1. Standard Hydrogen Electrode 2. Sequestering agents 3...

transcript

1 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

PC 306

Oral exam.

30/12/2012

........................................................... الرقم الجلوس....................االسم ................

1. Standard Hydrogen Electrode

2. Sequestering agents

3. Precision

2 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

االسم ................................................................... الرقم الجلوس............................

1. Saturated calomel electrode(S.C.E.)

2. Factors affecting on the Stability of complexes

3. Accuracy

3 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

1. Silver-silver chloride electrode

2. Complexones

3. Linearity

4 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

................................................... الرقم الجلوس............................االسم ................

1. Concentrated cell

2. General requirements for a good metal indicators

3. LOD

5 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

1. Zimmermann’s reagent

2. Replacement and Back titration

3. LQD

6 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

.......... الرقم الجلوس............................االسم .........................................................

1. Effect of pH on oxidation potential of oxygenated system.

2. Indirect complexometric titration (determination of anions).

3. Methods of Validation

7 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

1. Addition NaHCO3 before titration of arsenite with iodine.

2. Masking and Demasking.

3. Limit of detection

8 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

................................................................. الرقم الجلوس............................االسم ..

1. Desirable properties of redox indicators

2. Increasing selectivity of EDTA

3. Precision

9 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

1. Diphenyamine.

2. Liebeg’s Method for determination of cyanide

3. Accuracy

10 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

.............................. الرقم الجلوس............................االسم .....................................

1. Iodometric methods

2. Denige’s modification

3. Methods of validation

11 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

1. Iodimetric method,

2. Sequestering agents

3. LOD

12 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

1. Precaution must be considered in case of using starch as

indicator in iodometric method

2. Factors affecting on the Stability of complexes

3. LQD

13 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

............................................................. الرقم الجلوس............................االسم ......

1. “Andrews Reaction”

2. Complexones

3. Method of validation

14 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

1. Direct method for determination of Fe3+

2. Replacement and Back titration

3. Types of Error

15 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

1. redox determination of PbO

2. Indirect complexometric titration (determination of anions).

3. H2O2 as oxidizing and reducing agent

16 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

1. H2O2 as oxidizing and reducing agent

2. Masking and Demasking.

3. redox determination of PbO

17 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

.......... الرقم الجلوس............................االسم .........................................................

1. Karl Fischer reagent

2. Increasing selectivity of EDTA

3. Redox determination of Bleaching powder

18 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

................................................... الرقم الجلوس............................االسم ................

1. Redox determination of Bleaching powder

2. Liebeg’s Method for determination of cyanide

3. Karl Fischer reagent

19 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

1. Redox detetrmination of mixture of Glucose & sucrose

3. Concentrated cell

20 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

department

PC 306

Oral exam.

30/12/2012

1. Redox determination of Phenol

3. NHE

1. Standard Hydrogen Electrode 2. Sequestering agents 3...

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