Post on 07-Jul-2020
transcript
From: ed.gortner@epa.ohio.gov [mailto:ed.gortner@epa.ohio.gov] Sent: Friday, June 02, 2017 5:56 PMTo: Rich McGuire <Rich.McGuire@ferc.gov>; Terry Turpin <Terry.Turpin@ferc.gov>Subject: Data for Rover Stark Site
Hi Rich and Terry,
As you know, Ohio EPA recently discovered that diesel fuel constituents are present in the bentonite drilling mud associated with Rover’s large inadvertent return in Stark County. Out of an abundance of caution, Ohio EPA has begun ground water and drinking water well sampling near that Rover pipeline project.
Attached are the data results (originally sent you on May 26, 2017) from 2 separate sampling initiatives that resulted from 2 complaints of diesel fuel being added to the drilling fluid at the Stark site. The lab analyzed them using EPA Method 8015C for Diesel Range Organics (DRO). The attached pdf labeled “DRO Results” included 5 individual sampling locations and collection dates as follows:
1) IR Mud Breakout collected on 4/18/172) IR Mud Silo collected on 5/12/173) IR Mud Grid C1-D1 collected on 5/12/174) IR Mud 54 Return collected on 5/12/175) IR Mud W Reclaim Pit collected on 5/12/17
All of the above samples detected the presence of DRO.
Also attached are the lab data results (originally sent you on May 26, 2017) from supplemental sampling which were initiated based upon the DRO data. The lab analyzed them using EPA Method 8260B (Total VOCs), EPA Method 8270C (Total SVOCs), TCLP VOCs, TCLP SVOCs and TCLP Metals. The attached pdf labeled “Totals and TCLP Results prelim” included 7 individual sampling locations and collection dates as follows:
1) OSG Disposal Pit collected on 5/19/172) IR Mud Original collected on 5/19/173) IR Mud Silo collected on 5/19/174) IR Mud Grid A3 New collected on 5/19/175) West Borehole Return M collected on 5/19/176) West Reclaimer Pit collected on 5/19/177) East Reclaimer New Mud collected on 5/19/17
These results indicate that presence of petroleum hydrocarbons in 6 of the 7 samples. The sample of the new mud that has not been run through the machine came back as the cleanest of all samples. These results are consistent with the earlier DRO data, further confirming the presence of petroleum hydrocarbon constituents commonly found in diesel fuel. These results also include TCLP data which confirms that, although VOCs and SVOCs are present in the drilling fluid slurry, none of these constituents leach when subjected to the TCLP procedure. For your records, please find attached the final laboratory report of these samples for your records. At the time the email was sent on May 26, 2017, Ohio EPA had only received the preliminary data from the lab. The final lab report for the 7 samples collected on May 19, 2017 are attached and labeled as, “Totals and TCLP Results Final”.
20170605-4006 FERC PDF (Unofficial) 06/05/2017
At this time, the information obtained through Ohio EPA’s sampling efforts has not revealed diesel fuel contamination that constitutes an imminent threat to human health and the environment. However, Ohio EPA continues to be concerned with the presence of diesel fuel constituents in the bentonite mud generated by Rover and as a result, Ohio EPA will continue ground water monitoring to ensure that drinking water systems in the area remain safe. It is our understanding that FERC, with Ohio EPA coordination, will be requiring Rover to provide to FERC a plan to assume responsibility for ground water monitoring and, if necessary, response actions.
Ed
Please consider the environment before printing this email.
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Laboratory Report Number: L17050904
Frank ZingalesOhio Environmental Protection Agency2110 East Aurora RoadTwinsburg, OH 44087
Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac’s Ohio Valley Division (OVD). If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed below.
Laboratory Contact:Michelle Taylor – Client Services Specialist(740) 373-4071Michelle.Taylor@microbac.com
I certify that all test results meet all of the requirements of the accrediting authority listed below. All results for soil samples are reported on a 'dry-weight' basis unless specified otherwise. Analytical results for water and wastes are reported on a 'as received' basis unless specified otherwise. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received.
This report was certified on May 18 2017
Leslie Bucina – Managing Director State of Origin: OHAccrediting Authority: N/A ID:OH00218QAPP: Microbac OVD
Microbac Laboratories * Ohio Valley Division158 Starlite Drive, Marietta, OH 45750 * T: (740) 373-4071 F: (740) 373-4835 * www.microbac.com
Page 1
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17050904
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Record of Sample Receipt and InspectionComments/DiscrepanciesThis is the record of the shipment conditions and the inspection records for the samples received and reported as a sample delivery group (SDG). All of the samples were inspected and observed to conform to our receipt policies, except as noted below.
The following discrepancies were noted:Discrepancy Resolution
Sample ID: 17-0751 IR Mud Grid C1-D1 (5/12 @ 16:52). Container was received broken but a portion of the sample was still intact in the jar. Portion split out by lab to perform analyses. BRG
Please proceed. MRT
Sample ID: 17-0751 IR Mud Breakout (4/18 @ 11:30). No time on container. Will log per information on COC. BRG
Please log per the COC. MRT
Sample ID: 17-90751 IR Mud Breakout (4/18/17 @ 11:30). Sample received out of hold for DRO analyses. BRG
Please proceed. MRT
CoolersCooler # Temperature
GunTemperature COC # Airbill # Temp Required?
00114971 H 5.0 1Z98X0V30397689369 X
Inspection Checklist
# Question Result
1 Were shipping coolers sealed? Yes
2 Were custody seals intact? Yes
3 Were cooler temperatures in range of 0-6? Yes
4 Was ice present? Yes
5 Were COC's received/information complete/signed and dated? Yes
6 Were sample containers intact and match COC? No
7 Were sample labels intact and match COC? No
8 Were the correct containers and volumes received? Yes
9 Were samples received within EPA hold times? No
10 Were correct preservatives used? (water only) NA
11 Were pH ranges acceptable? (voa's excluded) NA
12 Were VOA samples free of headspace (less than 6mm)? NA
Microbac Laboratories ● Ohio Valley Division158 Starlite Drive, Marietta, OH 45750 ● T: (740)373-4071 F: (740)373-4835
www.microbac.com
Page 2
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17050904
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Samples ReceivedClient ID Laboratory ID Date Collected Date Received
17-0751 IR MUD SILO L17050904-01 05/12/2017 16:30 05/16/2017 10:11
17-0751 IR MUD GRID C1-D1 L17050904-02 05/12/2017 16:52 05/16/2017 10:11
17-0751 IR MUD 54 RETURN L17050904-03 05/12/2017 18:22 05/16/2017 10:11
17-0751 IR MUD WE RECLAIM PIT L17050904-04 05/12/2017 18:33 05/16/2017 10:11
17-0751 IR MUD BREAKOUT L17050904-05 04/18/2017 11:30 05/16/2017 10:11
Microbac Laboratories ● Ohio Valley Division158 Starlite Drive, Marietta, OH 45750 ● T: (740)373-4071 F: (740)373-4835
www.microbac.com
Page 3
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17050904
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisSample #: L17050904-01 PrePrep Method: N/A Instrument: HP14
Client ID: 17-0751 IR MUD SILO Prep Method: 3546 Prep Date: 05/16/2017 11:21
Matrix: Soil Analytical Method: 8015C Cal Date: 05/09/2017 13:30
Workgroup #: WG614544 Analyst: LJH Run Date: 05/16/2017 17:43
Collect Date: 05/12/2017 16:30 Dilution: 1 File ID: 14G67541
Sample Tag: 01 Units: ug/kg Percent Solid: 51.8
Analyte CAS # Result Qual RL MDL
Diesel Range (C10-C28) 68334-30-5 30400 18200 4540
Surrogate Recovery Lower Limit Upper Limit Q
o-Terphenyl 26.2 43 136 *
Octacosane 36.2 25 162
* Surrogate or spike compound out of range
Sample #: L17050904-02 PrePrep Method: N/A Instrument: HP14
Client ID: 17-0751 IR MUD GRID C1-D1
Prep Method: 3546 Prep Date: 05/16/2017 11:21
Matrix: Soil Analytical Method: 8015C Cal Date: 05/09/2017 13:30
Workgroup #: WG614544 Analyst: LJH Run Date: 05/16/2017 19:41
Collect Date: 05/12/2017 16:52 Dilution: 1 File ID: 14G67544
Sample Tag: 01 Units: ug/kg Percent Solid: 12.0
Analyte CAS # Result Qual RL MDL
Diesel Range (C10-C28) 68334-30-5 233000 96300 24100
Surrogate Recovery Lower Limit Upper Limit Q
o-Terphenyl 12.6 43 136 *
Octacosane 9.41 25 162 *
* Surrogate or spike compound out of range
Sample #: L17050904-03 PrePrep Method: N/A Instrument: HP14
Client ID: 17-0751 IR MUD 54 RETURN
Prep Method: 3546 Prep Date: 05/16/2017 11:21
Matrix: Soil Analytical Method: 8015C Cal Date: 05/09/2017 13:30
Workgroup #: WG614544 Analyst: LJH Run Date: 05/16/2017 17:04
Collect Date: 05/12/2017 18:22 Dilution: 1 File ID: 14G67540
Sample Tag: 01 Units: ug/kg Percent Solid: 25.9
Analyte CAS # Result Qual RL MDL
Diesel Range (C10-C28) 68334-30-5 256000 43900 11000
Surrogate Recovery Lower Limit Upper Limit Q
o-Terphenyl 53.4 43 136
Page 1 of 2 Generated at May 18, 2017 14:44
Page 4
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17050904
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisOctacosane 52.3 25 162
Sample #: L17050904-04 PrePrep Method: N/A Instrument: HP14
Client ID: 17-0751 IR MUD WE RECLAIM PIT
Prep Method: 3546 Prep Date: 05/16/2017 11:21
Matrix: Soil Analytical Method: 8015C Cal Date: 05/09/2017 13:30
Workgroup #: WG614544 Analyst: LJH Run Date: 05/16/2017 18:22
Collect Date: 05/12/2017 18:33 Dilution: 1 File ID: 14G67542
Sample Tag: 01 Units: ug/kg Percent Solid: 34.0
Analyte CAS # Result Qual RL MDL
Diesel Range (C10-C28) 68334-30-5 20500 J 30800 7700
Surrogate Recovery Lower Limit Upper Limit Q
o-Terphenyl 30.9 43 136 *
Octacosane 30.4 25 162
* Surrogate or spike compound out of range
J The analyte was positively identified, but the quantitation was below the RL
Sample #: L17050904-05 PrePrep Method: N/A Instrument: HP14
Client ID: 17-0751 IR MUD BREAKOUT Prep Method: 3546 Prep Date: 05/16/2017 11:21
Matrix: Soil Analytical Method: 8015C Cal Date: 05/09/2017 13:30
Workgroup #: WG614544 Analyst: LJH Run Date: 05/16/2017 19:02
Collect Date: 04/18/2017 11:30 Dilution: 1 File ID: 14G67543
Sample Tag: 01 Units: ug/kg Percent Solid: 37.1
Analyte CAS # Result Qual RL MDL
Diesel Range (C10-C28) 68334-30-5 17300 J,H1 27800 6950
Surrogate Recovery Lower Limit Upper Limit Q
o-Terphenyl 39.5 43 136 *
Octacosane 34.6 25 162
* Surrogate or spike compound out of range
J,H1 The analyte was positively identified, but the quantitation was below the RL. Sample analysis performed past holding time.
Page 2 of 2 Generated at May 18, 2017 14:44
Page 5
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17050904
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Sample #: L17050904-01 Client ID: 17-0751 IR MUD SILO Matrix: Soil Collect Date: 05/12/2017 16:30
Analyte Result Units Qualifier
Percent Solids 51.8 weight %
Sample #: L17050904-02 Client ID: 17-0751 IR MUD GRID C1-D1 Matrix: Soil Collect Date: 05/12/2017 16:52
Analyte Result Units Qualifier
Percent Solids 12.0 weight %
Sample #: L17050904-03 Client ID: 17-0751 IR MUD 54 RETURN Matrix: Soil Collect Date: 05/12/2017 18:22
Analyte Result Units Qualifier
Percent Solids 25.9 weight %
Sample #: L17050904-04 Client ID: 17-0751 IR MUD WE RECLAIM PIT
Matrix: Soil Collect Date: 05/12/2017 18:33
Analyte Result Units Qualifier
Percent Solids 34.0 weight %
Sample #: L17050904-05 Client ID: 17-0751 IR MUD BREAKOUT Matrix: Soil Collect Date: 04/18/2017 11:30
Analyte Result Units Qualifier
Percent Solids 37.1 weight %
Page 1 of 1 Generated at May 18, 2017 14:44
Page 6
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac LaboratoriesCase Narrative
Login Number: L17050904Department: General ChromatographyAnalyst: Lacey Hendershot
Preparation 3546
Analysis SW-846 8015
HOLDING TIMES
Sample Preparation: Sample 05 was received and extracted 14 days out of hold. All other holding times were met.
Sample Analysis: All holding times were met.
PREPARATION
Sample preparation proceeded normally.
CALIBRATION
Initial Calibration: For all compounds that yielded a %RSD greater than 20%, linear or higher order equations were applied. All acceptance criteria were met.
Alternate Source Standards: All acceptance criteria were met.
Continuing Calibration and Tune: All acceptance criteria were met.
BATCH QA/QC
Method Blank: Analytes were detected above the applicable reporting limit for the following analytes: Diesel Range (C10-C28). Please see the applicable QC report for a detailed presentation of the failures. The result was marginally above the MDL, but less than 1/2 of the RL.
Laboratory Control Sample: All acceptance criteria were met.
Matrix Spikes: There were no MS/MSD results associated with this sample delivery group, due to insufficient volume of sample. The laboratory included an LCS and LCS duplicate in the preparation batch in lieu of the NELAC prescribed MS/MSD. Microbac recommends site specific MS/MSD samples to avoid possible data qualification.
Page 1 of 3 Generated at May 18, 2017 12:03
Page 7
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
SAMPLES
Samples: All acceptance criteria were met.
Surrogates: Recoveries out of range were observed for the following analytes: o-Terphenyl, Octacosane. Please see the applicable QC report for a detailed presentation of the failures. Samples 01, 04, and 05 were not re-extracted for low surrogates; the recoveries were greater than 10%. Sample 02 had insufficient volume to re-extract.
Sample # Analyte Date Result Lower Upper Type
L17050904-01 o-Terphenyl 2017-05-16 17:43:27 26.2 43 136 Recovery
L17050904-04 o-Terphenyl 2017-05-16 18:22:54 30.9 43 136 Recovery
L17050904-05 o-Terphenyl 2017-05-16 19:02:09 39.5 43 136 Recovery
L17050904-02 Octacosane 2017-05-16 19:41:32 9.41 25 162 Recovery
L17050904-02 o-Terphenyl 2017-05-16 19:41:32 12.6 43 136 Recovery
Manual Integration Reason Codes
Reason #1: Data System Fails to Select Correct Peak In some cases the chromatography system selects and integrates the 'wrong peak'. In this case the analyst must correct the selection and force the system to integrate the proper peak. Other times the system may miss the peakcompletely.
Reason #2: Data System Splits the Peak Incorrectly or Integrates a False Peak as a Rider Peak This phenomena is common at low concentrations where the signal:noise ratio is low. A single compound (peak) is incorrectly split into multiple peaks or integrated as a main peak with one or more rider peaks resulting in low areacounts for the target compound.
Reason #3: Improperly Integrated Isomers and/or coeluting compounds. This system often fails to distinguish coeluting compounds and or isomers. The integration areas and concentrations are wrong, and they must be corrected by manual integration. Prime examples are benzo(k)fluoranthene andbenzo(b)fluoranthene which are often unresolved and integrated improperly when both are present at low concentrations in standards or samples.
Reason #4: System Establishes Incorrect Baseline There are numerous situations in chromatography where the system establishes the baseline incorrectly. Some baseline errors will be obvious to the analyst and should be corrected via manual procedures.
Reason #5: Miscellaneous Other situations involving integration errors may require in-depth review and technical judgment. These cases should be brought to the attention of the laboratory management. If the form of manual integration is not clearly covered by these four cases, then review and approval by the Laboratory Director or the QA/QC Supervisor will be required.
I certify that this data package is in compliance with the terms and conditions agreed to by the client and Microbac Laboratories Inc., both technically and for completeness, except for the conditions noted above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or designated person, as verified by the following signature.
Narrative ID: 125510Approved By: Eric Lawson
Page 2 of 3 Generated at May 18, 2017 12:03
Page 8
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Page 3 of 3 Generated at May 18, 2017 12:03
Page 9
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac Laboratories Inc.Ohio Valley Division Analyst List
May 18, 2017
001 - BIO-CHEM TESTING WVDEP 220 002 - REIC Consultants, Inc. WVDEP 060003 - Sturm Environmental 004 - MICROBAC PITTSBURGH005 - ES LABORATORIES 006 - ALCOSAN LABORATORIES007 - ALS LABORATORIES 008 - BENCHMARK LABORATORIES010 - MICROBAC CHICAGOLAND AC - AMBER R. CARMICHAELADC - ANTHONY D. CANTER ADG - APRIL D. GREENEALS - ADRIANE L. STEED AWE - ANDREW W. ESSIGAZH - AFTER HOURS BJO - BRIAN J. OGDENBLG - BRENDA L. GREENWALT BNB - Brandi N. BentleyBRG - BRENDA R. GREGORY CAS - Craig A. SmithCEB - CHAD E. BARNES CLC - CHRYS L. CRAWFORDCLS - CARA L. STRICKLER CPD - CHAD P. DAVISCSH - CHRIS S. HILL CV - Carl VolkmanDAK - DEAN A. KETELSEN DCM - DAVID C. MERCKLEDEV - DAVID E. VANDENBERG DIH - DEANNA I. HESSONDLB - DAVID L. BUMGARNER DLP - DOROTHY L. PAYNEDSM - DAVID S. MOSSOR DTG - DOMINIC T. GEHRETECL - ERIC C. LAWSON EPT - ETHAN P. TIDDERP - ERIN R. PORTER FJB - FRANCES J. BOLDENHRF - HEATHER R. FAIRCHILD JDH - JUSTIN D. HESSONJDS - JARED D. SMITH JKP - JACQUELINE K. PARSONSJLD - JESSICA L. DELONG JST - JOSHUA S. TAYLORJTP - JOSHUA T. PEMBERTON JWR - JOHN W. RICHARDSJWS - JACK W. SHEAVES JYH - JI Y. HUKAK - KATHY A. KIRBY KDD - Katelyn D. DaleyKEB - KATIE E. BARNES KHR - KIM H. RHODESKKB - KERRI K. BUCK KRA - KATHY R. ALBERTSONKRP - KATHY R. PARSONS LJH - Lacey J. HendershotLLS - LARRY L. STEPHENS LSB - LESLIE S. BUCINALSJ - LAURA S. JONES MAP - MARLA A. PORTERMBK - MORGAN B. KNOWLTON MES - MARY E. SCHILLINGMMB - MAREN M. BEERY MRT - MICHELLE R. TAYLOROJE - OMOYEMWEN J. ENGLISH PDM - PIERCE D. MORRISPIT - MICROBAC WARRENDALE REK - BOB E. KYERRLB - BOB BUCHANAN RNP - RICK N. PETTYSAV - SARAH A. VANDENBERG SCA - SUEELLEN C. ADAMSSCB - SARAH C. BOGOLIN SCJ - SUE ELLEN C. JOHNSONSDC - SHALYN D. CONLEY TB - TODD BOYLETMB - TIFFANY M. BAILEY TMM - TAMMY M. MORRISVC - VICKI COLLIER WTD - WADE T. DELONGXXX - UNAVAILABLE OR SUBCONTRACT ZTB - ZACH T. BARNES
Page 10
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
List of Valid QualifiersMay 18, 2017
Qualkey: STD_ND=U
Microbac Laboratories Inc.
Qualifier Description
*+<>AB
B1B3C
CGDLE
EDLEMPCF, SFL
FP1H1IJ
J,BJ,H1J,PJ,SLL1L2MN
NAND, SND,LNFNFLNINRNSPQ
QNSRARES
SMISPTIC
TNTCU
U,H1UJWX
X, SYZ
Surrogate or spike compound out of rangeCorrelation coefficient for the MSA is less than 0.995Result is less than the associated numerical value.Result is greater than the associated numerical value.See the report narrativeAnalyte present in method blankTarget analyte detected in method blank at or above the method reporting limitTarget analyte detected in calibration blank at or above the method reporting limitConfirmed by GC/MSConfluent growthSurrogate or spike compound was diluted outEstimated concentration due to sample matrix interferenceElevated sample reporting limits, presence of non-target analytesEstimated Maximum Possible ConcentrationEstimated result below quantitation limit; method of standard additions(MSA)Free LiquidDid not ignite.Sample analysis performed past holding time.Semiquantitative result (out of instrument calibration range)The analyte was positively identified, but the quantitation was below the RLAnalyte detected in both the method blank and sample above the MDL.The analyte was positively identified, but the quantitation was below the RL. Sample analysis performed past holding timeEstimate; columns don't agree to within 40%Estimated concentration; analyzed by method of standard addition (MSA)Sample reporting limits elevated due to matrix interferenceThe associated blank spike (LCS) recovery was above the laboratory acceptance limits.The associated blank spike (LCS) recovery was below the laboratory acceptance limits.Matrix effect; the concentration is an estimate due to matrix effect.Tentatively identified compound(TIC)Not applicableNot detected; analyzed by method of standard addition (MSA)Not detected; sample reporting limit (RL) elevated due to interferenceNot found by library searchNo free liquidNon-ignitableAnalyte is not required to be analyzedNot spikedConcentrations >40% difference between the two GC columnsOne or more quality control criteria failed. See narrative.Quantity of sample not sufficient to perform analysisReanalysis confirms reported resultsReanalysis confirms sample matrix interferenceAnalyzed by method of standard addition (MSA)Sample matrix interference on surrogateReported results are for spike compounds onlyLibrary Search CompoundToo numerous to countNot detected at or above adjusted sample detection limitNot detected; sample analysis performed past holding time.Undetected; the MDL and RL are estimated due to quality control discrepancies.Post-digestion spike for furnace AA out of control limitsExceeds regulatory limitExceeds regulatory limit; method of standard additions (MSA)This analyte is not on the laboratory's current scope of accreditation.Cannot be resolved from isomer - see below
Page 11
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Organic QA/QC
Page 12
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
05/17/2017 10:07Report generated5297722PDF File ID:
Microbac Laboratories Inc.
METHOD BLANK SUMMARY
Report Name: BLANK_SUMMARY
14G67536
05/16/17 11:21
05/16/17 14:27
WG614544
WG614301-01
HP14
Blank File ID:
Prep Date:
Analyzed Date:
Work Group:
Blank Sample ID:
Instrument ID:
8015CMethod:
LJHAnalyst:
L17050904Login Number:
LCS
LCS2
17-0751 IR MUD 54 RETURN
17-0751 IR MUD SILO
17-0751 IR MUD WE RECLAIM PIT
17-0751 IR MUD BREAKOUT
17-0751 IR MUD GRID C1-D1
WG614301-02
WG614301-03
L17050904-03
L17050904-01
L17050904-04
L17050904-05
L17050904-02
14G67537
14G67538
14G67540
14G67541
14G67542
14G67543
14G67544
05/16/17 15:06
05/16/17 15:45
05/16/17 17:04
05/16/17 17:43
05/16/17 18:22
05/16/17 19:02
05/16/17 19:41
This Method Blank Applies To The Following Samples:
Client ID Lab Sample ID Lab File ID Time Analyzed TAG
01
01
01
01
01
01
01
Page 13
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac Laboratories Inc.
METHOD BLANK REPORT
Report Name:BLANK
PDF ID: 5297723
17-MAY-2017 10:07
o-Terphenyl
Octacosane
69.6
62.6
Surrogates % Recovery Surrogate Limits
43
25
-
-
136
162
Qualifier
PASS
PASS
Analytes Concentration Dilution Qualifier
Diesel Range (C10-C28) 12500 10000 J3900
ND Analyte Not detected at or above reporting limit
* |Analyte concentration| > RL
14G67536
WG614544
Instrument ID:HP14
File ID:
Prep Date:05/16/17 11:21
Run Date:05/16/17 14:27
Analyst:LJH
Workgroup (AAB#): ug/kgUnits:
8015CMethod:
SoilMatrix:
L17050904Login Number: WG614301-01Sample ID:
09-MAY-17Cal ID: HP14-OT900917Contract #:
3546Prep Method:
MDL RL
MDL
RL
Method Detection Limit
Reporting/Practical Quantitation Limit
Page 14
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
LCS_LCS2 - Modified 03/06/2008
05/17/2017 10:07Report generated:5297724PDF File ID:
LABORATORY CONTROL SAMPLE (LCS)
Microbac Laboratories Inc.
Diesel Range (C10-C28)
LCS LCS2
4.13137000 143000
Analytes %RPD
250000 250000
Found FoundKnown Known
54.9 57.2
% REC % REC
26
RPDLmt
%RecLimits
35 120-
Q
Sample ID:
Sample ID:
WG614301-02
WG614301-03
LCS
LCS2
14G67537
14G67538
File ID:
File ID:
o-Terphenyl
Octacosane
LCS LCS2
69.7 73.4
68.2 74.9
Surogates% Recovery % Recovery
Surrogate Limits
43
25
136
162
-
-
Qualifier
PASS
PASS
Run Date:
Run Date:
05/16/2017 15:06
05/16/2017 15:45
WG614544
Instrument ID:HP14
Analyst:LJH
Workgroup (AAB#): ug/kgUnits:
8015CMethod:SoilMatrix:
L17050904Login Number: 3546Prep Method:
* EXCEEDS %REC LIMIT
# EXCEEDS RPD LIMIT
STDQC Key: STD81195Lot #:
Page 15
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
SURROGATES - Modified 03/06/2008
05/17/2017 10:07Report generated:5297728PDF File ID:
SURROGATE STANDARDS
Microbac Laboratories Inc.
L17050904-01
L17050904-02
L17050904-03
L17050904-04
L17050904-05
WG614301-01
WG614301-02
WG614301-03
01
01
01
01
01
01
01
01
1 2Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1
2
-
-
o-Terphenyl
Octacosane
8015Method:
HP14Instrument Id:
L17050904Login Number:
SoilMatrix:WG614544Workgroup (AAB#):
Underline = Result out of surrogate limits
26.2 36.2
12.6 9.41
53.4 52.3
30.9 30.4
39.5 34.6
69.6 62.6
69.7 68.2
73.4 74.9
43
25
-
-
136
162
Surrogates Surrogate Limits
DL = surrogate diluted out
HP14CAL ID: -09-MAY-17
ND = surrogate not detected
Page 16
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/17/2017 10:07Report generated5297727PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
Diesel Range (C10-C28) 1000000 1000000 51200 0.384
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
14G67535
WG614544
Instrument ID:HP14
File ID:
Run Date:05/16/2017
Run Time:09:32
Analyst:LJH
Workgroup (AAB#):
8015CMethod:
L17050904Login Number: WG614359-01Sample ID:
09-MAY-17HP14 -Cal ID:
UNITS
ug/kg
UCL20
STDQC Key:
WATERMatrix:
Page 17
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/17/2017 10:07Report generated5297727PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
Diesel Range (C10-C28) 1000000 1040000 53300 4.46
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
14G67546
WG614544
Instrument ID:HP14
File ID:
Run Date:05/16/2017
Run Time:20:59
Analyst:LJH
Workgroup (AAB#):
8015CMethod:
L17050904Login Number: WG614359-02Sample ID:
09-MAY-17HP14 -Cal ID:
UNITS
ug/kg
UCL20
STDQC Key:
WATERMatrix:
Page 18
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Response Factor Report HP14
Method : C:\MSDCHEM\1\METHODS\DROQUANT.M (Chemstation Integrator) Title : SOP:GCS02 8015B/C/D DRO ICAL 05/09/17 Last Update : Tue May 09 14:01:47 2017 WG613451 Calibration Files 10k =14G67512.D 5000 =14G67513.D 2500 =14G67514.D 1000 =14G67515.D 500 =14G67516.D 100 =14G67517.D
Compound 10k 5000 2500 1000 500 100 Avg %RSD -------------------------------------------------------------------------- 1) h Diesel Range (C1 4.697 4.957 4.498 4.973 5.404 6.089 5.103 E4 11.19 2) s O-Terphenyl 5.179 5.829 5.070 5.462 5.901 5.320 5.460 E4 6.25 3) s Octacosane 3.011 4.001 3.424 3.684 3.921 3.732 3.629 E4 10.02 -------------------------------------------------------------------------- (#) = Out of Range
DROQUANT.M Tue May 09 14:42:19 2017
Page 19
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/17/2017 10:07Version 1.5Report generated
5297726PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
Diesel Range (C10-C28) 1000000 1040000 53300ug/L 4.40
Analyte Expected Found
* Exceeds
%D
Limit %D
RF
14G67518
WG613451
Instrument ID:HP14
File ID:
Run Date:05/09/2017
Run Time:14:09
Analyst:LJH
ICal Workgroup:
8015CMethod:
L17050904Login Number: WG613451-07Sample ID:
09-MAY-17HP14 -Cal ID:
QUCL20
Units
QC Key:STD
Page 20
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:82035
Page: 1 Approved: 09-MAY-17
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HP14
LJH
8015 DRO
050917
NA
GCS02 19
Column 1 ID: Column 2 ID:RTX-CLP2 NA
Method: SOP: Rev:8015D OVAP GCS02 1
1
2
3
4
5
6
7
8
9
10
14G67509
14G67510
14G67511
14G67512
14G67513
14G67514
14G67515
14G67516
14G67517
14G67518
RINSE
PRO RT STD
T1005 RT STD
WG613451-01 10,000PPM DRO STD
WG613451-02 5,000PPM DRO STD
WG613451-03 2,500PPM DRO STD
WG613451-04 1,000PPM DRO STD
WG613451-05 500PPM DRO STD
WG613451-06 100PPM DRO STD
WG613451-07 1,000PPM ALT DRO STD
1
1
1
1
1
1
1
1
1
1
STD81451
STD81010
STD81110
STD81110
STD81110
STD81110
STD81110
STD81110
STD81381
05/09/17 08:17
05/09/17 08:56
05/09/17 09:35
05/09/17 10:14
05/09/17 10:53
05/09/17 11:33
05/09/17 12:12
05/09/17 12:51
05/09/17 13:30
05/09/17 14:09
Seq. File ID Sample Information Dil Reference Date/TimeMat
1
1
1
1
1
1
1
1
1
1
NAInternal STD: Surrogate STD: NA
Comments:
WG613451 (ICAL)Workgroups:
Comments
Seq. Rerun Dil. AnalytesReason
Maintenance Log ID:
STD81110 04/10/17Calibration STD
Syringe Filter Lot#:
STD81110CCV STD: LCS STD: MS/MSD STD:
Eluent ID#:
Page 21
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:82172
Page: 1 Approved: 17-MAY-17
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HP14
LJH
8015 DRO
051617
NA
GCS02 19
Column 1 ID: Column 2 ID:RTX-CLP2 NA
Method: SOP: Rev:8015D OVAP GCS02 1
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
14G67533
14G67534
14G67535
14G67536
14G67537
14G67538
14G67539
14G67540
14G67541
14G67542
14G67543
14G67544
14G67545
14G67546
14G67547
14G67548
14G67549
RINSE
PRO RT STD
WG614359-01 1,000PPM DRO STD
WG614301-01 BLANK
WG614301-02 LCS
WG614301-03 LCS2
L17050774-01 DRO
L17050904-03 DRO
L17050904-01 DRO
L17050904-04 DRO
L17050904-05 DRO
L17050904-02 DRO
L17050767-01 DRO
WG614359-02 1,000PPM DRO STD
RINSE
RINSE
RINSE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
STD81451
STD81110
SOIL
SOIL
SOIL
SOIL
SOIL
SOIL
SOIL
SOIL
SOIL
SOIL
STD81110
05/16/17 08:14
05/16/17 08:53
05/16/17 09:32
05/16/17 14:27
05/16/17 15:06
05/16/17 15:45
05/16/17 16:24
05/16/17 17:04
05/16/17 17:43
05/16/17 18:22
05/16/17 19:02
05/16/17 19:41
05/16/17 20:20
05/16/17 20:59
05/16/17 21:38
05/16/17 22:17
05/16/17 22:56
Seq. File ID Sample Information Dil Reference Date/TimeMat
1
1
1
7
7
7
7
7
7
7
7
7
7
1
1
1
1
NAInternal STD: Surrogate STD: NA
Comments:
WG614544Workgroups:
4
9
10
11
12
O-Terphenyl
O-Terphenyl
O-Terphenyl
O-Terphenyl, Octacosane
Surrogate standard failure
Surrogate standard failure
Surrogate standard failure
Surrogate standard failure
WG614301-01 BLANK had a hit in the Diesel Range (C10-C28), but was less than 1/2 the RL.
L17050904-01 DRO
L17050904-04 DRO
L17050904-05 DRO
L17050904-02 DRO needs re-extracted due to both surrogate recoveries being low. QNS-jar broken, not enough sample.
Comments
Seq. Rerun Dil. AnalytesReason
Maintenance Log ID:
STD81110 04/10/17Calibration STD
Syringe Filter Lot#:
STD81110CCV STD: LCS STD: MS/MSD STD:
Eluent ID#:
Page 22
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Sample Extract Log
EXTRACT - Modified 10/22/2008 PDF ID:Report generated: 05/17/2017 09:40
Microbac Laboratories Inc.
5297589
Reviewer:Analyst:
L17050767-01
L17050774-01
L17050904-01
L17050904-02
L17050904-03
L17050904-04
L17050904-05
WG614301-01
WG614301-02
WG614301-03
SAMPLE #
22.51 g
20.26 g
21.25 g
17.32 g
17.55 g
19.09 g
19.39 g
20 g
20 g
20 g
Init Amnt
1 mL
1 mL
1 mL
1 mL
1 mL
1 mL
1 mL
1 mL
1 mL
1 mL
Final Vol Color
Transparent
Transparent
Transparent
Transparent
Transparent
Transparent
Transparent
Transparent
Transparent
Transparent
Type
SAMP
SAMP
SAMP
SAMP
SAMP
SAMP
SAMP
BLANK
LCS
LCS2
WG614301
Method:3546
Analyst:JLD
Workgroup:
Run Date:05/16/2017 11:21
EXMW01-15 Revision SOP:
Spike Witness: JDH
Methylene Chloride Lot #:
sand Lot #:
Diatomaceous Earth Lot #:
Na2SO4, Anhydrous, Granular Lot #:
Prod
DRO
DRO
DRO
DRO
DRO
DRO
DRO
DRO
DRO
DRO
1
2
3
4
5
6
7
8
9
10
Spike Amnt
1 mL
1 mL
STD81081
COA19678
COA19640
COA19577
COA19660
Surr Solution:
Surr Amnt
1 mL
1 mL
1 mL
1 mL
1 mL
1 mL
1 mL
1 mL
1 mL
1 mL
L17050904-05 RAN OUT OF HOLD
JLDSpike Analyst:
Spike Sol
STD81195
STD81195
Reference pH
Due to insufficient sample volume, this preparation batch failed to include the method prescribed MS and MSD.
Page 23
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Page 24
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Page 25
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Internal Chain of Custody Report
Login:
Account:
Project:
Samples:
Due Date:
L17050904
2755
2755.044
5
19-MAY-2017
A1 - Sample Archive (COLD)A2 - Sample Archive (AMBIENT)F1 - Volatiles Freezer in LoginV1 - Volatiles Refrigerator in LoginW1 - Walkin Cooler in Login
Microbac Laboratories Inc.
L17050904-01
L17050904-02
L17050904-03
L17050904-04
909520
909521
909522
909523
Samplenum
Samplenum
Samplenum
Samplenum
Container ID
Container ID
Container ID
Container ID
1
1
1
1
Bottle:
Bottle:
Bottle:
Bottle:
1
2
3
4
1
2
3
4
1
2
3
4
1
2
3
4
LOGIN
PREP
PREP
STORE
LOGIN
PREP
PREP
STORE
LOGIN
PREP
PREP
STORE
LOGIN
PREP
PREP
STORE
COOLER
W1
EXT
DIG
COOLER
W1
EXT
DIG
COOLER
W1
EXT
DIG
COOLER
W1
EXT
DIG
W1
EXT
DIG
A2
W1
EXT
DIG
A2
W1
EXT
DIG
A2
W1
EXT
DIG
A2
16-MAY-2017 11:04
16-MAY-2017 11:07
16-MAY-2017 15:10
16-MAY-2017 16:46
16-MAY-2017 11:04
16-MAY-2017 11:07
16-MAY-2017 15:10
16-MAY-2017 16:46
16-MAY-2017 11:04
16-MAY-2017 11:07
16-MAY-2017 15:10
16-MAY-2017 16:46
16-MAY-2017 11:04
16-MAY-2017 11:07
16-MAY-2017 15:10
16-MAY-2017 16:46
BRG
JDH
AC
BRG
BRG
JDH
AC
BRG
BRG
JDH
AC
BRG
BRG
JDH
AC
BRG
CLS
JLD
AC
CLS
JLD
AC
CLS
JLD
AC
CLS
JLD
AC
Seq.
Seq.
Seq.
Seq.
Purpose
Purpose
Purpose
Purpose
From
From
From
From
To
To
To
To
Date/Time
Date/Time
Date/Time
Date/Time
Accept
Accept
Accept
Accept
Relinquish
Relinquish
Relinquish
Relinquish
Products
Products
Products
Products
DRO
DRO
DRO
DRO
pH
pH
pH
pH
Page 26
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Internal Chain of Custody Report
Login:
Account:
Project:
Samples:
Due Date:
L17050904
2755
2755.044
5
19-MAY-2017
A1 - Sample Archive (COLD)A2 - Sample Archive (AMBIENT)F1 - Volatiles Freezer in LoginV1 - Volatiles Refrigerator in LoginW1 - Walkin Cooler in Login
Microbac Laboratories Inc.
L17050904-05 909524
Samplenum Container ID
1Bottle:
1
2
3
4
LOGIN
PREP
PREP
STORE
COOLER
W1
EXT
DIG
W1
EXT
DIG
A2
16-MAY-2017 11:04
16-MAY-2017 11:07
16-MAY-2017 15:10
16-MAY-2017 16:46
BRG
JDH
AC
BRG
CLS
JLD
AC
Seq. Purpose From To Date/Time Accept Relinquish
Products
DRO
pH
Page 27
L17050904 / Revision: 0 / 27 total pages Generated: 05/18/2017 14:40
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Laboratory Report Number: L17051231 (Preliminary)
Frank ZingalesOhio Environmental Protection Agency2110 East Aurora RoadTwinsburg, OH 44087
Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac’s Ohio Valley Division (OVD). If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed below.
Laboratory Contact:Michelle Taylor – Client Services Specialist(740) 373-4071Michelle.Taylor@microbac.com
I certify that all test results meet all of the requirements of the accrediting authority listed below. All results for soil samples are reported on a 'dry-weight' basis unless specified otherwise. Analytical results for water and wastes are reported on a 'as received' basis unless specified otherwise. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received.
This report was certified on May 25 2017
Leslie Bucina – Managing Director State of Origin: OHAccrediting Authority: N/A ID:OH00218QAPP: Microbac OVD
Microbac Laboratories * Ohio Valley Division158 Starlite Drive, Marietta, OH 45750 * T: (740) 373-4071 F: (740) 373-4835 * www.microbac.com
Page 1
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Record of Sample Receipt and InspectionComments/DiscrepanciesThis is the record of the shipment conditions and the inspection records for the samples received and reported as a sample delivery group (SDG). All of the samples were inspected and observed to conform to our receipt policies, except as noted below.
There were no discrepancies.Discrepancy Resolution
CoolersCooler # Temperature
GunTemperature COC # Airbill # Temp Required?
