8270C 8/14/11 406316mg/KgNDBenzoic Acid 08/16/11 2120 125 337425SW8270C 8/14/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 22.1 125 337425SW8270C 8/14/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 39.4 125 337425SW8270C 8/14/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 27.8 125 337425SW8270C 8/14/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 39.4 125 337425SW8270C 8/14/11 406316mg/KgNDNaphthalene 08/16/11 34.1 125 337425SW8270C 8/14/11 406316mg/KgND4-Chloroaniline 08/16/11 37.5 125 337425SW8270C 8/14/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 24.8 125 337425SW8270C 8/14/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 38.6 125 337425SW8270C 8/14/11 406316mg/KgND2-Methylnaphthalene 08/16/11 30.0 125 337425SW8270C 8/14/11 406316mg/KgND1-Methylnaphthalene 08/16/11 30.0 125 337425SW8270C 8/14/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 10.5 125 337425SW8270C 8/14/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 36.0 125 337425SW8270C 8/14/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 45.8 125 337425SW8270C 8/14/11 406316mg/KgND2-Chloronaphthalene 08/16/11 22.5 1240 337425SW8270C 8/14/11 406316mg/KgND2-Nitroaniline 08/16/11 26.3 125 337425
Page 127 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 15:101204.22500 KirkhamB-9-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-022A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406316mg/KgNDDimethyl phthalate 08/16/11 44.6 125 337425SW8270C 8/14/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 40.0 125 337425SW8270C 8/14/11 406316mg/KgNDAcenaphthylene 08/16/11 32.3 125 337425SW8270C 8/14/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 10.1 125 337425SW8270C 8/14/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 32.5 125 337425SW8270C 8/14/11 406316mg/KgND3-Nitroaniline 08/16/11 26.3 125 337425SW8270C 8/14/11 406316mg/KgNDAcenaphthene 08/16/11 36.4 125 337425SW8270C 8/14/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 11.3 1240 337425SW8270C 8/14/11 406316mg/KgND4-Nitrophenol 08/16/11 25.1 125 337425SW8270C 8/14/11 406316mg/KgNDDibenzofuran 08/16/11 29.6 125 337425SW8270C 8/14/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 10.1 125 337425SW8270C 8/14/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 45.0 125 337425SW8270C 8/14/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 45.0 125 337425SW8270C 8/14/11 406316mg/KgNDDiethylphthalate 08/16/11 44.3 125 337425SW8270C 8/14/11 406316mg/KgNDFluorene 08/16/11 37.5 125 337425SW8270C 8/14/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 30.4 125 337425SW8270C 8/14/11 406316mg/KgND4-Nitroaniline 08/16/11 30.4 125 337425SW8270C 8/14/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 25.1 125 337425SW8270C 8/14/11 406316mg/KgNDDiphenylamine 08/16/11 25.1 125 337425SW8270C 8/14/11 406316mg/KgNDAzobenzene 08/16/11 41.3 125 337425SW8270C 8/14/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 30.8 1240 337425SW8270C 8/14/11 406316mg/KgNDHexachlorobenzene 08/16/11 38.3 125 337425SW8270C 8/14/11 406316mg/KgNDPentachlorophenol 08/16/11 38.6 1240 337425SW8270C 8/14/11 406316mg/KgNDPhenanthrene 08/16/11 53.6 125 337425SW8270C 8/14/11 406316mg/KgNDAnthracene 08/16/11 50.2 125 337425SW8270C 8/14/11 406316mg/KgNDCarbazole 08/16/11 50.2 125 337425SW8270C 8/14/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 40.9 638 337425SW8270C 8/14/11 406316mg/KgNDFluoranthene 08/16/11 50.1 248 337425SW8270C 8/14/11 406316mg/KgNDBenzidine 08/16/11 142 1240 337425SW8270C 8/14/11 406316mg/KgNDPyrene 08/16/11 55.6 125 337425SW8270C 8/14/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 33.8 125 337425SW8270C 8/14/11 406316mg/KgNDBenz[a]anthracene 08/16/11 56.6 125 337425SW8270C 8/14/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 57.8 125 337425SW8270C 8/14/11 406316mg/KgNDChrysene 08/16/11 66.8 125 337425SW8270C 8/14/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 31.5 125 337425
Page 128 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 15:101204.22500 KirkhamB-9-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-022A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 52.1 125 337425SW8270C 8/14/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 50.3 125 337425SW8270C 8/14/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 64.1 125 337425SW8270C 8/14/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 51.0 125 337425SW8270C 8/14/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 49.5 125 337425SW8270C 8/14/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 57.4 125 337425SW8270C 8/14/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 57.0 125 337425SW8270C 8/14/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 57.0 125 337425SW8270C 8/14/11 406316S,D %0.0002,4,6-Tribromophenol (S) 08/16/11 19 122 337425SW8270C 8/14/11 406316S,D %0.0002-Fluorobiphenyl (S) 08/16/11 30 115 337425SW8270C 8/14/11 406316S,D %0.0002-Fluorophenol (S) 08/16/11 25 121 337425SW8270C 8/14/11 406316S,D %0.000Nitrobenzene-d5 (S) 08/16/11 23 120 337425SW8270C 8/14/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 337425SW8270C 8/14/11 406316S,D %0.000p-Terphenyl-d14 (S) 08/16/11 18 137 337425
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406301ug/KgNDTPH(Gasoline) 08/15/11 19 110 NA18260TPH NA 406301%45.6(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 7.67 20 33981SW8015B(M) 8/16/11 406319mg/Kg720TPH as Motor Oil 08/17/11 16.7 40 33981SW8015B(M) 8/16/11 406319mg/Kg97.9Pentacosane (S) 08/17/11 59.7 129 33981
Page 129 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 15:151204.22500 KirkhamB-9-3.0
SoilSample Matrix:
Lab Sample ID: 1108073-023A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg3.8Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg78Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg38Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg17Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg19Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg44Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg24Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg41Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg41Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/Kg0.25Mercury 08/16/11 0.01 0.10 33921
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%90.2TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%102DCBP (S) 08/17/11 55.1 113 34001
Page 130 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 15:151204.22500 KirkhamB-9-3.0
SoilSample Matrix:
Lab Sample ID: 1108073-023A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDDichlorodifluoromethane 08/15/11 3.7 8.5 NA1SW8260B NA 406301ug/KgNDChloromethane 08/15/11 3.9 8.5 NA1SW8260B NA 406301ug/KgNDVinyl Chloride 08/15/11 2.2 8.5 NA1SW8260B NA 406301ug/KgNDBromomethane 08/15/11 4.0 8.5 NA1SW8260B NA 406301ug/KgNDTrichlorofluoromethane 08/15/11 2.4 8.5 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethene 08/15/11 1.3 8.5 NA1SW8260B NA 406301ug/KgNDFreon 113 08/15/11 3.2 8.5 NA1SW8260B NA 406301ug/KgNDMethylene Chloride 08/15/11 1.7 43 NA1SW8260B NA 406301ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.95 8.5 NA1SW8260B NA 406301ug/KgNDMTBE 08/15/11 2.2 8.5 NA1SW8260B NA 406301ug/KgNDtert-Butanol 08/15/11 18 43 NA1SW8260B NA 406301ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.9 8.5 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethane 08/15/11 1.1 8.5 NA1SW8260B NA 406301ug/KgNDETBE 08/15/11 2.1 8.5 NA1SW8260B NA 406301ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.5 8.5 NA1SW8260B NA 406301ug/KgND2,2-Dichloropropane 08/15/11 1.1 8.5 NA1SW8260B NA 406301ug/KgNDBromochloromethane 08/15/11 1.9 8.5 NA1SW8260B NA 406301ug/KgNDChloroform 08/15/11 1.0 8.5 NA1SW8260B NA 406301ug/KgNDCarbon Tetrachloride 08/15/11 1.4 8.5 NA1SW8260B NA 406301ug/KgND1,1,1-Trichloroethane 08/15/11 1.0 8.5 NA1SW8260B NA 406301ug/KgND1,1-Dichloropropene 08/15/11 1.2 8.5 NA1SW8260B NA 406301ug/KgNDBenzene 08/15/11 1.3 8.5 NA1SW8260B NA 406301ug/KgNDTAME 08/15/11 1.7 8.5 NA1SW8260B NA 406301ug/KgND1,2-Dichloroethane 08/15/11 1.6 8.5 NA1SW8260B NA 406301ug/KgNDTrichloroethylene 08/15/11 3.3 8.5 NA1SW8260B NA 406301ug/KgNDDibromomethane 08/15/11 1.9 8.5 NA1SW8260B NA 406301ug/KgND1,2-Dichloropropane 08/15/11 1.1 8.5 NA1SW8260B NA 406301ug/KgNDBromodichloromethane 08/15/11 0.95 8.5 NA1SW8260B NA 406301ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.2 8.5 NA1SW8260B NA 406301ug/KgNDToluene 08/15/11 0.83 8.5 NA1SW8260B NA 406301ug/KgNDTetrachloroethylene 08/15/11 1.5 8.5 NA1SW8260B NA 406301ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.98 8.5 NA1SW8260B NA 406301ug/KgND1,1,2-Trichloroethane 08/15/11 1.6 8.5 NA1SW8260B NA 406301ug/KgNDDibromochloromethane 08/15/11 0.95 8.5 NA1SW8260B NA 406301ug/KgND1,3-Dichloropropane 08/15/11 1.8 8.5 NA1SW8260B NA 406301ug/KgND1,2-Dibromoethane 08/15/11 1.5 8.5 NA1
Page 131 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 15:151204.22500 KirkhamB-9-3.0
SoilSample Matrix:
Lab Sample ID: 1108073-023A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDEthyl Benzene 08/15/11 0.73 8.5 NA1SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 3.6 8.5 NA1SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.73 8.5 NA1SW8260B NA 406301ug/KgNDm,p-Xylene 08/15/11 1.6 8.5 NA1SW8260B NA 406301ug/KgNDo-Xylene 08/15/11 0.56 4.3 NA1SW8260B NA 406301ug/KgNDStyrene 08/15/11 0.65 8.5 NA1SW8260B NA 406301ug/KgNDBromoform 08/15/11 1.6 8.5 NA1SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 1.1 8.5 NA1SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 1.2 8.5 NA1SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 1.0 8.5 NA1SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.6 8.5 NA1SW8260B NA 406301ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.96 8.5 NA1SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 2.8 8.5 NA1SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 1.4 8.5 NA1SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 1.4 8.5 NA1SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 1.2 8.5 NA1SW8260B NA 406301ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.92 8.5 NA1SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 1.4 8.5 NA1SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 1.2 8.5 NA1SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 1.5 8.5 NA1SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 1.3 8.5 NA1SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 1.9 8.5 NA1SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 1.1 8.5 NA1SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.6 8.5 NA1SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 2.2 8.5 NA1SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.8 8.5 NA1SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 2.4 8.5 NA1SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.4 8.5 NA1SW8260B NA 406301%99.8(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406301%95.3(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406301%109(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 132 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 15:151204.22500 KirkhamB-9-3.0
SoilSample Matrix:
Lab Sample ID: 1108073-023A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406316mg/KgNDPyridine 08/16/11 200 198 337420SW8270C 8/14/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 33.3 100 337420SW8270C 8/14/11 406316mg/KgNDAniline 08/16/11 37.2 100 337420SW8270C 8/14/11 406316mg/KgNDPhenol 08/16/11 39.0 100 337420SW8270C 8/14/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 20.7 100 337420SW8270C 8/14/11 406316mg/KgND2-Chlorophenol 08/16/11 39.0 100 337420SW8270C 8/14/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 22.2 100 337420SW8270C 8/14/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 20.1 2000 337420SW8270C 8/14/11 406316mg/KgNDBenzyl Alcohol 08/16/11 31.5 100 337420SW8270C 8/14/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 21.6 100 337420SW8270C 8/14/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 35.1 100 337420SW8270C 8/14/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 20.7 100 337420SW8270C 8/14/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 42.0 100 337420SW8270C 8/14/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 28.2 100 337420SW8270C 8/14/11 406316mg/KgNDHexachloroethane 08/16/11 14.1 100 337420SW8270C 8/14/11 406316mg/KgNDNitrobenzene 08/16/11 16.0 100 337420SW8270C 8/14/11 406316mg/KgNDIsophorone 08/16/11 17.4 198 337420SW8270C 8/14/11 406316mg/KgND2-Nitrophenol 08/16/11 15.9 198 337420SW8270C 8/14/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 40.2 2000 337420SW8270C 8/14/11 406316mg/KgNDBenzoic Acid 08/16/11 1700 100 337420SW8270C 8/14/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 17.7 100 337420SW8270C 8/14/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 31.5 100 337420SW8270C 8/14/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 22.2 100 337420SW8270C 8/14/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 31.5 100 337420SW8270C 8/14/11 406316mg/KgNDNaphthalene 08/16/11 27.3 100 337420SW8270C 8/14/11 406316mg/KgND4-Chloroaniline 08/16/11 30.0 100 337420SW8270C 8/14/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 19.8 100 337420SW8270C 8/14/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 30.9 100 337420SW8270C 8/14/11 406316mg/KgND2-Methylnaphthalene 08/16/11 24.0 100 337420SW8270C 8/14/11 406316mg/KgND1-Methylnaphthalene 08/16/11 24.0 100 337420SW8270C 8/14/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 8.40 100 337420SW8270C 8/14/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 28.8 100 337420SW8270C 8/14/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 36.6 100 337420SW8270C 8/14/11 406316mg/KgND2-Chloronaphthalene 08/16/11 18.0 990 337420SW8270C 8/14/11 406316mg/KgND2-Nitroaniline 08/16/11 21.0 100 337420
Page 133 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 15:151204.22500 KirkhamB-9-3.0
SoilSample Matrix:
Lab Sample ID: 1108073-023A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406316mg/KgNDDimethyl phthalate 08/16/11 35.7 100 337420SW8270C 8/14/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 32.0 100 337420SW8270C 8/14/11 406316mg/KgNDAcenaphthylene 08/16/11 25.8 100 337420SW8270C 8/14/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 8.10 100 337420SW8270C 8/14/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 26.0 100 337420SW8270C 8/14/11 406316mg/KgND3-Nitroaniline 08/16/11 21.0 100 337420SW8270C 8/14/11 406316mg/KgNDAcenaphthene 08/16/11 29.1 100 337420SW8270C 8/14/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 9.00 990 337420SW8270C 8/14/11 406316mg/KgND4-Nitrophenol 08/16/11 20.1 100 337420SW8270C 8/14/11 406316mg/KgNDDibenzofuran 08/16/11 23.7 100 337420SW8270C 8/14/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 8.10 100 337420SW8270C 8/14/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 36.0 100 337420SW8270C 8/14/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 36.0 100 337420SW8270C 8/14/11 406316mg/KgNDDiethylphthalate 08/16/11 35.4 100 337420SW8270C 8/14/11 406316mg/KgNDFluorene 08/16/11 30.0 100 337420SW8270C 8/14/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 24.3 100 337420SW8270C 8/14/11 406316mg/KgND4-Nitroaniline 08/16/11 24.3 100 337420SW8270C 8/14/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 20.1 100 337420SW8270C 8/14/11 406316mg/KgNDDiphenylamine 08/16/11 20.1 100 337420SW8270C 8/14/11 406316mg/KgNDAzobenzene 08/16/11 33.0 100 337420SW8270C 8/14/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 24.6 990 337420SW8270C 8/14/11 406316mg/KgNDHexachlorobenzene 08/16/11 30.6 100 337420SW8270C 8/14/11 406316mg/KgNDPentachlorophenol 08/16/11 30.9 990 337420SW8270C 8/14/11 406316mg/KgNDPhenanthrene 08/16/11 42.9 100 337420SW8270C 8/14/11 406316mg/KgNDAnthracene 08/16/11 40.1 100 337420SW8270C 8/14/11 406316mg/KgNDCarbazole 08/16/11 40.1 100 337420SW8270C 8/14/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 32.7 510 337420SW8270C 8/14/11 406316mg/KgNDFluoranthene 08/16/11 40.1 198 337420SW8270C 8/14/11 406316mg/KgNDBenzidine 08/16/11 113 990 337420SW8270C 8/14/11 406316mg/KgNDPyrene 08/16/11 44.5 100 337420SW8270C 8/14/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 27.0 100 337420SW8270C 8/14/11 406316mg/KgNDBenz[a]anthracene 08/16/11 45.3 100 337420SW8270C 8/14/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 46.2 100 337420SW8270C 8/14/11 406316mg/KgNDChrysene 08/16/11 53.4 100 337420SW8270C 8/14/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 25.2 100 337420
Page 134 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 15:151204.22500 KirkhamB-9-3.0
SoilSample Matrix:
Lab Sample ID: 1108073-023A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 41.7 100 337420SW8270C 8/14/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 40.2 100 337420SW8270C 8/14/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 51.3 100 337420SW8270C 8/14/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 40.8 100 337420SW8270C 8/14/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 39.6 100 337420SW8270C 8/14/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 45.9 100 337420SW8270C 8/14/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 45.6 100 337420SW8270C 8/14/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 45.6 100 337420SW8270C 8/14/11 406316S,D %0.0002,4,6-Tribromophenol (S) 08/16/11 19 122 337420SW8270C 8/14/11 406316S,D %0.0002-Fluorobiphenyl (S) 08/16/11 30 115 337420SW8270C 8/14/11 406316S,D %0.0002-Fluorophenol (S) 08/16/11 25 121 337420SW8270C 8/14/11 406316S,D %0.000Nitrobenzene-d5 (S) 08/16/11 23 120 337420SW8270C 8/14/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 337420SW8270C 8/14/11 406316S,D %0.000p-Terphenyl-d14 (S) 08/16/11 18 137 337420
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406301ug/KgNDTPH(Gasoline) 08/15/11 14 85 NA18260TPH NA 406301%56.1(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 3.83 10 33981SW8015B(M) 8/16/11 406319mg/Kg270TPH as Motor Oil 08/17/11 8.33 20 33981SW8015B(M) 8/16/11 406319mg/Kg95.4Pentacosane (S) 08/17/11 59.7 129 33981
Page 135 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:051204.22500 KirkhamB-5-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-025A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/KgNDArsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg37Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg23Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg6.0Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/KgNDCopper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg2.1Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg14Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg17Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg12Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921
Page 136 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:051204.22500 KirkhamB-5-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-025A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 0.44 2.0 34011SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 0.40 2.0 34011SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 0.36 2.0 34011SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 0.49 2.0 34011SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 1.1 2.0 34011SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 0.44 2.0 34011SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 0.32 2.0 34011SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 0.42 2.0 34011SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 0.36 2.0 34011SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 0.59 2.0 34011SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 0.48 2.0 34011SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 0.43 2.0 34011SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 0.57 2.0 34011SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 0.47 2.0 34011SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 1.5 2.0 34011SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 0.81 2.0 34011SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 1.0 2.0 34011SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 0.49 2.0 34011SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 0.62 5.0 34011SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 0.40 2.0 34011SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 10 20 34011SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 10 100 34011SW8081A 8/16/11 406314%63.9TCMX (S) 08/16/11 52.5 139 34011SW8081A 8/16/11 406314%58.7DCBP (S) 08/16/11 50.2 139 34011
Page 137 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:051204.22500 KirkhamB-5-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-025A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%93.6TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%103DCBP (S) 08/17/11 55.1 113 34001
Page 138 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:051204.22500 KirkhamB-5-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-025A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDDichlorodifluoromethane 08/15/11 3.8 8.6 NA1SW8260B NA 406301ug/KgNDChloromethane 08/15/11 4.0 8.6 NA1SW8260B NA 406301ug/KgNDVinyl Chloride 08/15/11 2.3 8.6 NA1SW8260B NA 406301ug/KgNDBromomethane 08/15/11 4.0 8.6 NA1SW8260B NA 406301ug/KgNDTrichlorofluoromethane 08/15/11 2.5 8.6 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethene 08/15/11 1.3 8.6 NA1SW8260B NA 406301ug/KgNDFreon 113 08/15/11 3.2 8.6 NA1SW8260B NA 406301ug/KgNDMethylene Chloride 08/15/11 1.7 43 NA1SW8260B NA 406301ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.96 8.6 NA1SW8260B NA 406301ug/KgNDMTBE 08/15/11 2.2 8.6 NA1SW8260B NA 406301ug/KgNDtert-Butanol 08/15/11 18 43 NA1SW8260B NA 406301ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.9 8.6 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethane 08/15/11 1.1 8.6 NA1SW8260B NA 406301ug/KgNDETBE 08/15/11 2.1 8.6 NA1SW8260B NA 406301ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.5 8.6 NA1SW8260B NA 406301ug/KgND2,2-Dichloropropane 08/15/11 1.1 8.6 NA1SW8260B NA 406301ug/KgNDBromochloromethane 08/15/11 2.0 8.6 NA1SW8260B NA 406301ug/KgNDChloroform 08/15/11 1.0 8.6 NA1SW8260B NA 406301ug/KgNDCarbon Tetrachloride 08/15/11 1.4 8.6 NA1SW8260B NA 406301ug/KgND1,1,1-Trichloroethane 08/15/11 1.0 8.6 NA1SW8260B NA 406301ug/KgND1,1-Dichloropropene 08/15/11 1.2 8.6 NA1SW8260B NA 406301ug/KgNDBenzene 08/15/11 1.3 8.6 NA1SW8260B NA 406301ug/KgNDTAME 08/15/11 1.8 8.6 NA1SW8260B NA 406301ug/KgND1,2-Dichloroethane 08/15/11 1.6 8.6 NA1SW8260B NA 406301ug/KgNDTrichloroethylene 08/15/11 3.3 8.6 NA1SW8260B NA 406301ug/KgNDDibromomethane 08/15/11 1.9 8.6 NA1SW8260B NA 406301ug/KgND1,2-Dichloropropane 08/15/11 1.1 8.6 NA1SW8260B NA 406301ug/KgNDBromodichloromethane 08/15/11 0.96 8.6 NA1SW8260B NA 406301ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.2 8.6 NA1SW8260B NA 406301ug/KgNDToluene 08/15/11 0.84 8.6 NA1SW8260B NA 406301ug/KgNDTetrachloroethylene 08/15/11 1.6 8.6 NA1SW8260B NA 406301ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.99 8.6 NA1SW8260B NA 406301ug/KgND1,1,2-Trichloroethane 08/15/11 1.6 8.6 NA1SW8260B NA 406301ug/KgNDDibromochloromethane 08/15/11 0.96 8.6 NA1SW8260B NA 406301ug/KgND1,3-Dichloropropane 08/15/11 1.8 8.6 NA1SW8260B NA 406301ug/KgND1,2-Dibromoethane 08/15/11 1.5 8.6 NA1
Page 139 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:051204.22500 KirkhamB-5-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-025A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDEthyl Benzene 08/15/11 0.74 8.6 NA1SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 3.6 8.6 NA1SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.74 8.6 NA1SW8260B NA 406301ug/KgNDm,p-Xylene 08/15/11 1.6 8.6 NA1SW8260B NA 406301ug/KgNDo-Xylene 08/15/11 0.57 4.3 NA1SW8260B NA 406301ug/KgNDStyrene 08/15/11 0.66 8.6 NA1SW8260B NA 406301ug/KgNDBromoform 08/15/11 1.6 8.6 NA1SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 1.1 8.6 NA1SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 1.2 8.6 NA1SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 1.0 8.6 NA1SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.6 8.6 NA1SW8260B NA 406301ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.97 8.6 NA1SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 2.9 8.6 NA1SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 1.4 8.6 NA1SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 1.4 8.6 NA1SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 1.2 8.6 NA1SW8260B NA 406301ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.93 8.6 NA1SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 1.4 8.6 NA1SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 1.3 8.6 NA1SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 1.5 8.6 NA1SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 1.3 8.6 NA1SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 1.9 8.6 NA1SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 1.1 8.6 NA1SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.6 8.6 NA1SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 2.2 8.6 NA1SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.8 8.6 NA1SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 2.4 8.6 NA1SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.5 8.6 NA1SW8260B NA 406301%99.7(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406301%90.6(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406301%109(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 140 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:051204.22500 KirkhamB-5-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-025A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 0.660 0.653 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 0.110 0.330 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 0.123 0.330 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 0.0663 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 0.0713 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 0.116 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 0.139 0.330 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 0.0931 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.0465 0.330 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.0528 0.330 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.0574 0.653 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.0525 0.653 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 0.133 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 5.59 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.0584 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 0.0901 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.0653 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 0.102 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.0277 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 0.0950 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 0.121 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.0594 3.27 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 0.118 0.330 33741
Page 141 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:051204.22500 KirkhamB-5-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-025A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 0.106 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 0.0851 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 0.0858 0.330 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 0.0960 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.0297 3.27 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 0.0782 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 0.117 0.330 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 0.109 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 0.0812 3.27 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 0.101 0.330 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 0.102 3.27 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 0.142 0.330 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 0.108 1.68 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 0.132 0.653 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 0.374 3.27 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 0.147 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 0.0891 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 0.149 0.330 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 0.152 0.330 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 0.176 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 0.0832 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 0.138 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 0.133 0.330 33741
Page 142 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:051204.22500 KirkhamB-5-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-025A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 0.169 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 0.135 0.330 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 0.131 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 0.151 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315%49.02,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%59.32-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%65.32-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%60.5Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%73.3Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315%58.8p-Terphenyl-d14 (S) 08/15/11 18 137 33741
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406301ug/KgNDTPH(Gasoline) 08/15/11 15 86 NA18260TPH NA 406301%68.9(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/Kg12TPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg108Pentacosane (S) 08/17/11 59.7 129 33981
Page 143 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:101204.22500 KirkhamB-5-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-026A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg1.8Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg28Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg45Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg5.4Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg5.5Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg3.0Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg31Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg30Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg19Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%79.5TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%90.5DCBP (S) 08/17/11 55.1 113 34001
Page 144 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:101204.22500 KirkhamB-5-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-026A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDDichlorodifluoromethane 08/15/11 3.3 7.6 NA1SW8260B NA 406301ug/KgNDChloromethane 08/15/11 3.5 7.6 NA1SW8260B NA 406301ug/KgNDVinyl Chloride 08/15/11 2.0 7.6 NA1SW8260B NA 406301ug/KgNDBromomethane 08/15/11 3.5 7.6 NA1SW8260B NA 406301ug/KgNDTrichlorofluoromethane 08/15/11 2.2 7.6 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethene 08/15/11 1.2 7.6 NA1SW8260B NA 406301ug/KgNDFreon 113 08/15/11 2.8 7.6 NA1SW8260B NA 406301ug/KgNDMethylene Chloride 08/15/11 1.5 38 NA1SW8260B NA 406301ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.85 7.6 NA1SW8260B NA 406301ug/KgNDMTBE 08/15/11 2.0 7.6 NA1SW8260B NA 406301ug/KgNDtert-Butanol 08/15/11 16 38 NA1SW8260B NA 406301ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.7 7.6 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethane 08/15/11 0.97 7.6 NA1SW8260B NA 406301ug/KgNDETBE 08/15/11 1.8 7.6 NA1SW8260B NA 406301ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.3 7.6 NA1SW8260B NA 406301ug/KgND2,2-Dichloropropane 08/15/11 0.94 7.6 NA1SW8260B NA 406301ug/KgNDBromochloromethane 08/15/11 1.7 7.6 NA1SW8260B NA 406301ug/KgNDChloroform 08/15/11 0.92 7.6 NA1SW8260B NA 406301ug/KgNDCarbon Tetrachloride 08/15/11 1.2 7.6 NA1SW8260B NA 406301ug/KgND1,1,1-Trichloroethane 08/15/11 0.92 7.6 NA1SW8260B NA 406301ug/KgND1,1-Dichloropropene 08/15/11 1.1 7.6 NA1SW8260B NA 406301ug/KgNDBenzene 08/15/11 1.1 7.6 NA1SW8260B NA 406301ug/KgNDTAME 08/15/11 1.6 7.6 NA1SW8260B NA 406301ug/KgND1,2-Dichloroethane 08/15/11 1.4 7.6 NA1SW8260B NA 406301ug/KgNDTrichloroethylene 08/15/11 2.9 7.6 NA1SW8260B NA 406301ug/KgNDDibromomethane 08/15/11 1.7 7.6 NA1SW8260B NA 406301ug/KgND1,2-Dichloropropane 08/15/11 0.99 7.6 NA1SW8260B NA 406301ug/KgNDBromodichloromethane 08/15/11 0.85 7.6 NA1SW8260B NA 406301ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.1 7.6 NA1SW8260B NA 406301ug/KgNDToluene 08/15/11 0.75 7.6 NA1SW8260B NA 406301ug/KgNDTetrachloroethylene 08/15/11 1.4 7.6 NA1SW8260B NA 406301ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.88 7.6 NA1SW8260B NA 406301ug/KgND1,1,2-Trichloroethane 08/15/11 1.4 7.6 NA1SW8260B NA 406301ug/KgNDDibromochloromethane 08/15/11 0.85 7.6 NA1SW8260B NA 406301ug/KgND1,3-Dichloropropane 08/15/11 1.6 7.6 NA1SW8260B NA 406301ug/KgND1,2-Dibromoethane 08/15/11 1.3 7.6 NA1
Page 145 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:101204.22500 KirkhamB-5-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-026A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDEthyl Benzene 08/15/11 0.66 7.6 NA1SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 3.2 7.6 NA1SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.65 7.6 NA1SW8260B NA 406301ug/KgNDm,p-Xylene 08/15/11 1.4 7.6 NA1SW8260B NA 406301ug/KgNDo-Xylene 08/15/11 0.50 3.8 NA1SW8260B NA 406301ug/KgNDStyrene 08/15/11 0.58 7.6 NA1SW8260B NA 406301ug/KgNDBromoform 08/15/11 1.4 7.6 NA1SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 0.94 7.6 NA1SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 1.1 7.6 NA1SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 0.90 7.6 NA1SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.3 7.6 NA1SW8260B NA 406301ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.86 7.6 NA1SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 2.5 7.6 NA1SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 1.2 7.6 NA1SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 1.2 7.6 NA1SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 1.1 7.6 NA1SW8260B NA 406301ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.83 7.6 NA1SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 1.2 7.6 NA1SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 1.1 7.6 NA1SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 1.4 7.6 NA1SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 1.1 7.6 NA1SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 1.7 7.6 NA1SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 1.0 7.6 NA1SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.2 7.6 NA1SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 1.9 7.6 NA1SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.6 7.6 NA1SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 2.2 7.6 NA1SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.2 7.6 NA1SW8260B NA 406301%88.8(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406301%87.6(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406301%101(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 146 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:101204.22500 KirkhamB-5-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-026A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 0.660 0.653 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 0.110 0.330 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 0.123 0.330 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 0.0663 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 0.0713 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 0.116 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 0.139 0.330 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 0.0931 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.0465 0.330 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.0528 0.330 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.0574 0.653 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.0525 0.653 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 0.133 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 5.59 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.0584 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 0.0901 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.0653 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 0.102 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.0277 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 0.0950 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 0.121 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.0594 3.27 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 0.118 0.330 33741
Page 147 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:101204.22500 KirkhamB-5-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-026A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 0.106 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 0.0851 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 0.0858 0.330 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 0.0960 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.0297 3.27 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 0.0782 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 0.117 0.330 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 0.109 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 0.0812 3.27 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 0.101 0.330 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 0.102 3.27 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 0.142 0.330 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 0.108 1.68 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 0.132 0.653 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 0.374 3.27 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 0.147 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 0.0891 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 0.149 0.330 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 0.152 0.330 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 0.176 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 0.0832 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 0.138 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 0.133 0.330 33741
Page 148 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:101204.22500 KirkhamB-5-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-026A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 0.169 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 0.135 0.330 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 0.131 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 0.151 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315%54.42,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%67.12-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%67.52-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%63.5Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%73.3Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315%72.4p-Terphenyl-d14 (S) 08/15/11 18 137 33741
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406301ug/KgNDTPH(Gasoline) 08/15/11 13 76 NA18260TPH NA 406301%68.0(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406319x mg/Kg2.4TPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/Kg4.8TPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg107Pentacosane (S) 08/17/11 59.7 129 33981
x-Not typical of Diesel standard pattern (unknown hydrocarbons present).NOTE:
Page 149 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:251204.22500 KirkhamB-13-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-028A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg4.3Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg94Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg30Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg7.0Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg19Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg53Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg33Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg29Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg58Zinc 08/16/11 0.59 5.0 33881
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921
Page 150 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:251204.22500 KirkhamB-13-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-028A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 18 80 340140SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 16 80 340140SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 15 80 340140SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 20 80 340140SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 44 80 340140SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 18 80 340140SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 13 80 340140SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 17 80 340140SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 14 80 340140SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 24 80 340140SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 19 80 340140SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 17 80 340140SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 23 80 340140SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 19 80 340140SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 61 80 340140SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 32 80 340140SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 41 80 340140SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 20 80 340140SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 25 200 340140SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 16 80 340140SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 400 800 340140SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 400 4000 340140SW8081A 8/16/11 406314S,D %0.000TCMX (S) 08/16/11 52.5 139 340140SW8081A 8/16/11 406314S,D %0.000DCBP (S) 08/16/11 50.2 139 340140
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (dark color extract).NOTE:
Page 151 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:251204.22500 KirkhamB-13-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-028A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.115 0.50 34005SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.460 1.0 34005SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.230 0.50 34005SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.215 0.50 34005SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.180 0.50 34005SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.120 0.50 34005SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.135 0.50 34005SW8082 8/16/11 406324%86.5TCMX (S) 08/17/11 50.4 136 34005SW8082 8/16/11 406324%107DCBP (S) 08/17/11 55.1 113 34005
Reporting limits increased due to the nature of the sample matrix (dark color extract).NOTE:
Page 152 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:251204.22500 KirkhamB-13-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-028A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDDichlorodifluoromethane 08/15/11 3.5 8.1 NA1SW8260B NA 406301ug/KgNDChloromethane 08/15/11 3.7 8.1 NA1SW8260B NA 406301ug/KgNDVinyl Chloride 08/15/11 2.1 8.1 NA1SW8260B NA 406301ug/KgNDBromomethane 08/15/11 3.8 8.1 NA1SW8260B NA 406301ug/KgNDTrichlorofluoromethane 08/15/11 2.3 8.1 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethene 08/15/11 1.3 8.1 NA1SW8260B NA 406301ug/KgNDFreon 113 08/15/11 3.0 8.1 NA1SW8260B NA 406301ug/KgNDMethylene Chloride 08/15/11 1.6 41 NA1SW8260B NA 406301ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.90 8.1 NA1SW8260B NA 406301ug/KgNDMTBE 08/15/11 2.1 8.1 NA1SW8260B NA 406301ug/KgNDtert-Butanol 08/15/11 17 41 NA1SW8260B NA 406301ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.8 8.1 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethane 08/15/11 1.0 8.1 NA1SW8260B NA 406301ug/KgNDETBE 08/15/11 2.0 8.1 NA1SW8260B NA 406301ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.4 8.1 NA1SW8260B NA 406301ug/KgND2,2-Dichloropropane 08/15/11 1.0 8.1 NA1SW8260B NA 406301ug/KgNDBromochloromethane 08/15/11 1.9 8.1 NA1SW8260B NA 406301ug/KgNDChloroform 08/15/11 0.99 8.1 NA1SW8260B NA 406301ug/KgNDCarbon Tetrachloride 08/15/11 1.3 8.1 NA1SW8260B NA 406301ug/KgND1,1,1-Trichloroethane 08/15/11 0.98 8.1 NA1SW8260B NA 406301ug/KgND1,1-Dichloropropene 08/15/11 1.2 8.1 NA1SW8260B NA 406301ug/KgNDBenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406301ug/KgNDTAME 08/15/11 1.7 8.1 NA1SW8260B NA 406301ug/KgND1,2-Dichloroethane 08/15/11 1.5 8.1 NA1SW8260B NA 406301ug/KgNDTrichloroethylene 08/15/11 3.1 8.1 NA1SW8260B NA 406301ug/KgNDDibromomethane 08/15/11 1.8 8.1 NA1SW8260B NA 406301ug/KgND1,2-Dichloropropane 08/15/11 1.1 8.1 NA1SW8260B NA 406301ug/KgNDBromodichloromethane 08/15/11 0.90 8.1 NA1SW8260B NA 406301ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.1 8.1 NA1SW8260B NA 406301ug/KgNDToluene 08/15/11 0.80 8.1 NA1SW8260B NA 406301ug/KgNDTetrachloroethylene 08/15/11 1.5 8.1 NA1SW8260B NA 406301ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.93 8.1 NA1SW8260B NA 406301ug/KgND1,1,2-Trichloroethane 08/15/11 1.5 8.1 NA1SW8260B NA 406301ug/KgNDDibromochloromethane 08/15/11 0.91 8.1 NA1SW8260B NA 406301ug/KgND1,3-Dichloropropane 08/15/11 1.7 8.1 NA1SW8260B NA 406301ug/KgND1,2-Dibromoethane 08/15/11 1.4 8.1 NA1
Page 153 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:251204.22500 KirkhamB-13-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-028A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDEthyl Benzene 08/15/11 0.70 8.1 NA1SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 3.4 8.1 NA1SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.69 8.1 NA1SW8260B NA 406301ug/KgNDm,p-Xylene 08/15/11 1.5 8.1 NA1SW8260B NA 406301ug/KgNDo-Xylene 08/15/11 0.54 4.1 NA1SW8260B NA 406301ug/KgNDStyrene 08/15/11 0.62 8.1 NA1SW8260B NA 406301ug/KgNDBromoform 08/15/11 1.5 8.1 NA1SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 1.0 8.1 NA1SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 0.96 8.1 NA1SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.4 8.1 NA1SW8260B NA 406301ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.91 8.1 NA1SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 2.7 8.1 NA1SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 1.3 8.1 NA1SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 1.3 8.1 NA1SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406301ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.88 8.1 NA1SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 1.3 8.1 NA1SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 1.2 8.1 NA1SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 1.5 8.1 NA1SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 1.8 8.1 NA1SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 1.1 8.1 NA1SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.4 8.1 NA1SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 2.1 8.1 NA1SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.7 8.1 NA1SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 2.3 8.1 NA1SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.3 8.1 NA1SW8260B NA 406301%96.5(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406301%97.9(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406301%129(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 154 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:251204.22500 KirkhamB-13-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-028A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406316mg/KgNDPyridine 08/16/11 250 248 337425SW8270C 8/14/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 41.6 125 337425SW8270C 8/14/11 406316mg/KgNDAniline 08/16/11 46.5 125 337425SW8270C 8/14/11 406316mg/KgNDPhenol 08/16/11 48.8 125 337425SW8270C 8/14/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 25.9 125 337425SW8270C 8/14/11 406316mg/KgND2-Chlorophenol 08/16/11 48.8 125 337425SW8270C 8/14/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 27.8 125 337425SW8270C 8/14/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 25.1 2500 337425SW8270C 8/14/11 406316mg/KgNDBenzyl Alcohol 08/16/11 39.4 125 337425SW8270C 8/14/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 27.0 125 337425SW8270C 8/14/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 43.9 125 337425SW8270C 8/14/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 25.9 125 337425SW8270C 8/14/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 52.5 125 337425SW8270C 8/14/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 35.3 125 337425SW8270C 8/14/11 406316mg/KgNDHexachloroethane 08/16/11 17.6 125 337425SW8270C 8/14/11 406316mg/KgNDNitrobenzene 08/16/11 20.0 125 337425SW8270C 8/14/11 406316mg/KgNDIsophorone 08/16/11 21.8 248 337425SW8270C 8/14/11 406316mg/KgND2-Nitrophenol 08/16/11 19.9 248 337425SW8270C 8/14/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 50.3 2500 337425SW8270C 8/14/11 406316mg/KgNDBenzoic Acid 08/16/11 2120 125 337425SW8270C 8/14/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 22.1 125 337425SW8270C 8/14/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 39.4 125 337425SW8270C 8/14/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 27.8 125 337425SW8270C 8/14/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 39.4 125 337425SW8270C 8/14/11 406316mg/KgNDNaphthalene 08/16/11 34.1 125 337425SW8270C 8/14/11 406316mg/KgND4-Chloroaniline 08/16/11 37.5 125 337425SW8270C 8/14/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 24.8 125 337425SW8270C 8/14/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 38.6 125 337425SW8270C 8/14/11 406316mg/KgND2-Methylnaphthalene 08/16/11 30.0 125 337425SW8270C 8/14/11 406316mg/KgND1-Methylnaphthalene 08/16/11 30.0 125 337425SW8270C 8/14/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 10.5 125 337425SW8270C 8/14/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 36.0 125 337425SW8270C 8/14/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 45.8 125 337425SW8270C 8/14/11 406316mg/KgND2-Chloronaphthalene 08/16/11 22.5 1240 337425SW8270C 8/14/11 406316mg/KgND2-Nitroaniline 08/16/11 26.3 125 337425
Page 155 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:251204.22500 KirkhamB-13-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-028A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406316mg/KgNDDimethyl phthalate 08/16/11 44.6 125 337425SW8270C 8/14/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 40.0 125 337425SW8270C 8/14/11 406316mg/KgNDAcenaphthylene 08/16/11 32.3 125 337425SW8270C 8/14/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 10.1 125 337425SW8270C 8/14/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 32.5 125 337425SW8270C 8/14/11 406316mg/KgND3-Nitroaniline 08/16/11 26.3 125 337425SW8270C 8/14/11 406316mg/KgNDAcenaphthene 08/16/11 36.4 125 337425SW8270C 8/14/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 11.3 1240 337425SW8270C 8/14/11 406316mg/KgND4-Nitrophenol 08/16/11 25.1 125 337425SW8270C 8/14/11 406316mg/KgNDDibenzofuran 08/16/11 29.6 125 337425SW8270C 8/14/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 10.1 125 337425SW8270C 8/14/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 45.0 125 337425SW8270C 8/14/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 45.0 125 337425SW8270C 8/14/11 406316mg/KgNDDiethylphthalate 08/16/11 44.3 125 337425SW8270C 8/14/11 406316mg/KgNDFluorene 08/16/11 37.5 125 337425SW8270C 8/14/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 30.4 125 337425SW8270C 8/14/11 406316mg/KgND4-Nitroaniline 08/16/11 30.4 125 337425SW8270C 8/14/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 25.1 125 337425SW8270C 8/14/11 406316mg/KgNDDiphenylamine 08/16/11 25.1 125 337425SW8270C 8/14/11 406316mg/KgNDAzobenzene 08/16/11 41.3 125 337425SW8270C 8/14/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 30.8 1240 337425SW8270C 8/14/11 406316mg/KgNDHexachlorobenzene 08/16/11 38.3 125 337425SW8270C 8/14/11 406316mg/KgNDPentachlorophenol 08/16/11 38.6 1240 337425SW8270C 8/14/11 406316mg/KgNDPhenanthrene 08/16/11 53.6 125 337425SW8270C 8/14/11 406316mg/KgNDAnthracene 08/16/11 50.2 125 337425SW8270C 8/14/11 406316mg/KgNDCarbazole 08/16/11 50.2 125 337425SW8270C 8/14/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 40.9 638 337425SW8270C 8/14/11 406316mg/KgNDFluoranthene 08/16/11 50.1 248 337425SW8270C 8/14/11 406316mg/KgNDBenzidine 08/16/11 142 1240 337425SW8270C 8/14/11 406316mg/KgNDPyrene 08/16/11 55.6 125 337425SW8270C 8/14/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 33.8 125 337425SW8270C 8/14/11 406316mg/KgNDBenz[a]anthracene 08/16/11 56.6 125 337425SW8270C 8/14/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 57.8 125 337425SW8270C 8/14/11 406316mg/KgNDChrysene 08/16/11 66.8 125 337425SW8270C 8/14/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 31.5 125 337425
Page 156 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:251204.22500 KirkhamB-13-1.0
SoilSample Matrix:
Lab Sample ID: 1108073-028A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/14/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 52.1 125 337425SW8270C 8/14/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 50.3 125 337425SW8270C 8/14/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 64.1 125 337425SW8270C 8/14/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 51.0 125 337425SW8270C 8/14/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 49.5 125 337425SW8270C 8/14/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 57.4 125 337425SW8270C 8/14/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 57.0 125 337425SW8270C 8/14/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 57.0 125 337425SW8270C 8/14/11 406316S,D %0.0002,4,6-Tribromophenol (S) 08/16/11 19 122 337425SW8270C 8/14/11 406316S,D %0.0002-Fluorobiphenyl (S) 08/16/11 30 115 337425SW8270C 8/14/11 406316S,D %0.0002-Fluorophenol (S) 08/16/11 25 121 337425SW8270C 8/14/11 406316S,D %0.000Nitrobenzene-d5 (S) 08/16/11 23 120 337425SW8270C 8/14/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 337425SW8270C 8/14/11 406316S,D %0.000p-Terphenyl-d14 (S) 08/16/11 18 137 337425
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406301ug/KgNDTPH(Gasoline) 08/15/11 14 81 NA18260TPH NA 406301%45.0(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 7.59 20 34181SW8015B(M) 8/18/11 406325mg/Kg960TPH as Motor Oil 08/18/11 16.5 40 34181SW8015B(M) 8/18/11 406325mg/Kg96.2Pentacosane (S) 08/18/11 59.7 129 34181
Page 157 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:301204.22500 KirkhamB-13-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-029A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406267mg/KgNDAntimony 08/16/11 0.20 5.0 33891SW6010B 8/15/11 406267mg/Kg2.5Arsenic 08/16/11 0.28 1.7 33891SW6010B 8/15/11 406267mg/Kg55Barium 08/16/11 1 5.0 33891SW6010B 8/15/11 406267mg/KgNDBeryllium 08/16/11 0.0840 2.0 33891SW6010B 8/15/11 406267mg/KgNDCadmium 08/16/11 0.0590 1.0 33891SW6010B 8/15/11 406267mg/Kg49Chromium 08/16/11 0.0590 5.0 33891SW6010B 8/15/11 406267mg/Kg6.2Cobalt 08/16/11 0.14 5.0 33891SW6010B 8/15/11 406267mg/Kg6.7Copper 08/16/11 0.0900 5.0 33891SW6010B 8/15/11 406267mg/Kg3.5Lead 08/16/11 0.043 1.0 33891SW6010B 8/15/11 406267mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33891SW6010B 8/15/11 406267mg/Kg37Nickel 08/16/11 0.0590 5.0 33891SW6010B 8/15/11 406267mg/KgNDSelenium 08/16/11 0.29 5.0 33891SW6010B 8/15/11 406267mg/KgNDSilver 08/16/11 1.0 1.0 33891SW6010B 8/15/11 406267mg/KgNDThallium 08/16/11 0.12 5.0 33891SW6010B 8/15/11 406267mg/Kg37Vanadium 08/16/11 0.12 5.0 33891SW6010B 8/15/11 406267mg/Kg21Zinc 08/16/11 0.59 5.0 33891
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/KgNDMercury 08/16/11 0.01 0.10 33931
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191SW8082 8/18/11 406326mg/KgNDAroclor1221 08/18/11 0.0920 0.20 34191SW8082 8/18/11 406326mg/KgNDAroclor1232 08/18/11 0.0460 0.10 34191SW8082 8/18/11 406326mg/KgNDAroclor1242 08/18/11 0.0430 0.10 34191SW8082 8/18/11 406326mg/KgNDAroclor1248 08/18/11 0.0360 0.10 34191SW8082 8/18/11 406326mg/KgNDAroclor1254 08/18/11 0.0240 0.10 34191SW8082 8/18/11 406326mg/KgNDAroclor1260 08/18/11 0.0270 0.10 34191SW8082 8/18/11 406326%92.1TCMX (S) 08/18/11 50.4 136 34191SW8082 8/18/11 406326%99.1DCBP (S) 08/18/11 55.1 113 34191
Page 158 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:301204.22500 KirkhamB-13-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-029A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406330ug/KgNDDichlorodifluoromethane 08/18/11 3.3 7.6 NA1SW8260B NA 406330ug/KgNDChloromethane 08/18/11 3.5 7.6 NA1SW8260B NA 406330ug/KgNDVinyl Chloride 08/18/11 2.0 7.6 NA1SW8260B NA 406330ug/KgNDBromomethane 08/18/11 3.5 7.6 NA1SW8260B NA 406330ug/KgNDTrichlorofluoromethane 08/18/11 2.2 7.6 NA1SW8260B NA 406330ug/KgND1,1-Dichloroethene 08/18/11 1.2 7.6 NA1SW8260B NA 406330ug/KgNDFreon 113 08/18/11 2.8 7.6 NA1SW8260B NA 406330ug/KgNDMethylene Chloride 08/18/11 1.5 38 NA1SW8260B NA 406330ug/KgNDtrans-1,2-Dichloroethene 08/18/11 0.85 7.6 NA1SW8260B NA 406330ug/KgNDMTBE 08/18/11 2.0 7.6 NA1SW8260B NA 406330ug/KgNDtert-Butanol 08/18/11 16 38 NA1SW8260B NA 406330ug/KgNDDiisopropyl ether (DIPE) 08/18/11 1.7 7.6 NA1SW8260B NA 406330ug/KgND1,1-Dichloroethane 08/18/11 0.97 7.6 NA1SW8260B NA 406330ug/KgNDETBE 08/18/11 1.8 7.6 NA1SW8260B NA 406330ug/KgNDcis-1,2-Dichloroethene 08/18/11 1.3 7.6 NA1SW8260B NA 406330ug/KgND2,2-Dichloropropane 08/18/11 0.94 7.6 NA1SW8260B NA 406330ug/KgNDBromochloromethane 08/18/11 1.7 7.6 NA1SW8260B NA 406330ug/KgNDChloroform 08/18/11 0.92 7.6 NA1SW8260B NA 406330ug/KgNDCarbon Tetrachloride 08/18/11 1.2 7.6 NA1SW8260B NA 406330ug/KgND1,1,1-Trichloroethane 08/18/11 0.92 7.6 NA1SW8260B NA 406330ug/KgND1,1-Dichloropropene 08/18/11 1.1 7.6 NA1SW8260B NA 406330ug/KgNDBenzene 08/18/11 1.1 7.6 NA1SW8260B NA 406330ug/KgNDTAME 08/18/11 1.6 7.6 NA1SW8260B NA 406330ug/KgND1,2-Dichloroethane 08/18/11 1.4 7.6 NA1SW8260B NA 406330ug/KgNDTrichloroethylene 08/18/11 2.9 7.6 NA1SW8260B NA 406330ug/KgNDDibromomethane 08/18/11 1.7 7.6 NA1SW8260B NA 406330ug/KgND1,2-Dichloropropane 08/18/11 0.99 7.6 NA1SW8260B NA 406330ug/KgNDBromodichloromethane 08/18/11 0.85 7.6 NA1SW8260B NA 406330ug/KgNDcis-1,3-Dichloropropene 08/18/11 1.1 7.6 NA1SW8260B NA 406330ug/KgNDToluene 08/18/11 0.75 7.6 NA1SW8260B NA 406330ug/KgNDTetrachloroethylene 08/18/11 1.4 7.6 NA1SW8260B NA 406330ug/KgNDtrans-1,3-Dichloropropene 08/18/11 0.88 7.6 NA1SW8260B NA 406330ug/KgND1,1,2-Trichloroethane 08/18/11 1.4 7.6 NA1SW8260B NA 406330ug/KgNDDibromochloromethane 08/18/11 0.85 7.6 NA1SW8260B NA 406330ug/KgND1,3-Dichloropropane 08/18/11 1.6 7.6 NA1SW8260B NA 406330ug/KgND1,2-Dibromoethane 08/18/11 1.3 7.6 NA1
Page 159 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:301204.22500 KirkhamB-13-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-029A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406330ug/KgNDEthyl Benzene 08/18/11 0.66 7.6 NA1SW8260B NA 406330ug/KgNDChlorobenzene 08/18/11 3.2 7.6 NA1SW8260B NA 406330ug/KgND1,1,1,2-Tetrachloroethane 08/18/11 0.65 7.6 NA1SW8260B NA 406330ug/KgNDm,p-Xylene 08/18/11 1.4 7.6 NA1SW8260B NA 406330ug/KgNDo-Xylene 08/18/11 0.50 3.8 NA1SW8260B NA 406330ug/KgNDStyrene 08/18/11 0.58 7.6 NA1SW8260B NA 406330ug/KgNDBromoform 08/18/11 1.4 7.6 NA1SW8260B NA 406330ug/KgNDIsopropyl Benzene 08/18/11 0.94 7.6 NA1SW8260B NA 406330ug/KgNDn-Propylbenzene 08/18/11 1.1 7.6 NA1SW8260B NA 406330ug/KgNDBromobenzene 08/18/11 0.90 7.6 NA1SW8260B NA 406330ug/KgND1,1,2,2-Tetrachloroethane 08/18/11 2.3 7.6 NA1SW8260B NA 406330ug/KgND1,3,5-Trimethylbenzene 08/18/11 0.86 7.6 NA1SW8260B NA 406330ug/KgND1,2,3-Trichloropropane 08/18/11 2.5 7.6 NA1SW8260B NA 406330ug/KgND4-Chlorotoluene 08/18/11 1.2 7.6 NA1SW8260B NA 406330ug/KgND2-Chlorotoluene 08/18/11 1.2 7.6 NA1SW8260B NA 406330ug/KgNDtert-Butylbenzene 08/18/11 1.1 7.6 NA1SW8260B NA 406330ug/KgND1,2,4-Trimethylbenzene 08/18/11 0.83 7.6 NA1SW8260B NA 406330ug/KgNDsec-Butyl Benzene 08/18/11 1.2 7.6 NA1SW8260B NA 406330ug/KgNDp-Isopropyltoluene 08/18/11 1.1 7.6 NA1SW8260B NA 406330ug/KgND1,3-Dichlorobenzene 08/18/11 1.4 7.6 NA1SW8260B NA 406330ug/KgND1,4-Dichlorobenzene 08/18/11 1.1 7.6 NA1SW8260B NA 406330ug/KgNDn-Butylbenzene 08/18/11 1.7 7.6 NA1SW8260B NA 406330ug/KgND1,2-Dichlorobenzene 08/18/11 1.0 7.6 NA1SW8260B NA 406330ug/KgND1,2-Dibromo-3-Chloropropane 08/18/11 3.2 7.6 NA1SW8260B NA 406330ug/KgNDHexachlorobutadiene 08/18/11 1.9 7.6 NA1SW8260B NA 406330ug/KgND1,2,4-Trichlorobenzene 08/18/11 1.6 7.6 NA1SW8260B NA 406330ug/KgNDNaphthalene 08/18/11 2.2 7.6 NA1SW8260B NA 406330ug/KgND1,2,3-Trichlorobenzene 08/18/11 2.2 7.6 NA1SW8260B NA 406330%86.0(S) Dibromofluoromethane 08/18/11 59.8 148 NA1SW8260B NA 406330%82.0(S) Toluene-d8 08/18/11 55.2 133 NA1SW8260B NA 406330%98.0(S) 4-Bromofluorobenzene 08/18/11 55.8 141 NA1
Final results and PQL (Reporting Limit) have been corrected for actual mass from pre-tarred 5035 VOAs.NOTE:
Page 160 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:301204.22500 KirkhamB-13-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-029A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 0.660 0.653 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 0.110 0.330 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 0.123 0.330 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 0.0663 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 0.0713 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 0.116 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 0.139 0.330 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 0.0931 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.0465 0.330 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.0528 0.330 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.0574 0.653 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.0525 0.653 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 0.133 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 5.59 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.0584 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 0.0901 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.0653 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 0.102 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.0277 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 0.0950 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 0.121 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.0594 3.27 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 0.118 0.330 33741
Page 161 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:301204.22500 KirkhamB-13-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-029A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 0.106 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 0.0851 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 0.0858 0.330 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 0.0960 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.0297 3.27 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 0.0782 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 0.117 0.330 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 0.109 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 0.0812 3.27 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 0.101 0.330 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 0.102 3.27 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 0.142 0.330 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 0.108 1.68 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 0.132 0.653 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 0.374 3.27 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 0.147 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 0.0891 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 0.149 0.330 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 0.152 0.330 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 0.176 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 0.0832 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 0.138 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 0.133 0.330 33741
Page 162 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:301204.22500 KirkhamB-13-5.0
SoilSample Matrix:
Lab Sample ID: 1108073-029A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 0.169 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 0.135 0.330 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 0.131 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 0.151 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315%55.32,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%69.12-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%60.52-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%64.6Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%73.8Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315%64.2p-Terphenyl-d14 (S) 08/15/11 18 137 33741
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/18/11 406330ug/KgNDTPH(Gasoline) 08/18/11 13 76 342718260TPH 8/18/11 406330%87.1(S) 4-Bromofluorobenzene 08/18/11 43.9 127 34271
Final results and PQL (Reporting Limit) have been corrected for actual mass from pre-tarred 5035 VOAs.NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 0.759 2.0 34181SW8015B(M) 8/18/11 406325mg/KgNDTPH as Motor Oil 08/18/11 1.65 4.0 34181SW8015B(M) 8/18/11 406325mg/Kg104Pentacosane (S) 08/18/11 59.7 129 34181
Page 163 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:401204.22500 KirkhamB-12-1.0 D
SoilSample Matrix:
Lab Sample ID: 1108073-031A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDDichlorodifluoromethane 08/15/11 3.3 7.6 NA1SW8260B NA 406301ug/KgNDChloromethane 08/15/11 3.5 7.6 NA1SW8260B NA 406301ug/KgNDVinyl Chloride 08/15/11 2.0 7.6 NA1SW8260B NA 406301ug/KgNDBromomethane 08/15/11 3.5 7.6 NA1SW8260B NA 406301ug/KgNDTrichlorofluoromethane 08/15/11 2.2 7.6 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethene 08/15/11 1.2 7.6 NA1SW8260B NA 406301ug/KgNDFreon 113 08/15/11 2.8 7.6 NA1SW8260B NA 406301ug/KgNDMethylene Chloride 08/15/11 1.5 38 NA1SW8260B NA 406301ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.85 7.6 NA1SW8260B NA 406301ug/KgNDMTBE 08/15/11 2.0 7.6 NA1SW8260B NA 406301ug/KgNDtert-Butanol 08/15/11 16 38 NA1SW8260B NA 406301ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.7 7.6 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethane 08/15/11 0.97 7.6 NA1SW8260B NA 406301ug/KgNDETBE 08/15/11 1.8 7.6 NA1SW8260B NA 406301ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.3 7.6 NA1SW8260B NA 406301ug/KgND2,2-Dichloropropane 08/15/11 0.94 7.6 NA1SW8260B NA 406301ug/KgNDBromochloromethane 08/15/11 1.7 7.6 NA1SW8260B NA 406301ug/KgNDChloroform 08/15/11 0.92 7.6 NA1SW8260B NA 406301ug/KgNDCarbon Tetrachloride 08/15/11 1.2 7.6 NA1SW8260B NA 406301ug/KgND1,1,1-Trichloroethane 08/15/11 0.92 7.6 NA1SW8260B NA 406301ug/KgND1,1-Dichloropropene 08/15/11 1.1 7.6 NA1SW8260B NA 406301ug/KgNDBenzene 08/15/11 1.1 7.6 NA1SW8260B NA 406301ug/KgNDTAME 08/15/11 1.6 7.6 NA1SW8260B NA 406301ug/KgND1,2-Dichloroethane 08/15/11 1.4 7.6 NA1SW8260B NA 406301ug/KgNDTrichloroethylene 08/15/11 2.9 7.6 NA1SW8260B NA 406301ug/KgNDDibromomethane 08/15/11 1.7 7.6 NA1SW8260B NA 406301ug/KgND1,2-Dichloropropane 08/15/11 0.99 7.6 NA1SW8260B NA 406301ug/KgNDBromodichloromethane 08/15/11 0.85 7.6 NA1SW8260B NA 406301ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.1 7.6 NA1SW8260B NA 406301ug/KgNDToluene 08/15/11 0.75 7.6 NA1SW8260B NA 406301ug/KgNDTetrachloroethylene 08/15/11 1.4 7.6 NA1SW8260B NA 406301ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.88 7.6 NA1SW8260B NA 406301ug/KgND1,1,2-Trichloroethane 08/15/11 1.4 7.6 NA1SW8260B NA 406301ug/KgNDDibromochloromethane 08/15/11 0.85 7.6 NA1SW8260B NA 406301ug/KgND1,3-Dichloropropane 08/15/11 1.6 7.6 NA1SW8260B NA 406301ug/KgND1,2-Dibromoethane 08/15/11 1.3 7.6 NA1
Page 164 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:401204.22500 KirkhamB-12-1.0 D
SoilSample Matrix:
Lab Sample ID: 1108073-031A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDEthyl Benzene 08/15/11 0.66 7.6 NA1SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 3.2 7.6 NA1SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.65 7.6 NA1SW8260B NA 406301ug/KgNDm,p-Xylene 08/15/11 1.4 7.6 NA1SW8260B NA 406301ug/KgNDo-Xylene 08/15/11 0.50 3.8 NA1SW8260B NA 406301ug/KgNDStyrene 08/15/11 0.58 7.6 NA1SW8260B NA 406301ug/KgNDBromoform 08/15/11 1.4 7.6 NA1SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 0.94 7.6 NA1SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 1.1 7.6 NA1SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 0.90 7.6 NA1SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.3 7.6 NA1SW8260B NA 406301ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.86 7.6 NA1SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 2.5 7.6 NA1SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 1.2 7.6 NA1SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 1.2 7.6 NA1SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 1.1 7.6 NA1SW8260B NA 406301ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.83 7.6 NA1SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 1.2 7.6 NA1SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 1.1 7.6 NA1SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 1.4 7.6 NA1SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 1.1 7.6 NA1SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 1.7 7.6 NA1SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 1.0 7.6 NA1SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.2 7.6 NA1SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 1.9 7.6 NA1SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.6 7.6 NA1SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 2.2 7.6 NA1SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.2 7.6 NA1SW8260B NA 406301%99.5(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406301%84.8(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406301%102(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 165 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 10:401204.22500 KirkhamB-12-1.0 D
SoilSample Matrix:
Lab Sample ID: 1108073-031A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406301ug/KgNDTPH(Gasoline) 08/15/11 13 76 NA18260TPH NA 406301%77.8(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Page 166 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:101204.22500 KirkhamB-5-5.0 D
SoilSample Matrix:
Lab Sample ID: 1108073-032A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406267mg/KgNDAntimony 08/16/11 0.20 5.0 33891SW6010B 8/15/11 406267mg/Kg2.5Arsenic 08/16/11 0.28 1.7 33891SW6010B 8/15/11 406267mg/Kg43Barium 08/16/11 1 5.0 33891SW6010B 8/15/11 406267mg/KgNDBeryllium 08/16/11 0.0840 2.0 33891SW6010B 8/15/11 406267mg/KgNDCadmium 08/16/11 0.0590 1.0 33891SW6010B 8/15/11 406267mg/Kg30Chromium 08/16/11 0.0590 5.0 33891SW6010B 8/15/11 406267mg/Kg6.2Cobalt 08/16/11 0.14 5.0 33891SW6010B 8/15/11 406267mg/KgNDCopper 08/16/11 0.0900 5.0 33891SW6010B 8/15/11 406267mg/Kg2.4Lead 08/16/11 0.043 1.0 33891SW6010B 8/15/11 406267mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33891SW6010B 8/15/11 406267mg/Kg29Nickel 08/16/11 0.0590 5.0 33891SW6010B 8/15/11 406267mg/KgNDSelenium 08/16/11 0.29 5.0 33891SW6010B 8/15/11 406267mg/KgNDSilver 08/16/11 1.0 1.0 33891SW6010B 8/15/11 406267mg/KgNDThallium 08/16/11 0.12 5.0 33891SW6010B 8/15/11 406267mg/Kg22Vanadium 08/16/11 0.12 5.0 33891SW6010B 8/15/11 406267mg/Kg16Zinc 08/16/11 0.59 5.0 33891
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/KgNDMercury 08/16/11 0.01 0.10 33931
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191SW8082 8/18/11 406326mg/KgNDAroclor1221 08/18/11 0.0920 0.20 34191SW8082 8/18/11 406326mg/KgNDAroclor1232 08/18/11 0.0460 0.10 34191SW8082 8/18/11 406326mg/KgNDAroclor1242 08/18/11 0.0430 0.10 34191SW8082 8/18/11 406326mg/KgNDAroclor1248 08/18/11 0.0360 0.10 34191SW8082 8/18/11 406326mg/KgNDAroclor1254 08/18/11 0.0240 0.10 34191SW8082 8/18/11 406326mg/KgNDAroclor1260 08/18/11 0.0270 0.10 34191SW8082 8/18/11 406326%95.0TCMX (S) 08/18/11 50.4 136 34191SW8082 8/18/11 406326%106DCBP (S) 08/18/11 55.1 113 34191
Page 167 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:101204.22500 KirkhamB-5-5.0 D
SoilSample Matrix:
Lab Sample ID: 1108073-032A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDDichlorodifluoromethane 08/15/11 3.2 7.3 NA1SW8260B NA 406301ug/KgNDChloromethane 08/15/11 3.4 7.3 NA1SW8260B NA 406301ug/KgNDVinyl Chloride 08/15/11 1.9 7.3 NA1SW8260B NA 406301ug/KgNDBromomethane 08/15/11 3.4 7.3 NA1SW8260B NA 406301ug/KgNDTrichlorofluoromethane 08/15/11 2.1 7.3 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethene 08/15/11 1.1 7.3 NA1SW8260B NA 406301ug/KgNDFreon 113 08/15/11 2.7 7.3 NA1SW8260B NA 406301ug/KgNDMethylene Chloride 08/15/11 1.4 37 NA1SW8260B NA 406301ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.81 7.3 NA1SW8260B NA 406301ug/KgNDMTBE 08/15/11 1.9 7.3 NA1SW8260B NA 406301ug/KgNDtert-Butanol 08/15/11 15 37 NA1SW8260B NA 406301ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.6 7.3 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethane 08/15/11 0.93 7.3 NA1SW8260B NA 406301ug/KgNDETBE 08/15/11 1.8 7.3 NA1SW8260B NA 406301ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.3 7.3 NA1SW8260B NA 406301ug/KgND2,2-Dichloropropane 08/15/11 0.90 7.3 NA1SW8260B NA 406301ug/KgNDBromochloromethane 08/15/11 1.7 7.3 NA1SW8260B NA 406301ug/KgNDChloroform 08/15/11 0.89 7.3 NA1SW8260B NA 406301ug/KgNDCarbon Tetrachloride 08/15/11 1.2 7.3 NA1SW8260B NA 406301ug/KgND1,1,1-Trichloroethane 08/15/11 0.89 7.3 NA1SW8260B NA 406301ug/KgND1,1-Dichloropropene 08/15/11 1.1 7.3 NA1SW8260B NA 406301ug/KgNDBenzene 08/15/11 1.1 7.3 NA1SW8260B NA 406301ug/KgNDTAME 08/15/11 1.5 7.3 NA1SW8260B NA 406301ug/KgND1,2-Dichloroethane 08/15/11 1.4 7.3 NA1SW8260B NA 406301ug/KgNDTrichloroethylene 08/15/11 2.8 7.3 NA1SW8260B NA 406301ug/KgNDDibromomethane 08/15/11 1.6 7.3 NA1SW8260B NA 406301ug/KgND1,2-Dichloropropane 08/15/11 0.95 7.3 NA1SW8260B NA 406301ug/KgNDBromodichloromethane 08/15/11 0.82 7.3 NA1SW8260B NA 406301ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.0 7.3 NA1SW8260B NA 406301ug/KgNDToluene 08/15/11 0.72 7.3 NA1SW8260B NA 406301ug/KgNDTetrachloroethylene 08/15/11 1.3 7.3 NA1SW8260B NA 406301ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.84 7.3 NA1SW8260B NA 406301ug/KgND1,1,2-Trichloroethane 08/15/11 1.3 7.3 NA1SW8260B NA 406301ug/KgNDDibromochloromethane 08/15/11 0.82 7.3 NA1SW8260B NA 406301ug/KgND1,3-Dichloropropane 08/15/11 1.5 7.3 NA1SW8260B NA 406301ug/KgND1,2-Dibromoethane 08/15/11 1.3 7.3 NA1
Page 168 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:101204.22500 KirkhamB-5-5.0 D
SoilSample Matrix:
Lab Sample ID: 1108073-032A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406301ug/KgNDEthyl Benzene 08/15/11 0.63 7.3 NA1SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 3.1 7.3 NA1SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.63 7.3 NA1SW8260B NA 406301ug/KgNDm,p-Xylene 08/15/11 1.4 7.3 NA1SW8260B NA 406301ug/KgNDo-Xylene 08/15/11 0.48 3.7 NA1SW8260B NA 406301ug/KgNDStyrene 08/15/11 0.56 7.3 NA1SW8260B NA 406301ug/KgNDBromoform 08/15/11 1.4 7.3 NA1SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 0.91 7.3 NA1SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 1.0 7.3 NA1SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 0.87 7.3 NA1SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.2 7.3 NA1SW8260B NA 406301ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.82 7.3 NA1SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 2.4 7.3 NA1SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 1.2 7.3 NA1SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 1.2 7.3 NA1SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 1.0 7.3 NA1SW8260B NA 406301ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.79 7.3 NA1SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 1.2 7.3 NA1SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 1.1 7.3 NA1SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 1.3 7.3 NA1SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 1.1 7.3 NA1SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 1.6 7.3 NA1SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 0.96 7.3 NA1SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.1 7.3 NA1SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 1.9 7.3 NA1SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.6 7.3 NA1SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 2.1 7.3 NA1SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.1 7.3 NA1SW8260B NA 406301%101(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406301%81.7(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406301%98.3(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 169 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:101204.22500 KirkhamB-5-5.0 D
SoilSample Matrix:
Lab Sample ID: 1108073-032A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 0.660 0.653 33851SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 0.110 0.330 33851SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 0.123 0.330 33851SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 0.129 0.330 33851SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 0.0683 0.330 33851SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 0.129 0.330 33851SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 0.0733 0.330 33851SW8270C 8/15/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 0.0663 6.59 33851SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 0.104 0.330 33851SW8270C 8/15/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 0.0713 0.330 33851SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 0.116 0.330 33851SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 0.0683 0.330 33851SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 0.139 0.330 33851SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 0.0931 0.330 33851SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 0.0465 0.330 33851SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 0.0528 0.330 33851SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 0.0574 0.653 33851SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 0.0525 0.653 33851SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 0.133 6.59 33851SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 5.59 0.330 33851SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 0.0584 0.330 33851SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 0.104 0.330 33851SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 0.0733 0.330 33851SW8270C 8/15/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 0.104 0.330 33851SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 0.0901 0.330 33851SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 0.0990 0.330 33851SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 0.0653 0.330 33851SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 0.102 0.330 33851SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 0.0792 0.330 33851SW8270C 8/15/11 406316mg/KgND1-Methylnaphthalene 08/16/11 0.0792 0.330 33851SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 0.0277 0.330 33851SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 0.0950 0.330 33851SW8270C 8/15/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 0.121 0.330 33851SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 0.0594 3.27 33851SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 0.0693 0.330 33851SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 0.118 0.330 33851
Page 170 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:101204.22500 KirkhamB-5-5.0 D
SoilSample Matrix:
Lab Sample ID: 1108073-032A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 0.106 0.330 33851SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 0.0851 0.330 33851SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 0.0267 0.330 33851SW8270C 8/15/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 0.0858 0.330 33851SW8270C 8/15/11 406316mg/KgND3-Nitroaniline 08/16/11 0.0693 0.330 33851SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 0.0960 0.330 33851SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 0.0297 3.27 33851SW8270C 8/15/11 406316mg/KgND4-Nitrophenol 08/16/11 0.0663 0.330 33851SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 0.0782 0.330 33851SW8270C 8/15/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 0.0267 0.330 33851SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 0.119 0.330 33851SW8270C 8/15/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 0.119 0.330 33851SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 0.117 0.330 33851SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 0.0990 0.330 33851SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 0.0802 0.330 33851SW8270C 8/15/11 406316mg/KgND4-Nitroaniline 08/16/11 0.0802 0.330 33851SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 0.0663 0.330 33851SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 0.0663 0.330 33851SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 0.109 0.330 33851SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 0.0812 3.27 33851SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 0.101 0.330 33851SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 0.102 3.27 33851SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 0.142 0.330 33851SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 0.132 0.330 33851SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 0.132 0.330 33851SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 0.108 1.68 33851SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 0.132 0.653 33851SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 0.374 3.27 33851SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 0.147 0.330 33851SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 0.0891 0.330 33851SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 0.149 0.330 33851SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 0.152 0.330 33851SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 0.176 0.330 33851SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 0.0832 0.330 33851SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 0.138 0.330 33851SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 0.133 0.330 33851
Page 171 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:101204.22500 KirkhamB-5-5.0 D
SoilSample Matrix:
Lab Sample ID: 1108073-032A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 0.169 0.330 33851SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 0.135 0.330 33851SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 0.131 0.330 33851SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 0.151 0.330 33851SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 0.150 0.330 33851SW8270C 8/15/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 0.150 0.330 33851SW8270C 8/15/11 406316%29.82,4,6-Tribromophenol (S) 08/16/11 19 122 33851SW8270C 8/15/11 406316%54.52-Fluorobiphenyl (S) 08/16/11 30 115 33851SW8270C 8/15/11 406316%40.82-Fluorophenol (S) 08/16/11 25 121 33851SW8270C 8/15/11 406316%51.1Nitrobenzene-d5 (S) 08/16/11 23 120 33851SW8270C 8/15/11 406316%41.5Phenol-d6 (S) 08/16/11 24 113 33851SW8270C 8/15/11 406316%49.9p-Terphenyl-d14 (S) 08/16/11 18 137 33851
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406301ug/KgNDTPH(Gasoline) 08/15/11 12 73 NA18260TPH NA 406301%75.0(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 0.759 2.0 34181SW8015B(M) 8/18/11 406325mg/KgNDTPH as Motor Oil 08/18/11 1.65 4.0 34181SW8015B(M) 8/18/11 406325mg/Kg109Pentacosane (S) 08/18/11 59.7 129 34181
Page 172 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:451204.22500 KirkhamB-1-GW
WaterSample Matrix:
Lab Sample ID: 1108073-033A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDDichlorodifluoromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDChloromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDVinyl Chloride 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromomethane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDTrichlorofluoromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDFreon 113 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDMethylene Chloride 08/17/11 0.18 5.0 NA1SW8260B NA 406320ug/LNDtrans-1,2-Dichloroethene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LNDMTBE 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDtert-Butanol 08/17/11 1.5 5.0 NA1SW8260B NA 406320ug/LNDDiisopropyl ether (DIPE) 08/17/11 0.36 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDETBE 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDcis-1,2-Dichloroethene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND2,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromochloromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LNDChloroform 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDCarbon Tetrachloride 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LND1,1,1-Trichloroethane 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloropropene 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDBenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDTAME 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDTrichloroethylene 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDDibromomethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromodichloromethane 08/17/11 0.23 0.50 NA1SW8260B NA 406320ug/LNDcis-1,3-Dichloropropene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LNDToluene 08/17/11 0.19 0.50 NA1SW8260B NA 406320ug/LNDTetrachloroethylene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LNDtrans-1,3-Dichloropropene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND1,1,2-Trichloroethane 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDDibromochloromethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichloropropane 08/17/11 0.18 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromoethane 08/17/11 0.19 0.50 NA1
Page 173 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:451204.22500 KirkhamB-1-GW
WaterSample Matrix:
Lab Sample ID: 1108073-033A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDChlorobenzene 08/17/11 0.14 0.50 NA1SW8260B NA 406320ug/LNDEthyl Benzene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LND1,1,1,2-Tetrachloroethane 08/17/11 0.10 0.50 NA1SW8260B NA 406320ug/LNDm,p-Xylene 08/17/11 0.20 1.0 NA1SW8260B NA 406320ug/LNDo-Xylene 08/17/11 0.13 0.50 NA1SW8260B NA 406320ug/LNDStyrene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDBromoform 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDIsopropyl Benzene 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDBromobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,1,2,2-Tetrachloroethane 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LNDn-Propylbenzene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LND2-Chlorotoluene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND1,3,5-Trimethylbenzene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND4-Chlorotoluene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LNDtert-Butylbenzene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LND1,2,3-Trichloropropane 08/17/11 0.59 1.0 NA1SW8260B NA 406320ug/LND1,2,4-Trimethylbenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDsec-Butyl Benzene 08/17/11 0.24 0.50 NA1SW8260B NA 406320ug/LNDp-Isopropyltoluene 08/17/11 0.25 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichlorobenzene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LND1,4-Dichlorobenzene 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDn-Butylbenzene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichlorobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromo-3-Chloropropane 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDHexachlorobutadiene 08/17/11 0.22 0.50 NA1SW8260B NA 406320ug/LND1,2,4-Trichlorobenzene 08/17/11 0.48 1.0 NA1SW8260B NA 406320ug/LNDNaphthalene 08/17/11 0.57 1.0 NA1SW8260B NA 406320ug/LND1,2,3-Trichlorobenzene 08/17/11 0.52 1.0 NA1SW8260B NA 406320%90.0(S) Dibromofluoromethane 08/17/11 61.2 131 NA1SW8260B NA 406320%91.5(S) Toluene-d8 08/17/11 75.1 127 NA1SW8260B NA 406320%90.6(S) 4-Bromofluorobenzene 08/17/11 64.1 120 NA1
Page 174 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:451204.22500 KirkhamB-1-GW
WaterSample Matrix:
Lab Sample ID: 1108073-033A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/17/11 406320ug/LNDTPH(Gasoline) 08/17/11 22 50 342218260TPH 8/17/11 406320%80.2(S) 4-Bromofluorobenzene 08/17/11 34 114 34221
Page 175 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:451204.22500 KirkhamB-1-GW
WaterSample Matrix:
Lab Sample ID: 1108073-033B
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021SW8015B(M) 8/16/11 406321%79.5Pentacosane (S) 08/17/11 57.9 125 34021
Page 176 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 9:451204.22500 KirkhamB-1-GW
WaterSample Matrix:
Lab Sample ID: 1108073-033C
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDArsenic (Dissolved) 08/15/11 0.005 0.009 33771SW6010B 8/12/11 406242mg/L0.035Barium (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCobalt (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771SW6010B 8/12/11 406242mg/L0.027Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/L0.012Nickel (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771SW6010B 8/12/11 406242mg/LNDSilver (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7470A 8/12/11 406238mg/LNDMercury 08/15/11 0.00005 0.0002 33651
Page 177 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:001204.22500 KirkhamB-12-GW
WaterSample Matrix:
Lab Sample ID: 1108073-034A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDDichlorodifluoromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDChloromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDVinyl Chloride 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromomethane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDTrichlorofluoromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDFreon 113 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDMethylene Chloride 08/17/11 0.18 5.0 NA1SW8260B NA 406320ug/LNDtrans-1,2-Dichloroethene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LNDMTBE 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDtert-Butanol 08/17/11 1.5 5.0 NA1SW8260B NA 406320ug/LNDDiisopropyl ether (DIPE) 08/17/11 0.36 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDETBE 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDcis-1,2-Dichloroethene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND2,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromochloromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LNDChloroform 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDCarbon Tetrachloride 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LND1,1,1-Trichloroethane 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloropropene 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDBenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDTAME 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDTrichloroethylene 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDDibromomethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromodichloromethane 08/17/11 0.23 0.50 NA1SW8260B NA 406320ug/LNDcis-1,3-Dichloropropene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LNDToluene 08/17/11 0.19 0.50 NA1SW8260B NA 406320ug/LNDTetrachloroethylene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LNDtrans-1,3-Dichloropropene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND1,1,2-Trichloroethane 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDDibromochloromethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichloropropane 08/17/11 0.18 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromoethane 08/17/11 0.19 0.50 NA1
Page 178 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:001204.22500 KirkhamB-12-GW
WaterSample Matrix:
Lab Sample ID: 1108073-034A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDChlorobenzene 08/17/11 0.14 0.50 NA1SW8260B NA 406320ug/LNDEthyl Benzene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LND1,1,1,2-Tetrachloroethane 08/17/11 0.10 0.50 NA1SW8260B NA 406320ug/LNDm,p-Xylene 08/17/11 0.20 1.0 NA1SW8260B NA 406320ug/LNDo-Xylene 08/17/11 0.13 0.50 NA1SW8260B NA 406320ug/LNDStyrene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDBromoform 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDIsopropyl Benzene 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDBromobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,1,2,2-Tetrachloroethane 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LNDn-Propylbenzene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LND2-Chlorotoluene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND1,3,5-Trimethylbenzene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND4-Chlorotoluene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LNDtert-Butylbenzene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LND1,2,3-Trichloropropane 08/17/11 0.59 1.0 NA1SW8260B NA 406320ug/LND1,2,4-Trimethylbenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDsec-Butyl Benzene 08/17/11 0.24 0.50 NA1SW8260B NA 406320ug/LNDp-Isopropyltoluene 08/17/11 0.25 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichlorobenzene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LND1,4-Dichlorobenzene 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDn-Butylbenzene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichlorobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromo-3-Chloropropane 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDHexachlorobutadiene 08/17/11 0.22 0.50 NA1SW8260B NA 406320ug/LND1,2,4-Trichlorobenzene 08/17/11 0.48 1.0 NA1SW8260B NA 406320ug/LNDNaphthalene 08/17/11 0.57 1.0 NA1SW8260B NA 406320ug/LND1,2,3-Trichlorobenzene 08/17/11 0.52 1.0 NA1SW8260B NA 406320%93.9(S) Dibromofluoromethane 08/17/11 61.2 131 NA1SW8260B NA 406320%91.5(S) Toluene-d8 08/17/11 75.1 127 NA1SW8260B NA 406320%88.3(S) 4-Bromofluorobenzene 08/17/11 64.1 120 NA1
Page 179 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:001204.22500 KirkhamB-12-GW
WaterSample Matrix:
Lab Sample ID: 1108073-034A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/17/11 406320ug/LNDTPH(Gasoline) 08/17/11 22 50 342218260TPH 8/17/11 406320%81.0(S) 4-Bromofluorobenzene 08/17/11 34 114 34221
Page 180 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:001204.22500 KirkhamB-12-GW
WaterSample Matrix:
Lab Sample ID: 1108073-034B
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021SW8015B(M) 8/16/11 406321%79.9Pentacosane (S) 08/17/11 57.9 125 34021
Page 181 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:001204.22500 KirkhamB-12-GW
WaterSample Matrix:
Lab Sample ID: 1108073-034C
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDArsenic (Dissolved) 08/15/11 0.005 0.009 33771SW6010B 8/12/11 406242mg/L0.022Barium (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/L0.012Cobalt (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771SW6010B 8/12/11 406242mg/L0.040Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/L0.019Nickel (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771SW6010B 8/12/11 406242mg/LNDSilver (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7470A 8/12/11 406238mg/LNDMercury 08/15/11 0.00005 0.0002 33651
Page 182 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:001204.22500 KirkhamB-12-GWD
WaterSample Matrix:
Lab Sample ID: 1108073-035A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDDichlorodifluoromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDChloromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDVinyl Chloride 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromomethane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDTrichlorofluoromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDFreon 113 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDMethylene Chloride 08/17/11 0.18 5.0 NA1SW8260B NA 406320ug/LNDtrans-1,2-Dichloroethene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LNDMTBE 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDtert-Butanol 08/17/11 1.5 5.0 NA1SW8260B NA 406320ug/LNDDiisopropyl ether (DIPE) 08/17/11 0.36 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDETBE 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDcis-1,2-Dichloroethene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND2,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromochloromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LNDChloroform 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDCarbon Tetrachloride 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LND1,1,1-Trichloroethane 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloropropene 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDBenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDTAME 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDTrichloroethylene 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDDibromomethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromodichloromethane 08/17/11 0.23 0.50 NA1SW8260B NA 406320ug/LNDcis-1,3-Dichloropropene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LNDToluene 08/17/11 0.19 0.50 NA1SW8260B NA 406320ug/LNDTetrachloroethylene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LNDtrans-1,3-Dichloropropene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND1,1,2-Trichloroethane 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDDibromochloromethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichloropropane 08/17/11 0.18 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromoethane 08/17/11 0.19 0.50 NA1
Page 183 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:001204.22500 KirkhamB-12-GWD
WaterSample Matrix:
Lab Sample ID: 1108073-035A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDChlorobenzene 08/17/11 0.14 0.50 NA1SW8260B NA 406320ug/LNDEthyl Benzene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LND1,1,1,2-Tetrachloroethane 08/17/11 0.10 0.50 NA1SW8260B NA 406320ug/LNDm,p-Xylene 08/17/11 0.20 1.0 NA1SW8260B NA 406320ug/LNDo-Xylene 08/17/11 0.13 0.50 NA1SW8260B NA 406320ug/LNDStyrene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDBromoform 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDIsopropyl Benzene 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDBromobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,1,2,2-Tetrachloroethane 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LNDn-Propylbenzene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LND2-Chlorotoluene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND1,3,5-Trimethylbenzene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND4-Chlorotoluene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LNDtert-Butylbenzene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LND1,2,3-Trichloropropane 08/17/11 0.59 1.0 NA1SW8260B NA 406320ug/LND1,2,4-Trimethylbenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDsec-Butyl Benzene 08/17/11 0.24 0.50 NA1SW8260B NA 406320ug/LNDp-Isopropyltoluene 08/17/11 0.25 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichlorobenzene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LND1,4-Dichlorobenzene 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDn-Butylbenzene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichlorobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromo-3-Chloropropane 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDHexachlorobutadiene 08/17/11 0.22 0.50 NA1SW8260B NA 406320ug/LND1,2,4-Trichlorobenzene 08/17/11 0.48 1.0 NA1SW8260B NA 406320ug/LNDNaphthalene 08/17/11 0.57 1.0 NA1SW8260B NA 406320ug/LND1,2,3-Trichlorobenzene 08/17/11 0.52 1.0 NA1SW8260B NA 406320%92.5(S) Dibromofluoromethane 08/17/11 61.2 131 NA1SW8260B NA 406320%90.7(S) Toluene-d8 08/17/11 75.1 127 NA1SW8260B NA 406320%86.6(S) 4-Bromofluorobenzene 08/17/11 64.1 120 NA1
Page 184 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:001204.22500 KirkhamB-12-GWD
WaterSample Matrix:
Lab Sample ID: 1108073-035A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/17/11 406320ug/LNDTPH(Gasoline) 08/17/11 22 50 342218260TPH 8/17/11 406320%70.0(S) 4-Bromofluorobenzene 08/17/11 34 114 34221
Page 185 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 11:001204.22500 KirkhamB-12-GWD
WaterSample Matrix:
Lab Sample ID: 1108073-035B
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021SW8015B(M) 8/16/11 406321%76.9Pentacosane (S) 08/17/11 57.9 125 34021
Page 186 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:101204.22500 KirkhamB-11-GW
WaterSample Matrix:
Lab Sample ID: 1108073-036A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDDichlorodifluoromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDChloromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDVinyl Chloride 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromomethane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDTrichlorofluoromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDFreon 113 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDMethylene Chloride 08/17/11 0.18 5.0 NA1SW8260B NA 406320ug/LNDtrans-1,2-Dichloroethene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LNDMTBE 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDtert-Butanol 08/17/11 1.5 5.0 NA1SW8260B NA 406320ug/LNDDiisopropyl ether (DIPE) 08/17/11 0.36 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDETBE 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDcis-1,2-Dichloroethene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND2,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromochloromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LNDChloroform 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDCarbon Tetrachloride 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LND1,1,1-Trichloroethane 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloropropene 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDBenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDTAME 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDTrichloroethylene 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDDibromomethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromodichloromethane 08/17/11 0.23 0.50 NA1SW8260B NA 406320ug/LNDcis-1,3-Dichloropropene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LNDToluene 08/17/11 0.19 0.50 NA1SW8260B NA 406320ug/LNDTetrachloroethylene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LNDtrans-1,3-Dichloropropene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND1,1,2-Trichloroethane 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDDibromochloromethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichloropropane 08/17/11 0.18 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromoethane 08/17/11 0.19 0.50 NA1
Page 187 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:101204.22500 KirkhamB-11-GW
WaterSample Matrix:
Lab Sample ID: 1108073-036A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDChlorobenzene 08/17/11 0.14 0.50 NA1SW8260B NA 406320ug/L45Ethyl Benzene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LND1,1,1,2-Tetrachloroethane 08/17/11 0.10 0.50 NA1SW8260B NA 406320ug/L110m,p-Xylene 08/17/11 0.20 1.0 NA1SW8260B NA 406320ug/L17o-Xylene 08/17/11 0.13 0.50 NA1SW8260B NA 406320ug/LNDStyrene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDBromoform 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/L6.1Isopropyl Benzene 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDBromobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,1,2,2-Tetrachloroethane 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/L21n-Propylbenzene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LND2-Chlorotoluene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/L261,3,5-Trimethylbenzene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND4-Chlorotoluene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LNDtert-Butylbenzene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LND1,2,3-Trichloropropane 08/17/11 0.59 1.0 NA1SW8260B NA 406320ug/L521,2,4-Trimethylbenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDsec-Butyl Benzene 08/17/11 0.24 0.50 NA1SW8260B NA 406320ug/LNDp-Isopropyltoluene 08/17/11 0.25 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichlorobenzene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LND1,4-Dichlorobenzene 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/L4.6n-Butylbenzene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichlorobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromo-3-Chloropropane 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDHexachlorobutadiene 08/17/11 0.22 0.50 NA1SW8260B NA 406320ug/LND1,2,4-Trichlorobenzene 08/17/11 0.48 1.0 NA1SW8260B NA 406320ug/L12Naphthalene 08/17/11 0.57 1.0 NA1SW8260B NA 406320ug/LND1,2,3-Trichlorobenzene 08/17/11 0.52 1.0 NA1SW8260B NA 406320%93.5(S) Dibromofluoromethane 08/17/11 61.2 131 NA1SW8260B NA 406320%92.1(S) Toluene-d8 08/17/11 75.1 127 NA1SW8260B NA 406320%90.1(S) 4-Bromofluorobenzene 08/17/11 64.1 120 NA1
Page 188 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:101204.22500 KirkhamB-11-GW
WaterSample Matrix:
Lab Sample ID: 1108073-036A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/17/11 406320x ug/L1300TPH(Gasoline) 08/17/11 22 50 342218260TPH 8/17/11 406320%83.2(S) 4-Bromofluorobenzene 08/17/11 34 114 34221
x - Does not match pattern of reference Gasoline standard. Result is elevated due to contribution from heavy end hydrocarbons (possibly aged gasoline) and non-fuel light hydrocarbons to the C5-C12 range quantified as Gasoline.
NOTE:
Page 189 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:101204.22500 KirkhamB-11-GW
WaterSample Matrix:
Lab Sample ID: 1108073-036B
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406321x mg/L0.35TPH as Diesel (SG) 08/17/11 0.0400 0.10 34021SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021SW8015B(M) 8/16/11 406321%82.1Pentacosane (S) 08/17/11 57.9 125 34021
x- Not typical of Diesel standard pattern (possibly fuel lighter than diesel)NOTE:
Page 190 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 12:101204.22500 KirkhamB-11-GW
WaterSample Matrix:
Lab Sample ID: 1108073-036C
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDArsenic (Dissolved) 08/15/11 0.005 0.009 33771SW6010B 8/12/11 406242mg/L0.047Barium (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/L0.0060Cobalt (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771SW6010B 8/12/11 406242mg/L0.030Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDNickel (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771SW6010B 8/12/11 406242mg/LNDSilver (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7470A 8/12/11 406238mg/LNDMercury 08/15/11 0.00005 0.0002 33651
Page 191 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:251204.22500 KirkhamB-9-GW
WaterSample Matrix:
Lab Sample ID: 1108073-037A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDDichlorodifluoromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDChloromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDVinyl Chloride 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromomethane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDTrichlorofluoromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDFreon 113 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDMethylene Chloride 08/17/11 0.18 5.0 NA1SW8260B NA 406320ug/LNDtrans-1,2-Dichloroethene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/L0.69MTBE 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDtert-Butanol 08/17/11 1.5 5.0 NA1SW8260B NA 406320ug/LNDDiisopropyl ether (DIPE) 08/17/11 0.36 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDETBE 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDcis-1,2-Dichloroethene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND2,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromochloromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LNDChloroform 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDCarbon Tetrachloride 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LND1,1,1-Trichloroethane 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloropropene 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDBenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDTAME 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDTrichloroethylene 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDDibromomethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromodichloromethane 08/17/11 0.23 0.50 NA1SW8260B NA 406320ug/LNDcis-1,3-Dichloropropene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LNDToluene 08/17/11 0.19 0.50 NA1SW8260B NA 406320ug/LNDTetrachloroethylene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LNDtrans-1,3-Dichloropropene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND1,1,2-Trichloroethane 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDDibromochloromethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichloropropane 08/17/11 0.18 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromoethane 08/17/11 0.19 0.50 NA1
Page 192 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:251204.22500 KirkhamB-9-GW
WaterSample Matrix:
Lab Sample ID: 1108073-037A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDChlorobenzene 08/17/11 0.14 0.50 NA1SW8260B NA 406320ug/LNDEthyl Benzene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LND1,1,1,2-Tetrachloroethane 08/17/11 0.10 0.50 NA1SW8260B NA 406320ug/LNDm,p-Xylene 08/17/11 0.20 1.0 NA1SW8260B NA 406320ug/LNDo-Xylene 08/17/11 0.13 0.50 NA1SW8260B NA 406320ug/LNDStyrene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDBromoform 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDIsopropyl Benzene 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDBromobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,1,2,2-Tetrachloroethane 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LNDn-Propylbenzene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LND2-Chlorotoluene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND1,3,5-Trimethylbenzene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND4-Chlorotoluene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LNDtert-Butylbenzene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LND1,2,3-Trichloropropane 08/17/11 0.59 1.0 NA1SW8260B NA 406320ug/LND1,2,4-Trimethylbenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDsec-Butyl Benzene 08/17/11 0.24 0.50 NA1SW8260B NA 406320ug/LNDp-Isopropyltoluene 08/17/11 0.25 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichlorobenzene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LND1,4-Dichlorobenzene 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDn-Butylbenzene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichlorobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromo-3-Chloropropane 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDHexachlorobutadiene 08/17/11 0.22 0.50 NA1SW8260B NA 406320ug/LND1,2,4-Trichlorobenzene 08/17/11 0.48 1.0 NA1SW8260B NA 406320ug/LNDNaphthalene 08/17/11 0.57 1.0 NA1SW8260B NA 406320ug/LND1,2,3-Trichlorobenzene 08/17/11 0.52 1.0 NA1SW8260B NA 406320%98.7(S) Dibromofluoromethane 08/17/11 61.2 131 NA1SW8260B NA 406320%92.2(S) Toluene-d8 08/17/11 75.1 127 NA1SW8260B NA 406320%91.2(S) 4-Bromofluorobenzene 08/17/11 64.1 120 NA1
Page 193 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:251204.22500 KirkhamB-9-GW
WaterSample Matrix:
Lab Sample ID: 1108073-037A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/17/11 406320ug/LNDTPH(Gasoline) 08/17/11 22 50 342218260TPH 8/17/11 406320%79.3(S) 4-Bromofluorobenzene 08/17/11 34 114 34221
Page 194 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:251204.22500 KirkhamB-9-GW
WaterSample Matrix:
Lab Sample ID: 1108073-037B
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021SW8015B(M) 8/16/11 406321%80.7Pentacosane (S) 08/17/11 57.9 125 34021
Page 195 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:251204.22500 KirkhamB-9-GW
WaterSample Matrix:
Lab Sample ID: 1108073-037C
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/L0.020Arsenic (Dissolved) 08/15/11 0.005 0.009 33771SW6010B 8/12/11 406242mg/L0.19Barium (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCobalt (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771SW6010B 8/12/11 406242mg/L0.016Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDNickel (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771SW6010B 8/12/11 406242mg/LNDSilver (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7470A 8/12/11 406238mg/LNDMercury 08/15/11 0.00005 0.0002 33651
Page 196 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 17:151204.22500 KirkhamB-13-GW
WaterSample Matrix:
Lab Sample ID: 1108073-038A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDDichlorodifluoromethane 08/17/11 0.48 0.60 NA1.19SW8260B NA 406320ug/LNDChloromethane 08/17/11 0.48 0.60 NA1.19SW8260B NA 406320ug/L1.1Vinyl Chloride 08/17/11 0.44 0.60 NA1.19SW8260B NA 406320ug/LNDBromomethane 08/17/11 0.45 0.60 NA1.19SW8260B NA 406320ug/LNDTrichlorofluoromethane 08/17/11 0.40 0.60 NA1.19SW8260B NA 406320ug/LND1,1-Dichloroethene 08/17/11 0.34 0.60 NA1.19SW8260B NA 406320ug/LNDFreon 113 08/17/11 0.45 0.60 NA1.19SW8260B NA 406320ug/LNDMethylene Chloride 08/17/11 0.21 6.0 NA1.19SW8260B NA 406320ug/L1.5trans-1,2-Dichloroethene 08/17/11 0.37 0.60 NA1.19SW8260B NA 406320ug/LNDMTBE 08/17/11 0.45 0.60 NA1.19SW8260B NA 406320ug/LNDtert-Butanol 08/17/11 1.8 6.0 NA1.19SW8260B NA 406320ug/LNDDiisopropyl ether (DIPE) 08/17/11 0.43 0.60 NA1.19SW8260B NA 406320ug/LND1,1-Dichloroethane 08/17/11 0.34 0.60 NA1.19SW8260B NA 406320ug/LNDETBE 08/17/11 0.47 0.60 NA1.19SW8260B NA 406320ug/L9.6cis-1,2-Dichloroethene 08/17/11 0.39 0.60 NA1.19SW8260B NA 406320ug/LND2,2-Dichloropropane 08/17/11 0.44 0.60 NA1.19SW8260B NA 406320ug/LNDBromochloromethane 08/17/11 0.41 0.60 NA1.19SW8260B NA 406320ug/L0.61Chloroform 08/17/11 0.35 0.60 NA1.19SW8260B NA 406320ug/LNDCarbon Tetrachloride 08/17/11 0.32 0.60 NA1.19SW8260B NA 406320ug/LND1,1,1-Trichloroethane 08/17/11 0.38 0.60 NA1.19SW8260B NA 406320ug/LND1,1-Dichloropropene 08/17/11 0.47 0.60 NA1.19SW8260B NA 406320ug/LNDBenzene 08/17/11 0.40 0.60 NA1.19SW8260B NA 406320ug/LNDTAME 08/17/11 0.38 0.60 NA1.19SW8260B NA 406320ug/LND1,2-Dichloroethane 08/17/11 0.33 0.60 NA1.19SW8260B NA 406320ug/L49Trichloroethylene 08/17/11 0.45 0.60 NA1.19SW8260B NA 406320ug/LNDDibromomethane 08/17/11 0.25 0.60 NA1.19SW8260B NA 406320ug/LND1,2-Dichloropropane 08/17/11 0.44 0.60 NA1.19SW8260B NA 406320ug/LNDBromodichloromethane 08/17/11 0.27 0.60 NA1.19SW8260B NA 406320ug/LNDcis-1,3-Dichloropropene 08/17/11 0.36 0.60 NA1.19SW8260B NA 406320ug/LNDToluene 08/17/11 0.23 0.60 NA1.19SW8260B NA 406320ug/L48Tetrachloroethylene 08/17/11 0.18 0.60 NA1.19SW8260B NA 406320ug/LNDtrans-1,3-Dichloropropene 08/17/11 0.24 0.60 NA1.19SW8260B NA 406320ug/LND1,1,2-Trichloroethane 08/17/11 0.24 0.60 NA1.19SW8260B NA 406320ug/LNDDibromochloromethane 08/17/11 0.26 0.60 NA1.19SW8260B NA 406320ug/LND1,3-Dichloropropane 08/17/11 0.21 0.60 NA1.19SW8260B NA 406320ug/LND1,2-Dibromoethane 08/17/11 0.23 0.60 NA1.19
Page 197 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 17:151204.22500 KirkhamB-13-GW
WaterSample Matrix:
Lab Sample ID: 1108073-038A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDChlorobenzene 08/17/11 0.17 0.60 NA1.19SW8260B NA 406320ug/LNDEthyl Benzene 08/17/11 0.18 0.60 NA1.19SW8260B NA 406320ug/LND1,1,1,2-Tetrachloroethane 08/17/11 0.12 0.60 NA1.19SW8260B NA 406320ug/LNDm,p-Xylene 08/17/11 0.24 1.2 NA1.19SW8260B NA 406320ug/LNDo-Xylene 08/17/11 0.15 0.60 NA1.19SW8260B NA 406320ug/LNDStyrene 08/17/11 0.24 0.60 NA1.19SW8260B NA 406320ug/LNDBromoform 08/17/11 0.54 1.2 NA1.19SW8260B NA 406320ug/LNDIsopropyl Benzene 08/17/11 0.34 0.60 NA1.19SW8260B NA 406320ug/LNDBromobenzene 08/17/11 0.46 0.60 NA1.19SW8260B NA 406320ug/LND1,1,2,2-Tetrachloroethane 08/17/11 0.30 0.60 NA1.19SW8260B NA 406320ug/LNDn-Propylbenzene 08/17/11 0.35 0.60 NA1.19SW8260B NA 406320ug/LND2-Chlorotoluene 08/17/11 0.39 0.60 NA1.19SW8260B NA 406320ug/LND1,3,5-Trimethylbenzene 08/17/11 0.24 0.60 NA1.19SW8260B NA 406320ug/LND4-Chlorotoluene 08/17/11 0.39 0.60 NA1.19SW8260B NA 406320ug/LNDtert-Butylbenzene 08/17/11 0.34 0.60 NA1.19SW8260B NA 406320ug/LND1,2,3-Trichloropropane 08/17/11 0.70 1.2 NA1.19SW8260B NA 406320ug/LND1,2,4-Trimethylbenzene 08/17/11 0.39 0.60 NA1.19SW8260B NA 406320ug/LNDsec-Butyl Benzene 08/17/11 0.29 0.60 NA1.19SW8260B NA 406320ug/LNDp-Isopropyltoluene 08/17/11 0.29 0.60 NA1.19SW8260B NA 406320ug/LND1,3-Dichlorobenzene 08/17/11 0.37 0.60 NA1.19SW8260B NA 406320ug/LND1,4-Dichlorobenzene 08/17/11 0.44 0.60 NA1.19SW8260B NA 406320ug/LNDn-Butylbenzene 08/17/11 0.38 0.60 NA1.19SW8260B NA 406320ug/LND1,2-Dichlorobenzene 08/17/11 0.47 0.60 NA1.19SW8260B NA 406320ug/LND1,2-Dibromo-3-Chloropropane 08/17/11 0.53 1.2 NA1.19SW8260B NA 406320ug/LNDHexachlorobutadiene 08/17/11 0.26 0.60 NA1.19SW8260B NA 406320ug/LND1,2,4-Trichlorobenzene 08/17/11 0.58 1.2 NA1.19SW8260B NA 406320ug/LNDNaphthalene 08/17/11 0.68 1.2 NA1.19SW8260B NA 406320ug/LND1,2,3-Trichlorobenzene 08/17/11 0.62 1.2 NA1.19SW8260B NA 406320%92.7(S) Dibromofluoromethane 08/17/11 61.2 131 NA1.19SW8260B NA 406320%90.9(S) Toluene-d8 08/17/11 75.1 127 NA1.19SW8260B NA 406320%89.0(S) 4-Bromofluorobenzene 08/17/11 64.1 120 NA1.19
Reporting limits were raised due to sediment in all VOAs.NOTE:
Page 198 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 17:151204.22500 KirkhamB-13-GW
WaterSample Matrix:
Lab Sample ID: 1108073-038A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. 8260TPH 8/17/11 406320J ug/L51TPH(Gasoline) 08/17/11 26 60 34221.198260TPH 8/17/11 406320%74.1(S) 4-Bromofluorobenzene 08/17/11 34 114 34221.19
Raised reporting limit - see comment for 8260B analysis.NOTE:
Page 199 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 17:151204.22500 KirkhamB-13-GW
WaterSample Matrix:
Lab Sample ID: 1108073-038B
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021SW8015B(M) 8/16/11 406321%82.7Pentacosane (S) 08/17/11 57.9 125 34021
Page 200 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 17:151204.22500 KirkhamB-13-GW
WaterSample Matrix:
Lab Sample ID: 1108073-038C
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDArsenic (Dissolved) 08/15/11 0.005 0.009 33771SW6010B 8/12/11 406242mg/L0.091Barium (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/L0.0095Cobalt (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771SW6010B 8/12/11 406242mg/L0.043Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/L0.020Nickel (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771SW6010B 8/12/11 406242mg/L0.0056Silver (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7470A 8/12/11 406238mg/LNDMercury 08/15/11 0.00005 0.0002 33651
Page 201 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:551204.22500 KirkhamB-5-GW
WaterSample Matrix:
Lab Sample ID: 1108073-039A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDDichlorodifluoromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDChloromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDVinyl Chloride 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromomethane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDTrichlorofluoromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDFreon 113 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDMethylene Chloride 08/17/11 0.18 5.0 NA1SW8260B NA 406320ug/LNDtrans-1,2-Dichloroethene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LNDMTBE 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDtert-Butanol 08/17/11 1.5 5.0 NA1SW8260B NA 406320ug/LNDDiisopropyl ether (DIPE) 08/17/11 0.36 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDETBE 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDcis-1,2-Dichloroethene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND2,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromochloromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LNDChloroform 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDCarbon Tetrachloride 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LND1,1,1-Trichloroethane 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloropropene 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDBenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDTAME 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDTrichloroethylene 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDDibromomethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromodichloromethane 08/17/11 0.23 0.50 NA1SW8260B NA 406320ug/LNDcis-1,3-Dichloropropene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LNDToluene 08/17/11 0.19 0.50 NA1SW8260B NA 406320ug/LNDTetrachloroethylene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LNDtrans-1,3-Dichloropropene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND1,1,2-Trichloroethane 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDDibromochloromethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichloropropane 08/17/11 0.18 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromoethane 08/17/11 0.19 0.50 NA1
Page 202 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:551204.22500 KirkhamB-5-GW
WaterSample Matrix:
Lab Sample ID: 1108073-039A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDChlorobenzene 08/17/11 0.14 0.50 NA1SW8260B NA 406320ug/LNDEthyl Benzene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LND1,1,1,2-Tetrachloroethane 08/17/11 0.10 0.50 NA1SW8260B NA 406320ug/LNDm,p-Xylene 08/17/11 0.20 1.0 NA1SW8260B NA 406320ug/LNDo-Xylene 08/17/11 0.13 0.50 NA1SW8260B NA 406320ug/LNDStyrene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDBromoform 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDIsopropyl Benzene 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDBromobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,1,2,2-Tetrachloroethane 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LNDn-Propylbenzene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LND2-Chlorotoluene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND1,3,5-Trimethylbenzene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND4-Chlorotoluene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LNDtert-Butylbenzene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LND1,2,3-Trichloropropane 08/17/11 0.59 1.0 NA1SW8260B NA 406320ug/LND1,2,4-Trimethylbenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDsec-Butyl Benzene 08/17/11 0.24 0.50 NA1SW8260B NA 406320ug/LNDp-Isopropyltoluene 08/17/11 0.25 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichlorobenzene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LND1,4-Dichlorobenzene 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDn-Butylbenzene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichlorobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromo-3-Chloropropane 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDHexachlorobutadiene 08/17/11 0.22 0.50 NA1SW8260B NA 406320ug/LND1,2,4-Trichlorobenzene 08/17/11 0.48 1.0 NA1SW8260B NA 406320ug/LNDNaphthalene 08/17/11 0.57 1.0 NA1SW8260B NA 406320ug/LND1,2,3-Trichlorobenzene 08/17/11 0.52 1.0 NA1SW8260B NA 406320%97.7(S) Dibromofluoromethane 08/17/11 61.2 131 NA1SW8260B NA 406320%91.5(S) Toluene-d8 08/17/11 75.1 127 NA1SW8260B NA 406320%90.2(S) 4-Bromofluorobenzene 08/17/11 64.1 120 NA1