0016980 I 2.0 X
Inspection Checklist
# Question Result
1 Were shipping coolers sealed? NA
2 Were custody seals intact? NA
3 Were cooler temperatures in range of 0-6? Yes
4 Was ice present? Yes
5 Were COC's received/information complete/signed and dated? Yes
6 Were sample containers intact and match COC? Yes
7 Were sample labels intact and match COC? Yes
8 Were the correct containers and volumes received? Yes
9 Were samples received within EPA hold times? Yes
10 Were correct preservatives used? (water only) NA
11 Were pH ranges acceptable? (voa's excluded) NA
12 Were VOA samples free of headspace (less than 6mm)? NA
Microbac Laboratories ● Ohio Valley Division158 Starlite Drive, Marietta, OH 45750 ● T: (740)373-4071 F: (740)373-4835
www.microbac.com
Page 2
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Samples ReceivedClient ID Laboratory ID Date Collected Date Received
17-0751 OSG DISPOSAL PIT L17051231-01 05/19/2017 13:24 05/19/2017 20:10
17-0751 OSG DISPOSAL PIT L17051231-02 05/19/2017 13:24 05/19/2017 20:10
17-0751 IR MUD ORIGINAL L17051231-03 05/19/2017 15:00 05/19/2017 20:10
17-0751 IR MUD ORIGINAL L17051231-04 05/19/2017 15:00 05/19/2017 20:10
17-0751 IR MUD SILO L17051231-05 05/19/2017 14:45 05/19/2017 20:10
17-0751 IR MUD SILO L17051231-06 05/19/2017 14:45 05/19/2017 20:10
17-0751 IR MUD GRID A3 NEW L17051231-07 05/19/2017 15:30 05/19/2017 20:10
17-0751 IR MUD GRID A3 NEW L17051231-08 05/19/2017 15:30 05/19/2017 20:10
17-0751 WEST BOREHOLE RETURN M
L17051231-09 05/19/2017 16:18 05/19/2017 20:10
17-0751 WEST BOREHOLE RETURN M
L17051231-10 05/19/2017 16:18 05/19/2017 20:10
17-0751 WEST RECLAIMER PIT L17051231-11 05/19/2017 16:30 05/19/2017 20:10
17-0751 WEST RECLAIMER PIT L17051231-12 05/19/2017 16:30 05/19/2017 20:10
17-0751 EAST RECLAIMER NEW MUD
L17051231-13 05/19/2017 17:12 05/19/2017 20:10
17-0751 EAST RECLAIMER NEW MUD
L17051231-14 05/19/2017 17:12 05/19/2017 20:10
Microbac Laboratories ● Ohio Valley Division158 Starlite Drive, Marietta, OH 45750 ● T: (740)373-4071 F: (740)373-4835
www.microbac.com
Page 3
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac LaboratoriesCase Narrative
Login Number: L17051231Department: SemivolatilesAnalyst: Mary Schilling
METHOD
Preparation 3510C/1311/3546
Analysis SW-846 8270C
HOLDING TIMES
Sample Preparation: All holding times were met.
Sample Analysis: All holding times were met.
PREPARATION
Sample preparation proceeded normally.
CALIBRATION
Initial Calibration: For all compounds that yielded a %RSD greater than 15%, linear or higher order equations were applied. All acceptance criteria were met.
Alternate Source Standards: All acceptance criteria were met.
Continuing Calibration and Tune: All acceptance criteria were met.
BATCH QA/QC
Method Blank: Analytes were detected above the applicable reporting limit for the following analytes: Benzoic Acid. Please see the applicable QC report for a detailed presentation of the failures.
Sample # Analyte Date Result Lower Upper Type
WG615091-01 Benzoic Acid 2017-05-23 11:25:00 343 250.0 RL
Laboratory Control Sample: All acceptance criteria were met.
Matrix Spikes: All acceptance criteria were met.
Page 1 of 2 Generated at May 25, 2017 09:33
Page 4
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
SAMPLES
Samples: All acceptance criteria were met.
Internal Standards: All acceptance criteria were met.
Surrogates: All acceptance criteria were met.
Manual Integration Reason Codes
Reason #1: Data System Fails to Select Correct Peak In some cases the chromatography system selects and integrates the 'wrong peak'. In this case the analyst must correct the selection and force the system to integrate the proper peak. Other times the system may miss the peakcompletely.
Reason #2: Data System Splits the Peak Incorrectly or Integrates a False Peak as a Rider Peak This phenomena is common at low concentrations where the signal:noise ratio is low. A single compound (peak) is incorrectly split into multiple peaks or integrated as a main peak with one or more rider peaks resulting in low areacounts for the target compound.
Reason #3: Improperly Integrated Isomers and/or coeluting compounds. This system often fails to distinguish coeluting compounds and or isomers. The integration areas and concentrations are wrong, and they must be corrected by manual integration. Prime examples are benzo(k)fluoranthene andbenzo(b)fluoranthene which are often unresolved and integrated improperly when both are present at low concentrations in standards or samples.
Reason #4: System Establishes Incorrect Baseline There are numerous situations in chromatography where the system establishes the baseline incorrectly. Some baseline errors will be obvious to the analyst and should be corrected via manual procedures.
Reason #5: Miscellaneous Other situations involving integration errors may require in-depth review and technical judgment. These cases should be brought to the attention of the laboratory management. If the form of manual integration is not clearly covered by these four cases, then review and approval by the Managing Director or the QAO will be required.
I certify that this data package is in compliance with the terms and conditions agreed to by the client and Microbac Laboratories Inc., both technically and for completeness, except for the conditions noted above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or designated person, as verified by the following signature.
Narrative ID: 125853Approved By: Mary Schilling
Page 2 of 2 Generated at May 25, 2017 09:33
Page 5
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac LaboratoriesCase Narrative
Login Number: L17051231Department: MetalsAnalyst: Kerri Buck
METHOD
Preparation: SW-846 3015
Analysis: SW-846 6010
HOLDING TIMES
Sample Preparation: All holding times were met.
Sample Analysis: All holding times were met.
PREPARATION
Sample preparation proceeded normally.
CALIBRATION
Initial Calibration: All acceptance criteria were met.
Alternate Source Standards: All acceptance criteria were met.
Interference Check Standards: All acceptance criteria were met.
Continuing Calibration Verification: All acceptance criteria were met.
Continuing Calibration Blank: All acceptance criteria were met.
BATCH QA/QC
Method Blank: All acceptance criteria were met.
Laboratory Control Sample: All acceptance criteria were met.
Serial Dilution/Post Digestion Spikes: WG615308 - All acceptance criteria were met.
Page 1 of 2 Generated at May 24, 2017 12:36
Page 6
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Matrix Spikes: All acceptance criteria were met.
SAMPLES
Samples: All acceptance criteria were met.
Narrative ID: 125811Approved By: Kim Rhodes
Page 2 of 2 Generated at May 24, 2017 12:36
Page 7
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac LaboratoriesCase Narrative
Login Number: L17051231Department: Metals - AAAnalyst: Laura Jones
METHOD
Preparation: SW-846 7470
Analysis: SW-846 7470
HOLDING TIMES
Sample Preparation: All holding times were met.
Sample Analysis: All holding times were met.
PREPARATION
Sample preparation proceeded normally.
CALIBRATION
Initial Calibration: All acceptance criteria were met.
Alternate Source Standards: All acceptance criteria were met.
Interference Check Standards: All acceptance criteria were met.
Continuing Calibration Verification: All acceptance criteria were met.
Continuing Calibration Blank: All acceptance criteria were met.
BATCH QA/QC
Method Blank: All acceptance criteria were met.
Laboratory Control Sample: All acceptance criteria were met.
Serial Dilution/Post Digestion Spikes: WG615315 - All acceptance criteria were met.
Page 1 of 2 Generated at May 24, 2017 12:36
Page 8
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Matrix Spikes: All acceptance criteria were met.
SAMPLES
Samples: All acceptance criteria were met.
Narrative ID: 125806Approved By: Kim Rhodes
Page 2 of 2 Generated at May 24, 2017 12:36
Page 9
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisSample #: L17051231-02 PrePrep Method: N/A Instrument: HPMS9
Client ID: 17-0751 OSG DISPOSAL PIT Prep Method: 5030B/5030C/5035A Prep Date: 05/23/2017 09:14
Matrix: Soil Analytical Method: 8260B Cal Date: 05/23/2017 14:46
Workgroup #: WG615352 Analyst: ADC Run Date: 05/23/2017 20:47
Collect Date: 05/19/2017 13:24 Dilution: 1 File ID: 9M980452
Sample Tag: 01 Units: ug/kg Percent Solid: 50.0
Analyte CAS # Result Qual RL MDL
Acetone 67-64-1 U 19.4 9.68
Benzene 71-43-2 5.32 J 9.68 0.968
Bromobenzene 108-86-1 U 9.68 0.968
Bromochloromethane 74-97-5 U 9.68 1.94
Bromodichloromethane 75-27-4 U 9.68 0.968
Bromoform 75-25-2 U 9.68 0.968
Bromomethane 74-83-9 U 19.4 1.94
2-Butanone 78-93-3 U 19.4 4.84
n-Butylbenzene 104-51-8 20.0 9.68 0.968
sec-Butylbenzene 135-98-8 6.38 J 9.68 0.968
tert-Butylbenzene 98-06-6 3.66 J 9.68 0.968
Carbon disulfide 75-15-0 4.53 J 9.68 0.968
Carbon tetrachloride 56-23-5 U 9.68 0.968
Chlorobenzene 108-90-7 U 9.68 0.968
Chlorodibromomethane 124-48-1 U 9.68 0.968
Chloroethane 75-00-3 U 19.4 1.94
2-Chloroethyl vinyl ether 110-75-8 U 19.4 3.87
Chloroform 67-66-3 U 9.68 0.968
Chloromethane 74-87-3 U 19.4 3.87
2-Chlorotoluene 95-49-8 U 9.68 0.968
4-Chlorotoluene 106-43-4 U 9.68 0.968
1,2-Dibromo-3-chloropropane 96-12-8 U 9.68 3.87
1,2-Dibromoethane 106-93-4 U 9.68 0.968
Dibromomethane 74-95-3 U 9.68 0.968
1,2-Dichlorobenzene 95-50-1 U 9.68 0.968
1,3-Dichlorobenzene 541-73-1 U 9.68 0.968
1,4-Dichlorobenzene 106-46-7 U 9.68 0.968
Dichlorodifluoromethane 75-71-8 U 19.4 1.94
1,1-Dichloroethane 75-34-3 U 9.68 1.94
1,2-Dichloroethane 107-06-2 U 9.68 0.968
1,1-Dichloroethene 75-35-4 U 9.68 0.968
cis-1,2-Dichloroethene 156-59-2 U 9.68 0.968
trans-1,2-Dichloroethene 156-60-5 U 9.68 0.968
Page 1 of 30 Generated at May 25, 2017 09:36
Page 10
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
1,2-Dichloropropane 78-87-5 U 9.68 0.968
1,3-Dichloropropane 142-28-9 U 9.68 0.968
2,2-Dichloropropane 594-20-7 U 9.68 0.968
cis-1,3-Dichloropropene 10061-01-5 U 9.68 0.968
trans-1,3-Dichloropropene 10061-02-6 U 9.68 0.968
1,1-Dichloropropene 563-58-6 U 9.68 0.968
Ethylbenzene 100-41-4 5.91 J 9.68 0.968
2-Hexanone 591-78-6 45.8 19.4 4.84
Hexachlorobutadiene 87-68-3 U 9.68 0.968
Isopropylbenzene 98-82-8 3.50 J 9.68 0.968
p-Isopropyltoluene 99-87-6 9.17 J 9.68 0.968
4-Methyl-2-pentanone 108-10-1 U 19.4 4.84
Methylene chloride 75-09-2 U 9.68 1.94
Naphthalene 91-20-3 11.0 J 19.4 0.968
n-Propylbenzene 103-65-1 6.84 J 9.68 0.968
Styrene 100-42-5 U 9.68 0.968
1,1,1,2-Tetrachloroethane 630-20-6 U 9.68 0.968
1,1,2,2-Tetrachloroethane 79-34-5 U 9.68 0.968
Tetrachloroethene 127-18-4 3.54 J 9.68 0.968
Toluene 108-88-3 16.3 9.68 0.968
1,2,3-Trichlorobenzene 87-61-6 15.7 9.68 0.968
1,2,4-Trichlorobenzene 120-82-1 U 9.68 0.968
1,1,1-Trichloroethane 71-55-6 U 9.68 0.968
1,1,2-Trichloroethane 79-00-5 U 9.68 0.968
Trichloroethene 79-01-6 U 9.68 0.968
Trichlorofluoromethane 75-69-4 U 19.4 1.94
1,2,3-Trichloropropane 96-18-4 U 9.68 1.94
1,2,4-Trimethylbenzene 95-63-6 28.7 9.68 0.968
1,3,5-Trimethylbenzene 108-67-8 72.6 9.68 0.968
Vinyl acetate 108-05-4 U 19.4 4.84
Vinyl chloride 75-01-4 U 19.4 1.94
o-Xylene 95-47-6 29.2 9.68 0.968
m-,p-Xylene 179601-23-1 23.0 9.68 0.968
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 100 80 120
1,2-Dichloroethane-d4 99.1 80 120
Toluene-d8 115 81 117
4-Bromofluorobenzene 150 74 121 *
* Surrogate or spike compound out of range
Page 2 of 30 Generated at May 25, 2017 09:36
Page 11
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisJ The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-02 PrePrep Method: N/A Instrument: HPMS12
Client ID: 17-0751 OSG DISPOSAL PIT Prep Method: 3546 Prep Date: 05/22/2017 11:48
Matrix: Soil Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615227 Analyst: SCB Run Date: 05/23/2017 15:49
Collect Date: 05/19/2017 13:24 Dilution: 1 File ID: 12M62307
Sample Tag: 01 Units: ug/kg Percent Solid: 50.0
Analyte CAS # Result Qual RL MDL
1,2,4-Trichlorobenzene 120-82-1 U 351 175
1,2-Dichlorobenzene 95-50-1 U 351 175
1,3-Dichlorobenzene 541-73-1 U 351 175
1,4-Dichlorobenzene 106-46-7 U 351 175
2,4,5-Trichlorophenol 95-95-4 U 351 175
2,4,6-Trichlorophenol 88-06-2 U 351 175
2,4-Dichlorophenol 120-83-2 U 351 175
2,4-Dimethylphenol 105-67-9 U 351 175
2,4-Dinitrophenol 51-28-5 U 1750 875
2,4-Dinitrotoluene 121-14-2 U 351 175
2,6-Dinitrotoluene 606-20-2 U 351 175
2-Chloronaphthalene 91-58-7 U 351 175
2-Chlorophenol 95-57-8 U 351 175
2-Methylnaphthalene 91-57-6 497 351 175
2-Methylphenol 95-48-7 U 351 175
2-Nitroaniline 88-74-4 U 1750 875
2-Nitrophenol 88-75-5 U 351 175
3,3'-Dichlorobenzidine 91-94-1 U 701 351
3-,4-Methylphenol 65794-96-9 U 351 175
3-Nitroaniline 99-09-2 U 1750 875
4,6-Dinitro-2-methylphenol 534-52-1 U 1750 875
4-Bromophenyl-phenylether 101-55-3 U 351 175
4-Chloro-3-methylphenol 59-50-7 U 351 175
4-Chloroaniline 106-47-8 U 351 175
4-Chlorophenyl-phenyl ether 7005-72-3 U 351 175
4-Nitroaniline 100-01-6 U 1750 875
4-Nitrophenol 100-02-7 U 1750 875
Acenaphthene 83-32-9 U 351 175
Acenaphthylene 208-96-8 U 351 175
Anthracene 120-12-7 U 351 175
Page 3 of 30 Generated at May 25, 2017 09:36
Page 12
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Benzo(a)anthracene 56-55-3 U 351 175
Benzo(a)pyrene 50-32-8 U 351 175
Benzo(b)fluoranthene 205-99-2 U 351 175
Benzo(g,h,i)Perylene 191-24-2 U 351 175
Benzo(k)fluoranthene 207-08-9 U 351 175
Benzoic acid 65-85-0 U 10600 701
Benzyl alcohol 100-51-6 U 351 175
Bis(2-Chloroethoxy)Methane 111-91-1 U 351 175
Bis(2-Chloroethyl)ether 111-44-4 U 351 175
bis(2-Chloroisopropyl)ether 39638-32-9 U 351 175
bis(2-Ethylhexyl)phthalate 117-81-7 U 351 175
Butylbenzylphthalate 85-68-7 U 351 175
Chrysene 218-01-9 U 351 175
Di-N-Butylphthalate 84-74-2 U 351 175
Di-n-octylphthalate 117-84-0 U 351 175
Dibenzo(a,h)Anthracene 53-70-3 U 351 175
Dibenzofuran 132-64-9 U 351 175
Diethylphthalate 84-66-2 U 351 175
Dimethylphthalate 131-11-3 U 351 175
Fluoranthene 206-44-0 U 351 175
Fluorene 86-73-7 U 351 175
Hexachlorobenzene 118-74-1 U 351 175
Hexachlorobutadiene 87-68-3 U 351 175
Hexachlorocyclopentadiene 77-47-4 U 1590 797
Hexachloroethane 67-72-1 U 351 175
Indeno(1,2,3-cd)pyrene 193-39-5 U 351 175
Isophorone 78-59-1 U 351 175
Diphenylamine/n-Nitrosodiphenylamine 86-30-6 755 351 175
N-Nitrosodipropylamine 621-64-7 U 351 175
Naphthalene 91-20-3 372 351 175
Nitrobenzene 98-95-3 U 351 175
Pentachlorophenol 87-86-5 U 1750 875
Phenanthrene 85-01-8 193 J 351 175
Phenol 108-95-2 U 351 175
Pyrene 129-00-0 U 351 175
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 101 19 122
2-Fluorobiphenyl 77.8 30 115
2-Fluorophenol 67.6 25 121
Page 4 of 30 Generated at May 25, 2017 09:36
Page 13
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisNitrobenzene-d5 86.7 23 120
p-Terphenyl-d14 92.1 18 137
Phenol-d5 69.3 24 113
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-04 PrePrep Method: N/A Instrument: HPMS9
Client ID: 17-0751 IR MUD ORIGINAL Prep Method: 5030B/5030C/5035A Prep Date: 05/23/2017 09:15
Matrix: Soil Analytical Method: 8260B Cal Date: 05/23/2017 14:46
Workgroup #: WG615352 Analyst: ADC Run Date: 05/23/2017 17:46
Collect Date: 05/19/2017 15:00 Dilution: 1 File ID: 9M980446
Sample Tag: 01 Units: ug/kg Percent Solid: 45.2
Analyte CAS # Result Qual RL MDL
Acetone 67-64-1 23.9 22.1 11.1
Benzene 71-43-2 3.16 J 11.1 1.11
Bromobenzene 108-86-1 U 11.1 1.11
Bromochloromethane 74-97-5 U 11.1 2.21
Bromodichloromethane 75-27-4 U 11.1 1.11
Bromoform 75-25-2 U 11.1 1.11
Bromomethane 74-83-9 U 22.1 2.21
2-Butanone 78-93-3 U 22.1 5.53
n-Butylbenzene 104-51-8 1.44 J 11.1 1.11
sec-Butylbenzene 135-98-8 U 11.1 1.11
tert-Butylbenzene 98-06-6 U 11.1 1.11
Carbon disulfide 75-15-0 8.31 J 11.1 1.11
Carbon tetrachloride 56-23-5 U 11.1 1.11
Chlorobenzene 108-90-7 U 11.1 1.11
Chlorodibromomethane 124-48-1 U 11.1 1.11
Chloroethane 75-00-3 U 22.1 2.21
2-Chloroethyl vinyl ether 110-75-8 U 22.1 4.43
Chloroform 67-66-3 U 11.1 1.11
Chloromethane 74-87-3 U 22.1 4.43
2-Chlorotoluene 95-49-8 U 11.1 1.11
4-Chlorotoluene 106-43-4 U 11.1 1.11
1,2-Dibromo-3-chloropropane 96-12-8 U 11.1 4.43
1,2-Dibromoethane 106-93-4 U 11.1 1.11
Dibromomethane 74-95-3 U 11.1 1.11
1,2-Dichlorobenzene 95-50-1 U 11.1 1.11
1,3-Dichlorobenzene 541-73-1 U 11.1 1.11
1,4-Dichlorobenzene 106-46-7 U 11.1 1.11
Page 5 of 30 Generated at May 25, 2017 09:36
Page 14
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Dichlorodifluoromethane 75-71-8 U 22.1 2.21
1,1-Dichloroethane 75-34-3 U 11.1 2.21
1,2-Dichloroethane 107-06-2 U 11.1 1.11
1,1-Dichloroethene 75-35-4 U 11.1 1.11
cis-1,2-Dichloroethene 156-59-2 U 11.1 1.11
trans-1,2-Dichloroethene 156-60-5 U 11.1 1.11
1,2-Dichloropropane 78-87-5 U 11.1 1.11
1,3-Dichloropropane 142-28-9 U 11.1 1.11
2,2-Dichloropropane 594-20-7 U 11.1 1.11
cis-1,3-Dichloropropene 10061-01-5 U 11.1 1.11
trans-1,3-Dichloropropene 10061-02-6 U 11.1 1.11
1,1-Dichloropropene 563-58-6 U 11.1 1.11
Ethylbenzene 100-41-4 2.42 J 11.1 1.11
2-Hexanone 591-78-6 U 22.1 5.53
Hexachlorobutadiene 87-68-3 U 11.1 1.11
Isopropylbenzene 98-82-8 U 11.1 1.11
p-Isopropyltoluene 99-87-6 U 11.1 1.11
4-Methyl-2-pentanone 108-10-1 U 22.1 5.53
Methylene chloride 75-09-2 U 11.1 2.21
Naphthalene 91-20-3 4.18 J 22.1 1.11
n-Propylbenzene 103-65-1 U 11.1 1.11
Styrene 100-42-5 U 11.1 1.11
1,1,1,2-Tetrachloroethane 630-20-6 U 11.1 1.11
1,1,2,2-Tetrachloroethane 79-34-5 U 11.1 1.11
Tetrachloroethene 127-18-4 9.55 J 11.1 1.11
Toluene 108-88-3 6.40 J 11.1 1.11
1,2,3-Trichlorobenzene 87-61-6 2.10 J 11.1 1.11
1,2,4-Trichlorobenzene 120-82-1 1.28 J 11.1 1.11
1,1,1-Trichloroethane 71-55-6 U 11.1 1.11
1,1,2-Trichloroethane 79-00-5 U 11.1 1.11
Trichloroethene 79-01-6 U 11.1 1.11
Trichlorofluoromethane 75-69-4 U 22.1 2.21
1,2,3-Trichloropropane 96-18-4 U 11.1 2.21
1,2,4-Trimethylbenzene 95-63-6 5.53 J 11.1 1.11
1,3,5-Trimethylbenzene 108-67-8 2.69 J 11.1 1.11
Vinyl acetate 108-05-4 U 22.1 5.53
Vinyl chloride 75-01-4 U 22.1 2.21
o-Xylene 95-47-6 4.26 J 11.1 1.11
m-,p-Xylene 179601-23-1 7.99 J 11.1 1.11
Page 6 of 30 Generated at May 25, 2017 09:36
Page 15
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisSurrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 102 80 120
1,2-Dichloroethane-d4 100 80 120
Toluene-d8 113 81 117
4-Bromofluorobenzene 127 74 121 *
* Surrogate or spike compound out of range
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-04 PrePrep Method: N/A Instrument: HPMS12
Client ID: 17-0751 IR MUD ORIGINAL Prep Method: 3546 Prep Date: 05/22/2017 11:48
Matrix: Soil Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615227 Analyst: SCB Run Date: 05/23/2017 13:03
Collect Date: 05/19/2017 15:00 Dilution: 1 File ID: 12M62302
Sample Tag: 01 Units: ug/kg Percent Solid: 45.2
Analyte CAS # Result Qual RL MDL
1,2,4-Trichlorobenzene 120-82-1 U 345 172
1,2-Dichlorobenzene 95-50-1 U 345 172
1,3-Dichlorobenzene 541-73-1 U 345 172
1,4-Dichlorobenzene 106-46-7 U 345 172
2,4,5-Trichlorophenol 95-95-4 U 345 172
2,4,6-Trichlorophenol 88-06-2 U 345 172
2,4-Dichlorophenol 120-83-2 U 345 172
2,4-Dimethylphenol 105-67-9 U 345 172
2,4-Dinitrophenol 51-28-5 U 1720 861
2,4-Dinitrotoluene 121-14-2 U 345 172
2,6-Dinitrotoluene 606-20-2 U 345 172
2-Chloronaphthalene 91-58-7 U 345 172
2-Chlorophenol 95-57-8 U 345 172
2-Methylnaphthalene 91-57-6 U 345 172
2-Methylphenol 95-48-7 U 345 172
2-Nitroaniline 88-74-4 U 1720 861
2-Nitrophenol 88-75-5 U 345 172
3,3'-Dichlorobenzidine 91-94-1 U 690 345
3-,4-Methylphenol 65794-96-9 U 345 172
3-Nitroaniline 99-09-2 U 1720 861
4,6-Dinitro-2-methylphenol 534-52-1 U 1720 861
4-Bromophenyl-phenylether 101-55-3 U 345 172
4-Chloro-3-methylphenol 59-50-7 U 345 172
4-Chloroaniline 106-47-8 U 345 172
Page 7 of 30 Generated at May 25, 2017 09:36
Page 16
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
4-Chlorophenyl-phenyl ether 7005-72-3 U 345 172
4-Nitroaniline 100-01-6 U 1720 861
4-Nitrophenol 100-02-7 U 1720 861
Acenaphthene 83-32-9 U 345 172
Acenaphthylene 208-96-8 U 345 172
Anthracene 120-12-7 U 345 172
Benzo(a)anthracene 56-55-3 U 345 172
Benzo(a)pyrene 50-32-8 U 345 172
Benzo(b)fluoranthene 205-99-2 U 345 172
Benzo(g,h,i)Perylene 191-24-2 U 345 172
Benzo(k)fluoranthene 207-08-9 U 345 172
Benzoic acid 65-85-0 U 10500 690
Benzyl alcohol 100-51-6 U 345 172
Bis(2-Chloroethoxy)Methane 111-91-1 U 345 172
Bis(2-Chloroethyl)ether 111-44-4 U 345 172
bis(2-Chloroisopropyl)ether 39638-32-9 U 345 172
bis(2-Ethylhexyl)phthalate 117-81-7 U 345 172
Butylbenzylphthalate 85-68-7 U 345 172
Chrysene 218-01-9 U 345 172
Di-N-Butylphthalate 84-74-2 U 345 172
Di-n-octylphthalate 117-84-0 U 345 172
Dibenzo(a,h)Anthracene 53-70-3 U 345 172
Dibenzofuran 132-64-9 U 345 172
Diethylphthalate 84-66-2 U 345 172
Dimethylphthalate 131-11-3 U 345 172
Fluoranthene 206-44-0 U 345 172
Fluorene 86-73-7 U 345 172
Hexachlorobenzene 118-74-1 U 345 172
Hexachlorobutadiene 87-68-3 U 345 172
Hexachlorocyclopentadiene 77-47-4 U 1570 784
Hexachloroethane 67-72-1 U 345 172
Indeno(1,2,3-cd)pyrene 193-39-5 U 345 172
Isophorone 78-59-1 U 345 172
Diphenylamine/n-Nitrosodiphenylamine 86-30-6 U 345 172
N-Nitrosodipropylamine 621-64-7 U 345 172
Naphthalene 91-20-3 U 345 172
Nitrobenzene 98-95-3 U 345 172
Pentachlorophenol 87-86-5 U 1720 861
Phenanthrene 85-01-8 U 345 172
Page 8 of 30 Generated at May 25, 2017 09:36
Page 17
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Phenol 108-95-2 U 345 172
Pyrene 129-00-0 U 345 172
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 85.5 19 122
2-Fluorobiphenyl 84.2 30 115
2-Fluorophenol 69.3 25 121
Nitrobenzene-d5 89.2 23 120
p-Terphenyl-d14 80.3 18 137
Phenol-d5 67.6 24 113
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-06 PrePrep Method: N/A Instrument: HPMS9
Client ID: 17-0751 IR MUD SILO Prep Method: 5030B/5030C/5035A Prep Date: 05/23/2017 09:20
Matrix: Soil Analytical Method: 8260B Cal Date: 05/23/2017 14:46
Workgroup #: WG615352 Analyst: ADC Run Date: 05/23/2017 18:16
Collect Date: 05/19/2017 14:45 Dilution: 1 File ID: 9M980447
Sample Tag: 01 Units: ug/kg Percent Solid: 49.0
Analyte CAS # Result Qual RL MDL
Acetone 67-64-1 88.2 20.5 10.2
Benzene 71-43-2 2.22 J 10.2 1.02
Bromobenzene 108-86-1 U 10.2 1.02
Bromochloromethane 74-97-5 U 10.2 2.05
Bromodichloromethane 75-27-4 U 10.2 1.02
Bromoform 75-25-2 U 10.2 1.02
Bromomethane 74-83-9 U 20.5 2.05
2-Butanone 78-93-3 19.9 J 20.5 5.12
n-Butylbenzene 104-51-8 14.5 10.2 1.02
sec-Butylbenzene 135-98-8 4.36 J 10.2 1.02
tert-Butylbenzene 98-06-6 U 10.2 1.02
Carbon disulfide 75-15-0 10.8 10.2 1.02
Carbon tetrachloride 56-23-5 U 10.2 1.02
Chlorobenzene 108-90-7 U 10.2 1.02
Chlorodibromomethane 124-48-1 U 10.2 1.02
Chloroethane 75-00-3 U 20.5 2.05
2-Chloroethyl vinyl ether 110-75-8 U 20.5 4.10
Chloroform 67-66-3 U 10.2 1.02
Chloromethane 74-87-3 U 20.5 4.10
2-Chlorotoluene 95-49-8 U 10.2 1.02
4-Chlorotoluene 106-43-4 U 10.2 1.02
Page 9 of 30 Generated at May 25, 2017 09:36
Page 18
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
1,2-Dibromo-3-chloropropane 96-12-8 U 10.2 4.10
1,2-Dibromoethane 106-93-4 U 10.2 1.02
Dibromomethane 74-95-3 U 10.2 1.02
1,2-Dichlorobenzene 95-50-1 U 10.2 1.02
1,3-Dichlorobenzene 541-73-1 U 10.2 1.02
1,4-Dichlorobenzene 106-46-7 U 10.2 1.02
Dichlorodifluoromethane 75-71-8 U 20.5 2.05
1,1-Dichloroethane 75-34-3 U 10.2 2.05
1,2-Dichloroethane 107-06-2 U 10.2 1.02
1,1-Dichloroethene 75-35-4 U 10.2 1.02
cis-1,2-Dichloroethene 156-59-2 U 10.2 1.02
trans-1,2-Dichloroethene 156-60-5 U 10.2 1.02
1,2-Dichloropropane 78-87-5 U 10.2 1.02
1,3-Dichloropropane 142-28-9 U 10.2 1.02
2,2-Dichloropropane 594-20-7 U 10.2 1.02
cis-1,3-Dichloropropene 10061-01-5 U 10.2 1.02
trans-1,3-Dichloropropene 10061-02-6 U 10.2 1.02
1,1-Dichloropropene 563-58-6 U 10.2 1.02
Ethylbenzene 100-41-4 4.50 J 10.2 1.02
2-Hexanone 591-78-6 U 20.5 5.12
Hexachlorobutadiene 87-68-3 U 10.2 1.02
Isopropylbenzene 98-82-8 1.95 J 10.2 1.02
p-Isopropyltoluene 99-87-6 4.77 J 10.2 1.02
4-Methyl-2-pentanone 108-10-1 U 20.5 5.12
Methylene chloride 75-09-2 U 10.2 2.05
Naphthalene 91-20-3 10.8 J 20.5 1.02
n-Propylbenzene 103-65-1 4.73 J 10.2 1.02
Styrene 100-42-5 U 10.2 1.02
1,1,1,2-Tetrachloroethane 630-20-6 U 10.2 1.02
1,1,2,2-Tetrachloroethane 79-34-5 U 10.2 1.02
Tetrachloroethene 127-18-4 2.36 J 10.2 1.02
Toluene 108-88-3 9.84 J 10.2 1.02
1,2,3-Trichlorobenzene 87-61-6 3.20 J 10.2 1.02
1,2,4-Trichlorobenzene 120-82-1 U 10.2 1.02
1,1,1-Trichloroethane 71-55-6 U 10.2 1.02
1,1,2-Trichloroethane 79-00-5 U 10.2 1.02
Trichloroethene 79-01-6 U 10.2 1.02
Trichlorofluoromethane 75-69-4 U 20.5 2.05
1,2,3-Trichloropropane 96-18-4 U 10.2 2.05
Page 10 of 30 Generated at May 25, 2017 09:36
Page 19
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
1,2,4-Trimethylbenzene 95-63-6 40.5 10.2 1.02
1,3,5-Trimethylbenzene 108-67-8 28.1 10.2 1.02
Vinyl acetate 108-05-4 U 20.5 5.12
Vinyl chloride 75-01-4 U 20.5 2.05
o-Xylene 95-47-6 13.3 10.2 1.02
m-,p-Xylene 179601-23-1 15.5 10.2 1.02
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 99.2 80 120
1,2-Dichloroethane-d4 96.0 80 120
Toluene-d8 108 81 117
4-Bromofluorobenzene 118 74 121
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-06 PrePrep Method: N/A Instrument: HPMS12
Client ID: 17-0751 IR MUD SILO Prep Method: 3546 Prep Date: 05/22/2017 11:48
Matrix: Soil Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615227 Analyst: SCB Run Date: 05/23/2017 14:10
Collect Date: 05/19/2017 14:45 Dilution: 1 File ID: 12M62304
Sample Tag: 01 Units: ug/kg Percent Solid: 49.0
Analyte CAS # Result Qual RL MDL
1,2,4-Trichlorobenzene 120-82-1 U 356 178
1,2-Dichlorobenzene 95-50-1 U 356 178
1,3-Dichlorobenzene 541-73-1 U 356 178
1,4-Dichlorobenzene 106-46-7 U 356 178
2,4,5-Trichlorophenol 95-95-4 U 356 178
2,4,6-Trichlorophenol 88-06-2 U 356 178
2,4-Dichlorophenol 120-83-2 U 356 178
2,4-Dimethylphenol 105-67-9 U 356 178
2,4-Dinitrophenol 51-28-5 U 1780 889
2,4-Dinitrotoluene 121-14-2 U 356 178
2,6-Dinitrotoluene 606-20-2 U 356 178
2-Chloronaphthalene 91-58-7 U 356 178
2-Chlorophenol 95-57-8 U 356 178
2-Methylnaphthalene 91-57-6 718 356 178
2-Methylphenol 95-48-7 U 356 178
2-Nitroaniline 88-74-4 U 1780 889
2-Nitrophenol 88-75-5 U 356 178
3,3'-Dichlorobenzidine 91-94-1 U 712 356
Page 11 of 30 Generated at May 25, 2017 09:36
Page 20
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
3-,4-Methylphenol 65794-96-9 U 356 178
3-Nitroaniline 99-09-2 U 1780 889
4,6-Dinitro-2-methylphenol 534-52-1 U 1780 889
4-Bromophenyl-phenylether 101-55-3 U 356 178
4-Chloro-3-methylphenol 59-50-7 U 356 178
4-Chloroaniline 106-47-8 U 356 178
4-Chlorophenyl-phenyl ether 7005-72-3 U 356 178
4-Nitroaniline 100-01-6 U 1780 889
4-Nitrophenol 100-02-7 U 1780 889
Acenaphthene 83-32-9 U 356 178
Acenaphthylene 208-96-8 U 356 178
Anthracene 120-12-7 U 356 178
Benzo(a)anthracene 56-55-3 U 356 178
Benzo(a)pyrene 50-32-8 U 356 178
Benzo(b)fluoranthene 205-99-2 U 356 178
Benzo(g,h,i)Perylene 191-24-2 U 356 178
Benzo(k)fluoranthene 207-08-9 U 356 178
Benzoic acid 65-85-0 U 10800 712
Benzyl alcohol 100-51-6 U 356 178
Bis(2-Chloroethoxy)Methane 111-91-1 U 356 178
Bis(2-Chloroethyl)ether 111-44-4 U 356 178
bis(2-Chloroisopropyl)ether 39638-32-9 U 356 178
bis(2-Ethylhexyl)phthalate 117-81-7 U 356 178
Butylbenzylphthalate 85-68-7 U 356 178
Chrysene 218-01-9 U 356 178
Di-N-Butylphthalate 84-74-2 U 356 178
Di-n-octylphthalate 117-84-0 U 356 178
Dibenzo(a,h)Anthracene 53-70-3 U 356 178
Dibenzofuran 132-64-9 U 356 178
Diethylphthalate 84-66-2 U 356 178
Dimethylphthalate 131-11-3 U 356 178
Fluoranthene 206-44-0 U 356 178
Fluorene 86-73-7 U 356 178
Hexachlorobenzene 118-74-1 U 356 178
Hexachlorobutadiene 87-68-3 U 356 178
Hexachlorocyclopentadiene 77-47-4 U 1620 809
Hexachloroethane 67-72-1 U 356 178
Indeno(1,2,3-cd)pyrene 193-39-5 U 356 178
Isophorone 78-59-1 U 356 178
Page 12 of 30 Generated at May 25, 2017 09:36
Page 21
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Diphenylamine/n-Nitrosodiphenylamine 86-30-6 U 356 178
N-Nitrosodipropylamine 621-64-7 U 356 178
Naphthalene 91-20-3 466 356 178
Nitrobenzene 98-95-3 U 356 178
Pentachlorophenol 87-86-5 U 1780 889
Phenanthrene 85-01-8 263 J 356 178
Phenol 108-95-2 U 356 178
Pyrene 129-00-0 U 356 178
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 91.0 19 122
2-Fluorobiphenyl 83.7 30 115
2-Fluorophenol 66.8 25 121
Nitrobenzene-d5 86.5 23 120
p-Terphenyl-d14 76.4 18 137
Phenol-d5 65.4 24 113
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-08 PrePrep Method: N/A Instrument: HPMS9
Client ID: 17-0751 IR MUD GRID A3 NEW
Prep Method: 5030B/5030C/5035A Prep Date: 05/23/2017 09:22
Matrix: Soil Analytical Method: 8260B Cal Date: 05/23/2017 14:46
Workgroup #: WG615352 Analyst: ADC Run Date: 05/23/2017 18:47
Collect Date: 05/19/2017 15:30 Dilution: 1 File ID: 9M980448
Sample Tag: 01 Units: ug/kg Percent Solid: 26.5
Analyte CAS # Result Qual RL MDL
Acetone 67-64-1 64.1 37.4 18.7
Benzene 71-43-2 U 18.7 1.87
Bromobenzene 108-86-1 U 18.7 1.87
Bromochloromethane 74-97-5 U 18.7 3.74
Bromodichloromethane 75-27-4 U 18.7 1.87
Bromoform 75-25-2 U 18.7 1.87
Bromomethane 74-83-9 U 37.4 3.74
2-Butanone 78-93-3 U 37.4 9.36
n-Butylbenzene 104-51-8 6.81 J 18.7 1.87
sec-Butylbenzene 135-98-8 2.21 J 18.7 1.87
tert-Butylbenzene 98-06-6 U 18.7 1.87
Carbon disulfide 75-15-0 11.6 J 18.7 1.87
Carbon tetrachloride 56-23-5 U 18.7 1.87
Page 13 of 30 Generated at May 25, 2017 09:36
Page 22
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Chlorobenzene 108-90-7 U 18.7 1.87
Chlorodibromomethane 124-48-1 U 18.7 1.87
Chloroethane 75-00-3 U 37.4 3.74
2-Chloroethyl vinyl ether 110-75-8 U 37.4 7.48
Chloroform 67-66-3 U 18.7 1.87
Chloromethane 74-87-3 U 37.4 7.48
2-Chlorotoluene 95-49-8 U 18.7 1.87
4-Chlorotoluene 106-43-4 U 18.7 1.87
1,2-Dibromo-3-chloropropane 96-12-8 U 18.7 7.48
1,2-Dibromoethane 106-93-4 U 18.7 1.87
Dibromomethane 74-95-3 U 18.7 1.87
1,2-Dichlorobenzene 95-50-1 U 18.7 1.87
1,3-Dichlorobenzene 541-73-1 U 18.7 1.87
1,4-Dichlorobenzene 106-46-7 U 18.7 1.87
Dichlorodifluoromethane 75-71-8 U 37.4 3.74
1,1-Dichloroethane 75-34-3 U 18.7 3.74
1,2-Dichloroethane 107-06-2 U 18.7 1.87
1,1-Dichloroethene 75-35-4 U 18.7 1.87
cis-1,2-Dichloroethene 156-59-2 U 18.7 1.87
trans-1,2-Dichloroethene 156-60-5 U 18.7 1.87
1,2-Dichloropropane 78-87-5 U 18.7 1.87
1,3-Dichloropropane 142-28-9 U 18.7 1.87
2,2-Dichloropropane 594-20-7 U 18.7 1.87
cis-1,3-Dichloropropene 10061-01-5 U 18.7 1.87
trans-1,3-Dichloropropene 10061-02-6 U 18.7 1.87
1,1-Dichloropropene 563-58-6 U 18.7 1.87
Ethylbenzene 100-41-4 4.07 J 18.7 1.87
2-Hexanone 591-78-6 U 37.4 9.36
Hexachlorobutadiene 87-68-3 U 18.7 1.87
Isopropylbenzene 98-82-8 2.21 J 18.7 1.87
p-Isopropyltoluene 99-87-6 2.82 J 18.7 1.87
4-Methyl-2-pentanone 108-10-1 U 37.4 9.36
Methylene chloride 75-09-2 U 18.7 3.74
Naphthalene 91-20-3 5.16 J 37.4 1.87
n-Propylbenzene 103-65-1 2.69 J 18.7 1.87
Styrene 100-42-5 U 18.7 1.87
1,1,1,2-Tetrachloroethane 630-20-6 U 18.7 1.87
1,1,2,2-Tetrachloroethane 79-34-5 U 18.7 1.87
Tetrachloroethene 127-18-4 3.81 J 18.7 1.87
Page 14 of 30 Generated at May 25, 2017 09:36
Page 23
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Toluene 108-88-3 7.46 J 18.7 1.87
1,2,3-Trichlorobenzene 87-61-6 U 18.7 1.87
1,2,4-Trichlorobenzene 120-82-1 U 18.7 1.87
1,1,1-Trichloroethane 71-55-6 U 18.7 1.87
1,1,2-Trichloroethane 79-00-5 U 18.7 1.87
Trichloroethene 79-01-6 U 18.7 1.87
Trichlorofluoromethane 75-69-4 U 37.4 3.74
1,2,3-Trichloropropane 96-18-4 U 18.7 3.74
1,2,4-Trimethylbenzene 95-63-6 15.6 J 18.7 1.87
1,3,5-Trimethylbenzene 108-67-8 9.22 J 18.7 1.87
Vinyl acetate 108-05-4 U 37.4 9.36
Vinyl chloride 75-01-4 U 37.4 3.74
o-Xylene 95-47-6 6.89 J 18.7 1.87
m-,p-Xylene 179601-23-1 8.61 J 18.7 1.87
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 100 80 120
1,2-Dichloroethane-d4 93.4 80 120
Toluene-d8 110 81 117
4-Bromofluorobenzene 117 74 121
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-08 PrePrep Method: N/A Instrument: HPMS12
Client ID: 17-0751 IR MUD GRID A3 NEW
Prep Method: 3546 Prep Date: 05/22/2017 11:48
Matrix: Soil Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615227 Analyst: SCB Run Date: 05/23/2017 13:36
Collect Date: 05/19/2017 15:30 Dilution: 1 File ID: 12M62303
Sample Tag: 01 Units: ug/kg Percent Solid: 26.5
Analyte CAS # Result Qual RL MDL
1,2,4-Trichlorobenzene 120-82-1 U 666 333
1,2-Dichlorobenzene 95-50-1 U 666 333
1,3-Dichlorobenzene 541-73-1 U 666 333
1,4-Dichlorobenzene 106-46-7 U 666 333
2,4,5-Trichlorophenol 95-95-4 U 666 333
2,4,6-Trichlorophenol 88-06-2 U 666 333
2,4-Dichlorophenol 120-83-2 U 666 333
2,4-Dimethylphenol 105-67-9 U 666 333
2,4-Dinitrophenol 51-28-5 U 3330 1660
Page 15 of 30 Generated at May 25, 2017 09:36
Page 24
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
2,4-Dinitrotoluene 121-14-2 U 666 333
2,6-Dinitrotoluene 606-20-2 U 666 333
2-Chloronaphthalene 91-58-7 U 666 333
2-Chlorophenol 95-57-8 U 666 333
2-Methylnaphthalene 91-57-6 514 J 666 333
2-Methylphenol 95-48-7 U 666 333
2-Nitroaniline 88-74-4 U 3330 1660
2-Nitrophenol 88-75-5 U 666 333
3,3'-Dichlorobenzidine 91-94-1 U 1330 666
3-,4-Methylphenol 65794-96-9 U 666 333
3-Nitroaniline 99-09-2 U 3330 1660
4,6-Dinitro-2-methylphenol 534-52-1 U 3330 1660
4-Bromophenyl-phenylether 101-55-3 U 666 333
4-Chloro-3-methylphenol 59-50-7 U 666 333
4-Chloroaniline 106-47-8 U 666 333
4-Chlorophenyl-phenyl ether 7005-72-3 U 666 333
4-Nitroaniline 100-01-6 U 3330 1660
4-Nitrophenol 100-02-7 U 3330 1660
Acenaphthene 83-32-9 U 666 333
Acenaphthylene 208-96-8 U 666 333
Anthracene 120-12-7 U 666 333
Benzo(a)anthracene 56-55-3 U 666 333
Benzo(a)pyrene 50-32-8 U 666 333
Benzo(b)fluoranthene 205-99-2 U 666 333
Benzo(g,h,i)Perylene 191-24-2 U 666 333
Benzo(k)fluoranthene 207-08-9 U 666 333
Benzoic acid 65-85-0 U 20200 1330
Benzyl alcohol 100-51-6 U 666 333
Bis(2-Chloroethoxy)Methane 111-91-1 U 666 333
Bis(2-Chloroethyl)ether 111-44-4 U 666 333
bis(2-Chloroisopropyl)ether 39638-32-9 U 666 333
bis(2-Ethylhexyl)phthalate 117-81-7 U 666 333
Butylbenzylphthalate 85-68-7 U 666 333
Chrysene 218-01-9 U 666 333
Di-N-Butylphthalate 84-74-2 U 666 333
Di-n-octylphthalate 117-84-0 U 666 333
Dibenzo(a,h)Anthracene 53-70-3 U 666 333
Dibenzofuran 132-64-9 U 666 333
Diethylphthalate 84-66-2 U 666 333
Page 16 of 30 Generated at May 25, 2017 09:36
Page 25
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Dimethylphthalate 131-11-3 U 666 333
Fluoranthene 206-44-0 U 666 333
Fluorene 86-73-7 U 666 333
Hexachlorobenzene 118-74-1 U 666 333
Hexachlorobutadiene 87-68-3 U 666 333
Hexachlorocyclopentadiene 77-47-4 U 3030 1510
Hexachloroethane 67-72-1 U 666 333
Indeno(1,2,3-cd)pyrene 193-39-5 U 666 333
Isophorone 78-59-1 U 666 333
Diphenylamine/n-Nitrosodiphenylamine 86-30-6 U 666 333
N-Nitrosodipropylamine 621-64-7 U 666 333
Naphthalene 91-20-3 U 666 333
Nitrobenzene 98-95-3 U 666 333
Pentachlorophenol 87-86-5 U 3330 1660
Phenanthrene 85-01-8 U 666 333
Phenol 108-95-2 U 666 333
Pyrene 129-00-0 U 666 333
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 83.4 19 122
2-Fluorobiphenyl 81.7 30 115
2-Fluorophenol 62.9 25 121
Nitrobenzene-d5 84.5 23 120
p-Terphenyl-d14 75.9 18 137
Phenol-d5 62.2 24 113
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-10 PrePrep Method: N/A Instrument: HPMS9
Client ID: 17-0751 WEST BOREHOLE RETURN M
Prep Method: 5030B/5030C/5035A Prep Date: 05/23/2017 09:23
Matrix: Soil Analytical Method: 8260B Cal Date: 05/23/2017 14:46
Workgroup #: WG615352 Analyst: ADC Run Date: 05/23/2017 19:17
Collect Date: 05/19/2017 16:18 Dilution: 1 File ID: 9M980449
Sample Tag: 01 Units: ug/kg Percent Solid: 41.6
Analyte CAS # Result Qual RL MDL
Acetone 67-64-1 U 23.2 11.6
Benzene 71-43-2 U 11.6 1.16
Bromobenzene 108-86-1 U 11.6 1.16
Bromochloromethane 74-97-5 U 11.6 2.32
Page 17 of 30 Generated at May 25, 2017 09:36
Page 26
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Bromodichloromethane 75-27-4 U 11.6 1.16
Bromoform 75-25-2 U 11.6 1.16
Bromomethane 74-83-9 U 23.2 2.32
2-Butanone 78-93-3 U 23.2 5.80
n-Butylbenzene 104-51-8 2.28 J 11.6 1.16
sec-Butylbenzene 135-98-8 U 11.6 1.16
tert-Butylbenzene 98-06-6 U 11.6 1.16
Carbon disulfide 75-15-0 4.00 J 11.6 1.16
Carbon tetrachloride 56-23-5 U 11.6 1.16
Chlorobenzene 108-90-7 U 11.6 1.16
Chlorodibromomethane 124-48-1 U 11.6 1.16
Chloroethane 75-00-3 U 23.2 2.32
2-Chloroethyl vinyl ether 110-75-8 U 23.2 4.64
Chloroform 67-66-3 U 11.6 1.16
Chloromethane 74-87-3 U 23.2 4.64
2-Chlorotoluene 95-49-8 U 11.6 1.16
4-Chlorotoluene 106-43-4 U 11.6 1.16
1,2-Dibromo-3-chloropropane 96-12-8 U 11.6 4.64
1,2-Dibromoethane 106-93-4 U 11.6 1.16
Dibromomethane 74-95-3 U 11.6 1.16
1,2-Dichlorobenzene 95-50-1 U 11.6 1.16
1,3-Dichlorobenzene 541-73-1 U 11.6 1.16
1,4-Dichlorobenzene 106-46-7 U 11.6 1.16
Dichlorodifluoromethane 75-71-8 U 23.2 2.32
1,1-Dichloroethane 75-34-3 U 11.6 2.32
1,2-Dichloroethane 107-06-2 U 11.6 1.16
1,1-Dichloroethene 75-35-4 U 11.6 1.16
cis-1,2-Dichloroethene 156-59-2 U 11.6 1.16
trans-1,2-Dichloroethene 156-60-5 U 11.6 1.16
1,2-Dichloropropane 78-87-5 U 11.6 1.16
1,3-Dichloropropane 142-28-9 U 11.6 1.16
2,2-Dichloropropane 594-20-7 U 11.6 1.16
cis-1,3-Dichloropropene 10061-01-5 U 11.6 1.16
trans-1,3-Dichloropropene 10061-02-6 U 11.6 1.16
1,1-Dichloropropene 563-58-6 U 11.6 1.16
Ethylbenzene 100-41-4 1.46 J 11.6 1.16
2-Hexanone 591-78-6 U 23.2 5.80
Hexachlorobutadiene 87-68-3 U 11.6 1.16
Isopropylbenzene 98-82-8 U 11.6 1.16
Page 18 of 30 Generated at May 25, 2017 09:36
Page 27
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
p-Isopropyltoluene 99-87-6 U 11.6 1.16
4-Methyl-2-pentanone 108-10-1 U 23.2 5.80
Methylene chloride 75-09-2 U 11.6 2.32
Naphthalene 91-20-3 2.93 J 23.2 1.16
n-Propylbenzene 103-65-1 1.63 J 11.6 1.16
Styrene 100-42-5 U 11.6 1.16
1,1,1,2-Tetrachloroethane 630-20-6 U 11.6 1.16
1,1,2,2-Tetrachloroethane 79-34-5 U 11.6 1.16
Tetrachloroethene 127-18-4 2.38 J 11.6 1.16
Toluene 108-88-3 2.31 J 11.6 1.16
1,2,3-Trichlorobenzene 87-61-6 U 11.6 1.16
1,2,4-Trichlorobenzene 120-82-1 U 11.6 1.16
1,1,1-Trichloroethane 71-55-6 U 11.6 1.16
1,1,2-Trichloroethane 79-00-5 U 11.6 1.16
Trichloroethene 79-01-6 U 11.6 1.16
Trichlorofluoromethane 75-69-4 U 23.2 2.32
1,2,3-Trichloropropane 96-18-4 U 11.6 2.32
1,2,4-Trimethylbenzene 95-63-6 3.89 J 11.6 1.16
1,3,5-Trimethylbenzene 108-67-8 1.88 J 11.6 1.16
Vinyl acetate 108-05-4 U 23.2 5.80
Vinyl chloride 75-01-4 U 23.2 2.32
o-Xylene 95-47-6 2.08 J 11.6 1.16
m-,p-Xylene 179601-23-1 2.96 J 11.6 1.16
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 99.9 80 120
1,2-Dichloroethane-d4 96.5 80 120
Toluene-d8 117 81 117
4-Bromofluorobenzene 135 74 121 *
* Surrogate or spike compound out of range
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-10 PrePrep Method: N/A Instrument: HPMS12
Client ID: 17-0751 WEST BOREHOLE RETURN M
Prep Method: 3546 Prep Date: 05/22/2017 11:48
Matrix: Soil Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615227 Analyst: SCB Run Date: 05/23/2017 14:43
Collect Date: 05/19/2017 16:18 Dilution: 1 File ID: 12M62305
Sample Tag: 01 Units: ug/kg Percent Solid: 41.6
Page 19 of 30 Generated at May 25, 2017 09:36
Page 28
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
1,2,4-Trichlorobenzene 120-82-1 U 360 180
1,2-Dichlorobenzene 95-50-1 U 360 180
1,3-Dichlorobenzene 541-73-1 U 360 180
1,4-Dichlorobenzene 106-46-7 U 360 180
2,4,5-Trichlorophenol 95-95-4 U 360 180
2,4,6-Trichlorophenol 88-06-2 U 360 180
2,4-Dichlorophenol 120-83-2 U 360 180
2,4-Dimethylphenol 105-67-9 U 360 180
2,4-Dinitrophenol 51-28-5 U 1800 900
2,4-Dinitrotoluene 121-14-2 U 360 180
2,6-Dinitrotoluene 606-20-2 U 360 180
2-Chloronaphthalene 91-58-7 U 360 180
2-Chlorophenol 95-57-8 U 360 180
2-Methylnaphthalene 91-57-6 316 J 360 180
2-Methylphenol 95-48-7 U 360 180
2-Nitroaniline 88-74-4 U 1800 900
2-Nitrophenol 88-75-5 U 360 180
3,3'-Dichlorobenzidine 91-94-1 U 721 360
3-,4-Methylphenol 65794-96-9 U 360 180
3-Nitroaniline 99-09-2 U 1800 900
4,6-Dinitro-2-methylphenol 534-52-1 U 1800 900
4-Bromophenyl-phenylether 101-55-3 U 360 180
4-Chloro-3-methylphenol 59-50-7 U 360 180
4-Chloroaniline 106-47-8 U 360 180
4-Chlorophenyl-phenyl ether 7005-72-3 U 360 180
4-Nitroaniline 100-01-6 U 1800 900
4-Nitrophenol 100-02-7 U 1800 900
Acenaphthene 83-32-9 U 360 180
Acenaphthylene 208-96-8 U 360 180
Anthracene 120-12-7 U 360 180
Benzo(a)anthracene 56-55-3 U 360 180
Benzo(a)pyrene 50-32-8 U 360 180
Benzo(b)fluoranthene 205-99-2 U 360 180
Benzo(g,h,i)Perylene 191-24-2 U 360 180
Benzo(k)fluoranthene 207-08-9 U 360 180
Benzoic acid 65-85-0 U 10900 721
Benzyl alcohol 100-51-6 U 360 180
Bis(2-Chloroethoxy)Methane 111-91-1 U 360 180
Bis(2-Chloroethyl)ether 111-44-4 U 360 180
Page 20 of 30 Generated at May 25, 2017 09:36
Page 29
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
bis(2-Chloroisopropyl)ether 39638-32-9 U 360 180
bis(2-Ethylhexyl)phthalate 117-81-7 U 360 180
Butylbenzylphthalate 85-68-7 U 360 180
Chrysene 218-01-9 U 360 180
Di-N-Butylphthalate 84-74-2 U 360 180
Di-n-octylphthalate 117-84-0 U 360 180
Dibenzo(a,h)Anthracene 53-70-3 U 360 180
Dibenzofuran 132-64-9 U 360 180
Diethylphthalate 84-66-2 U 360 180
Dimethylphthalate 131-11-3 U 360 180
Fluoranthene 206-44-0 U 360 180
Fluorene 86-73-7 U 360 180
Hexachlorobenzene 118-74-1 U 360 180
Hexachlorobutadiene 87-68-3 U 360 180
Hexachlorocyclopentadiene 77-47-4 U 1640 819
Hexachloroethane 67-72-1 U 360 180
Indeno(1,2,3-cd)pyrene 193-39-5 U 360 180
Isophorone 78-59-1 U 360 180
Diphenylamine/n-Nitrosodiphenylamine 86-30-6 U 360 180
N-Nitrosodipropylamine 621-64-7 U 360 180
Naphthalene 91-20-3 197 J 360 180
Nitrobenzene 98-95-3 U 360 180
Pentachlorophenol 87-86-5 U 1800 900
Phenanthrene 85-01-8 U 360 180
Phenol 108-95-2 U 360 180
Pyrene 129-00-0 U 360 180
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 70.9 19 122
2-Fluorobiphenyl 57.1 30 115
2-Fluorophenol 45.1 25 121
Nitrobenzene-d5 60.2 23 120
p-Terphenyl-d14 79.1 18 137
Phenol-d5 43.6 24 113
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Page 21 of 30 Generated at May 25, 2017 09:36
Page 30
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisSample #: L17051231-12 PrePrep Method: N/A Instrument: HPMS9
Client ID: 17-0751 WEST RECLAIMER PIT
Prep Method: 5030B/5030C/5035A Prep Date: 05/23/2017 09:25
Matrix: Soil Analytical Method: 8260B Cal Date: 05/23/2017 14:46
Workgroup #: WG615352 Analyst: ADC Run Date: 05/23/2017 19:47
Collect Date: 05/19/2017 16:30 Dilution: 1 File ID: 9M980450
Sample Tag: 01 Units: ug/kg Percent Solid: 56.8
Analyte CAS # Result Qual RL MDL
Acetone 67-64-1 19.0 17.0 8.52
Benzene 71-43-2 U 8.52 0.852
Bromobenzene 108-86-1 U 8.52 0.852
Bromochloromethane 74-97-5 U 8.52 1.70
Bromodichloromethane 75-27-4 U 8.52 0.852
Bromoform 75-25-2 U 8.52 0.852
Bromomethane 74-83-9 U 17.0 1.70
2-Butanone 78-93-3 U 17.0 4.26
n-Butylbenzene 104-51-8 1.10 J 8.52 0.852
sec-Butylbenzene 135-98-8 U 8.52 0.852
tert-Butylbenzene 98-06-6 U 8.52 0.852
Carbon disulfide 75-15-0 1.56 J 8.52 0.852
Carbon tetrachloride 56-23-5 U 8.52 0.852
Chlorobenzene 108-90-7 U 8.52 0.852
Chlorodibromomethane 124-48-1 U 8.52 0.852
Chloroethane 75-00-3 U 17.0 1.70
2-Chloroethyl vinyl ether 110-75-8 U 17.0 3.41
Chloroform 67-66-3 U 8.52 0.852
Chloromethane 74-87-3 U 17.0 3.41
2-Chlorotoluene 95-49-8 U 8.52 0.852
4-Chlorotoluene 106-43-4 U 8.52 0.852
1,2-Dibromo-3-chloropropane 96-12-8 U 8.52 3.41
1,2-Dibromoethane 106-93-4 U 8.52 0.852
Dibromomethane 74-95-3 U 8.52 0.852
1,2-Dichlorobenzene 95-50-1 U 8.52 0.852
1,3-Dichlorobenzene 541-73-1 U 8.52 0.852
1,4-Dichlorobenzene 106-46-7 U 8.52 0.852
Dichlorodifluoromethane 75-71-8 U 17.0 1.70
1,1-Dichloroethane 75-34-3 U 8.52 1.70
1,2-Dichloroethane 107-06-2 U 8.52 0.852
1,1-Dichloroethene 75-35-4 U 8.52 0.852
cis-1,2-Dichloroethene 156-59-2 U 8.52 0.852
Page 22 of 30 Generated at May 25, 2017 09:36
Page 31
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
trans-1,2-Dichloroethene 156-60-5 U 8.52 0.852
1,2-Dichloropropane 78-87-5 U 8.52 0.852
1,3-Dichloropropane 142-28-9 U 8.52 0.852
2,2-Dichloropropane 594-20-7 U 8.52 0.852
cis-1,3-Dichloropropene 10061-01-5 U 8.52 0.852
trans-1,3-Dichloropropene 10061-02-6 U 8.52 0.852
1,1-Dichloropropene 563-58-6 U 8.52 0.852
Ethylbenzene 100-41-4 U 8.52 0.852
2-Hexanone 591-78-6 U 17.0 4.26
Hexachlorobutadiene 87-68-3 U 8.52 0.852
Isopropylbenzene 98-82-8 U 8.52 0.852
p-Isopropyltoluene 99-87-6 U 8.52 0.852
4-Methyl-2-pentanone 108-10-1 U 17.0 4.26
Methylene chloride 75-09-2 U 8.52 1.70
Naphthalene 91-20-3 1.10 J 17.0 0.852
n-Propylbenzene 103-65-1 U 8.52 0.852
Styrene 100-42-5 U 8.52 0.852
1,1,1,2-Tetrachloroethane 630-20-6 U 8.52 0.852
1,1,2,2-Tetrachloroethane 79-34-5 U 8.52 0.852
Tetrachloroethene 127-18-4 1.41 J 8.52 0.852
Toluene 108-88-3 1.43 J 8.52 0.852
1,2,3-Trichlorobenzene 87-61-6 U 8.52 0.852
1,2,4-Trichlorobenzene 120-82-1 U 8.52 0.852
1,1,1-Trichloroethane 71-55-6 U 8.52 0.852
1,1,2-Trichloroethane 79-00-5 U 8.52 0.852
Trichloroethene 79-01-6 U 8.52 0.852
Trichlorofluoromethane 75-69-4 U 17.0 1.70
1,2,3-Trichloropropane 96-18-4 U 8.52 1.70
1,2,4-Trimethylbenzene 95-63-6 2.05 J 8.52 0.852
1,3,5-Trimethylbenzene 108-67-8 0.985 J 8.52 0.852
Vinyl acetate 108-05-4 U 17.0 4.26
Vinyl chloride 75-01-4 U 17.0 1.70
o-Xylene 95-47-6 1.14 J 8.52 0.852
m-,p-Xylene 179601-23-1 1.34 J 8.52 0.852
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 98.6 80 120
1,2-Dichloroethane-d4 97.4 80 120
Toluene-d8 114 81 117
4-Bromofluorobenzene 122 74 121 *
Page 23 of 30 Generated at May 25, 2017 09:36
Page 32
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis* Surrogate or spike compound out of range
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-12 PrePrep Method: N/A Instrument: HPMS12
Client ID: 17-0751 WEST RECLAIMER PIT
Prep Method: 3546 Prep Date: 05/22/2017 11:48
Matrix: Soil Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615227 Analyst: SCB Run Date: 05/23/2017 15:16
Collect Date: 05/19/2017 16:30 Dilution: 1 File ID: 12M62306
Sample Tag: 01 Units: ug/kg Percent Solid: 56.8
Analyte CAS # Result Qual RL MDL
1,2,4-Trichlorobenzene 120-82-1 U 301 151
1,2-Dichlorobenzene 95-50-1 U 301 151
1,3-Dichlorobenzene 541-73-1 U 301 151
1,4-Dichlorobenzene 106-46-7 U 301 151
2,4,5-Trichlorophenol 95-95-4 U 301 151
2,4,6-Trichlorophenol 88-06-2 U 301 151
2,4-Dichlorophenol 120-83-2 U 301 151
2,4-Dimethylphenol 105-67-9 U 301 151
2,4-Dinitrophenol 51-28-5 U 1510 752
2,4-Dinitrotoluene 121-14-2 U 301 151
2,6-Dinitrotoluene 606-20-2 U 301 151
2-Chloronaphthalene 91-58-7 U 301 151
2-Chlorophenol 95-57-8 U 301 151
2-Methylnaphthalene 91-57-6 2090 301 151
2-Methylphenol 95-48-7 U 301 151
2-Nitroaniline 88-74-4 U 1510 752
2-Nitrophenol 88-75-5 U 301 151
3,3'-Dichlorobenzidine 91-94-1 U 603 301
3-,4-Methylphenol 65794-96-9 U 301 151
3-Nitroaniline 99-09-2 U 1510 752
4,6-Dinitro-2-methylphenol 534-52-1 U 1510 752
4-Bromophenyl-phenylether 101-55-3 U 301 151
4-Chloro-3-methylphenol 59-50-7 U 301 151
4-Chloroaniline 106-47-8 U 301 151
4-Chlorophenyl-phenyl ether 7005-72-3 U 301 151
4-Nitroaniline 100-01-6 U 1510 752
4-Nitrophenol 100-02-7 U 1510 752
Acenaphthene 83-32-9 U 301 151
Page 24 of 30 Generated at May 25, 2017 09:36
Page 33
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Acenaphthylene 208-96-8 U 301 151
Anthracene 120-12-7 U 301 151
Benzo(a)anthracene 56-55-3 U 301 151
Benzo(a)pyrene 50-32-8 U 301 151
Benzo(b)fluoranthene 205-99-2 U 301 151
Benzo(g,h,i)Perylene 191-24-2 U 301 151
Benzo(k)fluoranthene 207-08-9 U 301 151
Benzoic acid 65-85-0 U 9130 603
Benzyl alcohol 100-51-6 U 301 151
Bis(2-Chloroethoxy)Methane 111-91-1 U 301 151
Bis(2-Chloroethyl)ether 111-44-4 U 301 151
bis(2-Chloroisopropyl)ether 39638-32-9 U 301 151
bis(2-Ethylhexyl)phthalate 117-81-7 U 301 151
Butylbenzylphthalate 85-68-7 U 301 151
Chrysene 218-01-9 U 301 151
Di-N-Butylphthalate 84-74-2 U 301 151
Di-n-octylphthalate 117-84-0 U 301 151
Dibenzo(a,h)Anthracene 53-70-3 U 301 151
Dibenzofuran 132-64-9 358 301 151
Diethylphthalate 84-66-2 U 301 151
Dimethylphthalate 131-11-3 U 301 151
Fluoranthene 206-44-0 175 J 301 151
Fluorene 86-73-7 U 301 151
Hexachlorobenzene 118-74-1 U 301 151
Hexachlorobutadiene 87-68-3 U 301 151
Hexachlorocyclopentadiene 77-47-4 U 1370 685
Hexachloroethane 67-72-1 U 301 151
Indeno(1,2,3-cd)pyrene 193-39-5 U 301 151
Isophorone 78-59-1 U 301 151
Diphenylamine/n-Nitrosodiphenylamine 86-30-6 U 301 151
N-Nitrosodipropylamine 621-64-7 U 301 151
Naphthalene 91-20-3 1310 301 151
Nitrobenzene 98-95-3 U 301 151
Pentachlorophenol 87-86-5 U 1510 752
Phenanthrene 85-01-8 789 301 151
Phenol 108-95-2 U 301 151
Pyrene 129-00-0 194 J 301 151
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 87.9 19 122
Page 25 of 30 Generated at May 25, 2017 09:36
Page 34
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis2-Fluorobiphenyl 82.1 30 115
2-Fluorophenol 62.5 25 121
Nitrobenzene-d5 88.7 23 120
p-Terphenyl-d14 77.3 18 137
Phenol-d5 59.8 24 113
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-14 PrePrep Method: N/A Instrument: HPMS9
Client ID: 17-0751 EAST RECLAIMER NEW MUD
Prep Method: 5030B/5030C/5035A Prep Date: 05/23/2017 09:28
Matrix: Soil Analytical Method: 8260B Cal Date: 05/23/2017 14:46
Workgroup #: WG615352 Analyst: ADC Run Date: 05/23/2017 20:17
Collect Date: 05/19/2017 17:12 Dilution: 1 File ID: 9M980451
Sample Tag: 01 Units: ug/kg Percent Solid: 1.96
Analyte CAS # Result Qual RL MDL
Acetone 67-64-1 U 502 251
Benzene 71-43-2 U 251 25.1
Bromobenzene 108-86-1 U 251 25.1
Bromochloromethane 74-97-5 U 251 50.2
Bromodichloromethane 75-27-4 U 251 25.1
Bromoform 75-25-2 U 251 25.1
Bromomethane 74-83-9 U 502 50.2
2-Butanone 78-93-3 U 502 125
n-Butylbenzene 104-51-8 U 251 25.1
sec-Butylbenzene 135-98-8 U 251 25.1
tert-Butylbenzene 98-06-6 U 251 25.1
Carbon disulfide 75-15-0 U 251 25.1
Carbon tetrachloride 56-23-5 U 251 25.1
Chlorobenzene 108-90-7 U 251 25.1
Chlorodibromomethane 124-48-1 U 251 25.1
Chloroethane 75-00-3 U 502 50.2
2-Chloroethyl vinyl ether 110-75-8 U 502 100
Chloroform 67-66-3 U 251 25.1
Chloromethane 74-87-3 U 502 100
2-Chlorotoluene 95-49-8 U 251 25.1
4-Chlorotoluene 106-43-4 U 251 25.1
1,2-Dibromo-3-chloropropane 96-12-8 U 251 100
1,2-Dibromoethane 106-93-4 U 251 25.1
Dibromomethane 74-95-3 U 251 25.1
Page 26 of 30 Generated at May 25, 2017 09:36
Page 35
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
1,2-Dichlorobenzene 95-50-1 U 251 25.1
1,3-Dichlorobenzene 541-73-1 U 251 25.1
1,4-Dichlorobenzene 106-46-7 U 251 25.1
Dichlorodifluoromethane 75-71-8 U 502 50.2
1,1-Dichloroethane 75-34-3 U 251 50.2
1,2-Dichloroethane 107-06-2 U 251 25.1
1,1-Dichloroethene 75-35-4 U 251 25.1
cis-1,2-Dichloroethene 156-59-2 U 251 25.1
trans-1,2-Dichloroethene 156-60-5 U 251 25.1
1,2-Dichloropropane 78-87-5 U 251 25.1
1,3-Dichloropropane 142-28-9 U 251 25.1
2,2-Dichloropropane 594-20-7 U 251 25.1
cis-1,3-Dichloropropene 10061-01-5 U 251 25.1
trans-1,3-Dichloropropene 10061-02-6 U 251 25.1
1,1-Dichloropropene 563-58-6 U 251 25.1
Ethylbenzene 100-41-4 U 251 25.1
2-Hexanone 591-78-6 U 502 125
Hexachlorobutadiene 87-68-3 U 251 25.1
Isopropylbenzene 98-82-8 U 251 25.1
p-Isopropyltoluene 99-87-6 U 251 25.1
4-Methyl-2-pentanone 108-10-1 U 502 125
Methylene chloride 75-09-2 U 251 50.2
Naphthalene 91-20-3 U 502 25.1
n-Propylbenzene 103-65-1 U 251 25.1
Styrene 100-42-5 U 251 25.1
1,1,1,2-Tetrachloroethane 630-20-6 U 251 25.1
1,1,2,2-Tetrachloroethane 79-34-5 U 251 25.1
Tetrachloroethene 127-18-4 62.4 J 251 25.1
Toluene 108-88-3 U 251 25.1
1,2,3-Trichlorobenzene 87-61-6 U 251 25.1
1,2,4-Trichlorobenzene 120-82-1 U 251 25.1
1,1,1-Trichloroethane 71-55-6 U 251 25.1
1,1,2-Trichloroethane 79-00-5 U 251 25.1
Trichloroethene 79-01-6 U 251 25.1
Trichlorofluoromethane 75-69-4 U 502 50.2
1,2,3-Trichloropropane 96-18-4 U 251 50.2
1,2,4-Trimethylbenzene 95-63-6 U 251 25.1
1,3,5-Trimethylbenzene 108-67-8 U 251 25.1
Vinyl acetate 108-05-4 U 502 125
Page 27 of 30 Generated at May 25, 2017 09:36
Page 36
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Vinyl chloride 75-01-4 U 502 50.2
o-Xylene 95-47-6 U 251 25.1
m-,p-Xylene 179601-23-1 U 251 25.1
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 97.4 80 120
1,2-Dichloroethane-d4 92.8 80 120
Toluene-d8 106 81 117
4-Bromofluorobenzene 111 74 121
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-14 PrePrep Method: N/A Instrument: HPMS12
Client ID: 17-0751 EAST RECLAIMER NEW MUD
Prep Method: 3546 Prep Date: 05/22/2017 11:48
Matrix: Soil Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615227 Analyst: SCB Run Date: 05/23/2017 12:31
Collect Date: 05/19/2017 17:12 Dilution: 1 File ID: 12M62301
Sample Tag: 01 Units: ug/kg Percent Solid: 1.96
Analyte CAS # Result Qual RL MDL
1,2,4-Trichlorobenzene 120-82-1 U 9740 4870
1,2-Dichlorobenzene 95-50-1 U 9740 4870
1,3-Dichlorobenzene 541-73-1 U 9740 4870
1,4-Dichlorobenzene 106-46-7 U 9740 4870
2,4,5-Trichlorophenol 95-95-4 U 9740 4870
2,4,6-Trichlorophenol 88-06-2 U 9740 4870
2,4-Dichlorophenol 120-83-2 U 9740 4870
2,4-Dimethylphenol 105-67-9 U 9740 4870
2,4-Dinitrophenol 51-28-5 U 48700 24300
2,4-Dinitrotoluene 121-14-2 U 9740 4870
2,6-Dinitrotoluene 606-20-2 U 9740 4870
2-Chloronaphthalene 91-58-7 U 9740 4870
2-Chlorophenol 95-57-8 U 9740 4870
2-Methylnaphthalene 91-57-6 U 9740 4870
2-Methylphenol 95-48-7 U 9740 4870
2-Nitroaniline 88-74-4 U 48700 24300
2-Nitrophenol 88-75-5 U 9740 4870
3,3'-Dichlorobenzidine 91-94-1 U 19500 9740
3-,4-Methylphenol 65794-96-9 U 9740 4870
3-Nitroaniline 99-09-2 U 48700 24300
Page 28 of 30 Generated at May 25, 2017 09:36
Page 37
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
4,6-Dinitro-2-methylphenol 534-52-1 U 48700 24300
4-Bromophenyl-phenylether 101-55-3 U 9740 4870
4-Chloro-3-methylphenol 59-50-7 U 9740 4870
4-Chloroaniline 106-47-8 U 9740 4870
4-Chlorophenyl-phenyl ether 7005-72-3 U 9740 4870
4-Nitroaniline 100-01-6 U 48700 24300
4-Nitrophenol 100-02-7 U 48700 24300
Acenaphthene 83-32-9 U 9740 4870
Acenaphthylene 208-96-8 U 9740 4870
Anthracene 120-12-7 U 9740 4870
Benzo(a)anthracene 56-55-3 U 9740 4870
Benzo(a)pyrene 50-32-8 U 9740 4870
Benzo(b)fluoranthene 205-99-2 U 9740 4870
Benzo(g,h,i)Perylene 191-24-2 U 9740 4870
Benzo(k)fluoranthene 207-08-9 U 9740 4870
Benzoic acid 65-85-0 U 295000 19500
Benzyl alcohol 100-51-6 U 9740 4870
Bis(2-Chloroethoxy)Methane 111-91-1 U 9740 4870
Bis(2-Chloroethyl)ether 111-44-4 U 9740 4870
bis(2-Chloroisopropyl)ether 39638-32-9 U 9740 4870
bis(2-Ethylhexyl)phthalate 117-81-7 U 9740 4870
Butylbenzylphthalate 85-68-7 U 9740 4870
Chrysene 218-01-9 U 9740 4870
Di-N-Butylphthalate 84-74-2 U 9740 4870
Di-n-octylphthalate 117-84-0 U 9740 4870
Dibenzo(a,h)Anthracene 53-70-3 U 9740 4870
Dibenzofuran 132-64-9 U 9740 4870
Diethylphthalate 84-66-2 U 9740 4870
Dimethylphthalate 131-11-3 U 9740 4870
Fluoranthene 206-44-0 U 9740 4870
Fluorene 86-73-7 U 9740 4870
Hexachlorobenzene 118-74-1 U 9740 4870
Hexachlorobutadiene 87-68-3 U 9740 4870
Hexachlorocyclopentadiene 77-47-4 U 44300 22100
Hexachloroethane 67-72-1 U 9740 4870
Indeno(1,2,3-cd)pyrene 193-39-5 U 9740 4870
Isophorone 78-59-1 U 9740 4870
Diphenylamine/n-Nitrosodiphenylamine 86-30-6 U 9740 4870
N-Nitrosodipropylamine 621-64-7 U 9740 4870
Page 29 of 30 Generated at May 25, 2017 09:36
Page 38
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Naphthalene 91-20-3 U 9740 4870
Nitrobenzene 98-95-3 U 9740 4870
Pentachlorophenol 87-86-5 U 48700 24300
Phenanthrene 85-01-8 U 9740 4870
Phenol 108-95-2 U 9740 4870
Pyrene 129-00-0 U 9740 4870
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 54.9 19 122
2-Fluorobiphenyl 64.3 30 115
2-Fluorophenol 46.1 25 121
Nitrobenzene-d5 72.5 23 120
p-Terphenyl-d14 68.3 18 137
Phenol-d5 49.0 24 113
U Not detected at or above adjusted sample detection limit
Page 30 of 30 Generated at May 25, 2017 09:36
Page 39
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Sample #: L17051231-01 PrePrep Method: Instrument: HPMS8
Client ID: 17-0751 OSG DISPOSAL PIT Prep Method: 5030B/5030C/5035A Prep Date: N/A
Matrix: TCLP Leach Analytical Method: 8260B Cal Date: 04/17/2017 18:24
Workgroup #: WG615405 Analyst: TMB Run Date: 05/24/2017 14:22
Collect Date: 05/19/2017 13:24 Dilution: 10 File ID: 8M419874
Sample Tag: DL01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Benzene U 50.0 1.25 D018 500
Carbon tetrachloride U 50.0 2.50 D019 500
Chlorobenzene U 50.0 1.25 D021 100000
Chloroform U 50.0 1.25 D022 6000
1,2-Dichloroethane U 50.0 2.50 D028 500
1,1-Dichloroethene U 50.0 5.00 D029 700
Methyl Ethyl Ketone U 100 25.0 D035 200000
Tetrachloroethene U 50.0 2.50 D039 700
Trichloroethene U 50.0 2.50 D040 500
Vinyl chloride U 100 2.50 D043 200
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 101 86 118
1,2-Dichloroethane-d4 96.9 80 120
Toluene-d8 107 88 110
4-Bromofluorobenzene 106 86 115
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-01 PrePrep Method: Instrument: HPMS12
Client ID: 17-0751 OSG DISPOSAL PIT Prep Method: 3510C Prep Date: 05/23/2017 14:05
Matrix: TCLP Leach Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615400 Analyst: MES Run Date: 05/24/2017 12:31
Collect Date: 05/19/2017 13:24 Dilution: 1 File ID: 12M62319
Sample Tag: 01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
o-Cresol U 50.0 25.0 D023 200000
m-,p-Cresol U 50.0 25.0 D025 200000
1,4-Dichlorobenzene U 50.0 25.0 D027 7500
2,4-Dinitrotoluene U 50.0 25.0 D030 130
Hexachlorobenzene U 50.0 25.0 D032 130
Hexachlorobutadiene U 50.0 25.0 D033 500
Hexachloroethane U 50.0 25.0 D034 3000
Page 1 of 16 Generated at May 25, 2017 09:35
Page 40
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Nitrobenzene U 50.0 25.0 D036 2000
Pentachlorophenol U 250 125 D037 100000
Pyridine U 250 125 D038 5000
2,4,5-Trichlorophenol U 50.0 25.0 D041 400000
2,4,6-Trichlorophenol U 50.0 25.0 D042 2000
Surrogate Recovery Lower Limit Upper Limit Q
2-Fluorophenol 41.7 21 100
Phenol-d5 29.6 10 94
Nitrobenzene-d5 78.9 35 114
2-Fluorobiphenyl 74.6 43 116
2,4,6-Tribromophenol 92.1 10 123
p-Terphenyl-d14 99.9 33 141
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-01 PrePrep Method: N/A Instrument: ICP-THERMO4
Client ID: 17-0751 OSG DISPOSAL PIT Prep Method: 3015A Prep Date: 05/23/2017 09:43
Matrix: TCLP Leach Analytical Method: 6010B Cal Date: 05/23/2017 14:24
Workgroup #: WG615308 Analyst: KKB Run Date: 05/23/2017 16:45
Collect Date: 05/19/2017 13:24 Dilution: 1 File ID: T4.052317.164558
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Arsenic, TCLP U 1.00 0.500 D004 5
Barium, TCLP 0.869 0.100 0.0500 D005 100
Cadmium, TCLP U 0.100 0.0500 D006 1
Chromium, TCLP U 0.200 0.100 D007 5
Lead, TCLP U 1.00 0.500 D008 5
Selenium, TCLP U 0.800 0.400 D010 1
Silver, TCLP U 0.100 0.0500 D011 5
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-01 PrePrep Method: Instrument: CVAA1
Client ID: 17-0751 OSG DISPOSAL PIT Prep Method: 7470A Prep Date: 05/23/2017 09:19
Matrix: TCLP Leach Analytical Method: 7470A Cal Date: 05/23/2017 14:40
Workgroup #: WG615315 Analyst: LSJ Run Date: 05/23/2017 15:46
Collect Date: 05/19/2017 13:24 Dilution: 1 File ID: M7.052317.154615
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Mercury U 0.00200 0.00100 D009 0.2