Page 203 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:551204.22500 KirkhamB-5-GW
WaterSample Matrix:
Lab Sample ID: 1108073-039A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/17/11 406320ug/LNDTPH(Gasoline) 08/17/11 22 50 342218260TPH 8/17/11 406320%75.5(S) 4-Bromofluorobenzene 08/17/11 34 114 34221
Page 204 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:551204.22500 KirkhamB-5-GW
WaterSample Matrix:
Lab Sample ID: 1108073-039B
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021SW8015B(M) 8/16/11 406321%75.2Pentacosane (S) 08/17/11 57.9 125 34021
Page 205 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:551204.22500 KirkhamB-5-GW
WaterSample Matrix:
Lab Sample ID: 1108073-039C
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDArsenic (Dissolved) 08/15/11 0.005 0.009 33771SW6010B 8/12/11 406242mg/L0.030Barium (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/L0.023Cobalt (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771SW6010B 8/12/11 406242mg/L0.023Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/L0.033Nickel (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771SW6010B 8/12/11 406242mg/L0.0054Silver (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7470A 8/12/11 406238mg/LNDMercury 08/15/11 0.00005 0.0002 33651
Page 206 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:451204.22500 KirkhamEquip BLANK
WaterSample Matrix:
Lab Sample ID: 1108073-040A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDDichlorodifluoromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDChloromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDVinyl Chloride 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromomethane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDTrichlorofluoromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDFreon 113 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDMethylene Chloride 08/17/11 0.18 5.0 NA1SW8260B NA 406320ug/LNDtrans-1,2-Dichloroethene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LNDMTBE 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDtert-Butanol 08/17/11 1.5 5.0 NA1SW8260B NA 406320ug/LNDDiisopropyl ether (DIPE) 08/17/11 0.36 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDETBE 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDcis-1,2-Dichloroethene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND2,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromochloromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LNDChloroform 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDCarbon Tetrachloride 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LND1,1,1-Trichloroethane 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloropropene 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDBenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDTAME 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDTrichloroethylene 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDDibromomethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromodichloromethane 08/17/11 0.23 0.50 NA1SW8260B NA 406320ug/LNDcis-1,3-Dichloropropene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LNDToluene 08/17/11 0.19 0.50 NA1SW8260B NA 406320ug/LNDTetrachloroethylene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LNDtrans-1,3-Dichloropropene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND1,1,2-Trichloroethane 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDDibromochloromethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichloropropane 08/17/11 0.18 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromoethane 08/17/11 0.19 0.50 NA1
Page 207 of 260Total Page Count: 260
SAMPLE RESULTS
Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/10/11 / 16:451204.22500 KirkhamEquip BLANK
WaterSample Matrix:
Lab Sample ID: 1108073-040A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406320ug/LNDChlorobenzene 08/17/11 0.14 0.50 NA1SW8260B NA 406320ug/LNDEthyl Benzene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LND1,1,1,2-Tetrachloroethane 08/17/11 0.10 0.50 NA1SW8260B NA 406320ug/LNDm,p-Xylene 08/17/11 0.20 1.0 NA1SW8260B NA 406320ug/LNDo-Xylene 08/17/11 0.13 0.50 NA1SW8260B NA 406320ug/LNDStyrene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDBromoform 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDIsopropyl Benzene 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDBromobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,1,2,2-Tetrachloroethane 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LNDn-Propylbenzene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LND2-Chlorotoluene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND1,3,5-Trimethylbenzene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND4-Chlorotoluene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LNDtert-Butylbenzene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LND1,2,3-Trichloropropane 08/17/11 0.59 1.0 NA1SW8260B NA 406320ug/LND1,2,4-Trimethylbenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDsec-Butyl Benzene 08/17/11 0.24 0.50 NA1SW8260B NA 406320ug/LNDp-Isopropyltoluene 08/17/11 0.25 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichlorobenzene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LND1,4-Dichlorobenzene 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDn-Butylbenzene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichlorobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromo-3-Chloropropane 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDHexachlorobutadiene 08/17/11 0.22 0.50 NA1SW8260B NA 406320ug/LND1,2,4-Trichlorobenzene 08/17/11 0.48 1.0 NA1SW8260B NA 406320ug/LNDNaphthalene 08/17/11 0.57 1.0 NA1SW8260B NA 406320ug/LND1,2,3-Trichlorobenzene 08/17/11 0.52 1.0 NA1SW8260B NA 406320%88.9(S) Dibromofluoromethane 08/17/11 61.2 131 NA1SW8260B NA 406320%92.3(S) Toluene-d8 08/17/11 75.1 127 NA1SW8260B NA 406320%89.7(S) 4-Bromofluorobenzene 08/17/11 64.1 120 NA1
Page 208 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW7470AAnalytical Method:
Prep Date:
Analyzed Date:
08/12/11 Prep Batch:
Analytical Batch:
406238
mg/L
08/15/11
33657470A1108073Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.00005 0.0002Mercury 0.00007
Work Order:
Matrix:
Units:
Prep Method:
SW8270CAnalytical Method:
Prep Date:
Analyzed Date:
08/14/11 Prep Batch:
Analytical Batch:
406315
mg/Kg
08/15/11
33743545_BNA1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.660 0.653Pyridine ND0.110 0.330N-Nitrosdimethylamine ND0.123 0.330Aniline ND0.129 0.330Phenol ND0.0683 0.330Bis(2-chloroethyl) ether ND0.129 0.3302-Chlorophenol ND
0.0733 0.3301,3-Dichlorobenzene ND0.0663 6.591,4-Dichlorobenzene ND0.104 0.330Benzyl Alcohol ND
0.0713 0.3301,2-Dichlorobenzene ND0.116 0.3302-Methylphenol (o-Cresol) ND0.0683 0.330Bis(2-chloroisopropyl)ether ND0.139 0.3303-/4-Methylphenol (p-/m-Cresol) ND0.0931 0.330N-nitroso-di-n-propylamine ND0.0465 0.330Hexachloroethane ND0.0528 0.330Nitrobenzene ND0.0574 0.653Isophorone ND0.0525 0.6532-Nitrophenol ND0.133 6.592,4-Dimethylphenol ND5.59 0.330Benzoic Acid ND
0.0584 0.330Bis(2-Chloroethoxy)methane ND0.104 0.3302,4-Dichlorophenol ND0.0733 0.3301,2,4-Trichlorobenzene ND0.104 0.3302,6-Dichlorophenol ND0.0901 0.330Naphthalene ND0.0990 0.3304-Chloroaniline ND0.0653 0.330Hexachloro-1,3-butadiene ND0.102 0.3304-Chloro-3-methylphenol ND0.0792 0.3302-Methylnaphthalene ND0.0792 0.3301-Methylnaphthalene ND0.0277 0.330Hexachlorocyclopentadiene ND
Page 209 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8270CAnalytical Method:
Prep Date:
Analyzed Date:
08/14/11 Prep Batch:
Analytical Batch:
406315
mg/Kg
08/15/11
33743545_BNA1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0950 0.3302,4,6-Trichlorophenol ND0.121 0.3302,4,5-Trichlorophenol ND
0.0594 3.272-Chloronaphthalene ND0.0693 0.3302-Nitroaniline ND0.118 0.330Dimethyl phthalate ND0.106 0.3301,3-Dinitrobenzene ND
0.0851 0.330Acenaphthylene ND0.0267 0.3302,6-Dinitrotoluene ND0.0858 0.3301,2-Dinitrobenzene ND0.0693 0.3303-Nitroaniline ND0.0960 0.330Acenaphthene ND0.0297 3.272,4-Dinitrophenol ND0.0663 0.3304-Nitrophenol ND0.0782 0.330Dibenzofuran ND0.0267 0.3302,4-Dinitrotoluene ND0.119 0.3302,3,5,6-Tetrachlorophenol ND0.119 0.3302,3,4,6-Tetrachlorophenol ND0.117 0.330Diethylphthalate ND0.0990 0.330Fluorene ND0.0802 0.3304-Chlorophenyl phenyl ether ND0.0802 0.3304-Nitroaniline ND0.0663 0.3304,6-Dinitro-2-methylphenol ND0.0663 0.330Diphenylamine ND0.109 0.330Azobenzene ND
0.0812 3.274-Bromophenyl phenyl ether ND0.101 0.330Hexachlorobenzene ND0.102 3.27Pentachlorophenol ND0.142 0.330Phenanthrene ND0.132 0.330Anthracene ND0.132 0.330Carbazole ND0.108 1.68Di-n-butylphthalate ND0.132 0.653Fluoranthene ND0.374 3.27Benzidine ND0.147 0.330Pyrene ND0.0891 0.330Benzyl butyl phthalate ND0.149 0.330Benz[a]anthracene ND0.152 0.3303,3'-Dichlorobenzidine ND0.176 0.330Chrysene ND
0.0832 0.330Bis(2-Ethylhexyl)phthalate ND0.138 0.330Di-n-octyl phthalate ND0.133 0.330Benzo[b]fluoranthene ND
Page 210 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8270CAnalytical Method:
Prep Date:
Analyzed Date:
08/14/11 Prep Batch:
Analytical Batch:
406315
mg/Kg
08/15/11
33743545_BNA1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.169 0.330Benzo[k]fluoranthene ND0.135 0.330Benzo[a]pyrene ND0.131 0.330Indeno[1,2,3-cd]pyrene ND0.151 0.330Dibenz[a,h]anthracene ND0.150 0.330Benzo[g,h,i]perylene ND0.150 0.3301,4-Dinitrobenzene ND
2,4,6-Tribromophenol (S) 33.52-Fluorobiphenyl (S) 52.02-Fluorophenol (S) 55.2Nitrobenzene-d5 (S) 50.7Phenol-d6 (S) 60.4p-Terphenyl-d14 (S) 85.4
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/12/11 Prep Batch:
Analytical Batch:
406242
mg/Kg
08/15/11
337730051108073Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.004 0.009Antimony (Dissolved) ND0.005 0.009Arsenic (Dissolved) ND0.002 0.009Barium (Dissolved) ND0.002 0.005Beryllium (Dissolved) ND0.001 0.005Cadmium (Dissolved) ND0.002 0.005Chromium (Dissolved) ND0.002 0.005Cobalt (Dissolved) ND0.003 0.009Copper (Dissolved) 0.003570.005 0.014Lead (Dissolved) ND0.002 0.009Molybdenum (Dissolved) ND0.002 0.009Nickel (Dissolved) ND0.004 0.02Selenium (Dissolved) ND0.002 0.005Silver (Dissolved) ND0.004 0.009Thallium (dissolved) ND0.004 0.009Vanadium (Dissolved) ND0.002 0.009Zinc (dissolved) ND
Page 211 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8270CAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406316
mg/Kg
08/16/11
33853545_BNA1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.660 0.653Pyridine ND0.110 0.330N-Nitrosdimethylamine ND0.123 0.330Aniline ND0.129 0.330Phenol ND0.0683 0.330Bis(2-chloroethyl) ether ND0.129 0.3302-Chlorophenol ND
0.0733 0.3301,3-Dichlorobenzene ND0.0663 6.591,4-Dichlorobenzene ND0.104 0.330Benzyl Alcohol ND
0.0713 0.3301,2-Dichlorobenzene ND0.116 0.3302-Methylphenol (o-Cresol) ND0.0683 0.330Bis(2-chloroisopropyl)ether ND0.139 0.3303-/4-Methylphenol (p-/m-Cresol) ND0.0931 0.330N-nitroso-di-n-propylamine ND0.0465 0.330Hexachloroethane ND0.0528 0.330Nitrobenzene ND0.0574 0.653Isophorone ND0.0525 0.6532-Nitrophenol ND0.133 6.592,4-Dimethylphenol ND5.59 0.330Benzoic Acid ND
0.0584 0.330Bis(2-Chloroethoxy)methane ND0.104 0.3302,4-Dichlorophenol ND0.0733 0.3301,2,4-Trichlorobenzene ND0.104 0.3302,6-Dichlorophenol ND0.0901 0.330Naphthalene ND0.0990 0.3304-Chloroaniline ND0.0653 0.330Hexachloro-1,3-butadiene ND0.102 0.3304-Chloro-3-methylphenol ND0.0792 0.3302-Methylnaphthalene ND0.0792 0.3301-Methylnaphthalene ND0.0277 0.330Hexachlorocyclopentadiene ND0.0950 0.3302,4,6-Trichlorophenol ND0.121 0.3302,4,5-Trichlorophenol ND
0.0594 3.272-Chloronaphthalene ND0.0693 0.3302-Nitroaniline ND0.118 0.330Dimethyl phthalate ND0.106 0.3301,3-Dinitrobenzene ND
0.0851 0.330Acenaphthylene ND0.0267 0.3302,6-Dinitrotoluene ND0.0858 0.3301,2-Dinitrobenzene ND0.0693 0.3303-Nitroaniline ND
Page 212 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8270CAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406316
mg/Kg
08/16/11
33853545_BNA1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0960 0.330Acenaphthene ND0.0297 3.272,4-Dinitrophenol ND0.0663 0.3304-Nitrophenol ND0.0782 0.330Dibenzofuran ND0.0267 0.3302,4-Dinitrotoluene ND0.119 0.3302,3,5,6-Tetrachlorophenol ND0.119 0.3302,3,4,6-Tetrachlorophenol ND0.117 0.330Diethylphthalate ND0.0990 0.330Fluorene ND0.0802 0.3304-Chlorophenyl phenyl ether ND0.0802 0.3304-Nitroaniline ND0.0663 0.3304,6-Dinitro-2-methylphenol ND0.0663 0.330Diphenylamine ND0.109 0.330Azobenzene ND
0.0812 3.274-Bromophenyl phenyl ether ND0.101 0.330Hexachlorobenzene ND0.102 3.27Pentachlorophenol ND0.142 0.330Phenanthrene ND0.132 0.330Anthracene ND0.132 0.330Carbazole ND0.108 1.68Di-n-butylphthalate ND0.132 0.653Fluoranthene ND0.374 3.27Benzidine ND0.147 0.330Pyrene ND0.0891 0.330Benzyl butyl phthalate ND0.149 0.330Benz[a]anthracene ND0.152 0.3303,3'-Dichlorobenzidine ND0.176 0.330Chrysene ND
0.0832 0.330Bis(2-Ethylhexyl)phthalate ND0.138 0.330Di-n-octyl phthalate ND0.133 0.330Benzo[b]fluoranthene ND0.169 0.330Benzo[k]fluoranthene ND0.135 0.330Benzo[a]pyrene ND0.131 0.330Indeno[1,2,3-cd]pyrene ND0.151 0.330Dibenz[a,h]anthracene ND0.150 0.330Benzo[g,h,i]perylene ND0.150 0.3301,4-Dinitrobenzene ND
2,4,6-Tribromophenol (S) 33.32-Fluorobiphenyl (S) 46.72-Fluorophenol (S) 59.8Nitrobenzene-d5 (S) 48.5
Page 213 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8270CAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406316
mg/Kg
08/16/11
33853545_BNA1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
Phenol-d6 (S) 60.6p-Terphenyl-d14 (S) 89.6
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406266
mg/Kg
08/16/11
338830501108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.20 5.0Antimony 0.350.28 1.7Arsenic 0.28
1 5.0Barium 1.10.0840 2.0Beryllium ND0.059 1.0Cadmium ND0.059 5.0Chromium 0.330.14 5.0Cobalt ND
0.090 5.0Copper 0.180.043 1.0Lead 0.340.059 5.0Molybdenum 0.120.059 5.0Nickel 0.150.29 5.0Selenium ND1.0 1.0Silver ND0.12 5.0Thallium ND0.12 5.0Vanadium 0.140.59 5.0Zinc 0.88
Page 214 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406267
mg/Kg
08/16/11
338930501108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.20 5.0Antimony 0.350.28 1.7Arsenic 0.28
1 5.0Barium 1.10.0840 2.0Beryllium ND0.059 1.0Cadmium ND0.059 5.0Chromium 0.330.14 5.0Cobalt ND
0.090 5.0Copper 0.180.043 1.0Lead 0.340.059 5.0Molybdenum 0.120.059 5.0Nickel 0.150.29 5.0Selenium ND1.0 1.0Silver ND0.12 5.0Thallium ND0.12 5.0Vanadium 0.140.59 5.0Zinc 0.88
Work Order:
Matrix:
Units:
Prep Method:
7471ABAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406269
mg/Kg
08/16/11
339274711108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.01 0.10Mercury ND
Work Order:
Matrix:
Units:
Prep Method:
7471ABAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406270
mg/Kg
08/16/11
339374711108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.01 0.10Mercury ND
Page 215 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
406298
mg/Kg
08/16/11
33983545_TPH1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.758 2.0TPH as Diesel 1.41.78 4.0TPH as Motor Oil 2.5
Pentacosane (S) 110
Work Order:
Matrix:
Units:
Prep Method:
SW8082Analytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
406324
mg/Kg
08/17/11
34003545_PCB1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0230 0.10Aroclor1016 ND0.0920 0.20Aroclor1221 ND0.0460 0.10Aroclor1232 ND0.0430 0.10Aroclor1242 ND0.0360 0.10Aroclor1248 ND0.0240 0.10Aroclor1254 ND0.0270 0.10Aroclor1260 ND
TCMX (S) 74.9DCBP (S) 71.6
Page 216 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8081AAnalytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
406314
ug/Kg
08/16/11
34013545_OCP1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.44 2.0alpha-BHC ND0.40 2.0gamma-BHC ND0.36 2.0beta-BHC ND0.49 2.0delta-BHC ND1.1 2.0Heptachlor ND0.44 2.0Aldrin ND0.32 2.0Heptachlor epoxide ND0.42 2.0gamma-Chlordane ND0.36 2.0alpha-Chlordane ND0.59 2.0Endosulfan I ND0.48 2.04,4'-DDE ND0.43 2.0Dieldrin ND0.57 2.0Endrin ND0.47 2.04,4'-DDD ND1.5 2.0Endosulfan II ND0.81 2.04,4'-DDT ND1.0 2.0Endrin aldehyde ND0.49 2.0Endosulfan sulfate ND0.62 5.0Methoxychlor ND0.40 2.0Endrin Ketone ND10 20Chlordane ND10 100Toxaphene ND
TCMX (S) 86.4DCBP (S) 77.1
Page 217 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8081AAnalytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
406314
ug/Kg
08/16/11
34013545_OCP1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.44 2.0alpha-BHC ND0.40 2.0gamma-BHC ND0.36 2.0beta-BHC ND0.49 2.0delta-BHC ND1.1 2.0Heptachlor ND0.44 2.0Aldrin ND0.32 2.0Heptachlor epoxide ND0.42 2.0gamma-Chlordane ND0.36 2.0alpha-Chlordane ND0.59 2.0Endosulfan I ND0.48 2.04,4'-DDE ND0.43 2.0Dieldrin ND0.57 2.0Endrin ND0.47 2.04,4'-DDD ND1.5 2.0Endosulfan II ND0.81 2.04,4'-DDT ND1.0 2.0Endrin aldehyde ND0.49 2.0Endosulfan sulfate ND0.62 5.0Methoxychlor ND0.40 2.0Endrin Ketone ND10 20Chlordane ND10 100Toxaphene ND
TCMX (S) 76.8DCBP (S) 72.8
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
406321
mg/L
08/17/11
34023510_TPHSG1108073Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0440 0.10TPH as Diesel (SG) ND0.0920 0.20TPH as Motor Oil (SG) ND
Pentacosane (S) 51.7 S
Page 218 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
406321
mg/L
08/17/11
34023510_TPHSG1108073Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0440 0.10TPH as Diesel (SG) ND0.0920 0.20TPH as Motor Oil (SG) 0.13
Pentacosane (S) 75.1
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406301
ug/Kg
08/15/11
341350351108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
17 100TPH(Gasoline) ND(S) 4-Bromofluorobenzene 97.7
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/18/11 Prep Batch:
Analytical Batch:
406325
mg/Kg
08/18/11
34183545_TPH1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.758 2.0TPH as Diesel 1.21.78 4.0TPH as Motor Oil 3.3
Pentacosane (S) 111
Page 219 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8082Analytical Method:
Prep Date:
Analyzed Date:
08/18/11 Prep Batch:
Analytical Batch:
406326
mg/Kg
08/18/11
34193545_PCB1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0230 0.10Aroclor1016 ND0.0920 0.20Aroclor1221 ND0.0460 0.10Aroclor1232 ND0.0430 0.10Aroclor1242 ND0.0360 0.10Aroclor1248 ND0.0240 0.10Aroclor1254 ND0.0270 0.10Aroclor1260 ND
TCMX (S) 99.1DCBP (S) 113
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/17/11 Prep Batch:
Analytical Batch:
406320
ug/L
08/17/11
342250301108073Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
22 50TPH(Gasoline) ND(S) 4-Bromofluorobenzene 79.7
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406328
ug/Kg
08/15/11
342550351108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
17 100TPH(Gasoline) ND(S) 4-Bromofluorobenzene 68.9
Page 220 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/18/11 Prep Batch:
Analytical Batch:
406330
ug/Kg
08/18/11
342750351108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
17 100TPH(Gasoline) ND(S) 4-Bromofluorobenzene 87.2
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/24/11 Prep Batch:
Analytical Batch:
406411
ug/Kg
08/24/11
348050351108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
17 100TPH(Gasoline) ND(S) 4-Bromofluorobenzene 83.4
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/25/11 Prep Batch:
Analytical Batch:
406447
mg/Kg
08/26/11
3496WET/3010B1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0500 0.10Lead (STLC) ND
Page 221 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
406301
ug/Kg
08/15/11
NANA1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
4.4 10Dichlorodifluoromethane ND4.6 10Chloromethane ND2.6 10Vinyl Chloride ND4.7 10Bromomethane ND2.9 10Trichlorofluoromethane ND1.5 101,1-Dichloroethene ND3.7 10Freon 113 ND2.0 50Methylene Chloride ND1.1 10trans-1,2-Dichloroethene ND2.6 10MTBE ND21 50tert-Butanol ND2.2 10Diisopropyl ether (DIPE) ND1.3 101,1-Dichloroethane ND2.4 10ETBE ND1.8 10cis-1,2-Dichloroethene ND1.2 102,2-Dichloropropane ND2.3 10Bromochloromethane ND1.2 10Chloroform ND1.6 10Carbon Tetrachloride ND1.2 101,1,1-Trichloroethane ND1.4 101,1-Dichloropropene ND1.5 10Benzene ND2.1 10TAME ND1.9 101,2-Dichloroethane ND3.9 10Trichloroethylene ND2.2 10Dibromomethane ND1.3 101,2-Dichloropropane ND1.1 10Bromodichloromethane ND1.4 10cis-1,3-Dichloropropene ND0.98 10Toluene ND1.8 10Tetrachloroethylene ND1.2 10trans-1,3-Dichloropropene ND1.8 101,1,2-Trichloroethane ND1.1 10Dibromochloromethane ND2.1 101,3-Dichloropropane ND1.7 101,2-Dibromoethane ND0.86 10Ethyl Benzene ND4.2 10Chlorobenzene ND0.86 101,1,1,2-Tetrachloroethane ND1.9 10m,p-Xylene ND0.66 5.0o-Xylene ND
Page 222 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
406301
ug/Kg
08/15/11
NANA1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.77 10Styrene ND1.9 10Bromoform ND1.2 10Isopropyl Benzene ND1.4 10n-Propylbenzene ND1.2 10Bromobenzene ND3.0 101,1,2,2-Tetrachloroethane ND1.1 101,3,5-Trimethylbenzene ND3.3 101,2,3-Trichloropropane ND1.6 104-Chlorotoluene ND1.6 102-Chlorotoluene ND1.4 10tert-Butylbenzene ND1.1 101,2,4-Trimethylbenzene ND1.6 10sec-Butyl Benzene ND1.5 10p-Isopropyltoluene ND1.8 101,3-Dichlorobenzene ND1.5 101,4-Dichlorobenzene ND2.2 10n-Butylbenzene ND1.3 101,2-Dichlorobenzene ND4.2 101,2-Dibromo-3-Chloropropane ND2.6 10Hexachlorobutadiene ND2.1 101,2,4-Trichlorobenzene ND2.8 10Naphthalene ND2.9 101,2,3-Trichlorobenzene ND
(S) Dibromofluoromethane 77.1(S) Toluene-d8 82.7(S) 4-Bromofluorobenzene 89.9
Page 223 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
406320
ug/L
08/17/11
NANA1108073Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.41 0.50Dichlorodifluoromethane ND0.41 0.50Chloromethane ND0.37 0.50Vinyl Chloride ND0.37 0.50Bromomethane ND0.34 0.50Trichlorofluoromethane ND0.29 0.501,1-Dichloroethene ND0.38 0.50Freon 113 ND0.18 5.0Methylene Chloride ND0.31 0.50trans-1,2-Dichloroethene ND0.38 0.50MTBE ND1.5 5.0tert-Butanol ND0.36 0.50Diisopropyl ether (DIPE) ND0.28 0.501,1-Dichloroethane ND0.40 0.50ETBE ND0.33 0.50cis-1,2-Dichloroethene ND0.37 0.502,2-Dichloropropane ND0.34 0.50Bromochloromethane ND0.29 0.50Chloroform ND0.26 0.50Carbon Tetrachloride ND0.32 0.501,1,1-Trichloroethane ND0.40 0.501,1-Dichloropropene ND0.33 0.50Benzene ND0.32 0.50TAME ND0.28 0.501,2-Dichloroethane ND0.38 0.50Trichloroethylene ND0.21 0.50Dibromomethane ND0.37 0.501,2-Dichloropropane ND0.23 0.50Bromodichloromethane ND0.30 0.50cis-1,3-Dichloropropene ND0.19 0.50Toluene ND0.15 0.50Tetrachloroethylene ND0.20 0.50trans-1,3-Dichloropropene ND0.20 0.501,1,2-Trichloroethane ND0.21 0.50Dibromochloromethane ND0.18 0.501,3-Dichloropropane ND0.19 0.501,2-Dibromoethane ND0.14 0.50Chlorobenzene ND0.15 0.50Ethyl Benzene ND0.10 0.501,1,1,2-Tetrachloroethane ND0.20 1.0m,p-Xylene ND0.13 0.50o-Xylene ND
Page 224 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
406320
ug/L
08/17/11
NANA1108073Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.20 0.50Styrene ND0.45 1.0Bromoform ND0.28 0.50Isopropyl Benzene ND0.39 0.50Bromobenzene ND0.26 0.501,1,2,2-Tetrachloroethane ND0.30 0.50n-Propylbenzene ND0.33 0.502-Chlorotoluene ND0.20 0.501,3,5-Trimethylbenzene ND0.32 0.504-Chlorotoluene ND0.29 0.50tert-Butylbenzene ND0.59 1.01,2,3-Trichloropropane ND0.33 0.501,2,4-Trimethylbenzene ND0.24 0.50sec-Butyl Benzene ND0.25 0.50p-Isopropyltoluene ND0.31 0.501,3-Dichlorobenzene ND0.37 0.501,4-Dichlorobenzene ND0.32 0.50n-Butylbenzene ND0.39 0.501,2-Dichlorobenzene ND0.45 1.01,2-Dibromo-3-Chloropropane ND0.22 0.50Hexachlorobutadiene ND0.48 1.01,2,4-Trichlorobenzene ND0.57 1.0Naphthalene ND0.52 1.01,2,3-Trichlorobenzene ND100 100Ethanol ND TIC
(S) Dibromofluoromethane 91.8(S) Toluene-d8 91.7(S) 4-Bromofluorobenzene 91.3
Page 225 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
406328
ug/Kg
08/15/11
NANA1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
4.4 10Dichlorodifluoromethane ND4.6 10Chloromethane ND2.6 10Vinyl Chloride ND4.7 10Bromomethane ND2.9 10Trichlorofluoromethane ND1.5 101,1-Dichloroethene ND3.7 10Freon 113 ND2.0 50Methylene Chloride ND1.1 10trans-1,2-Dichloroethene ND2.6 10MTBE ND21 50tert-Butanol ND2.2 10Diisopropyl ether (DIPE) ND1.3 101,1-Dichloroethane ND2.4 10ETBE ND1.8 10cis-1,2-Dichloroethene ND1.2 102,2-Dichloropropane ND2.3 10Bromochloromethane ND1.2 10Chloroform ND1.6 10Carbon Tetrachloride ND1.2 101,1,1-Trichloroethane ND1.4 101,1-Dichloropropene ND1.5 10Benzene ND2.1 10TAME ND1.9 101,2-Dichloroethane ND3.9 10Trichloroethylene ND2.2 10Dibromomethane ND1.3 101,2-Dichloropropane ND1.1 10Bromodichloromethane ND1.4 10cis-1,3-Dichloropropene ND0.98 10Toluene ND1.8 10Tetrachloroethylene ND1.2 10trans-1,3-Dichloropropene ND1.8 101,1,2-Trichloroethane ND1.1 10Dibromochloromethane ND2.1 101,3-Dichloropropane ND1.7 101,2-Dibromoethane ND0.86 10Ethyl Benzene ND4.2 10Chlorobenzene ND0.86 101,1,1,2-Tetrachloroethane ND1.9 10m,p-Xylene ND0.66 5.0o-Xylene ND
Page 226 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
406328
ug/Kg
08/15/11
NANA1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.77 10Styrene ND1.9 10Bromoform ND1.2 10Isopropyl Benzene ND1.4 10n-Propylbenzene ND1.2 10Bromobenzene ND3.0 101,1,2,2-Tetrachloroethane ND1.1 101,3,5-Trimethylbenzene ND3.3 101,2,3-Trichloropropane ND1.6 104-Chlorotoluene ND1.6 102-Chlorotoluene ND1.4 10tert-Butylbenzene ND1.1 101,2,4-Trimethylbenzene ND1.6 10sec-Butyl Benzene ND1.5 10p-Isopropyltoluene ND1.8 101,3-Dichlorobenzene ND1.5 101,4-Dichlorobenzene ND2.2 10n-Butylbenzene ND1.3 101,2-Dichlorobenzene ND4.2 101,2-Dibromo-3-Chloropropane ND2.6 10Hexachlorobutadiene ND2.1 101,2,4-Trichlorobenzene ND2.8 10Naphthalene ND2.9 101,2,3-Trichlorobenzene ND
(S) Dibromofluoromethane 73.3(S) Toluene-d8 89.0(S) 4-Bromofluorobenzene 90.7
Page 227 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
406330
ug/Kg
08/18/11
NANA1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
4.4 10Dichlorodifluoromethane ND4.6 10Chloromethane ND2.6 10Vinyl Chloride ND4.7 10Bromomethane ND2.9 10Trichlorofluoromethane ND1.5 101,1-Dichloroethene ND3.7 10Freon 113 ND2.0 50Methylene Chloride ND1.1 10trans-1,2-Dichloroethene ND2.6 10MTBE ND21 50tert-Butanol ND2.2 10Diisopropyl ether (DIPE) ND1.3 101,1-Dichloroethane ND2.4 10ETBE ND1.8 10cis-1,2-Dichloroethene ND1.2 102,2-Dichloropropane ND2.3 10Bromochloromethane ND1.2 10Chloroform ND1.6 10Carbon Tetrachloride ND1.2 101,1,1-Trichloroethane ND1.4 101,1-Dichloropropene ND1.5 10Benzene ND2.1 10TAME ND1.9 101,2-Dichloroethane ND3.9 10Trichloroethylene ND2.2 10Dibromomethane ND1.3 101,2-Dichloropropane ND1.1 10Bromodichloromethane ND1.4 10cis-1,3-Dichloropropene ND0.98 10Toluene ND1.8 10Tetrachloroethylene ND1.2 10trans-1,3-Dichloropropene ND1.8 101,1,2-Trichloroethane ND1.1 10Dibromochloromethane ND2.1 101,3-Dichloropropane ND1.7 101,2-Dibromoethane ND0.86 10Ethyl Benzene ND4.2 10Chlorobenzene ND0.86 101,1,1,2-Tetrachloroethane ND1.9 10m,p-Xylene ND0.66 5.0o-Xylene ND
Page 228 of 260Total Page Count: 260
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
406330
ug/Kg
08/18/11
NANA1108073Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.77 10Styrene ND1.9 10Bromoform ND1.2 10Isopropyl Benzene ND1.4 10n-Propylbenzene ND1.2 10Bromobenzene ND3.0 101,1,2,2-Tetrachloroethane ND1.1 101,3,5-Trimethylbenzene ND3.3 101,2,3-Trichloropropane ND1.6 104-Chlorotoluene ND1.6 102-Chlorotoluene ND1.4 10tert-Butylbenzene ND1.1 101,2,4-Trimethylbenzene ND1.6 10sec-Butyl Benzene ND1.5 10p-Isopropyltoluene ND1.8 101,3-Dichlorobenzene ND1.5 101,4-Dichlorobenzene ND2.2 10n-Butylbenzene ND1.3 101,2-Dichlorobenzene ND4.2 101,2-Dibromo-3-Chloropropane ND2.6 10Hexachlorobutadiene ND2.1 101,2,4-Trichlorobenzene ND2.8 10Naphthalene ND2.9 101,2,3-Trichlorobenzene ND
(S) Dibromofluoromethane 81.5(S) Toluene-d8 87.4(S) 4-Bromofluorobenzene 87.9
Page 229 of 260Total Page Count: 260
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW7470AAnalytical Method:
Prep Date:
Analyzed Date:
08/12/11 Prep Batch:
Analytical Batch:
40623808/15/11
mg/L
7470A 3365
Water
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.0002 0.0150.00005 0.188 0,80 - 120Mercury 106 1060.00007
Work Order:
Matrix:
Units:
Prep Method:
SW8270CAnalytical Method:
Prep Date:
Analyzed Date:
08/14/11 Prep Batch:
Analytical Batch:
40631508/15/11
mg/Kg
3545_BNA 3374
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.33 1.6670.129 14.2 3016 - 98.6Phenol 53.7 46.7ND
0.33 1.6670.129 13.6 3012.9 - 91.32-Chlorophenol 48.7 42.5ND
0.33 0.8330.0663 16.2 3021.9 - 79.81,4-Dichlorobenzene 54.0 45.9ND
0.33 1.6670.0931 16.2 3015.5 - 116N-nitroso-di-n-propylamine 55.8 47.5ND
0.33 0.8330.0733 13.6 3031.7 - 85.11,2,4-Trichlorobenzene 49.3 43.1ND
0.33 1.6670.102 14.8 3023.8 - 1164-Chloro-3-methylphenol 43.9 37.9ND
0.33 0.8330.0964 12.9 3029.1 - 94.8Acenaphthene 49.5 43.5ND
0.33 1.6670.0663 9.91 3010.4 - 1314-Nitrophenol 76.6 69.6ND
0.33 0.8330.0267 14.4 3030.8 - 1242,4-Dinitrotoluene 69.2 59.8ND
0.33 1.6670.102 12.9 3019.9 - 133Pentachlorophenol 72.9 64.0ND
0.33 0.8330.147 4.39 3034.2 - 127Pyrene 75.3 72.0ND
50 24 - 113Phenol-d6 (S) 67.1 58.0ND
50 25 - 1212-Fluorophenol (S) 49.3 42.2ND
50 19 - 1222,4,6-Tribromophenol (S) 63.9 51.2ND
25 23 - 120Nitrobenzene-d5 (S) 57.8 51.1ND
25 30 - 1152-Fluorobiphenyl (S) 56.0 47.9ND
25 18 - 137p-Terphenyl-d14 (S) 53.3 49.9ND
Page 230 of 260Total Page Count: 260
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/12/11 Prep Batch:
Analytical Batch:
40624208/15/11
mg/Kg
3005 3377
Water
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.009 10.004 0.269 0,80 - 120Antimony (Dissolved) 91.2 91.1ND
0.009 10.005 0.293 0,80 - 120Arsenic (Dissolved) 94.3 94.2ND
0.009 10.002 0.411 0,80 - 120Barium (Dissolved) 96.7 96.6ND
0.005 10.002 3.12 2080 - 120Beryllium (Dissolved) 97.9 95.0ND
0.005 10.001 0.221 2080 - 120Cadmium (Dissolved) 97.3 97.2ND
0.005 10.002 0.0737 2080 - 120Chromium (Dissolved) 96.6 97.1ND
0.005 10.002 0.711 2080 - 120Cobalt (Dissolved) 98.3 97.3ND
0.009 10.003 0.295 2080 - 120Copper (Dissolved) 97.2 96.70.00357
0.014 10.005 0.0753 2080 - 120Lead (Dissolved) 95.2 94.9ND
0.009 10.002 0.169 2080 - 120Molybdenum (Dissolved) 97.5 96.8ND
0.009 10.002 0.334 2080 - 120Nickel (Dissolved) 97.6 97.7ND
0.02 10.004 1.45 2080 - 120Selenium (Dissolved) 95.5 94.6ND
0.005 10.002 0.582 2080 - 120Silver (Dissolved) 94.7 94.4ND
0.009 10.004 0.0323 2080 - 120Thallium (dissolved) 95.4 95.0ND
0.009 10.004 0.169 2080 - 120Vanadium (Dissolved) 96.7 96.8ND
0.009 10.002 1.28 2080 - 120Zinc (dissolved) 99.1 97.8ND
Page 231 of 260Total Page Count: 260
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW8270CAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
40631608/16/11
mg/Kg
3545_BNA 3385
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.33 1.6670.129 20.3 3016 - 98.6Phenol 40.3 49.5ND
0.33 1.6670.129 19.2 3012.9 - 91.32-Chlorophenol 36.9 44.8ND
0.33 0.8330.0663 19.6 3021.9 - 79.81,4-Dichlorobenzene 40.9 49.8ND
0.33 1.6670.0931 20.9 3015.5 - 116N-nitroso-di-n-propylamine 41.3 50.8ND
0.33 0.8330.0733 25.7 3031.7 - 85.11,2,4-Trichlorobenzene 35.7 46.3ND
0.33 1.6670.102 17.8 3023.8 - 1164-Chloro-3-methylphenol 32.7 39.0ND
0.33 0.8330.0964 21.8 3029.1 - 94.8Acenaphthene 38.1 47.3ND
0.33 1.6670.0663 7.93 3010.4 - 1314-Nitrophenol 56.0 60.9ND
0.33 0.8330.0267 20.4 3030.8 - 1242,4-Dinitrotoluene 48.9 60.0ND
0.33 1.6670.102 13.8 3019.9 - 133Pentachlorophenol 50.9 58.7ND
0.33 0.8330.147 16.8 3034.2 - 127Pyrene 59.5 70.5ND
50 24 - 113Phenol-d6 (S) 54.0 64.1ND
50 25 - 1212-Fluorophenol (S) 40.6 50.0ND
50 19 - 1222,4,6-Tribromophenol (S) 48.3 57.3ND
25 23 - 120Nitrobenzene-d5 (S) 44.5 53.2ND
25 30 - 1152-Fluorobiphenyl (S) 42.2 53.5ND
25 18 - 137p-Terphenyl-d14 (S) 47.4 53.4ND
Page 232 of 260Total Page Count: 260
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
40626608/16/11
mg/Kg
3050 3388
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
5.0 500.20 1.27 3030.7 - 130Antimony 96.1 97.30.35
1.7 500.28 1.21 3071 - 121Arsenic 96.8 95.60.28
5.0 501 3.03 3070.2 - 130Barium 102 99.01.1
2.0 500.0840 1.52 3073.3 - 115Beryllium 95.1 93.6ND
1.0 500.059 2.75 3068.7 - 110Cadmium 98.4 95.7ND
5.0 500.059 1.60 3076 - 116Chromium 99.5 97.90.33
5.0 500.14 1.75 3057.4 - 122Cobalt 101 99.3ND
5.0 500.090 1.06 3074.8 - 119Copper 104 1030.18
1.0 500.13 0.0206 3067.9 - 118Lead 97.3 97.30.34
5.0 500.059 0.101 3062.9 - 123Molybdenum 98.7 98.80.12
5.0 500.059 2.35 3061.5 - 122Nickel 100 97.70.15
5.0 500.29 1.58 3062 - 111Selenium 93.7 92.2ND
1.0 501.0 2.03 3081.1 - 109Silver 96.7 94.8ND
5.0 500.12 0.214 3039.2 - 125Thallium 93.2 93.4ND
5.0 500.12 1.61 3065.8 - 122Vanadium 101 99.40.14
5.0 500.59 3.08 3059.9 - 122Zinc 122 1180.88
Page 233 of 260Total Page Count: 260
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
40626708/16/11
mg/Kg
3050 3389
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
5.0 500.20 1.07 3030.7 - 130Antimony 96.1 95.10.35
1.7 500.28 3.03 3071 - 121Arsenic 96.8 93.90.28
5.0 501 2.35 3070.2 - 130Barium 102 99.61.1
2.0 500.0840 1.35 3073.3 - 115Beryllium 95.1 96.3ND
1.0 500.059 2.07 3068.7 - 110Cadmium 98.4 96.4ND
5.0 500.059 1.63 3076 - 116Chromium 99.5 97.90.33
5.0 500.14 2.36 3057.4 - 122Cobalt 101 98.6ND
5.0 500.090 2.14 3074.8 - 119Copper 104 1020.18
1.0 500.13 0.784 3067.9 - 118Lead 97.3 96.50.34
5.0 500.059 0.936 3062.9 - 123Molybdenum 98.7 97.80.12
5.0 500.059 2.15 3061.5 - 122Nickel 100 97.90.15
5.0 500.29 4.36 3062 - 111Selenium 93.7 89.7ND
1.0 501.0 2.22 3081.1 - 109Silver 96.7 94.6ND
5.0 500.12 0.226 3039.2 - 125Thallium 93.2 93.0ND
5.0 500.12 1.89 3065.8 - 122Vanadium 101 99.10.14
5.0 500.59 3.08 3059.9 - 122Zinc 122 1180.88
Work Order:
Matrix:
Units:
Prep Method:
7471BAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
40626908/16/11
mg/Kg
7471 3392
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.10 1.250.01 8.13 30,80.5 - 133Mercury 101 110ND
Work Order:
Matrix:
Units:
Prep Method:
7471BAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
40627008/16/11
mg/Kg
7471 3393
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.10 1.250.01 6.58 30,80.5 - 133Mercury 109 116ND
Page 234 of 260Total Page Count: 260
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
40629808/16/11
mg/Kg
3545_TPH 3398
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
2 33.330.758 2.45 3052.7 - 115TPH as Diesel 89.7 87.51.4
200 59.7 - 129Pentacosane (S) 96.7 1232.5
Work Order:
Matrix:
Units:
Prep Method:
SW8082Analytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
40632408/17/11
mg/Kg
3545_PCB 3400
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.10 10.0230 4.95 3055.6 - 135Aroclor1016 94.2 99.0ND
0.10 0.50.0270 7.26 3065.6 - 132Aroclor1260 89.1 95.8ND
1.5 68.9 - 123TCMX (S) 103 101ND
1.5 69.5 - 119DCBP (S) 108 117ND
Work Order:
Matrix:
Units:
Prep Method:
SW8081AAnalytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
40631408/16/11
ug/Kg
3545_OCP 3401
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
2.0 200.40 1.09 3056.9 - 120gamma-BHC 84.6 83.7ND
2.0 201.1 0.0815 3063.6 - 117Heptachlor 96.3 96.4ND
2.0 200.44 0.997 3053 - 123Aldrin 87.3 86.4ND
2.0 200.43 0.827 3044 - 130Dieldrin 84.7 85.4ND
2.0 200.57 2.96 3044.1 - 121Endrin 100 97.5ND
2.0 200.81 1.01 3052.8 - 1344,4'-DDT 107 105ND
2100 52.5 - 139TCMX (S) 89.8 88.8ND
2100 50.2 - 139DCBP (S) 87.8 83.5ND
Page 235 of 260Total Page Count: 260
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
40632108/17/11
mg/L
3510_TPHSG 3402
Water
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.10 10.0440 2.00 30,34.5 - 95.6TPH as Diesel (SG) 51.6 52.7ND
100 57.9 - 125Pentacosane (S) 79.6 73.0ND
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
40630108/15/11
ug/Kg
5035 3413
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
100 100017 2.25 3048.2 - 132TPH(Gasoline) 91.4 93.5ND
50 57 - 127(S) 4-Bromofluorobenzene 89.7 92.897.7
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/18/11 Prep Batch:
Analytical Batch:
40632508/18/11
mg/Kg
3545_TPH 3418
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
2 33.330.758 0.871 3052.7 - 115TPH as Diesel 87.1 87.81.2
100 59.7 - 129Pentacosane (S) 96.8 98.13.3
Work Order:
Matrix:
Units:
Prep Method:
SW8082Analytical Method:
Prep Date:
Analyzed Date:
08/18/11 Prep Batch:
Analytical Batch:
40632608/18/11
mg/Kg
3545_PCB 3419
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.10 10.0230 4.27 3055.6 - 135Aroclor1016 92.7 88.8ND
0.10 0.50.0270 4.66 3065.6 - 132Aroclor1260 89.6 85.5ND
0.25 68.9 - 123TCMX (S) 91.7 83.8ND
0.250 69.5 - 119DCBP (S) 107 98.6ND
Page 236 of 260Total Page Count: 260
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/17/11 Prep Batch:
Analytical Batch:
40632008/17/11
ug/L
5030 3422
Water
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
50 227.2722 0.686 3052.4 - 127TPH(Gasoline) 83.3 82.7ND
11.36 58.4 - 133(S) 4-Bromofluorobenzene 81.0 81.479.7
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
40632808/15/11
ug/Kg
5035 3425
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
100 100017 9.94 3048.2 - 132TPH(Gasoline) 94.3 85.3ND
50 57 - 127(S) 4-Bromofluorobenzene 79.8 74.568.9
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/18/11 Prep Batch:
Analytical Batch:
40633008/18/11
ug/Kg
5035 3427
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
100 100017 12.1 3048.2 - 132TPH(Gasoline) 93.1 105ND
50 57 - 127(S) 4-Bromofluorobenzene 85.0 89.787.2
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/24/11 Prep Batch:
Analytical Batch:
40641108/24/11
ug/Kg
5035 3480
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
100 100017 4.88 3048.2 - 132TPH(Gasoline) 90.0 85.8ND
50 57 - 127(S) 4-Bromofluorobenzene 81.9 81.683.4
Page 237 of 260Total Page Count: 260
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/25/11 Prep Batch:
Analytical Batch:
40644708/26/11
mg/L
WET/3010B 3496
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.10 100.0500 2.49 2080 - 120Lead (STLC) 87.0 89.2ND
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
40630108/15/11
ug/Kg
NA NA
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
10 501.5 18.3 3053.7 - 1391,1-Dichloroethene 90.6 75.4ND
10 501.5 11.5 3066.5 - 135Benzene 91.5 81.6ND
10 503.9 20.3 3057.5 - 150Trichloroethylene 99.7 81.4ND
10 500.98 17.3 3056.8 - 134Toluene 102 85.4ND
10 504.2 14.0 3057.4 - 134Chlorobenzene 90.6 78.7ND
50 59.8 - 148(S) Dibromofluoromethane 73.5 88.3ND
50 55.2 - 133(S) Toluene-d8 86.9 89.4ND
50 55.8 - 141(S) 4-Bromofluorobenzene 92.8 99.0ND
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
40632008/17/11
ug/L
NA NA
Water
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.50 17.040.29 12.2 3061.4 - 1291,1-Dichloroethene 95.6 84.6ND
0.50 17.040.33 11.8 3066.9 - 140Benzene 101 89.7ND
0.50 17.040.38 18.6 3069.3 - 144Trichloroethylene 109 90.5ND
0.50 17.040.19 5.87 3076.6 - 123Toluene 98.1 92.4ND
0.50 17.040.14 7.45 3073.9 - 137Chlorobenzene 99.0 92.1ND
11.36 61.2 - 131(S) Dibromofluoromethane 91.5 89.5ND
11.36 75.1 - 127(S) Toluene-d8 93.8 92.0ND
11.36 64.1 - 120(S) 4-Bromofluorobenzene 93.0 90.2ND
Page 238 of 260Total Page Count: 260
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
40632808/15/11
ug/Kg
NA NA
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
10 501.5 27.3 3053.7 - 1391,1-Dichloroethene 82.3 108ND
10 501.5 19.9 3066.5 - 135Benzene 93.5 114ND
10 503.9 4.48 3057.5 - 150Trichloroethylene 115 121ND
10 500.98 2.81 3056.8 - 134Toluene 110 113ND
10 504.2 3.55 3057.4 - 134Chlorobenzene 107 111ND
50 59.8 - 148(S) Dibromofluoromethane 74.3 93.6ND
50 55.2 - 133(S) Toluene-d8 88.8 88.5ND
50 55.8 - 141(S) 4-Bromofluorobenzene 91.5 91.3ND
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
40633008/18/11
ug/Kg
NA NA
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
10 501.5 2.71 3053.7 - 1391,1-Dichloroethene 88.9 91.2ND
10 501.5 1.67 3066.5 - 135Benzene 90.7 89.3ND
10 503.9 12.4 3057.5 - 150Trichloroethylene 99.3 87.8ND
10 500.98 5.34 3056.8 - 134Toluene 101 95.6ND
10 504.2 14.8 3057.4 - 134Chlorobenzene 96.3 82.9ND
50 59.8 - 148(S) Dibromofluoromethane 80.0 80.5ND
50 55.2 - 133(S) Toluene-d8 86.3 86.0ND
50 55.8 - 141(S) 4-Bromofluorobenzene 90.2 92.0ND
Page 239 of 260Total Page Count: 260
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
40641108/24/11
ug/Kg
NA NA
Soil
1108073
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
10 501.5 1.97 3053.7 - 1391,1-Dichloroethene 81.5 83.0
10 501.5 2.77 3066.5 - 135Benzene 86.4 84.0
10 503.9 6.04 3057.5 - 150Trichloroethylene 90.0 84.7
10 500.98 10.9 3056.8 - 134Toluene 96.5 86.6
10 504.2 10.7 3057.4 - 134Chlorobenzene 89.5 80.5
50 59.8 - 148(S) Dibromofluoromethane 80.9 80.6
50 55.2 - 133(S) Toluene-d8 90.0 90.8
50 55.8 - 141(S) 4-Bromofluorobenzene 93.4 90.8
Page 240 of 260Total Page Count: 260
MS/MSD Summary ReportRaw values are used in quality control assessment.
Work Order: 1108073
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/12/11
1108073-037CSpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW7470A 40623808/15/11
mg/L
33657470A
Water
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
0.015 75 - 1250.00005 0.0002 10.4 20Mercury 104 1180.00009
Work Order: 1108073
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/12/11
1108073-036CSpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW6010B 40624208/15/11
mg/Kg
33773005
Water
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
1 75 - 1250.004 0.009 0.504 20Antimony (Dissolved) 91.1 91.30.001 75 - 1250.005 0.009 1.21 20Arsenic (Dissolved) 91.3 92.00.001 80 - 1200.002 0.009 1.66 20Barium (Dissolved) 92.8 90.70.04561 80 - 1200.002 0.005 6.28 20Beryllium (Dissolved) 87.6 93.501 75 - 1250.001 0.005 2.28 20Cadmium (Dissolved) 93.2 90.80.001 75 - 1250.002 0.005 1.65 20Chromium (Dissolved) 93.1 91.40.001 75 - 1250.002 0.005 1.95 20Cobalt (Dissolved) 92.5 91.10.001 75 - 1250.003 0.009 0.753 20Copper (Dissolved) 93.5 93.20.001 75 - 1250.005 0.014 0.452 20Lead (Dissolved) 87.9 88.20.001 75 - 1250.002 0.009 0.579 20Molybdenum (Dissolved) 92.1 92.40.0301 75 - 1250.002 0.009 2.39 20Nickel (Dissolved) 93.0 90.70.001 75 - 1250.004 0.02 0.460 20Selenium (Dissolved) 91.0 91.30.001 75 - 1250.002 0.005 1.75 20Silver (Dissolved) 90.8 89.30.001 75 - 1250.004 0.009 0.203 20Thallium (dissolved) 86.1 85.60.001 75 - 1250.004 0.009 1.21 20Vanadium (Dissolved) 93.3 91.80.001 75 - 1250.002 0.009 0.0990 20Zinc (dissolved) 92.8 92.80.00
Page 241 of 260Total Page Count: 260
MS/MSD Summary ReportRaw values are used in quality control assessment.
Work Order: 1108073
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/15/11
1108073-002ASpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW6010B 40626608/16/11
mg/Kg
33883050
Soil
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
50 30.7 - 1300.20 5.0 0.196 30Antimony 86.6 86.80.0050 71 - 1210.28 1.7 1.76 30Arsenic 91.5 89.80.04050 70.2 - 1301 S5.0 0.324 30Barium 130 1310.5550 73.3 - 1150.0840 2.0 7.05 30Beryllium 93.3 86.70.0050 68.7 - 1100.059 1.0 3.35 30Cadmium 95.7 92.60.0050 76 - 1160.059 S5.0 0.698 30Chromium 136 1350.5150 57.4 - 1220.14 5.0 1.39 30Cobalt 97.4 95.50.1250 74.8 - 1190.090 5.0 0.634 30Copper 110 1110.0050 67.9 - 1180.13 1.0 4.07 30Lead 96.2 92.00.04050 62.9 - 1230.059 5.0 3.08 30Molybdenum 93.9 91.10.0050 61.5 - 1220.059 S5.0 2.32 30Nickel 123 1190.3850 62 - 1110.29 5.0 2.38 30Selenium 88.1 86.00.0050 81.1 - 1091.0 1.0 0.538 30Silver 93.2 92.70.0050 39.2 - 1250.12 5.0 6.01 30Thallium 84.6 79.70.0050 65.8 - 1220.12 5.0 1.75 30Vanadium 121 1180.4050 59.9 - 1220.59 5.0 0.628 30Zinc 105 1060.22
Work Order: 1108073
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/15/11
1108073-002ASpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
7471B 40626908/16/11
mg/Kg
33927471
Soil
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
1.25 60 - 1400.01 0.10 1.20 30Mercury 109 1100.00017
Page 242 of 260Total Page Count: 260
MS/MSD Summary ReportRaw values are used in quality control assessment.
Work Order: 1108073
Analyzed Date:
Prep Date:
Matrix:
Prep Method: NA
1108073-032ASpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW8260B 40630108/15/11
ug/Kg
NANA
Soil
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
38 53.7 - 1391.2 7.6 6.13 301,1-Dichloroethene 83.5 88.7038 66.5 - 1351.1 7.6 6.15 30Benzene 84.1 89.5038 57.5 - 1502.9 7.6 0.498 30Trichloroethylene 88.2 88.6038 56.8 - 1340.75 7.6 4.02 30Toluene 85.7 89.2038 57.4 - 1343.2 7.6 0.242 30Chlorobenzene 91.1 90.8038 59.8 - 148(S) Dibromofluoromethane 95.3 10138 55.2 - 133(S) Toluene-d8 85.4 87.738 55.8 - 141(S) 4-Bromofluorobenzene 96.8 97.3
Work Order: 1108073
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/14/11
1108073-002ASpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW8270C 40631508/15/11
mg/Kg
33743545_BNA
Soil
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
1.667 16 - 98.60.129 0.33 30.2 30Phenol 50.9 68.70.0001.667 12.9 - 91.30.129 0.33 30.3 302-Chlorophenol 56.0 76.30.0000.833 21.9 - 79.80.0663 S0.33 32.2 301,4-Dichlorobenzene 59.3 82.10.0001.667 15.5 - 1160.0931 0.33 24.8 30N-Nitroso-di-n-propylamine 24.2 31.00.0000.833 31.7 - 85.10.0733 0.33 34.2 301,2,4-Trichlorobenzene 57.0 80.40.0001.667 23.8 - 1160.102 0.33 30.3 304-Chloro-3-methylphenol 48.2 65.50.0000.833 29.1 - 94.80.0964 0.33 33.7 30Acenaphthene 64.0 90.00.0001.667 10.4 - 1310.0663 0.33 3.46 304-Nitrophenol 68.7 71.30.0000.833 30.8 - 1240.0267 0.33 17.4 302,4-Dinitrotoluene 53.7 63.80.0001.667 19.9 - 1330.102 0.33 19.3 30Pentachlorophenol 72.2 87.40.0000.833 34.2 - 1270.147 0.33 14.2 30Pyrene 109 1260.000
50 24 - 113Phenol-d6 (S) 65.8 91.950 25 - 1212-Fluorophenol (S) 51.0 71.250 19 - 1222,4,6-Tribromophenol (S) 62.2 85.625 23 - 120Nitrobenzene-d5 (S) 60.8 86.425 30 - 1152-Fluorobiphenyl (S) 66.2 95.725 18 - 137p-Terphenyl-d14 (S) 69.7 72.7
Page 243 of 260Total Page Count: 260
MS/MSD Summary ReportRaw values are used in quality control assessment.
Work Order: 1108073
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/16/11
1108073-001ASpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW8015B(M) 40631908/17/11
mg/Kg
33983545_TPH
Soil
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
33.33 50.3 - 1253.8 S10 10.3 30TPH as Diesel 23.0 20.54.6511100 57.9 - 125Pentacosane (S) 90.3 86.2
Work Order: 1108073
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/16/11
1108073-001ASpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW8082 40632408/17/11
mg/Kg
34003545_PCB
Soil
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
1 55.6 - 1350.0230 0.10 1.86 30Aroclor1016 103 10100.5 65.6 - 1320.0270 0.10 2.68 30Aroclor1260 98.6 96.00.0031.5 50.4 - 136TCMX (S) 98.2 99.41.5 69.5 - 119DCBP (S) 112 112
Work Order: 1108073
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/25/11
1108073-004ASpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW6010B 40644708/26/11
mg/L
3496WET/3010B
Soil
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
10 75 - 1250.0500 0.10 0.390 20Lead (STLC) 86.4 87.10.414
Page 244 of 260Total Page Count: 260
Laboratory Qualifiers and Definitions
Method Detection Limit (MDL) - the minimum concentration of a substance that can be measured and reported with a 99% confidence that the analyte concentration is greater than zero
Matrix Spike (MS/MSD) - Client sample spiked with identical concentrations of target analyte (s). The spiking occurs prior to the sample preparation and analysis. They are used to document the precision and bias of a method in a given sample matrix.
Matrix - the component or substrate that contains the analyte of interest (e.g., - groundwater, sediment, soil, waste water, etc)
Laboratory Control Sample (LCS ad LCSD) - A known matrix spiked with compounds representative of the target analyte(s). This is used to document laboratory performance.
Duplicate - a field sample and/or laboratory QC sample prepared in duplicate following all of the same processes and procedures used on the original sample (sample duplicate, LCSD, MSD)
Blank (Method/Preparation Blank) -MB/PB - An analyte-free matrix to which all reagents are added in the same volumes/proportions as used in sample processing. The method blank is used to document contamination resulting from the analytical process.
Practical Quantitation Limit (PQL) - a laboratory determined value at 2 to 5 times above the MDL that can be reproduced in a manner that results in a 99% confidence level that the result is both accurate and precise. PQLs reflect all preparation factors and/or dilution factors that have been applied to the sample during the preparation and/or analytical processes.
Precision (%RPD) - The agreement among a set of replicate/duplicate measurements without regard to known value of the replicates
Surrogate (S) or (Surr) - An organic compound which is similar to the target analyte(s) in chemical composition and behavior in the analytical process, but which is not normally found in environmental samples. Surrogates are used in most organic analysis to demonstrate matrix compatibility with the chosen method of analysis
Tentatively Identified Compound (TIC) - A compound not contained within the analytical calibration standards but present in the GCMS library of defined compounds. When the library is searched for an unknown compound, it can frequently give a tentative identification to the compound based on retention time and primary and secondary ion match. TICs are reported as estimates and are candidates for further investigation.
Units: the unit of measure used to express the reported result - mg/L and mg/Kg (equivalent to PPM - parts per million in liquid and solid), ug/L and ug/Kg (equivalent to PPB - parts per billion in liquid and solid), ug/m3, mg.m3, ppbv and ppmv (all units of measure for reporting concentrations in air), % ( equivalent to 10000 ppm or 1,000,000 ppb), ug/Wipe ( concentration found on the surface of a single Wipe usually taken over a 100cm2 surface)
B - Indicates when the anlayte is found in the associated method or preparation blank D - Surrogate is not recoverable due to the necessary dilution of the sampleE - Indicates the reportable value is outside of the calibration range of the instrument but within the linear range of the instrument (unless otherwise noted) Values reported with an E qualifier should be considered as estimated.H- Indicates that the recommended holding time for the analyte or compound has been exceededJ- Indicates a value between the method MDL and PQL and that the reported concentration should be considered as estimated rather the quantitative NA - Not AnalyzedN/A - Not ApplicableNR - Not recoverable - a matrix spike concentration is not recoverable due to a concentration within the original sample that is greater than four times the spike concentration addedR- The % RPD between a duplicate set of samples is outside of the absolute values established by laboratory control chartsS- Spike recovery is outside of established method and/or laboratory control limits. Further explanation of the use of this qualifier should be included within a case narrative
X -Used to indicate that a value based on pattern identification is within the pattern range but not typical of the pattern found in standards. Further explanation may or may not be provided within the sample footnote and/or the case narrative.
DEFINITIONS:
Accuracy/Bias (% Recovery) - The closeness of agreement between an observed value and an accepted reference value.
LABORATORY QUALIFIERS:
Page 245 of 260Total Page Count: 260
pH Adjusted by: pH Checked by:
°C6
Yes
Yes
Yes
Temperature:
Water-pH acceptable upon receipt?
Water-VOA vials have zero headspace?
Container/Temp Blank temperature in compliance?
All samples received within holding time?
Sample Preservation and Hold Time (HT) Information
YesSamples containers intact?
Yes
Yes
Not Present
Yes
Sufficient sample volume for indicated test?
Samples in proper container/bottle?
Custody seals intact on shipping container/cooler?
Shipping Container/Cooler In Good Condition?
Sample Receipt Information
Yes
Yes
Yes
Not Present
Chain of custody agrees with sample labels?
Chain of custody signed when relinquished and received?
Chain of custody present?
Custody seals intact on sample bottles?
Chain of Custody (COC) Information
Checklist Completed By: NG
Carrier Name: First Courier
Physically Logged By: NG
Received By: NG
Date and Time Received: 8/23/2011 14:15
Work Order No.: 1108073
Project Name: 500 Kirkham
Client Name: Northgate Environmental Management Inc.
Sample Receipt Checklist
Page 246 of 260Total Page Count: 260
Login Summary Report
Report Due Date:
5 day TAT! Received 32 soils and 8 waters @ 6'C. Dissolved metals for GW samples. Silica gel cleanup for all waters.Pretarred voas for 8260.Sample 031A received only 3 voas no liner client informed. Per client request from 08/23/2011 additional analysis added: 004 (WET/TCLP Pb) and 015(TPH-G and VOC)on 3 day RUSH TAT. Due 08/26/2011. Only STLC Pb on 004 per client, not enough sample.
14:15
8/23/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/26/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
3 day:25
1108073Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
B-1-1.01108073-001A Soil 02/06/1208/10/11 8:30S_6010BCAM17S_7471BHGS_TPHDOS_8082PCBS_8081AOCPS_8270FullS_GCMS-GROS_8260Full
Sample Note: Pretarred voas for 8260 for soil samples. Use this sample for MS/MSD for all analyses.B-1-5.01108073-002A Soil 02/06/1208/10/11 8:35
S_6010BCAM17S_8082PCBS_TPHDOS_8260FullS_GCMS-GROS_8270FullS_7471BHG
B-1-7.01108073-003A Soil 02/06/12 On-Hold08/10/11 8:40Hold Samples
B-3-1.01108073-004A Soil 02/06/1208/10/11 9:15S_6010B(STLC)S_8081AOCPS_8270FullS_7471BHGS_GCMS-GROS_8260FullS_8082PCBS_TPHDOS_6010BCAM17
Sample Note: Per client request from 08/23/2011 add STLC Lead on sample 004. 3 day TAT RUSH Due 08/26/2011.B-3-5.01108073-005A Soil 02/06/1208/10/11 9:20
S_6010BCAM17
Page 247 of 260Total Page Count: 260
Login Summary Report
Report Due Date:
5 day TAT! Received 32 soils and 8 waters @ 6'C. Dissolved metals for GW samples. Silica gel cleanup for all waters.Pretarred voas for 8260.Sample 031A received only 3 voas no liner client informed. Per client request from 08/23/2011 additional analysis added: 004 (WET/TCLP Pb) and 015(TPH-G and VOC)on 3 day RUSH TAT. Due 08/26/2011. Only STLC Pb on 004 per client, not enough sample.
14:15
8/23/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/26/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
3 day:25
1108073Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
S_GCMS-GROS_8260FullS_8270FullS_TPHDOS_8082PCBS_7471BHG
B-3-9.01108073-006A Soil 02/06/12 On-Hold08/10/11 9:25Hold Samples
B-10-1.01108073-007A Soil 02/06/1208/10/11 9:50S_6010BCAM17S_8082PCBS_7471BHGS_TPHDOS_8270FullS_GCMS-GROS_8260FullS_8081AOCP
B-10-5.01108073-008A Soil 02/06/1208/10/11 9:55S_6010BCAM17S_8270FullS_7471BHGS_GCMS-GROS_8260FullS_TPHDOS_8082PCB
B-10-9.01108073-009A Soil 02/06/12 On-Hold08/10/11 10:00Hold Samples
B-12-1.01108073-010A Soil 02/06/1208/10/11 10:40S_6010BCAM17S_GCMS-GROS_8260FullS_8270FullS_8081AOCPS_8082PCB
Page 248 of 260Total Page Count: 260
Login Summary Report
Report Due Date:
5 day TAT! Received 32 soils and 8 waters @ 6'C. Dissolved metals for GW samples. Silica gel cleanup for all waters.Pretarred voas for 8260.Sample 031A received only 3 voas no liner client informed. Per client request from 08/23/2011 additional analysis added: 004 (WET/TCLP Pb) and 015(TPH-G and VOC)on 3 day RUSH TAT. Due 08/26/2011. Only STLC Pb on 004 per client, not enough sample.
14:15
8/23/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/26/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
3 day:25
1108073Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
S_TPHDOS_7471BHG
B-12-5.01108073-011A Soil 02/06/1208/10/11 10:50S_6010BCAM17S_GCMS-GROS_7471BHGS_8082PCBS_8260FullS_8270FullS_TPHDO
B-12-10.01108073-012A Soil 02/06/12 On-Hold08/10/11 11:10Hold Samples
B-11-1.01108073-013A Soil 02/06/1208/10/11 11:50S_6010BCAM17S_8081AOCPS_8082PCBS_7471BHGS_GCMS-GROS_8260FullS_TPHDOS_8270Full
B-11-6.01108073-014A Soil 02/06/1208/10/11 11:55S_6010BCAM17S_7471BHGS_8260FullS_GCMS-GROS_8082PCBS_8270FullS_TPHDO
B-11-10.01108073-015A Soil 02/06/1208/10/11 12:00S_GCMS-GROS_8260Full
Sample Note: Per client request added TPH-Gas and VOCs on sample 015A. HOLDING TIME IS UP on 08/24/2011. 3 day TAT Due 08/26/2011
Page 249 of 260Total Page Count: 260
Login Summary Report
Report Due Date:
5 day TAT! Received 32 soils and 8 waters @ 6'C. Dissolved metals for GW samples. Silica gel cleanup for all waters.Pretarred voas for 8260.Sample 031A received only 3 voas no liner client informed. Per client request from 08/23/2011 additional analysis added: 004 (WET/TCLP Pb) and 015(TPH-G and VOC)on 3 day RUSH TAT. Due 08/26/2011. Only STLC Pb on 004 per client, not enough sample.
14:15
8/23/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/26/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
3 day:25
1108073Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
B-14-1.01108073-016A Soil 02/06/1208/10/11 12:50S_6010BCAM17S_7471BHGS_TPHDOS_8270FullS_8081AOCPS_GCMS-GROS_8260FullS_8082PCB
B-14-5.01108073-017A Soil 02/06/1208/10/11 12:55S_6010BCAM17S_7471BHGS_TPHDOS_GCMS-GROS_8260FullS_8082PCBS_8270Full
B-14-7.01108073-018A Soil 02/06/12 On-Hold08/10/11 13:00Hold Samples
B-15-1.01108073-019A Soil 02/06/1208/10/11 13:40S_6010BCAM17S_GCMS-GROS_8260FullS_8081AOCPS_8082PCBS_8270FullS_TPHDOS_7471BHG
B-15-5.01108073-020A Soil 02/06/1208/10/11 13:45S_6010BCAM17S_8260FullS_7471BHGS_8082PCBS_GCMS-GRO
Page 250 of 260Total Page Count: 260
Login Summary Report
Report Due Date:
5 day TAT! Received 32 soils and 8 waters @ 6'C. Dissolved metals for GW samples. Silica gel cleanup for all waters.Pretarred voas for 8260.Sample 031A received only 3 voas no liner client informed. Per client request from 08/23/2011 additional analysis added: 004 (WET/TCLP Pb) and 015(TPH-G and VOC)on 3 day RUSH TAT. Due 08/26/2011. Only STLC Pb on 004 per client, not enough sample.
14:15
8/23/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/26/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
3 day:25
1108073Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
S_8270FullS_TPHDO
B-15-9.01108073-021A Soil 02/06/12 On-Hold08/10/11 13:50Hold Samples
B-9-1.01108073-022A Soil 02/06/1208/10/11 15:10S_7471BHGS_8081AOCPS_8082PCBS_6010BCAM17S_8260FullS_GCMS-GROS_TPHDOS_8270Full
B-9-3.01108073-023A Soil 02/06/1208/10/11 15:15S_7471BHGS_6010BCAM17S_8260FullS_GCMS-GROS_8082PCBS_8270FullS_TPHDO
B-9-13.01108073-024A Soil 02/06/12 On-Hold08/10/11 15:20Hold Samples
B-5-1.01108073-025A Soil 02/06/1208/10/11 16:05S_7471BHGS_TPHDOS_8081AOCPS_8082PCBS_8270FullS_6010BCAM17S_8260FullS_GCMS-GRO
B-5-5.01108073-026A Soil 02/06/1208/10/11 16:10S_7471BHG
Page 251 of 260Total Page Count: 260
Login Summary Report
Report Due Date:
5 day TAT! Received 32 soils and 8 waters @ 6'C. Dissolved metals for GW samples. Silica gel cleanup for all waters.Pretarred voas for 8260.Sample 031A received only 3 voas no liner client informed. Per client request from 08/23/2011 additional analysis added: 004 (WET/TCLP Pb) and 015(TPH-G and VOC)on 3 day RUSH TAT. Due 08/26/2011. Only STLC Pb on 004 per client, not enough sample.
14:15
8/23/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/26/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
3 day:25
1108073Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
S_8270FullS_8082PCBS_TPHDOS_8260FullS_GCMS-GROS_6010BCAM17
B-5-10.01108073-027A Soil 02/06/12 On-Hold08/10/11 16:15Hold Samples
B-13-1.01108073-028A Soil 02/06/1208/10/11 16:25S_7471BHGS_6010BCAM17S_8260FullS_GCMS-GROS_8081AOCPS_TPHDOS_8082PCBS_8270Full
B-13-5.01108073-029A Soil 02/06/1208/10/11 16:30S_6010BCAM17S_8270FullS_8260FullS_GCMS-GROS_7471BHGS_8082PCBS_TPHDO
B-13-8.01108073-030A Soil 02/06/12 On-Hold08/10/11 16:35Hold Samples
B-12-1.0 D1108073-031A Soil 02/06/1208/10/11 10:40S_GCMS-GROS_8260Full
Sample Note: Received only 3 pretarred voas no liner.B-5-5.0 D1108073-032A Soil 02/06/1208/10/11 16:10
S_6010BCAM17S_7471BHG
Page 252 of 260Total Page Count: 260
Login Summary Report
Report Due Date:
5 day TAT! Received 32 soils and 8 waters @ 6'C. Dissolved metals for GW samples. Silica gel cleanup for all waters.Pretarred voas for 8260.Sample 031A received only 3 voas no liner client informed. Per client request from 08/23/2011 additional analysis added: 004 (WET/TCLP Pb) and 015(TPH-G and VOC)on 3 day RUSH TAT. Due 08/26/2011. Only STLC Pb on 004 per client, not enough sample.
14:15
8/23/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/26/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
3 day:25
1108073Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
S_8260FullS_GCMS-GROS_TPHDOS_8082PCBS_8270Full
B-1-GW1108073-033A Water 09/24/1108/10/11 9:45W_8260FullW_GCMS-GRO
B-1-GW1108073-033B Water 09/24/1108/10/11 9:45W_TPHDOSG
B-1-GW1108073-033C Water 09/24/1108/10/11 9:45W_D6010BCAM17W_D7470AHG
B-12-GW1108073-034A Water 09/24/1108/10/11 11:00W_8260FullW_GCMS-GRO
B-12-GW1108073-034B Water 09/24/1108/10/11 11:00W_TPHDOSG
B-12-GW1108073-034C Water 09/24/1108/10/11 11:00W_D6010BCAM17W_D7470AHG
B-12-GWD1108073-035A Water 09/24/1108/10/11 11:00W_8260FullW_GCMS-GRO
B-12-GWD1108073-035B Water 09/24/1108/10/11 11:00W_TPHDOSG
B-11-GW1108073-036A Water 09/24/1108/10/11 12:10W_8260FullW_GCMS-GRO
B-11-GW1108073-036B Water 09/24/1108/10/11 12:10W_TPHDOSG
B-11-GW1108073-036C Water 09/24/1108/10/11 12:10W_D6010BCAM17W_D7470AHG
Page 253 of 260Total Page Count: 260
Login Summary Report
Report Due Date:
5 day TAT! Received 32 soils and 8 waters @ 6'C. Dissolved metals for GW samples. Silica gel cleanup for all waters.Pretarred voas for 8260.Sample 031A received only 3 voas no liner client informed. Per client request from 08/23/2011 additional analysis added: 004 (WET/TCLP Pb) and 015(TPH-G and VOC)on 3 day RUSH TAT. Due 08/26/2011. Only STLC Pb on 004 per client, not enough sample.