Page 2 of 16 Generated at May 25, 2017 09:35
Page 41
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-03 PrePrep Method: Instrument: HPMS11
Client ID: 17-0751 IR MUD ORIGINAL Prep Method: 5030B/5030C/5035A Prep Date: N/A
Matrix: TCLP Leach Analytical Method: 8260B Cal Date: 05/16/2017 17:16
Workgroup #: WG615282 Analyst: TMB/JDS Run Date: 05/23/2017 18:54
Collect Date: 05/19/2017 15:00 Dilution: 10 File ID: 11M18579
Sample Tag: DL01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Benzene U 50.0 1.25 D018 500
Carbon tetrachloride U 50.0 2.50 D019 500
Chlorobenzene U 50.0 1.25 D021 100000
Chloroform U 50.0 1.25 D022 6000
1,2-Dichloroethane U 50.0 2.50 D028 500
1,1-Dichloroethene U 50.0 5.00 D029 700
Methyl Ethyl Ketone U 100 25.0 D035 200000
Tetrachloroethene U 50.0 2.50 D039 700
Trichloroethene U 50.0 2.50 D040 500
Vinyl chloride U 100 2.50 D043 200
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 103 86 118
1,2-Dichloroethane-d4 105 80 120
Toluene-d8 110 88 110
4-Bromofluorobenzene 108 86 115
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-03 PrePrep Method: Instrument: HPMS12
Client ID: 17-0751 IR MUD ORIGINAL Prep Method: 3510C Prep Date: 05/23/2017 14:05
Matrix: TCLP Leach Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615400 Analyst: MES Run Date: 05/24/2017 13:04
Collect Date: 05/19/2017 15:00 Dilution: 1 File ID: 12M62320
Sample Tag: 01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
o-Cresol U 50.0 25.0 D023 200000
m-,p-Cresol U 50.0 25.0 D025 200000
1,4-Dichlorobenzene U 50.0 25.0 D027 7500
2,4-Dinitrotoluene U 50.0 25.0 D030 130
Hexachlorobenzene U 50.0 25.0 D032 130
Hexachlorobutadiene U 50.0 25.0 D033 500
Page 3 of 16 Generated at May 25, 2017 09:35
Page 42
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Hexachloroethane U 50.0 25.0 D034 3000
Nitrobenzene U 50.0 25.0 D036 2000
Pentachlorophenol U 250 125 D037 100000
Pyridine U 250 125 D038 5000
2,4,5-Trichlorophenol U 50.0 25.0 D041 400000
2,4,6-Trichlorophenol U 50.0 25.0 D042 2000
Surrogate Recovery Lower Limit Upper Limit Q
2-Fluorophenol 33.7 21 100
Phenol-d5 22.6 10 94
Nitrobenzene-d5 66.7 35 114
2-Fluorobiphenyl 58.9 43 116
2,4,6-Tribromophenol 97.8 10 123
p-Terphenyl-d14 97.0 33 141
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-03 PrePrep Method: N/A Instrument: ICP-THERMO4
Client ID: 17-0751 IR MUD ORIGINAL Prep Method: 3015A Prep Date: 05/23/2017 09:43
Matrix: TCLP Leach Analytical Method: 6010B Cal Date: 05/23/2017 14:24
Workgroup #: WG615308 Analyst: KKB Run Date: 05/23/2017 16:49
Collect Date: 05/19/2017 15:00 Dilution: 1 File ID: T4.052317.164940
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Arsenic, TCLP U 1.00 0.500 D004 5
Barium, TCLP 0.647 0.100 0.0500 D005 100
Cadmium, TCLP U 0.100 0.0500 D006 1
Chromium, TCLP U 0.200 0.100 D007 5
Lead, TCLP U 1.00 0.500 D008 5
Selenium, TCLP U 0.800 0.400 D010 1
Silver, TCLP U 0.100 0.0500 D011 5
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-03 PrePrep Method: Instrument: CVAA1
Client ID: 17-0751 IR MUD ORIGINAL Prep Method: 7470A Prep Date: 05/23/2017 09:19
Matrix: TCLP Leach Analytical Method: 7470A Cal Date: 05/23/2017 14:40
Workgroup #: WG615315 Analyst: LSJ Run Date: 05/23/2017 15:53
Collect Date: 05/19/2017 15:00 Dilution: 1 File ID: M7.052317.155351
Sample Tag: 01 Units: mg/L
Page 4 of 16 Generated at May 25, 2017 09:35
Page 43
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Mercury U 0.00200 0.00100 D009 0.2
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-05 PrePrep Method: Instrument: HPMS11
Client ID: 17-0751 IR MUD SILO Prep Method: 5030B/5030C/5035A Prep Date: N/A
Matrix: TCLP Leach Analytical Method: 8260B Cal Date: 05/16/2017 17:16
Workgroup #: WG615282 Analyst: TMB/JDS Run Date: 05/23/2017 19:23
Collect Date: 05/19/2017 14:45 Dilution: 10 File ID: 11M18580
Sample Tag: DL01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Benzene U 50.0 1.25 D018 500
Carbon tetrachloride U 50.0 2.50 D019 500
Chlorobenzene U 50.0 1.25 D021 100000
Chloroform U 50.0 1.25 D022 6000
1,2-Dichloroethane U 50.0 2.50 D028 500
1,1-Dichloroethene U 50.0 5.00 D029 700
Methyl Ethyl Ketone U 100 25.0 D035 200000
Tetrachloroethene U 50.0 2.50 D039 700
Trichloroethene U 50.0 2.50 D040 500
Vinyl chloride U 100 2.50 D043 200
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 106 86 118
1,2-Dichloroethane-d4 109 80 120
Toluene-d8 113 88 110 *
4-Bromofluorobenzene 113 86 115
* Surrogate or spike compound out of range
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-05 PrePrep Method: Instrument: HPMS12
Client ID: 17-0751 IR MUD SILO Prep Method: 3510C Prep Date: 05/23/2017 14:05
Matrix: TCLP Leach Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615400 Analyst: MES Run Date: 05/24/2017 13:37
Collect Date: 05/19/2017 14:45 Dilution: 1 File ID: 12M62321
Sample Tag: 01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
o-Cresol U 50.0 25.0 D023 200000
m-,p-Cresol U 50.0 25.0 D025 200000
1,4-Dichlorobenzene U 50.0 25.0 D027 7500
Page 5 of 16 Generated at May 25, 2017 09:35
Page 44
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Analyte Result Qual RL MDL EPA HW# Reg. Limit
2,4-Dinitrotoluene U 50.0 25.0 D030 130
Hexachlorobenzene U 50.0 25.0 D032 130
Hexachlorobutadiene U 50.0 25.0 D033 500
Hexachloroethane U 50.0 25.0 D034 3000
Nitrobenzene U 50.0 25.0 D036 2000
Pentachlorophenol U 250 125 D037 100000
Pyridine U 250 125 D038 5000
2,4,5-Trichlorophenol U 50.0 25.0 D041 400000
2,4,6-Trichlorophenol U 50.0 25.0 D042 2000
Surrogate Recovery Lower Limit Upper Limit Q
2-Fluorophenol 47.3 21 100
Phenol-d5 30.3 10 94
Nitrobenzene-d5 95.2 35 114
2-Fluorobiphenyl 85.2 43 116
2,4,6-Tribromophenol 113 10 123
p-Terphenyl-d14 107 33 141
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-05 PrePrep Method: N/A Instrument: ICP-THERMO4
Client ID: 17-0751 IR MUD SILO Prep Method: 3015A Prep Date: 05/23/2017 09:43
Matrix: TCLP Leach Analytical Method: 6010B Cal Date: 05/23/2017 14:24
Workgroup #: WG615308 Analyst: KKB Run Date: 05/23/2017 17:00
Collect Date: 05/19/2017 14:45 Dilution: 1 File ID: T4.052317.170036
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Arsenic, TCLP U 1.00 0.500 D004 5
Barium, TCLP 0.712 0.100 0.0500 D005 100
Cadmium, TCLP U 0.100 0.0500 D006 1
Chromium, TCLP U 0.200 0.100 D007 5
Lead, TCLP U 1.00 0.500 D008 5
Selenium, TCLP U 0.800 0.400 D010 1
Silver, TCLP U 0.100 0.0500 D011 5
U Not detected at or above adjusted sample detection limit
Page 6 of 16 Generated at May 25, 2017 09:35
Page 45
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Sample #: L17051231-05 PrePrep Method: Instrument: CVAA1
Client ID: 17-0751 IR MUD SILO Prep Method: 7470A Prep Date: 05/23/2017 09:19
Matrix: TCLP Leach Analytical Method: 7470A Cal Date: 05/23/2017 14:40
Workgroup #: WG615315 Analyst: LSJ Run Date: 05/23/2017 15:56
Collect Date: 05/19/2017 14:45 Dilution: 1 File ID: M7.052317.155624
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Mercury U 0.00200 0.00100 D009 0.2
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-07 PrePrep Method: Instrument: HPMS11
Client ID: 17-0751 IR MUD GRID A3 NEW
Prep Method: 5030B/5030C/5035A Prep Date: N/A
Matrix: TCLP Leach Analytical Method: 8260B Cal Date: 05/16/2017 17:16
Workgroup #: WG615282 Analyst: TMB/JDS Run Date: 05/23/2017 19:52
Collect Date: 05/19/2017 15:30 Dilution: 10 File ID: 11M18581
Sample Tag: DL01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Benzene U 50.0 1.25 D018 500
Carbon tetrachloride U 50.0 2.50 D019 500
Chlorobenzene U 50.0 1.25 D021 100000
Chloroform U 50.0 1.25 D022 6000
1,2-Dichloroethane U 50.0 2.50 D028 500
1,1-Dichloroethene U 50.0 5.00 D029 700
Methyl Ethyl Ketone U 100 25.0 D035 200000
Tetrachloroethene U 50.0 2.50 D039 700
Trichloroethene U 50.0 2.50 D040 500
Vinyl chloride U 100 2.50 D043 200
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 103 86 118
1,2-Dichloroethane-d4 107 80 120
Toluene-d8 111 88 110 *
4-Bromofluorobenzene 110 86 115
* Surrogate or spike compound out of range
U Not detected at or above adjusted sample detection limit
Page 7 of 16 Generated at May 25, 2017 09:35
Page 46
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Sample #: L17051231-07 PrePrep Method: Instrument: HPMS12
Client ID: 17-0751 IR MUD GRID A3 NEW
Prep Method: 3510C Prep Date: 05/23/2017 14:05
Matrix: TCLP Leach Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615400 Analyst: MES Run Date: 05/24/2017 14:10
Collect Date: 05/19/2017 15:30 Dilution: 1 File ID: 12M62322
Sample Tag: 01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
o-Cresol U 50.0 25.0 D023 200000
m-,p-Cresol U 50.0 25.0 D025 200000
1,4-Dichlorobenzene U 50.0 25.0 D027 7500
2,4-Dinitrotoluene U 50.0 25.0 D030 130
Hexachlorobenzene U 50.0 25.0 D032 130
Hexachlorobutadiene U 50.0 25.0 D033 500
Hexachloroethane U 50.0 25.0 D034 3000
Nitrobenzene U 50.0 25.0 D036 2000
Pentachlorophenol U 250 125 D037 100000
Pyridine U 250 125 D038 5000
2,4,5-Trichlorophenol U 50.0 25.0 D041 400000
2,4,6-Trichlorophenol U 50.0 25.0 D042 2000
Surrogate Recovery Lower Limit Upper Limit Q
2-Fluorophenol 41.1 21 100
Phenol-d5 29.5 10 94
Nitrobenzene-d5 84.5 35 114
2-Fluorobiphenyl 78.0 43 116
2,4,6-Tribromophenol 107 10 123
p-Terphenyl-d14 97.8 33 141
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-07 PrePrep Method: N/A Instrument: ICP-THERMO4
Client ID: 17-0751 IR MUD GRID A3 NEW
Prep Method: 3015A Prep Date: 05/23/2017 09:43
Matrix: TCLP Leach Analytical Method: 6010B Cal Date: 05/23/2017 14:24
Workgroup #: WG615308 Analyst: KKB Run Date: 05/23/2017 17:04
Collect Date: 05/19/2017 15:30 Dilution: 1 File ID: T4.052317.170417
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Arsenic, TCLP U 1.00 0.500 D004 5
Barium, TCLP 0.391 0.100 0.0500 D005 100
Page 8 of 16 Generated at May 25, 2017 09:35
Page 47
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Cadmium, TCLP U 0.100 0.0500 D006 1
Chromium, TCLP U 0.200 0.100 D007 5
Lead, TCLP U 1.00 0.500 D008 5
Selenium, TCLP U 0.800 0.400 D010 1
Silver, TCLP U 0.100 0.0500 D011 5
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-07 PrePrep Method: Instrument: CVAA1
Client ID: 17-0751 IR MUD GRID A3 NEW
Prep Method: 7470A Prep Date: 05/23/2017 09:19
Matrix: TCLP Leach Analytical Method: 7470A Cal Date: 05/23/2017 14:40
Workgroup #: WG615315 Analyst: LSJ Run Date: 05/23/2017 15:58
Collect Date: 05/19/2017 15:30 Dilution: 1 File ID: M7.052317.155857
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Mercury U 0.00200 0.00100 D009 0.2
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-09 PrePrep Method: Instrument: HPMS11
Client ID: 17-0751 WEST BOREHOLE RETURN M
Prep Method: 5030B/5030C/5035A Prep Date: N/A
Matrix: TCLP Leach Analytical Method: 8260B Cal Date: 05/16/2017 17:16
Workgroup #: WG615282 Analyst: TMB/JDS Run Date: 05/23/2017 20:20
Collect Date: 05/19/2017 16:18 Dilution: 10 File ID: 11M18582
Sample Tag: DL01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Benzene U 50.0 1.25 D018 500
Carbon tetrachloride U 50.0 2.50 D019 500
Chlorobenzene U 50.0 1.25 D021 100000
Chloroform U 50.0 1.25 D022 6000
1,2-Dichloroethane U 50.0 2.50 D028 500
1,1-Dichloroethene U 50.0 5.00 D029 700
Methyl Ethyl Ketone U 100 25.0 D035 200000
Tetrachloroethene U 50.0 2.50 D039 700
Trichloroethene U 50.0 2.50 D040 500
Vinyl chloride U 100 2.50 D043 200
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 102 86 118
Page 9 of 16 Generated at May 25, 2017 09:35
Page 48
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Surrogate Recovery Lower Limit Upper Limit Q
1,2-Dichloroethane-d4 108 80 120
Toluene-d8 111 88 110 *
4-Bromofluorobenzene 112 86 115
* Surrogate or spike compound out of range
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-09 PrePrep Method: Instrument: HPMS12
Client ID: 17-0751 WEST BOREHOLE RETURN M
Prep Method: 3510C Prep Date: 05/23/2017 14:05
Matrix: TCLP Leach Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615400 Analyst: MES Run Date: 05/24/2017 14:43
Collect Date: 05/19/2017 16:18 Dilution: 1 File ID: 12M62323
Sample Tag: 01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
o-Cresol U 50.0 25.0 D023 200000
m-,p-Cresol U 50.0 25.0 D025 200000
1,4-Dichlorobenzene U 50.0 25.0 D027 7500
2,4-Dinitrotoluene U 50.0 25.0 D030 130
Hexachlorobenzene U 50.0 25.0 D032 130
Hexachlorobutadiene U 50.0 25.0 D033 500
Hexachloroethane U 50.0 25.0 D034 3000
Nitrobenzene U 50.0 25.0 D036 2000
Pentachlorophenol U 250 125 D037 100000
Pyridine U 250 125 D038 5000
2,4,5-Trichlorophenol U 50.0 25.0 D041 400000
2,4,6-Trichlorophenol U 50.0 25.0 D042 2000
Surrogate Recovery Lower Limit Upper Limit Q
2-Fluorophenol 31.3 21 100
Phenol-d5 22.1 10 94
Nitrobenzene-d5 64.5 35 114
2-Fluorobiphenyl 61.6 43 116
2,4,6-Tribromophenol 84.5 10 123
p-Terphenyl-d14 99.8 33 141
U Not detected at or above adjusted sample detection limit
Page 10 of 16 Generated at May 25, 2017 09:35
Page 49
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Sample #: L17051231-09 PrePrep Method: N/A Instrument: ICP-THERMO4
Client ID: 17-0751 WEST BOREHOLE RETURN M
Prep Method: 3015A Prep Date: 05/23/2017 09:43
Matrix: TCLP Leach Analytical Method: 6010B Cal Date: 05/23/2017 14:24
Workgroup #: WG615308 Analyst: KKB Run Date: 05/23/2017 17:07
Collect Date: 05/19/2017 16:18 Dilution: 1 File ID: T4.052317.170759
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Arsenic, TCLP U 1.00 0.500 D004 5
Barium, TCLP 0.512 0.100 0.0500 D005 100
Cadmium, TCLP U 0.100 0.0500 D006 1
Chromium, TCLP U 0.200 0.100 D007 5
Lead, TCLP U 1.00 0.500 D008 5
Selenium, TCLP U 0.800 0.400 D010 1
Silver, TCLP U 0.100 0.0500 D011 5
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-09 PrePrep Method: Instrument: CVAA1
Client ID: 17-0751 WEST BOREHOLE RETURN M
Prep Method: 7470A Prep Date: 05/23/2017 09:19
Matrix: TCLP Leach Analytical Method: 7470A Cal Date: 05/23/2017 14:40
Workgroup #: WG615315 Analyst: LSJ Run Date: 05/23/2017 16:01
Collect Date: 05/19/2017 16:18 Dilution: 1 File ID: M7.052317.160130
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Mercury U 0.00200 0.00100 D009 0.2
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-11 PrePrep Method: Instrument: HPMS11
Client ID: 17-0751 WEST RECLAIMER PIT
Prep Method: 5030B/5030C/5035A Prep Date: N/A
Matrix: TCLP Leach Analytical Method: 8260B Cal Date: 05/16/2017 17:16
Workgroup #: WG615282 Analyst: TMB/JDS Run Date: 05/23/2017 20:49
Collect Date: 05/19/2017 16:30 Dilution: 10 File ID: 11M18583
Sample Tag: DL01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Benzene U 50.0 1.25 D018 500
Carbon tetrachloride U 50.0 2.50 D019 500
Chlorobenzene U 50.0 1.25 D021 100000
Page 11 of 16 Generated at May 25, 2017 09:35
Page 50
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Chloroform U 50.0 1.25 D022 6000
1,2-Dichloroethane U 50.0 2.50 D028 500
1,1-Dichloroethene U 50.0 5.00 D029 700
Methyl Ethyl Ketone U 100 25.0 D035 200000
Tetrachloroethene U 50.0 2.50 D039 700
Trichloroethene U 50.0 2.50 D040 500
Vinyl chloride U 100 2.50 D043 200
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 101 86 118
1,2-Dichloroethane-d4 104 80 120
Toluene-d8 108 88 110
4-Bromofluorobenzene 113 86 115
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-11 PrePrep Method: Instrument: HPMS12
Client ID: 17-0751 WEST RECLAIMER PIT
Prep Method: 3510C Prep Date: 05/23/2017 14:05
Matrix: TCLP Leach Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615400 Analyst: MES Run Date: 05/24/2017 15:16
Collect Date: 05/19/2017 16:30 Dilution: 1 File ID: 12M62324
Sample Tag: 01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
o-Cresol U 50.0 25.0 D023 200000
m-,p-Cresol U 50.0 25.0 D025 200000
1,4-Dichlorobenzene U 50.0 25.0 D027 7500
2,4-Dinitrotoluene U 50.0 25.0 D030 130
Hexachlorobenzene U 50.0 25.0 D032 130
Hexachlorobutadiene U 50.0 25.0 D033 500
Hexachloroethane U 50.0 25.0 D034 3000
Nitrobenzene U 50.0 25.0 D036 2000
Pentachlorophenol U 250 125 D037 100000
Pyridine U 250 125 D038 5000
2,4,5-Trichlorophenol U 50.0 25.0 D041 400000
2,4,6-Trichlorophenol U 50.0 25.0 D042 2000
Surrogate Recovery Lower Limit Upper Limit Q
2-Fluorophenol 43.2 21 100
Phenol-d5 28.7 10 94
Nitrobenzene-d5 84.4 35 114
2-Fluorobiphenyl 77.6 43 116
Page 12 of 16 Generated at May 25, 2017 09:35
Page 51
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 99.9 10 123
p-Terphenyl-d14 93.5 33 141
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-11 PrePrep Method: N/A Instrument: ICP-THERMO4
Client ID: 17-0751 WEST RECLAIMER PIT
Prep Method: 3015A Prep Date: 05/23/2017 09:43
Matrix: TCLP Leach Analytical Method: 6010B Cal Date: 05/23/2017 14:24
Workgroup #: WG615308 Analyst: KKB Run Date: 05/23/2017 17:11
Collect Date: 05/19/2017 16:30 Dilution: 1 File ID: T4.052317.171142
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Arsenic, TCLP U 1.00 0.500 D004 5
Barium, TCLP 0.441 0.100 0.0500 D005 100
Cadmium, TCLP U 0.100 0.0500 D006 1
Chromium, TCLP U 0.200 0.100 D007 5
Lead, TCLP U 1.00 0.500 D008 5
Selenium, TCLP U 0.800 0.400 D010 1
Silver, TCLP U 0.100 0.0500 D011 5
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-11 PrePrep Method: Instrument: CVAA1
Client ID: 17-0751 WEST RECLAIMER PIT
Prep Method: 7470A Prep Date: 05/23/2017 09:19
Matrix: TCLP Leach Analytical Method: 7470A Cal Date: 05/23/2017 14:40
Workgroup #: WG615315 Analyst: LSJ Run Date: 05/23/2017 16:04
Collect Date: 05/19/2017 16:30 Dilution: 1 File ID: M7.052317.160401
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Mercury U 0.00200 0.00100 D009 0.2
U Not detected at or above adjusted sample detection limit
Page 13 of 16 Generated at May 25, 2017 09:35
Page 52
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Sample #: L17051231-13 PrePrep Method: Instrument: HPMS11
Client ID: 17-0751 EAST RECLAIMER NEW MUD
Prep Method: 5030B/5030C/5035A Prep Date: N/A
Matrix: TCLP Leach Analytical Method: 8260B Cal Date: 05/16/2017 17:16
Workgroup #: WG615282 Analyst: TMB/JDS Run Date: 05/23/2017 21:18
Collect Date: 05/19/2017 17:12 Dilution: 10 File ID: 11M18584
Sample Tag: DL01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Benzene U 50.0 1.25 D018 500
Carbon tetrachloride U 50.0 2.50 D019 500
Chlorobenzene U 50.0 1.25 D021 100000
Chloroform U 50.0 1.25 D022 6000
1,2-Dichloroethane U 50.0 2.50 D028 500
1,1-Dichloroethene U 50.0 5.00 D029 700
Methyl Ethyl Ketone U 100 25.0 D035 200000
Tetrachloroethene U 50.0 2.50 D039 700
Trichloroethene U 50.0 2.50 D040 500
Vinyl chloride U 100 2.50 D043 200
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 101 86 118
1,2-Dichloroethane-d4 107 80 120
Toluene-d8 108 88 110
4-Bromofluorobenzene 107 86 115
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-13 PrePrep Method: Instrument: HPMS12
Client ID: 17-0751 EAST RECLAIMER NEW MUD
Prep Method: 3510C Prep Date: 05/23/2017 14:05
Matrix: TCLP Leach Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615400 Analyst: MES Run Date: 05/24/2017 15:49
Collect Date: 05/19/2017 17:12 Dilution: 1 File ID: 12M62325
Sample Tag: 01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
o-Cresol U 50.0 25.0 D023 200000
m-,p-Cresol U 50.0 25.0 D025 200000
1,4-Dichlorobenzene U 50.0 25.0 D027 7500
2,4-Dinitrotoluene U 50.0 25.0 D030 130
Hexachlorobenzene U 50.0 25.0 D032 130
Hexachlorobutadiene U 50.0 25.0 D033 500
Page 14 of 16 Generated at May 25, 2017 09:35
Page 53
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Hexachloroethane U 50.0 25.0 D034 3000
Nitrobenzene U 50.0 25.0 D036 2000
Pentachlorophenol U 250 125 D037 100000
Pyridine U 250 125 D038 5000
2,4,5-Trichlorophenol U 50.0 25.0 D041 400000
2,4,6-Trichlorophenol U 50.0 25.0 D042 2000
Surrogate Recovery Lower Limit Upper Limit Q
2-Fluorophenol 34.8 21 100
Phenol-d5 24.9 10 94
Nitrobenzene-d5 69.3 35 114
2-Fluorobiphenyl 66.2 43 116
2,4,6-Tribromophenol 77.0 10 123
p-Terphenyl-d14 100 33 141
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-13 PrePrep Method: N/A Instrument: ICP-THERMO4
Client ID: 17-0751 EAST RECLAIMER NEW MUD
Prep Method: 3015A Prep Date: 05/23/2017 09:43
Matrix: TCLP Leach Analytical Method: 6010B Cal Date: 05/23/2017 14:24
Workgroup #: WG615308 Analyst: KKB Run Date: 05/23/2017 17:15
Collect Date: 05/19/2017 17:12 Dilution: 1 File ID: T4.052317.171525
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Arsenic, TCLP U 1.00 0.500 D004 5
Barium, TCLP 0.131 0.100 0.0500 D005 100
Cadmium, TCLP U 0.100 0.0500 D006 1
Chromium, TCLP U 0.200 0.100 D007 5
Lead, TCLP U 1.00 0.500 D008 5
Selenium, TCLP U 0.800 0.400 D010 1
Silver, TCLP U 0.100 0.0500 D011 5
U Not detected at or above adjusted sample detection limit
Page 15 of 16 Generated at May 25, 2017 09:35
Page 54
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Sample #: L17051231-13 PrePrep Method: Instrument: CVAA1
Client ID: 17-0751 EAST RECLAIMER NEW MUD
Prep Method: 7470A Prep Date: 05/23/2017 09:19
Matrix: TCLP Leach Analytical Method: 7470A Cal Date: 05/23/2017 14:40
Workgroup #: WG615315 Analyst: LSJ Run Date: 05/23/2017 16:06
Collect Date: 05/19/2017 17:12 Dilution: 1 File ID: M7.052317.160631
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Mercury U 0.00200 0.00100 D009 0.2
U Not detected at or above adjusted sample detection limit
Page 16 of 16 Generated at May 25, 2017 09:35
Page 55
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Sample #: L17051231-02 Client ID: 17-0751 OSG DISPOSAL PIT Matrix: Soil Collect Date: 05/19/2017 13:24
Analyte Result Units Qualifier
Percent Solids 50.0 weight %
Sample #: L17051231-04 Client ID: 17-0751 IR MUD ORIGINAL Matrix: Soil Collect Date: 05/19/2017 15:00
Analyte Result Units Qualifier
Percent Solids 45.2 weight %
Sample #: L17051231-06 Client ID: 17-0751 IR MUD SILO Matrix: Soil Collect Date: 05/19/2017 14:45
Analyte Result Units Qualifier
Percent Solids 49.0 weight %
Sample #: L17051231-08 Client ID: 17-0751 IR MUD GRID A3 NEW Matrix: Soil Collect Date: 05/19/2017 15:30
Analyte Result Units Qualifier
Percent Solids 26.5 weight %
Sample #: L17051231-10 Client ID: 17-0751 WEST BOREHOLE RETURN M
Matrix: Soil Collect Date: 05/19/2017 16:18
Analyte Result Units Qualifier
Percent Solids 41.6 weight %
Sample #: L17051231-12 Client ID: 17-0751 WEST RECLAIMER PIT Matrix: Soil Collect Date: 05/19/2017 16:30
Analyte Result Units Qualifier
Percent Solids 56.8 weight %
Sample #: L17051231-14 Client ID: 17-0751 EAST RECLAIMER NEW MUD
Matrix: Soil Collect Date: 05/19/2017 17:12
Analyte Result Units Qualifier
Percent Solids 1.96 weight %
Page 1 of 1 Generated at May 25, 2017 09:35
Page 56
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac Laboratories Inc.Ohio Valley Division Analyst List
May 25, 2017
001 - BIO-CHEM TESTING WVDEP 220 002 - REIC Consultants, Inc. WVDEP 060003 - Sturm Environmental 004 - MICROBAC PITTSBURGH005 - ES LABORATORIES 006 - ALCOSAN LABORATORIES007 - ALS LABORATORIES 008 - BENCHMARK LABORATORIES010 - MICROBAC CHICAGOLAND AC - AMBER R. CARMICHAELADC - ANTHONY D. CANTER ADG - APRIL D. GREENEALS - ADRIANE L. STEED AWE - ANDREW W. ESSIGAZH - AFTER HOURS BJO - BRIAN J. OGDENBLG - BRENDA L. GREENWALT BNB - Brandi N. BentleyBRG - BRENDA R. GREGORY CAS - Craig A. SmithCEB - CHAD E. BARNES CLC - CHRYS L. CRAWFORDCLS - CARA L. STRICKLER CPD - CHAD P. DAVISCSH - CHRIS S. HILL CV - Carl VolkmanDAK - DEAN A. KETELSEN DCM - DAVID C. MERCKLEDEV - DAVID E. VANDENBERG DIH - DEANNA I. HESSONDLB - DAVID L. BUMGARNER DLP - DOROTHY L. PAYNEDSM - DAVID S. MOSSOR DTG - DOMINIC T. GEHRETECL - ERIC C. LAWSON EPT - ETHAN P. TIDDERP - ERIN R. PORTER FJB - FRANCES J. BOLDENHRF - HEATHER R. FAIRCHILD JDH - JUSTIN D. HESSONJDS - JARED D. SMITH JKP - JACQUELINE K. PARSONSJLD - JESSICA L. DELONG JST - JOSHUA S. TAYLORJTP - JOSHUA T. PEMBERTON JWR - JOHN W. RICHARDSJWS - JACK W. SHEAVES JYH - JI Y. HUKAK - KATHY A. KIRBY KDD - Katelyn D. DaleyKEB - KATIE E. BARNES KHR - KIM H. RHODESKKB - KERRI K. BUCK KRA - KATHY R. ALBERTSONKRP - KATHY R. PARSONS LJH - Lacey J. HendershotLLS - LARRY L. STEPHENS LSB - LESLIE S. BUCINALSJ - LAURA S. JONES MAP - MARLA A. PORTERMBK - MORGAN B. KNOWLTON MES - MARY E. SCHILLINGMMB - MAREN M. BEERY MRT - MICHELLE R. TAYLOROJE - OMOYEMWEN J. ENGLISH PDM - PIERCE D. MORRISPIT - MICROBAC WARRENDALE REK - BOB E. KYERRLB - BOB BUCHANAN RNP - RICK N. PETTYSAV - SARAH A. VANDENBERG SCA - SUEELLEN C. ADAMSSCB - SARAH C. BOGOLIN SCJ - SUE ELLEN C. JOHNSONSDC - SHALYN D. CONLEY TB - TODD BOYLETMB - TIFFANY M. BAILEY TMM - TAMMY M. MORRISVC - VICKI COLLIER WTD - WADE T. DELONGXXX - UNAVAILABLE OR SUBCONTRACT ZTB - ZACH T. BARNES
Page 57
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
List of Valid QualifiersMay 25, 2017
Qualkey: STD_ND=U
Microbac Laboratories Inc.
Qualifier Description
*+<>AB
B1B3C
CGDLE
EDLEMPCF, SFL
FP1H1IJ
J,BJ,H1J,PJ,SLL1L2MN
NAND, SND,LNFNFLNINRNSPQ
QNSRARES
SMISPTIC
TNTCU
U,H1UJWX
X, SYZ
Surrogate or spike compound out of rangeCorrelation coefficient for the MSA is less than 0.995Result is less than the associated numerical value.Result is greater than the associated numerical value.See the report narrativeAnalyte present in method blankTarget analyte detected in method blank at or above the method reporting limitTarget analyte detected in calibration blank at or above the method reporting limitConfirmed by GC/MSConfluent growthSurrogate or spike compound was diluted outEstimated concentration due to sample matrix interferenceElevated sample reporting limits, presence of non-target analytesEstimated Maximum Possible ConcentrationEstimated result below quantitation limit; method of standard additions(MSA)Free LiquidDid not ignite.Sample analysis performed past holding time.Semiquantitative result (out of instrument calibration range)The analyte was positively identified, but the quantitation was below the RLAnalyte detected in both the method blank and sample above the MDL.The analyte was positively identified, but the quantitation was below the RL. Sample analysis performed past holding timeEstimate; columns don't agree to within 40%Estimated concentration; analyzed by method of standard addition (MSA)Sample reporting limits elevated due to matrix interferenceThe associated blank spike (LCS) recovery was above the laboratory acceptance limits.The associated blank spike (LCS) recovery was below the laboratory acceptance limits.Matrix effect; the concentration is an estimate due to matrix effect.Tentatively identified compound(TIC)Not applicableNot detected; analyzed by method of standard addition (MSA)Not detected; sample reporting limit (RL) elevated due to interferenceNot found by library searchNo free liquidNon-ignitableAnalyte is not required to be analyzedNot spikedConcentrations >40% difference between the two GC columnsOne or more quality control criteria failed. See narrative.Quantity of sample not sufficient to perform analysisReanalysis confirms reported resultsReanalysis confirms sample matrix interferenceAnalyzed by method of standard addition (MSA)Sample matrix interference on surrogateReported results are for spike compounds onlyLibrary Search CompoundToo numerous to countNot detected at or above adjusted sample detection limitNot detected; sample analysis performed past holding time.Undetected; the MDL and RL are estimated due to quality control discrepancies.Post-digestion spike for furnace AA out of control limitsExceeds regulatory limitExceeds regulatory limit; method of standard additions (MSA)This analyte is not on the laboratory's current scope of accreditation.Cannot be resolved from isomer - see below
Page 58
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Page 59
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Page 60
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Internal Chain of Custody Report
Login:
Account:
Project:
Samples:
Due Date:
L17051231
2755
2755.044
14
24-MAY-2017
A1 - Sample Archive (COLD)A2 - Sample Archive (AMBIENT)F1 - Volatiles Freezer in LoginV1 - Volatiles Refrigerator in LoginW1 - Walkin Cooler in Login
Microbac Laboratories Inc.
L17051231-01
L17051231-02
L17051231-02
L17051231-03
L17051231-04
911918
911919
911920
911921
911922
Samplenum
Samplenum
Samplenum
Samplenum
Samplenum
Container ID
Container ID
Container ID
Container ID
Container ID
1
1
1
1
1
Bottle:
Bottle:
Bottle:
Bottle:
Bottle:
1
2
3
1
2
1
2
3
4
1
2
3
1
2
LOGIN
PREP
STORE
LOGIN
ANALYZ
LOGIN
PREP
PREP
STORE
LOGIN
PREP
STORE
LOGIN
ANALYZ
COOLER
W1
TCL
COOLER
V1
COOLER
W1
EXT
DIG
COOLER
W1
TCL
COOLER
V1
W1
TCL
A2
V1
ORG4
W1
EXT
DIG
A2
W1
TCL
A2
V1
ORG4
22-MAY-2017 10:46
22-MAY-2017 11:26
22-MAY-2017 15:43
22-MAY-2017 10:46
22-MAY-2017 10:57
22-MAY-2017 10:46
22-MAY-2017 11:53
22-MAY-2017 14:59
22-MAY-2017 16:26
22-MAY-2017 10:46
22-MAY-2017 11:26
22-MAY-2017 15:43
22-MAY-2017 10:46
22-MAY-2017 10:57
CLS
BNB
BRG
CLS
JDS
CLS
CPD
ZTB
CLS
CLS
BNB
BRG
CLS
JDS
BRG
BNB
CLS
CLS
JDH
AC
BRG
BNB
CLS
Seq.
Seq.
Seq.
Seq.
Seq.
Purpose
Purpose
Purpose
Purpose
Purpose
From
From
From
From
From
To
To
To
To
To
Date/Time
Date/Time
Date/Time
Date/Time
Date/Time
Accept
Accept
Accept
Accept
Accept
Relinquish
Relinquish
Relinquish
Relinquish
Relinquish
Products
Products
Products
Products
Products
TC-EX
8260
8270
TC-EX
8260
pH
pH
pH
pH
pH
Page 61
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Internal Chain of Custody Report
Login:
Account:
Project:
Samples:
Due Date:
L17051231
2755
2755.044
14
24-MAY-2017
A1 - Sample Archive (COLD)A2 - Sample Archive (AMBIENT)F1 - Volatiles Freezer in LoginV1 - Volatiles Refrigerator in LoginW1 - Walkin Cooler in Login
Microbac Laboratories Inc.
L17051231-04
L17051231-05
L17051231-06
L17051231-06
911923
911924
911925
911926
Samplenum
Samplenum
Samplenum
Samplenum
Container ID
Container ID
Container ID
Container ID
1
1
1
1
Bottle:
Bottle:
Bottle:
Bottle:
1
2
3
4
1
2
3
1
2
1
2
3
4
LOGIN
PREP
PREP
STORE
LOGIN
PREP
STORE
LOGIN
ANALYZ
LOGIN
PREP
PREP
STORE
COOLER
W1
EXT
DIG
COOLER
W1
TCL
COOLER
V1
COOLER
W1
EXT
DIG
W1
EXT
DIG
A2
W1
TCL
A2
V1
ORG4
W1
EXT
DIG
A2
22-MAY-2017 10:46
22-MAY-2017 11:53
22-MAY-2017 14:59
22-MAY-2017 16:26
22-MAY-2017 10:46
22-MAY-2017 11:26
22-MAY-2017 15:42
22-MAY-2017 10:46
22-MAY-2017 10:57
22-MAY-2017 10:46
22-MAY-2017 11:55
22-MAY-2017 14:59
22-MAY-2017 16:26
CLS
CPD
ZTB
CLS
CLS
BNB
BRG
CLS
JDS
CLS
CPD
ZTB
CLS
CLS
JDH
AC
BRG
BNB
CLS
CLS
JDH
AC
Seq.
Seq.
Seq.
Seq.
Purpose
Purpose
Purpose
Purpose
From
From
From
From
To
To
To
To
Date/Time
Date/Time
Date/Time
Date/Time
Accept
Accept
Accept
Accept
Relinquish
Relinquish
Relinquish
Relinquish
Products
Products
Products
Products
8270
TC-EX
8260
8270
pH
pH
pH
pH
Page 62
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Internal Chain of Custody Report
Login:
Account:
Project:
Samples:
Due Date:
L17051231
2755
2755.044
14
24-MAY-2017
A1 - Sample Archive (COLD)A2 - Sample Archive (AMBIENT)F1 - Volatiles Freezer in LoginV1 - Volatiles Refrigerator in LoginW1 - Walkin Cooler in Login
Microbac Laboratories Inc.
L17051231-07
L17051231-08
L17051231-08
L17051231-09
L17051231-10
911927
911928
911929
911930
911931
Samplenum
Samplenum
Samplenum
Samplenum
Samplenum
Container ID
Container ID
Container ID
Container ID
Container ID
1
1
1
1
1
Bottle:
Bottle:
Bottle:
Bottle:
Bottle:
1
2
3
1
2
1
2
3
4
1
2
3
1
2
LOGIN
PREP
STORE
LOGIN
ANALYZ
LOGIN
PREP
PREP
STORE
LOGIN
PREP
STORE
LOGIN
ANALYZ
COOLER
W1
TCL
COOLER
V1
COOLER
W1
EXT
DIG
COOLER
W1
TCL
COOLER
V1
W1
TCL
A2
V1
ORG4
W1
EXT
DIG
A2
W1
TCL
A2
V1
ORG4
22-MAY-2017 10:46
22-MAY-2017 11:26
22-MAY-2017 15:43
22-MAY-2017 10:46
22-MAY-2017 10:57
22-MAY-2017 10:46
22-MAY-2017 11:53
22-MAY-2017 14:59
22-MAY-2017 16:25
22-MAY-2017 10:46
22-MAY-2017 11:26
22-MAY-2017 15:42
22-MAY-2017 10:46
22-MAY-2017 10:57
CLS
BNB
BRG
CLS
JDS
CLS
CPD
ZTB
CLS
CLS
BNB
BRG
CLS
JDS
BRG
BNB
CLS
CLS
JDH
AC
BRG
BNB
CLS
Seq.
Seq.
Seq.
Seq.
Seq.
Purpose
Purpose
Purpose
Purpose
Purpose
From
From
From
From
From
To
To
To
To
To
Date/Time
Date/Time
Date/Time
Date/Time
Date/Time
Accept
Accept
Accept
Accept
Accept
Relinquish
Relinquish
Relinquish
Relinquish
Relinquish
Products
Products
Products
Products
Products
TC-EX
8260
8270
TC-EX
8260
pH
pH
pH
pH
pH
Page 63
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Internal Chain of Custody Report
Login:
Account:
Project:
Samples:
Due Date:
L17051231
2755
2755.044
14
24-MAY-2017
A1 - Sample Archive (COLD)A2 - Sample Archive (AMBIENT)F1 - Volatiles Freezer in LoginV1 - Volatiles Refrigerator in LoginW1 - Walkin Cooler in Login
Microbac Laboratories Inc.
L17051231-10
L17051231-11
L17051231-12
L17051231-12
911932
911933
911934
911935
Samplenum
Samplenum
Samplenum
Samplenum
Container ID
Container ID
Container ID
Container ID
1
1
1
1
Bottle:
Bottle:
Bottle:
Bottle:
1
2
3
4
1
2
3
1
2
1
2
3
4
LOGIN
PREP
PREP
STORE
LOGIN
PREP
STORE
LOGIN
ANALYZ
LOGIN
PREP
PREP
STORE
COOLER
W1
EXT
DIG
COOLER
W1
TCL
COOLER
V1
COOLER
W1
EXT
DIG
W1
EXT
DIG
A2
W1
TCL
A2
V1
ORG4
W1
EXT
DIG
A2
22-MAY-2017 10:46
22-MAY-2017 11:53
22-MAY-2017 14:59
22-MAY-2017 16:25
22-MAY-2017 10:46
22-MAY-2017 11:26
22-MAY-2017 15:42
22-MAY-2017 10:46
22-MAY-2017 10:57
22-MAY-2017 10:46
22-MAY-2017 11:53
22-MAY-2017 14:59
22-MAY-2017 16:25
CLS
CPD
ZTB
CLS
CLS
BNB
BRG
CLS
JDS
CLS
CPD
ZTB
CLS
CLS
JDH
AC
BRG
BNB
CLS
CLS
JDH
AC
Seq.
Seq.
Seq.
Seq.
Purpose
Purpose
Purpose
Purpose
From
From
From
From
To
To
To
To
Date/Time
Date/Time
Date/Time
Date/Time
Accept
Accept
Accept
Accept
Relinquish
Relinquish
Relinquish
Relinquish
Products
Products
Products
Products
8270
TC-EX
8260
8270
pH
pH
pH
pH
Page 64
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Internal Chain of Custody Report
Login:
Account:
Project:
Samples:
Due Date:
L17051231
2755
2755.044
14
24-MAY-2017
A1 - Sample Archive (COLD)A2 - Sample Archive (AMBIENT)F1 - Volatiles Freezer in LoginV1 - Volatiles Refrigerator in LoginW1 - Walkin Cooler in Login
Microbac Laboratories Inc.
L17051231-13
L17051231-14
L17051231-14
911936
911937
911938
Samplenum
Samplenum
Samplenum
Container ID
Container ID
Container ID
1
1
1
Bottle:
Bottle:
Bottle:
1
2
3
1
2
1
2
3
4
LOGIN
PREP
STORE
LOGIN
ANALYZ
LOGIN
PREP
PREP
STORE
COOLER
W1
TCL
COOLER
V1
COOLER
W1
EXT
DIG
W1
TCL
A2
V1
ORG4
W1
EXT
DIG
A2
22-MAY-2017 10:46
22-MAY-2017 11:26
22-MAY-2017 15:43
22-MAY-2017 10:46
22-MAY-2017 10:57
22-MAY-2017 10:46
22-MAY-2017 11:53
22-MAY-2017 14:59
22-MAY-2017 16:25
CLS
BNB
BRG
CLS
JDS
CLS
CPD
ZTB
CLS
BRG
BNB
CLS
CLS
JDH
AC
Seq.
Seq.
Seq.
Purpose
Purpose
Purpose
From
From
From
To
To
To
Date/Time
Date/Time
Date/Time
Accept
Accept
Accept
Relinquish
Relinquish
Relinquish
Products
Products
Products
TC-EX
8260
8270
pH
pH
pH
Page 65
L17051231 / Revision: 0 / 65 total pages Generated: 05/25/2017 09:32
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Laboratory Report Number: L17051231
Frank ZingalesOhio Environmental Protection Agency2110 East Aurora RoadTwinsburg, OH 44087
Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac’s Ohio Valley Division (OVD). If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed below.
Laboratory Contact:Michelle Taylor – Client Services Specialist(740) 373-4071Michelle.Taylor@microbac.com
I certify that all test results meet all of the requirements of the accrediting authority listed below. All results for soil samples are reported on a 'dry-weight' basis unless specified otherwise. Analytical results for water and wastes are reported on a 'as received' basis unless specified otherwise. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received.
This report was certified on May 30 2017
Leslie Bucina – Managing Director State of Origin: OHAccrediting Authority: N/A ID:OH00218QAPP: Microbac OVD
Microbac Laboratories * Ohio Valley Division158 Starlite Drive, Marietta, OH 45750 * T: (740) 373-4071 F: (740) 373-4835 * www.microbac.com
Page 1
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Record of Sample Receipt and InspectionComments/DiscrepanciesThis is the record of the shipment conditions and the inspection records for the samples received and reported as a sample delivery group (SDG). All of the samples were inspected and observed to conform to our receipt policies, except as noted below.
There were no discrepancies.Discrepancy Resolution
CoolersCooler # Temperature
GunTemperature COC # Airbill # Temp Required?
0016980 I 2.0 X
Inspection Checklist
# Question Result
1 Were shipping coolers sealed? NA
2 Were custody seals intact? NA
3 Were cooler temperatures in range of 0-6? Yes
4 Was ice present? Yes
5 Were COC's received/information complete/signed and dated? Yes
6 Were sample containers intact and match COC? Yes
7 Were sample labels intact and match COC? Yes
8 Were the correct containers and volumes received? Yes
9 Were samples received within EPA hold times? Yes
10 Were correct preservatives used? (water only) NA
11 Were pH ranges acceptable? (voa's excluded) NA
12 Were VOA samples free of headspace (less than 6mm)? NA
Microbac Laboratories ● Ohio Valley Division158 Starlite Drive, Marietta, OH 45750 ● T: (740)373-4071 F: (740)373-4835
www.microbac.com
Page 2
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Samples ReceivedClient ID Laboratory ID Date Collected Date Received
17-0751 OSG DISPOSAL PIT L17051231-01 05/19/2017 13:24 05/19/2017 20:10
17-0751 OSG DISPOSAL PIT L17051231-02 05/19/2017 13:24 05/19/2017 20:10
17-0751 IR MUD ORIGINAL L17051231-03 05/19/2017 15:00 05/19/2017 20:10
17-0751 IR MUD ORIGINAL L17051231-04 05/19/2017 15:00 05/19/2017 20:10
17-0751 IR MUD SILO L17051231-05 05/19/2017 14:45 05/19/2017 20:10
17-0751 IR MUD SILO L17051231-06 05/19/2017 14:45 05/19/2017 20:10
17-0751 IR MUD GRID A3 NEW L17051231-07 05/19/2017 15:30 05/19/2017 20:10
17-0751 IR MUD GRID A3 NEW L17051231-08 05/19/2017 15:30 05/19/2017 20:10
17-0751 WEST BOREHOLE RETURN M
L17051231-09 05/19/2017 16:18 05/19/2017 20:10
17-0751 WEST BOREHOLE RETURN M
L17051231-10 05/19/2017 16:18 05/19/2017 20:10
17-0751 WEST RECLAIMER PIT L17051231-11 05/19/2017 16:30 05/19/2017 20:10
17-0751 WEST RECLAIMER PIT L17051231-12 05/19/2017 16:30 05/19/2017 20:10
17-0751 EAST RECLAIMER NEW MUD
L17051231-13 05/19/2017 17:12 05/19/2017 20:10
17-0751 EAST RECLAIMER NEW MUD
L17051231-14 05/19/2017 17:12 05/19/2017 20:10
Microbac Laboratories ● Ohio Valley Division158 Starlite Drive, Marietta, OH 45750 ● T: (740)373-4071 F: (740)373-4835
www.microbac.com
Page 3
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisSample #: L17051231-02 PrePrep Method: N/A Instrument: HPMS9
Client ID: 17-0751 OSG DISPOSAL PIT Prep Method: 5030B/5030C/5035A Prep Date: 05/23/2017 09:14
Matrix: Soil Analytical Method: 8260B Cal Date: 05/23/2017 14:46
Workgroup #: WG615352 Analyst: ADC Run Date: 05/23/2017 20:47
Collect Date: 05/19/2017 13:24 Dilution: 1 File ID: 9M980452
Sample Tag: 01 Units: ug/kg Percent Solid: 50.0
Analyte CAS # Result Qual RL MDL
Acetone 67-64-1 U 19.4 9.68
Benzene 71-43-2 5.32 J 9.68 0.968
Bromobenzene 108-86-1 U 9.68 0.968
Bromochloromethane 74-97-5 U 9.68 1.94
Bromodichloromethane 75-27-4 U 9.68 0.968
Bromoform 75-25-2 U 9.68 0.968
Bromomethane 74-83-9 U 19.4 1.94
2-Butanone 78-93-3 U 19.4 4.84
n-Butylbenzene 104-51-8 20.0 9.68 0.968
sec-Butylbenzene 135-98-8 6.38 J 9.68 0.968
tert-Butylbenzene 98-06-6 3.66 J 9.68 0.968
Carbon disulfide 75-15-0 4.53 J 9.68 0.968
Carbon tetrachloride 56-23-5 U 9.68 0.968
Chlorobenzene 108-90-7 U 9.68 0.968
Chlorodibromomethane 124-48-1 U 9.68 0.968
Chloroethane 75-00-3 U 19.4 1.94
2-Chloroethyl vinyl ether 110-75-8 U 19.4 3.87
Chloroform 67-66-3 U 9.68 0.968
Chloromethane 74-87-3 U 19.4 3.87
2-Chlorotoluene 95-49-8 U 9.68 0.968
4-Chlorotoluene 106-43-4 U 9.68 0.968
1,2-Dibromo-3-chloropropane 96-12-8 U 9.68 3.87
1,2-Dibromoethane 106-93-4 U 9.68 0.968
Dibromomethane 74-95-3 U 9.68 0.968
1,2-Dichlorobenzene 95-50-1 U 9.68 0.968
1,3-Dichlorobenzene 541-73-1 U 9.68 0.968
1,4-Dichlorobenzene 106-46-7 U 9.68 0.968
Dichlorodifluoromethane 75-71-8 U 19.4 1.94
1,1-Dichloroethane 75-34-3 U 9.68 1.94
1,2-Dichloroethane 107-06-2 U 9.68 0.968
1,1-Dichloroethene 75-35-4 U 9.68 0.968
cis-1,2-Dichloroethene 156-59-2 U 9.68 0.968
trans-1,2-Dichloroethene 156-60-5 U 9.68 0.968
Page 1 of 30 Generated at May 30, 2017 08:37
Page 4
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
1,2-Dichloropropane 78-87-5 U 9.68 0.968
1,3-Dichloropropane 142-28-9 U 9.68 0.968
2,2-Dichloropropane 594-20-7 U 9.68 0.968
cis-1,3-Dichloropropene 10061-01-5 U 9.68 0.968
trans-1,3-Dichloropropene 10061-02-6 U 9.68 0.968
1,1-Dichloropropene 563-58-6 U 9.68 0.968
Ethylbenzene 100-41-4 5.91 J 9.68 0.968
2-Hexanone 591-78-6 45.8 19.4 4.84
Hexachlorobutadiene 87-68-3 U 9.68 0.968
Isopropylbenzene 98-82-8 3.50 J 9.68 0.968
p-Isopropyltoluene 99-87-6 9.17 J 9.68 0.968
4-Methyl-2-pentanone 108-10-1 U 19.4 4.84
Methylene chloride 75-09-2 U 9.68 1.94
Naphthalene 91-20-3 11.0 J 19.4 0.968
n-Propylbenzene 103-65-1 6.84 J 9.68 0.968
Styrene 100-42-5 U 9.68 0.968
1,1,1,2-Tetrachloroethane 630-20-6 U 9.68 0.968
1,1,2,2-Tetrachloroethane 79-34-5 U 9.68 0.968
Tetrachloroethene 127-18-4 3.54 J 9.68 0.968
Toluene 108-88-3 16.3 9.68 0.968
1,2,3-Trichlorobenzene 87-61-6 15.7 9.68 0.968
1,2,4-Trichlorobenzene 120-82-1 U 9.68 0.968
1,1,1-Trichloroethane 71-55-6 U 9.68 0.968
1,1,2-Trichloroethane 79-00-5 U 9.68 0.968
Trichloroethene 79-01-6 U 9.68 0.968
Trichlorofluoromethane 75-69-4 U 19.4 1.94
1,2,3-Trichloropropane 96-18-4 U 9.68 1.94
1,2,4-Trimethylbenzene 95-63-6 28.7 9.68 0.968
1,3,5-Trimethylbenzene 108-67-8 72.6 9.68 0.968
Vinyl acetate 108-05-4 U 19.4 4.84
Vinyl chloride 75-01-4 U 19.4 1.94
o-Xylene 95-47-6 29.2 9.68 0.968
m-,p-Xylene 179601-23-1 23.0 9.68 0.968
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 100 80 120
1,2-Dichloroethane-d4 99.1 80 120
Toluene-d8 115 81 117
4-Bromofluorobenzene 150 74 121 *
* Surrogate or spike compound out of range
Page 2 of 30 Generated at May 30, 2017 08:37
Page 5
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisJ The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-02 PrePrep Method: N/A Instrument: HPMS12
Client ID: 17-0751 OSG DISPOSAL PIT Prep Method: 3546 Prep Date: 05/22/2017 11:48
Matrix: Soil Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615227 Analyst: SCB Run Date: 05/23/2017 15:49
Collect Date: 05/19/2017 13:24 Dilution: 1 File ID: 12M62307
Sample Tag: 01 Units: ug/kg Percent Solid: 50.0
Analyte CAS # Result Qual RL MDL
1,2,4-Trichlorobenzene 120-82-1 U 351 175
1,2-Dichlorobenzene 95-50-1 U 351 175
1,3-Dichlorobenzene 541-73-1 U 351 175
1,4-Dichlorobenzene 106-46-7 U 351 175
2,4,5-Trichlorophenol 95-95-4 U 351 175
2,4,6-Trichlorophenol 88-06-2 U 351 175
2,4-Dichlorophenol 120-83-2 U 351 175
2,4-Dimethylphenol 105-67-9 U 351 175
2,4-Dinitrophenol 51-28-5 U 1750 875
2,4-Dinitrotoluene 121-14-2 U 351 175
2,6-Dinitrotoluene 606-20-2 U 351 175
2-Chloronaphthalene 91-58-7 U 351 175
2-Chlorophenol 95-57-8 U 351 175
2-Methylnaphthalene 91-57-6 497 351 175
2-Methylphenol 95-48-7 U 351 175
2-Nitroaniline 88-74-4 U 1750 875
2-Nitrophenol 88-75-5 U 351 175
3,3'-Dichlorobenzidine 91-94-1 U 701 351
3-,4-Methylphenol 65794-96-9 U 351 175
3-Nitroaniline 99-09-2 U 1750 875
4,6-Dinitro-2-methylphenol 534-52-1 U 1750 875
4-Bromophenyl-phenylether 101-55-3 U 351 175
4-Chloro-3-methylphenol 59-50-7 U 351 175
4-Chloroaniline 106-47-8 U 351 175
4-Chlorophenyl-phenyl ether 7005-72-3 U 351 175
4-Nitroaniline 100-01-6 U 1750 875
4-Nitrophenol 100-02-7 U 1750 875
Acenaphthene 83-32-9 U 351 175
Acenaphthylene 208-96-8 U 351 175
Anthracene 120-12-7 U 351 175
Page 3 of 30 Generated at May 30, 2017 08:37
Page 6
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Benzo(a)anthracene 56-55-3 U 351 175
Benzo(a)pyrene 50-32-8 U 351 175
Benzo(b)fluoranthene 205-99-2 U 351 175
Benzo(g,h,i)Perylene 191-24-2 U 351 175
Benzo(k)fluoranthene 207-08-9 U 351 175
Benzoic acid 65-85-0 U 10600 701
Benzyl alcohol 100-51-6 U 351 175
Bis(2-Chloroethoxy)Methane 111-91-1 U 351 175
Bis(2-Chloroethyl)ether 111-44-4 U 351 175
bis(2-Chloroisopropyl)ether 39638-32-9 U 351 175
bis(2-Ethylhexyl)phthalate 117-81-7 U 351 175
Butylbenzylphthalate 85-68-7 U 351 175
Chrysene 218-01-9 U 351 175
Di-N-Butylphthalate 84-74-2 U 351 175
Di-n-octylphthalate 117-84-0 U 351 175
Dibenzo(a,h)Anthracene 53-70-3 U 351 175
Dibenzofuran 132-64-9 U 351 175
Diethylphthalate 84-66-2 U 351 175
Dimethylphthalate 131-11-3 U 351 175
Fluoranthene 206-44-0 U 351 175
Fluorene 86-73-7 U 351 175
Hexachlorobenzene 118-74-1 U 351 175
Hexachlorobutadiene 87-68-3 U 351 175
Hexachlorocyclopentadiene 77-47-4 U 1590 797
Hexachloroethane 67-72-1 U 351 175
Indeno(1,2,3-cd)pyrene 193-39-5 U 351 175
Isophorone 78-59-1 U 351 175
Diphenylamine/n-Nitrosodiphenylamine 86-30-6 755 351 175
N-Nitrosodipropylamine 621-64-7 U 351 175
Naphthalene 91-20-3 372 351 175
Nitrobenzene 98-95-3 U 351 175
Pentachlorophenol 87-86-5 U 1750 875
Phenanthrene 85-01-8 193 J 351 175
Phenol 108-95-2 U 351 175
Pyrene 129-00-0 U 351 175
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 101 19 122
2-Fluorobiphenyl 77.8 30 115
2-Fluorophenol 67.6 25 121
Page 4 of 30 Generated at May 30, 2017 08:37
Page 7
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisNitrobenzene-d5 86.7 23 120
p-Terphenyl-d14 92.1 18 137
Phenol-d5 69.3 24 113
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-04 PrePrep Method: N/A Instrument: HPMS9
Client ID: 17-0751 IR MUD ORIGINAL Prep Method: 5030B/5030C/5035A Prep Date: 05/23/2017 09:15
Matrix: Soil Analytical Method: 8260B Cal Date: 05/23/2017 14:46
Workgroup #: WG615352 Analyst: ADC Run Date: 05/23/2017 17:46
Collect Date: 05/19/2017 15:00 Dilution: 1 File ID: 9M980446
Sample Tag: 01 Units: ug/kg Percent Solid: 45.2
Analyte CAS # Result Qual RL MDL
Acetone 67-64-1 23.9 22.1 11.1
Benzene 71-43-2 3.16 J 11.1 1.11
Bromobenzene 108-86-1 U 11.1 1.11
Bromochloromethane 74-97-5 U 11.1 2.21
Bromodichloromethane 75-27-4 U 11.1 1.11
Bromoform 75-25-2 U 11.1 1.11
Bromomethane 74-83-9 U 22.1 2.21
2-Butanone 78-93-3 U 22.1 5.53
n-Butylbenzene 104-51-8 1.44 J 11.1 1.11
sec-Butylbenzene 135-98-8 U 11.1 1.11
tert-Butylbenzene 98-06-6 U 11.1 1.11
Carbon disulfide 75-15-0 8.31 J 11.1 1.11
Carbon tetrachloride 56-23-5 U 11.1 1.11
Chlorobenzene 108-90-7 U 11.1 1.11
Chlorodibromomethane 124-48-1 U 11.1 1.11
Chloroethane 75-00-3 U 22.1 2.21
2-Chloroethyl vinyl ether 110-75-8 U 22.1 4.43
Chloroform 67-66-3 U 11.1 1.11
Chloromethane 74-87-3 U 22.1 4.43
2-Chlorotoluene 95-49-8 U 11.1 1.11
4-Chlorotoluene 106-43-4 U 11.1 1.11
1,2-Dibromo-3-chloropropane 96-12-8 U 11.1 4.43
1,2-Dibromoethane 106-93-4 U 11.1 1.11
Dibromomethane 74-95-3 U 11.1 1.11
1,2-Dichlorobenzene 95-50-1 U 11.1 1.11
1,3-Dichlorobenzene 541-73-1 U 11.1 1.11
1,4-Dichlorobenzene 106-46-7 U 11.1 1.11
Page 5 of 30 Generated at May 30, 2017 08:37
Page 8
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Dichlorodifluoromethane 75-71-8 U 22.1 2.21
1,1-Dichloroethane 75-34-3 U 11.1 2.21
1,2-Dichloroethane 107-06-2 U 11.1 1.11
1,1-Dichloroethene 75-35-4 U 11.1 1.11
cis-1,2-Dichloroethene 156-59-2 U 11.1 1.11
trans-1,2-Dichloroethene 156-60-5 U 11.1 1.11
1,2-Dichloropropane 78-87-5 U 11.1 1.11
1,3-Dichloropropane 142-28-9 U 11.1 1.11
2,2-Dichloropropane 594-20-7 U 11.1 1.11
cis-1,3-Dichloropropene 10061-01-5 U 11.1 1.11
trans-1,3-Dichloropropene 10061-02-6 U 11.1 1.11
1,1-Dichloropropene 563-58-6 U 11.1 1.11
Ethylbenzene 100-41-4 2.42 J 11.1 1.11
2-Hexanone 591-78-6 U 22.1 5.53
Hexachlorobutadiene 87-68-3 U 11.1 1.11
Isopropylbenzene 98-82-8 U 11.1 1.11
p-Isopropyltoluene 99-87-6 U 11.1 1.11
4-Methyl-2-pentanone 108-10-1 U 22.1 5.53
Methylene chloride 75-09-2 U 11.1 2.21
Naphthalene 91-20-3 4.18 J 22.1 1.11
n-Propylbenzene 103-65-1 U 11.1 1.11
Styrene 100-42-5 U 11.1 1.11
1,1,1,2-Tetrachloroethane 630-20-6 U 11.1 1.11
1,1,2,2-Tetrachloroethane 79-34-5 U 11.1 1.11
Tetrachloroethene 127-18-4 9.55 J 11.1 1.11
Toluene 108-88-3 6.40 J 11.1 1.11
1,2,3-Trichlorobenzene 87-61-6 2.10 J 11.1 1.11
1,2,4-Trichlorobenzene 120-82-1 1.28 J 11.1 1.11
1,1,1-Trichloroethane 71-55-6 U 11.1 1.11
1,1,2-Trichloroethane 79-00-5 U 11.1 1.11
Trichloroethene 79-01-6 U 11.1 1.11
Trichlorofluoromethane 75-69-4 U 22.1 2.21
1,2,3-Trichloropropane 96-18-4 U 11.1 2.21
1,2,4-Trimethylbenzene 95-63-6 5.53 J 11.1 1.11
1,3,5-Trimethylbenzene 108-67-8 2.69 J 11.1 1.11
Vinyl acetate 108-05-4 U 22.1 5.53
Vinyl chloride 75-01-4 U 22.1 2.21
o-Xylene 95-47-6 4.26 J 11.1 1.11
m-,p-Xylene 179601-23-1 7.99 J 11.1 1.11
Page 6 of 30 Generated at May 30, 2017 08:37
Page 9
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisSurrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 102 80 120
1,2-Dichloroethane-d4 100 80 120
Toluene-d8 113 81 117
4-Bromofluorobenzene 127 74 121 *
* Surrogate or spike compound out of range
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-04 PrePrep Method: N/A Instrument: HPMS12
Client ID: 17-0751 IR MUD ORIGINAL Prep Method: 3546 Prep Date: 05/22/2017 11:48
Matrix: Soil Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615227 Analyst: SCB Run Date: 05/23/2017 13:03
Collect Date: 05/19/2017 15:00 Dilution: 1 File ID: 12M62302
Sample Tag: 01 Units: ug/kg Percent Solid: 45.2
Analyte CAS # Result Qual RL MDL
1,2,4-Trichlorobenzene 120-82-1 U 345 172
1,2-Dichlorobenzene 95-50-1 U 345 172
1,3-Dichlorobenzene 541-73-1 U 345 172
1,4-Dichlorobenzene 106-46-7 U 345 172
2,4,5-Trichlorophenol 95-95-4 U 345 172
2,4,6-Trichlorophenol 88-06-2 U 345 172
2,4-Dichlorophenol 120-83-2 U 345 172
2,4-Dimethylphenol 105-67-9 U 345 172
2,4-Dinitrophenol 51-28-5 U 1720 861
2,4-Dinitrotoluene 121-14-2 U 345 172
2,6-Dinitrotoluene 606-20-2 U 345 172
2-Chloronaphthalene 91-58-7 U 345 172
2-Chlorophenol 95-57-8 U 345 172
2-Methylnaphthalene 91-57-6 U 345 172
2-Methylphenol 95-48-7 U 345 172
2-Nitroaniline 88-74-4 U 1720 861
2-Nitrophenol 88-75-5 U 345 172
3,3'-Dichlorobenzidine 91-94-1 U 690 345
3-,4-Methylphenol 65794-96-9 U 345 172
3-Nitroaniline 99-09-2 U 1720 861
4,6-Dinitro-2-methylphenol 534-52-1 U 1720 861
4-Bromophenyl-phenylether 101-55-3 U 345 172
4-Chloro-3-methylphenol 59-50-7 U 345 172
4-Chloroaniline 106-47-8 U 345 172
Page 7 of 30 Generated at May 30, 2017 08:37
Page 10
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
4-Chlorophenyl-phenyl ether 7005-72-3 U 345 172
4-Nitroaniline 100-01-6 U 1720 861
4-Nitrophenol 100-02-7 U 1720 861
Acenaphthene 83-32-9 U 345 172
Acenaphthylene 208-96-8 U 345 172
Anthracene 120-12-7 U 345 172
Benzo(a)anthracene 56-55-3 U 345 172
Benzo(a)pyrene 50-32-8 U 345 172
Benzo(b)fluoranthene 205-99-2 U 345 172
Benzo(g,h,i)Perylene 191-24-2 U 345 172
Benzo(k)fluoranthene 207-08-9 U 345 172
Benzoic acid 65-85-0 U 10500 690
Benzyl alcohol 100-51-6 U 345 172
Bis(2-Chloroethoxy)Methane 111-91-1 U 345 172
Bis(2-Chloroethyl)ether 111-44-4 U 345 172
bis(2-Chloroisopropyl)ether 39638-32-9 U 345 172
bis(2-Ethylhexyl)phthalate 117-81-7 U 345 172
Butylbenzylphthalate 85-68-7 U 345 172
Chrysene 218-01-9 U 345 172
Di-N-Butylphthalate 84-74-2 U 345 172
Di-n-octylphthalate 117-84-0 U 345 172
Dibenzo(a,h)Anthracene 53-70-3 U 345 172
Dibenzofuran 132-64-9 U 345 172
Diethylphthalate 84-66-2 U 345 172
Dimethylphthalate 131-11-3 U 345 172
Fluoranthene 206-44-0 U 345 172
Fluorene 86-73-7 U 345 172
Hexachlorobenzene 118-74-1 U 345 172
Hexachlorobutadiene 87-68-3 U 345 172
Hexachlorocyclopentadiene 77-47-4 U 1570 784
Hexachloroethane 67-72-1 U 345 172
Indeno(1,2,3-cd)pyrene 193-39-5 U 345 172
Isophorone 78-59-1 U 345 172
Diphenylamine/n-Nitrosodiphenylamine 86-30-6 U 345 172
N-Nitrosodipropylamine 621-64-7 U 345 172
Naphthalene 91-20-3 U 345 172
Nitrobenzene 98-95-3 U 345 172
Pentachlorophenol 87-86-5 U 1720 861
Phenanthrene 85-01-8 U 345 172
Page 8 of 30 Generated at May 30, 2017 08:37
Page 11
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Phenol 108-95-2 U 345 172
Pyrene 129-00-0 U 345 172
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 85.5 19 122
2-Fluorobiphenyl 84.2 30 115
2-Fluorophenol 69.3 25 121
Nitrobenzene-d5 89.2 23 120
p-Terphenyl-d14 80.3 18 137
Phenol-d5 67.6 24 113
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-06 PrePrep Method: N/A Instrument: HPMS9
Client ID: 17-0751 IR MUD SILO Prep Method: 5030B/5030C/5035A Prep Date: 05/23/2017 09:20
Matrix: Soil Analytical Method: 8260B Cal Date: 05/23/2017 14:46
Workgroup #: WG615352 Analyst: ADC Run Date: 05/23/2017 18:16
Collect Date: 05/19/2017 14:45 Dilution: 1 File ID: 9M980447
Sample Tag: 01 Units: ug/kg Percent Solid: 49.0
Analyte CAS # Result Qual RL MDL
Acetone 67-64-1 88.2 20.5 10.2
Benzene 71-43-2 2.22 J 10.2 1.02
Bromobenzene 108-86-1 U 10.2 1.02
Bromochloromethane 74-97-5 U 10.2 2.05
Bromodichloromethane 75-27-4 U 10.2 1.02
Bromoform 75-25-2 U 10.2 1.02
Bromomethane 74-83-9 U 20.5 2.05
2-Butanone 78-93-3 19.9 J 20.5 5.12
n-Butylbenzene 104-51-8 14.5 10.2 1.02
sec-Butylbenzene 135-98-8 4.36 J 10.2 1.02
tert-Butylbenzene 98-06-6 U 10.2 1.02
Carbon disulfide 75-15-0 10.8 10.2 1.02
Carbon tetrachloride 56-23-5 U 10.2 1.02
Chlorobenzene 108-90-7 U 10.2 1.02
Chlorodibromomethane 124-48-1 U 10.2 1.02
Chloroethane 75-00-3 U 20.5 2.05
2-Chloroethyl vinyl ether 110-75-8 U 20.5 4.10
Chloroform 67-66-3 U 10.2 1.02
Chloromethane 74-87-3 U 20.5 4.10
2-Chlorotoluene 95-49-8 U 10.2 1.02
4-Chlorotoluene 106-43-4 U 10.2 1.02
Page 9 of 30 Generated at May 30, 2017 08:37
Page 12
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
1,2-Dibromo-3-chloropropane 96-12-8 U 10.2 4.10
1,2-Dibromoethane 106-93-4 U 10.2 1.02
Dibromomethane 74-95-3 U 10.2 1.02
1,2-Dichlorobenzene 95-50-1 U 10.2 1.02
1,3-Dichlorobenzene 541-73-1 U 10.2 1.02
1,4-Dichlorobenzene 106-46-7 U 10.2 1.02
Dichlorodifluoromethane 75-71-8 U 20.5 2.05
1,1-Dichloroethane 75-34-3 U 10.2 2.05
1,2-Dichloroethane 107-06-2 U 10.2 1.02
1,1-Dichloroethene 75-35-4 U 10.2 1.02
cis-1,2-Dichloroethene 156-59-2 U 10.2 1.02
trans-1,2-Dichloroethene 156-60-5 U 10.2 1.02
1,2-Dichloropropane 78-87-5 U 10.2 1.02
1,3-Dichloropropane 142-28-9 U 10.2 1.02
2,2-Dichloropropane 594-20-7 U 10.2 1.02
cis-1,3-Dichloropropene 10061-01-5 U 10.2 1.02
trans-1,3-Dichloropropene 10061-02-6 U 10.2 1.02
1,1-Dichloropropene 563-58-6 U 10.2 1.02
Ethylbenzene 100-41-4 4.50 J 10.2 1.02
2-Hexanone 591-78-6 U 20.5 5.12
Hexachlorobutadiene 87-68-3 U 10.2 1.02
Isopropylbenzene 98-82-8 1.95 J 10.2 1.02
p-Isopropyltoluene 99-87-6 4.77 J 10.2 1.02
4-Methyl-2-pentanone 108-10-1 U 20.5 5.12
Methylene chloride 75-09-2 U 10.2 2.05
Naphthalene 91-20-3 10.8 J 20.5 1.02
n-Propylbenzene 103-65-1 4.73 J 10.2 1.02
Styrene 100-42-5 U 10.2 1.02
1,1,1,2-Tetrachloroethane 630-20-6 U 10.2 1.02
1,1,2,2-Tetrachloroethane 79-34-5 U 10.2 1.02
Tetrachloroethene 127-18-4 2.36 J 10.2 1.02
Toluene 108-88-3 9.84 J 10.2 1.02
1,2,3-Trichlorobenzene 87-61-6 3.20 J 10.2 1.02
1,2,4-Trichlorobenzene 120-82-1 U 10.2 1.02
1,1,1-Trichloroethane 71-55-6 U 10.2 1.02
1,1,2-Trichloroethane 79-00-5 U 10.2 1.02
Trichloroethene 79-01-6 U 10.2 1.02
Trichlorofluoromethane 75-69-4 U 20.5 2.05
1,2,3-Trichloropropane 96-18-4 U 10.2 2.05
Page 10 of 30 Generated at May 30, 2017 08:37
Page 13
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
1,2,4-Trimethylbenzene 95-63-6 40.5 10.2 1.02
1,3,5-Trimethylbenzene 108-67-8 28.1 10.2 1.02
Vinyl acetate 108-05-4 U 20.5 5.12
Vinyl chloride 75-01-4 U 20.5 2.05
o-Xylene 95-47-6 13.3 10.2 1.02
m-,p-Xylene 179601-23-1 15.5 10.2 1.02
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 99.2 80 120
1,2-Dichloroethane-d4 96.0 80 120
Toluene-d8 108 81 117
4-Bromofluorobenzene 118 74 121
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-06 PrePrep Method: N/A Instrument: HPMS12
Client ID: 17-0751 IR MUD SILO Prep Method: 3546 Prep Date: 05/22/2017 11:48
Matrix: Soil Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615227 Analyst: SCB Run Date: 05/23/2017 14:10
Collect Date: 05/19/2017 14:45 Dilution: 1 File ID: 12M62304
Sample Tag: 01 Units: ug/kg Percent Solid: 49.0
Analyte CAS # Result Qual RL MDL
1,2,4-Trichlorobenzene 120-82-1 U 356 178
1,2-Dichlorobenzene 95-50-1 U 356 178
1,3-Dichlorobenzene 541-73-1 U 356 178
1,4-Dichlorobenzene 106-46-7 U 356 178
2,4,5-Trichlorophenol 95-95-4 U 356 178
2,4,6-Trichlorophenol 88-06-2 U 356 178
2,4-Dichlorophenol 120-83-2 U 356 178
2,4-Dimethylphenol 105-67-9 U 356 178
2,4-Dinitrophenol 51-28-5 U 1780 889
2,4-Dinitrotoluene 121-14-2 U 356 178
2,6-Dinitrotoluene 606-20-2 U 356 178
2-Chloronaphthalene 91-58-7 U 356 178
2-Chlorophenol 95-57-8 U 356 178
2-Methylnaphthalene 91-57-6 718 356 178
2-Methylphenol 95-48-7 U 356 178
2-Nitroaniline 88-74-4 U 1780 889
2-Nitrophenol 88-75-5 U 356 178
3,3'-Dichlorobenzidine 91-94-1 U 712 356
Page 11 of 30 Generated at May 30, 2017 08:37
Page 14
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
3-,4-Methylphenol 65794-96-9 U 356 178
3-Nitroaniline 99-09-2 U 1780 889
4,6-Dinitro-2-methylphenol 534-52-1 U 1780 889
4-Bromophenyl-phenylether 101-55-3 U 356 178
4-Chloro-3-methylphenol 59-50-7 U 356 178
4-Chloroaniline 106-47-8 U 356 178
4-Chlorophenyl-phenyl ether 7005-72-3 U 356 178
4-Nitroaniline 100-01-6 U 1780 889
4-Nitrophenol 100-02-7 U 1780 889
Acenaphthene 83-32-9 U 356 178
Acenaphthylene 208-96-8 U 356 178
Anthracene 120-12-7 U 356 178
Benzo(a)anthracene 56-55-3 U 356 178
Benzo(a)pyrene 50-32-8 U 356 178
Benzo(b)fluoranthene 205-99-2 U 356 178
Benzo(g,h,i)Perylene 191-24-2 U 356 178
Benzo(k)fluoranthene 207-08-9 U 356 178
Benzoic acid 65-85-0 U 10800 712
Benzyl alcohol 100-51-6 U 356 178
Bis(2-Chloroethoxy)Methane 111-91-1 U 356 178
Bis(2-Chloroethyl)ether 111-44-4 U 356 178
bis(2-Chloroisopropyl)ether 39638-32-9 U 356 178
bis(2-Ethylhexyl)phthalate 117-81-7 U 356 178
Butylbenzylphthalate 85-68-7 U 356 178
Chrysene 218-01-9 U 356 178
Di-N-Butylphthalate 84-74-2 U 356 178
Di-n-octylphthalate 117-84-0 U 356 178
Dibenzo(a,h)Anthracene 53-70-3 U 356 178
Dibenzofuran 132-64-9 U 356 178
Diethylphthalate 84-66-2 U 356 178
Dimethylphthalate 131-11-3 U 356 178
Fluoranthene 206-44-0 U 356 178
Fluorene 86-73-7 U 356 178
Hexachlorobenzene 118-74-1 U 356 178
Hexachlorobutadiene 87-68-3 U 356 178
Hexachlorocyclopentadiene 77-47-4 U 1620 809
Hexachloroethane 67-72-1 U 356 178
Indeno(1,2,3-cd)pyrene 193-39-5 U 356 178
Isophorone 78-59-1 U 356 178
Page 12 of 30 Generated at May 30, 2017 08:37
Page 15