14:15
8/23/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/26/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
3 day:25
1108073Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
B-9-GW1108073-037A Water 09/24/1108/10/11 16:25W_8260FullW_GCMS-GRO
Sample Note: 4 vaos unpreservedB-9-GW1108073-037B Water 09/24/1108/10/11 16:25
W_TPHDOSGB-9-GW1108073-037C Water 09/24/1108/10/11 16:25
W_D6010BCAM17W_D7470AHG
B-13-GW1108073-038A Water 09/24/1108/10/11 17:15W_8260FullW_GCMS-GRO
Sample Note: For GW one voa unpreservedB-13-GW1108073-038B Water 09/24/1108/10/11 17:15
W_TPHDOSGB-13-GW1108073-038C Water 09/24/1108/10/11 17:15
W_D6010BCAM17W_D7470AHG
B-5-GW1108073-039A Water 09/24/1108/10/11 16:55W_8260FullW_GCMS-GRO
B-5-GW1108073-039B Water 09/24/1108/10/11 16:55W_TPHDOSG
B-5-GW1108073-039C Water 09/24/1108/10/11 16:55W_D6010BCAM17W_D7470AHG
Equip BLANK1108073-040A Water 09/24/1108/10/11 16:45W_8260Full
Page 254 of 260Total Page Count: 260
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Northgate Environmental Management Inc.300 Frank H. Ogawa Plaza, Suite 510Oakland, California 94612Tel: 5108390688Fax: (510) 839-4350
RE: 500 Kirkham
Torrent Laboratory, Inc. received sample(s) on August 23, 2011 for the analyses presented in the following Report.
Dear Anya Starovoytov:
Work Order No.: 1108084 Rev: 2
All data for associated QC met EPA or laboratory specification(s) except where noted in the case narrative.
Torrent Laboratory, Inc. is certified by the State of California, ELAP #1991. If you have any questions regarding these test results, please feel free to contact the Project Management Team at (408)263-5258; ext 204.
Date
August 26, 2011
Patti Sandrock
Page 1 of 159Total Page Count: 159
Date: 8/26/2011
Client: Northgate Environmental Management Inc.
Project: 500 Kirkham
Work Order: 1108084
CASE NARRATIVE
No issues encountered with the receiving, preparation, analysis or reporting of the results associated with this work order.
Note for 8260B/GCMS-GRO: Final results and PQL (Reporting Limit) have been corrected for actual mass from pre-tarred 5035 VOAs.
Analytical Comments for method S_6010B, 1108084-008 MS/MSD, QC Analytical Batch ID 406288, Note:The % recoveries for Copper and Lead are outside of laboratory control limits but are within % RPD limits. The associated LCS/LCSD % recoveries and % RPD are within limits. No corrective action required.
REVISIONS:
Per client request, Lead and TPH analysis was performed on samples 006 and 009 and additional STLC and TCLP extraction and analysis was performed on samples 004, 008, 010. Due to insufficeint remaining sample mass for -004, only STLC was performed per client instruction.
Note: Extraction of 100 g sample / 2000g TCLP Fluid # 1 was performed according to Toxicity Characteristic Leaching Procedure (TCLP) which was rotated in a rotary shaker for 18 hours.
TCLP:Extraction started on 8/23/11 @4.30 PM and ended on 8/24/11 @10.30 AM
__________
Note: Extraction of 50 g sample / 500g 0.2M Sodium Citrate Solution was performed according to wet extraction procedure (WET) which was rotated in a rotary shaker for 48 hours. STLC:Extraction started on 8/23/11 @4.30 PM and ended on 8/25/[email protected] PM.
Rev 1 (8/26/11)
Report revised to revise above comment to include information regarding limited mass for TCLP analysis on sample 004.
Report revised to release data for samples 006 and 009 from "hold" status.
Rev 2 (9/7/11)
Page 2 of 159Total Page Count: 159
Report prepared for: Anya Starovoytov
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/26/11
Sample Result Summary
1108084-001B-4-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg2.41.70.28SW6010B 1
Barium mg/Kg675.01SW6010B 1
Chromium mg/Kg315.00.0590SW6010B 1
Copper mg/Kg6.55.00.0900SW6010B 1
Lead mg/Kg341.00.043SW6010B 1
Nickel mg/Kg195.00.0590SW6010B 1
Vanadium mg/Kg235.00.12SW6010B 1
Zinc mg/Kg355.00.59SW6010B 1
TPH as Motor Oil mg/Kg124.01.65SW8015B(M) 1
1108084-002B-4-5.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg1.91.70.28SW6010B 1
Barium mg/Kg655.01SW6010B 1
Chromium mg/Kg255.00.0590SW6010B 1
Copper mg/Kg5.65.00.0900SW6010B 1
Lead mg/Kg121.00.043SW6010B 1
Nickel mg/Kg125.00.0590SW6010B 1
Vanadium mg/Kg205.00.12SW6010B 1
Zinc mg/Kg195.00.59SW6010B 1
Page 3 of 159Total Page Count: 159
Report prepared for: Anya Starovoytov
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/26/11
Sample Result Summary
1108084-004B-8-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg2.91.70.28SW6010B 1
Barium mg/Kg765.01SW6010B 1
Chromium mg/Kg295.00.0590SW6010B 1
Cobalt mg/Kg6.35.00.14SW6010B 1
Copper mg/Kg555.00.0900SW6010B 1
Lead mg/Kg981.00.043SW6010B 1
Nickel mg/Kg195.00.0590SW6010B 1
Vanadium mg/Kg245.00.12SW6010B 1
Zinc mg/Kg1305.00.59SW6010B 1
Mercury mg/Kg0.170.100.01SW7471A 1
TPH as Motor Oil mg/Kg134.01.65SW8015B(M) 1
Lead (STLC) mg/L110.100.0500SW6010B 1
Page 4 of 159Total Page Count: 159
Report prepared for: Anya Starovoytov
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/26/11
Sample Result Summary
1108084-005B-8-5.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg1.81.70.28SW6010B 1
Barium mg/Kg895.01SW6010B 1
Chromium mg/Kg265.00.0590SW6010B 1
Copper mg/Kg6.15.00.0900SW6010B 1
Lead mg/Kg131.00.043SW6010B 1
Nickel mg/Kg165.00.0590SW6010B 1
Vanadium mg/Kg195.00.12SW6010B 1
Zinc mg/Kg225.00.59SW6010B 1
TPH as Motor Oil mg/Kg5503816.0SW8015B(M) 4
1108084-006B-8-8.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Lead mg/Kg3.81.00.043SW6010B 1
Page 5 of 159Total Page Count: 159
Report prepared for: Anya Starovoytov
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/26/11
Sample Result Summary
1108084-007B-2-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg5.31.70.28SW6010B 1
Barium mg/Kg1005.01SW6010B 1
Chromium mg/Kg315.00.0590SW6010B 1
Cobalt mg/Kg6.95.00.14SW6010B 1
Copper mg/Kg445.00.0900SW6010B 1
Lead mg/Kg1201.00.043SW6010B 1
Nickel mg/Kg265.00.0590SW6010B 1
Vanadium mg/Kg305.00.12SW6010B 1
Zinc mg/Kg1205.00.59SW6010B 1
Mercury mg/Kg0.310.100.01SW7471A 1
TPH as Motor Oil mg/Kg1209.64.00SW8015B(M) 1
Page 6 of 159Total Page Count: 159
Report prepared for: Anya Starovoytov
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/26/11
Sample Result Summary
1108084-008B-2-5.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg6.61.70.28SW6010B 1
Barium mg/Kg1905.01SW6010B 1
Chromium mg/Kg215.00.0590SW6010B 1
Cobalt mg/Kg125.00.14SW6010B 1
Copper mg/Kg405.00.0900SW6010B 1
Lead mg/Kg1301.00.043SW6010B 1
Nickel mg/Kg215.00.0590SW6010B 1
Vanadium mg/Kg375.00.12SW6010B 1
Zinc mg/Kg1305.00.59SW6010B 1
Mercury mg/Kg0.240.100.01SW7471A 1
TPH as Motor Oil mg/Kg1609.64.00SW8015B(M) 1
Lead (STLC) mg/L4.60.100.0500SW6010B 1
1108084-009B-2-9.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Lead mg/Kg2.11.00.043SW6010B 1
Page 7 of 159Total Page Count: 159
Report prepared for: Anya Starovoytov
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/26/11
Sample Result Summary
1108084-010B-7-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Barium mg/Kg535.01SW6010B 1
Chromium mg/Kg295.00.0590SW6010B 1
Copper mg/Kg6.85.00.0900SW6010B 1
Lead mg/Kg501.00.043SW6010B 1
Nickel mg/Kg145.00.0590SW6010B 1
Vanadium mg/Kg215.00.12SW6010B 1
Zinc mg/Kg1305.00.59SW6010B 1
Mercury mg/Kg0.120.100.01SW7471A 1
TPH as Motor Oil mg/Kg9.24.01.65SW8015B(M) 1
Lead (STLC) mg/L5.70.100.0500SW6010B 1
1108084-011B-7-5.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Barium mg/Kg585.01SW6010B 1
Chromium mg/Kg255.00.0590SW6010B 1
Lead mg/Kg4.21.00.043SW6010B 1
Nickel mg/Kg125.00.0590SW6010B 1
Vanadium mg/Kg165.00.12SW6010B 1
Zinc mg/Kg135.00.59SW6010B 1
TPH as Motor Oil mg/Kg5.24.01.65SW8015B(M) 1
Page 8 of 159Total Page Count: 159
Report prepared for: Anya Starovoytov
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/26/11
Sample Result Summary
1108084-013B-6-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Barium mg/Kg425.01SW6010B 1
Chromium mg/Kg215.00.0590SW6010B 1
Lead mg/Kg2.71.00.043SW6010B 1
Nickel mg/Kg135.00.0590SW6010B 1
Vanadium mg/Kg155.00.12SW6010B 1
Zinc mg/Kg145.00.59SW6010B 1
TPH as Motor Oil mg/Kg4.04.01.65SW8015B(M) 1
1108084-014B-6-5.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Barium mg/Kg505.01SW6010B 1
Chromium mg/Kg225.00.0590SW6010B 1
Lead mg/Kg1.91.00.043SW6010B 1
Nickel mg/Kg9.25.00.0590SW6010B 1
Vanadium mg/Kg185.00.12SW6010B 1
Zinc mg/Kg9.05.00.59SW6010B 1
TPH as Motor Oil mg/Kg5.54.01.65SW8015B(M) 1
Page 9 of 159Total Page Count: 159
Report prepared for: Anya Starovoytov
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/26/11
Sample Result Summary
1108084-016B-16-1.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg2.51.70.28SW6010B 1
Barium mg/Kg585.01SW6010B 1
Chromium mg/Kg245.00.0590SW6010B 1
Cobalt mg/Kg5.15.00.14SW6010B 1
Copper mg/Kg125.00.0900SW6010B 1
Lead mg/Kg411.00.043SW6010B 1
Nickel mg/Kg195.00.0590SW6010B 1
Vanadium mg/Kg215.00.12SW6010B 1
Zinc mg/Kg455.00.59SW6010B 1
TPH as Motor Oil mg/Kg2709.64.00SW8015B(M) 1
1108084-017B-16-5.0
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic mg/Kg2.01.70.28SW6010B 1
Barium mg/Kg505.01SW6010B 1
Chromium mg/Kg385.00.0590SW6010B 1
Cobalt mg/Kg6.95.00.14SW6010B 1
Copper mg/Kg5.65.00.0900SW6010B 1
Lead mg/Kg3.21.00.043SW6010B 1
Nickel mg/Kg295.00.0590SW6010B 1
Vanadium mg/Kg275.00.12SW6010B 1
Zinc mg/Kg185.00.59SW6010B 1
Page 10 of 159Total Page Count: 159
Report prepared for: Anya Starovoytov
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/26/11
Sample Result Summary
1108084-019B-7-1.0D
Parameters: PQLMDL UnitResultsDFAnalysisMethod
TPH as Motor Oil mg/Kg8.94.01.65SW8015B(M) 1
1108084-020B-4-GW
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Chloromethane ug/L0.880.500.41SW8260B 1
Barium (Dissolved) mg/L0.0440.0090.002SW6010B 1
1108084-021B-8-GW
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Methylene Chloride ug/L0.366.10.21SW8260B 1.22
Chloroform ug/L4.90.610.36SW8260B 1.22
Barium (Dissolved) mg/L0.0910.0090.002SW6010B 1
Cobalt (Dissolved) mg/L0.00520.0050.002SW6010B 1
Molybdenum (Dissolved) mg/L0.0150.0090.002SW6010B 1
Page 11 of 159Total Page Count: 159
Report prepared for: Anya Starovoytov
Northgate Environmental Management Inc.
Date Received: 08/23/11
Date Reported: 08/26/11
Sample Result Summary
1108084-022B-16-GW
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Arsenic (Dissolved) mg/L0.0100.0090.005SW6010B 1
Barium (Dissolved) mg/L0.120.0090.002SW6010B 1
Cobalt (Dissolved) mg/L0.00570.0050.002SW6010B 1
Molybdenum (Dissolved) mg/L0.0220.0090.002SW6010B 1
Nickel (Dissolved) mg/L0.0590.0090.002SW6010B 1
1108084-023FB
Parameters: PQLMDL UnitResultsDFAnalysisMethod
All compounds were non-detectable for this sample.
1108084-024IDW
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Barium mg/Kg395.01SW6010B 1
Chromium mg/Kg315.00.0590SW6010B 1
Cobalt mg/Kg5.55.00.14SW6010B 1
Lead mg/Kg3.01.00.043SW6010B 1
Nickel mg/Kg255.00.0590SW6010B 1
Vanadium mg/Kg215.00.12SW6010B 1
Zinc mg/Kg185.00.59SW6010B 1
TPH as Motor Oil mg/Kg579.64.00SW8015B(M) 1
1108084-025EQUIP BLANK
Parameters: PQLMDL UnitResultsDFAnalysisMethod
All compounds were non-detectable for this sample.
Page 12 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:15
1204.22
500 Kirkham
B-4-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 3.9 8.9 NA1
SW8260B NA 406253ug/KgNDChloromethane 08/15/11 4.1 8.9 NA1
SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.4 8.9 NA1
SW8260B NA 406253ug/KgNDBromomethane 08/15/11 4.2 8.9 NA1
SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 2.6 8.9 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.4 8.9 NA1
SW8260B NA 406253ug/KgNDFreon 113 08/15/11 3.3 8.9 NA1
SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 1.8 8.9 NA1
SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.99 8.9 NA1
SW8260B NA 406253ug/KgNDMTBE 08/15/11 2.3 8.9 NA1
SW8260B NA 406253ug/KgNDtert-Butanol 08/15/11 18 45 NA1
SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.9 8.9 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 1.1 8.9 NA1
SW8260B NA 406253ug/KgNDETBE 08/15/11 2.1 8.9 NA1
SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.6 8.9 NA1
SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 1.1 8.9 NA1
SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 2.0 8.9 NA1
SW8260B NA 406253ug/KgNDChloroform 08/15/11 1.1 8.9 NA1
SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.4 8.9 NA1
SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 1.1 8.9 NA1
SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.3 8.9 NA1
SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.3 8.9 NA1
SW8260B NA 406253ug/KgNDTAME 08/15/11 1.8 8.9 NA1
SW8260B NA 406253ug/KgND1,2-Dichloroethane 08/15/11 1.7 8.9 NA1
SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 3.5 8.9 NA1
SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 2.0 8.9 NA1
SW8260B NA 406253ug/KgND1,2-Dichloropropane 08/15/11 1.2 8.9 NA1
SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 0.99 8.9 NA1
SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 4.0 8.9 NA1
SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.3 8.9 NA1
SW8260B NA 406253ug/KgNDToluene 08/15/11 0.87 8.9 NA1
SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.6 8.9 NA1
SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.0 8.9 NA1
SW8260B NA 406253ug/KgND1,1,2-Trichloroethane 08/15/11 1.6 8.9 NA1
SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 1.0 8.9 NA1
SW8260B NA 406253ug/KgND1,3-Dichloropropane 08/15/11 1.8 8.9 NA1
Page 13 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:15
1204.22
500 Kirkham
B-4-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.6 8.9 NA1
SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.77 8.9 NA1
SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 3.7 8.9 NA1
SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.76 8.9 NA1
SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.6 8.9 NA1
SW8260B NA 406253ug/KgNDo-Xylene 08/15/11 0.59 4.5 NA1
SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.68 8.9 NA1
SW8260B NA 406253ug/KgNDBromoform 08/15/11 1.7 8.9 NA1
SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 1.1 8.9 NA1
SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.3 8.9 NA1
SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 1.1 8.9 NA1
SW8260B NA 406253ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.7 8.9 NA1
SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.0 8.9 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 3.0 8.9 NA1
SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.4 8.9 NA1
SW8260B NA 406253ug/KgND2-Chlorotoluene 08/15/11 1.4 8.9 NA1
SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.3 8.9 NA1
SW8260B NA 406253ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.97 8.9 NA1
SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.5 8.9 NA1
SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.3 8.9 NA1
SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.6 8.9 NA1
SW8260B NA 406253ug/KgND1,4-Dichlorobenzene 08/15/11 1.3 8.9 NA1
SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 1.9 8.9 NA1
SW8260B NA 406253ug/KgND1,2-Dichlorobenzene 08/15/11 1.2 8.9 NA1
SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.8 8.9 NA1
SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 2.3 8.9 NA1
SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.9 8.9 NA1
SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.5 8.9 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.6 8.9 NA1
SW8260B NA 406253%93.1(S) Dibromofluoromethane 08/15/11 59.8 148 NA1
SW8260B NA 406253%83.6(S) Toluene-d8 08/15/11 55.2 133 NA1
SW8260B NA 406253%97.0(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 14 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:15
1204.22
500 Kirkham
B-4-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406267mg/KgNDAntimony 08/16/11 0.20 5.0 33891
SW6010B 8/15/11 406267mg/Kg2.4Arsenic 08/16/11 0.28 1.7 33891
SW6010B 8/15/11 406267mg/Kg67Barium 08/16/11 1 5.0 33891
SW6010B 8/15/11 406267mg/KgNDBeryllium 08/16/11 0.0840 2.0 33891
SW6010B 8/15/11 406267mg/KgNDCadmium 08/16/11 0.0590 1.0 33891
SW6010B 8/15/11 406267mg/Kg31Chromium 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/KgNDCobalt 08/16/11 0.14 5.0 33891
SW6010B 8/15/11 406267mg/Kg6.5Copper 08/16/11 0.0900 5.0 33891
SW6010B 8/15/11 406267mg/Kg34Lead 08/16/11 0.043 1.0 33891
SW6010B 8/15/11 406267mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/Kg19Nickel 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/KgNDSelenium 08/16/11 0.29 5.0 33891
SW6010B 8/15/11 406267mg/KgNDSilver 08/16/11 1.0 1.0 33891
SW6010B 8/15/11 406267mg/KgNDThallium 08/16/11 0.12 5.0 33891
SW6010B 8/15/11 406267mg/Kg23Vanadium 08/16/11 0.12 5.0 33891
SW6010B 8/15/11 406267mg/Kg35Zinc 08/16/11 0.59 5.0 33891
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/KgNDMercury 08/16/11 0.01 0.10 33931
Page 15 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:15
1204.22
500 Kirkham
B-4-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8081A 8/18/11 406333ug/KgNDalpha-BHC 08/18/11 0.44 2.0 34201
SW8081A 8/18/11 406333ug/KgNDgamma-BHC 08/18/11 0.40 2.0 34201
SW8081A 8/18/11 406333ug/KgNDbeta-BHC 08/18/11 0.36 2.0 34201
SW8081A 8/18/11 406333ug/KgNDdelta-BHC 08/18/11 0.49 2.0 34201
SW8081A 8/18/11 406333ug/KgNDHeptachlor 08/18/11 1.1 2.0 34201
SW8081A 8/18/11 406333ug/KgNDAldrin 08/18/11 0.44 2.0 34201
SW8081A 8/18/11 406333ug/KgNDHeptachlor epoxide 08/18/11 0.32 2.0 34201
SW8081A 8/18/11 406333ug/KgNDgamma-Chlordane 08/18/11 0.42 2.0 34201
SW8081A 8/18/11 406333ug/KgNDalpha-Chlordane 08/18/11 0.36 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndosulfan I 08/18/11 0.59 2.0 34201
SW8081A 8/18/11 406333ug/KgND4,4'-DDE 08/18/11 0.48 2.0 34201
SW8081A 8/18/11 406333ug/KgNDDieldrin 08/18/11 0.43 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndrin 08/18/11 0.57 2.0 34201
SW8081A 8/18/11 406333ug/KgND4,4'-DDD 08/18/11 0.47 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndosulfan II 08/18/11 1.5 2.0 34201
SW8081A 8/18/11 406333ug/KgND4,4'-DDT 08/18/11 0.81 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndrin aldehyde 08/18/11 1.0 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndosulfan sulfate 08/18/11 0.49 2.0 34201
SW8081A 8/18/11 406333ug/KgNDMethoxychlor 08/18/11 0.62 5.0 34201
SW8081A 8/18/11 406333ug/KgNDEndrin Ketone 08/18/11 0.40 2.0 34201
SW8081A 8/18/11 406333ug/KgNDChlordane 08/18/11 10 20 34201
SW8081A 8/18/11 406333ug/KgNDToxaphene 08/18/11 10 100 34201
SW8081A 8/18/11 406333%98.2TCMX (S) 08/18/11 52.5 139 34201
SW8081A 8/18/11 406333%88.6DCBP (S) 08/18/11 50.2 139 34201
Page 16 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:15
1204.22
500 Kirkham
B-4-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1221 08/18/11 0.0920 0.20 34191
SW8082 8/18/11 406326mg/KgNDAroclor1232 08/18/11 0.0460 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1242 08/18/11 0.0430 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1248 08/18/11 0.0360 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1254 08/18/11 0.0240 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1260 08/18/11 0.0270 0.10 34191
SW8082 8/18/11 406326%95.6TCMX (S) 08/18/11 50.4 136 34191
SW8082 8/18/11 406326%104DCBP (S) 08/18/11 55.1 113 34191
Page 17 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:15
1204.22
500 Kirkham
B-4-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 0.660 0.653 33851
SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 0.110 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 0.123 0.330 33851
SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 0.129 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 0.0683 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 0.129 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 0.0733 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 0.0663 6.59 33851
SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 0.0713 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 0.116 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 0.0683 0.330 33851
SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 0.139 0.330 33851
SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 0.0931 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 0.0465 0.330 33851
SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 0.0528 0.330 33851
SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 0.0574 0.653 33851
SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 0.0525 0.653 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 0.133 6.59 33851
SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 5.59 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 0.0584 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 0.0733 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 0.0901 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 0.0990 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 0.0653 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 0.102 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 0.0792 0.330 33851
SW8270C 8/15/11 406316mg/KgND1-Methylnaphthalene 08/16/11 0.0792 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 0.0277 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 0.0950 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 0.121 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 0.0594 3.27 33851
SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 0.0693 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 0.118 0.330 33851
Page 18 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:15
1204.22
500 Kirkham
B-4-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 0.106 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 0.0851 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 0.0267 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 0.0858 0.330 33851
SW8270C 8/15/11 406316mg/KgND3-Nitroaniline 08/16/11 0.0693 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 0.0960 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 0.0297 3.27 33851
SW8270C 8/15/11 406316mg/KgND4-Nitrophenol 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 0.0782 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 0.0267 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 0.119 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 0.119 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 0.117 0.330 33851
SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 0.0990 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 0.0802 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Nitroaniline 08/16/11 0.0802 0.330 33851
SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 0.109 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 0.0812 3.27 33851
SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 0.101 0.330 33851
SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 0.102 3.27 33851
SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 0.142 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 0.132 0.330 33851
SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 0.132 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 0.108 1.68 33851
SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 0.132 0.653 33851
SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 0.374 3.27 33851
SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 0.147 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 0.0891 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 0.149 0.330 33851
SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 0.152 0.330 33851
SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 0.176 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 0.0832 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 0.138 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 0.133 0.330 33851
Page 19 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:15
1204.22
500 Kirkham
B-4-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 0.169 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 0.135 0.330 33851
SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 0.131 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 0.151 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 0.150 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 0.150 0.330 33851
SW8270C 8/15/11 406316%45.52,4,6-Tribromophenol (S) 08/16/11 19 122 33851
SW8270C 8/15/11 406316%51.82-Fluorobiphenyl (S) 08/16/11 30 115 33851
SW8270C 8/15/11 406316%56.92-Fluorophenol (S) 08/16/11 25 121 33851
SW8270C 8/15/11 406316%51.3Nitrobenzene-d5 (S) 08/16/11 23 120 33851
SW8270C 8/15/11 406316%61.5Phenol-d6 (S) 08/16/11 24 113 33851
SW8270C 8/15/11 406316%48.7p-Terphenyl-d14 (S) 08/16/11 18 137 33851
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 15 89 NA1
8260TPH NA 406253%96.4(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 0.759 2.0 34181
SW8015B(M) 8/18/11 406325mg/Kg12TPH as Motor Oil 08/18/11 1.65 4.0 34181
SW8015B(M) 8/18/11 406325mg/Kg114Pentacosane (S) 08/18/11 59.7 129 34181
Page 20 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:20
1204.22
500 Kirkham
B-4-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 3.8 8.7 NA1
SW8260B NA 406253ug/KgNDChloromethane 08/15/11 4.0 8.7 NA1
SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.3 8.7 NA1
SW8260B NA 406253ug/KgNDBromomethane 08/15/11 4.1 8.7 NA1
SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 2.5 8.7 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.3 8.7 NA1
SW8260B NA 406253ug/KgNDFreon 113 08/15/11 3.2 8.7 NA1
SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 1.7 8.7 NA1
SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.97 8.7 NA1
SW8260B NA 406253ug/KgNDMTBE 08/15/11 2.2 8.7 NA1
SW8260B NA 406253ug/KgNDtert-Butanol 08/15/11 18 44 NA1
SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.9 8.7 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 1.1 8.7 NA1
SW8260B NA 406253ug/KgNDETBE 08/15/11 2.1 8.7 NA1
SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.5 8.7 NA1
SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 1.1 8.7 NA1
SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 2.0 8.7 NA1
SW8260B NA 406253ug/KgNDChloroform 08/15/11 1.1 8.7 NA1
SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.4 8.7 NA1
SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 1.1 8.7 NA1
SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.3 8.7 NA1
SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.3 8.7 NA1
SW8260B NA 406253ug/KgNDTAME 08/15/11 1.8 8.7 NA1
SW8260B NA 406253ug/KgND1,2-Dichloroethane 08/15/11 1.7 8.7 NA1
SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 3.4 8.7 NA1
SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 1.9 8.7 NA1
SW8260B NA 406253ug/KgND1,2-Dichloropropane 08/15/11 1.1 8.7 NA1
SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 0.97 8.7 NA1
SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 3.9 8.7 NA1
SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.2 8.7 NA1
SW8260B NA 406253ug/KgNDToluene 08/15/11 0.85 8.7 NA1
SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.6 8.7 NA1
SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.0 8.7 NA1
SW8260B NA 406253ug/KgND1,1,2-Trichloroethane 08/15/11 1.6 8.7 NA1
SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 0.98 8.7 NA1
SW8260B NA 406253ug/KgND1,3-Dichloropropane 08/15/11 1.8 8.7 NA1
Page 21 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:20
1204.22
500 Kirkham
B-4-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.5 8.7 NA1
SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.75 8.7 NA1
SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 3.7 8.7 NA1
SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.75 8.7 NA1
SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.6 8.7 NA1
SW8260B NA 406253ug/KgNDo-Xylene 08/15/11 0.58 4.4 NA1
SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.67 8.7 NA1
SW8260B NA 406253ug/KgNDBromoform 08/15/11 1.7 8.7 NA1
SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 1.1 8.7 NA1
SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.2 8.7 NA1
SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 1.0 8.7 NA1
SW8260B NA 406253ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.6 8.7 NA1
SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.98 8.7 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 2.9 8.7 NA1
SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.4 8.7 NA1
SW8260B NA 406253ug/KgND2-Chlorotoluene 08/15/11 1.4 8.7 NA1
SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.2 8.7 NA1
SW8260B NA 406253ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.94 8.7 NA1
SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.4 8.7 NA1
SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.3 8.7 NA1
SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.6 8.7 NA1
SW8260B NA 406253ug/KgND1,4-Dichlorobenzene 08/15/11 1.3 8.7 NA1
SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 1.9 8.7 NA1
SW8260B NA 406253ug/KgND1,2-Dichlorobenzene 08/15/11 1.1 8.7 NA1
SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.7 8.7 NA1
SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 2.2 8.7 NA1
SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.9 8.7 NA1
SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.5 8.7 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.5 8.7 NA1
SW8260B NA 406253%88.9(S) Dibromofluoromethane 08/15/11 59.8 148 NA1
SW8260B NA 406253%89.2(S) Toluene-d8 08/15/11 55.2 133 NA1
SW8260B NA 406253%97.9(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 22 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:20
1204.22
500 Kirkham
B-4-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406267mg/KgNDAntimony 08/16/11 0.20 5.0 33891
SW6010B 8/15/11 406267mg/Kg1.9Arsenic 08/16/11 0.28 1.7 33891
SW6010B 8/15/11 406267mg/Kg65Barium 08/16/11 1 5.0 33891
SW6010B 8/15/11 406267mg/KgNDBeryllium 08/16/11 0.0840 2.0 33891
SW6010B 8/15/11 406267mg/KgNDCadmium 08/16/11 0.0590 1.0 33891
SW6010B 8/15/11 406267mg/Kg25Chromium 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/KgNDCobalt 08/16/11 0.14 5.0 33891
SW6010B 8/15/11 406267mg/Kg5.6Copper 08/16/11 0.0900 5.0 33891
SW6010B 8/15/11 406267mg/Kg12Lead 08/16/11 0.043 1.0 33891
SW6010B 8/15/11 406267mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/Kg12Nickel 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/KgNDSelenium 08/16/11 0.29 5.0 33891
SW6010B 8/15/11 406267mg/KgNDSilver 08/16/11 1.0 1.0 33891
SW6010B 8/15/11 406267mg/KgNDThallium 08/16/11 0.12 5.0 33891
SW6010B 8/15/11 406267mg/Kg20Vanadium 08/16/11 0.12 5.0 33891
SW6010B 8/15/11 406267mg/Kg19Zinc 08/16/11 0.59 5.0 33891
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/KgNDMercury 08/16/11 0.01 0.10 33931
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1221 08/18/11 0.0920 0.20 34191
SW8082 8/18/11 406326mg/KgNDAroclor1232 08/18/11 0.0460 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1242 08/18/11 0.0430 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1248 08/18/11 0.0360 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1254 08/18/11 0.0240 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1260 08/18/11 0.0270 0.10 34191
SW8082 8/18/11 406326%90.6TCMX (S) 08/18/11 50.4 136 34191
SW8082 8/18/11 406326%83.1DCBP (S) 08/18/11 55.1 113 34191
Page 23 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:20
1204.22
500 Kirkham
B-4-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 0.660 0.653 33851
SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 0.110 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 0.123 0.330 33851
SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 0.129 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 0.0683 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 0.129 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 0.0733 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 0.0663 6.59 33851
SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 0.0713 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 0.116 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 0.0683 0.330 33851
SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 0.139 0.330 33851
SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 0.0931 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 0.0465 0.330 33851
SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 0.0528 0.330 33851
SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 0.0574 0.653 33851
SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 0.0525 0.653 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 0.133 6.59 33851
SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 5.59 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 0.0584 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 0.0733 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 0.0901 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 0.0990 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 0.0653 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 0.102 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 0.0792 0.330 33851
SW8270C 8/15/11 406316mg/KgND1-Methylnaphthalene 08/16/11 0.0792 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 0.0277 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 0.0950 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 0.121 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 0.0594 3.27 33851
SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 0.0693 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 0.118 0.330 33851
Page 24 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:20
1204.22
500 Kirkham
B-4-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 0.106 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 0.0851 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 0.0267 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 0.0858 0.330 33851
SW8270C 8/15/11 406316mg/KgND3-Nitroaniline 08/16/11 0.0693 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 0.0960 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 0.0297 3.27 33851
SW8270C 8/15/11 406316mg/KgND4-Nitrophenol 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 0.0782 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 0.0267 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 0.119 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 0.119 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 0.117 0.330 33851
SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 0.0990 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 0.0802 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Nitroaniline 08/16/11 0.0802 0.330 33851
SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 0.109 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 0.0812 3.27 33851
SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 0.101 0.330 33851
SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 0.102 3.27 33851
SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 0.142 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 0.132 0.330 33851
SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 0.132 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 0.108 1.68 33851
SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 0.132 0.653 33851
SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 0.374 3.27 33851
SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 0.147 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 0.0891 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 0.149 0.330 33851
SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 0.152 0.330 33851
SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 0.176 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 0.0832 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 0.138 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 0.133 0.330 33851
Page 25 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:20
1204.22
500 Kirkham
B-4-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 0.169 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 0.135 0.330 33851
SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 0.131 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 0.151 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 0.150 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 0.150 0.330 33851
SW8270C 8/15/11 406316%44.52,4,6-Tribromophenol (S) 08/16/11 19 122 33851
SW8270C 8/15/11 406316%53.02-Fluorobiphenyl (S) 08/16/11 30 115 33851
SW8270C 8/15/11 406316%62.62-Fluorophenol (S) 08/16/11 25 121 33851
SW8270C 8/15/11 406316%54.4Nitrobenzene-d5 (S) 08/16/11 23 120 33851
SW8270C 8/15/11 406316%66.0Phenol-d6 (S) 08/16/11 24 113 33851
SW8270C 8/15/11 406316%50.9p-Terphenyl-d14 (S) 08/16/11 18 137 33851
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 15 87 NA1
8260TPH NA 406253%86.3(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 0.759 2.0 34181
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Motor Oil 08/18/11 1.65 4.0 34181
SW8015B(M) 8/18/11 406325mg/Kg120Pentacosane (S) 08/18/11 59.7 129 34181
Page 26 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:55
1204.22
500 Kirkham
B-8-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 3.8 8.7 NA1
SW8260B NA 406253ug/KgNDChloromethane 08/15/11 4.0 8.7 NA1
SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.3 8.7 NA1
SW8260B NA 406253ug/KgNDBromomethane 08/15/11 4.1 8.7 NA1
SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 2.5 8.7 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.3 8.7 NA1
SW8260B NA 406253ug/KgNDFreon 113 08/15/11 3.2 8.7 NA1
SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 1.7 8.7 NA1
SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.97 8.7 NA1
SW8260B NA 406253ug/KgNDMTBE 08/15/11 2.2 8.7 NA1
SW8260B NA 406253ug/KgNDtert-Butanol 08/15/11 18 44 NA1
SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.9 8.7 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 1.1 8.7 NA1
SW8260B NA 406253ug/KgNDETBE 08/15/11 2.1 8.7 NA1
SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.5 8.7 NA1
SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 1.1 8.7 NA1
SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 2.0 8.7 NA1
SW8260B NA 406253ug/KgNDChloroform 08/15/11 1.1 8.7 NA1
SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.4 8.7 NA1
SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 1.1 8.7 NA1
SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.3 8.7 NA1
SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.3 8.7 NA1
SW8260B NA 406253ug/KgNDTAME 08/15/11 1.8 8.7 NA1
SW8260B NA 406253ug/KgND1,2-Dichloroethane 08/15/11 1.7 8.7 NA1
SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 3.4 8.7 NA1
SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 1.9 8.7 NA1
SW8260B NA 406253ug/KgND1,2-Dichloropropane 08/15/11 1.1 8.7 NA1
SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 0.97 8.7 NA1
SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 3.9 8.7 NA1
SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.2 8.7 NA1
SW8260B NA 406253ug/KgNDToluene 08/15/11 0.85 8.7 NA1
SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.6 8.7 NA1
SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.0 8.7 NA1
SW8260B NA 406253ug/KgND1,1,2-Trichloroethane 08/15/11 1.6 8.7 NA1
SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 0.98 8.7 NA1
SW8260B NA 406253ug/KgND1,3-Dichloropropane 08/15/11 1.8 8.7 NA1
Page 27 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:55
1204.22
500 Kirkham
B-8-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.5 8.7 NA1
SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.75 8.7 NA1
SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 3.7 8.7 NA1
SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.75 8.7 NA1
SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.6 8.7 NA1
SW8260B NA 406253ug/KgNDo-Xylene 08/15/11 0.58 4.4 NA1
SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.67 8.7 NA1
SW8260B NA 406253ug/KgNDBromoform 08/15/11 1.7 8.7 NA1
SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 1.1 8.7 NA1
SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.2 8.7 NA1
SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 1.0 8.7 NA1
SW8260B NA 406253ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.6 8.7 NA1
SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.98 8.7 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 2.9 8.7 NA1
SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.4 8.7 NA1
SW8260B NA 406253ug/KgND2-Chlorotoluene 08/15/11 1.4 8.7 NA1
SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.2 8.7 NA1
SW8260B NA 406253ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.94 8.7 NA1
SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.4 8.7 NA1
SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.3 8.7 NA1
SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.6 8.7 NA1
SW8260B NA 406253ug/KgND1,4-Dichlorobenzene 08/15/11 1.3 8.7 NA1
SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 1.9 8.7 NA1
SW8260B NA 406253ug/KgND1,2-Dichlorobenzene 08/15/11 1.1 8.7 NA1
SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.7 8.7 NA1
SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 2.2 8.7 NA1
SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.9 8.7 NA1
SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.5 8.7 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.5 8.7 NA1
SW8260B NA 406253%92.9(S) Dibromofluoromethane 08/15/11 59.8 148 NA1
SW8260B NA 406253%90.3(S) Toluene-d8 08/15/11 55.2 133 NA1
SW8260B NA 406253%92.8(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 28 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:55
1204.22
500 Kirkham
B-8-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/25/11 406447mg/L11Lead (STLC) 08/26/11 0.0500 0.10 34961
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406267mg/KgNDAntimony 08/16/11 0.20 5.0 33891
SW6010B 8/15/11 406267mg/Kg2.9Arsenic 08/16/11 0.28 1.7 33891
SW6010B 8/15/11 406267mg/Kg76Barium 08/16/11 1 5.0 33891
SW6010B 8/15/11 406267mg/KgNDBeryllium 08/16/11 0.0840 2.0 33891
SW6010B 8/15/11 406267mg/KgNDCadmium 08/16/11 0.0590 1.0 33891
SW6010B 8/15/11 406267mg/Kg29Chromium 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/Kg6.3Cobalt 08/16/11 0.14 5.0 33891
SW6010B 8/15/11 406267mg/Kg55Copper 08/16/11 0.0900 5.0 33891
SW6010B 8/15/11 406267mg/Kg98Lead 08/16/11 0.043 1.0 33891
SW6010B 8/15/11 406267mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/Kg19Nickel 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/KgNDSelenium 08/16/11 0.29 5.0 33891
SW6010B 8/15/11 406267mg/KgNDSilver 08/16/11 1.0 1.0 33891
SW6010B 8/15/11 406267mg/KgNDThallium 08/16/11 0.12 5.0 33891
SW6010B 8/15/11 406267mg/Kg24Vanadium 08/16/11 0.12 5.0 33891
SW6010B 8/15/11 406267mg/Kg130Zinc 08/16/11 0.59 5.0 33891
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/Kg0.17Mercury 08/16/11 0.01 0.10 33931
Page 29 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:55
1204.22
500 Kirkham
B-8-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8081A 8/18/11 406333ug/KgNDalpha-BHC 08/18/11 0.44 2.0 34201
SW8081A 8/18/11 406333ug/KgNDgamma-BHC 08/18/11 0.40 2.0 34201
SW8081A 8/18/11 406333ug/KgNDbeta-BHC 08/18/11 0.36 2.0 34201
SW8081A 8/18/11 406333ug/KgNDdelta-BHC 08/18/11 0.49 2.0 34201
SW8081A 8/18/11 406333ug/KgNDHeptachlor 08/18/11 1.1 2.0 34201
SW8081A 8/18/11 406333ug/KgNDAldrin 08/18/11 0.44 2.0 34201
SW8081A 8/18/11 406333ug/KgNDHeptachlor epoxide 08/18/11 0.32 2.0 34201
SW8081A 8/18/11 406333ug/KgNDgamma-Chlordane 08/18/11 0.42 2.0 34201
SW8081A 8/18/11 406333ug/KgNDalpha-Chlordane 08/18/11 0.36 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndosulfan I 08/18/11 0.59 2.0 34201
SW8081A 8/18/11 406333ug/KgND4,4'-DDE 08/18/11 0.48 2.0 34201
SW8081A 8/18/11 406333ug/KgNDDieldrin 08/18/11 0.43 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndrin 08/18/11 0.57 2.0 34201
SW8081A 8/18/11 406333ug/KgND4,4'-DDD 08/18/11 0.47 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndosulfan II 08/18/11 1.5 2.0 34201
SW8081A 8/18/11 406333ug/KgND4,4'-DDT 08/18/11 0.81 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndrin aldehyde 08/18/11 1.0 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndosulfan sulfate 08/18/11 0.49 2.0 34201
SW8081A 8/18/11 406333ug/KgNDMethoxychlor 08/18/11 0.62 5.0 34201
SW8081A 8/18/11 406333ug/KgNDEndrin Ketone 08/18/11 0.40 2.0 34201
SW8081A 8/18/11 406333ug/KgNDChlordane 08/18/11 10 20 34201
SW8081A 8/18/11 406333ug/KgNDToxaphene 08/18/11 10 100 34201
SW8081A 8/18/11 406333%99.2TCMX (S) 08/18/11 52.5 139 34201
SW8081A 8/18/11 406333%94.3DCBP (S) 08/18/11 50.2 139 34201
Page 30 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:55
1204.22
500 Kirkham
B-8-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1221 08/18/11 0.0920 0.20 34191
SW8082 8/18/11 406326mg/KgNDAroclor1232 08/18/11 0.0460 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1242 08/18/11 0.0430 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1248 08/18/11 0.0360 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1254 08/18/11 0.0240 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1260 08/18/11 0.0270 0.10 34191
SW8082 8/18/11 406326%93.4TCMX (S) 08/18/11 50.4 136 34191
SW8082 8/18/11 406326%97.6DCBP (S) 08/18/11 55.1 113 34191
Page 31 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:55
1204.22
500 Kirkham
B-8-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 100 99.0 338510
SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 16.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 18.6 50.0 338510
SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 19.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 10.4 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 19.5 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 11.1 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 10.1 999 338510
SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 15.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 10.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 17.6 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 10.4 50.0 338510
SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 21.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 14.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 7.05 50.0 338510
SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 8.00 50.0 338510
SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 8.70 99.0 338510
SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 7.95 99.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 20.1 999 338510
SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 848 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 8.85 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 15.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 11.1 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 15.8 50.0 338510
SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 13.7 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 15.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 9.90 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 15.5 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 12.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND1-Methylnaphthalene 08/16/11 12.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 4.20 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 14.4 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 18.3 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 9.00 495 338510
SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 10.5 50.0 338510
Page 32 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:55
1204.22
500 Kirkham
B-8-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 17.9 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 16.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 12.9 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 4.05 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 13.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND3-Nitroaniline 08/16/11 10.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 14.6 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 4.50 495 338510
SW8270C 8/15/11 406316mg/KgND4-Nitrophenol 08/16/11 10.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 11.9 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 4.05 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 18.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 18.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 17.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 15.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 12.2 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Nitroaniline 08/16/11 12.2 50.0 338510
SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 10.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 10.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 16.5 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 12.3 495 338510
SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 15.3 50.0 338510
SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 15.5 495 338510
SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 21.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 20.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 20.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 16.4 255 338510
SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 20.1 99.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 56.7 495 338510
SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 22.3 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 13.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 22.7 50.0 338510
SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 23.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 26.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 12.6 50.0 338510
Page 33 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 8:55
1204.22
500 Kirkham
B-8-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 20.9 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 20.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 25.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 20.4 50.0 338510
SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 19.8 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 23.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 22.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 22.8 50.0 338510
SW8270C 8/15/11 406316S,D %0.0002,4,6-Tribromophenol (S) 08/16/11 19 122 338510
SW8270C 8/15/11 406316S,D %0.0002-Fluorobiphenyl (S) 08/16/11 30 115 338510
SW8270C 8/15/11 406316S,D %0.0002-Fluorophenol (S) 08/16/11 25 121 338510
SW8270C 8/15/11 406316S,D %0.000Nitrobenzene-d5 (S) 08/16/11 23 120 338510
SW8270C 8/15/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 338510
SW8270C 8/15/11 406316S,D %0.000p-Terphenyl-d14 (S) 08/16/11 18 137 338510
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 15 87 NA1
8260TPH NA 406253%74.6(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 0.759 2.0 34181
SW8015B(M) 8/18/11 406325mg/Kg13TPH as Motor Oil 08/18/11 1.65 4.0 34181
SW8015B(M) 8/18/11 406325mg/Kg117Pentacosane (S) 08/18/11 59.7 129 34181
Page 34 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:00
1204.22
500 Kirkham
B-8-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 3.4 7.8 NA1
SW8260B NA 406253ug/KgNDChloromethane 08/15/11 3.6 7.8 NA1
SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.1 7.8 NA1
SW8260B NA 406253ug/KgNDBromomethane 08/15/11 3.6 7.8 NA1
SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 2.2 7.8 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.2 7.8 NA1
SW8260B NA 406253ug/KgNDFreon 113 08/15/11 2.9 7.8 NA1
SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 1.5 7.8 NA1
SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.87 7.8 NA1
SW8260B NA 406253ug/KgNDMTBE 08/15/11 2.0 7.8 NA1
SW8260B NA 406253ug/KgNDtert-Butanol 08/15/11 16 39 NA1
SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.7 7.8 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 1.0 7.8 NA1
SW8260B NA 406253ug/KgNDETBE 08/15/11 1.9 7.8 NA1
SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.4 7.8 NA1
SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 0.97 7.8 NA1
SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 1.8 7.8 NA1
SW8260B NA 406253ug/KgNDChloroform 08/15/11 0.95 7.8 NA1
SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.3 7.8 NA1
SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 0.95 7.8 NA1
SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.1 7.8 NA1
SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.2 7.8 NA1
SW8260B NA 406253ug/KgNDTAME 08/15/11 1.6 7.8 NA1
SW8260B NA 406253ug/KgND1,2-Dichloroethane 08/15/11 1.5 7.8 NA1
SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 3.0 7.8 NA1
SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 1.7 7.8 NA1
SW8260B NA 406253ug/KgND1,2-Dichloropropane 08/15/11 1.0 7.8 NA1
SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 0.87 7.8 NA1
SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 3.5 7.8 NA1
SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.1 7.8 NA1
SW8260B NA 406253ug/KgNDToluene 08/15/11 0.77 7.8 NA1
SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.4 7.8 NA1
SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.90 7.8 NA1
SW8260B NA 406253ug/KgND1,1,2-Trichloroethane 08/15/11 1.4 7.8 NA1
SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 0.87 7.8 NA1
SW8260B NA 406253ug/KgND1,3-Dichloropropane 08/15/11 1.6 7.8 NA1
Page 35 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:00
1204.22
500 Kirkham
B-8-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.4 7.8 NA1
SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.67 7.8 NA1
SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 3.3 7.8 NA1
SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.67 7.8 NA1
SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.4 7.8 NA1
SW8260B NA 406253ug/KgNDo-Xylene 08/15/11 0.52 3.9 NA1
SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.60 7.8 NA1
SW8260B NA 406253ug/KgNDBromoform 08/15/11 1.5 7.8 NA1
SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 0.97 7.8 NA1
SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.1 7.8 NA1
SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 0.93 7.8 NA1
SW8260B NA 406253ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.4 7.8 NA1
SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.88 7.8 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 2.6 7.8 NA1
SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.2 7.8 NA1
SW8260B NA 406253ug/KgND2-Chlorotoluene 08/15/11 1.2 7.8 NA1
SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.1 7.8 NA1
SW8260B NA 406253ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.85 7.8 NA1
SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.3 7.8 NA1
SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.1 7.8 NA1
SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.4 7.8 NA1
SW8260B NA 406253ug/KgND1,4-Dichlorobenzene 08/15/11 1.2 7.8 NA1
SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 1.7 7.8 NA1
SW8260B NA 406253ug/KgND1,2-Dichlorobenzene 08/15/11 1.0 7.8 NA1
SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.3 7.8 NA1
SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 2.0 7.8 NA1
SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.7 7.8 NA1
SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.2 7.8 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.2 7.8 NA1
SW8260B NA 406253%93.6(S) Dibromofluoromethane 08/15/11 59.8 148 NA1
SW8260B NA 406253%90.2(S) Toluene-d8 08/15/11 55.2 133 NA1
SW8260B NA 406253%106(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 36 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:00
1204.22
500 Kirkham
B-8-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406267mg/KgNDAntimony 08/16/11 0.20 5.0 33891
SW6010B 8/15/11 406267mg/Kg1.8Arsenic 08/16/11 0.28 1.7 33891
SW6010B 8/15/11 406267mg/Kg89Barium 08/16/11 1 5.0 33891
SW6010B 8/15/11 406267mg/KgNDBeryllium 08/16/11 0.0840 2.0 33891
SW6010B 8/15/11 406267mg/KgNDCadmium 08/16/11 0.0590 1.0 33891
SW6010B 8/15/11 406267mg/Kg26Chromium 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/KgNDCobalt 08/16/11 0.14 5.0 33891
SW6010B 8/15/11 406267mg/Kg6.1Copper 08/16/11 0.0900 5.0 33891
SW6010B 8/15/11 406267mg/Kg13Lead 08/16/11 0.043 1.0 33891
SW6010B 8/15/11 406267mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/Kg16Nickel 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/KgNDSelenium 08/16/11 0.29 5.0 33891
SW6010B 8/15/11 406267mg/KgNDSilver 08/16/11 1.0 1.0 33891
SW6010B 8/15/11 406267mg/KgNDThallium 08/16/11 0.12 5.0 33891
SW6010B 8/15/11 406267mg/Kg19Vanadium 08/16/11 0.12 5.0 33891
SW6010B 8/15/11 406267mg/Kg22Zinc 08/16/11 0.59 5.0 33891
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/KgNDMercury 08/16/11 0.01 0.10 33931
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1221 08/18/11 0.0920 0.20 34191
SW8082 8/18/11 406326mg/KgNDAroclor1232 08/18/11 0.0460 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1242 08/18/11 0.0430 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1248 08/18/11 0.0360 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1254 08/18/11 0.0240 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1260 08/18/11 0.0270 0.10 34191
SW8082 8/18/11 406326%81.8TCMX (S) 08/18/11 50.4 136 34191
SW8082 8/18/11 406326%78.5DCBP (S) 08/18/11 55.1 113 34191
Page 37 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:00
1204.22
500 Kirkham
B-8-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 250 248 338525
SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 41.6 125 338525
SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 46.5 125 338525
SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 48.8 125 338525
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 25.9 125 338525
SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 48.8 125 338525
SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 27.8 125 338525
SW8270C 8/15/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 25.1 2500 338525
SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 39.4 125 338525
SW8270C 8/15/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 27.0 125 338525
SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 43.9 125 338525
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 25.9 125 338525
SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 52.5 125 338525
SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 35.3 125 338525
SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 17.6 125 338525
SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 20.0 125 338525
SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 21.8 248 338525
SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 19.9 248 338525
SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 50.3 2500 338525
SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 2120 125 338525
SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 22.1 125 338525
SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 39.4 125 338525
SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 27.8 125 338525
SW8270C 8/15/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 39.4 125 338525
SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 34.1 125 338525
SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 37.5 125 338525
SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 24.8 125 338525
SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 38.6 125 338525
SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 30.0 125 338525
SW8270C 8/15/11 406316mg/KgND1-Methylnaphthalene 08/16/11 30.0 125 338525
SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 10.5 125 338525
SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 36.0 125 338525
SW8270C 8/15/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 45.8 125 338525
SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 22.5 1240 338525
SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 26.3 125 338525
Page 38 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:00
1204.22
500 Kirkham
B-8-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 44.6 125 338525
SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 40.0 125 338525
SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 32.3 125 338525
SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 10.1 125 338525
SW8270C 8/15/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 32.5 125 338525
SW8270C 8/15/11 406316mg/KgND3-Nitroaniline 08/16/11 26.3 125 338525
SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 36.4 125 338525
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 11.3 1240 338525
SW8270C 8/15/11 406316mg/KgND4-Nitrophenol 08/16/11 25.1 125 338525
SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 29.6 125 338525
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 10.1 125 338525
SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 45.0 125 338525
SW8270C 8/15/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 45.0 125 338525
SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 44.3 125 338525
SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 37.5 125 338525
SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 30.4 125 338525
SW8270C 8/15/11 406316mg/KgND4-Nitroaniline 08/16/11 30.4 125 338525
SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 25.1 125 338525
SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 25.1 125 338525
SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 41.3 125 338525
SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 30.8 1240 338525
SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 38.3 125 338525
SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 38.6 1240 338525
SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 53.6 125 338525
SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 50.2 125 338525
SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 50.2 125 338525
SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 40.9 638 338525
SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 50.1 248 338525
SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 142 1240 338525
SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 55.6 125 338525
SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 33.8 125 338525
SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 56.6 125 338525
SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 57.8 125 338525
SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 66.8 125 338525
SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 31.5 125 338525
Page 39 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:00
1204.22
500 Kirkham
B-8-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 52.1 125 338525
SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 50.3 125 338525
SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 64.1 125 338525
SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 51.0 125 338525
SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 49.5 125 338525
SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 57.4 125 338525
SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 57.0 125 338525
SW8270C 8/15/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 57.0 125 338525
SW8270C 8/15/11 406316S,D %0.0002,4,6-Tribromophenol (S) 08/16/11 19 122 338525
SW8270C 8/15/11 406316S,D %0.0002-Fluorobiphenyl (S) 08/16/11 30 115 338525
SW8270C 8/15/11 406316S,D %0.0002-Fluorophenol (S) 08/16/11 25 121 338525
SW8270C 8/15/11 406316S,D %0.000Nitrobenzene-d5 (S) 08/16/11 23 120 338525
SW8270C 8/15/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 338525
SW8270C 8/15/11 406316S,D %0.000p-Terphenyl-d14 (S) 08/16/11 18 137 338525
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 13 78 NA1
8260TPH NA 406253%67.8(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 7.36 19 34184
SW8015B(M) 8/18/11 406325mg/Kg550TPH as Motor Oil 08/18/11 16.0 38 34184
SW8015B(M) 8/18/11 406325mg/Kg91.4Pentacosane (S) 08/18/11 59.7 129 34184
Page 40 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:05
1204.22
500 Kirkham
B-8-8.0
SoilSample Matrix:
Lab Sample ID: 1108084-006A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/24/11 406410mg/Kg3.8Lead 08/24/11 0.043 1.0 34791
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/25/11 406448mg/KgNDTPH as Motor Oil 08/25/11 1.65 4.0 34941
SW8015B(M) 8/25/11 406448mg/Kg117Pentacosane (S) 08/25/11 59.7 129 34941
Page 41 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:15
1204.22
500 Kirkham
B-2-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 4.0 9.2 NA1
SW8260B NA 406253ug/KgNDChloromethane 08/15/11 4.2 9.2 NA1
SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.4 9.2 NA1
SW8260B NA 406253ug/KgNDBromomethane 08/15/11 4.3 9.2 NA1
SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 2.7 9.2 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.4 9.2 NA1
SW8260B NA 406253ug/KgNDFreon 113 08/15/11 3.4 9.2 NA1
SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 1.8 9.2 NA1
SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 1.0 9.2 NA1
SW8260B NA 406253ug/KgNDMTBE 08/15/11 2.4 9.2 NA1
SW8260B NA 406253ug/KgNDtert-Butanol 08/15/11 19 46 NA1
SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 2.0 9.2 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 1.2 9.2 NA1
SW8260B NA 406253ug/KgNDETBE 08/15/11 2.2 9.2 NA1
SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.6 9.2 NA1
SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 1.1 9.2 NA1
SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 2.1 9.2 NA1
SW8260B NA 406253ug/KgNDChloroform 08/15/11 1.1 9.2 NA1
SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.5 9.2 NA1
SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 1.1 9.2 NA1
SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.3 9.2 NA1
SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.4 9.2 NA1
SW8260B NA 406253ug/KgNDTAME 08/15/11 1.9 9.2 NA1
SW8260B NA 406253ug/KgND1,2-Dichloroethane 08/15/11 1.8 9.2 NA1
SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 3.6 9.2 NA1
SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 2.0 9.2 NA1
SW8260B NA 406253ug/KgND1,2-Dichloropropane 08/15/11 1.2 9.2 NA1
SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 1.0 9.2 NA1
SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 4.1 9.2 NA1
SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.3 9.2 NA1
SW8260B NA 406253ug/KgNDToluene 08/15/11 0.90 9.2 NA1
SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.7 9.2 NA1
SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.1 9.2 NA1
SW8260B NA 406253ug/KgND1,1,2-Trichloroethane 08/15/11 1.7 9.2 NA1
SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 1.0 9.2 NA1
SW8260B NA 406253ug/KgND1,3-Dichloropropane 08/15/11 1.9 9.2 NA1
Page 42 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:15
1204.22
500 Kirkham
B-2-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.6 9.2 NA1
SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.79 9.2 NA1
SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 3.9 9.2 NA1
SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.79 9.2 NA1
SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.7 9.2 NA1
SW8260B NA 406253ug/KgNDo-Xylene 08/15/11 0.61 4.6 NA1
SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.70 9.2 NA1
SW8260B NA 406253ug/KgNDBromoform 08/15/11 1.7 9.2 NA1
SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 1.1 9.2 NA1
SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.3 9.2 NA1
SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 1.1 9.2 NA1
SW8260B NA 406253ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.8 9.2 NA1
SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.0 9.2 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 3.1 9.2 NA1
SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.5 9.2 NA1
SW8260B NA 406253ug/KgND2-Chlorotoluene 08/15/11 1.5 9.2 NA1
SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.3 9.2 NA1
SW8260B NA 406253ug/KgND1,2,4-Trimethylbenzene 08/15/11 1.0 9.2 NA1
SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.5 9.2 NA1
SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.3 9.2 NA1
SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.6 9.2 NA1
SW8260B NA 406253ug/KgND1,4-Dichlorobenzene 08/15/11 1.4 9.2 NA1
SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 2.0 9.2 NA1
SW8260B NA 406253ug/KgND1,2-Dichlorobenzene 08/15/11 1.2 9.2 NA1
SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.9 9.2 NA1
SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 2.3 9.2 NA1
SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 2.0 9.2 NA1
SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.6 9.2 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.6 9.2 NA1
SW8260B NA 406253%95.1(S) Dibromofluoromethane 08/15/11 59.8 148 NA1
SW8260B NA 406253%95.8(S) Toluene-d8 08/15/11 55.2 133 NA1
SW8260B NA 406253%117(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 43 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:15
1204.22
500 Kirkham
B-2-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/15/11 406267mg/KgNDAntimony 08/16/11 0.20 5.0 33891
SW6010B 8/15/11 406267mg/Kg5.3Arsenic 08/16/11 0.28 1.7 33891
SW6010B 8/15/11 406267mg/Kg100Barium 08/16/11 1 5.0 33891
SW6010B 8/15/11 406267mg/KgNDBeryllium 08/16/11 0.0840 2.0 33891
SW6010B 8/15/11 406267mg/KgNDCadmium 08/16/11 0.0590 1.0 33891
SW6010B 8/15/11 406267mg/Kg31Chromium 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/Kg6.9Cobalt 08/16/11 0.14 5.0 33891
SW6010B 8/15/11 406267mg/Kg44Copper 08/16/11 0.0900 5.0 33891
SW6010B 8/15/11 406267mg/Kg120Lead 08/16/11 0.043 1.0 33891
SW6010B 8/15/11 406267mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/Kg26Nickel 08/16/11 0.0590 5.0 33891
SW6010B 8/15/11 406267mg/KgNDSelenium 08/16/11 0.29 5.0 33891
SW6010B 8/15/11 406267mg/KgNDSilver 08/16/11 1.0 1.0 33891
SW6010B 8/15/11 406267mg/KgNDThallium 08/16/11 0.12 5.0 33891
SW6010B 8/15/11 406267mg/Kg30Vanadium 08/16/11 0.12 5.0 33891
SW6010B 8/15/11 406267mg/Kg120Zinc 08/16/11 0.59 5.0 33891
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/Kg0.31Mercury 08/16/11 0.01 0.10 33931
Page 44 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:15
1204.22
500 Kirkham
B-2-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8081A 8/18/11 406333ug/KgNDalpha-BHC 08/18/11 4.4 20 342010
SW8081A 8/18/11 406333ug/KgNDgamma-BHC 08/18/11 4.0 20 342010
SW8081A 8/18/11 406333ug/KgNDbeta-BHC 08/18/11 3.6 20 342010
SW8081A 8/18/11 406333ug/KgNDdelta-BHC 08/18/11 4.9 20 342010
SW8081A 8/18/11 406333ug/KgNDHeptachlor 08/18/11 11 20 342010
SW8081A 8/18/11 406333ug/KgNDAldrin 08/18/11 4.4 20 342010
SW8081A 8/18/11 406333ug/KgNDHeptachlor epoxide 08/18/11 3.2 20 342010
SW8081A 8/18/11 406333ug/KgNDgamma-Chlordane 08/18/11 4.2 20 342010
SW8081A 8/18/11 406333ug/KgNDalpha-Chlordane 08/18/11 3.6 20 342010
SW8081A 8/18/11 406333ug/KgNDEndosulfan I 08/18/11 5.9 20 342010
SW8081A 8/18/11 406333ug/KgND4,4'-DDE 08/18/11 4.8 20 342010
SW8081A 8/18/11 406333ug/KgNDDieldrin 08/18/11 4.3 20 342010
SW8081A 8/18/11 406333ug/KgNDEndrin 08/18/11 5.7 20 342010
SW8081A 8/18/11 406333ug/KgND4,4'-DDD 08/18/11 4.7 20 342010
SW8081A 8/18/11 406333ug/KgNDEndosulfan II 08/18/11 15 20 342010
SW8081A 8/18/11 406333ug/KgND4,4'-DDT 08/18/11 8.1 20 342010
SW8081A 8/18/11 406333ug/KgNDEndrin aldehyde 08/18/11 10 20 342010
SW8081A 8/18/11 406333ug/KgNDEndosulfan sulfate 08/18/11 4.9 20 342010
SW8081A 8/18/11 406333ug/KgNDMethoxychlor 08/18/11 6.2 50 342010
SW8081A 8/18/11 406333ug/KgNDEndrin Ketone 08/18/11 4.0 20 342010
SW8081A 8/18/11 406333ug/KgNDChlordane 08/18/11 100 200 342010
SW8081A 8/18/11 406333ug/KgNDToxaphene 08/18/11 100 100 342010
SW8081A 8/18/11 406333%91.5TCMX (S) 08/18/11 52.5 139 342010
SW8081A 8/18/11 406333%90.0DCBP (S) 08/18/11 50.2 139 342010
Reporting limits increased due to the nature of the sample matrix (dark color extract). Toxaphene reported to the MDL.NOTE:
Page 45 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:15
1204.22
500 Kirkham
B-2-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1221 08/18/11 0.0920 0.20 34191
SW8082 8/18/11 406326mg/KgNDAroclor1232 08/18/11 0.0460 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1242 08/18/11 0.0430 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1248 08/18/11 0.0360 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1254 08/18/11 0.0240 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1260 08/18/11 0.0270 0.10 34191
SW8082 8/18/11 406326%88.5TCMX (S) 08/18/11 50.4 136 34191
SW8082 8/18/11 406326%94.6DCBP (S) 08/18/11 55.1 113 34191
Page 46 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:15
1204.22
500 Kirkham
B-2-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 200 198 338520
SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 33.3 100 338520
SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 37.2 100 338520
SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 39.0 100 338520
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 20.7 100 338520
SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 39.0 100 338520
SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 22.2 100 338520
SW8270C 8/15/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 20.1 2000 338520
SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 31.5 100 338520
SW8270C 8/15/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 21.6 100 338520
SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 35.1 100 338520
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 20.7 100 338520
SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 42.0 100 338520
SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 28.2 100 338520
SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 14.1 100 338520
SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 16.0 100 338520
SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 17.4 198 338520
SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 15.9 198 338520
SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 40.2 2000 338520
SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 1700 100 338520
SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 17.7 100 338520
SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 31.5 100 338520
SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 22.2 100 338520
SW8270C 8/15/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 31.5 100 338520
SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 27.3 100 338520
SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 30.0 100 338520
SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 19.8 100 338520
SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 30.9 100 338520
SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 24.0 100 338520
SW8270C 8/15/11 406316mg/KgND1-Methylnaphthalene 08/16/11 24.0 100 338520
SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 8.40 100 338520
SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 28.8 100 338520
SW8270C 8/15/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 36.6 100 338520
SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 18.0 990 338520
SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 21.0 100 338520
Page 47 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:15
1204.22
500 Kirkham
B-2-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 35.7 100 338520
SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 32.0 100 338520
SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 25.8 100 338520
SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 8.10 100 338520
SW8270C 8/15/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 26.0 100 338520
SW8270C 8/15/11 406316mg/KgND3-Nitroaniline 08/16/11 21.0 100 338520
SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 29.1 100 338520
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 9.00 990 338520
SW8270C 8/15/11 406316mg/KgND4-Nitrophenol 08/16/11 20.1 100 338520
SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 23.7 100 338520
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 8.10 100 338520
SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 36.0 100 338520
SW8270C 8/15/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 36.0 100 338520
SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 35.4 100 338520
SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 30.0 100 338520
SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 24.3 100 338520
SW8270C 8/15/11 406316mg/KgND4-Nitroaniline 08/16/11 24.3 100 338520
SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 20.1 100 338520
SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 20.1 100 338520
SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 33.0 100 338520
SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 24.6 990 338520
SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 30.6 100 338520
SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 30.9 990 338520
SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 42.9 100 338520
SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 40.1 100 338520
SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 40.1 100 338520
SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 32.7 510 338520
SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 40.1 198 338520
SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 113 990 338520
SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 44.5 100 338520
SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 27.0 100 338520
SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 45.3 100 338520
SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 46.2 100 338520
SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 53.4 100 338520
SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 25.2 100 338520
Page 48 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:15
1204.22
500 Kirkham
B-2-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 41.7 100 338520
SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 40.2 100 338520
SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 51.3 100 338520
SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 40.8 100 338520
SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 39.6 100 338520
SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 45.9 100 338520
SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 45.6 100 338520
SW8270C 8/15/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 45.6 100 338520
SW8270C 8/15/11 406316S,D %0.0002,4,6-Tribromophenol (S) 08/16/11 19 122 338520
SW8270C 8/15/11 406316S,D %0.0002-Fluorobiphenyl (S) 08/16/11 30 115 338520
SW8270C 8/15/11 406316S,D %0.0002-Fluorophenol (S) 08/16/11 25 121 338520
SW8270C 8/15/11 406316S,D %0.000Nitrobenzene-d5 (S) 08/16/11 23 120 338520
SW8270C 8/15/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 338520
SW8270C 8/15/11 406316S,D %0.000p-Terphenyl-d14 (S) 08/16/11 18 137 338520
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 16 92 NA1
8260TPH NA 406253%60.8(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 1.84 4.8 34181
SW8015B(M) 8/18/11 406325mg/Kg120TPH as Motor Oil 08/18/11 4.00 9.6 34181
SW8015B(M) 8/18/11 406325mg/Kg86.1Pentacosane (S) 08/18/11 59.7 129 34181
Page 49 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-2-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-008A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 4.1 9.3 NA1
SW8260B NA 406253ug/KgNDChloromethane 08/15/11 4.3 9.3 NA1
SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.5 9.3 NA1
SW8260B NA 406253ug/KgNDBromomethane 08/15/11 4.3 9.3 NA1
SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 2.7 9.3 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.4 9.3 NA1
SW8260B NA 406253ug/KgNDFreon 113 08/15/11 3.5 9.3 NA1
SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 1.8 9.3 NA1
SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 1.0 9.3 NA1
SW8260B NA 406253ug/KgNDMTBE 08/15/11 2.4 9.3 NA1
SW8260B NA 406253ug/KgNDtert-Butanol 08/15/11 19 47 NA1
SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 2.0 9.3 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 1.2 9.3 NA1
SW8260B NA 406253ug/KgNDETBE 08/15/11 2.2 9.3 NA1
SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.6 9.3 NA1
SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 1.2 9.3 NA1
SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 2.1 9.3 NA1
SW8260B NA 406253ug/KgNDChloroform 08/15/11 1.1 9.3 NA1
SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.5 9.3 NA1
SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 1.1 9.3 NA1
SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.3 9.3 NA1
SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.4 9.3 NA1
SW8260B NA 406253ug/KgNDTAME 08/15/11 1.9 9.3 NA1
SW8260B NA 406253ug/KgND1,2-Dichloroethane 08/15/11 1.8 9.3 NA1
SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 3.6 9.3 NA1
SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 2.0 9.3 NA1
SW8260B NA 406253ug/KgND1,2-Dichloropropane 08/15/11 1.2 9.3 NA1
SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 1.0 9.3 NA1
SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 4.2 9.3 NA1
SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.3 9.3 NA1
SW8260B NA 406253ug/KgNDToluene 08/15/11 0.91 9.3 NA1
SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.7 9.3 NA1
SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.1 9.3 NA1
SW8260B NA 406253ug/KgND1,1,2-Trichloroethane 08/15/11 1.7 9.3 NA1
SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 1.0 9.3 NA1
SW8260B NA 406253ug/KgND1,3-Dichloropropane 08/15/11 1.9 9.3 NA1
Page 50 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-2-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-008A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.6 9.3 NA1
SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.80 9.3 NA1
SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 3.9 9.3 NA1
SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.80 9.3 NA1
SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.7 9.3 NA1
SW8260B NA 406253ug/KgNDo-Xylene 08/15/11 0.61 4.7 NA1
SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.71 9.3 NA1
SW8260B NA 406253ug/KgNDBromoform 08/15/11 1.8 9.3 NA1
SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 1.2 9.3 NA1
SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.3 9.3 NA1
SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 1.1 9.3 NA1
SW8260B NA 406253ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.8 9.3 NA1
SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.0 9.3 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 3.1 9.3 NA1
SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.5 9.3 NA1
SW8260B NA 406253ug/KgND2-Chlorotoluene 08/15/11 1.5 9.3 NA1
SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.3 9.3 NA1
SW8260B NA 406253ug/KgND1,2,4-Trimethylbenzene 08/15/11 1.0 9.3 NA1
SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.5 9.3 NA1
SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.4 9.3 NA1
SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.7 9.3 NA1
SW8260B NA 406253ug/KgND1,4-Dichlorobenzene 08/15/11 1.4 9.3 NA1
SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 2.0 9.3 NA1
SW8260B NA 406253ug/KgND1,2-Dichlorobenzene 08/15/11 1.2 9.3 NA1
SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.9 9.3 NA1
SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 2.4 9.3 NA1
SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 2.0 9.3 NA1
SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.6 9.3 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.7 9.3 NA1
SW8260B NA 406253%96.7(S) Dibromofluoromethane 08/15/11 59.8 148 NA1
SW8260B NA 406253%91.2(S) Toluene-d8 08/15/11 55.2 133 NA1
SW8260B NA 406253%112(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 51 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-2-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-008A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/25/11 406447mg/L4.6Lead (STLC) 08/26/11 0.0500 0.10 34961
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/24/11 406421mg/LNDLead (TCLP) 08/25/11 0.05 0.10 34891
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/16/11 406288mg/KgNDAntimony 08/17/11 0.20 5.0 34051
SW6010B 8/16/11 406288mg/Kg6.6Arsenic 08/17/11 0.28 1.7 34051
SW6010B 8/16/11 406288mg/Kg190Barium 08/17/11 1 5.0 34051
SW6010B 8/16/11 406288mg/KgNDBeryllium 08/17/11 0.0840 2.0 34051
SW6010B 8/16/11 406288mg/KgNDCadmium 08/17/11 0.0590 1.0 34051
SW6010B 8/16/11 406288mg/Kg21Chromium 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/Kg12Cobalt 08/17/11 0.14 5.0 34051
SW6010B 8/16/11 406288mg/Kg40Copper 08/17/11 0.0900 5.0 34051
SW6010B 8/16/11 406288mg/Kg130Lead 08/17/11 0.043 1.0 34051
SW6010B 8/16/11 406288mg/KgNDMolybdenum 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/Kg21Nickel 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSelenium 08/17/11 0.29 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSilver 08/17/11 1.0 1.0 34051
SW6010B 8/16/11 406288mg/KgNDThallium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg37Vanadium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg130Zinc 08/17/11 0.59 5.0 34051
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/Kg0.24Mercury 08/16/11 0.01 0.10 33931
Page 52 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-2-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-008A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1221 08/18/11 0.0920 0.20 34191
SW8082 8/18/11 406326mg/KgNDAroclor1232 08/18/11 0.0460 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1242 08/18/11 0.0430 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1248 08/18/11 0.0360 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1254 08/18/11 0.0240 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1260 08/18/11 0.0270 0.10 34191
SW8082 8/18/11 406326%87.0TCMX (S) 08/18/11 50.4 136 34191
SW8082 8/18/11 406326%100DCBP (S) 08/18/11 55.1 113 34191
Page 53 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-2-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-008A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 100 99.0 338510
SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 16.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 18.6 50.0 338510
SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 19.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 10.4 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 19.5 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 11.1 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 10.1 999 338510
SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 15.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 10.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 17.6 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 10.4 50.0 338510
SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 21.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 14.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 7.05 50.0 338510
SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 8.00 50.0 338510
SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 8.70 99.0 338510
SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 7.95 99.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 20.1 999 338510
SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 848 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 8.85 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 15.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 11.1 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 15.8 50.0 338510
SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 13.7 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 15.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 9.90 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 15.5 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 12.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND1-Methylnaphthalene 08/16/11 12.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 4.20 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 14.4 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 18.3 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 9.00 495 338510
SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 10.5 50.0 338510
Page 54 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-2-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-008A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 17.9 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 16.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 12.9 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 4.05 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 13.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND3-Nitroaniline 08/16/11 10.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 14.6 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 4.50 495 338510
SW8270C 8/15/11 406316mg/KgND4-Nitrophenol 08/16/11 10.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 11.9 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 4.05 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 18.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 18.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 17.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 15.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 12.2 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Nitroaniline 08/16/11 12.2 50.0 338510
SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 10.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 10.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 16.5 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 12.3 495 338510
SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 15.3 50.0 338510
SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 15.5 495 338510
SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 21.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 20.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 20.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 16.4 255 338510
SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 20.1 99.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 56.7 495 338510
SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 22.3 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 13.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 22.7 50.0 338510
SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 23.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 26.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 12.6 50.0 338510
Page 55 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-2-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-008A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 20.9 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 20.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 25.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 20.4 50.0 338510
SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 19.8 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 23.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 22.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 22.8 50.0 338510
SW8270C 8/15/11 406316S,D %0.0002,4,6-Tribromophenol (S) 08/16/11 19 122 338510
SW8270C 8/15/11 406316S,D %0.0002-Fluorobiphenyl (S) 08/16/11 30 115 338510
SW8270C 8/15/11 406316S,D %0.0002-Fluorophenol (S) 08/16/11 25 121 338510
SW8270C 8/15/11 406316S,D %0.000Nitrobenzene-d5 (S) 08/16/11 23 120 338510
SW8270C 8/15/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 338510
SW8270C 8/15/11 406316S,D %0.000p-Terphenyl-d14 (S) 08/16/11 18 137 338510
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 16 93 NA1
8260TPH NA 406253%72.4(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 1.84 4.8 34181
SW8015B(M) 8/18/11 406325mg/Kg160TPH as Motor Oil 08/18/11 4.00 9.6 34181
SW8015B(M) 8/18/11 406325mg/Kg83.7Pentacosane (S) 08/18/11 59.7 129 34181
Page 56 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:25
1204.22
500 Kirkham
B-2-9.0
SoilSample Matrix:
Lab Sample ID: 1108084-009A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/24/11 406410mg/Kg2.1Lead 08/24/11 0.043 1.0 34791
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/25/11 406448mg/KgNDTPH as Motor Oil 08/25/11 1.65 4.0 34941
SW8015B(M) 8/25/11 406448mg/Kg95.3Pentacosane (S) 08/25/11 59.7 129 34941
Page 57 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:30
1204.22
500 Kirkham
B-7-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 4.5 10 NA1
SW8260B NA 406253ug/KgNDChloromethane 08/15/11 4.7 10 NA1
SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.7 10 NA1
SW8260B NA 406253ug/KgNDBromomethane 08/15/11 4.8 10 NA1
SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 3.0 10 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.6 10 NA1
SW8260B NA 406253ug/KgNDFreon 113 08/15/11 3.8 10 NA1
SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 2.0 10 NA1
SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 1.1 10 NA1
SW8260B NA 406253ug/KgNDMTBE 08/15/11 2.7 10 NA1
SW8260B NA 406253ug/KgNDtert-Butanol 08/15/11 21 52 NA1
SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 2.3 10 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 1.3 10 NA1
SW8260B NA 406253ug/KgNDETBE 08/15/11 2.5 10 NA1
SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.8 10 NA1
SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 1.3 10 NA1
SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 2.4 10 NA1
SW8260B NA 406253ug/KgNDChloroform 08/15/11 1.3 10 NA1
SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.7 10 NA1
SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 1.3 10 NA1
SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.5 10 NA1
SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.5 10 NA1
SW8260B NA 406253ug/KgNDTAME 08/15/11 2.1 10 NA1
SW8260B NA 406253ug/KgND1,2-Dichloroethane 08/15/11 2.0 10 NA1
SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 4.0 10 NA1
SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 2.3 10 NA1
SW8260B NA 406253ug/KgND1,2-Dichloropropane 08/15/11 1.3 10 NA1
SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 1.2 10 NA1
SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 4.6 10 NA1
SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.5 10 NA1
SW8260B NA 406253ug/KgNDToluene 08/15/11 1.0 10 NA1
SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.9 10 NA1
SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.2 10 NA1
SW8260B NA 406253ug/KgND1,1,2-Trichloroethane 08/15/11 1.9 10 NA1
SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 1.2 10 NA1
SW8260B NA 406253ug/KgND1,3-Dichloropropane 08/15/11 2.1 10 NA1
Page 58 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:30
1204.22
500 Kirkham
B-7-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.8 10 NA1
SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.89 10 NA1
SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 4.3 10 NA1
SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.88 10 NA1
SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.9 10 NA1
SW8260B NA 406253ug/KgNDo-Xylene 08/15/11 0.68 5.2 NA1
SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.79 10 NA1
SW8260B NA 406253ug/KgNDBromoform 08/15/11 2.0 10 NA1
SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 1.3 10 NA1
SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.5 10 NA1
SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 1.2 10 NA1
SW8260B NA 406253ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 3.1 10 NA1
SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.2 10 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 3.4 10 NA1
SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.6 10 NA1
SW8260B NA 406253ug/KgND2-Chlorotoluene 08/15/11 1.6 10 NA1
SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.5 10 NA1
SW8260B NA 406253ug/KgND1,2,4-Trimethylbenzene 08/15/11 1.1 10 NA1
SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.7 10 NA1
SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.5 10 NA1
SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.8 10 NA1
SW8260B NA 406253ug/KgND1,4-Dichlorobenzene 08/15/11 1.5 10 NA1
SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 2.3 10 NA1
SW8260B NA 406253ug/KgND1,2-Dichlorobenzene 08/15/11 1.4 10 NA1
SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 4.4 10 NA1
SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 2.6 10 NA1
SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 2.2 10 NA1
SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.9 10 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichlorobenzene 08/15/11 3.0 10 NA1
SW8260B NA 406253%95.6(S) Dibromofluoromethane 08/15/11 59.8 148 NA1
SW8260B NA 406253%86.7(S) Toluene-d8 08/15/11 55.2 133 NA1
SW8260B NA 406253%103(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 59 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:30
1204.22
500 Kirkham
B-7-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/25/11 406447mg/L5.7Lead (STLC) 08/26/11 0.0500 0.10 34961
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/16/11 406288mg/KgNDAntimony 08/17/11 0.20 5.0 34051
SW6010B 8/16/11 406288mg/KgNDArsenic 08/17/11 0.28 1.7 34051
SW6010B 8/16/11 406288mg/Kg53Barium 08/17/11 1 5.0 34051
SW6010B 8/16/11 406288mg/KgNDBeryllium 08/17/11 0.0840 2.0 34051
SW6010B 8/16/11 406288mg/KgNDCadmium 08/17/11 0.0590 1.0 34051
SW6010B 8/16/11 406288mg/Kg29Chromium 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/KgNDCobalt 08/17/11 0.14 5.0 34051
SW6010B 8/16/11 406288mg/Kg6.8Copper 08/17/11 0.0900 5.0 34051
SW6010B 8/16/11 406288mg/Kg50Lead 08/17/11 0.043 1.0 34051
SW6010B 8/16/11 406288mg/KgNDMolybdenum 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/Kg14Nickel 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSelenium 08/17/11 0.29 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSilver 08/17/11 1.0 1.0 34051
SW6010B 8/16/11 406288mg/KgNDThallium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg21Vanadium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg130Zinc 08/17/11 0.59 5.0 34051
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/Kg0.12Mercury 08/16/11 0.01 0.10 33931
Page 60 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:30
1204.22
500 Kirkham
B-7-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8081A 8/18/11 406333ug/KgNDalpha-BHC 08/18/11 0.44 2.0 34201
SW8081A 8/18/11 406333ug/KgNDgamma-BHC 08/18/11 0.40 2.0 34201
SW8081A 8/18/11 406333ug/KgNDbeta-BHC 08/18/11 0.36 2.0 34201
SW8081A 8/18/11 406333ug/KgNDdelta-BHC 08/18/11 0.49 2.0 34201
SW8081A 8/18/11 406333ug/KgNDHeptachlor 08/18/11 1.1 2.0 34201
SW8081A 8/18/11 406333ug/KgNDAldrin 08/18/11 0.44 2.0 34201
SW8081A 8/18/11 406333ug/KgNDHeptachlor epoxide 08/18/11 0.32 2.0 34201
SW8081A 8/18/11 406333ug/KgNDgamma-Chlordane 08/18/11 0.42 2.0 34201
SW8081A 8/18/11 406333ug/KgNDalpha-Chlordane 08/18/11 0.36 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndosulfan I 08/18/11 0.59 2.0 34201
SW8081A 8/18/11 406333ug/KgND4,4'-DDE 08/18/11 0.48 2.0 34201
SW8081A 8/18/11 406333ug/KgNDDieldrin 08/18/11 0.43 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndrin 08/18/11 0.57 2.0 34201
SW8081A 8/18/11 406333ug/KgND4,4'-DDD 08/18/11 0.47 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndosulfan II 08/18/11 1.5 2.0 34201
SW8081A 8/18/11 406333ug/KgND4,4'-DDT 08/18/11 0.81 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndrin aldehyde 08/18/11 1.0 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndosulfan sulfate 08/18/11 0.49 2.0 34201
SW8081A 8/18/11 406333ug/KgNDMethoxychlor 08/18/11 0.62 5.0 34201
SW8081A 8/18/11 406333ug/KgNDEndrin Ketone 08/18/11 0.40 2.0 34201
SW8081A 8/18/11 406333ug/KgNDChlordane 08/18/11 10 20 34201
SW8081A 8/18/11 406333ug/KgNDToxaphene 08/18/11 10 100 34201
SW8081A 8/18/11 406333%85.0TCMX (S) 08/18/11 52.5 139 34201
SW8081A 8/18/11 406333%58.9DCBP (S) 08/18/11 50.2 139 34201
Reporting limits increased due to the nature of the sample matrix (dark color extract). Toxaphene reported to the MDL.NOTE:
Page 61 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:30
1204.22
500 Kirkham
B-7-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1221 08/18/11 0.0920 0.20 34191
SW8082 8/18/11 406326mg/KgNDAroclor1232 08/18/11 0.0460 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1242 08/18/11 0.0430 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1248 08/18/11 0.0360 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1254 08/18/11 0.0240 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1260 08/18/11 0.0270 0.10 34191
SW8082 8/18/11 406326%87.2TCMX (S) 08/18/11 50.4 136 34191
SW8082 8/18/11 406326%87.9DCBP (S) 08/18/11 55.1 113 34191
Page 62 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:30
1204.22
500 Kirkham
B-7-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 100 99.0 338510
SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 16.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 18.6 50.0 338510
SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 19.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 10.4 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 19.5 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 11.1 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 10.1 999 338510
SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 15.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 10.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 17.6 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 10.4 50.0 338510
SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 21.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 14.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 7.05 50.0 338510
SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 8.00 50.0 338510
SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 8.70 99.0 338510
SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 7.95 99.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 20.1 999 338510
SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 848 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 8.85 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 15.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 11.1 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 15.8 50.0 338510
SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 13.7 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 15.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 9.90 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 15.5 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 12.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND1-Methylnaphthalene 08/16/11 12.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 4.20 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 14.4 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 18.3 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 9.00 495 338510
SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 10.5 50.0 338510
Page 63 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:30
1204.22
500 Kirkham
B-7-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 17.9 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 16.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 12.9 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 4.05 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 13.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND3-Nitroaniline 08/16/11 10.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 14.6 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 4.50 495 338510
SW8270C 8/15/11 406316mg/KgND4-Nitrophenol 08/16/11 10.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 11.9 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 4.05 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 18.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 18.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 17.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 15.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 12.2 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Nitroaniline 08/16/11 12.2 50.0 338510
SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 10.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 10.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 16.5 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 12.3 495 338510
SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 15.3 50.0 338510
SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 15.5 495 338510
SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 21.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 20.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 20.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 16.4 255 338510
SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 20.1 99.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 56.7 495 338510
SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 22.3 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 13.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 22.7 50.0 338510
SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 23.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 26.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 12.6 50.0 338510
Page 64 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:30
1204.22
500 Kirkham
B-7-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-010A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 20.9 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 20.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 25.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 20.4 50.0 338510
SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 19.8 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 23.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 22.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 22.8 50.0 338510
SW8270C 8/15/11 406316S,D %0.0002,4,6-Tribromophenol (S) 08/16/11 19 122 338510
SW8270C 8/15/11 406316S,D %0.0002-Fluorobiphenyl (S) 08/16/11 30 115 338510
SW8270C 8/15/11 406316S,D %0.0002-Fluorophenol (S) 08/16/11 25 121 338510
SW8270C 8/15/11 406316S,D %0.000Nitrobenzene-d5 (S) 08/16/11 23 120 338510
SW8270C 8/15/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 338510
SW8270C 8/15/11 406316S,D %0.000p-Terphenyl-d14 (S) 08/16/11 18 137 338510
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 18 100 NA1
8260TPH NA 406253%85.0(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 0.759 2.0 34181
SW8015B(M) 8/18/11 406325mg/Kg9.2TPH as Motor Oil 08/18/11 1.65 4.0 34181
SW8015B(M) 8/18/11 406325mg/Kg104Pentacosane (S) 08/18/11 59.7 129 34181
Page 65 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:35
1204.22
500 Kirkham
B-7-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-011A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 3.4 7.7 NA1
SW8260B NA 406253ug/KgNDChloromethane 08/15/11 3.5 7.7 NA1
SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.0 7.7 NA1
SW8260B NA 406253ug/KgNDBromomethane 08/15/11 3.6 7.7 NA1
SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 2.2 7.7 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.2 7.7 NA1
SW8260B NA 406253ug/KgNDFreon 113 08/15/11 2.9 7.7 NA1
SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 1.5 7.7 NA1
SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.86 7.7 NA1
SW8260B NA 406253ug/KgNDMTBE 08/15/11 2.0 7.7 NA1
SW8260B NA 406253ug/KgNDtert-Butanol 08/15/11 16 39 NA1
SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.7 7.7 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 0.98 7.7 NA1
SW8260B NA 406253ug/KgNDETBE 08/15/11 1.9 7.7 NA1
SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.4 7.7 NA1
SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 0.95 7.7 NA1
SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 1.8 7.7 NA1
SW8260B NA 406253ug/KgNDChloroform 08/15/11 0.94 7.7 NA1
SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.2 7.7 NA1
SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 0.94 7.7 NA1
SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.1 7.7 NA1
SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.2 7.7 NA1
SW8260B NA 406253ug/KgNDTAME 08/15/11 1.6 7.7 NA1
SW8260B NA 406253ug/KgND1,2-Dichloroethane 08/15/11 1.5 7.7 NA1
SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 3.0 7.7 NA1
SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 1.7 7.7 NA1
SW8260B NA 406253ug/KgND1,2-Dichloropropane 08/15/11 1.0 7.7 NA1
SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 0.86 7.7 NA1
SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 3.5 7.7 NA1
SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.1 7.7 NA1
SW8260B NA 406253ug/KgNDToluene 08/15/11 0.76 7.7 NA1
SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.4 7.7 NA1
SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.89 7.7 NA1
SW8260B NA 406253ug/KgND1,1,2-Trichloroethane 08/15/11 1.4 7.7 NA1
SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 0.86 7.7 NA1
SW8260B NA 406253ug/KgND1,3-Dichloropropane 08/15/11 1.6 7.7 NA1
Page 66 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:35
1204.22
500 Kirkham
B-7-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-011A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.3 7.7 NA1
SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.66 7.7 NA1
SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 3.2 7.7 NA1
SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.66 7.7 NA1
SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.4 7.7 NA1
SW8260B NA 406253ug/KgNDo-Xylene 08/15/11 0.51 3.9 NA1
SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.59 7.7 NA1
SW8260B NA 406253ug/KgNDBromoform 08/15/11 1.5 7.7 NA1
SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 0.95 7.7 NA1
SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.1 7.7 NA1
SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 0.91 7.7 NA1
SW8260B NA 406253ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.3 7.7 NA1
SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.87 7.7 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 2.6 7.7 NA1
SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.2 7.7 NA1
SW8260B NA 406253ug/KgND2-Chlorotoluene 08/15/11 1.2 7.7 NA1
SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.1 7.7 NA1
SW8260B NA 406253ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.84 7.7 NA1
SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.3 7.7 NA1
SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.1 7.7 NA1
SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.4 7.7 NA1
SW8260B NA 406253ug/KgND1,4-Dichlorobenzene 08/15/11 1.2 7.7 NA1
SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 1.7 7.7 NA1
SW8260B NA 406253ug/KgND1,2-Dichlorobenzene 08/15/11 1.0 7.7 NA1
SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.3 7.7 NA1
SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 2.0 7.7 NA1
SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.6 7.7 NA1
SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.2 7.7 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.2 7.7 NA1
SW8260B NA 406253%93.6(S) Dibromofluoromethane 08/15/11 59.8 148 NA1
SW8260B NA 406253%91.1(S) Toluene-d8 08/15/11 55.2 133 NA1
SW8260B NA 406253%102(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 67 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:35
1204.22
500 Kirkham
B-7-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-011A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/16/11 406288mg/KgNDAntimony 08/17/11 0.20 5.0 34051
SW6010B 8/16/11 406288mg/KgNDArsenic 08/17/11 0.28 1.7 34051
SW6010B 8/16/11 406288mg/Kg58Barium 08/17/11 1 5.0 34051
SW6010B 8/16/11 406288mg/KgNDBeryllium 08/17/11 0.0840 2.0 34051
SW6010B 8/16/11 406288mg/KgNDCadmium 08/17/11 0.0590 1.0 34051
SW6010B 8/16/11 406288mg/Kg25Chromium 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/KgNDCobalt 08/17/11 0.14 5.0 34051
SW6010B 8/16/11 406288mg/KgNDCopper 08/17/11 0.0900 5.0 34051
SW6010B 8/16/11 406288mg/Kg4.2Lead 08/17/11 0.043 1.0 34051
SW6010B 8/16/11 406288mg/KgNDMolybdenum 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/Kg12Nickel 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSelenium 08/17/11 0.29 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSilver 08/17/11 1.0 1.0 34051
SW6010B 8/16/11 406288mg/KgNDThallium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg16Vanadium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg13Zinc 08/17/11 0.59 5.0 34051
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/KgNDMercury 08/16/11 0.01 0.10 33931
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1221 08/18/11 0.0920 0.20 34191
SW8082 8/18/11 406326mg/KgNDAroclor1232 08/18/11 0.0460 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1242 08/18/11 0.0430 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1248 08/18/11 0.0360 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1254 08/18/11 0.0240 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1260 08/18/11 0.0270 0.10 34191
SW8082 8/18/11 406326%67.8TCMX (S) 08/18/11 50.4 136 34191
SW8082 8/18/11 406326S %52.5DCBP (S) 08/18/11 55.1 113 34191
Surrogate recovery of DCBP is bias low possibly due to matrix effects; recovery of second surrogate supports data quality.NOTE:
Page 68 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:35
1204.22
500 Kirkham
B-7-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-011A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 0.660 0.653 33851
SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 0.110 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 0.123 0.330 33851
SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 0.129 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 0.0683 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 0.129 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 0.0733 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 0.0663 6.59 33851
SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 0.0713 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 0.116 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 0.0683 0.330 33851
SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 0.139 0.330 33851
SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 0.0931 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 0.0465 0.330 33851
SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 0.0528 0.330 33851
SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 0.0574 0.653 33851
SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 0.0525 0.653 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 0.133 6.59 33851
SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 5.59 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 0.0584 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 0.0733 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 0.0901 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 0.0990 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 0.0653 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 0.102 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 0.0792 0.330 33851
SW8270C 8/15/11 406316mg/KgND1-Methylnaphthalene 08/16/11 0.0792 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 0.0277 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 0.0950 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 0.121 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 0.0594 3.27 33851
SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 0.0693 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 0.118 0.330 33851
Page 69 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:35
1204.22
500 Kirkham
B-7-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-011A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 0.106 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 0.0851 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 0.0267 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 0.0858 0.330 33851
SW8270C 8/15/11 406316mg/KgND3-Nitroaniline 08/16/11 0.0693 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 0.0960 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 0.0297 3.27 33851
SW8270C 8/15/11 406316mg/KgND4-Nitrophenol 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 0.0782 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 0.0267 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 0.119 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 0.119 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 0.117 0.330 33851
SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 0.0990 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 0.0802 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Nitroaniline 08/16/11 0.0802 0.330 33851
SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 0.109 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 0.0812 3.27 33851
SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 0.101 0.330 33851
SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 0.102 3.27 33851
SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 0.142 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 0.132 0.330 33851
SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 0.132 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 0.108 1.68 33851
SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 0.132 0.653 33851
SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 0.374 3.27 33851
SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 0.147 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 0.0891 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 0.149 0.330 33851
SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 0.152 0.330 33851
SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 0.176 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 0.0832 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 0.138 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 0.133 0.330 33851
Page 70 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:35
1204.22
500 Kirkham
B-7-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-011A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 0.169 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 0.135 0.330 33851
SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 0.131 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 0.151 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 0.150 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 0.150 0.330 33851
SW8270C 8/15/11 406316%48.92,4,6-Tribromophenol (S) 08/16/11 19 122 33851
SW8270C 8/15/11 406316%62.32-Fluorobiphenyl (S) 08/16/11 30 115 33851
SW8270C 8/15/11 406316%74.12-Fluorophenol (S) 08/16/11 25 121 33851
SW8270C 8/15/11 406316%63.4Nitrobenzene-d5 (S) 08/16/11 23 120 33851
SW8270C 8/15/11 406316%77.2Phenol-d6 (S) 08/16/11 24 113 33851
SW8270C 8/15/11 406316%80.9p-Terphenyl-d14 (S) 08/16/11 18 137 33851
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 13 77 NA1
8260TPH NA 406253%67.2(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 0.759 2.0 34181
SW8015B(M) 8/18/11 406325mg/Kg5.2TPH as Motor Oil 08/18/11 1.65 4.0 34181
SW8015B(M) 8/18/11 406325mg/Kg104Pentacosane (S) 08/18/11 59.7 129 34181
Page 71 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:55
1204.22
500 Kirkham
B-6-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 4.1 9.4 NA1
SW8260B NA 406253ug/KgNDChloromethane 08/15/11 4.3 9.4 NA1
SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.5 9.4 NA1
SW8260B NA 406253ug/KgNDBromomethane 08/15/11 4.4 9.4 NA1
SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 2.7 9.4 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.5 9.4 NA1
SW8260B NA 406253ug/KgNDFreon 113 08/15/11 3.5 9.4 NA1
SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 1.9 9.4 NA1
SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 1.0 9.4 NA1
SW8260B NA 406253ug/KgNDMTBE 08/15/11 2.4 9.4 NA1
SW8260B NA 406253ug/KgNDtert-Butanol 08/15/11 20 47 NA1
SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 2.1 9.4 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 1.2 9.4 NA1
SW8260B NA 406253ug/KgNDETBE 08/15/11 2.3 9.4 NA1
SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.7 9.4 NA1
SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 1.2 9.4 NA1
SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 2.2 9.4 NA1
SW8260B NA 406253ug/KgNDChloroform 08/15/11 1.1 9.4 NA1
SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.5 9.4 NA1
SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 1.1 9.4 NA1
SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.4 9.4 NA1
SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.4 9.4 NA1
SW8260B NA 406253ug/KgNDTAME 08/15/11 1.9 9.4 NA1
SW8260B NA 406253ug/KgND1,2-Dichloroethane 08/15/11 1.8 9.4 NA1
SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 3.6 9.4 NA1
SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 2.1 9.4 NA1
SW8260B NA 406253ug/KgND1,2-Dichloropropane 08/15/11 1.2 9.4 NA1
SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 1.0 9.4 NA1
SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 4.2 9.4 NA1
SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.3 9.4 NA1
SW8260B NA 406253ug/KgNDToluene 08/15/11 0.92 9.4 NA1
SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.7 9.4 NA1
SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.1 9.4 NA1
SW8260B NA 406253ug/KgND1,1,2-Trichloroethane 08/15/11 1.7 9.4 NA1
SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 1.1 9.4 NA1
SW8260B NA 406253ug/KgND1,3-Dichloropropane 08/15/11 1.9 9.4 NA1
Page 72 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:55
1204.22
500 Kirkham
B-6-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.6 9.4 NA1
SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.81 9.4 NA1
SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 4.0 9.4 NA1
SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.81 9.4 NA1
SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.7 9.4 NA1
SW8260B NA 406253ug/KgNDo-Xylene 08/15/11 0.62 4.7 NA1
SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.72 9.4 NA1
SW8260B NA 406253ug/KgNDBromoform 08/15/11 1.8 9.4 NA1
SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 1.2 9.4 NA1
SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.3 9.4 NA1
SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 1.1 9.4 NA1
SW8260B NA 406253ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.8 9.4 NA1
SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.1 9.4 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 3.1 9.4 NA1
SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.5 9.4 NA1
SW8260B NA 406253ug/KgND2-Chlorotoluene 08/15/11 1.5 9.4 NA1
SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.3 9.4 NA1
SW8260B NA 406253ug/KgND1,2,4-Trimethylbenzene 08/15/11 1.0 9.4 NA1
SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.5 9.4 NA1
SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.4 9.4 NA1
SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.7 9.4 NA1
SW8260B NA 406253ug/KgND1,4-Dichlorobenzene 08/15/11 1.4 9.4 NA1
SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 2.1 9.4 NA1
SW8260B NA 406253ug/KgND1,2-Dichlorobenzene 08/15/11 1.2 9.4 NA1
SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 4.0 9.4 NA1
SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 2.4 9.4 NA1
SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 2.0 9.4 NA1
SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.7 9.4 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.7 9.4 NA1
SW8260B NA 406253%90.7(S) Dibromofluoromethane 08/15/11 59.8 148 NA1
SW8260B NA 406253%86.5(S) Toluene-d8 08/15/11 55.2 133 NA1
SW8260B NA 406253%106(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 73 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:55
1204.22
500 Kirkham
B-6-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/16/11 406288mg/KgNDAntimony 08/17/11 0.20 5.0 34051
SW6010B 8/16/11 406288mg/KgNDArsenic 08/17/11 0.28 1.7 34051
SW6010B 8/16/11 406288mg/Kg42Barium 08/17/11 1 5.0 34051
SW6010B 8/16/11 406288mg/KgNDBeryllium 08/17/11 0.0840 2.0 34051
SW6010B 8/16/11 406288mg/KgNDCadmium 08/17/11 0.0590 1.0 34051
SW6010B 8/16/11 406288mg/Kg21Chromium 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/KgNDCobalt 08/17/11 0.14 5.0 34051
SW6010B 8/16/11 406288mg/KgNDCopper 08/17/11 0.0900 5.0 34051
SW6010B 8/16/11 406288mg/Kg2.7Lead 08/17/11 0.043 1.0 34051
SW6010B 8/16/11 406288mg/KgNDMolybdenum 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/Kg13Nickel 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSelenium 08/17/11 0.29 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSilver 08/17/11 1.0 1.0 34051
SW6010B 8/16/11 406288mg/KgNDThallium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg15Vanadium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg14Zinc 08/17/11 0.59 5.0 34051
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/KgNDMercury 08/16/11 0.01 0.10 33931
Page 74 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:55
1204.22
500 Kirkham
B-6-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8081A 8/18/11 406333ug/KgNDalpha-BHC 08/18/11 0.44 2.0 34201
SW8081A 8/18/11 406333ug/KgNDgamma-BHC 08/18/11 0.40 2.0 34201
SW8081A 8/18/11 406333ug/KgNDbeta-BHC 08/18/11 0.36 2.0 34201
SW8081A 8/18/11 406333ug/KgNDdelta-BHC 08/18/11 0.49 2.0 34201
SW8081A 8/18/11 406333ug/KgNDHeptachlor 08/18/11 1.1 2.0 34201
SW8081A 8/18/11 406333ug/KgNDAldrin 08/18/11 0.44 2.0 34201
SW8081A 8/18/11 406333ug/KgNDHeptachlor epoxide 08/18/11 0.32 2.0 34201
SW8081A 8/18/11 406333ug/KgNDgamma-Chlordane 08/18/11 0.42 2.0 34201
SW8081A 8/18/11 406333ug/KgNDalpha-Chlordane 08/18/11 0.36 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndosulfan I 08/18/11 0.59 2.0 34201
SW8081A 8/18/11 406333ug/KgND4,4'-DDE 08/18/11 0.48 2.0 34201
SW8081A 8/18/11 406333ug/KgNDDieldrin 08/18/11 0.43 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndrin 08/18/11 0.57 2.0 34201
SW8081A 8/18/11 406333ug/KgND4,4'-DDD 08/18/11 0.47 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndosulfan II 08/18/11 1.5 2.0 34201
SW8081A 8/18/11 406333ug/KgND4,4'-DDT 08/18/11 0.81 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndrin aldehyde 08/18/11 1.0 2.0 34201
SW8081A 8/18/11 406333ug/KgNDEndosulfan sulfate 08/18/11 0.49 2.0 34201
SW8081A 8/18/11 406333ug/KgNDMethoxychlor 08/18/11 0.62 5.0 34201
SW8081A 8/18/11 406333ug/KgNDEndrin Ketone 08/18/11 0.40 2.0 34201
SW8081A 8/18/11 406333ug/KgNDChlordane 08/18/11 10 20 34201
SW8081A 8/18/11 406333ug/KgNDToxaphene 08/18/11 10 100 34201
SW8081A 8/18/11 406333%87.6TCMX (S) 08/18/11 52.5 139 34201
SW8081A 8/18/11 406333%70.0DCBP (S) 08/18/11 50.2 139 34201
Page 75 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:55
1204.22
500 Kirkham
B-6-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1221 08/18/11 0.0920 0.20 34191
SW8082 8/18/11 406326mg/KgNDAroclor1232 08/18/11 0.0460 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1242 08/18/11 0.0430 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1248 08/18/11 0.0360 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1254 08/18/11 0.0240 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1260 08/18/11 0.0270 0.10 34191
SW8082 8/18/11 406326%87.9TCMX (S) 08/18/11 50.4 136 34191
SW8082 8/18/11 406326%87.7DCBP (S) 08/18/11 55.1 113 34191
Page 76 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:55
1204.22
500 Kirkham
B-6-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 0.660 0.653 33851
SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 0.110 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 0.123 0.330 33851
SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 0.129 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 0.0683 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 0.129 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 0.0733 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 0.0663 6.59 33851
SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 0.0713 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 0.116 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 0.0683 0.330 33851
SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 0.139 0.330 33851
SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 0.0931 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 0.0465 0.330 33851
SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 0.0528 0.330 33851
SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 0.0574 0.653 33851
SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 0.0525 0.653 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 0.133 6.59 33851
SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 5.59 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 0.0584 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 0.0733 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 0.0901 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 0.0990 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 0.0653 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 0.102 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 0.0792 0.330 33851
SW8270C 8/15/11 406316mg/KgND1-Methylnaphthalene 08/16/11 0.0792 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 0.0277 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 0.0950 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 0.121 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 0.0594 3.27 33851
SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 0.0693 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 0.118 0.330 33851
Page 77 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:55
1204.22
500 Kirkham
B-6-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 0.106 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 0.0851 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 0.0267 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 0.0858 0.330 33851
SW8270C 8/15/11 406316mg/KgND3-Nitroaniline 08/16/11 0.0693 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 0.0960 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 0.0297 3.27 33851
SW8270C 8/15/11 406316mg/KgND4-Nitrophenol 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 0.0782 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 0.0267 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 0.119 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 0.119 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 0.117 0.330 33851
SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 0.0990 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 0.0802 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Nitroaniline 08/16/11 0.0802 0.330 33851
SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 0.109 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 0.0812 3.27 33851
SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 0.101 0.330 33851
SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 0.102 3.27 33851
SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 0.142 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 0.132 0.330 33851
SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 0.132 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 0.108 1.68 33851
SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 0.132 0.653 33851
SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 0.374 3.27 33851
SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 0.147 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 0.0891 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 0.149 0.330 33851
SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 0.152 0.330 33851
SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 0.176 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 0.0832 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 0.138 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 0.133 0.330 33851
Page 78 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:55
1204.22
500 Kirkham
B-6-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-013A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 0.169 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 0.135 0.330 33851
SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 0.131 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 0.151 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 0.150 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 0.150 0.330 33851
SW8270C 8/15/11 406316%67.42,4,6-Tribromophenol (S) 08/16/11 19 122 33851
SW8270C 8/15/11 406316%72.72-Fluorobiphenyl (S) 08/16/11 30 115 33851
SW8270C 8/15/11 406316%77.12-Fluorophenol (S) 08/16/11 25 121 33851
SW8270C 8/15/11 406316%69.4Nitrobenzene-d5 (S) 08/16/11 23 120 33851
SW8270C 8/15/11 406316%80.5Phenol-d6 (S) 08/16/11 24 113 33851
SW8270C 8/15/11 406316%82.8p-Terphenyl-d14 (S) 08/16/11 18 137 33851
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 16 94 NA1
8260TPH NA 406253%82.8(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 0.759 2.0 34181
SW8015B(M) 8/18/11 406325mg/Kg4.0TPH as Motor Oil 08/18/11 1.65 4.0 34181
SW8015B(M) 8/18/11 406325mg/Kg110Pentacosane (S) 08/18/11 59.7 129 34181
Page 79 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 11:00
1204.22
500 Kirkham
B-6-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-014A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 3.5 7.9 NA1
SW8260B NA 406253ug/KgNDChloromethane 08/15/11 3.6 7.9 NA1
SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.1 7.9 NA1
SW8260B NA 406253ug/KgNDBromomethane 08/15/11 3.7 7.9 NA1
SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 2.3 7.9 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.2 7.9 NA1
SW8260B NA 406253ug/KgNDFreon 113 08/15/11 2.9 7.9 NA1
SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 1.6 7.9 NA1
SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.88 7.9 NA1
SW8260B NA 406253ug/KgNDMTBE 08/15/11 2.0 7.9 NA1
SW8260B NA 406253ug/KgNDtert-Butanol 08/15/11 16 40 NA1
SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.7 7.9 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 1.0 7.9 NA1
SW8260B NA 406253ug/KgNDETBE 08/15/11 1.9 7.9 NA1
SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.4 7.9 NA1
SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 0.98 7.9 NA1
SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 1.8 7.9 NA1
SW8260B NA 406253ug/KgNDChloroform 08/15/11 0.96 7.9 NA1
SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.3 7.9 NA1
SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 0.96 7.9 NA1
SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.1 7.9 NA1
SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.2 7.9 NA1
SW8260B NA 406253ug/KgNDTAME 08/15/11 1.6 7.9 NA1
SW8260B NA 406253ug/KgND1,2-Dichloroethane 08/15/11 1.5 7.9 NA1
SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 3.1 7.9 NA1
SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 1.7 7.9 NA1
SW8260B NA 406253ug/KgND1,2-Dichloropropane 08/15/11 1.0 7.9 NA1
SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 0.88 7.9 NA1
SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 3.5 7.9 NA1
SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.1 7.9 NA1
SW8260B NA 406253ug/KgNDToluene 08/15/11 0.78 7.9 NA1
SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.4 7.9 NA1
SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.91 7.9 NA1
SW8260B NA 406253ug/KgND1,1,2-Trichloroethane 08/15/11 1.4 7.9 NA1
SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 0.89 7.9 NA1
SW8260B NA 406253ug/KgND1,3-Dichloropropane 08/15/11 1.6 7.9 NA1
Page 80 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 11:00
1204.22
500 Kirkham
B-6-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-014A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.4 7.9 NA1
SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.68 7.9 NA1
SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 3.3 7.9 NA1
SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.68 7.9 NA1
SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.5 7.9 NA1
SW8260B NA 406253ug/KgNDo-Xylene 08/15/11 0.52 4.0 NA1
SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.60 7.9 NA1
SW8260B NA 406253ug/KgNDBromoform 08/15/11 1.5 7.9 NA1
SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 0.98 7.9 NA1
SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.1 7.9 NA1
SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 0.94 7.9 NA1
SW8260B NA 406253ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.4 7.9 NA1
SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.89 7.9 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 2.6 7.9 NA1
SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.3 7.9 NA1
SW8260B NA 406253ug/KgND2-Chlorotoluene 08/15/11 1.3 7.9 NA1
SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.1 7.9 NA1
SW8260B NA 406253ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.86 7.9 NA1
SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.3 7.9 NA1
SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.2 7.9 NA1
SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.4 7.9 NA1
SW8260B NA 406253ug/KgND1,4-Dichlorobenzene 08/15/11 1.2 7.9 NA1
SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 1.7 7.9 NA1
SW8260B NA 406253ug/KgND1,2-Dichlorobenzene 08/15/11 1.0 7.9 NA1
SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.3 7.9 NA1
SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 2.0 7.9 NA1
SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.7 7.9 NA1
SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.2 7.9 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.3 7.9 NA1
SW8260B NA 406253%95.9(S) Dibromofluoromethane 08/15/11 59.8 148 NA1
SW8260B NA 406253%97.6(S) Toluene-d8 08/15/11 55.2 133 NA1
SW8260B NA 406253%122(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 81 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 11:00
1204.22
500 Kirkham
B-6-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-014A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/16/11 406288mg/KgNDAntimony 08/17/11 0.20 5.0 34051
SW6010B 8/16/11 406288mg/KgNDArsenic 08/17/11 0.28 1.7 34051
SW6010B 8/16/11 406288mg/Kg50Barium 08/17/11 1 5.0 34051
SW6010B 8/16/11 406288mg/KgNDBeryllium 08/17/11 0.0840 2.0 34051
SW6010B 8/16/11 406288mg/KgNDCadmium 08/17/11 0.0590 1.0 34051
SW6010B 8/16/11 406288mg/Kg22Chromium 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/KgNDCobalt 08/17/11 0.14 5.0 34051
SW6010B 8/16/11 406288mg/KgNDCopper 08/17/11 0.0900 5.0 34051
SW6010B 8/16/11 406288mg/Kg1.9Lead 08/17/11 0.043 1.0 34051
SW6010B 8/16/11 406288mg/KgNDMolybdenum 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/Kg9.2Nickel 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSelenium 08/17/11 0.29 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSilver 08/17/11 1.0 1.0 34051
SW6010B 8/16/11 406288mg/KgNDThallium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg18Vanadium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg9.0Zinc 08/17/11 0.59 5.0 34051
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/KgNDMercury 08/16/11 0.01 0.10 33931
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1221 08/18/11 0.0920 0.20 34191
SW8082 8/18/11 406326mg/KgNDAroclor1232 08/18/11 0.0460 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1242 08/18/11 0.0430 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1248 08/18/11 0.0360 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1254 08/18/11 0.0240 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1260 08/18/11 0.0270 0.10 34191
SW8082 8/18/11 406326%133TCMX (S) 08/18/11 50.4 136 34191
SW8082 8/18/11 406326%79.2DCBP (S) 08/18/11 55.1 113 34191
Page 82 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 11:00
1204.22
500 Kirkham
B-6-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-014A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 0.660 0.653 33851
SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 0.110 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 0.123 0.330 33851
SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 0.129 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 0.0683 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 0.129 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 0.0733 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 0.0663 6.59 33851
SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 0.0713 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 0.116 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 0.0683 0.330 33851
SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 0.139 0.330 33851
SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 0.0931 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 0.0465 0.330 33851
SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 0.0528 0.330 33851
SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 0.0574 0.653 33851
SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 0.0525 0.653 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 0.133 6.59 33851
SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 5.59 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 0.0584 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 0.0733 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 0.104 0.330 33851
SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 0.0901 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 0.0990 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 0.0653 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 0.102 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 0.0792 0.330 33851
SW8270C 8/15/11 406316mg/KgND1-Methylnaphthalene 08/16/11 0.0792 0.330 33851
SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 0.0277 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 0.0950 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 0.121 0.330 33851
SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 0.0594 3.27 33851
SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 0.0693 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 0.118 0.330 33851
Page 83 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 11:00
1204.22
500 Kirkham
B-6-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-014A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 0.106 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 0.0851 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 0.0267 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 0.0858 0.330 33851
SW8270C 8/15/11 406316mg/KgND3-Nitroaniline 08/16/11 0.0693 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 0.0960 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 0.0297 3.27 33851
SW8270C 8/15/11 406316mg/KgND4-Nitrophenol 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 0.0782 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 0.0267 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 0.119 0.330 33851
SW8270C 8/15/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 0.119 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 0.117 0.330 33851
SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 0.0990 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 0.0802 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Nitroaniline 08/16/11 0.0802 0.330 33851
SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 0.0663 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 0.109 0.330 33851
SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 0.0812 3.27 33851
SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 0.101 0.330 33851
SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 0.102 3.27 33851
SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 0.142 0.330 33851
SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 0.132 0.330 33851
SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 0.132 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 0.108 1.68 33851
SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 0.132 0.653 33851
SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 0.374 3.27 33851
SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 0.147 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 0.0891 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 0.149 0.330 33851
SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 0.152 0.330 33851
SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 0.176 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 0.0832 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 0.138 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 0.133 0.330 33851
Page 84 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 11:00
1204.22
500 Kirkham
B-6-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-014A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 0.169 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 0.135 0.330 33851
SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 0.131 0.330 33851
SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 0.151 0.330 33851
SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 0.150 0.330 33851
SW8270C 8/15/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 0.150 0.330 33851
SW8270C 8/15/11 406316%61.02,4,6-Tribromophenol (S) 08/16/11 19 122 33851
SW8270C 8/15/11 406316%61.02-Fluorobiphenyl (S) 08/16/11 30 115 33851
SW8270C 8/15/11 406316%67.52-Fluorophenol (S) 08/16/11 25 121 33851
SW8270C 8/15/11 406316%60.2Nitrobenzene-d5 (S) 08/16/11 23 120 33851
SW8270C 8/15/11 406316%71.5Phenol-d6 (S) 08/16/11 24 113 33851
SW8270C 8/15/11 406316%84.6p-Terphenyl-d14 (S) 08/16/11 18 137 33851
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 13 79 NA1
8260TPH NA 406253%50.5(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 0.759 2.0 34181
SW8015B(M) 8/18/11 406325mg/Kg5.5TPH as Motor Oil 08/18/11 1.65 4.0 34181
SW8015B(M) 8/18/11 406325mg/Kg123Pentacosane (S) 08/18/11 59.7 129 34181
Page 85 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:05
1204.22
500 Kirkham
B-16-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 3.3 7.5 NA1
SW8260B NA 406253ug/KgNDChloromethane 08/15/11 3.5 7.5 NA1
SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.0 7.5 NA1
SW8260B NA 406253ug/KgNDBromomethane 08/15/11 3.5 7.5 NA1
SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 2.2 7.5 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.2 7.5 NA1
SW8260B NA 406253ug/KgNDFreon 113 08/15/11 2.8 7.5 NA1
SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 1.5 7.5 NA1
SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.83 7.5 NA1
SW8260B NA 406253ug/KgNDMTBE 08/15/11 1.9 7.5 NA1
SW8260B NA 406253ug/KgNDtert-Butanol 08/15/11 16 38 NA1
SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.6 7.5 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 0.96 7.5 NA1
SW8260B NA 406253ug/KgNDETBE 08/15/11 1.8 7.5 NA1
SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.3 7.5 NA1
SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 0.93 7.5 NA1
SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 1.7 7.5 NA1
SW8260B NA 406253ug/KgNDChloroform 08/15/11 0.91 7.5 NA1
SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.2 7.5 NA1
SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 0.91 7.5 NA1
SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.1 7.5 NA1
SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.1 7.5 NA1
SW8260B NA 406253ug/KgNDTAME 08/15/11 1.5 7.5 NA1
SW8260B NA 406253ug/KgND1,2-Dichloroethane 08/15/11 1.4 7.5 NA1
SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 2.9 7.5 NA1
SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 1.6 7.5 NA1
SW8260B NA 406253ug/KgND1,2-Dichloropropane 08/15/11 0.98 7.5 NA1
SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 0.84 7.5 NA1
SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 3.4 7.5 NA1
SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.1 7.5 NA1
SW8260B NA 406253ug/KgNDToluene 08/15/11 0.74 7.5 NA1
SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.4 7.5 NA1
SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 0.87 7.5 NA1
SW8260B NA 406253ug/KgND1,1,2-Trichloroethane 08/15/11 1.4 7.5 NA1
SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 0.84 7.5 NA1
SW8260B NA 406253ug/KgND1,3-Dichloropropane 08/15/11 1.5 7.5 NA1
Page 86 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:05
1204.22
500 Kirkham
B-16-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.3 7.5 NA1
SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.65 7.5 NA1
SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 3.2 7.5 NA1
SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.64 7.5 NA1
SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.4 7.5 NA1
SW8260B NA 406253ug/KgNDo-Xylene 08/15/11 0.50 3.8 NA1
SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.57 7.5 NA1
SW8260B NA 406253ug/KgNDBromoform 08/15/11 1.4 7.5 NA1
SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 0.93 7.5 NA1
SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.1 7.5 NA1
SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 0.89 7.5 NA1
SW8260B NA 406253ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.3 7.5 NA1
SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.84 7.5 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 2.5 7.5 NA1
SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.2 7.5 NA1
SW8260B NA 406253ug/KgND2-Chlorotoluene 08/15/11 1.2 7.5 NA1
SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.1 7.5 NA1
SW8260B NA 406253ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.81 7.5 NA1
SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.2 7.5 NA1
SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.1 7.5 NA1
SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.3 7.5 NA1
SW8260B NA 406253ug/KgND1,4-Dichlorobenzene 08/15/11 1.1 7.5 NA1
SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 1.6 7.5 NA1
SW8260B NA 406253ug/KgND1,2-Dichlorobenzene 08/15/11 0.98 7.5 NA1
SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.2 7.5 NA1
SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 1.9 7.5 NA1
SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.6 7.5 NA1
SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.1 7.5 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.2 7.5 NA1
SW8260B NA 406253%89.1(S) Dibromofluoromethane 08/15/11 59.8 148 NA1
SW8260B NA 406253%86.9(S) Toluene-d8 08/15/11 55.2 133 NA1
SW8260B NA 406253%89.9(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 87 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:05
1204.22
500 Kirkham
B-16-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/16/11 406288mg/KgNDAntimony 08/17/11 0.20 5.0 34051
SW6010B 8/16/11 406288mg/Kg2.5Arsenic 08/17/11 0.28 1.7 34051
SW6010B 8/16/11 406288mg/Kg58Barium 08/17/11 1 5.0 34051
SW6010B 8/16/11 406288mg/KgNDBeryllium 08/17/11 0.0840 2.0 34051
SW6010B 8/16/11 406288mg/KgNDCadmium 08/17/11 0.0590 1.0 34051
SW6010B 8/16/11 406288mg/Kg24Chromium 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/Kg5.1Cobalt 08/17/11 0.14 5.0 34051
SW6010B 8/16/11 406288mg/Kg12Copper 08/17/11 0.0900 5.0 34051
SW6010B 8/16/11 406288mg/Kg41Lead 08/17/11 0.043 1.0 34051
SW6010B 8/16/11 406288mg/KgNDMolybdenum 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/Kg19Nickel 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSelenium 08/17/11 0.29 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSilver 08/17/11 1.0 1.0 34051
SW6010B 8/16/11 406288mg/KgNDThallium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg21Vanadium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg45Zinc 08/17/11 0.59 5.0 34051
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/KgNDMercury 08/16/11 0.01 0.10 33931
Page 88 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:05
1204.22
500 Kirkham
B-16-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8081A 8/18/11 406333ug/KgNDalpha-BHC 08/18/11 8.8 40 342020
SW8081A 8/18/11 406333ug/KgNDgamma-BHC 08/18/11 7.9 40 342020
SW8081A 8/18/11 406333ug/KgNDbeta-BHC 08/18/11 7.3 40 342020
SW8081A 8/18/11 406333ug/KgNDdelta-BHC 08/18/11 9.8 40 342020
SW8081A 8/18/11 406333ug/KgNDHeptachlor 08/18/11 22 40 342020
SW8081A 8/18/11 406333ug/KgNDAldrin 08/18/11 8.8 40 342020
SW8081A 8/18/11 406333ug/KgNDHeptachlor epoxide 08/18/11 6.3 40 342020
SW8081A 8/18/11 406333ug/KgNDgamma-Chlordane 08/18/11 8.4 40 342020
SW8081A 8/18/11 406333ug/KgNDalpha-Chlordane 08/18/11 7.2 40 342020
SW8081A 8/18/11 406333ug/KgNDEndosulfan I 08/18/11 12 40 342020
SW8081A 8/18/11 406333ug/KgND4,4'-DDE 08/18/11 9.5 40 342020
SW8081A 8/18/11 406333ug/KgNDDieldrin 08/18/11 8.5 40 342020
SW8081A 8/18/11 406333ug/KgNDEndrin 08/18/11 11 40 342020
SW8081A 8/18/11 406333ug/KgND4,4'-DDD 08/18/11 9.4 40 342020
SW8081A 8/18/11 406333ug/KgNDEndosulfan II 08/18/11 31 40 342020
SW8081A 8/18/11 406333ug/KgND4,4'-DDT 08/18/11 16 40 342020
SW8081A 8/18/11 406333ug/KgNDEndrin aldehyde 08/18/11 21 40 342020
SW8081A 8/18/11 406333ug/KgNDEndosulfan sulfate 08/18/11 9.8 40 342020
SW8081A 8/18/11 406333ug/KgNDMethoxychlor 08/18/11 12 100 342020
SW8081A 8/18/11 406333ug/KgNDEndrin Ketone 08/18/11 8.0 40 342020
SW8081A 8/18/11 406333ug/KgNDChlordane 08/18/11 200 400 342020
SW8081A 8/18/11 406333ug/KgNDToxaphene 08/18/11 200 2000 342020
SW8081A 8/18/11 406333%112TCMX (S) 08/18/11 52.5 139 342020
SW8081A 8/18/11 406333%107DCBP (S) 08/18/11 50.2 139 342020
Reporting limits increased due to the nature of the sample matrix (dark color extract).NOTE:
Page 89 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:05
1204.22
500 Kirkham
B-16-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1221 08/18/11 0.0920 0.20 34191
SW8082 8/18/11 406326mg/KgNDAroclor1232 08/18/11 0.0460 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1242 08/18/11 0.0430 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1248 08/18/11 0.0360 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1254 08/18/11 0.0240 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1260 08/18/11 0.0270 0.10 34191
SW8082 8/18/11 406326%93.6TCMX (S) 08/18/11 50.4 136 34191
SW8082 8/18/11 406326%99.6DCBP (S) 08/18/11 55.1 113 34191
Page 90 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:05
1204.22
500 Kirkham
B-16-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 1000 990 338510
SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 167 500 338510
SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 186 500 338510
SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 195 500 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 104 500 338510
SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 195 500 338510
SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 111 500 338510
SW8270C 8/15/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 101 9990 338510
SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 158 500 338510
SW8270C 8/15/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 108 500 338510
SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 176 500 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 104 500 338510
SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 210 500 338510
SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 141 500 338510
SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 70.5 500 338510
SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 80.0 500 338510
SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 87.0 990 338510
SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 79.5 990 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 201 9990 338510
SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 8480 500 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 88.5 500 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 158 500 338510
SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 111 500 338510
SW8270C 8/15/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 158 500 338510
SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 137 500 338510
SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 150 500 338510
SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 99.0 500 338510
SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 155 500 338510
SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 120 500 338510
SW8270C 8/15/11 406316mg/KgND1-Methylnaphthalene 08/16/11 120 500 338510
SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 42.0 500 338510
SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 144 500 338510
SW8270C 8/15/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 183 500 338510
SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 90.0 4950 338510
SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 105 500 338510
Page 91 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:05
1204.22
500 Kirkham
B-16-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 179 500 338510
SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 160 500 338510
SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 129 500 338510
SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 40.5 500 338510
SW8270C 8/15/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 130 500 338510
SW8270C 8/15/11 406316mg/KgND3-Nitroaniline 08/16/11 105 500 338510
SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 146 500 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 45.0 4950 338510
SW8270C 8/15/11 406316mg/KgND4-Nitrophenol 08/16/11 101 500 338510
SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 119 500 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 40.5 500 338510
SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 180 500 338510
SW8270C 8/15/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 180 500 338510
SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 177 500 338510
SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 150 500 338510
SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 122 500 338510
SW8270C 8/15/11 406316mg/KgND4-Nitroaniline 08/16/11 122 500 338510
SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 101 500 338510
SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 101 500 338510
SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 165 500 338510
SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 123 4950 338510
SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 153 500 338510
SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 155 4950 338510
SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 215 500 338510
SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 201 500 338510
SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 201 500 338510
SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 164 2550 338510
SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 201 990 338510
SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 567 4950 338510
SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 223 500 338510
SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 135 500 338510
SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 227 500 338510
SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 231 500 338510
SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 267 500 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 126 500 338510
Page 92 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:05
1204.22
500 Kirkham
B-16-1.0
SoilSample Matrix:
Lab Sample ID: 1108084-016A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 209 500 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 201 500 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 257 500 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 204 500 338510
SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 198 500 338510
SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 230 500 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 228 500 338510
SW8270C 8/15/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 228 500 338510
SW8270C 8/15/11 406316S,D %0.0002,4,6-Tribromophenol (S) 08/16/11 19 122 338510
SW8270C 8/15/11 406316S,D %0.0002-Fluorobiphenyl (S) 08/16/11 30 115 338510
SW8270C 8/15/11 406316S,D %0.0002-Fluorophenol (S) 08/16/11 25 121 338510
SW8270C 8/15/11 406316S,D %0.000Nitrobenzene-d5 (S) 08/16/11 23 120 338510
SW8270C 8/15/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 338510
SW8270C 8/15/11 406316S,D %0.000p-Terphenyl-d14 (S) 08/16/11 18 137 338510
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 13 75 NA1
8260TPH NA 406253%65.7(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 1.84 4.8 34181
SW8015B(M) 8/18/11 406325mg/Kg270TPH as Motor Oil 08/18/11 4.00 9.6 34181
SW8015B(M) 8/18/11 406325mg/Kg95.8Pentacosane (S) 08/18/11 59.7 129 34181
Page 93 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:10
1204.22
500 Kirkham
B-16-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-017A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 4.0 9.2 NA1
SW8260B NA 406253ug/KgNDChloromethane 08/15/11 4.2 9.2 NA1
SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.4 9.2 NA1
SW8260B NA 406253ug/KgNDBromomethane 08/15/11 4.3 9.2 NA1
SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 2.7 9.2 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.4 9.2 NA1
SW8260B NA 406253ug/KgNDFreon 113 08/15/11 3.4 9.2 NA1
SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 1.8 9.2 NA1
SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 1.0 9.2 NA1
SW8260B NA 406253ug/KgNDMTBE 08/15/11 2.4 9.2 NA1
SW8260B NA 406253ug/KgNDtert-Butanol 08/15/11 19 46 NA1
SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 2.0 9.2 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 1.2 9.2 NA1
SW8260B NA 406253ug/KgNDETBE 08/15/11 2.2 9.2 NA1
SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.6 9.2 NA1
SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 1.1 9.2 NA1
SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 2.1 9.2 NA1
SW8260B NA 406253ug/KgNDChloroform 08/15/11 1.1 9.2 NA1
SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.5 9.2 NA1
SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 1.1 9.2 NA1
SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.3 9.2 NA1
SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.4 9.2 NA1
SW8260B NA 406253ug/KgNDTAME 08/15/11 1.9 9.2 NA1
SW8260B NA 406253ug/KgND1,2-Dichloroethane 08/15/11 1.8 9.2 NA1
SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 3.6 9.2 NA1
SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 2.0 9.2 NA1
SW8260B NA 406253ug/KgND1,2-Dichloropropane 08/15/11 1.2 9.2 NA1
SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 1.0 9.2 NA1
SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 4.1 9.2 NA1
SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.3 9.2 NA1
SW8260B NA 406253ug/KgNDToluene 08/15/11 0.90 9.2 NA1
SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.7 9.2 NA1
SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.1 9.2 NA1
SW8260B NA 406253ug/KgND1,1,2-Trichloroethane 08/15/11 1.7 9.2 NA1
SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 1.0 9.2 NA1
SW8260B NA 406253ug/KgND1,3-Dichloropropane 08/15/11 1.9 9.2 NA1
Page 94 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:10
1204.22
500 Kirkham
B-16-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-017A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.6 9.2 NA1
SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.79 9.2 NA1
SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 3.9 9.2 NA1
SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.79 9.2 NA1
SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.7 9.2 NA1
SW8260B NA 406253ug/KgNDo-Xylene 08/15/11 0.61 4.6 NA1
SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.70 9.2 NA1
SW8260B NA 406253ug/KgNDBromoform 08/15/11 1.7 9.2 NA1
SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 1.1 9.2 NA1
SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.3 9.2 NA1
SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 1.1 9.2 NA1
SW8260B NA 406253ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.8 9.2 NA1
SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.0 9.2 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 3.1 9.2 NA1
SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.5 9.2 NA1
SW8260B NA 406253ug/KgND2-Chlorotoluene 08/15/11 1.5 9.2 NA1
SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.3 9.2 NA1
SW8260B NA 406253ug/KgND1,2,4-Trimethylbenzene 08/15/11 1.0 9.2 NA1
SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.5 9.2 NA1
SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.3 9.2 NA1
SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.6 9.2 NA1
SW8260B NA 406253ug/KgND1,4-Dichlorobenzene 08/15/11 1.4 9.2 NA1
SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 2.0 9.2 NA1
SW8260B NA 406253ug/KgND1,2-Dichlorobenzene 08/15/11 1.2 9.2 NA1
SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.9 9.2 NA1
SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 2.3 9.2 NA1
SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 2.0 9.2 NA1
SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.6 9.2 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.6 9.2 NA1
SW8260B NA 406253%91.6(S) Dibromofluoromethane 08/15/11 59.8 148 NA1
SW8260B NA 406253%93.4(S) Toluene-d8 08/15/11 55.2 133 NA1
SW8260B NA 406253%106(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 95 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:10
1204.22
500 Kirkham
B-16-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-017A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/16/11 406288mg/KgNDAntimony 08/17/11 0.20 5.0 34051
SW6010B 8/16/11 406288mg/Kg2.0Arsenic 08/17/11 0.28 1.7 34051
SW6010B 8/16/11 406288mg/Kg50Barium 08/17/11 1 5.0 34051
SW6010B 8/16/11 406288mg/KgNDBeryllium 08/17/11 0.0840 2.0 34051
SW6010B 8/16/11 406288mg/KgNDCadmium 08/17/11 0.0590 1.0 34051
SW6010B 8/16/11 406288mg/Kg38Chromium 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/Kg6.9Cobalt 08/17/11 0.14 5.0 34051
SW6010B 8/16/11 406288mg/Kg5.6Copper 08/17/11 0.0900 5.0 34051
SW6010B 8/16/11 406288mg/Kg3.2Lead 08/17/11 0.043 1.0 34051
SW6010B 8/16/11 406288mg/KgNDMolybdenum 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/Kg29Nickel 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSelenium 08/17/11 0.29 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSilver 08/17/11 1.0 1.0 34051
SW6010B 8/16/11 406288mg/KgNDThallium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg27Vanadium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg18Zinc 08/17/11 0.59 5.0 34051
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/KgNDMercury 08/16/11 0.01 0.10 33931
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1221 08/18/11 0.0920 0.20 34191
SW8082 8/18/11 406326mg/KgNDAroclor1232 08/18/11 0.0460 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1242 08/18/11 0.0430 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1248 08/18/11 0.0360 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1254 08/18/11 0.0240 0.10 34191
SW8082 8/18/11 406326mg/KgNDAroclor1260 08/18/11 0.0270 0.10 34191
SW8082 8/18/11 406326%81.8TCMX (S) 08/18/11 50.4 136 34191
SW8082 8/18/11 406326%83.2DCBP (S) 08/18/11 55.1 113 34191
Page 96 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:10
1204.22
500 Kirkham
B-16-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-017A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 100 99.0 338510
SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 16.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 18.6 50.0 338510
SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 19.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 10.4 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 19.5 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 11.1 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 10.1 999 338510
SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 15.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,2-Dichlorobenzene 08/16/11 10.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 17.6 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 10.4 50.0 338510
SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 21.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 14.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 7.05 50.0 338510
SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 8.00 50.0 338510
SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 8.70 99.0 338510
SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 7.95 99.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 20.1 999 338510
SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 848 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 8.85 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 15.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 11.1 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 15.8 50.0 338510
SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 13.7 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 15.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 9.90 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 15.5 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 12.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND1-Methylnaphthalene 08/16/11 12.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 4.20 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 14.4 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 18.3 50.0 338510
SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 9.00 495 338510
SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 10.5 50.0 338510
Page 97 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:10
1204.22
500 Kirkham
B-16-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-017A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 17.9 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 16.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 12.9 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 4.05 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,2-Dinitrobenzene 08/16/11 13.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND3-Nitroaniline 08/16/11 10.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 14.6 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 4.50 495 338510
SW8270C 8/15/11 406316mg/KgND4-Nitrophenol 08/16/11 10.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 11.9 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,4-Dinitrotoluene 08/16/11 4.05 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 18.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 18.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 17.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 15.0 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 12.2 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Nitroaniline 08/16/11 12.2 50.0 338510
SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 10.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 10.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 16.5 50.0 338510
SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 12.3 495 338510
SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 15.3 50.0 338510
SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 15.5 495 338510
SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 21.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 20.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 20.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 16.4 255 338510
SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 20.1 99.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 56.7 495 338510
SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 22.3 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 13.5 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 22.7 50.0 338510
SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 23.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 26.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 12.6 50.0 338510
Page 98 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:10
1204.22
500 Kirkham
B-16-5.0
SoilSample Matrix:
Lab Sample ID: 1108084-017A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 20.9 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 20.1 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 25.7 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 20.4 50.0 338510
SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 19.8 50.0 338510
SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 23.0 50.0 338510
SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 22.8 50.0 338510
SW8270C 8/15/11 406316mg/KgND1,4-Dinitrobenzene 08/16/11 22.8 50.0 338510
SW8270C 8/15/11 406316S,D %0.0002,4,6-Tribromophenol (S) 08/16/11 19 122 338510
SW8270C 8/15/11 406316S,D %0.0002-Fluorobiphenyl (S) 08/16/11 30 115 338510
SW8270C 8/15/11 406316S,D %0.0002-Fluorophenol (S) 08/16/11 25 121 338510
SW8270C 8/15/11 406316S,D %0.000Nitrobenzene-d5 (S) 08/16/11 23 120 338510
SW8270C 8/15/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 338510
SW8270C 8/15/11 406316S,D %0.000p-Terphenyl-d14 (S) 08/16/11 18 137 338510
D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).
NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 16 92 NA1
8260TPH NA 406253%60.6(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 0.759 2.0 34181
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Motor Oil 08/18/11 1.65 4.0 34181
SW8015B(M) 8/18/11 406325mg/Kg108Pentacosane (S) 08/18/11 59.7 129 34181
Page 99 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:30
1204.22
500 Kirkham
B-7-1.0D
SoilSample Matrix:
Lab Sample ID: 1108084-019A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 4.1 9.3 NA1
SW8260B NA 406253ug/KgNDChloromethane 08/15/11 4.3 9.3 NA1
SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.5 9.3 NA1
SW8260B NA 406253ug/KgNDBromomethane 08/15/11 4.3 9.3 NA1
SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 2.7 9.3 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.4 9.3 NA1
SW8260B NA 406253ug/KgNDFreon 113 08/15/11 3.5 9.3 NA1
SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 1.8 9.3 NA1
SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 1.0 9.3 NA1
SW8260B NA 406253ug/KgNDMTBE 08/15/11 2.4 9.3 NA1
SW8260B NA 406253ug/KgNDtert-Butanol 08/15/11 19 47 NA1
SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 2.0 9.3 NA1
SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 1.2 9.3 NA1
SW8260B NA 406253ug/KgNDETBE 08/15/11 2.2 9.3 NA1
SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.6 9.3 NA1
SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 1.2 9.3 NA1
SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 2.1 9.3 NA1
SW8260B NA 406253ug/KgNDChloroform 08/15/11 1.1 9.3 NA1
SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.5 9.3 NA1
SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 1.1 9.3 NA1
SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.3 9.3 NA1
SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.4 9.3 NA1
SW8260B NA 406253ug/KgNDTAME 08/15/11 1.9 9.3 NA1
SW8260B NA 406253ug/KgND1,2-Dichloroethane 08/15/11 1.8 9.3 NA1
SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 3.6 9.3 NA1
SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 2.0 9.3 NA1
SW8260B NA 406253ug/KgND1,2-Dichloropropane 08/15/11 1.2 9.3 NA1
SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 1.0 9.3 NA1
SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 4.2 9.3 NA1
SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.3 9.3 NA1
SW8260B NA 406253ug/KgNDToluene 08/15/11 0.91 9.3 NA1
SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.7 9.3 NA1
SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.1 9.3 NA1
SW8260B NA 406253ug/KgND1,1,2-Trichloroethane 08/15/11 1.7 9.3 NA1
SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 1.0 9.3 NA1
SW8260B NA 406253ug/KgND1,3-Dichloropropane 08/15/11 1.9 9.3 NA1
Page 100 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:30
1204.22
500 Kirkham
B-7-1.0D
SoilSample Matrix:
Lab Sample ID: 1108084-019A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.6 9.3 NA1
SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.80 9.3 NA1
SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 3.9 9.3 NA1
SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.80 9.3 NA1
SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.7 9.3 NA1
SW8260B NA 406253ug/KgNDo-Xylene 08/15/11 0.61 4.7 NA1
SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.71 9.3 NA1
SW8260B NA 406253ug/KgNDBromoform 08/15/11 1.8 9.3 NA1
SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 1.2 9.3 NA1
SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.3 9.3 NA1
SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 1.1 9.3 NA1
SW8260B NA 406253ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.8 9.3 NA1
SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.0 9.3 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 3.1 9.3 NA1
SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.5 9.3 NA1
SW8260B NA 406253ug/KgND2-Chlorotoluene 08/15/11 1.5 9.3 NA1
SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.3 9.3 NA1
SW8260B NA 406253ug/KgND1,2,4-Trimethylbenzene 08/15/11 1.0 9.3 NA1
SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.5 9.3 NA1
SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.4 9.3 NA1
SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.7 9.3 NA1
SW8260B NA 406253ug/KgND1,4-Dichlorobenzene 08/15/11 1.4 9.3 NA1
SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 2.0 9.3 NA1
SW8260B NA 406253ug/KgND1,2-Dichlorobenzene 08/15/11 1.2 9.3 NA1
SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.9 9.3 NA1
SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 2.4 9.3 NA1
SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 2.0 9.3 NA1
SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.6 9.3 NA1
SW8260B NA 406253ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.7 9.3 NA1
SW8260B NA 406253%91.5(S) Dibromofluoromethane 08/15/11 59.8 148 NA1
SW8260B NA 406253%93.1(S) Toluene-d8 08/15/11 55.2 133 NA1
SW8260B NA 406253%109(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1
Page 101 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 10:30
1204.22
500 Kirkham
B-7-1.0D
SoilSample Matrix:
Lab Sample ID: 1108084-019A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 16 93 NA1
8260TPH NA 406253%68.9(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 0.759 2.0 34181
SW8015B(M) 8/18/11 406325mg/Kg8.9TPH as Motor Oil 08/18/11 1.65 4.0 34181
SW8015B(M) 8/18/11 406325mg/Kg105Pentacosane (S) 08/18/11 59.7 129 34181
Page 102 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-4-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-020A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406300ug/LNDDichlorodifluoromethane 08/16/11 0.41 0.50 NA1
SW8260B NA 406300ug/L0.88Chloromethane 08/16/11 0.41 0.50 NA1
SW8260B NA 406300ug/LNDVinyl Chloride 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDBromomethane 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDTrichlorofluoromethane 08/16/11 0.34 0.50 NA1
SW8260B NA 406300ug/LND1,1-Dichloroethene 08/16/11 0.29 0.50 NA1
SW8260B NA 406300ug/LNDFreon 113 08/16/11 0.38 0.50 NA1
SW8260B NA 406300ug/LNDMethylene Chloride 08/16/11 0.18 5.0 NA1
SW8260B NA 406300ug/LNDtrans-1,2-Dichloroethene 08/16/11 0.31 0.50 NA1
SW8260B NA 406300ug/LNDMTBE 08/16/11 0.38 0.50 NA1
SW8260B NA 406300ug/LNDtert-Butanol 08/16/11 1.5 5.0 NA1
SW8260B NA 406300ug/LNDDiisopropyl ether (DIPE) 08/16/11 0.36 0.50 NA1
SW8260B NA 406300ug/LND1,1-Dichloroethane 08/16/11 0.28 0.50 NA1
SW8260B NA 406300ug/LNDETBE 08/16/11 0.40 0.50 NA1
SW8260B NA 406300ug/LNDcis-1,2-Dichloroethene 08/16/11 0.33 0.50 NA1
SW8260B NA 406300ug/LND2,2-Dichloropropane 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDBromochloromethane 08/16/11 0.34 0.50 NA1
SW8260B NA 406300ug/LNDChloroform 08/16/11 0.29 0.50 NA1
SW8260B NA 406300ug/LNDCarbon Tetrachloride 08/16/11 0.26 0.50 NA1
SW8260B NA 406300ug/LND1,1,1-Trichloroethane 08/16/11 0.32 0.50 NA1
SW8260B NA 406300ug/LND1,1-Dichloropropene 08/16/11 0.40 0.50 NA1
SW8260B NA 406300ug/LNDBenzene 08/16/11 0.33 0.50 NA1
SW8260B NA 406300ug/LNDTAME 08/16/11 0.32 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dichloroethane 08/16/11 0.28 0.50 NA1
SW8260B NA 406300ug/LNDTrichloroethylene 08/16/11 0.38 0.50 NA1
SW8260B NA 406300ug/LNDDibromomethane 08/16/11 0.21 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dichloropropane 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDBromodichloromethane 08/16/11 0.23 0.50 NA1
SW8260B NA 406300ug/LNDcis-1,3-Dichloropropene 08/16/11 0.30 0.50 NA1
SW8260B NA 406300ug/LNDToluene 08/16/11 0.19 0.50 NA1
SW8260B NA 406300ug/LNDTetrachloroethylene 08/16/11 0.15 0.50 NA1
SW8260B NA 406300ug/LNDtrans-1,3-Dichloropropene 08/16/11 0.20 0.50 NA1
SW8260B NA 406300ug/LND1,1,2-Trichloroethane 08/16/11 0.20 0.50 NA1
SW8260B NA 406300ug/LNDDibromochloromethane 08/16/11 0.21 0.50 NA1
SW8260B NA 406300ug/LND1,3-Dichloropropane 08/16/11 0.18 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dibromoethane 08/16/11 0.19 0.50 NA1
Page 103 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-4-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-020A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406300ug/LNDChlorobenzene 08/16/11 0.14 0.50 NA1
SW8260B NA 406300ug/LNDEthyl Benzene 08/16/11 0.15 0.50 NA1
SW8260B NA 406300ug/LND1,1,1,2-Tetrachloroethane 08/16/11 0.10 0.50 NA1
SW8260B NA 406300ug/LNDm,p-Xylene 08/16/11 0.20 1.0 NA1
SW8260B NA 406300ug/LNDo-Xylene 08/16/11 0.13 0.50 NA1
SW8260B NA 406300ug/LNDStyrene 08/16/11 0.20 0.50 NA1
SW8260B NA 406300ug/LNDBromoform 08/16/11 0.45 1.0 NA1
SW8260B NA 406300ug/LNDIsopropyl Benzene 08/16/11 0.28 0.50 NA1
SW8260B NA 406300ug/LNDBromobenzene 08/16/11 0.39 0.50 NA1
SW8260B NA 406300ug/LND1,1,2,2-Tetrachloroethane 08/16/11 0.26 0.50 NA1
SW8260B NA 406300ug/LNDn-Propylbenzene 08/16/11 0.30 0.50 NA1
SW8260B NA 406300ug/LND2-Chlorotoluene 08/16/11 0.33 0.50 NA1
SW8260B NA 406300ug/LND1,3,5-Trimethylbenzene 08/16/11 0.20 0.50 NA1
SW8260B NA 406300ug/LND4-Chlorotoluene 08/16/11 0.32 0.50 NA1
SW8260B NA 406300ug/LNDtert-Butylbenzene 08/16/11 0.29 0.50 NA1
SW8260B NA 406300ug/LND1,2,3-Trichloropropane 08/16/11 0.59 1.0 NA1
SW8260B NA 406300ug/LND1,2,4-Trimethylbenzene 08/16/11 0.33 0.50 NA1
SW8260B NA 406300ug/LNDsec-Butyl Benzene 08/16/11 0.24 0.50 NA1
SW8260B NA 406300ug/LNDp-Isopropyltoluene 08/16/11 0.25 0.50 NA1
SW8260B NA 406300ug/LND1,3-Dichlorobenzene 08/16/11 0.31 0.50 NA1
SW8260B NA 406300ug/LND1,4-Dichlorobenzene 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDn-Butylbenzene 08/16/11 0.32 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dichlorobenzene 08/16/11 0.39 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dibromo-3-Chloropropane 08/16/11 0.45 1.0 NA1
SW8260B NA 406300ug/LNDHexachlorobutadiene 08/16/11 0.22 0.50 NA1
SW8260B NA 406300ug/LND1,2,4-Trichlorobenzene 08/16/11 0.48 1.0 NA1
SW8260B NA 406300ug/LNDNaphthalene 08/16/11 0.57 1.0 NA1
SW8260B NA 406300ug/LND1,2,3-Trichlorobenzene 08/16/11 0.52 1.0 NA1
SW8260B NA 406300%95.2(S) Dibromofluoromethane 08/16/11 61.2 131 NA1
SW8260B NA 406300%92.3(S) Toluene-d8 08/16/11 75.1 127 NA1
SW8260B NA 406300%91.3(S) 4-Bromofluorobenzene 08/16/11 64.1 120 NA1
Page 104 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-4-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-020A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406300ug/LNDTPH(Gasoline) 08/16/11 22 50 NA1
8260TPH NA 406300%71.1(S) 4-Bromofluorobenzene 08/16/11 34 114 NA1
Page 105 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-4-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-020B
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021
SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021
SW8015B(M) 8/16/11 406321%82.2Pentacosane (S) 08/17/11 57.9 125 34021
Page 106 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-4-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-020C
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771
SW6010B 8/12/11 406242mg/LNDArsenic (Dissolved) 08/15/11 0.005 0.009 33771
SW6010B 8/12/11 406242mg/L0.044Barium (Dissolved) 08/15/11 0.002 0.009 33771
SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771
SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/LNDCobalt (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771
SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771
SW6010B 8/12/11 406242mg/LNDMolybdenum (Dissolved) 08/15/11 0.002 0.009 33771
SW6010B 8/12/11 406242mg/LNDNickel (Dissolved) 08/15/11 0.002 0.009 33771
SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771
SW6010B 8/12/11 406242mg/LNDSilver (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771
SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771
SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7470A 8/12/11 406238mg/LNDMercury 08/15/11 0.00005 0.0002 33651
Page 107 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-8-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-021A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8260B NA 406300ug/LNDDichlorodifluoromethane 08/16/11 0.50 0.61 NA1.22
SW8260B NA 406300ug/LNDChloromethane 08/16/11 0.50 0.61 NA1.22
SW8260B NA 406300ug/LNDVinyl Chloride 08/16/11 0.45 0.61 NA1.22
SW8260B NA 406300ug/LNDBromomethane 08/16/11 0.46 0.61 NA1.22
SW8260B NA 406300ug/LNDTrichlorofluoromethane 08/16/11 0.42 0.61 NA1.22
SW8260B NA 406300ug/LND1,1-Dichloroethene 08/16/11 0.35 0.61 NA1.22
SW8260B NA 406300ug/LNDFreon 113 08/16/11 0.46 0.61 NA1.22
SW8260B NA 406300J ug/L0.36Methylene Chloride 08/16/11 0.21 6.1 NA1.22
SW8260B NA 406300ug/LNDtrans-1,2-Dichloroethene 08/16/11 0.38 0.61 NA1.22
SW8260B NA 406300ug/LNDMTBE 08/16/11 0.46 0.61 NA1.22
SW8260B NA 406300ug/LNDtert-Butanol 08/16/11 1.8 6.1 NA1.22
SW8260B NA 406300ug/LNDDiisopropyl ether (DIPE) 08/16/11 0.44 0.61 NA1.22
SW8260B NA 406300ug/LND1,1-Dichloroethane 08/16/11 0.34 0.61 NA1.22
SW8260B NA 406300ug/LNDETBE 08/16/11 0.48 0.61 NA1.22
SW8260B NA 406300ug/LNDcis-1,2-Dichloroethene 08/16/11 0.40 0.61 NA1.22
SW8260B NA 406300ug/LND2,2-Dichloropropane 08/16/11 0.46 0.61 NA1.22
SW8260B NA 406300ug/LNDBromochloromethane 08/16/11 0.42 0.61 NA1.22
SW8260B NA 406300ug/L4.9Chloroform 08/16/11 0.36 0.61 NA1.22
SW8260B NA 406300ug/LNDCarbon Tetrachloride 08/16/11 0.32 0.61 NA1.22
SW8260B NA 406300ug/LND1,1,1-Trichloroethane 08/16/11 0.39 0.61 NA1.22
SW8260B NA 406300ug/LND1,1-Dichloropropene 08/16/11 0.48 0.61 NA1.22
SW8260B NA 406300ug/LNDBenzene 08/16/11 0.41 0.61 NA1.22
SW8260B NA 406300ug/LNDTAME 08/16/11 0.39 0.61 NA1.22
SW8260B NA 406300ug/LND1,2-Dichloroethane 08/16/11 0.34 0.61 NA1.22
SW8260B NA 406300ug/LNDTrichloroethylene 08/16/11 0.46 0.61 NA1.22
SW8260B NA 406300ug/LNDDibromomethane 08/16/11 0.26 0.61 NA1.22
SW8260B NA 406300ug/LND1,2-Dichloropropane 08/16/11 0.45 0.61 NA1.22
SW8260B NA 406300ug/LNDBromodichloromethane 08/16/11 0.28 0.61 NA1.22
SW8260B NA 406300ug/LNDcis-1,3-Dichloropropene 08/16/11 0.37 0.61 NA1.22
SW8260B NA 406300ug/LNDToluene 08/16/11 0.23 0.61 NA1.22
SW8260B NA 406300ug/LNDTetrachloroethylene 08/16/11 0.18 0.61 NA1.22
SW8260B NA 406300ug/LNDtrans-1,3-Dichloropropene 08/16/11 0.25 0.61 NA1.22
SW8260B NA 406300ug/LND1,1,2-Trichloroethane 08/16/11 0.25 0.61 NA1.22
SW8260B NA 406300ug/LNDDibromochloromethane 08/16/11 0.26 0.61 NA1.22
SW8260B NA 406300ug/LND1,3-Dichloropropane 08/16/11 0.22 0.61 NA1.22
Page 108 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-8-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-021A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. SW8260B NA 406300ug/LND1,2-Dibromoethane 08/16/11 0.24 0.61 NA1.22
SW8260B NA 406300ug/LNDChlorobenzene 08/16/11 0.17 0.61 NA1.22
SW8260B NA 406300ug/LNDEthyl Benzene 08/16/11 0.19 0.61 NA1.22
SW8260B NA 406300ug/LND1,1,1,2-Tetrachloroethane 08/16/11 0.12 0.61 NA1.22
SW8260B NA 406300ug/LNDm,p-Xylene 08/16/11 0.24 1.2 NA1.22
SW8260B NA 406300ug/LNDo-Xylene 08/16/11 0.16 0.61 NA1.22
SW8260B NA 406300ug/LNDStyrene 08/16/11 0.24 0.61 NA1.22
SW8260B NA 406300ug/LNDBromoform 08/16/11 0.55 1.2 NA1.22
SW8260B NA 406300ug/LNDIsopropyl Benzene 08/16/11 0.34 0.61 NA1.22
SW8260B NA 406300ug/LNDBromobenzene 08/16/11 0.48 0.61 NA1.22
SW8260B NA 406300ug/LND1,1,2,2-Tetrachloroethane 08/16/11 0.31 0.61 NA1.22
SW8260B NA 406300ug/LNDn-Propylbenzene 08/16/11 0.36 0.61 NA1.22
SW8260B NA 406300ug/LND2-Chlorotoluene 08/16/11 0.40 0.61 NA1.22
SW8260B NA 406300ug/LND1,3,5-Trimethylbenzene 08/16/11 0.24 0.61 NA1.22
SW8260B NA 406300ug/LND4-Chlorotoluene 08/16/11 0.40 0.61 NA1.22
SW8260B NA 406300ug/LNDtert-Butylbenzene 08/16/11 0.35 0.61 NA1.22
SW8260B NA 406300ug/LND1,2,3-Trichloropropane 08/16/11 0.72 1.2 NA1.22
SW8260B NA 406300ug/LND1,2,4-Trimethylbenzene 08/16/11 0.40 0.61 NA1.22
SW8260B NA 406300ug/LNDsec-Butyl Benzene 08/16/11 0.30 0.61 NA1.22
SW8260B NA 406300ug/LNDp-Isopropyltoluene 08/16/11 0.30 0.61 NA1.22
SW8260B NA 406300ug/LND1,3-Dichlorobenzene 08/16/11 0.38 0.61 NA1.22
SW8260B NA 406300ug/LND1,4-Dichlorobenzene 08/16/11 0.45 0.61 NA1.22
SW8260B NA 406300ug/LNDn-Butylbenzene 08/16/11 0.39 0.61 NA1.22
SW8260B NA 406300ug/LND1,2-Dichlorobenzene 08/16/11 0.48 0.61 NA1.22
SW8260B NA 406300ug/LND1,2-Dibromo-3-Chloropropane 08/16/11 0.55 1.2 NA1.22
SW8260B NA 406300ug/LNDHexachlorobutadiene 08/16/11 0.27 0.61 NA1.22
SW8260B NA 406300ug/LND1,2,4-Trichlorobenzene 08/16/11 0.59 1.2 NA1.22
SW8260B NA 406300ug/LNDNaphthalene 08/16/11 0.70 1.2 NA1.22
SW8260B NA 406300ug/LND1,2,3-Trichlorobenzene 08/16/11 0.64 1.2 NA1.22
SW8260B NA 406300%94.7(S) Dibromofluoromethane 08/16/11 61.2 131 NA1.22
SW8260B NA 406300%92.1(S) Toluene-d8 08/16/11 75.1 127 NA1.22
SW8260B NA 406300%92.5(S) 4-Bromofluorobenzene 08/16/11 64.1 120 NA1.22
Reporting limits were raised due to sediment in all VOAs.NOTE:
Page 109 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-8-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-021A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
The results shown below are reported using their MDL. 8260TPH NA 406300ug/LNDTPH(Gasoline) 08/16/11 26 61 NA1.22
8260TPH NA 406300%71.1(S) 4-Bromofluorobenzene 08/16/11 34 114 NA1.22
Raised reporting limit - see comment for 8260B analysis.NOTE:
Page 110 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-8-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-021B
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021
SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021
SW8015B(M) 8/16/11 406321%73.4Pentacosane (S) 08/17/11 57.9 125 34021
Page 111 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 9:20
1204.22
500 Kirkham
B-8-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-021C
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771
SW6010B 8/12/11 406242mg/LNDArsenic (Dissolved) 08/15/11 0.005 0.009 33771
SW6010B 8/12/11 406242mg/L0.091Barium (Dissolved) 08/15/11 0.002 0.009 33771
SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771
SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/L0.0052Cobalt (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771
SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771
SW6010B 8/12/11 406242mg/L0.015Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771
SW6010B 8/12/11 406242mg/LNDNickel (Dissolved) 08/15/11 0.002 0.009 33771
SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771
SW6010B 8/12/11 406242mg/LNDSilver (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771
SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771
SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7470A 8/12/11 406238mg/LNDMercury 08/15/11 0.00005 0.0002 33651
Page 112 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:30
1204.22
500 Kirkham
B-16-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-022A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406300ug/LNDDichlorodifluoromethane 08/16/11 0.41 0.50 NA1
SW8260B NA 406300ug/LNDChloromethane 08/16/11 0.41 0.50 NA1
SW8260B NA 406300ug/LNDVinyl Chloride 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDBromomethane 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDTrichlorofluoromethane 08/16/11 0.34 0.50 NA1
SW8260B NA 406300ug/LND1,1-Dichloroethene 08/16/11 0.29 0.50 NA1
SW8260B NA 406300ug/LNDFreon 113 08/16/11 0.38 0.50 NA1
SW8260B NA 406300ug/LNDMethylene Chloride 08/16/11 0.18 5.0 NA1
SW8260B NA 406300ug/LNDtrans-1,2-Dichloroethene 08/16/11 0.31 0.50 NA1
SW8260B NA 406300ug/LNDMTBE 08/16/11 0.38 0.50 NA1
SW8260B NA 406300ug/LNDtert-Butanol 08/16/11 1.5 5.0 NA1
SW8260B NA 406300ug/LNDDiisopropyl ether (DIPE) 08/16/11 0.36 0.50 NA1
SW8260B NA 406300ug/LND1,1-Dichloroethane 08/16/11 0.28 0.50 NA1
SW8260B NA 406300ug/LNDETBE 08/16/11 0.40 0.50 NA1
SW8260B NA 406300ug/LNDcis-1,2-Dichloroethene 08/16/11 0.33 0.50 NA1
SW8260B NA 406300ug/LND2,2-Dichloropropane 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDBromochloromethane 08/16/11 0.34 0.50 NA1
SW8260B NA 406300ug/LNDChloroform 08/16/11 0.29 0.50 NA1
SW8260B NA 406300ug/LNDCarbon Tetrachloride 08/16/11 0.26 0.50 NA1
SW8260B NA 406300ug/LND1,1,1-Trichloroethane 08/16/11 0.32 0.50 NA1
SW8260B NA 406300ug/LND1,1-Dichloropropene 08/16/11 0.40 0.50 NA1
SW8260B NA 406300ug/LNDBenzene 08/16/11 0.33 0.50 NA1
SW8260B NA 406300ug/LNDTAME 08/16/11 0.32 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dichloroethane 08/16/11 0.28 0.50 NA1
SW8260B NA 406300ug/LNDTrichloroethylene 08/16/11 0.38 0.50 NA1
SW8260B NA 406300ug/LNDDibromomethane 08/16/11 0.21 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dichloropropane 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDBromodichloromethane 08/16/11 0.23 0.50 NA1
SW8260B NA 406300ug/LNDcis-1,3-Dichloropropene 08/16/11 0.30 0.50 NA1
SW8260B NA 406300ug/LNDToluene 08/16/11 0.19 0.50 NA1
SW8260B NA 406300ug/LNDTetrachloroethylene 08/16/11 0.15 0.50 NA1
SW8260B NA 406300ug/LNDtrans-1,3-Dichloropropene 08/16/11 0.20 0.50 NA1
SW8260B NA 406300ug/LND1,1,2-Trichloroethane 08/16/11 0.20 0.50 NA1
SW8260B NA 406300ug/LNDDibromochloromethane 08/16/11 0.21 0.50 NA1
SW8260B NA 406300ug/LND1,3-Dichloropropane 08/16/11 0.18 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dibromoethane 08/16/11 0.19 0.50 NA1
Page 113 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:30
1204.22
500 Kirkham
B-16-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-022A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406300ug/LNDChlorobenzene 08/16/11 0.14 0.50 NA1
SW8260B NA 406300ug/LNDEthyl Benzene 08/16/11 0.15 0.50 NA1
SW8260B NA 406300ug/LND1,1,1,2-Tetrachloroethane 08/16/11 0.10 0.50 NA1
SW8260B NA 406300ug/LNDm,p-Xylene 08/16/11 0.20 1.0 NA1
SW8260B NA 406300ug/LNDo-Xylene 08/16/11 0.13 0.50 NA1
SW8260B NA 406300ug/LNDStyrene 08/16/11 0.20 0.50 NA1
SW8260B NA 406300ug/LNDBromoform 08/16/11 0.45 1.0 NA1
SW8260B NA 406300ug/LNDIsopropyl Benzene 08/16/11 0.28 0.50 NA1
SW8260B NA 406300ug/LNDBromobenzene 08/16/11 0.39 0.50 NA1
SW8260B NA 406300ug/LND1,1,2,2-Tetrachloroethane 08/16/11 0.26 0.50 NA1
SW8260B NA 406300ug/LNDn-Propylbenzene 08/16/11 0.30 0.50 NA1
SW8260B NA 406300ug/LND2-Chlorotoluene 08/16/11 0.33 0.50 NA1
SW8260B NA 406300ug/LND1,3,5-Trimethylbenzene 08/16/11 0.20 0.50 NA1
SW8260B NA 406300ug/LND4-Chlorotoluene 08/16/11 0.32 0.50 NA1
SW8260B NA 406300ug/LNDtert-Butylbenzene 08/16/11 0.29 0.50 NA1
SW8260B NA 406300ug/LND1,2,3-Trichloropropane 08/16/11 0.59 1.0 NA1
SW8260B NA 406300ug/LND1,2,4-Trimethylbenzene 08/16/11 0.33 0.50 NA1
SW8260B NA 406300ug/LNDsec-Butyl Benzene 08/16/11 0.24 0.50 NA1
SW8260B NA 406300ug/LNDp-Isopropyltoluene 08/16/11 0.25 0.50 NA1
SW8260B NA 406300ug/LND1,3-Dichlorobenzene 08/16/11 0.31 0.50 NA1
SW8260B NA 406300ug/LND1,4-Dichlorobenzene 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDn-Butylbenzene 08/16/11 0.32 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dichlorobenzene 08/16/11 0.39 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dibromo-3-Chloropropane 08/16/11 0.45 1.0 NA1
SW8260B NA 406300ug/LNDHexachlorobutadiene 08/16/11 0.22 0.50 NA1
SW8260B NA 406300ug/LND1,2,4-Trichlorobenzene 08/16/11 0.48 1.0 NA1
SW8260B NA 406300ug/LNDNaphthalene 08/16/11 0.57 1.0 NA1
SW8260B NA 406300ug/LND1,2,3-Trichlorobenzene 08/16/11 0.52 1.0 NA1
SW8260B NA 406300%95.8(S) Dibromofluoromethane 08/16/11 61.2 131 NA1
SW8260B NA 406300%93.1(S) Toluene-d8 08/16/11 75.1 127 NA1
SW8260B NA 406300%93.0(S) 4-Bromofluorobenzene 08/16/11 64.1 120 NA1
Page 114 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:30
1204.22
500 Kirkham
B-16-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-022A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406300ug/LNDTPH(Gasoline) 08/16/11 22 50 NA1
8260TPH NA 406300%68.7(S) 4-Bromofluorobenzene 08/16/11 34 114 NA1
Page 115 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:30
1204.22
500 Kirkham
B-16-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-022B
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021
SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021
SW8015B(M) 8/16/11 406321%79.0Pentacosane (S) 08/17/11 57.9 125 34021
Page 116 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 12:30
1204.22
500 Kirkham
B-16-GW
GroundwaterSample Matrix:
Lab Sample ID: 1108084-022C
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771
SW6010B 8/12/11 406242mg/L0.010Arsenic (Dissolved) 08/15/11 0.005 0.009 33771
SW6010B 8/12/11 406242mg/L0.12Barium (Dissolved) 08/15/11 0.002 0.009 33771
SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771
SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/L0.0057Cobalt (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771
SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771
SW6010B 8/12/11 406242mg/L0.022Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771
SW6010B 8/12/11 406242mg/L0.059Nickel (Dissolved) 08/15/11 0.002 0.009 33771
SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771
SW6010B 8/12/11 406242mg/LNDSilver (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771
SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771
SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7470A 8/12/11 406238mg/LNDMercury 08/15/11 0.00005 0.0002 33651
Page 117 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 13:00
1204.22
500 Kirkham
FB
GroundwaterSample Matrix:
Lab Sample ID: 1108084-023A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406300ug/LNDDichlorodifluoromethane 08/16/11 0.41 0.50 NA1
SW8260B NA 406300ug/LNDChloromethane 08/16/11 0.41 0.50 NA1
SW8260B NA 406300ug/LNDVinyl Chloride 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDBromomethane 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDTrichlorofluoromethane 08/16/11 0.34 0.50 NA1
SW8260B NA 406300ug/LND1,1-Dichloroethene 08/16/11 0.29 0.50 NA1
SW8260B NA 406300ug/LNDFreon 113 08/16/11 0.38 0.50 NA1
SW8260B NA 406300ug/LNDMethylene Chloride 08/16/11 0.18 5.0 NA1
SW8260B NA 406300ug/LNDtrans-1,2-Dichloroethene 08/16/11 0.31 0.50 NA1
SW8260B NA 406300ug/LNDMTBE 08/16/11 0.38 0.50 NA1
SW8260B NA 406300ug/LNDtert-Butanol 08/16/11 1.5 5.0 NA1
SW8260B NA 406300ug/LNDDiisopropyl ether (DIPE) 08/16/11 0.36 0.50 NA1
SW8260B NA 406300ug/LND1,1-Dichloroethane 08/16/11 0.28 0.50 NA1
SW8260B NA 406300ug/LNDETBE 08/16/11 0.40 0.50 NA1
SW8260B NA 406300ug/LNDcis-1,2-Dichloroethene 08/16/11 0.33 0.50 NA1
SW8260B NA 406300ug/LND2,2-Dichloropropane 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDBromochloromethane 08/16/11 0.34 0.50 NA1
SW8260B NA 406300ug/LNDChloroform 08/16/11 0.29 0.50 NA1
SW8260B NA 406300ug/LNDCarbon Tetrachloride 08/16/11 0.26 0.50 NA1
SW8260B NA 406300ug/LND1,1,1-Trichloroethane 08/16/11 0.32 0.50 NA1
SW8260B NA 406300ug/LND1,1-Dichloropropene 08/16/11 0.40 0.50 NA1
SW8260B NA 406300ug/LNDBenzene 08/16/11 0.33 0.50 NA1
SW8260B NA 406300ug/LNDTAME 08/16/11 0.32 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dichloroethane 08/16/11 0.28 0.50 NA1
SW8260B NA 406300ug/LNDTrichloroethylene 08/16/11 0.38 0.50 NA1
SW8260B NA 406300ug/LNDDibromomethane 08/16/11 0.21 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dichloropropane 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDBromodichloromethane 08/16/11 0.23 0.50 NA1
SW8260B NA 406300ug/LNDcis-1,3-Dichloropropene 08/16/11 0.30 0.50 NA1
SW8260B NA 406300ug/LNDToluene 08/16/11 0.19 0.50 NA1
SW8260B NA 406300ug/LNDTetrachloroethylene 08/16/11 0.15 0.50 NA1
SW8260B NA 406300ug/LNDtrans-1,3-Dichloropropene 08/16/11 0.20 0.50 NA1
SW8260B NA 406300ug/LND1,1,2-Trichloroethane 08/16/11 0.20 0.50 NA1
SW8260B NA 406300ug/LNDDibromochloromethane 08/16/11 0.21 0.50 NA1
SW8260B NA 406300ug/LND1,3-Dichloropropane 08/16/11 0.18 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dibromoethane 08/16/11 0.19 0.50 NA1
Page 118 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 13:00
1204.22
500 Kirkham
FB
GroundwaterSample Matrix:
Lab Sample ID: 1108084-023A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406300ug/LNDChlorobenzene 08/16/11 0.14 0.50 NA1
SW8260B NA 406300ug/LNDEthyl Benzene 08/16/11 0.15 0.50 NA1
SW8260B NA 406300ug/LND1,1,1,2-Tetrachloroethane 08/16/11 0.10 0.50 NA1
SW8260B NA 406300ug/LNDm,p-Xylene 08/16/11 0.20 1.0 NA1
SW8260B NA 406300ug/LNDo-Xylene 08/16/11 0.13 0.50 NA1
SW8260B NA 406300ug/LNDStyrene 08/16/11 0.20 0.50 NA1
SW8260B NA 406300ug/LNDBromoform 08/16/11 0.45 1.0 NA1
SW8260B NA 406300ug/LNDIsopropyl Benzene 08/16/11 0.28 0.50 NA1
SW8260B NA 406300ug/LNDBromobenzene 08/16/11 0.39 0.50 NA1
SW8260B NA 406300ug/LND1,1,2,2-Tetrachloroethane 08/16/11 0.26 0.50 NA1
SW8260B NA 406300ug/LNDn-Propylbenzene 08/16/11 0.30 0.50 NA1
SW8260B NA 406300ug/LND2-Chlorotoluene 08/16/11 0.33 0.50 NA1
SW8260B NA 406300ug/LND1,3,5-Trimethylbenzene 08/16/11 0.20 0.50 NA1
SW8260B NA 406300ug/LND4-Chlorotoluene 08/16/11 0.32 0.50 NA1
SW8260B NA 406300ug/LNDtert-Butylbenzene 08/16/11 0.29 0.50 NA1
SW8260B NA 406300ug/LND1,2,3-Trichloropropane 08/16/11 0.59 1.0 NA1
SW8260B NA 406300ug/LND1,2,4-Trimethylbenzene 08/16/11 0.33 0.50 NA1
SW8260B NA 406300ug/LNDsec-Butyl Benzene 08/16/11 0.24 0.50 NA1
SW8260B NA 406300ug/LNDp-Isopropyltoluene 08/16/11 0.25 0.50 NA1
SW8260B NA 406300ug/LND1,3-Dichlorobenzene 08/16/11 0.31 0.50 NA1
SW8260B NA 406300ug/LND1,4-Dichlorobenzene 08/16/11 0.37 0.50 NA1
SW8260B NA 406300ug/LNDn-Butylbenzene 08/16/11 0.32 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dichlorobenzene 08/16/11 0.39 0.50 NA1
SW8260B NA 406300ug/LND1,2-Dibromo-3-Chloropropane 08/16/11 0.45 1.0 NA1
SW8260B NA 406300ug/LNDHexachlorobutadiene 08/16/11 0.22 0.50 NA1
SW8260B NA 406300ug/LND1,2,4-Trichlorobenzene 08/16/11 0.48 1.0 NA1
SW8260B NA 406300ug/LNDNaphthalene 08/16/11 0.57 1.0 NA1
SW8260B NA 406300ug/LND1,2,3-Trichlorobenzene 08/16/11 0.52 1.0 NA1
SW8260B NA 406300%89.9(S) Dibromofluoromethane 08/16/11 61.2 131 NA1
SW8260B NA 406300%91.6(S) Toluene-d8 08/16/11 75.1 127 NA1
SW8260B NA 406300%88.4(S) 4-Bromofluorobenzene 08/16/11 64.1 120 NA1
Page 119 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 13:15
1204.22
500 Kirkham
IDW
SoilSample Matrix:
Lab Sample ID: 1108084-024A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/16/11 406288mg/KgNDAntimony 08/17/11 0.20 5.0 34051
SW6010B 8/16/11 406288mg/KgNDArsenic 08/17/11 0.28 1.7 34051
SW6010B 8/16/11 406288mg/Kg39Barium 08/17/11 1 5.0 34051
SW6010B 8/16/11 406288mg/KgNDBeryllium 08/17/11 0.0840 2.0 34051
SW6010B 8/16/11 406288mg/KgNDCadmium 08/17/11 0.0590 1.0 34051
SW6010B 8/16/11 406288mg/Kg31Chromium 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/Kg5.5Cobalt 08/17/11 0.14 5.0 34051
SW6010B 8/16/11 406288mg/KgNDCopper 08/17/11 0.0900 5.0 34051
SW6010B 8/16/11 406288mg/Kg3.0Lead 08/17/11 0.043 1.0 34051
SW6010B 8/16/11 406288mg/KgNDMolybdenum 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/Kg25Nickel 08/17/11 0.0590 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSelenium 08/17/11 0.29 5.0 34051
SW6010B 8/16/11 406288mg/KgNDSilver 08/17/11 1.0 1.0 34051
SW6010B 8/16/11 406288mg/KgNDThallium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg21Vanadium 08/17/11 0.12 5.0 34051
SW6010B 8/16/11 406288mg/Kg18Zinc 08/17/11 0.59 5.0 34051
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7471A 8/15/11 406270mg/KgNDMercury 08/16/11 0.01 0.10 33931
Page 120 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 13:15
1204.22
500 Kirkham
IDW
SoilSample Matrix:
Lab Sample ID: 1108084-024A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8081A 8/18/11 406333ug/KgNDalpha-BHC 08/18/11 1.8 8.0 34204
SW8081A 8/18/11 406333ug/KgNDgamma-BHC 08/18/11 1.6 8.0 34204
SW8081A 8/18/11 406333ug/KgNDbeta-BHC 08/18/11 1.5 8.0 34204
SW8081A 8/18/11 406333ug/KgNDdelta-BHC 08/18/11 2.0 8.0 34204
SW8081A 8/18/11 406333ug/KgNDHeptachlor 08/18/11 4.4 8.0 34204
SW8081A 8/18/11 406333ug/KgNDAldrin 08/18/11 1.8 8.0 34204
SW8081A 8/18/11 406333ug/KgNDHeptachlor epoxide 08/18/11 1.3 8.0 34204
SW8081A 8/18/11 406333ug/KgNDgamma-Chlordane 08/18/11 1.7 8.0 34204
SW8081A 8/18/11 406333ug/KgNDalpha-Chlordane 08/18/11 1.4 8.0 34204
SW8081A 8/18/11 406333ug/KgNDEndosulfan I 08/18/11 2.4 8.0 34204
SW8081A 8/18/11 406333ug/KgND4,4'-DDE 08/18/11 1.9 8.0 34204
SW8081A 8/18/11 406333ug/KgNDDieldrin 08/18/11 1.7 8.0 34204
SW8081A 8/18/11 406333ug/KgNDEndrin 08/18/11 2.3 8.0 34204
SW8081A 8/18/11 406333ug/KgND4,4'-DDD 08/18/11 1.9 8.0 34204
SW8081A 8/18/11 406333ug/KgNDEndosulfan II 08/18/11 6.1 8.0 34204
SW8081A 8/18/11 406333ug/KgND4,4'-DDT 08/18/11 3.2 8.0 34204
SW8081A 8/18/11 406333ug/KgNDEndrin aldehyde 08/18/11 4.1 8.0 34204
SW8081A 8/18/11 406333ug/KgNDEndosulfan sulfate 08/18/11 2.0 8.0 34204
SW8081A 8/18/11 406333ug/KgNDMethoxychlor 08/18/11 2.5 20 34204
SW8081A 8/18/11 406333ug/KgNDEndrin Ketone 08/18/11 1.6 8.0 34204
SW8081A 8/18/11 406333ug/KgNDChlordane 08/18/11 40 80 34204
SW8081A 8/18/11 406333ug/KgNDToxaphene 08/18/11 40 400 34204
SW8081A 8/18/11 406333%85.0TCMX (S) 08/18/11 52.5 139 34204
SW8081A 8/18/11 406333%73.5DCBP (S) 08/18/11 50.2 139 34204
Reporting limits increased due to the nature of the sample matrix (dark color extract).NOTE:
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 17 100 NA1
8260TPH NA 406253%73.3(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1
Page 121 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 13:15
1204.22
500 Kirkham
IDW
SoilSample Matrix:
Lab Sample ID: 1108084-024A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 1.84 4.8 34181
SW8015B(M) 8/18/11 406325mg/Kg57TPH as Motor Oil 08/18/11 4.00 9.6 34181
SW8015B(M) 8/18/11 406325mg/Kg90.7Pentacosane (S) 08/18/11 59.7 129 34181
Page 122 of 159Total Page Count: 159
SAMPLE RESULTS
Report prepared for: Date Reported: 08/26/11Date Received: 08/23/11
Northgate Environmental Management Inc.Anya Starovoytov
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/11/11 / 13:22
1204.22
500 Kirkham
EQUIP BLANK
GroundwaterSample Matrix:
Lab Sample ID: 1108084-025A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771
SW6010B 8/12/11 406242mg/LNDArsenic (Dissolved) 08/15/11 0.005 0.009 33771
SW6010B 8/12/11 406242mg/LNDBarium (Dissolved) 08/15/11 0.002 0.009 33771
SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771
SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/LNDCobalt (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771
SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771
SW6010B 8/12/11 406242mg/LNDMolybdenum (Dissolved) 08/15/11 0.002 0.009 33771
SW6010B 8/12/11 406242mg/LNDNickel (Dissolved) 08/15/11 0.002 0.009 33771
SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771
SW6010B 8/12/11 406242mg/LNDSilver (Dissolved) 08/15/11 0.002 0.005 33771
SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771
SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771
SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7470A 8/12/11 406238mg/LNDMercury 08/15/11 0.00005 0.0002 33651
Page 123 of 159Total Page Count: 159
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW7470AAnalytical Method:
Prep Date:
Analyzed Date:
08/12/11 Prep Batch:
Analytical Batch:
406238
mg/L
08/15/11
33657470A1108084
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.00005 0.0002Mercury 0.00007
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/12/11 Prep Batch:
Analytical Batch:
406242
mg/Kg
08/15/11
337730051108084
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.004 0.009Antimony (Dissolved) ND
0.005 0.009Arsenic (Dissolved) ND
0.002 0.009Barium (Dissolved) ND
0.002 0.005Beryllium (Dissolved) ND
0.001 0.005Cadmium (Dissolved) ND
0.002 0.005Chromium (Dissolved) ND
0.002 0.005Cobalt (Dissolved) ND
0.003 0.009Copper (Dissolved) 0.00357
0.005 0.014Lead (Dissolved) ND
0.002 0.009Molybdenum (Dissolved) ND
0.002 0.009Nickel (Dissolved) ND
0.004 0.02Selenium (Dissolved) ND
0.002 0.005Silver (Dissolved) ND
0.004 0.009Thallium (dissolved) ND
0.004 0.009Vanadium (Dissolved) ND
0.002 0.009Zinc (dissolved) ND
Page 124 of 159Total Page Count: 159
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8270CAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406316
mg/Kg
08/16/11
33853545_BNA1108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.660 0.653Pyridine ND
0.110 0.330N-Nitrosdimethylamine ND
0.123 0.330Aniline ND
0.129 0.330Phenol ND
0.0683 0.330Bis(2-chloroethyl) ether ND
0.129 0.3302-Chlorophenol ND
0.0733 0.3301,3-Dichlorobenzene ND
0.0663 6.591,4-Dichlorobenzene ND
0.104 0.330Benzyl Alcohol ND
0.0713 0.3301,2-Dichlorobenzene ND
0.116 0.3302-Methylphenol (o-Cresol) ND
0.0683 0.330Bis(2-chloroisopropyl)ether ND
0.139 0.3303-/4-Methylphenol (p-/m-Cresol) ND
0.0931 0.330N-nitroso-di-n-propylamine ND
0.0465 0.330Hexachloroethane ND
0.0528 0.330Nitrobenzene ND
0.0574 0.653Isophorone ND
0.0525 0.6532-Nitrophenol ND
0.133 6.592,4-Dimethylphenol ND
5.59 0.330Benzoic Acid ND
0.0584 0.330Bis(2-Chloroethoxy)methane ND
0.104 0.3302,4-Dichlorophenol ND
0.0733 0.3301,2,4-Trichlorobenzene ND
0.104 0.3302,6-Dichlorophenol ND
0.0901 0.330Naphthalene ND
0.0990 0.3304-Chloroaniline ND
0.0653 0.330Hexachloro-1,3-butadiene ND
0.102 0.3304-Chloro-3-methylphenol ND
0.0792 0.3302-Methylnaphthalene ND
0.0792 0.3301-Methylnaphthalene ND
0.0277 0.330Hexachlorocyclopentadiene ND
0.0950 0.3302,4,6-Trichlorophenol ND
0.121 0.3302,4,5-Trichlorophenol ND
0.0594 3.272-Chloronaphthalene ND
0.0693 0.3302-Nitroaniline ND
0.118 0.330Dimethyl phthalate ND
0.106 0.3301,3-Dinitrobenzene ND
0.0851 0.330Acenaphthylene ND
0.0267 0.3302,6-Dinitrotoluene ND
0.0858 0.3301,2-Dinitrobenzene ND
0.0693 0.3303-Nitroaniline ND
Page 125 of 159Total Page Count: 159
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8270CAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406316
mg/Kg
08/16/11
33853545_BNA1108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0960 0.330Acenaphthene ND
0.0297 3.272,4-Dinitrophenol ND
0.0663 0.3304-Nitrophenol ND
0.0782 0.330Dibenzofuran ND
0.0267 0.3302,4-Dinitrotoluene ND
0.119 0.3302,3,5,6-Tetrachlorophenol ND
0.119 0.3302,3,4,6-Tetrachlorophenol ND
0.117 0.330Diethylphthalate ND
0.0990 0.330Fluorene ND
0.0802 0.3304-Chlorophenyl phenyl ether ND
0.0802 0.3304-Nitroaniline ND
0.0663 0.3304,6-Dinitro-2-methylphenol ND
0.0663 0.330Diphenylamine ND
0.109 0.330Azobenzene ND
0.0812 3.274-Bromophenyl phenyl ether ND
0.101 0.330Hexachlorobenzene ND
0.102 3.27Pentachlorophenol ND
0.142 0.330Phenanthrene ND
0.132 0.330Anthracene ND
0.132 0.330Carbazole ND
0.108 1.68Di-n-butylphthalate ND
0.132 0.653Fluoranthene ND
0.374 3.27Benzidine ND
0.147 0.330Pyrene ND
0.0891 0.330Benzyl butyl phthalate ND
0.149 0.330Benz[a]anthracene ND
0.152 0.3303,3'-Dichlorobenzidine ND
0.176 0.330Chrysene ND
0.0832 0.330Bis(2-Ethylhexyl)phthalate ND
0.138 0.330Di-n-octyl phthalate ND
0.133 0.330Benzo[b]fluoranthene ND
0.169 0.330Benzo[k]fluoranthene ND
0.135 0.330Benzo[a]pyrene ND
0.131 0.330Indeno[1,2,3-cd]pyrene ND
0.151 0.330Dibenz[a,h]anthracene ND
0.150 0.330Benzo[g,h,i]perylene ND
0.150 0.3301,4-Dinitrobenzene ND
2,4,6-Tribromophenol (S) 33.3
2-Fluorobiphenyl (S) 46.7
2-Fluorophenol (S) 59.8
Nitrobenzene-d5 (S) 48.5
Page 126 of 159Total Page Count: 159
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8270CAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406316
mg/Kg
08/16/11