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Diphenylamine/n-Nitrosodiphenylamine 86-30-6 U 356 178
N-Nitrosodipropylamine 621-64-7 U 356 178
Naphthalene 91-20-3 466 356 178
Nitrobenzene 98-95-3 U 356 178
Pentachlorophenol 87-86-5 U 1780 889
Phenanthrene 85-01-8 263 J 356 178
Phenol 108-95-2 U 356 178
Pyrene 129-00-0 U 356 178
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 91.0 19 122
2-Fluorobiphenyl 83.7 30 115
2-Fluorophenol 66.8 25 121
Nitrobenzene-d5 86.5 23 120
p-Terphenyl-d14 76.4 18 137
Phenol-d5 65.4 24 113
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-08 PrePrep Method: N/A Instrument: HPMS9
Client ID: 17-0751 IR MUD GRID A3 NEW
Prep Method: 5030B/5030C/5035A Prep Date: 05/23/2017 09:22
Matrix: Soil Analytical Method: 8260B Cal Date: 05/23/2017 14:46
Workgroup #: WG615352 Analyst: ADC Run Date: 05/23/2017 18:47
Collect Date: 05/19/2017 15:30 Dilution: 1 File ID: 9M980448
Sample Tag: 01 Units: ug/kg Percent Solid: 26.5
Analyte CAS # Result Qual RL MDL
Acetone 67-64-1 64.1 37.4 18.7
Benzene 71-43-2 U 18.7 1.87
Bromobenzene 108-86-1 U 18.7 1.87
Bromochloromethane 74-97-5 U 18.7 3.74
Bromodichloromethane 75-27-4 U 18.7 1.87
Bromoform 75-25-2 U 18.7 1.87
Bromomethane 74-83-9 U 37.4 3.74
2-Butanone 78-93-3 U 37.4 9.36
n-Butylbenzene 104-51-8 6.81 J 18.7 1.87
sec-Butylbenzene 135-98-8 2.21 J 18.7 1.87
tert-Butylbenzene 98-06-6 U 18.7 1.87
Carbon disulfide 75-15-0 11.6 J 18.7 1.87
Carbon tetrachloride 56-23-5 U 18.7 1.87
Page 13 of 30 Generated at May 30, 2017 08:37
Page 16
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Chlorobenzene 108-90-7 U 18.7 1.87
Chlorodibromomethane 124-48-1 U 18.7 1.87
Chloroethane 75-00-3 U 37.4 3.74
2-Chloroethyl vinyl ether 110-75-8 U 37.4 7.48
Chloroform 67-66-3 U 18.7 1.87
Chloromethane 74-87-3 U 37.4 7.48
2-Chlorotoluene 95-49-8 U 18.7 1.87
4-Chlorotoluene 106-43-4 U 18.7 1.87
1,2-Dibromo-3-chloropropane 96-12-8 U 18.7 7.48
1,2-Dibromoethane 106-93-4 U 18.7 1.87
Dibromomethane 74-95-3 U 18.7 1.87
1,2-Dichlorobenzene 95-50-1 U 18.7 1.87
1,3-Dichlorobenzene 541-73-1 U 18.7 1.87
1,4-Dichlorobenzene 106-46-7 U 18.7 1.87
Dichlorodifluoromethane 75-71-8 U 37.4 3.74
1,1-Dichloroethane 75-34-3 U 18.7 3.74
1,2-Dichloroethane 107-06-2 U 18.7 1.87
1,1-Dichloroethene 75-35-4 U 18.7 1.87
cis-1,2-Dichloroethene 156-59-2 U 18.7 1.87
trans-1,2-Dichloroethene 156-60-5 U 18.7 1.87
1,2-Dichloropropane 78-87-5 U 18.7 1.87
1,3-Dichloropropane 142-28-9 U 18.7 1.87
2,2-Dichloropropane 594-20-7 U 18.7 1.87
cis-1,3-Dichloropropene 10061-01-5 U 18.7 1.87
trans-1,3-Dichloropropene 10061-02-6 U 18.7 1.87
1,1-Dichloropropene 563-58-6 U 18.7 1.87
Ethylbenzene 100-41-4 4.07 J 18.7 1.87
2-Hexanone 591-78-6 U 37.4 9.36
Hexachlorobutadiene 87-68-3 U 18.7 1.87
Isopropylbenzene 98-82-8 2.21 J 18.7 1.87
p-Isopropyltoluene 99-87-6 2.82 J 18.7 1.87
4-Methyl-2-pentanone 108-10-1 U 37.4 9.36
Methylene chloride 75-09-2 U 18.7 3.74
Naphthalene 91-20-3 5.16 J 37.4 1.87
n-Propylbenzene 103-65-1 2.69 J 18.7 1.87
Styrene 100-42-5 U 18.7 1.87
1,1,1,2-Tetrachloroethane 630-20-6 U 18.7 1.87
1,1,2,2-Tetrachloroethane 79-34-5 U 18.7 1.87
Tetrachloroethene 127-18-4 3.81 J 18.7 1.87
Page 14 of 30 Generated at May 30, 2017 08:37
Page 17
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Toluene 108-88-3 7.46 J 18.7 1.87
1,2,3-Trichlorobenzene 87-61-6 U 18.7 1.87
1,2,4-Trichlorobenzene 120-82-1 U 18.7 1.87
1,1,1-Trichloroethane 71-55-6 U 18.7 1.87
1,1,2-Trichloroethane 79-00-5 U 18.7 1.87
Trichloroethene 79-01-6 U 18.7 1.87
Trichlorofluoromethane 75-69-4 U 37.4 3.74
1,2,3-Trichloropropane 96-18-4 U 18.7 3.74
1,2,4-Trimethylbenzene 95-63-6 15.6 J 18.7 1.87
1,3,5-Trimethylbenzene 108-67-8 9.22 J 18.7 1.87
Vinyl acetate 108-05-4 U 37.4 9.36
Vinyl chloride 75-01-4 U 37.4 3.74
o-Xylene 95-47-6 6.89 J 18.7 1.87
m-,p-Xylene 179601-23-1 8.61 J 18.7 1.87
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 100 80 120
1,2-Dichloroethane-d4 93.4 80 120
Toluene-d8 110 81 117
4-Bromofluorobenzene 117 74 121
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-08 PrePrep Method: N/A Instrument: HPMS12
Client ID: 17-0751 IR MUD GRID A3 NEW
Prep Method: 3546 Prep Date: 05/22/2017 11:48
Matrix: Soil Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615227 Analyst: SCB Run Date: 05/23/2017 13:36
Collect Date: 05/19/2017 15:30 Dilution: 1 File ID: 12M62303
Sample Tag: 01 Units: ug/kg Percent Solid: 26.5
Analyte CAS # Result Qual RL MDL
1,2,4-Trichlorobenzene 120-82-1 U 666 333
1,2-Dichlorobenzene 95-50-1 U 666 333
1,3-Dichlorobenzene 541-73-1 U 666 333
1,4-Dichlorobenzene 106-46-7 U 666 333
2,4,5-Trichlorophenol 95-95-4 U 666 333
2,4,6-Trichlorophenol 88-06-2 U 666 333
2,4-Dichlorophenol 120-83-2 U 666 333
2,4-Dimethylphenol 105-67-9 U 666 333
2,4-Dinitrophenol 51-28-5 U 3330 1660
Page 15 of 30 Generated at May 30, 2017 08:37
Page 18
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
2,4-Dinitrotoluene 121-14-2 U 666 333
2,6-Dinitrotoluene 606-20-2 U 666 333
2-Chloronaphthalene 91-58-7 U 666 333
2-Chlorophenol 95-57-8 U 666 333
2-Methylnaphthalene 91-57-6 514 J 666 333
2-Methylphenol 95-48-7 U 666 333
2-Nitroaniline 88-74-4 U 3330 1660
2-Nitrophenol 88-75-5 U 666 333
3,3'-Dichlorobenzidine 91-94-1 U 1330 666
3-,4-Methylphenol 65794-96-9 U 666 333
3-Nitroaniline 99-09-2 U 3330 1660
4,6-Dinitro-2-methylphenol 534-52-1 U 3330 1660
4-Bromophenyl-phenylether 101-55-3 U 666 333
4-Chloro-3-methylphenol 59-50-7 U 666 333
4-Chloroaniline 106-47-8 U 666 333
4-Chlorophenyl-phenyl ether 7005-72-3 U 666 333
4-Nitroaniline 100-01-6 U 3330 1660
4-Nitrophenol 100-02-7 U 3330 1660
Acenaphthene 83-32-9 U 666 333
Acenaphthylene 208-96-8 U 666 333
Anthracene 120-12-7 U 666 333
Benzo(a)anthracene 56-55-3 U 666 333
Benzo(a)pyrene 50-32-8 U 666 333
Benzo(b)fluoranthene 205-99-2 U 666 333
Benzo(g,h,i)Perylene 191-24-2 U 666 333
Benzo(k)fluoranthene 207-08-9 U 666 333
Benzoic acid 65-85-0 U 20200 1330
Benzyl alcohol 100-51-6 U 666 333
Bis(2-Chloroethoxy)Methane 111-91-1 U 666 333
Bis(2-Chloroethyl)ether 111-44-4 U 666 333
bis(2-Chloroisopropyl)ether 39638-32-9 U 666 333
bis(2-Ethylhexyl)phthalate 117-81-7 U 666 333
Butylbenzylphthalate 85-68-7 U 666 333
Chrysene 218-01-9 U 666 333
Di-N-Butylphthalate 84-74-2 U 666 333
Di-n-octylphthalate 117-84-0 U 666 333
Dibenzo(a,h)Anthracene 53-70-3 U 666 333
Dibenzofuran 132-64-9 U 666 333
Diethylphthalate 84-66-2 U 666 333
Page 16 of 30 Generated at May 30, 2017 08:37
Page 19
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Dimethylphthalate 131-11-3 U 666 333
Fluoranthene 206-44-0 U 666 333
Fluorene 86-73-7 U 666 333
Hexachlorobenzene 118-74-1 U 666 333
Hexachlorobutadiene 87-68-3 U 666 333
Hexachlorocyclopentadiene 77-47-4 U 3030 1510
Hexachloroethane 67-72-1 U 666 333
Indeno(1,2,3-cd)pyrene 193-39-5 U 666 333
Isophorone 78-59-1 U 666 333
Diphenylamine/n-Nitrosodiphenylamine 86-30-6 U 666 333
N-Nitrosodipropylamine 621-64-7 U 666 333
Naphthalene 91-20-3 U 666 333
Nitrobenzene 98-95-3 U 666 333
Pentachlorophenol 87-86-5 U 3330 1660
Phenanthrene 85-01-8 U 666 333
Phenol 108-95-2 U 666 333
Pyrene 129-00-0 U 666 333
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 83.4 19 122
2-Fluorobiphenyl 81.7 30 115
2-Fluorophenol 62.9 25 121
Nitrobenzene-d5 84.5 23 120
p-Terphenyl-d14 75.9 18 137
Phenol-d5 62.2 24 113
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-10 PrePrep Method: N/A Instrument: HPMS9
Client ID: 17-0751 WEST BOREHOLE RETURN M
Prep Method: 5030B/5030C/5035A Prep Date: 05/23/2017 09:23
Matrix: Soil Analytical Method: 8260B Cal Date: 05/23/2017 14:46
Workgroup #: WG615352 Analyst: ADC Run Date: 05/23/2017 19:17
Collect Date: 05/19/2017 16:18 Dilution: 1 File ID: 9M980449
Sample Tag: 01 Units: ug/kg Percent Solid: 41.6
Analyte CAS # Result Qual RL MDL
Acetone 67-64-1 U 23.2 11.6
Benzene 71-43-2 U 11.6 1.16
Bromobenzene 108-86-1 U 11.6 1.16
Bromochloromethane 74-97-5 U 11.6 2.32
Page 17 of 30 Generated at May 30, 2017 08:37
Page 20
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Bromodichloromethane 75-27-4 U 11.6 1.16
Bromoform 75-25-2 U 11.6 1.16
Bromomethane 74-83-9 U 23.2 2.32
2-Butanone 78-93-3 U 23.2 5.80
n-Butylbenzene 104-51-8 2.28 E 11.6 1.16
sec-Butylbenzene 135-98-8 U 11.6 1.16
tert-Butylbenzene 98-06-6 U 11.6 1.16
Carbon disulfide 75-15-0 4.00 J 11.6 1.16
Carbon tetrachloride 56-23-5 U 11.6 1.16
Chlorobenzene 108-90-7 U 11.6 1.16
Chlorodibromomethane 124-48-1 U 11.6 1.16
Chloroethane 75-00-3 U 23.2 2.32
2-Chloroethyl vinyl ether 110-75-8 U 23.2 4.64
Chloroform 67-66-3 U 11.6 1.16
Chloromethane 74-87-3 U 23.2 4.64
2-Chlorotoluene 95-49-8 U 11.6 1.16
4-Chlorotoluene 106-43-4 U 11.6 1.16
1,2-Dibromo-3-chloropropane 96-12-8 U 11.6 4.64
1,2-Dibromoethane 106-93-4 U 11.6 1.16
Dibromomethane 74-95-3 U 11.6 1.16
1,2-Dichlorobenzene 95-50-1 U 11.6 1.16
1,3-Dichlorobenzene 541-73-1 U 11.6 1.16
1,4-Dichlorobenzene 106-46-7 U 11.6 1.16
Dichlorodifluoromethane 75-71-8 U 23.2 2.32
1,1-Dichloroethane 75-34-3 U 11.6 2.32
1,2-Dichloroethane 107-06-2 U 11.6 1.16
1,1-Dichloroethene 75-35-4 U 11.6 1.16
cis-1,2-Dichloroethene 156-59-2 U 11.6 1.16
trans-1,2-Dichloroethene 156-60-5 U 11.6 1.16
1,2-Dichloropropane 78-87-5 U 11.6 1.16
1,3-Dichloropropane 142-28-9 U 11.6 1.16
2,2-Dichloropropane 594-20-7 U 11.6 1.16
cis-1,3-Dichloropropene 10061-01-5 U 11.6 1.16
trans-1,3-Dichloropropene 10061-02-6 U 11.6 1.16
1,1-Dichloropropene 563-58-6 U 11.6 1.16
Ethylbenzene 100-41-4 1.46 J 11.6 1.16
2-Hexanone 591-78-6 U 23.2 5.80
Hexachlorobutadiene 87-68-3 U 11.6 1.16
Isopropylbenzene 98-82-8 U 11.6 1.16
Page 18 of 30 Generated at May 30, 2017 08:37
Page 21
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
p-Isopropyltoluene 99-87-6 U 11.6 1.16
4-Methyl-2-pentanone 108-10-1 U 23.2 5.80
Methylene chloride 75-09-2 U 11.6 2.32
Naphthalene 91-20-3 2.93 E 23.2 1.16
n-Propylbenzene 103-65-1 1.63 J 11.6 1.16
Styrene 100-42-5 U 11.6 1.16
1,1,1,2-Tetrachloroethane 630-20-6 U 11.6 1.16
1,1,2,2-Tetrachloroethane 79-34-5 U 11.6 1.16
Tetrachloroethene 127-18-4 2.38 J 11.6 1.16
Toluene 108-88-3 2.31 J 11.6 1.16
1,2,3-Trichlorobenzene 87-61-6 U 11.6 1.16
1,2,4-Trichlorobenzene 120-82-1 U 11.6 1.16
1,1,1-Trichloroethane 71-55-6 U 11.6 1.16
1,1,2-Trichloroethane 79-00-5 U 11.6 1.16
Trichloroethene 79-01-6 U 11.6 1.16
Trichlorofluoromethane 75-69-4 U 23.2 2.32
1,2,3-Trichloropropane 96-18-4 U 11.6 2.32
1,2,4-Trimethylbenzene 95-63-6 3.89 J 11.6 1.16
1,3,5-Trimethylbenzene 108-67-8 1.88 J 11.6 1.16
Vinyl acetate 108-05-4 U 23.2 5.80
Vinyl chloride 75-01-4 U 23.2 2.32
o-Xylene 95-47-6 2.08 J 11.6 1.16
m-,p-Xylene 179601-23-1 2.96 J 11.6 1.16
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 99.9 80 120
1,2-Dichloroethane-d4 96.5 80 120
Toluene-d8 117 81 117
4-Bromofluorobenzene 135 74 121 *
* Surrogate or spike compound out of range
E Estimated concentration due to sample matrix interference
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Page 19 of 30 Generated at May 30, 2017 08:37
Page 22
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisSample #: L17051231-10 PrePrep Method: N/A Instrument: HPMS12
Client ID: 17-0751 WEST BOREHOLE RETURN M
Prep Method: 3546 Prep Date: 05/22/2017 11:48
Matrix: Soil Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615227 Analyst: SCB Run Date: 05/23/2017 14:43
Collect Date: 05/19/2017 16:18 Dilution: 1 File ID: 12M62305
Sample Tag: 01 Units: ug/kg Percent Solid: 41.6
Analyte CAS # Result Qual RL MDL
1,2,4-Trichlorobenzene 120-82-1 U 360 180
1,2-Dichlorobenzene 95-50-1 U 360 180
1,3-Dichlorobenzene 541-73-1 U 360 180
1,4-Dichlorobenzene 106-46-7 U 360 180
2,4,5-Trichlorophenol 95-95-4 U 360 180
2,4,6-Trichlorophenol 88-06-2 U 360 180
2,4-Dichlorophenol 120-83-2 U 360 180
2,4-Dimethylphenol 105-67-9 U 360 180
2,4-Dinitrophenol 51-28-5 U 1800 900
2,4-Dinitrotoluene 121-14-2 U 360 180
2,6-Dinitrotoluene 606-20-2 U 360 180
2-Chloronaphthalene 91-58-7 U 360 180
2-Chlorophenol 95-57-8 U 360 180
2-Methylnaphthalene 91-57-6 316 J 360 180
2-Methylphenol 95-48-7 U 360 180
2-Nitroaniline 88-74-4 U 1800 900
2-Nitrophenol 88-75-5 U 360 180
3,3'-Dichlorobenzidine 91-94-1 U 721 360
3-,4-Methylphenol 65794-96-9 U 360 180
3-Nitroaniline 99-09-2 U 1800 900
4,6-Dinitro-2-methylphenol 534-52-1 U 1800 900
4-Bromophenyl-phenylether 101-55-3 U 360 180
4-Chloro-3-methylphenol 59-50-7 U 360 180
4-Chloroaniline 106-47-8 U 360 180
4-Chlorophenyl-phenyl ether 7005-72-3 U 360 180
4-Nitroaniline 100-01-6 U 1800 900
4-Nitrophenol 100-02-7 U 1800 900
Acenaphthene 83-32-9 U 360 180
Acenaphthylene 208-96-8 U 360 180
Anthracene 120-12-7 U 360 180
Benzo(a)anthracene 56-55-3 U 360 180
Benzo(a)pyrene 50-32-8 U 360 180
Page 20 of 30 Generated at May 30, 2017 08:37
Page 23
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Benzo(b)fluoranthene 205-99-2 U 360 180
Benzo(g,h,i)Perylene 191-24-2 U 360 180
Benzo(k)fluoranthene 207-08-9 U 360 180
Benzoic acid 65-85-0 U 10900 721
Benzyl alcohol 100-51-6 U 360 180
Bis(2-Chloroethoxy)Methane 111-91-1 U 360 180
Bis(2-Chloroethyl)ether 111-44-4 U 360 180
bis(2-Chloroisopropyl)ether 39638-32-9 U 360 180
bis(2-Ethylhexyl)phthalate 117-81-7 U 360 180
Butylbenzylphthalate 85-68-7 U 360 180
Chrysene 218-01-9 U 360 180
Di-N-Butylphthalate 84-74-2 U 360 180
Di-n-octylphthalate 117-84-0 U 360 180
Dibenzo(a,h)Anthracene 53-70-3 U 360 180
Dibenzofuran 132-64-9 U 360 180
Diethylphthalate 84-66-2 U 360 180
Dimethylphthalate 131-11-3 U 360 180
Fluoranthene 206-44-0 U 360 180
Fluorene 86-73-7 U 360 180
Hexachlorobenzene 118-74-1 U 360 180
Hexachlorobutadiene 87-68-3 U 360 180
Hexachlorocyclopentadiene 77-47-4 U 1640 819
Hexachloroethane 67-72-1 U 360 180
Indeno(1,2,3-cd)pyrene 193-39-5 U 360 180
Isophorone 78-59-1 U 360 180
Diphenylamine/n-Nitrosodiphenylamine 86-30-6 U 360 180
N-Nitrosodipropylamine 621-64-7 U 360 180
Naphthalene 91-20-3 197 J 360 180
Nitrobenzene 98-95-3 U 360 180
Pentachlorophenol 87-86-5 U 1800 900
Phenanthrene 85-01-8 U 360 180
Phenol 108-95-2 U 360 180
Pyrene 129-00-0 U 360 180
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 70.9 19 122
2-Fluorobiphenyl 57.1 30 115
2-Fluorophenol 45.1 25 121
Nitrobenzene-d5 60.2 23 120
p-Terphenyl-d14 79.1 18 137
Page 21 of 30 Generated at May 30, 2017 08:38
Page 24
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisPhenol-d5 43.6 24 113
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-12 PrePrep Method: N/A Instrument: HPMS9
Client ID: 17-0751 WEST RECLAIMER PIT
Prep Method: 5030B/5030C/5035A Prep Date: 05/23/2017 09:25
Matrix: Soil Analytical Method: 8260B Cal Date: 05/23/2017 14:46
Workgroup #: WG615352 Analyst: ADC Run Date: 05/23/2017 19:47
Collect Date: 05/19/2017 16:30 Dilution: 1 File ID: 9M980450
Sample Tag: 01 Units: ug/kg Percent Solid: 56.8
Analyte CAS # Result Qual RL MDL
Acetone 67-64-1 19.0 17.0 8.52
Benzene 71-43-2 U 8.52 0.852
Bromobenzene 108-86-1 U 8.52 0.852
Bromochloromethane 74-97-5 U 8.52 1.70
Bromodichloromethane 75-27-4 U 8.52 0.852
Bromoform 75-25-2 U 8.52 0.852
Bromomethane 74-83-9 U 17.0 1.70
2-Butanone 78-93-3 U 17.0 4.26
n-Butylbenzene 104-51-8 1.10 J 8.52 0.852
sec-Butylbenzene 135-98-8 U 8.52 0.852
tert-Butylbenzene 98-06-6 U 8.52 0.852
Carbon disulfide 75-15-0 1.56 J 8.52 0.852
Carbon tetrachloride 56-23-5 U 8.52 0.852
Chlorobenzene 108-90-7 U 8.52 0.852
Chlorodibromomethane 124-48-1 U 8.52 0.852
Chloroethane 75-00-3 U 17.0 1.70
2-Chloroethyl vinyl ether 110-75-8 U 17.0 3.41
Chloroform 67-66-3 U 8.52 0.852
Chloromethane 74-87-3 U 17.0 3.41
2-Chlorotoluene 95-49-8 U 8.52 0.852
4-Chlorotoluene 106-43-4 U 8.52 0.852
1,2-Dibromo-3-chloropropane 96-12-8 U 8.52 3.41
1,2-Dibromoethane 106-93-4 U 8.52 0.852
Dibromomethane 74-95-3 U 8.52 0.852
1,2-Dichlorobenzene 95-50-1 U 8.52 0.852
1,3-Dichlorobenzene 541-73-1 U 8.52 0.852
1,4-Dichlorobenzene 106-46-7 U 8.52 0.852
Dichlorodifluoromethane 75-71-8 U 17.0 1.70
Page 22 of 30 Generated at May 30, 2017 08:38
Page 25
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
1,1-Dichloroethane 75-34-3 U 8.52 1.70
1,2-Dichloroethane 107-06-2 U 8.52 0.852
1,1-Dichloroethene 75-35-4 U 8.52 0.852
cis-1,2-Dichloroethene 156-59-2 U 8.52 0.852
trans-1,2-Dichloroethene 156-60-5 U 8.52 0.852
1,2-Dichloropropane 78-87-5 U 8.52 0.852
1,3-Dichloropropane 142-28-9 U 8.52 0.852
2,2-Dichloropropane 594-20-7 U 8.52 0.852
cis-1,3-Dichloropropene 10061-01-5 U 8.52 0.852
trans-1,3-Dichloropropene 10061-02-6 U 8.52 0.852
1,1-Dichloropropene 563-58-6 U 8.52 0.852
Ethylbenzene 100-41-4 U 8.52 0.852
2-Hexanone 591-78-6 U 17.0 4.26
Hexachlorobutadiene 87-68-3 U 8.52 0.852
Isopropylbenzene 98-82-8 U 8.52 0.852
p-Isopropyltoluene 99-87-6 U 8.52 0.852
4-Methyl-2-pentanone 108-10-1 U 17.0 4.26
Methylene chloride 75-09-2 U 8.52 1.70
Naphthalene 91-20-3 1.10 J 17.0 0.852
n-Propylbenzene 103-65-1 U 8.52 0.852
Styrene 100-42-5 U 8.52 0.852
1,1,1,2-Tetrachloroethane 630-20-6 U 8.52 0.852
1,1,2,2-Tetrachloroethane 79-34-5 U 8.52 0.852
Tetrachloroethene 127-18-4 1.41 J 8.52 0.852
Toluene 108-88-3 1.43 J 8.52 0.852
1,2,3-Trichlorobenzene 87-61-6 U 8.52 0.852
1,2,4-Trichlorobenzene 120-82-1 U 8.52 0.852
1,1,1-Trichloroethane 71-55-6 U 8.52 0.852
1,1,2-Trichloroethane 79-00-5 U 8.52 0.852
Trichloroethene 79-01-6 U 8.52 0.852
Trichlorofluoromethane 75-69-4 U 17.0 1.70
1,2,3-Trichloropropane 96-18-4 U 8.52 1.70
1,2,4-Trimethylbenzene 95-63-6 2.05 J 8.52 0.852
1,3,5-Trimethylbenzene 108-67-8 0.985 J 8.52 0.852
Vinyl acetate 108-05-4 U 17.0 4.26
Vinyl chloride 75-01-4 U 17.0 1.70
o-Xylene 95-47-6 1.14 J 8.52 0.852
m-,p-Xylene 179601-23-1 1.34 J 8.52 0.852
Surrogate Recovery Lower Limit Upper Limit Q
Page 23 of 30 Generated at May 30, 2017 08:38
Page 26
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisDibromofluoromethane 98.6 80 120
1,2-Dichloroethane-d4 97.4 80 120
Toluene-d8 114 81 117
4-Bromofluorobenzene 122 74 121 *
* Surrogate or spike compound out of range
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-12 PrePrep Method: N/A Instrument: HPMS12
Client ID: 17-0751 WEST RECLAIMER PIT
Prep Method: 3546 Prep Date: 05/22/2017 11:48
Matrix: Soil Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615227 Analyst: SCB Run Date: 05/23/2017 15:16
Collect Date: 05/19/2017 16:30 Dilution: 1 File ID: 12M62306
Sample Tag: 01 Units: ug/kg Percent Solid: 56.8
Analyte CAS # Result Qual RL MDL
1,2,4-Trichlorobenzene 120-82-1 U 301 151
1,2-Dichlorobenzene 95-50-1 U 301 151
1,3-Dichlorobenzene 541-73-1 U 301 151
1,4-Dichlorobenzene 106-46-7 U 301 151
2,4,5-Trichlorophenol 95-95-4 U 301 151
2,4,6-Trichlorophenol 88-06-2 U 301 151
2,4-Dichlorophenol 120-83-2 U 301 151
2,4-Dimethylphenol 105-67-9 U 301 151
2,4-Dinitrophenol 51-28-5 U 1510 752
2,4-Dinitrotoluene 121-14-2 U 301 151
2,6-Dinitrotoluene 606-20-2 U 301 151
2-Chloronaphthalene 91-58-7 U 301 151
2-Chlorophenol 95-57-8 U 301 151
2-Methylnaphthalene 91-57-6 2090 301 151
2-Methylphenol 95-48-7 U 301 151
2-Nitroaniline 88-74-4 U 1510 752
2-Nitrophenol 88-75-5 U 301 151
3,3'-Dichlorobenzidine 91-94-1 U 603 301
3-,4-Methylphenol 65794-96-9 U 301 151
3-Nitroaniline 99-09-2 U 1510 752
4,6-Dinitro-2-methylphenol 534-52-1 U 1510 752
4-Bromophenyl-phenylether 101-55-3 U 301 151
4-Chloro-3-methylphenol 59-50-7 U 301 151
4-Chloroaniline 106-47-8 U 301 151
Page 24 of 30 Generated at May 30, 2017 08:38
Page 27
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
4-Chlorophenyl-phenyl ether 7005-72-3 U 301 151
4-Nitroaniline 100-01-6 U 1510 752
4-Nitrophenol 100-02-7 U 1510 752
Acenaphthene 83-32-9 U 301 151
Acenaphthylene 208-96-8 U 301 151
Anthracene 120-12-7 U 301 151
Benzo(a)anthracene 56-55-3 U 301 151
Benzo(a)pyrene 50-32-8 U 301 151
Benzo(b)fluoranthene 205-99-2 U 301 151
Benzo(g,h,i)Perylene 191-24-2 U 301 151
Benzo(k)fluoranthene 207-08-9 U 301 151
Benzoic acid 65-85-0 U 9130 603
Benzyl alcohol 100-51-6 U 301 151
Bis(2-Chloroethoxy)Methane 111-91-1 U 301 151
Bis(2-Chloroethyl)ether 111-44-4 U 301 151
bis(2-Chloroisopropyl)ether 39638-32-9 U 301 151
bis(2-Ethylhexyl)phthalate 117-81-7 U 301 151
Butylbenzylphthalate 85-68-7 U 301 151
Chrysene 218-01-9 U 301 151
Di-N-Butylphthalate 84-74-2 U 301 151
Di-n-octylphthalate 117-84-0 U 301 151
Dibenzo(a,h)Anthracene 53-70-3 U 301 151
Dibenzofuran 132-64-9 358 301 151
Diethylphthalate 84-66-2 U 301 151
Dimethylphthalate 131-11-3 U 301 151
Fluoranthene 206-44-0 175 J 301 151
Fluorene 86-73-7 U 301 151
Hexachlorobenzene 118-74-1 U 301 151
Hexachlorobutadiene 87-68-3 U 301 151
Hexachlorocyclopentadiene 77-47-4 U 1370 685
Hexachloroethane 67-72-1 U 301 151
Indeno(1,2,3-cd)pyrene 193-39-5 U 301 151
Isophorone 78-59-1 U 301 151
Diphenylamine/n-Nitrosodiphenylamine 86-30-6 U 301 151
N-Nitrosodipropylamine 621-64-7 U 301 151
Naphthalene 91-20-3 1310 301 151
Nitrobenzene 98-95-3 U 301 151
Pentachlorophenol 87-86-5 U 1510 752
Phenanthrene 85-01-8 789 301 151
Page 25 of 30 Generated at May 30, 2017 08:38
Page 28
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Phenol 108-95-2 U 301 151
Pyrene 129-00-0 194 J 301 151
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 87.9 19 122
2-Fluorobiphenyl 82.1 30 115
2-Fluorophenol 62.5 25 121
Nitrobenzene-d5 88.7 23 120
p-Terphenyl-d14 77.3 18 137
Phenol-d5 59.8 24 113
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-14 PrePrep Method: N/A Instrument: HPMS9
Client ID: 17-0751 EAST RECLAIMER NEW MUD
Prep Method: 5030B/5030C/5035A Prep Date: 05/23/2017 09:28
Matrix: Soil Analytical Method: 8260B Cal Date: 05/23/2017 14:46
Workgroup #: WG615352 Analyst: ADC Run Date: 05/23/2017 20:17
Collect Date: 05/19/2017 17:12 Dilution: 1 File ID: 9M980451
Sample Tag: 01 Units: ug/kg Percent Solid: 1.96
Analyte CAS # Result Qual RL MDL
Acetone 67-64-1 U 502 251
Benzene 71-43-2 U 251 25.1
Bromobenzene 108-86-1 U 251 25.1
Bromochloromethane 74-97-5 U 251 50.2
Bromodichloromethane 75-27-4 U 251 25.1
Bromoform 75-25-2 U 251 25.1
Bromomethane 74-83-9 U 502 50.2
2-Butanone 78-93-3 U 502 125
n-Butylbenzene 104-51-8 U 251 25.1
sec-Butylbenzene 135-98-8 U 251 25.1
tert-Butylbenzene 98-06-6 U 251 25.1
Carbon disulfide 75-15-0 U 251 25.1
Carbon tetrachloride 56-23-5 U 251 25.1
Chlorobenzene 108-90-7 U 251 25.1
Chlorodibromomethane 124-48-1 U 251 25.1
Chloroethane 75-00-3 U 502 50.2
2-Chloroethyl vinyl ether 110-75-8 U 502 100
Chloroform 67-66-3 U 251 25.1
Chloromethane 74-87-3 U 502 100
Page 26 of 30 Generated at May 30, 2017 08:38
Page 29
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
2-Chlorotoluene 95-49-8 U 251 25.1
4-Chlorotoluene 106-43-4 U 251 25.1
1,2-Dibromo-3-chloropropane 96-12-8 U 251 100
1,2-Dibromoethane 106-93-4 U 251 25.1
Dibromomethane 74-95-3 U 251 25.1
1,2-Dichlorobenzene 95-50-1 U 251 25.1
1,3-Dichlorobenzene 541-73-1 U 251 25.1
1,4-Dichlorobenzene 106-46-7 U 251 25.1
Dichlorodifluoromethane 75-71-8 U 502 50.2
1,1-Dichloroethane 75-34-3 U 251 50.2
1,2-Dichloroethane 107-06-2 U 251 25.1
1,1-Dichloroethene 75-35-4 U 251 25.1
cis-1,2-Dichloroethene 156-59-2 U 251 25.1
trans-1,2-Dichloroethene 156-60-5 U 251 25.1
1,2-Dichloropropane 78-87-5 U 251 25.1
1,3-Dichloropropane 142-28-9 U 251 25.1
2,2-Dichloropropane 594-20-7 U 251 25.1
cis-1,3-Dichloropropene 10061-01-5 U 251 25.1
trans-1,3-Dichloropropene 10061-02-6 U 251 25.1
1,1-Dichloropropene 563-58-6 U 251 25.1
Ethylbenzene 100-41-4 U 251 25.1
2-Hexanone 591-78-6 U 502 125
Hexachlorobutadiene 87-68-3 U 251 25.1
Isopropylbenzene 98-82-8 U 251 25.1
p-Isopropyltoluene 99-87-6 U 251 25.1
4-Methyl-2-pentanone 108-10-1 U 502 125
Methylene chloride 75-09-2 U 251 50.2
Naphthalene 91-20-3 U 502 25.1
n-Propylbenzene 103-65-1 U 251 25.1
Styrene 100-42-5 U 251 25.1
1,1,1,2-Tetrachloroethane 630-20-6 U 251 25.1
1,1,2,2-Tetrachloroethane 79-34-5 U 251 25.1
Tetrachloroethene 127-18-4 62.4 J 251 25.1
Toluene 108-88-3 U 251 25.1
1,2,3-Trichlorobenzene 87-61-6 U 251 25.1
1,2,4-Trichlorobenzene 120-82-1 U 251 25.1
1,1,1-Trichloroethane 71-55-6 U 251 25.1
1,1,2-Trichloroethane 79-00-5 U 251 25.1
Trichloroethene 79-01-6 U 251 25.1
Page 27 of 30 Generated at May 30, 2017 08:38
Page 30
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Trichlorofluoromethane 75-69-4 U 502 50.2
1,2,3-Trichloropropane 96-18-4 U 251 50.2
1,2,4-Trimethylbenzene 95-63-6 U 251 25.1
1,3,5-Trimethylbenzene 108-67-8 U 251 25.1
Vinyl acetate 108-05-4 U 502 125
Vinyl chloride 75-01-4 U 502 50.2
o-Xylene 95-47-6 U 251 25.1
m-,p-Xylene 179601-23-1 U 251 25.1
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 97.4 80 120
1,2-Dichloroethane-d4 92.8 80 120
Toluene-d8 106 81 117
4-Bromofluorobenzene 111 74 121
J The analyte was positively identified, but the quantitation was below the RL
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-14 PrePrep Method: N/A Instrument: HPMS12
Client ID: 17-0751 EAST RECLAIMER NEW MUD
Prep Method: 3546 Prep Date: 05/22/2017 11:48
Matrix: Soil Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615227 Analyst: SCB Run Date: 05/23/2017 12:31
Collect Date: 05/19/2017 17:12 Dilution: 1 File ID: 12M62301
Sample Tag: 01 Units: ug/kg Percent Solid: 1.96
Analyte CAS # Result Qual RL MDL
1,2,4-Trichlorobenzene 120-82-1 U 9740 4870
1,2-Dichlorobenzene 95-50-1 U 9740 4870
1,3-Dichlorobenzene 541-73-1 U 9740 4870
1,4-Dichlorobenzene 106-46-7 U 9740 4870
2,4,5-Trichlorophenol 95-95-4 U 9740 4870
2,4,6-Trichlorophenol 88-06-2 U 9740 4870
2,4-Dichlorophenol 120-83-2 U 9740 4870
2,4-Dimethylphenol 105-67-9 U 9740 4870
2,4-Dinitrophenol 51-28-5 U 48700 24300
2,4-Dinitrotoluene 121-14-2 U 9740 4870
2,6-Dinitrotoluene 606-20-2 U 9740 4870
2-Chloronaphthalene 91-58-7 U 9740 4870
2-Chlorophenol 95-57-8 U 9740 4870
2-Methylnaphthalene 91-57-6 U 9740 4870
2-Methylphenol 95-48-7 U 9740 4870
Page 28 of 30 Generated at May 30, 2017 08:38
Page 31
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
2-Nitroaniline 88-74-4 U 48700 24300
2-Nitrophenol 88-75-5 U 9740 4870
3,3'-Dichlorobenzidine 91-94-1 U 19500 9740
3-,4-Methylphenol 65794-96-9 U 9740 4870
3-Nitroaniline 99-09-2 U 48700 24300
4,6-Dinitro-2-methylphenol 534-52-1 U 48700 24300
4-Bromophenyl-phenylether 101-55-3 U 9740 4870
4-Chloro-3-methylphenol 59-50-7 U 9740 4870
4-Chloroaniline 106-47-8 U 9740 4870
4-Chlorophenyl-phenyl ether 7005-72-3 U 9740 4870
4-Nitroaniline 100-01-6 U 48700 24300
4-Nitrophenol 100-02-7 U 48700 24300
Acenaphthene 83-32-9 U 9740 4870
Acenaphthylene 208-96-8 U 9740 4870
Anthracene 120-12-7 U 9740 4870
Benzo(a)anthracene 56-55-3 U 9740 4870
Benzo(a)pyrene 50-32-8 U 9740 4870
Benzo(b)fluoranthene 205-99-2 U 9740 4870
Benzo(g,h,i)Perylene 191-24-2 U 9740 4870
Benzo(k)fluoranthene 207-08-9 U 9740 4870
Benzoic acid 65-85-0 U 295000 19500
Benzyl alcohol 100-51-6 U 9740 4870
Bis(2-Chloroethoxy)Methane 111-91-1 U 9740 4870
Bis(2-Chloroethyl)ether 111-44-4 U 9740 4870
bis(2-Chloroisopropyl)ether 39638-32-9 U 9740 4870
bis(2-Ethylhexyl)phthalate 117-81-7 U 9740 4870
Butylbenzylphthalate 85-68-7 U 9740 4870
Chrysene 218-01-9 U 9740 4870
Di-N-Butylphthalate 84-74-2 U 9740 4870
Di-n-octylphthalate 117-84-0 U 9740 4870
Dibenzo(a,h)Anthracene 53-70-3 U 9740 4870
Dibenzofuran 132-64-9 U 9740 4870
Diethylphthalate 84-66-2 U 9740 4870
Dimethylphthalate 131-11-3 U 9740 4870
Fluoranthene 206-44-0 U 9740 4870
Fluorene 86-73-7 U 9740 4870
Hexachlorobenzene 118-74-1 U 9740 4870
Hexachlorobutadiene 87-68-3 U 9740 4870
Hexachlorocyclopentadiene 77-47-4 U 44300 22100
Page 29 of 30 Generated at May 30, 2017 08:38
Page 32
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of AnalysisAnalyte CAS # Result Qual RL MDL
Hexachloroethane 67-72-1 U 9740 4870
Indeno(1,2,3-cd)pyrene 193-39-5 U 9740 4870
Isophorone 78-59-1 U 9740 4870
Diphenylamine/n-Nitrosodiphenylamine 86-30-6 U 9740 4870
N-Nitrosodipropylamine 621-64-7 U 9740 4870
Naphthalene 91-20-3 U 9740 4870
Nitrobenzene 98-95-3 U 9740 4870
Pentachlorophenol 87-86-5 U 48700 24300
Phenanthrene 85-01-8 U 9740 4870
Phenol 108-95-2 U 9740 4870
Pyrene 129-00-0 U 9740 4870
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 54.9 19 122
2-Fluorobiphenyl 64.3 30 115
2-Fluorophenol 46.1 25 121
Nitrobenzene-d5 72.5 23 120
p-Terphenyl-d14 68.3 18 137
Phenol-d5 49.0 24 113
U Not detected at or above adjusted sample detection limit
Page 30 of 30 Generated at May 30, 2017 08:38
Page 33
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Sample #: L17051231-01 PrePrep Method: Instrument: HPMS8
Client ID: 17-0751 OSG DISPOSAL PIT Prep Method: 5030B/5030C/5035A Prep Date: N/A
Matrix: TCLP Leach Analytical Method: 8260B Cal Date: 04/17/2017 18:24
Workgroup #: WG615405 Analyst: TMB Run Date: 05/24/2017 14:22
Collect Date: 05/19/2017 13:24 Dilution: 10 File ID: 8M419874
Sample Tag: DL01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Benzene U 50.0 1.25 D018 500
Carbon tetrachloride U 50.0 2.50 D019 500
Chlorobenzene U 50.0 1.25 D021 100000
Chloroform U 50.0 1.25 D022 6000
1,2-Dichloroethane U 50.0 2.50 D028 500
1,1-Dichloroethene U 50.0 5.00 D029 700
Methyl Ethyl Ketone U 100 25.0 D035 200000
Tetrachloroethene U 50.0 2.50 D039 700
Trichloroethene U 50.0 2.50 D040 500
Vinyl chloride U 100 2.50 D043 200
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 101 86 118
1,2-Dichloroethane-d4 96.9 80 120
Toluene-d8 107 88 110
4-Bromofluorobenzene 106 86 115
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-01 PrePrep Method: Instrument: HPMS12
Client ID: 17-0751 OSG DISPOSAL PIT Prep Method: 3510C Prep Date: 05/23/2017 14:05
Matrix: TCLP Leach Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615400 Analyst: MES Run Date: 05/24/2017 12:31
Collect Date: 05/19/2017 13:24 Dilution: 1 File ID: 12M62319
Sample Tag: 01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
o-Cresol U 50.0 25.0 D023 200000
m-,p-Cresol U 50.0 25.0 D025 200000
1,4-Dichlorobenzene U 50.0 25.0 D027 7500
2,4-Dinitrotoluene U 50.0 25.0 D030 130
Hexachlorobenzene U 50.0 25.0 D032 130
Hexachlorobutadiene U 50.0 25.0 D033 500
Hexachloroethane U 50.0 25.0 D034 3000
Page 1 of 16 Generated at May 30, 2017 08:37
Page 34
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Nitrobenzene U 50.0 25.0 D036 2000
Pentachlorophenol U 250 125 D037 100000
Pyridine U 250 125 D038 5000
2,4,5-Trichlorophenol U 50.0 25.0 D041 400000
2,4,6-Trichlorophenol U 50.0 25.0 D042 2000
Surrogate Recovery Lower Limit Upper Limit Q
2-Fluorophenol 41.7 21 100
Phenol-d5 29.6 10 94
Nitrobenzene-d5 78.9 35 114
2-Fluorobiphenyl 74.6 43 116
2,4,6-Tribromophenol 92.1 10 123
p-Terphenyl-d14 99.9 33 141
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-01 PrePrep Method: N/A Instrument: ICP-THERMO4
Client ID: 17-0751 OSG DISPOSAL PIT Prep Method: 3015A Prep Date: 05/23/2017 09:43
Matrix: TCLP Leach Analytical Method: 6010B Cal Date: 05/23/2017 14:24
Workgroup #: WG615308 Analyst: KKB Run Date: 05/23/2017 16:45
Collect Date: 05/19/2017 13:24 Dilution: 1 File ID: T4.052317.164558
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Arsenic, TCLP U 1.00 0.500 D004 5
Barium, TCLP 0.869 0.100 0.0500 D005 100
Cadmium, TCLP U 0.100 0.0500 D006 1
Chromium, TCLP U 0.200 0.100 D007 5
Lead, TCLP U 1.00 0.500 D008 5
Selenium, TCLP U 0.800 0.400 D010 1
Silver, TCLP U 0.100 0.0500 D011 5
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-01 PrePrep Method: Instrument: CVAA1
Client ID: 17-0751 OSG DISPOSAL PIT Prep Method: 7470A Prep Date: 05/23/2017 09:19
Matrix: TCLP Leach Analytical Method: 7470A Cal Date: 05/23/2017 14:40
Workgroup #: WG615315 Analyst: LSJ Run Date: 05/23/2017 15:46
Collect Date: 05/19/2017 13:24 Dilution: 1 File ID: M7.052317.154615
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Mercury U 0.00200 0.00100 D009 0.2
Page 2 of 16 Generated at May 30, 2017 08:37
Page 35
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-03 PrePrep Method: Instrument: HPMS11
Client ID: 17-0751 IR MUD ORIGINAL Prep Method: 5030B/5030C/5035A Prep Date: N/A
Matrix: TCLP Leach Analytical Method: 8260B Cal Date: 05/16/2017 17:16
Workgroup #: WG615282 Analyst: TMB/JDS Run Date: 05/23/2017 18:54
Collect Date: 05/19/2017 15:00 Dilution: 10 File ID: 11M18579
Sample Tag: DL01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Benzene U 50.0 1.25 D018 500
Carbon tetrachloride U 50.0 2.50 D019 500
Chlorobenzene U 50.0 1.25 D021 100000
Chloroform U 50.0 1.25 D022 6000
1,2-Dichloroethane U 50.0 2.50 D028 500
1,1-Dichloroethene U 50.0 5.00 D029 700
Methyl Ethyl Ketone U 100 25.0 D035 200000
Tetrachloroethene U 50.0 2.50 D039 700
Trichloroethene U 50.0 2.50 D040 500
Vinyl chloride U 100 2.50 D043 200
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 103 86 118
1,2-Dichloroethane-d4 105 80 120
Toluene-d8 110 88 110
4-Bromofluorobenzene 108 86 115
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-03 PrePrep Method: Instrument: HPMS12
Client ID: 17-0751 IR MUD ORIGINAL Prep Method: 3510C Prep Date: 05/23/2017 14:05
Matrix: TCLP Leach Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615400 Analyst: MES Run Date: 05/24/2017 13:04
Collect Date: 05/19/2017 15:00 Dilution: 1 File ID: 12M62320
Sample Tag: 01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
o-Cresol U 50.0 25.0 D023 200000
m-,p-Cresol U 50.0 25.0 D025 200000
1,4-Dichlorobenzene U 50.0 25.0 D027 7500
2,4-Dinitrotoluene U 50.0 25.0 D030 130
Hexachlorobenzene U 50.0 25.0 D032 130
Hexachlorobutadiene U 50.0 25.0 D033 500
Page 3 of 16 Generated at May 30, 2017 08:37
Page 36
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Hexachloroethane U 50.0 25.0 D034 3000
Nitrobenzene U 50.0 25.0 D036 2000
Pentachlorophenol U 250 125 D037 100000
Pyridine U 250 125 D038 5000
2,4,5-Trichlorophenol U 50.0 25.0 D041 400000
2,4,6-Trichlorophenol U 50.0 25.0 D042 2000
Surrogate Recovery Lower Limit Upper Limit Q
2-Fluorophenol 33.7 21 100
Phenol-d5 22.6 10 94
Nitrobenzene-d5 66.7 35 114
2-Fluorobiphenyl 58.9 43 116
2,4,6-Tribromophenol 97.8 10 123
p-Terphenyl-d14 97.0 33 141
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-03 PrePrep Method: N/A Instrument: ICP-THERMO4
Client ID: 17-0751 IR MUD ORIGINAL Prep Method: 3015A Prep Date: 05/23/2017 09:43
Matrix: TCLP Leach Analytical Method: 6010B Cal Date: 05/23/2017 14:24
Workgroup #: WG615308 Analyst: KKB Run Date: 05/23/2017 16:49
Collect Date: 05/19/2017 15:00 Dilution: 1 File ID: T4.052317.164940
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Arsenic, TCLP U 1.00 0.500 D004 5
Barium, TCLP 0.647 0.100 0.0500 D005 100
Cadmium, TCLP U 0.100 0.0500 D006 1
Chromium, TCLP U 0.200 0.100 D007 5
Lead, TCLP U 1.00 0.500 D008 5
Selenium, TCLP U 0.800 0.400 D010 1
Silver, TCLP U 0.100 0.0500 D011 5
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-03 PrePrep Method: Instrument: CVAA1
Client ID: 17-0751 IR MUD ORIGINAL Prep Method: 7470A Prep Date: 05/23/2017 09:19
Matrix: TCLP Leach Analytical Method: 7470A Cal Date: 05/23/2017 14:40
Workgroup #: WG615315 Analyst: LSJ Run Date: 05/23/2017 15:53
Collect Date: 05/19/2017 15:00 Dilution: 1 File ID: M7.052317.155351
Sample Tag: 01 Units: mg/L
Page 4 of 16 Generated at May 30, 2017 08:37
Page 37
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Mercury U 0.00200 0.00100 D009 0.2
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-05 PrePrep Method: Instrument: HPMS11
Client ID: 17-0751 IR MUD SILO Prep Method: 5030B/5030C/5035A Prep Date: N/A
Matrix: TCLP Leach Analytical Method: 8260B Cal Date: 05/16/2017 17:16
Workgroup #: WG615282 Analyst: TMB/JDS Run Date: 05/23/2017 19:23
Collect Date: 05/19/2017 14:45 Dilution: 10 File ID: 11M18580
Sample Tag: DL01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Benzene U 50.0 1.25 D018 500
Carbon tetrachloride U 50.0 2.50 D019 500
Chlorobenzene U 50.0 1.25 D021 100000
Chloroform U 50.0 1.25 D022 6000
1,2-Dichloroethane U 50.0 2.50 D028 500
1,1-Dichloroethene U 50.0 5.00 D029 700
Methyl Ethyl Ketone U 100 25.0 D035 200000
Tetrachloroethene U 50.0 2.50 D039 700
Trichloroethene U 50.0 2.50 D040 500
Vinyl chloride U 100 2.50 D043 200
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 106 86 118
1,2-Dichloroethane-d4 109 80 120
Toluene-d8 113 88 110 *
4-Bromofluorobenzene 113 86 115
* Surrogate or spike compound out of range
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-05 PrePrep Method: Instrument: HPMS12
Client ID: 17-0751 IR MUD SILO Prep Method: 3510C Prep Date: 05/23/2017 14:05
Matrix: TCLP Leach Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615400 Analyst: MES Run Date: 05/24/2017 13:37
Collect Date: 05/19/2017 14:45 Dilution: 1 File ID: 12M62321
Sample Tag: 01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
o-Cresol U 50.0 25.0 D023 200000
m-,p-Cresol U 50.0 25.0 D025 200000
1,4-Dichlorobenzene U 50.0 25.0 D027 7500
Page 5 of 16 Generated at May 30, 2017 08:37
Page 38
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Analyte Result Qual RL MDL EPA HW# Reg. Limit
2,4-Dinitrotoluene U 50.0 25.0 D030 130
Hexachlorobenzene U 50.0 25.0 D032 130
Hexachlorobutadiene U 50.0 25.0 D033 500
Hexachloroethane U 50.0 25.0 D034 3000
Nitrobenzene U 50.0 25.0 D036 2000
Pentachlorophenol U 250 125 D037 100000
Pyridine U 250 125 D038 5000
2,4,5-Trichlorophenol U 50.0 25.0 D041 400000
2,4,6-Trichlorophenol U 50.0 25.0 D042 2000
Surrogate Recovery Lower Limit Upper Limit Q
2-Fluorophenol 47.3 21 100
Phenol-d5 30.3 10 94
Nitrobenzene-d5 95.2 35 114
2-Fluorobiphenyl 85.2 43 116
2,4,6-Tribromophenol 113 10 123
p-Terphenyl-d14 107 33 141
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-05 PrePrep Method: N/A Instrument: ICP-THERMO4
Client ID: 17-0751 IR MUD SILO Prep Method: 3015A Prep Date: 05/23/2017 09:43
Matrix: TCLP Leach Analytical Method: 6010B Cal Date: 05/23/2017 14:24
Workgroup #: WG615308 Analyst: KKB Run Date: 05/23/2017 17:00
Collect Date: 05/19/2017 14:45 Dilution: 1 File ID: T4.052317.170036
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Arsenic, TCLP U 1.00 0.500 D004 5
Barium, TCLP 0.712 0.100 0.0500 D005 100
Cadmium, TCLP U 0.100 0.0500 D006 1
Chromium, TCLP U 0.200 0.100 D007 5
Lead, TCLP U 1.00 0.500 D008 5
Selenium, TCLP U 0.800 0.400 D010 1
Silver, TCLP U 0.100 0.0500 D011 5
U Not detected at or above adjusted sample detection limit
Page 6 of 16 Generated at May 30, 2017 08:37
Page 39
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Sample #: L17051231-05 PrePrep Method: Instrument: CVAA1
Client ID: 17-0751 IR MUD SILO Prep Method: 7470A Prep Date: 05/23/2017 09:19
Matrix: TCLP Leach Analytical Method: 7470A Cal Date: 05/23/2017 14:40
Workgroup #: WG615315 Analyst: LSJ Run Date: 05/23/2017 15:56
Collect Date: 05/19/2017 14:45 Dilution: 1 File ID: M7.052317.155624
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Mercury U 0.00200 0.00100 D009 0.2
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-07 PrePrep Method: Instrument: HPMS11
Client ID: 17-0751 IR MUD GRID A3 NEW
Prep Method: 5030B/5030C/5035A Prep Date: N/A
Matrix: TCLP Leach Analytical Method: 8260B Cal Date: 05/16/2017 17:16
Workgroup #: WG615282 Analyst: TMB/JDS Run Date: 05/23/2017 19:52
Collect Date: 05/19/2017 15:30 Dilution: 10 File ID: 11M18581
Sample Tag: DL01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Benzene U 50.0 1.25 D018 500
Carbon tetrachloride U 50.0 2.50 D019 500
Chlorobenzene U 50.0 1.25 D021 100000
Chloroform U 50.0 1.25 D022 6000
1,2-Dichloroethane U 50.0 2.50 D028 500
1,1-Dichloroethene U 50.0 5.00 D029 700
Methyl Ethyl Ketone U 100 25.0 D035 200000
Tetrachloroethene U 50.0 2.50 D039 700
Trichloroethene U 50.0 2.50 D040 500
Vinyl chloride U 100 2.50 D043 200
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 103 86 118
1,2-Dichloroethane-d4 107 80 120
Toluene-d8 111 88 110 *
4-Bromofluorobenzene 110 86 115
* Surrogate or spike compound out of range
U Not detected at or above adjusted sample detection limit
Page 7 of 16 Generated at May 30, 2017 08:37
Page 40
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Sample #: L17051231-07 PrePrep Method: Instrument: HPMS12
Client ID: 17-0751 IR MUD GRID A3 NEW
Prep Method: 3510C Prep Date: 05/23/2017 14:05
Matrix: TCLP Leach Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615400 Analyst: MES Run Date: 05/24/2017 14:10
Collect Date: 05/19/2017 15:30 Dilution: 1 File ID: 12M62322
Sample Tag: 01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
o-Cresol U 50.0 25.0 D023 200000
m-,p-Cresol U 50.0 25.0 D025 200000
1,4-Dichlorobenzene U 50.0 25.0 D027 7500
2,4-Dinitrotoluene U 50.0 25.0 D030 130
Hexachlorobenzene U 50.0 25.0 D032 130
Hexachlorobutadiene U 50.0 25.0 D033 500
Hexachloroethane U 50.0 25.0 D034 3000
Nitrobenzene U 50.0 25.0 D036 2000
Pentachlorophenol U 250 125 D037 100000
Pyridine U 250 125 D038 5000
2,4,5-Trichlorophenol U 50.0 25.0 D041 400000
2,4,6-Trichlorophenol U 50.0 25.0 D042 2000
Surrogate Recovery Lower Limit Upper Limit Q
2-Fluorophenol 41.1 21 100
Phenol-d5 29.5 10 94
Nitrobenzene-d5 84.5 35 114
2-Fluorobiphenyl 78.0 43 116
2,4,6-Tribromophenol 107 10 123
p-Terphenyl-d14 97.8 33 141
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-07 PrePrep Method: N/A Instrument: ICP-THERMO4
Client ID: 17-0751 IR MUD GRID A3 NEW
Prep Method: 3015A Prep Date: 05/23/2017 09:43
Matrix: TCLP Leach Analytical Method: 6010B Cal Date: 05/23/2017 14:24
Workgroup #: WG615308 Analyst: KKB Run Date: 05/23/2017 17:04
Collect Date: 05/19/2017 15:30 Dilution: 1 File ID: T4.052317.170417
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Arsenic, TCLP U 1.00 0.500 D004 5
Barium, TCLP 0.391 0.100 0.0500 D005 100
Page 8 of 16 Generated at May 30, 2017 08:37
Page 41
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Cadmium, TCLP U 0.100 0.0500 D006 1
Chromium, TCLP U 0.200 0.100 D007 5
Lead, TCLP U 1.00 0.500 D008 5
Selenium, TCLP U 0.800 0.400 D010 1
Silver, TCLP U 0.100 0.0500 D011 5
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-07 PrePrep Method: Instrument: CVAA1
Client ID: 17-0751 IR MUD GRID A3 NEW
Prep Method: 7470A Prep Date: 05/23/2017 09:19
Matrix: TCLP Leach Analytical Method: 7470A Cal Date: 05/23/2017 14:40
Workgroup #: WG615315 Analyst: LSJ Run Date: 05/23/2017 15:58
Collect Date: 05/19/2017 15:30 Dilution: 1 File ID: M7.052317.155857
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Mercury U 0.00200 0.00100 D009 0.2
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-09 PrePrep Method: Instrument: HPMS11
Client ID: 17-0751 WEST BOREHOLE RETURN M
Prep Method: 5030B/5030C/5035A Prep Date: N/A
Matrix: TCLP Leach Analytical Method: 8260B Cal Date: 05/16/2017 17:16
Workgroup #: WG615282 Analyst: TMB/JDS Run Date: 05/23/2017 20:20
Collect Date: 05/19/2017 16:18 Dilution: 10 File ID: 11M18582
Sample Tag: DL01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Benzene U 50.0 1.25 D018 500
Carbon tetrachloride U 50.0 2.50 D019 500
Chlorobenzene U 50.0 1.25 D021 100000
Chloroform U 50.0 1.25 D022 6000
1,2-Dichloroethane U 50.0 2.50 D028 500
1,1-Dichloroethene U 50.0 5.00 D029 700
Methyl Ethyl Ketone U 100 25.0 D035 200000
Tetrachloroethene U 50.0 2.50 D039 700
Trichloroethene U 50.0 2.50 D040 500
Vinyl chloride U 100 2.50 D043 200
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 102 86 118
Page 9 of 16 Generated at May 30, 2017 08:37
Page 42
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Surrogate Recovery Lower Limit Upper Limit Q
1,2-Dichloroethane-d4 108 80 120
Toluene-d8 111 88 110 *
4-Bromofluorobenzene 112 86 115
* Surrogate or spike compound out of range
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-09 PrePrep Method: Instrument: HPMS12
Client ID: 17-0751 WEST BOREHOLE RETURN M
Prep Method: 3510C Prep Date: 05/23/2017 14:05
Matrix: TCLP Leach Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615400 Analyst: MES Run Date: 05/24/2017 14:43
Collect Date: 05/19/2017 16:18 Dilution: 1 File ID: 12M62323
Sample Tag: 01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
o-Cresol U 50.0 25.0 D023 200000
m-,p-Cresol U 50.0 25.0 D025 200000
1,4-Dichlorobenzene U 50.0 25.0 D027 7500
2,4-Dinitrotoluene U 50.0 25.0 D030 130
Hexachlorobenzene U 50.0 25.0 D032 130
Hexachlorobutadiene U 50.0 25.0 D033 500
Hexachloroethane U 50.0 25.0 D034 3000
Nitrobenzene U 50.0 25.0 D036 2000
Pentachlorophenol U 250 125 D037 100000
Pyridine U 250 125 D038 5000
2,4,5-Trichlorophenol U 50.0 25.0 D041 400000
2,4,6-Trichlorophenol U 50.0 25.0 D042 2000
Surrogate Recovery Lower Limit Upper Limit Q
2-Fluorophenol 31.3 21 100
Phenol-d5 22.1 10 94
Nitrobenzene-d5 64.5 35 114
2-Fluorobiphenyl 61.6 43 116
2,4,6-Tribromophenol 84.5 10 123
p-Terphenyl-d14 99.8 33 141
U Not detected at or above adjusted sample detection limit
Page 10 of 16 Generated at May 30, 2017 08:37
Page 43
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Sample #: L17051231-09 PrePrep Method: N/A Instrument: ICP-THERMO4
Client ID: 17-0751 WEST BOREHOLE RETURN M
Prep Method: 3015A Prep Date: 05/23/2017 09:43
Matrix: TCLP Leach Analytical Method: 6010B Cal Date: 05/23/2017 14:24
Workgroup #: WG615308 Analyst: KKB Run Date: 05/23/2017 17:07
Collect Date: 05/19/2017 16:18 Dilution: 1 File ID: T4.052317.170759
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Arsenic, TCLP U 1.00 0.500 D004 5
Barium, TCLP 0.512 0.100 0.0500 D005 100
Cadmium, TCLP U 0.100 0.0500 D006 1
Chromium, TCLP U 0.200 0.100 D007 5
Lead, TCLP U 1.00 0.500 D008 5
Selenium, TCLP U 0.800 0.400 D010 1
Silver, TCLP U 0.100 0.0500 D011 5
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-09 PrePrep Method: Instrument: CVAA1
Client ID: 17-0751 WEST BOREHOLE RETURN M
Prep Method: 7470A Prep Date: 05/23/2017 09:19
Matrix: TCLP Leach Analytical Method: 7470A Cal Date: 05/23/2017 14:40
Workgroup #: WG615315 Analyst: LSJ Run Date: 05/23/2017 16:01
Collect Date: 05/19/2017 16:18 Dilution: 1 File ID: M7.052317.160130
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Mercury U 0.00200 0.00100 D009 0.2
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-11 PrePrep Method: Instrument: HPMS11
Client ID: 17-0751 WEST RECLAIMER PIT
Prep Method: 5030B/5030C/5035A Prep Date: N/A
Matrix: TCLP Leach Analytical Method: 8260B Cal Date: 05/16/2017 17:16
Workgroup #: WG615282 Analyst: TMB/JDS Run Date: 05/23/2017 20:49
Collect Date: 05/19/2017 16:30 Dilution: 10 File ID: 11M18583
Sample Tag: DL01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Benzene U 50.0 1.25 D018 500
Carbon tetrachloride U 50.0 2.50 D019 500
Chlorobenzene U 50.0 1.25 D021 100000
Page 11 of 16 Generated at May 30, 2017 08:37
Page 44
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Chloroform U 50.0 1.25 D022 6000
1,2-Dichloroethane U 50.0 2.50 D028 500
1,1-Dichloroethene U 50.0 5.00 D029 700
Methyl Ethyl Ketone U 100 25.0 D035 200000
Tetrachloroethene U 50.0 2.50 D039 700
Trichloroethene U 50.0 2.50 D040 500
Vinyl chloride U 100 2.50 D043 200
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 101 86 118
1,2-Dichloroethane-d4 104 80 120
Toluene-d8 108 88 110
4-Bromofluorobenzene 113 86 115
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-11 PrePrep Method: Instrument: HPMS12
Client ID: 17-0751 WEST RECLAIMER PIT
Prep Method: 3510C Prep Date: 05/23/2017 14:05
Matrix: TCLP Leach Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615400 Analyst: MES Run Date: 05/24/2017 15:16
Collect Date: 05/19/2017 16:30 Dilution: 1 File ID: 12M62324
Sample Tag: 01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
o-Cresol U 50.0 25.0 D023 200000
m-,p-Cresol U 50.0 25.0 D025 200000
1,4-Dichlorobenzene U 50.0 25.0 D027 7500
2,4-Dinitrotoluene U 50.0 25.0 D030 130
Hexachlorobenzene U 50.0 25.0 D032 130
Hexachlorobutadiene U 50.0 25.0 D033 500
Hexachloroethane U 50.0 25.0 D034 3000
Nitrobenzene U 50.0 25.0 D036 2000
Pentachlorophenol U 250 125 D037 100000
Pyridine U 250 125 D038 5000
2,4,5-Trichlorophenol U 50.0 25.0 D041 400000
2,4,6-Trichlorophenol U 50.0 25.0 D042 2000
Surrogate Recovery Lower Limit Upper Limit Q
2-Fluorophenol 43.2 21 100
Phenol-d5 28.7 10 94
Nitrobenzene-d5 84.4 35 114
2-Fluorobiphenyl 77.6 43 116
Page 12 of 16 Generated at May 30, 2017 08:37
Page 45
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Surrogate Recovery Lower Limit Upper Limit Q
2,4,6-Tribromophenol 99.9 10 123
p-Terphenyl-d14 93.5 33 141
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-11 PrePrep Method: N/A Instrument: ICP-THERMO4
Client ID: 17-0751 WEST RECLAIMER PIT
Prep Method: 3015A Prep Date: 05/23/2017 09:43
Matrix: TCLP Leach Analytical Method: 6010B Cal Date: 05/23/2017 14:24
Workgroup #: WG615308 Analyst: KKB Run Date: 05/23/2017 17:11
Collect Date: 05/19/2017 16:30 Dilution: 1 File ID: T4.052317.171142
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Arsenic, TCLP U 1.00 0.500 D004 5
Barium, TCLP 0.441 0.100 0.0500 D005 100
Cadmium, TCLP U 0.100 0.0500 D006 1
Chromium, TCLP U 0.200 0.100 D007 5
Lead, TCLP U 1.00 0.500 D008 5
Selenium, TCLP U 0.800 0.400 D010 1
Silver, TCLP U 0.100 0.0500 D011 5
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-11 PrePrep Method: Instrument: CVAA1
Client ID: 17-0751 WEST RECLAIMER PIT
Prep Method: 7470A Prep Date: 05/23/2017 09:19
Matrix: TCLP Leach Analytical Method: 7470A Cal Date: 05/23/2017 14:40
Workgroup #: WG615315 Analyst: LSJ Run Date: 05/23/2017 16:04
Collect Date: 05/19/2017 16:30 Dilution: 1 File ID: M7.052317.160401
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Mercury U 0.00200 0.00100 D009 0.2
U Not detected at or above adjusted sample detection limit
Page 13 of 16 Generated at May 30, 2017 08:37
Page 46
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Sample #: L17051231-13 PrePrep Method: Instrument: HPMS11
Client ID: 17-0751 EAST RECLAIMER NEW MUD
Prep Method: 5030B/5030C/5035A Prep Date: N/A
Matrix: TCLP Leach Analytical Method: 8260B Cal Date: 05/16/2017 17:16
Workgroup #: WG615282 Analyst: TMB/JDS Run Date: 05/23/2017 21:18
Collect Date: 05/19/2017 17:12 Dilution: 10 File ID: 11M18584
Sample Tag: DL01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Benzene U 50.0 1.25 D018 500
Carbon tetrachloride U 50.0 2.50 D019 500
Chlorobenzene U 50.0 1.25 D021 100000
Chloroform U 50.0 1.25 D022 6000
1,2-Dichloroethane U 50.0 2.50 D028 500
1,1-Dichloroethene U 50.0 5.00 D029 700
Methyl Ethyl Ketone U 100 25.0 D035 200000
Tetrachloroethene U 50.0 2.50 D039 700
Trichloroethene U 50.0 2.50 D040 500
Vinyl chloride U 100 2.50 D043 200
Surrogate Recovery Lower Limit Upper Limit Q
Dibromofluoromethane 101 86 118
1,2-Dichloroethane-d4 107 80 120
Toluene-d8 108 88 110
4-Bromofluorobenzene 107 86 115
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-13 PrePrep Method: Instrument: HPMS12
Client ID: 17-0751 EAST RECLAIMER NEW MUD
Prep Method: 3510C Prep Date: 05/23/2017 14:05
Matrix: TCLP Leach Analytical Method: 8270C Cal Date: 04/10/2017 20:59
Workgroup #: WG615400 Analyst: MES Run Date: 05/24/2017 15:49
Collect Date: 05/19/2017 17:12 Dilution: 1 File ID: 12M62325
Sample Tag: 01 Units: ug/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
o-Cresol U 50.0 25.0 D023 200000
m-,p-Cresol U 50.0 25.0 D025 200000
1,4-Dichlorobenzene U 50.0 25.0 D027 7500
2,4-Dinitrotoluene U 50.0 25.0 D030 130
Hexachlorobenzene U 50.0 25.0 D032 130
Hexachlorobutadiene U 50.0 25.0 D033 500
Page 14 of 16 Generated at May 30, 2017 08:37
Page 47
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Hexachloroethane U 50.0 25.0 D034 3000
Nitrobenzene U 50.0 25.0 D036 2000
Pentachlorophenol U 250 125 D037 100000
Pyridine U 250 125 D038 5000
2,4,5-Trichlorophenol U 50.0 25.0 D041 400000
2,4,6-Trichlorophenol U 50.0 25.0 D042 2000
Surrogate Recovery Lower Limit Upper Limit Q
2-Fluorophenol 34.8 21 100
Phenol-d5 24.9 10 94
Nitrobenzene-d5 69.3 35 114
2-Fluorobiphenyl 66.2 43 116
2,4,6-Tribromophenol 77.0 10 123
p-Terphenyl-d14 100 33 141
U Not detected at or above adjusted sample detection limit
Sample #: L17051231-13 PrePrep Method: N/A Instrument: ICP-THERMO4
Client ID: 17-0751 EAST RECLAIMER NEW MUD
Prep Method: 3015A Prep Date: 05/23/2017 09:43
Matrix: TCLP Leach Analytical Method: 6010B Cal Date: 05/23/2017 14:24
Workgroup #: WG615308 Analyst: KKB Run Date: 05/23/2017 17:15
Collect Date: 05/19/2017 17:12 Dilution: 1 File ID: T4.052317.171525
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Arsenic, TCLP U 1.00 0.500 D004 5
Barium, TCLP 0.131 0.100 0.0500 D005 100
Cadmium, TCLP U 0.100 0.0500 D006 1
Chromium, TCLP U 0.200 0.100 D007 5
Lead, TCLP U 1.00 0.500 D008 5
Selenium, TCLP U 0.800 0.400 D010 1
Silver, TCLP U 0.100 0.0500 D011 5
U Not detected at or above adjusted sample detection limit
Page 15 of 16 Generated at May 30, 2017 08:37
Page 48
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Certificate of Analysis
Sample #: L17051231-13 PrePrep Method: Instrument: CVAA1
Client ID: 17-0751 EAST RECLAIMER NEW MUD
Prep Method: 7470A Prep Date: 05/23/2017 09:19
Matrix: TCLP Leach Analytical Method: 7470A Cal Date: 05/23/2017 14:40
Workgroup #: WG615315 Analyst: LSJ Run Date: 05/23/2017 16:06
Collect Date: 05/19/2017 17:12 Dilution: 1 File ID: M7.052317.160631
Sample Tag: 01 Units: mg/L
Analyte Result Qual RL MDL EPA HW# Reg. Limit
Mercury U 0.00200 0.00100 D009 0.2
U Not detected at or above adjusted sample detection limit
Page 16 of 16 Generated at May 30, 2017 08:37
Page 49
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Lab Report #: L17051231
Lab Project #: 2755.044
Project Name: NORTHEAST DISTRICT OFFICE #3
Lab Contact: Michelle Taylor
Sample #: L17051231-02 Client ID: 17-0751 OSG DISPOSAL PIT Matrix: Soil Collect Date: 05/19/2017 13:24
Analyte Result Units Qualifier
Percent Solids 50.0 weight %
Sample #: L17051231-04 Client ID: 17-0751 IR MUD ORIGINAL Matrix: Soil Collect Date: 05/19/2017 15:00
Analyte Result Units Qualifier
Percent Solids 45.2 weight %
Sample #: L17051231-06 Client ID: 17-0751 IR MUD SILO Matrix: Soil Collect Date: 05/19/2017 14:45
Analyte Result Units Qualifier
Percent Solids 49.0 weight %
Sample #: L17051231-08 Client ID: 17-0751 IR MUD GRID A3 NEW Matrix: Soil Collect Date: 05/19/2017 15:30
Analyte Result Units Qualifier
Percent Solids 26.5 weight %
Sample #: L17051231-10 Client ID: 17-0751 WEST BOREHOLE RETURN M
Matrix: Soil Collect Date: 05/19/2017 16:18
Analyte Result Units Qualifier
Percent Solids 41.6 weight %
Sample #: L17051231-12 Client ID: 17-0751 WEST RECLAIMER PIT Matrix: Soil Collect Date: 05/19/2017 16:30
Analyte Result Units Qualifier
Percent Solids 56.8 weight %
Sample #: L17051231-14 Client ID: 17-0751 EAST RECLAIMER NEW MUD
Matrix: Soil Collect Date: 05/19/2017 17:12
Analyte Result Units Qualifier
Percent Solids 1.96 weight %
Page 1 of 1 Generated at May 30, 2017 08:37
Page 50
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac LaboratoriesCase Narrative
Login Number: L17051231Department: VolatilesAnalyst: Anthony Canter
METHOD
Preparation SW-846 5030B/5030C/5035A
Analysis SW-846 8260B
HOLDING TIMES
Sample Preparation: All holding times were met.
Sample Analysis: All holding times were met.
PREPARATION
Sample preparation proceeded normally.
CALIBRATION
Initial Calibration: For all compounds that yielded a %RSD greater than 15%, linear or higher order equations were applied. All acceptance criteria were met.
Alternate Source Standards: Chloromethane, Bromomethane, 4-Chlorotoluene, Dichlorodifluoromethane, n-Propylbenzene, Vinyl Acetate exceeded the upper limit, and Carbon Disulfide was below the lower limit in ICV WG615237-11 analyzed 05/23/2017 on HPMS9. Outliers were not detected above reporting limits in associated samples. All other acceptance criteria were met. Please see the applicable QC report for a detailed presentation of the failures.
Continuing Calibration and Tune: Chloromethane (non-target system performance check compound) exceeded the upper limit in CCV WG615404-02 analyzed 05/24/2017 on HPMS8. SPCC criteria were met. All other acceptance criteria were met. Please see the applicable QC report for a detailed presentation of the failures.
BATCH QA/QC
Method Blank: All acceptance criteria were met.
Laboratory Control Sample: Bromomethane and Dichlorodifluoromethane exceeded the upper limit in LCS WG615352-02 analyzed 05/23/2017 on HPMS9. All other acceptance criteria were met. Please see the applicable QC report for a detailed presentation of the failures.
Page 1 of 3 Generated at May 27, 2017 20:00
Page 51
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Sample # Analyte Date Result Lower Upper Type
WG615352-02 Bromomethane 2017-05-23 17:16:00 145 37 143 Recovery
WG615352-02 Dichlorodifluoromethane 2017-05-23 17:16:00 158 25 130 Recovery
Matrix Spikes: The MS/MSD results were not associated with this sample delivery group (SDG), due to insufficient volume of sample. The laboratory included an LCS and LCS duplicate in the preparation batch in lieu of the NELAC prescribed MS/MSD. Microbac Laboratories recommends site specific MS/MSD samples to avoid possible data qualifications.
SAMPLES
Internal Standards: Sample 10 yielded low recovery for 1,4-Dichlorobenzene-d4. Sample matrix interference was obvious due to hydrocarbon. Other samples with similar amounts of hydrocarbon also yielded recovery lower than expected, but within acceptance limits. All other acceptance criteria were met.
Surrogates: Recoveries out of range were observed for the following surrogates: 4-Bromofluorobenzene, Toluene-d8. Samples 02, 04, 05, 07, 09, 10, 12 had one surrogate outlier per sample. No reanalysis required. Please see the applicable QC report for a detailed presentation of the failures.