33853545_BNA1108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
Phenol-d6 (S) 60.6
p-Terphenyl-d14 (S) 89.6
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406267
mg/Kg
08/16/11
338930501108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.20 5.0Antimony 0.35
0.28 1.7Arsenic 0.28
1 5.0Barium 1.1
0.0840 2.0Beryllium ND
0.059 1.0Cadmium ND
0.059 5.0Chromium 0.33
0.14 5.0Cobalt ND
0.090 5.0Copper 0.18
0.043 1.0Lead 0.34
0.059 5.0Molybdenum 0.12
0.059 5.0Nickel 0.15
0.29 5.0Selenium ND
1.0 1.0Silver ND
0.12 5.0Thallium ND
0.12 5.0Vanadium 0.14
0.59 5.0Zinc 0.88
Work Order:
Matrix:
Units:
Prep Method:
7471ABAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406270
mg/Kg
08/16/11
339374711108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.01 0.10Mercury ND
Page 127 of 159Total Page Count: 159
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
406321
mg/L
08/17/11
34023510_TPHSG1108084
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0440 0.10TPH as Diesel (SG) ND
0.0920 0.20TPH as Motor Oil (SG) ND
Pentacosane (S) 51.7 S
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
406321
mg/L
08/17/11
34023510_TPHSG1108084
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0440 0.10TPH as Diesel (SG) ND
0.0920 0.20TPH as Motor Oil (SG) 0.13
Pentacosane (S) 75.1
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
406288
mg/Kg
08/17/11
340530501108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.20 5.0Antimony 0.30
0.28 1.7Arsenic ND
1 5.0Barium 1.1
0.0840 2.0Beryllium ND
0.059 1.0Cadmium ND
0.059 5.0Chromium 0.35
0.14 5.0Cobalt ND
0.090 5.0Copper 0.25
0.043 1.0Lead 0.25
0.059 5.0Molybdenum 0.060
0.059 5.0Nickel 0.12
0.29 5.0Selenium ND
1.0 1.0Silver ND
0.12 5.0Thallium ND
0.12 5.0Vanadium 0.12
0.59 5.0Zinc 0.85
Page 128 of 159Total Page Count: 159
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
406300
ug/L
08/16/11
341450301108084
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
22 50TPH(Gasoline) ND
(S) 4-Bromofluorobenzene 90.2
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
406253
ug/Kg
08/15/11
341750351108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
17 100TPH(Gasoline) ND
(S) 4-Bromofluorobenzene 101
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/18/11 Prep Batch:
Analytical Batch:
406325
mg/Kg
08/18/11
34183545_TPH1108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.758 2.0TPH as Diesel 1.2
1.78 4.0TPH as Motor Oil 3.3
Pentacosane (S) 111
Page 129 of 159Total Page Count: 159
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8082Analytical Method:
Prep Date:
Analyzed Date:
08/18/11 Prep Batch:
Analytical Batch:
406326
mg/Kg
08/18/11
34193545_PCB1108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0230 0.10Aroclor1016 ND
0.0920 0.20Aroclor1221 ND
0.0460 0.10Aroclor1232 ND
0.0430 0.10Aroclor1242 ND
0.0360 0.10Aroclor1248 ND
0.0240 0.10Aroclor1254 ND
0.0270 0.10Aroclor1260 ND
TCMX (S) 99.1
DCBP (S) 113
Page 130 of 159Total Page Count: 159
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8081AAnalytical Method:
Prep Date:
Analyzed Date:
08/18/11 Prep Batch:
Analytical Batch:
406333
ug/Kg
08/18/11
34203545_OCP1108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.44 2.0alpha-BHC ND
0.40 2.0gamma-BHC ND
0.36 2.0beta-BHC ND
0.49 2.0delta-BHC ND
1.1 2.0Heptachlor ND
0.44 2.0Aldrin ND
0.32 2.0Heptachlor epoxide ND
0.42 2.0gamma-Chlordane ND
0.36 2.0alpha-Chlordane ND
0.59 2.0Endosulfan I ND
0.48 2.04,4'-DDE ND
0.43 2.0Dieldrin ND
0.57 2.0Endrin ND
0.47 2.04,4'-DDD ND
1.5 2.0Endosulfan II ND
0.81 2.04,4'-DDT ND
1.0 2.0Endrin aldehyde ND
0.49 2.0Endosulfan sulfate ND
0.62 5.0Methoxychlor ND
0.40 2.0Endrin Ketone ND
10 20Chlordane ND
10 100Toxaphene ND
TCMX (S) 100
DCBP (S) 101
Page 131 of 159Total Page Count: 159
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/24/11 Prep Batch:
Analytical Batch:
406410
mg/Kg
08/24/11
347930501108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.20 5.0Antimony ND
0.28 1.7Arsenic ND
1 5.0Barium 1.8
0.0840 2.0Beryllium ND
0.059 1.0Cadmium ND
0.059 5.0Chromium 0.14
0.14 5.0Cobalt ND
0.090 5.0Copper 0.96
0.043 1.0Lead 0.25
0.059 5.0Molybdenum 0.17
0.059 5.0Nickel 0.095
0.29 5.0Selenium ND
1.0 1.0Silver ND
0.12 5.0Thallium 0.60
0.12 5.0Vanadium ND
0.59 5.0Zinc 1.2
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/24/11 Prep Batch:
Analytical Batch:
406421
mg/L
08/25/11
34891311/3010B1108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0500 0.10Lead (TCLP) ND
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/25/11 Prep Batch:
Analytical Batch:
406448
mg/Kg
08/25/11
34943545_TPH1108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.758 2.0TPH as Diesel 1.7
1.78 4.0TPH as Motor Oil 2.8
Pentacosane (S) 120
Page 132 of 159Total Page Count: 159
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/25/11 Prep Batch:
Analytical Batch:
406447
mg/Kg
08/26/11
3496WET/3010B1108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0500 0.10Lead (STLC) ND
Page 133 of 159Total Page Count: 159
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
406253
ug/Kg
08/15/11
NANA1108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
4.4 10Dichlorodifluoromethane ND
4.6 10Chloromethane ND
2.6 10Vinyl Chloride ND
4.7 10Bromomethane ND
2.9 10Trichlorofluoromethane ND
1.5 101,1-Dichloroethene ND
3.7 10Freon 113 ND
2.0 50Methylene Chloride ND
1.1 10trans-1,2-Dichloroethene ND
2.6 10MTBE ND
21 50tert-Butanol ND
2.2 10Diisopropyl ether (DIPE) ND
1.3 101,1-Dichloroethane ND
2.4 10ETBE ND
1.8 10cis-1,2-Dichloroethene ND
1.2 102,2-Dichloropropane ND
2.3 10Bromochloromethane ND
1.2 10Chloroform ND
1.6 10Carbon Tetrachloride ND
1.2 101,1,1-Trichloroethane ND
1.4 101,1-Dichloropropene ND
1.5 10Benzene ND
2.1 10TAME ND
1.9 101,2-Dichloroethane ND
3.9 10Trichloroethylene ND
2.2 10Dibromomethane ND
1.3 101,2-Dichloropropane ND
1.1 10Bromodichloromethane ND
1.4 10cis-1,3-Dichloropropene ND
0.98 10Toluene ND
1.8 10Tetrachloroethylene ND
1.2 10trans-1,3-Dichloropropene ND
1.8 101,1,2-Trichloroethane ND
1.1 10Dibromochloromethane ND
2.1 101,3-Dichloropropane ND
1.7 101,2-Dibromoethane ND
0.86 10Ethyl Benzene ND
4.2 10Chlorobenzene ND
0.86 101,1,1,2-Tetrachloroethane ND
1.9 10m,p-Xylene ND
0.66 5.0o-Xylene ND
Page 134 of 159Total Page Count: 159
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
406253
ug/Kg
08/15/11
NANA1108084
Soil
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.77 10Styrene ND
1.9 10Bromoform ND
1.2 10Isopropyl Benzene ND
1.4 10n-Propylbenzene ND
1.2 10Bromobenzene ND
3.0 101,1,2,2-Tetrachloroethane ND
1.1 101,3,5-Trimethylbenzene ND
3.3 101,2,3-Trichloropropane ND
1.6 104-Chlorotoluene ND
1.6 102-Chlorotoluene ND
1.4 10tert-Butylbenzene ND
1.1 101,2,4-Trimethylbenzene ND
1.6 10sec-Butyl Benzene ND
1.5 10p-Isopropyltoluene ND
1.8 101,3-Dichlorobenzene ND
1.5 101,4-Dichlorobenzene ND
2.2 10n-Butylbenzene ND
1.3 101,2-Dichlorobenzene ND
4.2 101,2-Dibromo-3-Chloropropane ND
2.6 10Hexachlorobutadiene ND
2.1 101,2,4-Trichlorobenzene ND
2.8 10Naphthalene ND
2.9 101,2,3-Trichlorobenzene ND
(S) Dibromofluoromethane 92.9
(S) Toluene-d8 86.1
(S) 4-Bromofluorobenzene 97.2
Page 135 of 159Total Page Count: 159
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
406300
ug/L
08/16/11
NANA1108084
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.41 0.50Dichlorodifluoromethane ND
0.41 0.50Chloromethane ND
0.37 0.50Vinyl Chloride ND
0.37 0.50Bromomethane ND
0.34 0.50Trichlorofluoromethane ND
0.29 0.501,1-Dichloroethene ND
0.38 0.50Freon 113 ND
0.18 5.0Methylene Chloride 0.22
0.31 0.50trans-1,2-Dichloroethene ND
0.38 0.50MTBE ND
1.5 5.0tert-Butanol ND
0.36 0.50Diisopropyl ether (DIPE) ND
0.28 0.501,1-Dichloroethane ND
0.40 0.50ETBE ND
0.33 0.50cis-1,2-Dichloroethene ND
0.37 0.502,2-Dichloropropane ND
0.34 0.50Bromochloromethane ND
0.29 0.50Chloroform ND
0.26 0.50Carbon Tetrachloride ND
0.32 0.501,1,1-Trichloroethane ND
0.40 0.501,1-Dichloropropene ND
0.33 0.50Benzene ND
0.32 0.50TAME ND
0.28 0.501,2-Dichloroethane ND
0.38 0.50Trichloroethylene ND
0.21 0.50Dibromomethane ND
0.37 0.501,2-Dichloropropane ND
0.23 0.50Bromodichloromethane ND
0.30 0.50cis-1,3-Dichloropropene ND
0.19 0.50Toluene ND
0.15 0.50Tetrachloroethylene ND
0.20 0.50trans-1,3-Dichloropropene ND
0.20 0.501,1,2-Trichloroethane ND
0.21 0.50Dibromochloromethane ND
0.18 0.501,3-Dichloropropane ND
0.19 0.501,2-Dibromoethane ND
0.14 0.50Chlorobenzene ND
0.15 0.50Ethyl Benzene ND
0.10 0.501,1,1,2-Tetrachloroethane ND
0.20 1.0m,p-Xylene ND
0.13 0.50o-Xylene ND
Page 136 of 159Total Page Count: 159
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
406300
ug/L
08/16/11
NANA1108084
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.20 0.50Styrene ND
0.45 1.0Bromoform ND
0.28 0.50Isopropyl Benzene ND
0.39 0.50Bromobenzene ND
0.26 0.501,1,2,2-Tetrachloroethane ND
0.30 0.50n-Propylbenzene ND
0.33 0.502-Chlorotoluene ND
0.20 0.501,3,5-Trimethylbenzene ND
0.32 0.504-Chlorotoluene ND
0.29 0.50tert-Butylbenzene ND
0.59 1.01,2,3-Trichloropropane ND
0.33 0.501,2,4-Trimethylbenzene ND
0.24 0.50sec-Butyl Benzene ND
0.25 0.50p-Isopropyltoluene ND
0.31 0.501,3-Dichlorobenzene ND
0.37 0.501,4-Dichlorobenzene ND
0.32 0.50n-Butylbenzene ND
0.39 0.501,2-Dichlorobenzene ND
0.45 1.01,2-Dibromo-3-Chloropropane ND
0.22 0.50Hexachlorobutadiene ND
0.48 1.01,2,4-Trichlorobenzene ND
0.57 1.0Naphthalene ND
0.52 1.01,2,3-Trichlorobenzene ND
100 100Ethanol ND TIC
(S) Dibromofluoromethane 91.0
(S) Toluene-d8 92.1
(S) 4-Bromofluorobenzene 89.8
Page 137 of 159Total Page Count: 159
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW7470AAnalytical Method:
Prep Date:
Analyzed Date:
08/12/11 Prep Batch:
Analytical Batch:
40623808/15/11
mg/L
7470A 3365
Water
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.0002 0.0150.00005 0.188 2080 - 120Mercury 106 1060.00007
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/12/11 Prep Batch:
Analytical Batch:
40624208/15/11
mg/Kg
3005 3377
Water
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.009 10.004 0.269 2080 - 120Antimony (Dissolved) 91.2 91.1ND
0.009 10.005 0.293 2080 - 120Arsenic (Dissolved) 94.3 94.2ND
0.009 10.002 0.411 2080 - 120Barium (Dissolved) 96.7 96.6ND
0.005 10.002 3.12 2080 - 120Beryllium (Dissolved) 97.9 95.0ND
0.005 10.001 0.221 2080 - 120Cadmium (Dissolved) 97.3 97.2ND
0.005 10.002 0.0737 2080 - 120Chromium (Dissolved) 96.6 97.1ND
0.005 10.002 0.711 2080 - 120Cobalt (Dissolved) 98.3 97.3ND
0.009 10.003 0.295 2080 - 120Copper (Dissolved) 97.2 96.70.00357
0.014 10.005 0.0753 2080 - 120Lead (Dissolved) 95.2 94.9ND
0.009 10.002 0.169 2080 - 120Molybdenum (Dissolved) 97.5 96.8ND
0.009 10.002 0.334 2080 - 120Nickel (Dissolved) 97.6 97.7ND
0.02 10.004 1.45 2080 - 120Selenium (Dissolved) 95.5 94.6ND
0.005 10.002 0.582 2080 - 120Silver (Dissolved) 94.7 94.4ND
0.009 10.004 0.0323 2080 - 120Thallium (dissolved) 95.4 95.0ND
0.009 10.004 0.169 2080 - 120Vanadium (Dissolved) 96.7 96.8ND
0.009 10.002 1.28 2080 - 120Zinc (dissolved) 99.1 97.8ND
Page 138 of 159Total Page Count: 159
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW8270CAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
40631608/16/11
mg/Kg
3545_BNA 3385
Soil
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.33 1.6670.129 20.3 3016 - 98.6Phenol 40.3 49.5ND
0.33 1.6670.129 19.2 3012.9 - 91.32-Chlorophenol 36.9 44.8ND
0.33 0.8330.0663 19.6 3021.9 - 79.81,4-Dichlorobenzene 40.9 49.8ND
0.33 1.6670.0931 20.9 3015.5 - 116N-nitroso-di-n-propylamine 41.3 50.8ND
0.33 0.8330.0733 25.7 3031.7 - 85.11,2,4-Trichlorobenzene 35.7 46.3ND
0.33 1.6670.102 17.8 3023.8 - 1164-Chloro-3-methylphenol 32.7 39.0ND
0.33 0.8330.0964 21.8 3029.1 - 94.8Acenaphthene 38.1 47.3ND
0.33 1.6670.0663 7.93 3010.4 - 1314-Nitrophenol 56.0 60.9ND
0.33 0.8330.0267 20.4 3030.8 - 1242,4-Dinitrotoluene 48.9 60.0ND
0.33 1.6670.102 13.8 3019.9 - 133Pentachlorophenol 50.9 58.7ND
0.33 0.8330.147 16.8 3034.2 - 127Pyrene 59.5 70.5ND
50 24 - 113Phenol-d6 (S) 54.0 64.1ND
50 25 - 1212-Fluorophenol (S) 40.6 50.0ND
50 19 - 1222,4,6-Tribromophenol (S) 48.3 57.3ND
25 23 - 120Nitrobenzene-d5 (S) 44.5 53.2ND
25 30 - 1152-Fluorobiphenyl (S) 42.2 53.5ND
25 18 - 137p-Terphenyl-d14 (S) 47.4 53.4ND
Page 139 of 159Total Page Count: 159
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
40626708/16/11
mg/Kg
3050 3389
Soil
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
5.0 500.20 1.07 3030.7 - 130Antimony 96.1 95.10.35
1.7 500.28 3.03 3071 - 121Arsenic 96.8 93.90.28
5.0 501 2.35 3070.2 - 130Barium 102 99.61.1
2.0 500.0840 1.35 3073.3 - 115Beryllium 95.1 96.3ND
1.0 500.059 2.07 3068.7 - 110Cadmium 98.4 96.4ND
5.0 500.059 1.63 3076 - 116Chromium 99.5 97.90.33
5.0 500.14 2.36 3057.4 - 122Cobalt 101 98.6ND
5.0 500.090 2.14 3074.8 - 119Copper 104 1020.18
1.0 500.13 0.784 3067.9 - 118Lead 97.3 96.50.34
5.0 500.059 0.936 3062.9 - 123Molybdenum 98.7 97.80.12
5.0 500.059 2.15 3061.5 - 122Nickel 100 97.90.15
5.0 500.29 4.36 3062 - 111Selenium 93.7 89.7ND
1.0 501.0 2.22 3081.1 - 109Silver 96.7 94.6ND
5.0 500.12 0.226 3039.2 - 125Thallium 93.2 93.0ND
5.0 500.12 1.89 3065.8 - 122Vanadium 101 99.10.14
5.0 500.59 3.08 3059.9 - 122Zinc 122 1180.88
Work Order:
Matrix:
Units:
Prep Method:
7471BAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
40627008/16/11
mg/Kg
7471 3393
Soil
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.10 1.250.01 6.58 3080.5 - 133Mercury 109 116ND
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
40632108/17/11
mg/L
3510_TPHSG 3402
Water
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.10 10.0440 2.00 3034.5 - 95.6TPH as Diesel (SG) 51.6 52.7ND
100 57.9 - 125Pentacosane (S) 79.6 73.0ND
Page 140 of 159Total Page Count: 159
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
40628808/17/11
mg/Kg
3050 3405
Soil
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
5 500.2 1.79 3030.7 - 130Antimony 97.13 98.90.30
1.7 500.28 1.66 3071 - 121Arsenic 96.33 97.9ND
5 501.1 4.59 3070.2 - 130Barium 103.4 98.41.1
2 500.084 3.66 3073.3 - 115Beryllium 98.33 94.8ND
1 500.059 5.40 3068.7 - 110Cadmium 99.51 94.3ND
5 500.059 4.69 3076 - 116Chromium 104.2 99.20.35
5 500.14 5.72 3057.4 - 122Cobalt 101.8 96.3ND
5 500.09 4.58 3074.8 - 119Copper 104.2 99.30.25
1 500.13 0.996 3067.9 - 118Lead 97.89 98.90.25
5 500.059 1.51 3062.9 - 123Molybdenum 98.92 1000.060
5 500.059 5.44 3061.5 - 122Nickel 101.7 96.60.12
5 500.29 2.56 3062 - 111Selenium 91.96 94.4ND
1 501 4.38 3081.1 - 109Silver 98.56 94.4ND
5 500.12 1.50 3039.2 - 125Thallium 92.93 94.3ND
5 500.12 5.40 3065.8 - 122Vanadium 103.9 98.50.12
5 500.59 5.37 3059.9 - 122Zinc 100 94.80.85
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
40630008/16/11
ug/L
5030 3414
Water
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
50 227.2722 21.5 3052.4 - 127TPH(Gasoline) 114 92.1ND
11.36 58.4 - 133(S) 4-Bromofluorobenzene 98.8 91.890.2
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/15/11 Prep Batch:
Analytical Batch:
40625308/15/11
ug/Kg
5035 3417
Soil
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
100 100017 2.25 3048.2 - 132TPH(Gasoline) 91.4 93.5ND
50 57 - 127(S) 4-Bromofluorobenzene 89.7 92.8101
Page 141 of 159Total Page Count: 159
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/18/11 Prep Batch:
Analytical Batch:
40632508/18/11
mg/Kg
3545_TPH 3418
Soil
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
2 33.330.758 0.871 3052.7 - 115TPH as Diesel 87.1 87.81.2
100 59.7 - 129Pentacosane (S) 96.8 98.13.3
Work Order:
Matrix:
Units:
Prep Method:
SW8082Analytical Method:
Prep Date:
Analyzed Date:
08/18/11 Prep Batch:
Analytical Batch:
40632608/18/11
mg/Kg
3545_PCB 3419
Soil
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.10 10.0230 4.27 3055.6 - 135Aroclor1016 92.7 88.8ND
0.10 0.50.0270 4.66 3065.6 - 132Aroclor1260 89.6 85.5ND
0.25 68.9 - 123TCMX (S) 91.7 83.8ND
0.250 69.5 - 119DCBP (S) 107 98.6ND
Work Order:
Matrix:
Units:
Prep Method:
SW8081AAnalytical Method:
Prep Date:
Analyzed Date:
08/18/11 Prep Batch:
Analytical Batch:
40633308/18/11
ug/Kg
3545_OCP 3420
Soil
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
2.0 200.40 9.23 3056.9 - 120gamma-BHC 74.9 68.3ND
2.0 201.1 10.9 3063.6 - 117Heptachlor 76.4 68.5ND
2.0 200.44 0.805 3053 - 123Aldrin 78.4 79.1ND
2.0 200.43 8.92 3044 - 130Dieldrin 76.7 70.2ND
2.0 200.57 12.2 3044.1 - 121Endrin 75.3 66.6ND
2.0 200.81 10.4 3052.8 - 1344,4'-DDT 81.3 73.3ND
350 52.5 - 139TCMX (S) 76.3 70.7ND
350 50.2 - 139DCBP (S) 75.7 68.4ND
Page 142 of 159Total Page Count: 159
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/24/11 Prep Batch:
Analytical Batch:
40641008/24/11
mg/Kg
3050 3479
Soil
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
5.0 500.20 0.719 3030.7 - 130Antimony 98.4 99.1ND
1.7 500.28 0.802 3071 - 121Arsenic 99.3 100ND
5.0 501 0.939 3070.2 - 130Barium 106 1071.8
2.0 500.0840 3.41 3073.3 - 115Beryllium 101 97.6ND
1.0 500.059 1.60 3068.7 - 110Cadmium 99.2 101ND
5.0 500.059 1.61 3076 - 116Chromium 105 1070.14
5.0 500.14 1.92 3057.4 - 122Cobalt 103 105ND
5.0 500.090 1.03 3074.8 - 119Copper 106 1070.96
1.0 500.13 0.695 3067.9 - 118Lead 101 1000.25
5.0 500.059 2.26 3062.9 - 123Molybdenum 105 1070.17
5.0 500.059 2.93 3061.5 - 122Nickel 101 1040.095
5.0 500.29 0.118 3062 - 111Selenium 93.3 93.2ND
1.0 501.0 0.587 3081.1 - 109Silver 102 103ND
5.0 500.12 3.75 3039.2 - 125Thallium 94.1 97.70.60
5.0 500.12 1.04 3065.8 - 122Vanadium 105 106ND
5.0 500.59 0.292 3059.9 - 122Zinc 103 1031.2
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/24/11 Prep Batch:
Analytical Batch:
40642108/25/11
mg/L
1311/3010B 3489
Soil
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.10 100.0500 0.343 2080 - 120Lead (TCLP) 99.4 99.1ND
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/25/11 Prep Batch:
Analytical Batch:
40644808/25/11
mg/Kg
3545_TPH 3494
Soil
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
2 33.330.758 2.84 3052.7 - 125TPH as Diesel 85.8 83.41.7
100 59.7 - 129Pentacosane (S) 127 1262.8
Page 143 of 159Total Page Count: 159
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/25/11 Prep Batch:
Analytical Batch:
40644708/26/11
mg/L
WET/3010B 3496
Soil
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.10 100.0500 2.49 2080 - 120Lead (STLC) 87.0 89.2ND
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
40625308/15/11
ug/Kg
NA NA
Soil
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
10 501.5 6.56 3053.7 - 1391,1-Dichloroethene 81.6 76.4ND
10 501.5 0.170 3066.5 - 135Benzene 82.5 82.5ND
10 503.9 5.87 3057.5 - 150Trichloroethylene 89.3 84.3ND
10 500.98 0.730 3056.8 - 134Toluene 88.1 87.4ND
10 504.2 9.79 3057.4 - 134Chlorobenzene 87.2 79.1ND
50 59.8 - 148(S) Dibromofluoromethane 76.3 84.1ND
50 55.2 - 133(S) Toluene-d8 87.9 87.4ND
50 55.8 - 141(S) 4-Bromofluorobenzene 87.3 95.4ND
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
40630008/16/11
ug/L
NA NA
Water
1108084
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.50 17.040.29 14.7 3061.4 - 1291,1-Dichloroethene 87.0 101ND
0.50 17.040.33 8.61 3066.9 - 140Benzene 93.2 102ND
0.50 17.040.38 8.38 3069.3 - 144Trichloroethylene 99.4 108ND
0.50 17.040.19 8.26 3076.6 - 123Toluene 95.3 103ND
0.50 17.040.14 8.04 3073.9 - 137Chlorobenzene 97.0 105ND
11.36 61.2 - 131(S) Dibromofluoromethane 88.9 103ND
11.36 75.1 - 127(S) Toluene-d8 92.0 104ND
11.36 64.1 - 120(S) 4-Bromofluorobenzene 89.2 99.10.22
Page 144 of 159Total Page Count: 159
MS/MSD Summary ReportRaw values are used in quality control assessment.
Work Order: 1108084
Analyzed Date:
Prep Date:
Matrix:
Prep Method: NA
1108084-002ASpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW8260B 40625308/15/11
ug/Kg
NANA
Soil
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
50 53.7 - 1391.5 10 1.47 301,1-Dichloroethene 92.0 90.60
50 66.5 - 1351.5 10 0.523 30Benzene 91.5 92.00
50 57.5 - 1503.9 10 1.26 30Trichloroethylene 88.1 89.20
50 56.8 - 1340.98 10 5.59 30Toluene 91.2 96.40
50 57.4 - 1344.2 10 5.90 30Chlorobenzene 94.1 99.80
50 59.8 - 148(S) Dibromofluoromethane 84.2 91.9
50 55.2 - 133(S) Toluene-d8 86.2 87.8
50 55.8 - 141(S) 4-Bromofluorobenzene 94.0 102
Work Order: 1108084
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/15/11
1108084-001ASpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW6010B 40626708/16/11
mg/Kg
33893050
Soil
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
50 30.7 - 1300.20 5.0 2.94 30Antimony 92.0 89.30.00
50 71 - 1210.28 1.7 2.37 30Arsenic 92.7 90.40.048
50 70.2 - 1301 5.0 3.47 30Barium 108 1161.3
50 73.3 - 1150.0840 2.0 1.06 30Beryllium 94.1 93.10.00
50 68.7 - 1100.059 1.0 0.659 30Cadmium 92.9 92.30.00
50 76 - 1160.059 5.0 1.94 30Chromium 96.7 1000.61
50 57.4 - 1220.14 5.0 6.75 30Cobalt 98.7 1060.00
50 74.8 - 1190.090 5.0 6.54 30Copper 98.3 1060.13
50 67.9 - 1180.13 1.0 25.4 30Lead 115 73.50.69
50 62.9 - 1230.059 5.0 2.15 30Molybdenum 92.3 90.30.00
50 61.5 - 1220.059 5.0 0.310 30Nickel 91.1 91.40.38
50 62 - 1110.29 5.0 0.560 30Selenium 89.5 89.00.00
50 81.1 - 1091.0 1.0 5.99 30Silver 92.4 98.10.00
50 39.2 - 1250.12 5.0 2.64 30Thallium 83.6 81.40.00
50 65.8 - 1220.12 5.0 8.74 30Vanadium 91.7 1050.47
50 59.9 - 1220.59 5.0 4.06 30Zinc 96.7 90.40.69
Page 145 of 159Total Page Count: 159
MS/MSD Summary ReportRaw values are used in quality control assessment.
Work Order: 1108084
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/15/11
1108084-001ASpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
7471B 40627008/16/11
mg/Kg
33937471
Soil
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
1.25 60 - 1400.01 0.10 8.29 30Mercury 114 1050.00057
Work Order: 1108084
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/16/11
1108084-008ASpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW6010B 40628808/17/11
mg/Kg
34053050
Soil
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
50 30.7 - 1300.20 5.0 4.24 30Antimony 88.6 84.90.00
50 71 - 1210.28 1.7 3.04 30Arsenic 93.9 90.80.13
50 70.2 - 1301 5.0 3.08 30Barium 81.2 95.43.8
50 73.3 - 1150.0840 2.0 4.92 30Beryllium 98.2 93.50.00
50 68.7 - 1100.059 1.0 2.04 30Cadmium 98.1 96.10.00
50 76 - 1160.059 5.0 2.93 30Chromium 92.9 89.10.42
50 57.4 - 1220.14 5.0 13.5 30Cobalt 104 87.80.24
50 74.8 - 1190.090 S5.0 23.1 30Copper 155 1070.79
50 67.9 - 1180.13 S1.0 0.000 30Lead 3.80 4.002.6
50 62.9 - 1230.059 5.0 0.771 30Molybdenum 91.2 90.50.00
50 61.5 - 1220.059 5.0 6.72 30Nickel 98.7 89.90.41
50 62 - 1110.29 5.0 0.815 30Selenium 92.4 91.70.00
50 81.1 - 1091.0 1.0 3.10 30Silver 94.3 97.30.00
50 39.2 - 1250.12 5.0 0.185 30Thallium 81.2 81.40.00
50 65.8 - 1220.12 5.0 2.30 30Vanadium 105 1010.75
50 59.9 - 1220.59 5.0 2.96 30Zinc 82.9 93.32.6
Work Order: 1108084
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/24/11
1108084-008ASpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW6010B 40642108/25/11
mg/L
34891311/3010B
Soil
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
10 75 - 1250.0500 0.10 0.964 20Lead (TCLP) 93.9 94.80.000
Page 146 of 159Total Page Count: 159
MS/MSD Summary ReportRaw values are used in quality control assessment.
Work Order: 1108084
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/25/11
1108084-009ASpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW8015B(M) 40644808/25/11
mg/Kg
34943545_TPH
Soil
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
33.33 50.3 - 1250.76 2.0 1.78 30TPH as Diesel 78.4 79.828.2966
100 57.9 - 125Pentacosane (S) 116 121
Page 147 of 159Total Page Count: 159
Laboratory Qualifiers and Definitions
Method Detection Limit (MDL) - the minimum concentration of a substance that can be measured and reported with a 99% confidence that the analyte concentration is greater than zero
Matrix Spike (MS/MSD) - Client sample spiked with identical concentrations of target analyte (s). The spiking occurs prior to the sample preparation and analysis. They are used to document the precision and bias of a method in a given sample matrix.
Matrix - the component or substrate that contains the analyte of interest (e.g., - groundwater, sediment, soil, waste water, etc)
Laboratory Control Sample (LCS ad LCSD) - A known matrix spiked with compounds representative of the target analyte(s). This is used to document laboratory performance.
Duplicate - a field sample and/or laboratory QC sample prepared in duplicate following all of the same processes and procedures used on the original sample (sample duplicate, LCSD, MSD)
Blank (Method/Preparation Blank) -MB/PB - An analyte-free matrix to which all reagents are added in the same volumes/proportions as used in sample processing. The method blank is used to document contamination resulting from the analytical process.
Practical Quantitation Limit (PQL) - a laboratory determined value at 2 to 5 times above the MDL that can be reproduced in a manner that results in a 99% confidence level that the result is both accurate and precise. PQLs reflect all preparation factors and/or dilution factors that have been applied to the sample during the preparation and/or analytical processes.
Precision (%RPD) - The agreement among a set of replicate/duplicate measurements without regard to known value of the replicates
Surrogate (S) or (Surr) - An organic compound which is similar to the target analyte(s) in chemical composition and behavior in the analytical process, but which is not normally found in environmental samples. Surrogates are used in most organic analysis to demonstrate matrix compatibility with the chosen method of analysis
Tentatively Identified Compound (TIC) - A compound not contained within the analytical calibration standards but present in the GCMS library of defined compounds. When the library is searched for an unknown compound, it can frequently give a tentative identification to the compound based on retention time and primary and secondary ion match. TICs are reported as estimates and are candidates for further investigation.
Units: the unit of measure used to express the reported result - mg/L and mg/Kg (equivalent to PPM - parts per million in liquid and solid), ug/L and ug/Kg (equivalent to PPB - parts per billion in liquid and solid), ug/m3, mg.m3, ppbv and ppmv (all units of measure for reporting concentrations in air), % ( equivalent to 10000 ppm or 1,000,000 ppb), ug/Wipe ( concentration found on the surface of a single Wipe usually taken over a 100cm2 surface)
B - Indicates when the anlayte is found in the associated method or preparation blank D - Surrogate is not recoverable due to the necessary dilution of the sampleE - Indicates the reportable value is outside of the calibration range of the instrument but within the linear range of the instrument (unless otherwise noted) Values reported with an E qualifier should be considered as estimated.H- Indicates that the recommended holding time for the analyte or compound has been exceededJ- Indicates a value between the method MDL and PQL and that the reported concentration should be considered as estimated rather the quantitative NA - Not AnalyzedN/A - Not ApplicableNR - Not recoverable - a matrix spike concentration is not recoverable due to a concentration within the original sample that is greater than four times the spike concentration addedR- The % RPD between a duplicate set of samples is outside of the absolute values established by laboratory control chartsS- Spike recovery is outside of established method and/or laboratory control limits. Further explanation of the use of this qualifier should be included within a case narrative
X -Used to indicate that a value based on pattern identification is within the pattern range but not typical of the pattern found in standards. Further explanation may or may not be provided within the sample footnote and/or the case narrative.
DEFINITIONS:
Accuracy/Bias (% Recovery) - The closeness of agreement between an observed value and an accepted reference value.
LABORATORY QUALIFIERS:
Page 148 of 159Total Page Count: 159
pH Adjusted by: pH Checked by:
°C5
Yes
Yes
Yes
Temperature:
Water-pH acceptable upon receipt?
Water-VOA vials have zero headspace?
Container/Temp Blank temperature in compliance?
All samples received within holding time?
Sample Preservation and Hold Time (HT) Information
YesSamples containers intact?
Yes
Yes
Not Present
Yes
Sufficient sample volume for indicated test?
Samples in proper container/bottle?
Custody seals intact on shipping container/cooler?
Shipping Container/Cooler In Good Condition?
Sample Receipt Information
Yes
Yes
Yes
Not Present
Chain of custody agrees with sample labels?
Chain of custody signed when relinquished and received?
Chain of custody present?
Custody seals intact on sample bottles?
Chain of Custody (COC) Information
Checklist Completed By: NG
Carrier Name: First Courier
Physically Logged By: NG
Received By: NK
Date and Time Received: 8/23/2011 16:35
Work Order No.: 1108084
Project Name: 500 Kirkham
Client Name: Northgate Environmental Management Inc.
Sample Receipt Checklist
Page 149 of 159Total Page Count: 159
Login Summary Report
Report Due Date:
5 Day TAT!! Received 20 soils and 5 waters @ 5'C. Dissolved metals analysis for Waters samples. SG clean up on all waters.Sample 004 amd 010 for Lead STLC. Sample 008 for STLC and TCLP Lead. Sample 009 and 006 off Hold, added total Lead on both and TPH-oil. Added per client on 08/23/2011. 3 day RUSH TAT Due 08/26/2011.
16:35
8/23/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/26/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
3 day:25
1108084Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
B-4-1.01108084-001A Soil 02/07/1208/11/11 8:15S_6010BCAM17S_7471BHGEn_8260FullS_8081AOCPS_8082PCBS_TPHDOS_8270FullS_GCMS-GRO
Sample Note: Pretarred voas for 8260, TPHg. Use for MS/MSD.
B-4-5.01108084-002A Soil 02/07/1208/11/11 8:20S_6010BCAM17S_TPHDOS_8082PCBS_8270FullEn_8260FullS_GCMS-GROS_7471BHG
B-4-101108084-003A Soil 02/07/12 On-Hold08/11/11 8:25Hold Samples
Sample Note:
B-8-1.01108084-004A Soil 02/07/1208/11/11 8:55S_6010B(STLC)S_7471BHGS_GCMS-GROS_TPHDOS_8270FullS_8082PCBS_8081AOCPEn_8260FullS_6010BCAM17
Sample Note: Sample 004 amd 010 for Lead STLC. Sample 008 for STLC and TCLP Lead. Sample 009 and 006 off Hold, added total Lead on both. Added per client on 08/23/2011. 3 day RUSH TAT Due 08/26/2011
Page 150 of 159Total Page Count: 159
Login Summary Report
Report Due Date:
5 Day TAT!! Received 20 soils and 5 waters @ 5'C. Dissolved metals analysis for Waters samples. SG clean up on all waters.Sample 004 amd 010 for Lead STLC. Sample 008 for STLC and TCLP Lead. Sample 009 and 006 off Hold, added total Lead on both and TPH-oil. Added per client on 08/23/2011. 3 day RUSH TAT Due 08/26/2011.
16:35
8/23/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/26/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
3 day:25
1108084Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
B-8-5.01108084-005A Soil 02/07/1208/11/11 9:00S_6010BCAM17S_8270FullS_8082PCBS_TPHDOEn_8260FullS_GCMS-GROS_7471BHG
B-8-8.01108084-006A Soil 02/07/1208/11/11 9:05S_6010BCAM17S_TPHDO
Sample Note: Sample 004 amd 010 for Lead STLC. Sample 008 for STLC and TCLP Lead. Sample 009 and 006 off Hold, added total Lead on both and TPH-oil(watch the hloding time). Added per client on 08/23/2011. 3 day RUSH TAT Due 08/26/2011.B-2-1.01108084-007A Soil 02/07/1208/11/11 9:15
S_6010BCAM17En_8260FullS_GCMS-GROS_7471BHGS_TPHDOS_8270FullS_8082PCBS_8081AOCP
B-2-5.01108084-008A Soil 02/07/1208/11/11 9:20S_6010B(STLC)S_7471BHGS_6010B(TCLP)S_6010BCAM17S_8270FullS_8082PCBS_TPHDOEn_8260FullS_GCMS-GRO
B-2-9.01108084-009A Soil 02/07/1208/11/11 9:25S_6010BCAM17
Page 151 of 159Total Page Count: 159
Login Summary Report
Report Due Date:
5 Day TAT!! Received 20 soils and 5 waters @ 5'C. Dissolved metals analysis for Waters samples. SG clean up on all waters.Sample 004 amd 010 for Lead STLC. Sample 008 for STLC and TCLP Lead. Sample 009 and 006 off Hold, added total Lead on both and TPH-oil. Added per client on 08/23/2011. 3 day RUSH TAT Due 08/26/2011.
16:35
8/23/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/26/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
3 day:25
1108084Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
S_TPHDOB-7-1.01108084-010A Soil 02/07/1208/11/11 10:30
S_6010B(STLC)S_7471BHGS_GCMS-GROS_6010BCAM17En_8260FullS_8270FullS_8082PCBS_TPHDOS_8081AOCP
B-7-5.01108084-011A Soil 02/07/1208/11/11 10:35S_7471BHGS_TPHDOS_8082PCBS_8270FullS_6010BCAM17En_8260FullS_GCMS-GRO
B-7-7.01108084-012A Soil 02/07/1208/11/11 10:40Hold Samples
B-6-1.01108084-013A Soil 02/07/1208/11/11 10:55S_7471BHGS_8082PCBS_TPHDOS_8270FullS_8081AOCPS_6010BCAM17S_GCMS-GROEn_8260Full
B-6-5.01108084-014A Soil 02/07/1208/11/11 11:00S_7471BHGEn_8260FullS_8270Full
Page 152 of 159Total Page Count: 159
Login Summary Report
Report Due Date:
5 Day TAT!! Received 20 soils and 5 waters @ 5'C. Dissolved metals analysis for Waters samples. SG clean up on all waters.Sample 004 amd 010 for Lead STLC. Sample 008 for STLC and TCLP Lead. Sample 009 and 006 off Hold, added total Lead on both and TPH-oil. Added per client on 08/23/2011. 3 day RUSH TAT Due 08/26/2011.
16:35
8/23/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/26/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
3 day:25
1108084Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
S_TPHDOS_8082PCBS_6010BCAM17S_GCMS-GRO
B-6-9.01108084-015A Soil 02/07/1208/11/11 11:05Hold Samples
B-16-1.01108084-016A Soil 02/07/1208/11/11 12:05S_7471BHGS_6010BCAM17En_8260FullS_8082PCBS_8270FullS_TPHDOS_8081AOCPS_GCMS-GRO
B-16-5.01108084-017A Soil 02/07/1208/11/11 12:10S_7471BHGS_8270FullS_8082PCBS_TPHDOEn_8260FullS_GCMS-GROS_6010BCAM17
B-16-10.01108084-018A Soil 02/07/1208/11/11 12:15Hold Samples
B-7-1.0D1108084-019A Soil 02/07/1208/11/11 10:30S_GCMS-GROEn_8260FullS_TPHDO
B-4-GW1108084-020A Water 09/25/1108/11/11 9:20W_GCMS-GROW_8260Full
Sample Note:
B-4-GW1108084-020B Water 09/25/1108/11/11 9:20
Page 153 of 159Total Page Count: 159
Login Summary Report
Report Due Date:
5 Day TAT!! Received 20 soils and 5 waters @ 5'C. Dissolved metals analysis for Waters samples. SG clean up on all waters.Sample 004 amd 010 for Lead STLC. Sample 008 for STLC and TCLP Lead. Sample 009 and 006 off Hold, added total Lead on both and TPH-oil. Added per client on 08/23/2011. 3 day RUSH TAT Due 08/26/2011.
16:35
8/23/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/26/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
3 day:25
1108084Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
W_TPHDOSGB-4-GW1108084-020C Water 09/25/1108/11/11 9:20
W_D6010BCAM17W_D7470AHG
Sample Note: Dissolved metals analysis for all waters samples. SG clean up on all waters.
B-8-GW1108084-021A Water 09/25/1108/11/11 9:20W_GCMS-GROW_8260Full
B-8-GW1108084-021B Water 09/25/1108/11/11 9:20W_TPHDOSG
Sample Note: Dissolved metals analysis for all waters samples. SG clean up on all waters.
B-8-GW1108084-021C Water 09/25/1108/11/11 9:20W_D6010BCAM17W_D7470AHG
B-16-GW1108084-022A Water 09/25/1108/11/11 12:30W_GCMS-GROW_8260Full
B-16-GW1108084-022B Water 09/25/1108/11/11 12:30W_TPHDOSG
B-16-GW1108084-022C Water 09/25/1108/11/11 12:30W_D6010BCAM17W_D7470AHG
FB1108084-023A Water 09/25/1108/11/11 13:00W_8260Full
IDW1108084-024A Soil 09/25/1108/11/11 13:15S_7471BHGS_TPHDOS_8081AOCPS_GCMS-GROS_6010BCAM17
EQUIP BLANK1108084-025A Water 09/25/1108/11/11 13:22W_D6010BCAM17W_D7470AHG
Page 154 of 159Total Page Count: 159
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Northgate Environmental Management Inc.300 Frank H. Ogawa Plaza, Suite 510Oakland, California 94612Tel: 5108390688Fax: (510) 839-4350
RE: 500 Kirkham
Torrent Laboratory, Inc. received 7 sample(s) on August 15, 2011 for the analyses presented in the following Report.
Dear Dennis Laduzinsky:
Work Order No.: 1108103
All data for associated QC met EPA or laboratory specification(s) except where noted in the case narrative.
Torrent Laboratory, Inc. is certified by the State of California, ELAP #1991. If you have any questions regarding these test results, please feel free to contact the Project Management Team at (408)263-5258; ext 204.
Date
August 22, 2011
G.Gueorguieva
Sr. Project Manager
Page 1 of 48Total Page Count: 48
Date: 8/22/2011
Client: Northgate Environmental Management Inc.
Project: 500 Kirkham
Work Order: 1108103
CASE NARRATIVE
No issues encountered with the receiving, preparation, analysis or reporting of the results associated with this work order.
Analytical Comments for method W_D7470A, 1108103-002C MS/MSD, QC Analytical Batch ID 406291, Note:The % recoveries for Mercury are outside of laboratory control limits. The associated LCS/LCSD % recoveries and % RPD are within limits. No corrective action required.
Page 2 of 48Total Page Count: 48
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/15/11
Date Reported: 08/22/11
Sample Result Summary
1108103-001JA-2
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Barium (Dissolved) mg/L0.130.0090.002SW6010B 1
1108103-002JA-3
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Barium (Dissolved) mg/L0.0740.0090.002SW6010B 1
Nickel (Dissolved) mg/L0.0360.0090.002SW6010B 1
Page 3 of 48Total Page Count: 48
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/15/11
Date Reported: 08/22/11
Sample Result Summary
1108103-003JA-4
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Vinyl Chloride ug/L2.50.500.37SW8260B 1
1,1-Dichloroethene ug/L5.20.500.29SW8260B 1
trans-1,2-Dichloroethene ug/L2.60.500.31SW8260B 1
1,1-Dichloroethane ug/L460.500.28SW8260B 1
Chloroform ug/L0.530.500.29SW8260B 1
Benzene ug/L0.530.500.33SW8260B 1
Tetrachloroethylene ug/L360.500.15SW8260B 1
1,1,2-Trichloroethane ug/L0.910.500.20SW8260B 1
TPH(Gasoline) ug/L18050228260TPH 1
cis-1,2-Dichloroethene ug/L1602.21.4SW8260B 4.4
Trichloroethylene ug/L1402.21.7SW8260B 4.4
Barium (Dissolved) mg/L0.170.0090.002SW6010B 1
Chromium (Dissolved) mg/L0.00700.0050.002SW6010B 1
Cobalt (Dissolved) mg/L0.00800.0050.002SW6010B 1
Nickel (Dissolved) mg/L0.300.0090.002SW6010B 1
Page 4 of 48Total Page Count: 48
Report prepared for: Dennis Laduzinsky
Northgate Environmental Management Inc.
Date Received: 08/15/11
Date Reported: 08/22/11
Sample Result Summary
1108103-004JA-4D
Parameters: PQLMDL UnitResultsDFAnalysisMethod
Vinyl Chloride ug/L2.50.500.37SW8260B 1
1,1-Dichloroethene ug/L5.20.500.29SW8260B 1
trans-1,2-Dichloroethene ug/L2.70.500.31SW8260B 1
1,1-Dichloroethane ug/L450.500.28SW8260B 1
Tetrachloroethylene ug/L340.500.15SW8260B 1
1,1,2-Trichloroethane ug/L0.850.500.20SW8260B 1
TPH(Gasoline) ug/L19050228260TPH 1
cis-1,2-Dichloroethene ug/L1702.21.4SW8260B 4.4
Trichloroethylene ug/L1502.21.7SW8260B 4.4
Barium (Dissolved) mg/L0.160.0090.002SW6010B 1
Chromium (Dissolved) mg/L0.00670.0050.002SW6010B 1
Cobalt (Dissolved) mg/L0.00790.0050.002SW6010B 1
Nickel (Dissolved) mg/L0.290.0090.002SW6010B 1
1108103-005Equipment Blank
Parameters: PQLMDL UnitResultsDFAnalysisMethod
All compounds were non-detectable for this sample.
1108103-006TB080911 #4
Parameters: PQLMDL UnitResultsDFAnalysisMethod
All compounds were non-detectable for this sample.
1108103-007TB080911 #3
Parameters: PQLMDL UnitResultsDFAnalysisMethod
All compounds were non-detectable for this sample.
Page 5 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 11:15
1204.22
500 Kirkham
JA-2
WaterSample Matrix:
Lab Sample ID: 1108103-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406355ug/LNDDichlorodifluoromethane 08/19/11 0.41 0.50 NA1
SW8260B NA 406355ug/LNDChloromethane 08/19/11 0.41 0.50 NA1
SW8260B NA 406355ug/LNDVinyl Chloride 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromomethane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDTrichlorofluoromethane 08/19/11 0.34 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloroethene 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LNDFreon 113 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDMethylene Chloride 08/19/11 0.18 5.0 NA1
SW8260B NA 406355ug/LNDtrans-1,2-Dichloroethene 08/19/11 0.31 0.50 NA1
SW8260B NA 406355ug/LNDMTBE 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDtert-Butanol 08/19/11 1.5 5.0 NA1
SW8260B NA 406355ug/LNDDiisopropyl ether (DIPE) 08/19/11 0.36 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloroethane 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDETBE 08/19/11 0.40 0.50 NA1
SW8260B NA 406355ug/LNDcis-1,2-Dichloroethene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LND2,2-Dichloropropane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromochloromethane 08/19/11 0.34 0.50 NA1
SW8260B NA 406355ug/LNDChloroform 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LNDCarbon Tetrachloride 08/19/11 0.26 0.50 NA1
SW8260B NA 406355ug/LND1,1,1-Trichloroethane 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloropropene 08/19/11 0.40 0.50 NA1
SW8260B NA 406355ug/LNDBenzene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LNDTAME 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichloroethane 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDTrichloroethylene 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDDibromomethane 08/19/11 0.21 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichloropropane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromodichloromethane 08/19/11 0.23 0.50 NA1
SW8260B NA 406355ug/LNDcis-1,3-Dichloropropene 08/19/11 0.30 0.50 NA1
SW8260B NA 406355ug/LNDToluene 08/19/11 0.19 0.50 NA1
SW8260B NA 406355ug/LNDTetrachloroethylene 08/19/11 0.15 0.50 NA1
SW8260B NA 406355ug/LNDtrans-1,3-Dichloropropene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LND1,1,2-Trichloroethane 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LNDDibromochloromethane 08/19/11 0.21 0.50 NA1
SW8260B NA 406355ug/LND1,3-Dichloropropane 08/19/11 0.18 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dibromoethane 08/19/11 0.19 0.50 NA1
Page 6 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 11:15
1204.22
500 Kirkham
JA-2
WaterSample Matrix:
Lab Sample ID: 1108103-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406355ug/LNDChlorobenzene 08/19/11 0.14 0.50 NA1
SW8260B NA 406355ug/LNDEthyl Benzene 08/19/11 0.15 0.50 NA1
SW8260B NA 406355ug/LND1,1,1,2-Tetrachloroethane 08/19/11 0.10 0.50 NA1
SW8260B NA 406355ug/LNDm,p-Xylene 08/19/11 0.20 1.0 NA1
SW8260B NA 406355ug/LNDo-Xylene 08/19/11 0.13 0.50 NA1
SW8260B NA 406355ug/LNDStyrene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LNDBromoform 08/19/11 0.45 1.0 NA1
SW8260B NA 406355ug/LNDIsopropyl Benzene 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDBromobenzene 08/19/11 0.39 0.50 NA1
SW8260B NA 406355ug/LND1,1,2,2-Tetrachloroethane 08/19/11 0.26 0.50 NA1
SW8260B NA 406355ug/LNDn-Propylbenzene 08/19/11 0.30 0.50 NA1
SW8260B NA 406355ug/LND2-Chlorotoluene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LND1,3,5-Trimethylbenzene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LND4-Chlorotoluene 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LNDtert-Butylbenzene 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LND1,2,3-Trichloropropane 08/19/11 0.59 1.0 NA1
SW8260B NA 406355ug/LND1,2,4-Trimethylbenzene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LNDsec-Butyl Benzene 08/19/11 0.24 0.50 NA1
SW8260B NA 406355ug/LNDp-Isopropyltoluene 08/19/11 0.25 0.50 NA1
SW8260B NA 406355ug/LND1,3-Dichlorobenzene 08/19/11 0.31 0.50 NA1
SW8260B NA 406355ug/LND1,4-Dichlorobenzene 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDn-Butylbenzene 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichlorobenzene 08/19/11 0.39 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dibromo-3-Chloropropane 08/19/11 0.45 1.0 NA1
SW8260B NA 406355ug/LNDHexachlorobutadiene 08/19/11 0.22 0.50 NA1
SW8260B NA 406355ug/LND1,2,4-Trichlorobenzene 08/19/11 0.48 1.0 NA1
SW8260B NA 406355ug/LNDNaphthalene 08/19/11 0.57 1.0 NA1
SW8260B NA 406355ug/LND1,2,3-Trichlorobenzene 08/19/11 0.52 1.0 NA1
SW8260B NA 406355%103(S) Dibromofluoromethane 08/19/11 61.2 131 NA1
SW8260B NA 406355%92.4(S) Toluene-d8 08/19/11 75.1 127 NA1
SW8260B NA 406355%88.0(S) 4-Bromofluorobenzene 08/19/11 64.1 120 NA1
Page 7 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 11:15
1204.22
500 Kirkham
JA-2
WaterSample Matrix:
Lab Sample ID: 1108103-001A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/19/11 406355ug/LNDTPH(Gasoline) 08/19/11 22 50 34441
8260TPH 8/19/11 406355%83.4(S) 4-Bromofluorobenzene 08/19/11 34 114 34441
Page 8 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 11:15
1204.22
500 Kirkham
JA-2
WaterSample Matrix:
Lab Sample ID: 1108103-001B
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021
SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021
SW8015B(M) 8/16/11 406321%85.3Pentacosane (S) 08/17/11 57.9 125 34021
Page 9 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 11:15
1204.22
500 Kirkham
JA-2
WaterSample Matrix:
Lab Sample ID: 1108103-001C
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/16/11 406289mg/LNDAntimony (Dissolved) 08/18/11 0.004 0.009 34061
SW6010B 8/16/11 406289mg/LNDArsenic (Dissolved) 08/18/11 0.005 0.009 34061
SW6010B 8/16/11 406289mg/L0.13Barium (Dissolved) 08/18/11 0.002 0.009 34061
SW6010B 8/16/11 406289mg/LNDBeryllium (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/LNDCadmium (Dissolved) 08/18/11 0.001 0.005 34061
SW6010B 8/16/11 406289mg/LNDChromium (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/LNDCobalt (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/LNDCopper (Dissolved) 08/18/11 0.003 0.009 34061
SW6010B 8/16/11 406289mg/LNDLead (Dissolved) 08/18/11 0.005 0.014 34061
SW6010B 8/16/11 406289mg/LNDMolybdenum (Dissolved) 08/18/11 0.002 0.009 34061
SW6010B 8/16/11 406289mg/LNDNickel (Dissolved) 08/18/11 0.002 0.009 34061
SW6010B 8/16/11 406289mg/LNDSelenium (Dissolved) 08/18/11 0.004 0.02 34061
SW6010B 8/16/11 406289mg/LNDSilver (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/LNDThallium (dissolved) 08/18/11 0.004 0.009 34061
SW6010B 8/16/11 406289mg/LNDVanadium (Dissolved) 08/18/11 0.004 0.009 34061
SW6010B 8/16/11 406289mg/LNDZinc (dissolved) 08/18/11 0.002 0.009 34061
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7470A 8/16/11 406291mg/LNDMercury (Dissolved) 08/17/11 0.00005 0.0002 34091
Page 10 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 12:45
1204.22
500 Kirkham
JA-3
WaterSample Matrix:
Lab Sample ID: 1108103-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406355ug/LNDDichlorodifluoromethane 08/19/11 0.41 0.50 NA1
SW8260B NA 406355ug/LNDChloromethane 08/19/11 0.41 0.50 NA1
SW8260B NA 406355ug/LNDVinyl Chloride 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromomethane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDTrichlorofluoromethane 08/19/11 0.34 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloroethene 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LNDFreon 113 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDMethylene Chloride 08/19/11 0.18 5.0 NA1
SW8260B NA 406355ug/LNDtrans-1,2-Dichloroethene 08/19/11 0.31 0.50 NA1
SW8260B NA 406355ug/LNDMTBE 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDtert-Butanol 08/19/11 1.5 5.0 NA1
SW8260B NA 406355ug/LNDDiisopropyl ether (DIPE) 08/19/11 0.36 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloroethane 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDETBE 08/19/11 0.40 0.50 NA1
SW8260B NA 406355ug/LNDcis-1,2-Dichloroethene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LND2,2-Dichloropropane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromochloromethane 08/19/11 0.34 0.50 NA1
SW8260B NA 406355ug/LNDChloroform 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LNDCarbon Tetrachloride 08/19/11 0.26 0.50 NA1
SW8260B NA 406355ug/LND1,1,1-Trichloroethane 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloropropene 08/19/11 0.40 0.50 NA1
SW8260B NA 406355ug/LNDBenzene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LNDTAME 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichloroethane 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDTrichloroethylene 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDDibromomethane 08/19/11 0.21 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichloropropane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromodichloromethane 08/19/11 0.23 0.50 NA1
SW8260B NA 406355ug/LNDcis-1,3-Dichloropropene 08/19/11 0.30 0.50 NA1
SW8260B NA 406355ug/LNDToluene 08/19/11 0.19 0.50 NA1
SW8260B NA 406355ug/LNDTetrachloroethylene 08/19/11 0.15 0.50 NA1
SW8260B NA 406355ug/LNDtrans-1,3-Dichloropropene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LND1,1,2-Trichloroethane 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LNDDibromochloromethane 08/19/11 0.21 0.50 NA1
SW8260B NA 406355ug/LND1,3-Dichloropropane 08/19/11 0.18 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dibromoethane 08/19/11 0.19 0.50 NA1
Page 11 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 12:45
1204.22
500 Kirkham
JA-3
WaterSample Matrix:
Lab Sample ID: 1108103-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406355ug/LNDChlorobenzene 08/19/11 0.14 0.50 NA1
SW8260B NA 406355ug/LNDEthyl Benzene 08/19/11 0.15 0.50 NA1
SW8260B NA 406355ug/LND1,1,1,2-Tetrachloroethane 08/19/11 0.10 0.50 NA1
SW8260B NA 406355ug/LNDm,p-Xylene 08/19/11 0.20 1.0 NA1
SW8260B NA 406355ug/LNDo-Xylene 08/19/11 0.13 0.50 NA1
SW8260B NA 406355ug/LNDStyrene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LNDBromoform 08/19/11 0.45 1.0 NA1
SW8260B NA 406355ug/LNDIsopropyl Benzene 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDBromobenzene 08/19/11 0.39 0.50 NA1
SW8260B NA 406355ug/LND1,1,2,2-Tetrachloroethane 08/19/11 0.26 0.50 NA1
SW8260B NA 406355ug/LNDn-Propylbenzene 08/19/11 0.30 0.50 NA1
SW8260B NA 406355ug/LND2-Chlorotoluene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LND1,3,5-Trimethylbenzene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LND4-Chlorotoluene 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LNDtert-Butylbenzene 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LND1,2,3-Trichloropropane 08/19/11 0.59 1.0 NA1
SW8260B NA 406355ug/LND1,2,4-Trimethylbenzene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LNDsec-Butyl Benzene 08/19/11 0.24 0.50 NA1
SW8260B NA 406355ug/LNDp-Isopropyltoluene 08/19/11 0.25 0.50 NA1
SW8260B NA 406355ug/LND1,3-Dichlorobenzene 08/19/11 0.31 0.50 NA1
SW8260B NA 406355ug/LND1,4-Dichlorobenzene 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDn-Butylbenzene 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichlorobenzene 08/19/11 0.39 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dibromo-3-Chloropropane 08/19/11 0.45 1.0 NA1
SW8260B NA 406355ug/LNDHexachlorobutadiene 08/19/11 0.22 0.50 NA1
SW8260B NA 406355ug/LND1,2,4-Trichlorobenzene 08/19/11 0.48 1.0 NA1
SW8260B NA 406355ug/LNDNaphthalene 08/19/11 0.57 1.0 NA1
SW8260B NA 406355ug/LND1,2,3-Trichlorobenzene 08/19/11 0.52 1.0 NA1
SW8260B NA 406355%95.6(S) Dibromofluoromethane 08/19/11 61.2 131 NA1
SW8260B NA 406355%89.8(S) Toluene-d8 08/19/11 75.1 127 NA1
SW8260B NA 406355%86.4(S) 4-Bromofluorobenzene 08/19/11 64.1 120 NA1
Page 12 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 12:45
1204.22
500 Kirkham
JA-3
WaterSample Matrix:
Lab Sample ID: 1108103-002A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/19/11 406355ug/LNDTPH(Gasoline) 08/19/11 22 50 34441
8260TPH 8/19/11 406355%88.3(S) 4-Bromofluorobenzene 08/19/11 34 114 34441
Page 13 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 12:45
1204.22
500 Kirkham
JA-3
WaterSample Matrix:
Lab Sample ID: 1108103-002B
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021
SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021
SW8015B(M) 8/16/11 406321%92.1Pentacosane (S) 08/17/11 57.9 125 34021
Page 14 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 12:45
1204.22
500 Kirkham
JA-3
WaterSample Matrix:
Lab Sample ID: 1108103-002C
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/16/11 406289mg/LNDAntimony (Dissolved) 08/18/11 0.004 0.009 34061
SW6010B 8/16/11 406289mg/LNDArsenic (Dissolved) 08/18/11 0.005 0.009 34061
SW6010B 8/16/11 406289mg/L0.074Barium (Dissolved) 08/18/11 0.002 0.009 34061
SW6010B 8/16/11 406289mg/LNDBeryllium (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/LNDCadmium (Dissolved) 08/18/11 0.001 0.005 34061
SW6010B 8/16/11 406289mg/LNDChromium (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/LNDCobalt (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/LNDCopper (Dissolved) 08/18/11 0.003 0.009 34061
SW6010B 8/16/11 406289mg/LNDLead (Dissolved) 08/18/11 0.005 0.014 34061
SW6010B 8/16/11 406289mg/LNDMolybdenum (Dissolved) 08/18/11 0.002 0.009 34061
SW6010B 8/16/11 406289mg/L0.036Nickel (Dissolved) 08/18/11 0.002 0.009 34061
SW6010B 8/16/11 406289mg/LNDSelenium (Dissolved) 08/18/11 0.004 0.02 34061
SW6010B 8/16/11 406289mg/LNDSilver (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/LNDThallium (dissolved) 08/18/11 0.004 0.009 34061
SW6010B 8/16/11 406289mg/LNDVanadium (Dissolved) 08/18/11 0.004 0.009 34061
SW6010B 8/16/11 406289mg/LNDZinc (dissolved) 08/18/11 0.002 0.009 34061
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7470A 8/16/11 406291mg/LNDMercury (Dissolved) 08/17/11 0.00005 0.0002 34091
Page 15 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 14:20
1204.22
500 Kirkham
JA-4
WaterSample Matrix:
Lab Sample ID: 1108103-003A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406355ug/LNDDichlorodifluoromethane 08/19/11 0.41 0.50 NA1
SW8260B NA 406355ug/LNDChloromethane 08/19/11 0.41 0.50 NA1
SW8260B NA 406355ug/L2.5Vinyl Chloride 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromomethane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDTrichlorofluoromethane 08/19/11 0.34 0.50 NA1
SW8260B NA 406355ug/L5.21,1-Dichloroethene 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LNDFreon 113 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDMethylene Chloride 08/19/11 0.18 5.0 NA1
SW8260B NA 406355ug/L2.6trans-1,2-Dichloroethene 08/19/11 0.31 0.50 NA1
SW8260B NA 406355ug/LNDMTBE 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDtert-Butanol 08/19/11 1.5 5.0 NA1
SW8260B NA 406355ug/LNDDiisopropyl ether (DIPE) 08/19/11 0.36 0.50 NA1
SW8260B NA 406355ug/L461,1-Dichloroethane 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDETBE 08/19/11 0.40 0.50 NA1
SW8260B NA 406355ug/LND2,2-Dichloropropane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromochloromethane 08/19/11 0.34 0.50 NA1
SW8260B NA 406355ug/L0.53Chloroform 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LNDCarbon Tetrachloride 08/19/11 0.26 0.50 NA1
SW8260B NA 406355ug/LND1,1,1-Trichloroethane 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloropropene 08/19/11 0.40 0.50 NA1
SW8260B NA 406355ug/L0.53Benzene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LNDTAME 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichloroethane 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDDibromomethane 08/19/11 0.21 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichloropropane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromodichloromethane 08/19/11 0.23 0.50 NA1
SW8260B NA 406355ug/LNDcis-1,3-Dichloropropene 08/19/11 0.30 0.50 NA1
SW8260B NA 406355ug/LNDToluene 08/19/11 0.19 0.50 NA1
SW8260B NA 406355ug/L36Tetrachloroethylene 08/19/11 0.15 0.50 NA1
SW8260B NA 406355ug/LNDtrans-1,3-Dichloropropene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/L0.911,1,2-Trichloroethane 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LNDDibromochloromethane 08/19/11 0.21 0.50 NA1
SW8260B NA 406355ug/LND1,3-Dichloropropane 08/19/11 0.18 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dibromoethane 08/19/11 0.19 0.50 NA1
SW8260B NA 406355ug/LNDChlorobenzene 08/19/11 0.14 0.50 NA1
SW8260B NA 406355ug/LNDEthyl Benzene 08/19/11 0.15 0.50 NA1
Page 16 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 14:20
1204.22
500 Kirkham
JA-4
WaterSample Matrix:
Lab Sample ID: 1108103-003A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406355ug/LND1,1,1,2-Tetrachloroethane 08/19/11 0.10 0.50 NA1
SW8260B NA 406355ug/LNDm,p-Xylene 08/19/11 0.20 1.0 NA1
SW8260B NA 406355ug/LNDo-Xylene 08/19/11 0.13 0.50 NA1
SW8260B NA 406355ug/LNDStyrene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LNDBromoform 08/19/11 0.45 1.0 NA1
SW8260B NA 406355ug/LNDIsopropyl Benzene 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDBromobenzene 08/19/11 0.39 0.50 NA1
SW8260B NA 406355ug/LND1,1,2,2-Tetrachloroethane 08/19/11 0.26 0.50 NA1
SW8260B NA 406355ug/LNDn-Propylbenzene 08/19/11 0.30 0.50 NA1
SW8260B NA 406355ug/LND2-Chlorotoluene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LND1,3,5-Trimethylbenzene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LND4-Chlorotoluene 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LNDtert-Butylbenzene 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LND1,2,3-Trichloropropane 08/19/11 0.59 1.0 NA1
SW8260B NA 406355ug/LND1,2,4-Trimethylbenzene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LNDsec-Butyl Benzene 08/19/11 0.24 0.50 NA1
SW8260B NA 406355ug/LNDp-Isopropyltoluene 08/19/11 0.25 0.50 NA1
SW8260B NA 406355ug/LND1,3-Dichlorobenzene 08/19/11 0.31 0.50 NA1
SW8260B NA 406355ug/LND1,4-Dichlorobenzene 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDn-Butylbenzene 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichlorobenzene 08/19/11 0.39 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dibromo-3-Chloropropane 08/19/11 0.45 1.0 NA1
SW8260B NA 406355ug/LNDHexachlorobutadiene 08/19/11 0.22 0.50 NA1
SW8260B NA 406355ug/LND1,2,4-Trichlorobenzene 08/19/11 0.48 1.0 NA1
SW8260B NA 406355ug/LNDNaphthalene 08/19/11 0.57 1.0 NA1
SW8260B NA 406355ug/LND1,2,3-Trichlorobenzene 08/19/11 0.52 1.0 NA1
SW8260B NA 406355%97.6(S) Dibromofluoromethane 08/19/11 61.2 131 NA1
SW8260B NA 406355%91.8(S) Toluene-d8 08/19/11 75.1 127 NA1
SW8260B NA 406355%89.5(S) 4-Bromofluorobenzene 08/19/11 64.1 120 NA1
SW8260B NA 406363ug/L160cis-1,2-Dichloroethene 08/22/11 1.4 2.2 NA4.4
SW8260B NA 406363ug/L140Trichloroethylene 08/22/11 1.7 2.2 NA4.4
SW8260B NA 406363%84.4(S) Dibromofluoromethane 08/22/11 61.2 131 NA4.4
SW8260B NA 406363%90.8(S) Toluene-d8 08/22/11 75.1 127 NA4.4
SW8260B NA 406363%86.9(S) 4-Bromofluorobenzene 08/22/11 64.1 120 NA4.4
Page 17 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 14:20
1204.22
500 Kirkham
JA-4
WaterSample Matrix:
Lab Sample ID: 1108103-003A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/19/11 406355x ug/L180TPH(Gasoline) 08/19/11 22 50 34441
8260TPH 8/19/11 406355%79.6(S) 4-Bromofluorobenzene 08/19/11 34 114 34441
x-Not typical of Gasoline standard pattern. Result due to discrete peaks of non-fuel compounds (see 8260 results).NOTE:
Page 18 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 14:20
1204.22
500 Kirkham
JA-4
WaterSample Matrix:
Lab Sample ID: 1108103-003B
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021
SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021
SW8015B(M) 8/16/11 406321%78.0Pentacosane (S) 08/17/11 57.9 125 34021
Page 19 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 14:20
1204.22
500 Kirkham
JA-4
WaterSample Matrix:
Lab Sample ID: 1108103-003C
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/16/11 406289mg/LNDAntimony (Dissolved) 08/18/11 0.004 0.009 34061
SW6010B 8/16/11 406289mg/LNDArsenic (Dissolved) 08/18/11 0.005 0.009 34061
SW6010B 8/16/11 406289mg/L0.17Barium (Dissolved) 08/18/11 0.002 0.009 34061
SW6010B 8/16/11 406289mg/LNDBeryllium (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/LNDCadmium (Dissolved) 08/18/11 0.001 0.005 34061
SW6010B 8/16/11 406289mg/L0.0070Chromium (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/L0.0080Cobalt (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/LNDCopper (Dissolved) 08/18/11 0.003 0.009 34061
SW6010B 8/16/11 406289mg/LNDLead (Dissolved) 08/18/11 0.005 0.014 34061
SW6010B 8/16/11 406289mg/LNDMolybdenum (Dissolved) 08/18/11 0.002 0.009 34061
SW6010B 8/16/11 406289mg/L0.30Nickel (Dissolved) 08/18/11 0.002 0.009 34061
SW6010B 8/16/11 406289mg/LNDSelenium (Dissolved) 08/18/11 0.004 0.02 34061
SW6010B 8/16/11 406289mg/LNDSilver (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/LNDThallium (dissolved) 08/18/11 0.004 0.009 34061
SW6010B 8/16/11 406289mg/LNDVanadium (Dissolved) 08/18/11 0.004 0.009 34061
SW6010B 8/16/11 406289mg/LNDZinc (dissolved) 08/18/11 0.002 0.009 34061
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7470A 8/16/11 406291mg/LNDMercury (Dissolved) 08/17/11 0.00005 0.0002 34091
Page 20 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 14:20
1204.22
500 Kirkham
JA-4D
WaterSample Matrix:
Lab Sample ID: 1108103-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406355ug/LNDDichlorodifluoromethane 08/19/11 0.41 0.50 NA1
SW8260B NA 406355ug/LNDChloromethane 08/19/11 0.41 0.50 NA1
SW8260B NA 406355ug/L2.5Vinyl Chloride 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromomethane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDTrichlorofluoromethane 08/19/11 0.34 0.50 NA1
SW8260B NA 406355ug/L5.21,1-Dichloroethene 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LNDFreon 113 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDMethylene Chloride 08/19/11 0.18 5.0 NA1
SW8260B NA 406355ug/L2.7trans-1,2-Dichloroethene 08/19/11 0.31 0.50 NA1
SW8260B NA 406355ug/LNDMTBE 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDtert-Butanol 08/19/11 1.5 5.0 NA1
SW8260B NA 406355ug/LNDDiisopropyl ether (DIPE) 08/19/11 0.36 0.50 NA1
SW8260B NA 406355ug/L451,1-Dichloroethane 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDETBE 08/19/11 0.40 0.50 NA1
SW8260B NA 406355ug/LND2,2-Dichloropropane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromochloromethane 08/19/11 0.34 0.50 NA1
SW8260B NA 406355ug/LNDChloroform 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LNDCarbon Tetrachloride 08/19/11 0.26 0.50 NA1
SW8260B NA 406355ug/LND1,1,1-Trichloroethane 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloropropene 08/19/11 0.40 0.50 NA1
SW8260B NA 406355ug/LNDBenzene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LNDTAME 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichloroethane 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDDibromomethane 08/19/11 0.21 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichloropropane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromodichloromethane 08/19/11 0.23 0.50 NA1
SW8260B NA 406355ug/LNDcis-1,3-Dichloropropene 08/19/11 0.30 0.50 NA1
SW8260B NA 406355ug/LNDToluene 08/19/11 0.19 0.50 NA1
SW8260B NA 406355ug/L34Tetrachloroethylene 08/19/11 0.15 0.50 NA1
SW8260B NA 406355ug/LNDtrans-1,3-Dichloropropene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/L0.851,1,2-Trichloroethane 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LNDDibromochloromethane 08/19/11 0.21 0.50 NA1
SW8260B NA 406355ug/LND1,3-Dichloropropane 08/19/11 0.18 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dibromoethane 08/19/11 0.19 0.50 NA1
SW8260B NA 406355ug/LNDChlorobenzene 08/19/11 0.14 0.50 NA1
SW8260B NA 406355ug/LNDEthyl Benzene 08/19/11 0.15 0.50 NA1
Page 21 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 14:20
1204.22
500 Kirkham
JA-4D
WaterSample Matrix:
Lab Sample ID: 1108103-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406355ug/LND1,1,1,2-Tetrachloroethane 08/19/11 0.10 0.50 NA1
SW8260B NA 406355ug/LNDm,p-Xylene 08/19/11 0.20 1.0 NA1
SW8260B NA 406355ug/LNDo-Xylene 08/19/11 0.13 0.50 NA1
SW8260B NA 406355ug/LNDStyrene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LNDBromoform 08/19/11 0.45 1.0 NA1
SW8260B NA 406355ug/LNDIsopropyl Benzene 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDBromobenzene 08/19/11 0.39 0.50 NA1
SW8260B NA 406355ug/LND1,1,2,2-Tetrachloroethane 08/19/11 0.26 0.50 NA1
SW8260B NA 406355ug/LNDn-Propylbenzene 08/19/11 0.30 0.50 NA1
SW8260B NA 406355ug/LND2-Chlorotoluene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LND1,3,5-Trimethylbenzene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LND4-Chlorotoluene 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LNDtert-Butylbenzene 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LND1,2,3-Trichloropropane 08/19/11 0.59 1.0 NA1
SW8260B NA 406355ug/LND1,2,4-Trimethylbenzene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LNDsec-Butyl Benzene 08/19/11 0.24 0.50 NA1
SW8260B NA 406355ug/LNDp-Isopropyltoluene 08/19/11 0.25 0.50 NA1
SW8260B NA 406355ug/LND1,3-Dichlorobenzene 08/19/11 0.31 0.50 NA1
SW8260B NA 406355ug/LND1,4-Dichlorobenzene 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDn-Butylbenzene 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichlorobenzene 08/19/11 0.39 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dibromo-3-Chloropropane 08/19/11 0.45 1.0 NA1
SW8260B NA 406355ug/LNDHexachlorobutadiene 08/19/11 0.22 0.50 NA1
SW8260B NA 406355ug/LND1,2,4-Trichlorobenzene 08/19/11 0.48 1.0 NA1
SW8260B NA 406355ug/LNDNaphthalene 08/19/11 0.57 1.0 NA1
SW8260B NA 406355ug/LND1,2,3-Trichlorobenzene 08/19/11 0.52 1.0 NA1
SW8260B NA 406355%93.2(S) Dibromofluoromethane 08/19/11 61.2 131 NA1
SW8260B NA 406355%89.8(S) Toluene-d8 08/19/11 75.1 127 NA1
SW8260B NA 406355%87.1(S) 4-Bromofluorobenzene 08/19/11 64.1 120 NA1
SW8260B NA 406363ug/L170cis-1,2-Dichloroethene 08/22/11 1.4 2.2 NA4.4
SW8260B NA 406363ug/L150Trichloroethylene 08/22/11 1.7 2.2 NA4.4
SW8260B NA 406363%85.0(S) Dibromofluoromethane 08/22/11 61.2 131 NA4.4
SW8260B NA 406363%90.6(S) Toluene-d8 08/22/11 75.1 127 NA4.4
SW8260B NA 406363%82.8(S) 4-Bromofluorobenzene 08/22/11 64.1 120 NA4.4
Page 22 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 14:20
1204.22
500 Kirkham
JA-4D
WaterSample Matrix:
Lab Sample ID: 1108103-004A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/19/11 406355x ug/L190TPH(Gasoline) 08/19/11 22 50 34441
8260TPH 8/19/11 406355%88.0(S) 4-Bromofluorobenzene 08/19/11 34 114 34441
x-Not typical of Gasoline standard pattern. Result due to discrete peaks of non-fuel compounds (see 8260 results).NOTE:
Page 23 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 14:20
1204.22
500 Kirkham
JA-4D
WaterSample Matrix:
Lab Sample ID: 1108103-004B
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021
SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021
SW8015B(M) 8/16/11 406321%79.8Pentacosane (S) 08/17/11 57.9 125 34021
Page 24 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 14:20
1204.22
500 Kirkham
JA-4D
WaterSample Matrix:
Lab Sample ID: 1108103-004C
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW6010B 8/16/11 406289mg/LNDAntimony (Dissolved) 08/18/11 0.004 0.009 34061
SW6010B 8/16/11 406289mg/LNDArsenic (Dissolved) 08/18/11 0.005 0.009 34061
SW6010B 8/16/11 406289mg/L0.16Barium (Dissolved) 08/18/11 0.002 0.009 34061
SW6010B 8/16/11 406289mg/LNDBeryllium (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/LNDCadmium (Dissolved) 08/18/11 0.001 0.005 34061
SW6010B 8/16/11 406289mg/L0.0067Chromium (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/L0.0079Cobalt (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/LNDCopper (Dissolved) 08/18/11 0.003 0.009 34061
SW6010B 8/16/11 406289mg/LNDLead (Dissolved) 08/18/11 0.005 0.014 34061
SW6010B 8/16/11 406289mg/LNDMolybdenum (Dissolved) 08/18/11 0.002 0.009 34061
SW6010B 8/16/11 406289mg/L0.29Nickel (Dissolved) 08/18/11 0.002 0.009 34061
SW6010B 8/16/11 406289mg/LNDSelenium (Dissolved) 08/18/11 0.004 0.02 34061
SW6010B 8/16/11 406289mg/LNDSilver (Dissolved) 08/18/11 0.002 0.005 34061
SW6010B 8/16/11 406289mg/LNDThallium (dissolved) 08/18/11 0.004 0.009 34061
SW6010B 8/16/11 406289mg/LNDVanadium (Dissolved) 08/18/11 0.004 0.009 34061
SW6010B 8/16/11 406289mg/LNDZinc (dissolved) 08/18/11 0.002 0.009 34061
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW7470A 8/16/11 406291mg/LNDMercury (Dissolved) 08/17/11 0.00005 0.0002 34091
Page 25 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 10:00
1204.22
500 Kirkham
Equipment Blank
WaterSample Matrix:
Lab Sample ID: 1108103-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406355ug/LNDDichlorodifluoromethane 08/19/11 0.41 0.50 NA1
SW8260B NA 406355ug/LNDChloromethane 08/19/11 0.41 0.50 NA1
SW8260B NA 406355ug/LNDVinyl Chloride 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromomethane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDTrichlorofluoromethane 08/19/11 0.34 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloroethene 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LNDFreon 113 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDMethylene Chloride 08/19/11 0.18 5.0 NA1
SW8260B NA 406355ug/LNDtrans-1,2-Dichloroethene 08/19/11 0.31 0.50 NA1
SW8260B NA 406355ug/LNDMTBE 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDtert-Butanol 08/19/11 1.5 5.0 NA1
SW8260B NA 406355ug/LNDDiisopropyl ether (DIPE) 08/19/11 0.36 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloroethane 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDETBE 08/19/11 0.40 0.50 NA1
SW8260B NA 406355ug/LNDcis-1,2-Dichloroethene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LND2,2-Dichloropropane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromochloromethane 08/19/11 0.34 0.50 NA1
SW8260B NA 406355ug/LNDChloroform 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LNDCarbon Tetrachloride 08/19/11 0.26 0.50 NA1
SW8260B NA 406355ug/LND1,1,1-Trichloroethane 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloropropene 08/19/11 0.40 0.50 NA1
SW8260B NA 406355ug/LNDBenzene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LNDTAME 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichloroethane 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDTrichloroethylene 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDDibromomethane 08/19/11 0.21 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichloropropane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromodichloromethane 08/19/11 0.23 0.50 NA1
SW8260B NA 406355ug/LNDcis-1,3-Dichloropropene 08/19/11 0.30 0.50 NA1
SW8260B NA 406355ug/LNDToluene 08/19/11 0.19 0.50 NA1
SW8260B NA 406355ug/LNDTetrachloroethylene 08/19/11 0.15 0.50 NA1
SW8260B NA 406355ug/LNDtrans-1,3-Dichloropropene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LND1,1,2-Trichloroethane 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LNDDibromochloromethane 08/19/11 0.21 0.50 NA1
SW8260B NA 406355ug/LND1,3-Dichloropropane 08/19/11 0.18 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dibromoethane 08/19/11 0.19 0.50 NA1
Page 26 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 10:00
1204.22
500 Kirkham
Equipment Blank
WaterSample Matrix:
Lab Sample ID: 1108103-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406355ug/LNDChlorobenzene 08/19/11 0.14 0.50 NA1
SW8260B NA 406355ug/LNDEthyl Benzene 08/19/11 0.15 0.50 NA1
SW8260B NA 406355ug/LND1,1,1,2-Tetrachloroethane 08/19/11 0.10 0.50 NA1
SW8260B NA 406355ug/LNDm,p-Xylene 08/19/11 0.20 1.0 NA1
SW8260B NA 406355ug/LNDo-Xylene 08/19/11 0.13 0.50 NA1
SW8260B NA 406355ug/LNDStyrene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LNDBromoform 08/19/11 0.45 1.0 NA1
SW8260B NA 406355ug/LNDIsopropyl Benzene 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDBromobenzene 08/19/11 0.39 0.50 NA1
SW8260B NA 406355ug/LND1,1,2,2-Tetrachloroethane 08/19/11 0.26 0.50 NA1
SW8260B NA 406355ug/LNDn-Propylbenzene 08/19/11 0.30 0.50 NA1
SW8260B NA 406355ug/LND2-Chlorotoluene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LND1,3,5-Trimethylbenzene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LND4-Chlorotoluene 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LNDtert-Butylbenzene 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LND1,2,3-Trichloropropane 08/19/11 0.59 1.0 NA1
SW8260B NA 406355ug/LND1,2,4-Trimethylbenzene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LNDsec-Butyl Benzene 08/19/11 0.24 0.50 NA1
SW8260B NA 406355ug/LNDp-Isopropyltoluene 08/19/11 0.25 0.50 NA1
SW8260B NA 406355ug/LND1,3-Dichlorobenzene 08/19/11 0.31 0.50 NA1
SW8260B NA 406355ug/LND1,4-Dichlorobenzene 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDn-Butylbenzene 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichlorobenzene 08/19/11 0.39 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dibromo-3-Chloropropane 08/19/11 0.45 1.0 NA1
SW8260B NA 406355ug/LNDHexachlorobutadiene 08/19/11 0.22 0.50 NA1
SW8260B NA 406355ug/LND1,2,4-Trichlorobenzene 08/19/11 0.48 1.0 NA1
SW8260B NA 406355ug/LNDNaphthalene 08/19/11 0.57 1.0 NA1
SW8260B NA 406355ug/LND1,2,3-Trichlorobenzene 08/19/11 0.52 1.0 NA1
SW8260B NA 406355%102(S) Dibromofluoromethane 08/19/11 61.2 131 NA1
SW8260B NA 406355%91.3(S) Toluene-d8 08/19/11 75.1 127 NA1
SW8260B NA 406355%87.8(S) 4-Bromofluorobenzene 08/19/11 64.1 120 NA1
Page 27 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/15/11 / 10:00
1204.22
500 Kirkham
Equipment Blank
WaterSample Matrix:
Lab Sample ID: 1108103-005A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
8260TPH 8/19/11 406355ug/LNDTPH(Gasoline) 08/19/11 22 50 34441
8260TPH 8/19/11 406355%82.4(S) 4-Bromofluorobenzene 08/19/11 34 114 34441
Page 28 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/09/11 /
1204.22
500 Kirkham
TB080911 #4
WaterSample Matrix:
Lab Sample ID: 1108103-006A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406355ug/LNDDichlorodifluoromethane 08/19/11 0.41 0.50 NA1
SW8260B NA 406355ug/LNDChloromethane 08/19/11 0.41 0.50 NA1
SW8260B NA 406355ug/LNDVinyl Chloride 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromomethane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDTrichlorofluoromethane 08/19/11 0.34 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloroethene 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LNDFreon 113 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDMethylene Chloride 08/19/11 0.18 5.0 NA1
SW8260B NA 406355ug/LNDtrans-1,2-Dichloroethene 08/19/11 0.31 0.50 NA1
SW8260B NA 406355ug/LNDMTBE 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDtert-Butanol 08/19/11 1.5 5.0 NA1
SW8260B NA 406355ug/LNDDiisopropyl ether (DIPE) 08/19/11 0.36 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloroethane 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDETBE 08/19/11 0.40 0.50 NA1
SW8260B NA 406355ug/LNDcis-1,2-Dichloroethene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LND2,2-Dichloropropane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromochloromethane 08/19/11 0.34 0.50 NA1
SW8260B NA 406355ug/LNDChloroform 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LNDCarbon Tetrachloride 08/19/11 0.26 0.50 NA1
SW8260B NA 406355ug/LND1,1,1-Trichloroethane 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloropropene 08/19/11 0.40 0.50 NA1
SW8260B NA 406355ug/LNDBenzene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LNDTAME 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichloroethane 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDTrichloroethylene 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDDibromomethane 08/19/11 0.21 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichloropropane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromodichloromethane 08/19/11 0.23 0.50 NA1
SW8260B NA 406355ug/LNDcis-1,3-Dichloropropene 08/19/11 0.30 0.50 NA1
SW8260B NA 406355ug/LNDToluene 08/19/11 0.19 0.50 NA1
SW8260B NA 406355ug/LNDTetrachloroethylene 08/19/11 0.15 0.50 NA1
SW8260B NA 406355ug/LNDtrans-1,3-Dichloropropene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LND1,1,2-Trichloroethane 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LNDDibromochloromethane 08/19/11 0.21 0.50 NA1
SW8260B NA 406355ug/LND1,3-Dichloropropane 08/19/11 0.18 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dibromoethane 08/19/11 0.19 0.50 NA1
Page 29 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/09/11 /
1204.22
500 Kirkham
TB080911 #4
WaterSample Matrix:
Lab Sample ID: 1108103-006A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406355ug/LNDChlorobenzene 08/19/11 0.14 0.50 NA1
SW8260B NA 406355ug/LNDEthyl Benzene 08/19/11 0.15 0.50 NA1
SW8260B NA 406355ug/LND1,1,1,2-Tetrachloroethane 08/19/11 0.10 0.50 NA1
SW8260B NA 406355ug/LNDm,p-Xylene 08/19/11 0.20 1.0 NA1
SW8260B NA 406355ug/LNDo-Xylene 08/19/11 0.13 0.50 NA1
SW8260B NA 406355ug/LNDStyrene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LNDBromoform 08/19/11 0.45 1.0 NA1
SW8260B NA 406355ug/LNDIsopropyl Benzene 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDBromobenzene 08/19/11 0.39 0.50 NA1
SW8260B NA 406355ug/LND1,1,2,2-Tetrachloroethane 08/19/11 0.26 0.50 NA1
SW8260B NA 406355ug/LNDn-Propylbenzene 08/19/11 0.30 0.50 NA1
SW8260B NA 406355ug/LND2-Chlorotoluene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LND1,3,5-Trimethylbenzene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LND4-Chlorotoluene 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LNDtert-Butylbenzene 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LND1,2,3-Trichloropropane 08/19/11 0.59 1.0 NA1
SW8260B NA 406355ug/LND1,2,4-Trimethylbenzene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LNDsec-Butyl Benzene 08/19/11 0.24 0.50 NA1
SW8260B NA 406355ug/LNDp-Isopropyltoluene 08/19/11 0.25 0.50 NA1
SW8260B NA 406355ug/LND1,3-Dichlorobenzene 08/19/11 0.31 0.50 NA1
SW8260B NA 406355ug/LND1,4-Dichlorobenzene 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDn-Butylbenzene 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichlorobenzene 08/19/11 0.39 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dibromo-3-Chloropropane 08/19/11 0.45 1.0 NA1
SW8260B NA 406355ug/LNDHexachlorobutadiene 08/19/11 0.22 0.50 NA1
SW8260B NA 406355ug/LND1,2,4-Trichlorobenzene 08/19/11 0.48 1.0 NA1
SW8260B NA 406355ug/LNDNaphthalene 08/19/11 0.57 1.0 NA1
SW8260B NA 406355ug/LND1,2,3-Trichlorobenzene 08/19/11 0.52 1.0 NA1
SW8260B NA 406355%109(S) Dibromofluoromethane 08/19/11 61.2 131 NA1
SW8260B NA 406355%91.5(S) Toluene-d8 08/19/11 75.1 127 NA1
SW8260B NA 406355%89.6(S) 4-Bromofluorobenzene 08/19/11 64.1 120 NA1
Page 30 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/09/11 /
1204.22
500 Kirkham
TB080911 #3
WaterSample Matrix:
Lab Sample ID: 1108103-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406355ug/LNDDichlorodifluoromethane 08/19/11 0.41 0.50 NA1
SW8260B NA 406355ug/LNDChloromethane 08/19/11 0.41 0.50 NA1
SW8260B NA 406355ug/LNDVinyl Chloride 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromomethane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDTrichlorofluoromethane 08/19/11 0.34 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloroethene 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LNDFreon 113 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDMethylene Chloride 08/19/11 0.18 5.0 NA1
SW8260B NA 406355ug/LNDtrans-1,2-Dichloroethene 08/19/11 0.31 0.50 NA1
SW8260B NA 406355ug/LNDMTBE 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDtert-Butanol 08/19/11 1.5 5.0 NA1
SW8260B NA 406355ug/LNDDiisopropyl ether (DIPE) 08/19/11 0.36 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloroethane 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDETBE 08/19/11 0.40 0.50 NA1
SW8260B NA 406355ug/LNDcis-1,2-Dichloroethene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LND2,2-Dichloropropane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromochloromethane 08/19/11 0.34 0.50 NA1
SW8260B NA 406355ug/LNDChloroform 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LNDCarbon Tetrachloride 08/19/11 0.26 0.50 NA1
SW8260B NA 406355ug/LND1,1,1-Trichloroethane 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,1-Dichloropropene 08/19/11 0.40 0.50 NA1
SW8260B NA 406355ug/LNDBenzene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LNDTAME 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichloroethane 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDTrichloroethylene 08/19/11 0.38 0.50 NA1
SW8260B NA 406355ug/LNDDibromomethane 08/19/11 0.21 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichloropropane 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDBromodichloromethane 08/19/11 0.23 0.50 NA1
SW8260B NA 406355ug/LNDcis-1,3-Dichloropropene 08/19/11 0.30 0.50 NA1
SW8260B NA 406355ug/LNDToluene 08/19/11 0.19 0.50 NA1
SW8260B NA 406355ug/LNDTetrachloroethylene 08/19/11 0.15 0.50 NA1
SW8260B NA 406355ug/LNDtrans-1,3-Dichloropropene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LND1,1,2-Trichloroethane 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LNDDibromochloromethane 08/19/11 0.21 0.50 NA1
SW8260B NA 406355ug/LND1,3-Dichloropropane 08/19/11 0.18 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dibromoethane 08/19/11 0.19 0.50 NA1
Page 31 of 48Total Page Count: 48
SAMPLE RESULTS
Report prepared for: Date Reported: 08/22/11Date Received: 08/15/11
Northgate Environmental Management Inc.Dennis Laduzinsky
Client Sample ID:
Date/Time Sampled:
Project Number:
Project Name/Location:
08/09/11 /
1204.22
500 Kirkham
TB080911 #3
WaterSample Matrix:
Lab Sample ID: 1108103-007A
Tag Number: 500 Kirkham
Parameters: PrepBatch
AnalyticalBatch
UnitLabQualifier
ResultsPQLMDLDFDateAnalyzed
PrepDate
AnalysisMethod
SW8260B NA 406355ug/LNDChlorobenzene 08/19/11 0.14 0.50 NA1
SW8260B NA 406355ug/LNDEthyl Benzene 08/19/11 0.15 0.50 NA1
SW8260B NA 406355ug/LND1,1,1,2-Tetrachloroethane 08/19/11 0.10 0.50 NA1
SW8260B NA 406355ug/LNDm,p-Xylene 08/19/11 0.20 1.0 NA1
SW8260B NA 406355ug/LNDo-Xylene 08/19/11 0.13 0.50 NA1
SW8260B NA 406355ug/LNDStyrene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LNDBromoform 08/19/11 0.45 1.0 NA1
SW8260B NA 406355ug/LNDIsopropyl Benzene 08/19/11 0.28 0.50 NA1
SW8260B NA 406355ug/LNDBromobenzene 08/19/11 0.39 0.50 NA1
SW8260B NA 406355ug/LND1,1,2,2-Tetrachloroethane 08/19/11 0.26 0.50 NA1
SW8260B NA 406355ug/LNDn-Propylbenzene 08/19/11 0.30 0.50 NA1
SW8260B NA 406355ug/LND2-Chlorotoluene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LND1,3,5-Trimethylbenzene 08/19/11 0.20 0.50 NA1
SW8260B NA 406355ug/LND4-Chlorotoluene 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LNDtert-Butylbenzene 08/19/11 0.29 0.50 NA1
SW8260B NA 406355ug/LND1,2,3-Trichloropropane 08/19/11 0.59 1.0 NA1
SW8260B NA 406355ug/LND1,2,4-Trimethylbenzene 08/19/11 0.33 0.50 NA1
SW8260B NA 406355ug/LNDsec-Butyl Benzene 08/19/11 0.24 0.50 NA1
SW8260B NA 406355ug/LNDp-Isopropyltoluene 08/19/11 0.25 0.50 NA1
SW8260B NA 406355ug/LND1,3-Dichlorobenzene 08/19/11 0.31 0.50 NA1
SW8260B NA 406355ug/LND1,4-Dichlorobenzene 08/19/11 0.37 0.50 NA1
SW8260B NA 406355ug/LNDn-Butylbenzene 08/19/11 0.32 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dichlorobenzene 08/19/11 0.39 0.50 NA1
SW8260B NA 406355ug/LND1,2-Dibromo-3-Chloropropane 08/19/11 0.45 1.0 NA1
SW8260B NA 406355ug/LNDHexachlorobutadiene 08/19/11 0.22 0.50 NA1
SW8260B NA 406355ug/LND1,2,4-Trichlorobenzene 08/19/11 0.48 1.0 NA1
SW8260B NA 406355ug/LNDNaphthalene 08/19/11 0.57 1.0 NA1
SW8260B NA 406355ug/LND1,2,3-Trichlorobenzene 08/19/11 0.52 1.0 NA1
SW8260B NA 406355%106(S) Dibromofluoromethane 08/19/11 61.2 131 NA1
SW8260B NA 406355%91.3(S) Toluene-d8 08/19/11 75.1 127 NA1
SW8260B NA 406355%88.4(S) 4-Bromofluorobenzene 08/19/11 64.1 120 NA1
Page 32 of 48Total Page Count: 48
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
406321
mg/L
08/17/11
34023510_TPHSG1108103
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0440 0.10TPH as Diesel (SG) ND
0.0920 0.20TPH as Motor Oil (SG) ND
Pentacosane (S) 51.7 S
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
406321
mg/L
08/17/11
34023510_TPHSG1108103
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.0440 0.10TPH as Diesel (SG) ND
0.0920 0.20TPH as Motor Oil (SG) 0.13
Pentacosane (S) 75.1
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
406289
mg/Kg
08/18/11
340630051108103
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.004 0.009Antimony (Dissolved) ND
0.005 0.009Arsenic (Dissolved) ND
0.002 0.009Barium (Dissolved) ND
0.002 0.005Beryllium (Dissolved) ND
0.001 0.005Cadmium (Dissolved) ND
0.002 0.005Chromium (Dissolved) ND
0.002 0.005Cobalt (Dissolved) ND
0.003 0.009Copper (Dissolved) ND
0.005 0.014Lead (Dissolved) ND
0.002 0.009Molybdenum (Dissolved) ND
0.002 0.009Nickel (Dissolved) ND
0.004 0.02Selenium (Dissolved) ND
0.002 0.005Silver (Dissolved) 0.00255
0.004 0.009Thallium (dissolved) ND
0.004 0.009Vanadium (Dissolved) ND
0.002 0.009Zinc (dissolved) ND
Page 33 of 48Total Page Count: 48
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW7470AAnalytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
406291
mg/L
08/17/11
34097470A1108103
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.00005 0.0002Mercury (Dissolved) ND
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/19/11 Prep Batch:
Analytical Batch:
406362
ug/L
08/19/11
344450301108103
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
22 50TPH(Gasoline) ND
(S) 4-Bromofluorobenzene 90.4
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/19/11 Prep Batch:
Analytical Batch:
406355
ug/L
08/19/11
345050301108103
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
22 50TPH(Gasoline) ND
(S) 4-Bromofluorobenzene 87.3
Page 34 of 48Total Page Count: 48
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
ug/L
NA1108103
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.41 0.50Dichlorodifluoromethane ND
0.41 0.50Chloromethane ND
0.37 0.50Vinyl Chloride ND
0.37 0.50Bromomethane ND
0.34 0.50Trichlorofluoromethane ND
0.29 0.501,1-Dichloroethene ND
0.38 0.50Freon 113 ND
0.18 5.0Methylene Chloride ND
0.31 0.50trans-1,2-Dichloroethene ND
0.38 0.50MTBE ND
1.5 5.0tert-Butanol ND
0.36 0.50Diisopropyl ether (DIPE) ND
0.28 0.501,1-Dichloroethane ND
0.40 0.50ETBE ND
0.33 0.50cis-1,2-Dichloroethene ND
0.37 0.502,2-Dichloropropane ND
0.34 0.50Bromochloromethane ND
0.29 0.50Chloroform ND
0.26 0.50Carbon Tetrachloride ND
0.32 0.501,1,1-Trichloroethane ND
0.40 0.501,1-Dichloropropene ND
0.33 0.50Benzene ND
0.32 0.50TAME ND
0.28 0.501,2-Dichloroethane ND
0.38 0.50Trichloroethylene ND
0.21 0.50Dibromomethane ND
0.37 0.501,2-Dichloropropane ND
0.23 0.50Bromodichloromethane ND
0.30 0.50cis-1,3-Dichloropropene ND
0.19 0.50Toluene ND
0.15 0.50Tetrachloroethylene ND
0.20 0.50trans-1,3-Dichloropropene ND
0.20 0.501,1,2-Trichloroethane ND
0.21 0.50Dibromochloromethane ND
0.18 0.501,3-Dichloropropane ND
0.19 0.501,2-Dibromoethane ND
0.14 0.50Chlorobenzene ND
0.15 0.50Ethyl Benzene ND
0.10 0.501,1,1,2-Tetrachloroethane ND
0.20 1.0m,p-Xylene ND
0.13 0.50o-Xylene ND
Page 35 of 48Total Page Count: 48
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
ug/L
NA1108103
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.20 0.50Styrene ND
0.45 1.0Bromoform ND
0.28 0.50Isopropyl Benzene ND
0.39 0.50Bromobenzene ND
0.26 0.501,1,2,2-Tetrachloroethane ND
0.30 0.50n-Propylbenzene ND
0.33 0.502-Chlorotoluene ND
0.20 0.501,3,5-Trimethylbenzene ND
0.32 0.504-Chlorotoluene ND
0.29 0.50tert-Butylbenzene ND
0.59 1.01,2,3-Trichloropropane ND
0.33 0.501,2,4-Trimethylbenzene ND
0.24 0.50sec-Butyl Benzene ND
0.25 0.50p-Isopropyltoluene ND
0.31 0.501,3-Dichlorobenzene ND
0.37 0.501,4-Dichlorobenzene ND
0.32 0.50n-Butylbenzene ND
0.39 0.501,2-Dichlorobenzene ND
0.45 1.01,2-Dibromo-3-Chloropropane ND
0.22 0.50Hexachlorobutadiene ND
0.48 1.01,2,4-Trichlorobenzene ND
0.57 1.0Naphthalene ND
0.52 1.01,2,3-Trichlorobenzene ND
100 100Ethanol ND TIC
(S) Dibromofluoromethane 83.5
(S) Toluene-d8 93.3
(S) 4-Bromofluorobenzene 89.3
Page 36 of 48Total Page Count: 48
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
406363
ug/L
08/22/11
NANA1108103
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.41 0.50Dichlorodifluoromethane ND
0.41 0.50Chloromethane ND
0.37 0.50Vinyl Chloride ND
0.37 0.50Bromomethane ND
0.34 0.50Trichlorofluoromethane ND
0.29 0.501,1-Dichloroethene ND
0.38 0.50Freon 113 ND
0.18 5.0Methylene Chloride ND
0.31 0.50trans-1,2-Dichloroethene ND
0.38 0.50MTBE ND
1.5 5.0tert-Butanol ND
0.36 0.50Diisopropyl ether (DIPE) ND
0.28 0.501,1-Dichloroethane ND
0.40 0.50ETBE ND
0.33 0.50cis-1,2-Dichloroethene ND
0.37 0.502,2-Dichloropropane ND
0.34 0.50Bromochloromethane ND
0.29 0.50Chloroform ND
0.26 0.50Carbon Tetrachloride ND
0.32 0.501,1,1-Trichloroethane ND
0.40 0.501,1-Dichloropropene ND
0.33 0.50Benzene ND
0.32 0.50TAME ND
0.28 0.501,2-Dichloroethane ND
0.38 0.50Trichloroethylene ND
0.21 0.50Dibromomethane ND
0.37 0.501,2-Dichloropropane ND
0.23 0.50Bromodichloromethane ND
0.30 0.50cis-1,3-Dichloropropene ND
0.19 0.50Toluene ND
0.15 0.50Tetrachloroethylene ND
0.20 0.50trans-1,3-Dichloropropene ND
0.20 0.501,1,2-Trichloroethane ND
0.21 0.50Dibromochloromethane ND
0.18 0.501,3-Dichloropropane ND
0.19 0.501,2-Dibromoethane ND
0.14 0.50Chlorobenzene ND
0.15 0.50Ethyl Benzene ND
0.10 0.501,1,1,2-Tetrachloroethane ND
0.20 1.0m,p-Xylene ND
0.13 0.50o-Xylene ND
Page 37 of 48Total Page Count: 48
MB Summary Report
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
406363
ug/L
08/22/11
NANA1108103
Water
ParametersMethodBlankConc.
PQL MDL Lab
Qualifier
0.20 0.50Styrene ND
0.45 1.0Bromoform ND
0.28 0.50Isopropyl Benzene ND
0.39 0.50Bromobenzene ND
0.26 0.501,1,2,2-Tetrachloroethane ND
0.30 0.50n-Propylbenzene ND
0.33 0.502-Chlorotoluene ND
0.20 0.501,3,5-Trimethylbenzene ND
0.32 0.504-Chlorotoluene ND
0.29 0.50tert-Butylbenzene ND
0.59 1.01,2,3-Trichloropropane ND
0.33 0.501,2,4-Trimethylbenzene ND
0.24 0.50sec-Butyl Benzene ND
0.25 0.50p-Isopropyltoluene ND
0.31 0.501,3-Dichlorobenzene ND
0.37 0.501,4-Dichlorobenzene ND
0.32 0.50n-Butylbenzene ND
0.39 0.501,2-Dichlorobenzene ND
0.45 1.01,2-Dibromo-3-Chloropropane ND
0.22 0.50Hexachlorobutadiene ND
0.48 1.01,2,4-Trichlorobenzene ND
0.57 1.0Naphthalene ND
0.52 1.01,2,3-Trichlorobenzene ND
100 100Ethanol ND TIC
(S) Dibromofluoromethane 96.9
(S) Toluene-d8 90.3
(S) 4-Bromofluorobenzene 88.4
Page 38 of 48Total Page Count: 48
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW8015B(M)Analytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
40632108/17/11
mg/L
3510_TPHSG 3402
Water
1108103
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.10 10.0440 2.00 0,34.5 - 95.6TPH as Diesel (SG) 51.6 52.7ND
100 57.9 - 125Pentacosane (S) 79.6 73.0ND
Work Order:
Matrix:
Units:
Prep Method:
SW6010BAnalytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
40628908/18/11
mg/Kg
3005 3406
Water
1108103
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.009 10.004 0.195 0,80 - 120Antimony (Dissolved) 88.5 89.0ND
0.009 10.005 1.71 0,80 - 120Arsenic (Dissolved) 89.9 91.4ND
0.009 10.002 0.739 0,80 - 120Barium (Dissolved) 91.0 91.5ND
0.005 10.002 0.963 2080 - 120Beryllium (Dissolved) 97.4 96.1ND
0.005 10.001 0.149 2080 - 120Cadmium (Dissolved) 89.1 89.0ND
0.005 10.002 0.576 2080 - 120Chromium (Dissolved) 92.2 92.4ND
0.005 10.002 1.42 2080 - 120Cobalt (Dissolved) 92.2 93.2ND
0.009 10.003 0.951 2080 - 120Copper (Dissolved) 91.2 91.7ND
0.014 10.005 0.423 2080 - 120Lead (Dissolved) 93.5 94.3ND
0.009 10.002 1.27 2080 - 120Molybdenum (Dissolved) 95.4 96.2ND
0.009 10.002 0.526 2080 - 120Nickel (Dissolved) 92.7 93.4ND
0.02 10.004 1.09 2080 - 120Selenium (Dissolved) 93.3 93.9ND
0.005 10.002 0.114 2080 - 120Silver (Dissolved) 89.4 90.00.00255
0.009 10.004 1.43 2080 - 120Thallium (dissolved) 92.1 93.2ND
0.009 10.004 0.0898 2080 - 120Vanadium (Dissolved) 90.7 91.0ND
0.009 10.002 0.515 2080 - 120Zinc (dissolved) 93.1 93.4ND
Work Order:
Matrix:
Units:
Prep Method:
SW7470AAnalytical Method:
Prep Date:
Analyzed Date:
08/16/11 Prep Batch:
Analytical Batch:
40629108/17/11
mg/L
7470A 3409
Water
1108103
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.0002 0.0150.00005 14.1 0,80 - 120Mercury (Dissolved) 110 98.4ND
Page 39 of 48Total Page Count: 48
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/19/11 Prep Batch:
Analytical Batch:
40636208/19/11
ug/L
5030 3444
Water
1108103
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
50 227.2722 10.2 3052.4 - 127TPH(Gasoline) 98.2 109ND
11.36 58.4 - 133(S) 4-Bromofluorobenzene 98.8 94.590.4
Work Order:
Matrix:
Units:
Prep Method:
8260TPHAnalytical Method:
Prep Date:
Analyzed Date:
08/19/11 Prep Batch:
Analytical Batch:
40635508/19/11
ug/L
5030 3450
Water
1108103
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
50 227.2722 52.4 - 127TPH(Gasoline) 81.8ND
11.36 58.4 - 133(S) 4-Bromofluorobenzene 89.487.3
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
ug/L
NA
Water
1108103
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.50 17.040.29 1.53 3061.4 - 1291,1-Dichloroethene 81.9 80.9ND
0.50 17.040.33 2.97 3066.9 - 140Benzene 90.5 93.1ND
0.50 17.040.38 1.31 3069.3 - 144Trichloroethylene 101 103ND
0.50 17.040.19 1.10 3076.6 - 123Toluene 92.9 93.7ND
0.50 17.040.14 0.0494 3073.9 - 137Chlorobenzene 95.0 95.1ND
11.36 61.2 - 131(S) Dibromofluoromethane 88.7 91.5ND
11.36 75.1 - 127(S) Toluene-d8 89.5 91.2ND
11.36 64.1 - 120(S) 4-Bromofluorobenzene 82.7 86.4ND
Page 40 of 48Total Page Count: 48
LCS/LCSD Summary ReportRaw values are used in quality control assessment.
Work Order:
Matrix:
Units:
Prep Method:
SW8260BAnalytical Method:
Prep Date:
Analyzed Date:
NA Prep Batch:
Analytical Batch:
40636308/22/11
ug/L
NA NA
Water
1108103
Parameters MDL PQL MethodBlankConc.
SpikeConc.
LCS %Recovery
LCSD %Recovery
LCS/LCSD% RPD
%Recovery
Limits% RPDLimits
LabQualifier
0.50 17.040.29 7.77 3061.4 - 1291,1-Dichloroethene 76.9 83.1ND
0.50 17.040.33 8.18 3066.9 - 140Benzene 86.8 94.3ND
0.50 17.040.38 9.08 3069.3 - 144Trichloroethylene 87.7 95.8ND
0.50 17.040.19 9.09 3076.6 - 123Toluene 86.8 95.1ND
0.50 17.040.14 8.25 3073.9 - 137Chlorobenzene 88.3 95.6ND
11.36 61.2 - 131(S) Dibromofluoromethane 93.8 89.8ND
11.36 75.1 - 127(S) Toluene-d8 89.1 89.3ND
11.36 64.1 - 120(S) 4-Bromofluorobenzene 80.3 85.0ND
Page 41 of 48Total Page Count: 48
MS/MSD Summary ReportRaw values are used in quality control assessment.
Work Order: 1108103
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/16/11
1108103-001CSpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW6010B 40628908/18/11
mg/Kg
34063005
Water
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
1 75 - 1250.004 0.009 0.669 20Antimony (Dissolved) 88.4 88.20.00
1 75 - 1250.005 0.009 1.22 20Arsenic (Dissolved) 87.1 87.80.00
1 80 - 1200.002 0.009 1.84 20Barium (Dissolved) 86.4 84.30.127
1 80 - 1200.002 0.005 0.460 20Beryllium (Dissolved) 92.7 93.30
1 75 - 1250.001 0.005 2.17 20Cadmium (Dissolved) 86.1 83.90.00
1 75 - 1250.002 0.005 2.16 20Chromium (Dissolved) 89.8 87.90.00
1 75 - 1250.002 0.005 0.274 20Cobalt (Dissolved) 86.0 85.50.00
1 75 - 1250.003 0.009 2.62 20Copper (Dissolved) 92.6 90.50.00
1 75 - 1250.005 0.014 1.08 20Lead (Dissolved) 85.9 84.80.00
1 75 - 1250.002 0.009 0.595 20Molybdenum (Dissolved) 92.8 92.40.00
1 75 - 1250.002 0.009 0.0476 20Nickel (Dissolved) 85.9 85.70.00
1 75 - 1250.004 0.02 0.157 20Selenium (Dissolved) 91.1 90.70.00
1 75 - 1250.002 0.005 2.93 20Silver (Dissolved) 90.5 88.20.00
1 75 - 1250.004 0.009 0.602 20Thallium (dissolved) 81.6 81.20.00
1 75 - 1250.004 0.009 1.91 20Vanadium (Dissolved) 89.3 87.10.00
1 75 - 1250.002 0.009 3.54 20Zinc (dissolved) 87.3 84.80.00
Work Order: 1108103
Analyzed Date:
Prep Date:
Matrix:
Prep Method: 08/16/11
1108103-002CSpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW7470A 40629108/17/11
mg/L
34097470A
Water
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
0.015 75 - 1250.00005 S,R0.0002 28.4 20Mercury (Dissolved) 52.3 69.3-0.00001
Page 42 of 48Total Page Count: 48
MS/MSD Summary ReportRaw values are used in quality control assessment.
Work Order: 1108103
Analyzed Date:
Prep Date:
Matrix:
Prep Method: NA
1108103-001ASpiked Sample:
Analytical Method:
Prep Batch:
Units:
Analytical Batch:
SW8260B 40636308/22/11
ug/L
NANA
Water
Parameters MDL PQL SampleConc.
SpikeConc.
MS %Recovery
MSD %Recovery
MS/MSD% RPD
%Recovery
Limits
% RPDLimits
LabQualifier
17.04 61.4 - 1290.29 0.50 2.88 301,1-Dichloroethene 112 1150
17.04 66.9 - 1400.33 0.50 4.26 30Benzene 103 1080
17.04 69.3 - 1440.38 0.50 0.213 30Trichloroethylene 107 1070
17.04 76.6 - 1230.19 0.50 0.594 30Toluene 106 1050
17.04 73.9 - 1370.14 0.50 0.115 30Chlorobenzene 102 1020
11.36 61.2 - 131(S) Dibromofluoromethane 85.7 89.4
11.36 75.1 - 127(S) Toluene-d8 89.8 87.2
11.36 64.1 - 120(S) 4-Bromofluorobenzene 84.2 82.7
Page 43 of 48Total Page Count: 48
Laboratory Qualifiers and Definitions
Method Detection Limit (MDL) - the minimum concentration of a substance that can be measured and reported with a 99% confidence that the analyte concentration is greater than zero
Matrix Spike (MS/MSD) - Client sample spiked with identical concentrations of target analyte (s). The spiking occurs prior to the sample preparation and analysis. They are used to document the precision and bias of a method in a given sample matrix.
Matrix - the component or substrate that contains the analyte of interest (e.g., - groundwater, sediment, soil, waste water, etc)
Laboratory Control Sample (LCS ad LCSD) - A known matrix spiked with compounds representative of the target analyte(s). This is used to document laboratory performance.
Duplicate - a field sample and/or laboratory QC sample prepared in duplicate following all of the same processes and procedures used on the original sample (sample duplicate, LCSD, MSD)
Blank (Method/Preparation Blank) -MB/PB - An analyte-free matrix to which all reagents are added in the same volumes/proportions as used in sample processing. The method blank is used to document contamination resulting from the analytical process.
Practical Quantitation Limit (PQL) - a laboratory determined value at 2 to 5 times above the MDL that can be reproduced in a manner that results in a 99% confidence level that the result is both accurate and precise. PQLs reflect all preparation factors and/or dilution factors that have been applied to the sample during the preparation and/or analytical processes.
Precision (%RPD) - The agreement among a set of replicate/duplicate measurements without regard to known value of the replicates
Surrogate (S) or (Surr) - An organic compound which is similar to the target analyte(s) in chemical composition and behavior in the analytical process, but which is not normally found in environmental samples. Surrogates are used in most organic analysis to demonstrate matrix compatibility with the chosen method of analysis
Tentatively Identified Compound (TIC) - A compound not contained within the analytical calibration standards but present in the GCMS library of defined compounds. When the library is searched for an unknown compound, it can frequently give a tentative identification to the compound based on retention time and primary and secondary ion match. TICs are reported as estimates and are candidates for further investigation.
Units: the unit of measure used to express the reported result - mg/L and mg/Kg (equivalent to PPM - parts per million in liquid and solid), ug/L and ug/Kg (equivalent to PPB - parts per billion in liquid and solid), ug/m3, mg.m3, ppbv and ppmv (all units of measure for reporting concentrations in air), % ( equivalent to 10000 ppm or 1,000,000 ppb), ug/Wipe ( concentration found on the surface of a single Wipe usually taken over a 100cm2 surface)
B - Indicates when the anlayte is found in the associated method or preparation blank D - Surrogate is not recoverable due to the necessary dilution of the sampleE - Indicates the reportable value is outside of the calibration range of the instrument but within the linear range of the instrument (unless otherwise noted) Values reported with an E qualifier should be considered as estimated.H- Indicates that the recommended holding time for the analyte or compound has been exceededJ- Indicates a value between the method MDL and PQL and that the reported concentration should be considered as estimated rather the quantitative NA - Not AnalyzedN/A - Not ApplicableNR - Not recoverable - a matrix spike concentration is not recoverable due to a concentration within the original sample that is greater than four times the spike concentration addedR- The % RPD between a duplicate set of samples is outside of the absolute values established by laboratory control chartsS- Spike recovery is outside of established method and/or laboratory control limits. Further explanation of the use of this qualifier should be included within a case narrative
X -Used to indicate that a value based on pattern identification is within the pattern range but not typical of the pattern found in standards. Further explanation may or may not be provided within the sample footnote and/or the case narrative.
DEFINITIONS:
Accuracy/Bias (% Recovery) - The closeness of agreement between an observed value and an accepted reference value.
LABORATORY QUALIFIERS:
Page 44 of 48Total Page Count: 48
pH Adjusted by: pH Checked by:
°C4
Yes
Yes
Yes
Temperature:
Water-pH acceptable upon receipt?
Water-VOA vials have zero headspace?
Container/Temp Blank temperature in compliance?
All samples received within holding time?
Sample Preservation and Hold Time (HT) Information
YesSamples containers intact?
Yes
Yes
Not Present
Yes
Sufficient sample volume for indicated test?
Samples in proper container/bottle?
Custody seals intact on shipping container/cooler?
Shipping Container/Cooler In Good Condition?
Sample Receipt Information
Yes
Yes
Yes
Not Present
Chain of custody agrees with sample labels?
Chain of custody signed when relinquished and received?
Chain of custody present?
Custody seals intact on sample bottles?
Chain of Custody (COC) Information
Checklist Completed By: NG
Carrier Name: First Courier
Physically Logged By: NG
Received By: NG
Date and Time Received: 8/15/2011 16:15
Work Order No.: 1108103
Project Name: 500 Kirkham
Client Name: Northgate Environmental Management Inc.
Sample Receipt Checklist
Page 45 of 48Total Page Count: 48
Login Summary Report
Report Due Date:
On 08/15/2011, 7 samples received on 5 day TAT.
16:15
8/15/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/22/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
5+ day:0
1108103Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
JA-21108103-001A Water 09/29/1108/15/11 11:15W_GCMS-GROW_8260Full
Sample Note: TPH-D/O Silica Gel clean up on all samples. Dissolved Metals CAM 17 on all samples. Use JA-2(sample 001) for MS/MSD. VOAs for JA-4 and JA-4D are unpreserved. Watch for the holding time on samples 006 and 007.JA-21108103-001B Water 09/29/1108/15/11 11:15
W_TPHDOSGJA-21108103-001C Water 09/29/1108/15/11 11:15
W_D7470AHGW_D6010BCAM17
JA-31108103-002A Water 09/29/1108/15/11 12:45W_GCMS-GROW_8260Full
JA-31108103-002B Water 09/29/1108/15/11 12:45W_TPHDOSG
JA-31108103-002C Water 09/29/1108/15/11 12:45W_D7470AHGW_D6010BCAM17
JA-41108103-003A Water 09/29/1108/15/11 14:20W_GCMS-GROW_8260Full
JA-41108103-003B Water 09/29/1108/15/11 14:20W_TPHDOSG
JA-41108103-003C Water 09/29/1108/15/11 14:20W_D7470AHGW_D6010BCAM17
JA-4D1108103-004A Water 09/29/1108/15/11 14:20W_GCMS-GROW_8260Full
JA-4D1108103-004B Water 09/29/1108/15/11 14:20W_TPHDOSG
JA-4D1108103-004C Water 09/29/1108/15/11 14:20W_D7470AHGW_D6010BCAM17
Equipment Blank1108103-005A Water 09/29/1108/15/11 10:00W_GCMS-GROW_8260Full
Page 46 of 48Total Page Count: 48
Login Summary Report
Report Due Date:
On 08/15/2011, 7 samples received on 5 day TAT.
16:15
8/15/2011
Northgate Environmental Management Inc.TL5143
500 Kirkham
1204.22
8/22/2011
TAT Requested:
Date Received:
Time Received:
QC Level:
Project Name:
Project # :
Comments:
Client ID:
5+ day:0
1108103Work Order # :
SubbedRequestedTests
TestOn Hold
SampleOn Hold
ScheduledDisposal
MatrixCollection Date/Time
Client Sample ID
WO Sample ID
TB080911 #41108103-006A Water 09/29/1108/09/11W_8260Full
TB080911 #31108103-007A Water 09/29/1108/09/11W_8260Full
Page 47 of 48Total Page Count: 48
Page 48 of 48Total Page Count: 48