Sample # Analyte Date Result Lower Upper Type
L17051231-04 4-Bromofluorobenzene 2017-05-23 17:46:00 127 74 121 Recovery
L17051231-10 4-Bromofluorobenzene 2017-05-23 19:17:00 135 74 121 Recovery
L17051231-05 Toluene-d8 2017-05-23 19:23:00 113 88 110 Recovery
L17051231-12 4-Bromofluorobenzene 2017-05-23 19:47:00 122 74 121 Recovery
L17051231-07 Toluene-d8 2017-05-23 19:52:00 111 88 110 Recovery
L17051231-09 Toluene-d8 2017-05-23 20:20:00 111 88 110 Recovery
L17051231-02 4-Bromofluorobenzene 2017-05-23 20:47:00 150 74 121 Recovery
Other: Samples 01, 03, 05, 07, 09, 11, 13 were run at a dilution due to TCLP matrix.
Manual Integration Reason Codes
Reason #1: Data System Fails to Select Correct Peak. In some cases the chromatography system selects and integrates the 'wrong peak'. In this case the analyst must correct the selection and force the system to integrate the proper peak. Other times the system may miss the peak completely.
Reason #2: Data System Splits the Peak Incorrectly or Integrates a False Peak as a Rider Peak. This phenomena is common at low concentrations where the signal:noise ratio is low. A single compound (peak) is incorrectly split into multiple peaks or integrated as a main peak with one or more rider peaks resulting in low areacounts for the target compound.
Reason #3: Improperly Integrated Isomers and/or coeluting compounds. This system often fails to distinguish coeluting compounds and or isomers. The integration areas and concentrations are wrong, and they must be corrected by manual integration. Prime examples are benzo(k)fluoranthene and benzo(b)fluoranthene which are often unresolved and integrated improperly when both are present at low concentrations in standards or samples.
Reason #4: System Establishes Incorrect Baseline. There are numerous situations in chromatography where the system establishes the baseline incorrectly. Some baseline errors will be obvious to the analyst and should be corrected via manual procedures.
Page 2 of 3 Generated at May 27, 2017 20:00
Page 52
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Reason #5: Miscellaneous. Other situations involving integration errors may require in-depth review and technical judgment. These cases should be brought to the attention of the laboratory management. If the form of manual integration is not clearly covered by these four cases, then review and approval by the Managing Director or the QAO will be required.
I certify that this data package is in compliance with the terms and conditions agreed to by the client and Microbac Laboratories Inc., both technically and for completeness, except for the conditions noted above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or designated person, as verified by the following signature.
Narrative ID: 125950Approved By: Franci Bolden
Page 3 of 3 Generated at May 27, 2017 20:00
Page 53
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac LaboratoriesCase Narrative
Login Number: L17051231Department: SemivolatilesAnalyst: Mary Schilling
METHOD
Preparation 3510C/1311/3546
Analysis SW-846 8270C
HOLDING TIMES
Sample Preparation: All holding times were met.
Sample Analysis: All holding times were met.
PREPARATION
Sample preparation proceeded normally.
CALIBRATION
Initial Calibration: For all compounds that yielded a %RSD greater than 15%, linear or higher order equations were applied. All acceptance criteria were met.
Alternate Source Standards: All acceptance criteria were met.
Continuing Calibration and Tune: All acceptance criteria were met.
BATCH QA/QC
Method Blank: In the blank analyzed 5/23/17 on HPMS12, WG615091-01, benzoic acid was above the MDL, but below the RL. The samples were non-detect for benzoic acid. Please see the applicable QC report for a detailed presentation of the failures.
Laboratory Control Sample: All acceptance criteria were met.
Matrix Spikes: The client did not specify an MS/MSD for this sample delivery group. The laboratory selected sample 02 for MS/MSD analysis and recoveries out of range were observed for benzoic acid and hexachlorocyclopentadiene. Please see the applicable QC report for a detailed presentation of the failures.
Page 1 of 2 Generated at May 25, 2017 10:06
Page 54
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
SAMPLES
Samples: All acceptance criteria were met.
Internal Standards: All acceptance criteria were met.
Surrogates: All acceptance criteria were met.
Manual Integration Reason Codes
Reason #1: Data System Fails to Select Correct Peak In some cases the chromatography system selects and integrates the 'wrong peak'. In this case the analyst must correct the selection and force the system to integrate the proper peak. Other times the system may miss the peakcompletely.
Reason #2: Data System Splits the Peak Incorrectly or Integrates a False Peak as a Rider Peak This phenomena is common at low concentrations where the signal:noise ratio is low. A single compound (peak) is incorrectly split into multiple peaks or integrated as a main peak with one or more rider peaks resulting in low areacounts for the target compound.
Reason #3: Improperly Integrated Isomers and/or coeluting compounds. This system often fails to distinguish coeluting compounds and or isomers. The integration areas and concentrations are wrong, and they must be corrected by manual integration. Prime examples are benzo(k)fluoranthene andbenzo(b)fluoranthene which are often unresolved and integrated improperly when both are present at low concentrations in standards or samples.
Reason #4: System Establishes Incorrect Baseline There are numerous situations in chromatography where the system establishes the baseline incorrectly. Some baseline errors will be obvious to the analyst and should be corrected via manual procedures.
Reason #5: Miscellaneous Other situations involving integration errors may require in-depth review and technical judgment. These cases should be brought to the attention of the laboratory management. If the form of manual integration is not clearly covered by these four cases, then review and approval by the Managing Director or the QAO will be required.
I certify that this data package is in compliance with the terms and conditions agreed to by the client and Microbac Laboratories Inc., both technically and for completeness, except for the conditions noted above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or designated person, as verified by the following signature.
Narrative ID: 125853Approved By: Eric Lawson
Page 2 of 2 Generated at May 25, 2017 10:06
Page 55
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac LaboratoriesCase Narrative
Login Number: L17051231Department: MetalsAnalyst: Kerri Buck
METHOD
Preparation: SW-846 3015
Analysis: SW-846 6010
HOLDING TIMES
Sample Preparation: All holding times were met.
Sample Analysis: All holding times were met.
PREPARATION
Sample preparation proceeded normally.
CALIBRATION
Initial Calibration: All acceptance criteria were met.
Alternate Source Standards: All acceptance criteria were met.
Interference Check Standards: All acceptance criteria were met.
Continuing Calibration Verification: All acceptance criteria were met.
Continuing Calibration Blank: All acceptance criteria were met.
BATCH QA/QC
Method Blank: All acceptance criteria were met.
Laboratory Control Sample: All acceptance criteria were met.
Serial Dilution/Post Digestion Spikes: WG615308 - All acceptance criteria were met.
Page 1 of 2 Generated at May 24, 2017 12:36
Page 56
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Matrix Spikes: All acceptance criteria were met.
SAMPLES
Samples: All acceptance criteria were met.
Narrative ID: 125811Approved By: Kim Rhodes
Page 2 of 2 Generated at May 24, 2017 12:36
Page 57
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac LaboratoriesCase Narrative
Login Number: L17051231Department: Metals - AAAnalyst: Laura Jones
METHOD
Preparation: SW-846 7470
Analysis: SW-846 7470
HOLDING TIMES
Sample Preparation: All holding times were met.
Sample Analysis: All holding times were met.
PREPARATION
Sample preparation proceeded normally.
CALIBRATION
Initial Calibration: All acceptance criteria were met.
Alternate Source Standards: All acceptance criteria were met.
Interference Check Standards: All acceptance criteria were met.
Continuing Calibration Verification: All acceptance criteria were met.
Continuing Calibration Blank: All acceptance criteria were met.
BATCH QA/QC
Method Blank: All acceptance criteria were met.
Laboratory Control Sample: All acceptance criteria were met.
Serial Dilution/Post Digestion Spikes: WG615315 - All acceptance criteria were met.
Page 1 of 2 Generated at May 24, 2017 12:36
Page 58
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Matrix Spikes: All acceptance criteria were met.
SAMPLES
Samples: All acceptance criteria were met.
Narrative ID: 125806Approved By: Kim Rhodes
Page 2 of 2 Generated at May 24, 2017 12:36
Page 59
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac Laboratories Inc.Ohio Valley Division Analyst List
May 30, 2017
001 - BIO-CHEM TESTING WVDEP 220 002 - REIC Consultants, Inc. WVDEP 060003 - Sturm Environmental 004 - MICROBAC PITTSBURGH005 - ES LABORATORIES 006 - ALCOSAN LABORATORIES007 - ALS LABORATORIES 008 - BENCHMARK LABORATORIES010 - MICROBAC CHICAGOLAND AC - AMBER R. CARMICHAELADC - ANTHONY D. CANTER ADG - APRIL D. GREENEALS - ADRIANE L. STEED AWE - ANDREW W. ESSIGAZH - AFTER HOURS BJO - BRIAN J. OGDENBLG - BRENDA L. GREENWALT BNB - Brandi N. BentleyBRG - BRENDA R. GREGORY CAS - Craig A. SmithCEB - CHAD E. BARNES CLC - CHRYS L. CRAWFORDCLS - CARA L. STRICKLER CPD - CHAD P. DAVISCSH - CHRIS S. HILL CV - Carl VolkmanDAK - DEAN A. KETELSEN DCM - DAVID C. MERCKLEDEV - DAVID E. VANDENBERG DIH - DEANNA I. HESSONDLB - DAVID L. BUMGARNER DLP - DOROTHY L. PAYNEDSM - DAVID S. MOSSOR DTG - DOMINIC T. GEHRETECL - ERIC C. LAWSON EPT - ETHAN P. TIDDERP - ERIN R. PORTER FJB - FRANCES J. BOLDENHRF - HEATHER R. FAIRCHILD JDH - JUSTIN D. HESSONJDS - JARED D. SMITH JKP - JACQUELINE K. PARSONSJLD - JESSICA L. DELONG JST - JOSHUA S. TAYLORJTP - JOSHUA T. PEMBERTON JWR - JOHN W. RICHARDSJWS - JACK W. SHEAVES JYH - JI Y. HUKAK - KATHY A. KIRBY KDD - Katelyn D. DaleyKEB - KATIE E. BARNES KHR - KIM H. RHODESKKB - KERRI K. BUCK KRA - KATHY R. ALBERTSONKRP - KATHY R. PARSONS LJH - Lacey J. HendershotLLS - LARRY L. STEPHENS LSB - LESLIE S. BUCINALSJ - LAURA S. JONES MAP - MARLA A. PORTERMBK - MORGAN B. KNOWLTON MES - MARY E. SCHILLINGMMB - MAREN M. BEERY MRT - MICHELLE R. TAYLOROJE - OMOYEMWEN J. ENGLISH PDM - PIERCE D. MORRISPIT - MICROBAC WARRENDALE REK - BOB E. KYERRLB - BOB BUCHANAN RNP - RICK N. PETTYSAV - SARAH A. VANDENBERG SCA - SUEELLEN C. ADAMSSCB - SARAH C. BOGOLIN SCJ - SUE ELLEN C. JOHNSONSDC - SHALYN D. CONLEY TB - TODD BOYLETMB - TIFFANY M. BAILEY TMM - TAMMY M. MORRISVC - VICKI COLLIER WTD - WADE T. DELONGXXX - UNAVAILABLE OR SUBCONTRACT ZTB - ZACH T. BARNES
Page 60
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
List of Valid QualifiersMay 30, 2017
Qualkey: STD_ND=U
Microbac Laboratories Inc.
Qualifier Description
*+<>AB
B1B3C
CGDLE
EDLEMPCF, SFL
FP1H1IJ
J,BJ,H1J,PJ,SLL1L2MN
NAND, SND,LNFNFLNINRNSPQ
QNSRARES
SMISPTIC
TNTCU
U,H1UJWX
X, SYZ
Surrogate or spike compound out of rangeCorrelation coefficient for the MSA is less than 0.995Result is less than the associated numerical value.Result is greater than the associated numerical value.See the report narrativeAnalyte present in method blankTarget analyte detected in method blank at or above the method reporting limitTarget analyte detected in calibration blank at or above the method reporting limitConfirmed by GC/MSConfluent growthSurrogate or spike compound was diluted outEstimated concentration due to sample matrix interferenceElevated sample reporting limits, presence of non-target analytesEstimated Maximum Possible ConcentrationEstimated result below quantitation limit; method of standard additions(MSA)Free LiquidDid not ignite.Sample analysis performed past holding time.Semiquantitative result (out of instrument calibration range)The analyte was positively identified, but the quantitation was below the RLAnalyte detected in both the method blank and sample above the MDL.The analyte was positively identified, but the quantitation was below the RL. Sample analysis performed past holding timeEstimate; columns don't agree to within 40%Estimated concentration; analyzed by method of standard addition (MSA)Sample reporting limits elevated due to matrix interferenceThe associated blank spike (LCS) recovery was above the laboratory acceptance limits.The associated blank spike (LCS) recovery was below the laboratory acceptance limits.Matrix effect; the concentration is an estimate due to matrix effect.Tentatively identified compound(TIC)Not applicableNot detected; analyzed by method of standard addition (MSA)Not detected; sample reporting limit (RL) elevated due to interferenceNot found by library searchNo free liquidNon-ignitableAnalyte is not required to be analyzedNot spikedConcentrations >40% difference between the two GC columnsOne or more quality control criteria failed. See narrative.Quantity of sample not sufficient to perform analysisReanalysis confirms reported resultsReanalysis confirms sample matrix interferenceAnalyzed by method of standard addition (MSA)Sample matrix interference on surrogateReported results are for spike compounds onlyLibrary Search CompoundToo numerous to countNot detected at or above adjusted sample detection limitNot detected; sample analysis performed past holding time.Undetected; the MDL and RL are estimated due to quality control discrepancies.Post-digestion spike for furnace AA out of control limitsExceeds regulatory limitExceeds regulatory limit; method of standard additions (MSA)This analyte is not on the laboratory's current scope of accreditation.Cannot be resolved from isomer - see below
Page 61
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Organic QA/QC
Page 62
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
05/17/2017 10:07Report generated5297722PDF File ID:
Microbac Laboratories Inc.
METHOD BLANK SUMMARY
Report Name: BLANK_SUMMARY
14G67536
05/16/17 11:21
05/16/17 14:27
WG614544
WG614301-01
HP14
Blank File ID:
Prep Date:
Analyzed Date:
Work Group:
Blank Sample ID:
Instrument ID:
8015CMethod:
LJHAnalyst:
L17050904Login Number:
LCS
LCS2
17-0751 IR MUD 54 RETURN
17-0751 IR MUD SILO
17-0751 IR MUD WE RECLAIM PIT
17-0751 IR MUD BREAKOUT
17-0751 IR MUD GRID C1-D1
WG614301-02
WG614301-03
L17050904-03
L17050904-01
L17050904-04
L17050904-05
L17050904-02
14G67537
14G67538
14G67540
14G67541
14G67542
14G67543
14G67544
05/16/17 15:06
05/16/17 15:45
05/16/17 17:04
05/16/17 17:43
05/16/17 18:22
05/16/17 19:02
05/16/17 19:41
This Method Blank Applies To The Following Samples:
Client ID Lab Sample ID Lab File ID Time Analyzed TAG
01
01
01
01
01
01
01
Page 63
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
05/26/2017 14:28Report generated5309107PDF File ID:
Microbac Laboratories Inc.
METHOD BLANK SUMMARY
Report Name: BLANK_SUMMARY
8M419871
05/24/17 12:57
05/24/17 12:57
WG615405
WG615405-01
HPMS8
Blank File ID:
Prep Date:
Analyzed Date:
Work Group:
Blank Sample ID:
Instrument ID:
8260BMethod:
TMBAnalyst:
L17051231Login Number:
LCS
LCS2
17-0751 OSG DISPOSAL PIT
WG615405-02
WG615405-03
L17051231-01
8M419872
8M419873
8M419874
05/24/17 13:25
05/24/17 13:53
05/24/17 14:22
This Method Blank Applies To The Following Samples:
Client ID Lab Sample ID Lab File ID Time Analyzed TAG
01
01
DL01
Page 64
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
05/26/2017 14:28Report generated5309107PDF File ID:
Microbac Laboratories Inc.
METHOD BLANK SUMMARY
Report Name: BLANK_SUMMARY
8M419884
05/24/17 19:08
05/24/17 19:08
WG615405
WG615405-04
HPMS8
Blank File ID:
Prep Date:
Analyzed Date:
Work Group:
Blank Sample ID:
Instrument ID:
8260BMethod:
TMBAnalyst:
L17051231Login Number:
LCS
LCS2
17-0751 OSG DISPOSAL PIT
WG615405-02
WG615405-03
L17051231-01
8M419872
8M419873
8M419874
05/24/17 13:25
05/24/17 13:53
05/24/17 14:22
This Method Blank Applies To The Following Samples:
Client ID Lab Sample ID Lab File ID Time Analyzed TAG
01
01
DL01
Page 65
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
05/26/2017 14:28Report generated5308756PDF File ID:
Microbac Laboratories Inc.
METHOD BLANK SUMMARY
Report Name: BLANK_SUMMARY
9M980444
05/23/17 16:46
05/23/17 16:46
WG615352
WG615352-01
HPMS9
Blank File ID:
Prep Date:
Analyzed Date:
Work Group:
Blank Sample ID:
Instrument ID:
8260BMethod:
ADCAnalyst:
L17051231Login Number:
LCS
17-0751 IR MUD ORIGINAL
17-0751 IR MUD SILO
17-0751 IR MUD GRID A3 NEW
17-0751 WEST BOREHOLE RETURN M
17-0751 WEST RECLAIMER PIT
17-0751 EAST RECLAIMER NEW MUD
17-0751 OSG DISPOSAL PIT
WG615352-02
L17051231-04
L17051231-06
L17051231-08
L17051231-10
L17051231-12
L17051231-14
L17051231-02
9M980445
9M980446
9M980447
9M980448
9M980449
9M980450
9M980451
9M980452
05/23/17 17:16
05/23/17 17:46
05/23/17 18:16
05/23/17 18:47
05/23/17 19:17
05/23/17 19:47
05/23/17 20:17
05/23/17 20:47
This Method Blank Applies To The Following Samples:
Client ID Lab Sample ID Lab File ID Time Analyzed TAG
01
01
01
01
01
01
01
01
Page 66
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac Laboratories Inc.
METHOD BLANK REPORT
Report Name:BLANK
PDF ID: 5309108
26-MAY-2017 14:28
Dibromofluoromethane
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
99.8
103
106
112
Surrogates % Recovery Surrogate Limits
86
80
88
86
-
-
-
-
118
120
110
115
Qualifier
PASS
PASS
PASS
PASS
Analytes Concentration Dilution Qualifier
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
1,2-Dichloroethane
1,1-Dichloroethene
Methyl Ethyl Ketone
Tetrachloroethene
Trichloroethene
Vinyl chloride
1
1
1
1
1
1
1
1
1
1
0.125
0.250
0.125
0.125
0.250
0.500
2.50
0.250
0.250
0.250
5.00
5.00
5.00
5.00
5.00
5.00
10.0
5.00
5.00
10.0
U
U
U
U
U
U
U
U
U
U
0.125
0.250
0.125
0.125
0.250
0.500
2.50
0.250
0.250
0.250
ND Analyte Not detected at or above reporting limit
* |Analyte concentration| > RL
11M18567
WG615282
Instrument ID:HPMS11
File ID:
Prep Date:05/23/17 13:37
Run Date:05/23/17 13:37
Analyst:TMB/JDS
Workgroup (AAB#): ug/LUnits:
8260BMethod:
WaterMatrix:
L17051231Login Number: WG615282-01Sample ID:
16-MAY-17Cal ID:HPMS11-OT900917Contract #:
5030B/5030C/503Prep Method:
MDL RL
MDL
RL
Method Detection Limit
Reporting/Practical Quantitation Limit
Page 67
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac Laboratories Inc.
METHOD BLANK REPORT
Report Name:BLANK
PDF ID: 5309108
26-MAY-2017 14:28
Dibromofluoromethane
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
103
99.6
107
107
Surrogates % Recovery Surrogate Limits
86
80
88
86
-
-
-
-
118
120
110
115
Qualifier
PASS
PASS
PASS
PASS
Analytes Concentration Dilution Qualifier
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
1,2-Dichloroethane
1,1-Dichloroethene
Methyl Ethyl Ketone
Tetrachloroethene
Trichloroethene
Vinyl chloride
1
1
1
1
1
1
1
1
1
1
0.125
0.250
0.125
0.125
0.250
0.500
2.50
0.250
0.250
0.250
5.00
5.00
5.00
5.00
5.00
5.00
10.0
5.00
5.00
10.0
U
U
U
U
U
U
U
U
U
U
0.125
0.250
0.125
0.125
0.250
0.500
2.50
0.250
0.250
0.250
ND Analyte Not detected at or above reporting limit
* |Analyte concentration| > RL
8M419871
WG615405
Instrument ID:HPMS8
File ID:
Prep Date:05/24/17 12:57
Run Date:05/24/17 12:57
Analyst:TMB
Workgroup (AAB#): ug/LUnits:
8260BMethod:
WaterMatrix:
L17051231Login Number: WG615405-01Sample ID:
17-APR-17Cal ID: HPMS8-OT900917Contract #:
5030B/5030C/503Prep Method:
MDL RL
MDL
RL
Method Detection Limit
Reporting/Practical Quantitation Limit
Page 68
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
SURROGATES - Modified 03/06/2008
05/17/2017 10:07Report generated:5297728PDF File ID:
SURROGATE STANDARDS
Microbac Laboratories Inc.
L17050904-01
L17050904-02
L17050904-03
L17050904-04
L17050904-05
WG614301-01
WG614301-02
WG614301-03
01
01
01
01
01
01
01
01
1 2Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1
2
-
-
o-Terphenyl
Octacosane
8015Method:
HP14Instrument Id:
L17050904Login Number:
SoilMatrix:WG614544Workgroup (AAB#):
Underline = Result out of surrogate limits
26.2 36.2
12.6 9.41
53.4 52.3
30.9 30.4
39.5 34.6
69.6 62.6
69.7 68.2
73.4 74.9
43
25
-
-
136
162
Surrogates Surrogate Limits
DL = surrogate diluted out
HP14CAL ID: -09-MAY-17
ND = surrogate not detected
Page 69
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/17/2017 10:07Report generated5297727PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
Diesel Range (C10-C28) 1000000 1000000 51200 0.384
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
14G67535
WG614544
Instrument ID:HP14
File ID:
Run Date:05/16/2017
Run Time:09:32
Analyst:LJH
Workgroup (AAB#):
8015CMethod:
L17050904Login Number: WG614359-01Sample ID:
09-MAY-17HP14 -Cal ID:
UNITS
ug/kg
UCL20
STDQC Key:
WATERMatrix:
Page 70
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/17/2017 10:07Report generated5297727PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
Diesel Range (C10-C28) 1000000 1040000 53300 4.46
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
14G67546
WG614544
Instrument ID:HP14
File ID:
Run Date:05/16/2017
Run Time:20:59
Analyst:LJH
Workgroup (AAB#):
8015CMethod:
L17050904Login Number: WG614359-02Sample ID:
09-MAY-17HP14 -Cal ID:
UNITS
ug/kg
UCL20
STDQC Key:
WATERMatrix:
Page 71
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Response Factor Report HP14
Method : C:\MSDCHEM\1\METHODS\DROQUANT.M (Chemstation Integrator) Title : SOP:GCS02 8015B/C/D DRO ICAL 05/09/17 Last Update : Tue May 09 14:01:47 2017 WG613451 Calibration Files 10k =14G67512.D 5000 =14G67513.D 2500 =14G67514.D 1000 =14G67515.D 500 =14G67516.D 100 =14G67517.D
Compound 10k 5000 2500 1000 500 100 Avg %RSD -------------------------------------------------------------------------- 1) h Diesel Range (C1 4.697 4.957 4.498 4.973 5.404 6.089 5.103 E4 11.19 2) s O-Terphenyl 5.179 5.829 5.070 5.462 5.901 5.320 5.460 E4 6.25 3) s Octacosane 3.011 4.001 3.424 3.684 3.921 3.732 3.629 E4 10.02 -------------------------------------------------------------------------- (#) = Out of Range
DROQUANT.M Tue May 09 14:42:19 2017
Page 72
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
LCS - Modified 03/06/2008
05/26/2017 14:28Report generated:5308758PDF File ID:
LABORATORY CONTROL SAMPLE (LCS)
Microbac Laboratories Inc.
9M980445
WG615352
Instrument ID:HPMS9
File ID:
Run Date:05/23/2017
Run Time:17:16
Analyst:ADC
Workgroup (AAB#): ug/kgUnits:
5030B/5030C/503Prep Method:
SoilMatrix:
L17051231Login Number:
Analytes Expected Found LCS Limits Q% Rec
Dibromofluoromethane
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
105
103
108
109
Surrogates % Recovery Surrogate Limits
80
80
81
74
-
-
-
-
120
120
117
121
Qualifier
PASS
PASS
PASS
PASS
WG615352-02Sample ID:
23-MAY-17Cal ID: HPMS9-STDQC Key:
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
4-Methyl-2-pentanone
Methylene chloride
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
o-Xylene
m-,p-Xylene
65
68
72
47
74
50
72
74
71
55
72
77
60
65
70
60
72
48
65
75
74
10
45
70
70
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
40.0
21.5
21.4
22.2
20.6
23.2
25.7
23.6
22.4
22.2
23.2
22.1
23.0
23.7
22.8
22.2
23.3
21.4
21.2
23.4
23.4
23.2
25.9
25.7
22.9
45.5
108
107
111
103
116
129
118
112
111
116
110
115
119
114
111
117
107
106
117
117
116
130
129
115
114
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
135
129
128
146
128
146
136
130
137
130
130
126
135
130
135
125
126
154
130
132
133
150
140
130
130
8260BMethod:
* EXCEEDS %REC LIMIT
Lot#:STD81766
Page 73
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
LCS_LCS2 - Modified 03/06/2008
05/26/2017 14:28Report generated:5309109PDF File ID:
LABORATORY CONTROL SAMPLE (LCS)
Microbac Laboratories Inc.
1,1-Dichloroethene
1,2-Dichloroethane
Methyl Ethyl Ketone
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
LCS LCS2
4.01
1.54
5.32
2.70
2.37
2.22
2.08
0.870
1.31
0.804
20.1 20.9
20.8 21.1
18.6 19.6
21.1 21.6
20.4 20.9
21.2 21.7
18.9 19.3
21.4 21.6
20.6 20.8
21.8 22.0
Analytes %RPD
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
Found FoundKnown Known
100 105
104 105
93.0 98.1
105 108
102 105
106 108
94.3 96.3
107 108
103 104
109 110
% REC % REC
20
20
20
20
20
20
20
20
20
20
RPDLmt
%RecLimits
80
80
10
80
65
80
80
80
80
50
132
129
170
121
140
120
125
124
122
170
-
-
-
-
-
-
-
-
-
-
Q
Sample ID:
Sample ID:
WG615282-02
WG615282-03
LCS
LCS2
11M18568
11M18569
File ID:
File ID:
1,2-Dichloroethane-d4
Dibromofluoromethane
4-Bromofluorobenzene
Toluene-d8
LCS LCS2
105 107
101 106
106 106
107 108
Surogates% Recovery % Recovery
Surrogate Limits
80
86
86
88
120
118
115
110
-
-
-
-
Qualifier
PASS
PASS
PASS
PASS
Run Date:
Run Date:
05/23/2017 14:06
05/23/2017 14:35
WG615282
Instrument ID:HPMS11
Analyst:TMB/JDS
Workgroup (AAB#): ug/LUnits:
8260BMethod:TCLP LeachMatrix:
L17051231Login Number: 5030B/5030C/503Prep Method:
* EXCEEDS %REC LIMIT
# EXCEEDS RPD LIMIT
STDQC Key: STD82009Lot #:
Page 74
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
LCS_LCS2 - Modified 03/06/2008
05/26/2017 14:28Report generated:5309109PDF File ID:
LABORATORY CONTROL SAMPLE (LCS)
Microbac Laboratories Inc.
1,1-Dichloroethene
1,2-Dichloroethane
Methyl Ethyl Ketone
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
LCS LCS2
1.45
0.755
4.37
0.537
2.71
0.343
0.881
2.05
3.30
2.69
21.9 22.2
20.1 20.2
15.8 16.5
21.8 21.7
22.5 21.9
19.5 19.4
19.3 19.5
21.1 20.6
21.7 21.0
26.0 25.3
Analytes %RPD
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
Found FoundKnown Known
109 111
100 101
79.2 82.7
109 108
113 110
97.3 97.0
96.5 97.4
105 103
108 105
130 126
% REC % REC
20
20
20
20
20
20
20
20
20
20
RPDLmt
%RecLimits
80
80
10
80
65
80
80
80
80
50
132
129
170
121
140
120
125
124
122
170
-
-
-
-
-
-
-
-
-
-
Q
Sample ID:
Sample ID:
WG615405-02
WG615405-03
LCS
LCS2
8M419872
8M419873
File ID:
File ID:
1,2-Dichloroethane-d4
Dibromofluoromethane
4-Bromofluorobenzene
Toluene-d8
LCS LCS2
95.4 97.5
100 103
104 103
106 107
Surogates% Recovery % Recovery
Surrogate Limits
80
86
86
88
120
118
115
110
-
-
-
-
Qualifier
PASS
PASS
PASS
PASS
Run Date:
Run Date:
05/24/2017 13:25
05/24/2017 13:53
WG615405
Instrument ID:HPMS8
Analyst:TMB
Workgroup (AAB#): ug/LUnits:
8260BMethod:TCLP LeachMatrix:
L17051231Login Number: 5030B/5030C/503Prep Method:
* EXCEEDS %REC LIMIT
# EXCEEDS RPD LIMIT
STDQC Key: STD82009Lot #:
Page 75
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
SURROGATES - Modified 03/06/2008
05/26/2017 14:28Report generated:5309114PDF File ID:
SURROGATE STANDARDS
Microbac Laboratories Inc.
L17051231-01
WG615405-01
WG615405-02
WG615405-03
WG615405-04
DL01
01
01
01
01
1 2 3 4Sample Number Dilution Tag
10.0
1.00
1.00
1.00
1.00
1
2
3
4
-
-
-
-
1,2-Dichloroethane-d4
Dibromofluoromethane
4-Bromofluorobenzene
Toluene-d8
8260Method:
HPMS8Instrument Id:
L17051231Login Number:
TCLP LeachMatrix:WG615405Workgroup (AAB#):
Underline = Result out of surrogate limits
96.9 101 106 107
99.6 103 107 107
95.4 100 104 106
97.5 103 103 107
96.2 100 107 108
80
86
86
88
-
-
-
-
120
118
115
110
Surrogates Surrogate Limits
DL = surrogate diluted out
HPMS8CAL ID: -17-APR-17
ND = surrogate not detected
Page 76
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
SURROGATES - Modified 03/06/2008
05/26/2017 14:28Report generated:5309114PDF File ID:
SURROGATE STANDARDS
Microbac Laboratories Inc.
L17051231-03
L17051231-05
L17051231-07
L17051231-09
L17051231-11
L17051231-13
WG615282-01
WG615282-02
WG615282-03
WG615282-04
WG615282-05
DL01
DL01
DL01
DL01
DL01
DL01
01
01
01
02
02
1 2 3 4Sample Number Dilution Tag
10.0
10.0
10.0
10.0
10.0
10.0
1.00
1.00
1.00
1.00
1.00
1
2
3
4
-
-
-
-
1,2-Dichloroethane-d4
Dibromofluoromethane
4-Bromofluorobenzene
Toluene-d8
8260Method:
HPMS11Instrument Id:
L17051231Login Number:
TCLP LeachMatrix:WG615282Workgroup (AAB#):
Underline = Result out of surrogate limits
105 103 108 110
109 106 113 113
107 103 110 111
108 102 112 111
104 101 113 108
107 101 107 108
103 99.8 112 106
105 101 106 107
107 106 106 108
106 105 113 112
104 102 114 110
80
86
86
88
-
-
-
-
120
118
115
110
Surrogates Surrogate Limits
DL = surrogate diluted out
HPMS11CAL ID: -16-MAY-17
ND = surrogate not detected
Page 77
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
SURROGATES - Modified 03/06/2008
05/26/2017 14:29Report generated:5308762PDF File ID:
SURROGATE STANDARDS
Microbac Laboratories Inc.
L17051231-02
L17051231-04
L17051231-06
L17051231-08
L17051231-10
L17051231-12
L17051231-14
WG615352-01
WG615352-02
01
01
01
01
01
01
01
01
01
1 2 3 4Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1
2
3
4
-
-
-
-
1,2-Dichloroethane-d4
Dibromofluoromethane
4-Bromofluorobenzene
Toluene-d8
8260Method:
HPMS9Instrument Id:
L17051231Login Number:
SoilMatrix:WG615352Workgroup (AAB#):
Underline = Result out of surrogate limits
99.1 100 150 115
100 102 127 113
96.0 99.2 118 108
93.4 100 117 110
96.5 99.9 135 117
97.4 98.6 122 114
92.8 97.4 111 106
101 101 108 104
103 105 109 108
80
80
74
81
-
-
-
-
120
120
121
117
Surrogates Surrogate Limits
DL = surrogate diluted out
HPMS9CAL ID: -23-MAY-17
ND = surrogate not detected
Page 78
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/26/2017 14:28Report generated5309112PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
1,2-Dichloropropane
Ethylbenzene
Toluene
Chloroform
1,1-Dichloroethene
Vinyl Chloride
1,1,2,2-Tetrachloroethane
1,1-Dichloroethane
Bromoform
Chloromethane
Chlorobenzene
Benzene
Carbon Tetrachloride
1,2-Dichloroethane
2-Butanone
Tetrachloroethene
Trichloroethene
CCC
CCC
CCC
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
SPCC
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.3
50.7
50.2
44.2
48.3
49.4
49.5
48.2
43.4
42.2
48.8
48.1
51.7
47.2
43.9
51.9
48.1
0.341
0.584
1.54
0.491
0.478
0.427
0.712
0.590
0.265
0.467
1.02
1.06
0.401
0.426
0.129
0.328
0.281
0.611
1.40
0.480
11.7
3.46
1.17
0.938
3.68
13.3
15.6
2.34
3.78
3.46
5.66
12.2
3.84
3.72
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
11M18564
WG615282
Instrument ID:HPMS11
File ID:
Run Date:05/23/2017
Run Time:12:27
Analyst:TMB
Workgroup (AAB#):
8260BMethod:
L17051231Login Number: WG615277-02Sample ID:
16-MAY-17HPMS11 -Cal ID:
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UCL20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
STDQC Key:
WATERMatrix:
Page 79
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/26/2017 14:28Report generated5309112PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
Analyte Expected Found Q* Exceeds
%D Criteria %D
RF
11M18566
WG615282
Instrument ID:HPMS11
File ID:
Run Date:05/23/2017
Run Time:13:08
Analyst:TMB/JDS
Workgroup (AAB#):
8260BMethod:
L17051231Login Number: WG615279-01Sample ID:
03-MAY-17HPMS11 -Cal ID:
UNITS UCL
STDQC Key:
WATERMatrix:
Page 80
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/26/2017 14:28Report generated5309112PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
1,2-Dichloropropane
Ethylbenzene
Toluene
Chloroform
1,1-Dichloroethene
Vinyl Chloride
1,1,2,2-Tetrachloroethane
1,1-Dichloroethane
Bromoform
Chloromethane
Chlorobenzene
Benzene
Carbon Tetrachloride
1,2-Dichloroethane
2-Butanone
Tetrachloroethene
Trichloroethene
CCC
CCC
CCC
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
SPCC
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
53.4
55.2
55.5
49.9
57.2
59.8
45.7
56.1
43.6
60.1
52.2
55.3
59.1
50.8
42.3
56.0
54.8
0.269
0.613
1.54
0.501
0.414
0.478
0.432
0.509
0.177
0.509
1.04
1.14
0.445
0.288
0.0467
0.327
0.318
*
6.72
10.5
10.9
0.218
14.5
19.7
8.51
12.2
12.9
20.2
4.49
10.6
18.3
1.53
15.3
12.0
9.51
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
8M419869
WG615405
Instrument ID:HPMS8
File ID:
Run Date:05/24/2017
Run Time:11:59
Analyst:TMB
Workgroup (AAB#):
8260BMethod:
L17051231Login Number: WG615404-02Sample ID:
17-APR-17HPMS8 -Cal ID:
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UCL20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
STDQC Key:
WATERMatrix:
Page 81
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/26/2017 14:29Report generated5312953PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
Page 82
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Calibration Table Report
Method: A9FOOWTR.M
Title: Appendix IX (SOP:OVL MSV01) Water 050317 HPMS11
Last Calibration: Thu May 04 07:07:15 2017
Curve: WG612759
Calibration Files
5 20 50 100 200 300 400 500
11M18002.D 11M18003.D 11M18004.D 11M18005.D 11M18006.D 11M18007.D 11M18008.D 11M18009.D
Compound Avg %RSD Linear Quadratic
I Fluorobenzene ISTD
T Acetonitrile 0.028 0.032 0.033 0.032 0.034 0.033 0.034 0.035 0.033 6.933
T 3-Chloro-1-propene 0.480 0.493 0.499 0.481 0.462 0.420 0.394 0.364 0.449 11.191
T 2-Chloro-1,3-butadiene 0.439 0.462 0.480 0.471 0.458 0.418 0.395 0.364 0.436 9.323
T Methacrylonitrile 0.149 0.176 0.191 0.188 0.193 0.186 0.185 0.178 0.181 7.820
T Isobutyl Alcohol 0.009 0.012 0.011 0.012 0.013 0.014 0.014 0.012 13.767
T 1-Butanol 0.005 0.006 0.006 0.007 0.007 0.006 11.655
T Cyclohexanone 0.008 0.008 0.010 0.010 0.011 0.011 0.010 12.441
T 2-Nitropropane 0.066 0.071 0.076 0.078 0.081 0.080 0.075 7.608
T Ethyl Acetate 0.229 0.253 0.260 0.255 0.254 0.241 0.233 0.221 0.243 5.885
T Methyl methacrylate 0.186 0.234 0.248 0.249 0.251 0.240 0.233 0.220 0.233 9.226
I Chlorobenzene-d5 ISTD
I 1,4-Dichlorobenzene-d4 ISTD
Mon May 08 16:08:06 2017
Page 83
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Calibration Table Report
Method: 8260WT.M
Title: 8260B/624 (SOP: OVL MSV01) Water 051617 HPMS11
Last Calibration: Wed May 17 12:46:08 2017
Curve: WG614378
Calibration Files
0.3 0.4 1 2 5 20 50 100 200 30011M18431.D 11M18432.D 11M18433.D 11M18434.D 11M18435.D 11M18436.D 11M18437.D 11M18438.D 11M18439.D 11M18440.D
Compound Avg %RSD Linear Quadratic
Fluorobenzene ISTD
Dichlorodifluoromethane 0.317 0.353 0.357 0.424 0.407 0.378 0.368 0.372 9.541
Chloromethane 0.560 0.639 0.584 0.630 0.536 0.486 0.439 0.553 13.227
Vinyl Chloride 0.498 0.417 0.470 0.439 0.478 0.442 0.375 0.336 0.432 12.564
1,3-Butadiene 0.343 0.282 0.295 0.228 0.162 0.153 0.130 0.227 36.032 1.002
Bromomethane 0.207 0.210 0.206 0.193 0.198 0.204 0.219 0.205 4.082
Chloroethane 0.219 0.239 0.241 0.249 0.245 0.237 0.248 0.240 4.259
Trichlorofluoromethane 0.441 0.417 0.471 0.462 0.480 0.472 0.439 0.448 0.454 4.729
Diethyl ether 0.273 0.297 0.290 0.286 0.284 0.278 0.284 0.285 2.761
Isoprene 0.305 0.365 0.389 0.401 0.441 0.443 0.441 0.439 0.403 12.220
Acrolein 0.029 0.040 0.038 0.039 0.040 0.042 0.042 0.039 11.129
1,1,2-Trichloro-1,2,2-Trifluoroethane 0.195 0.234 0.242 0.249 0.253 0.241 0.255 0.239 8.688
Acetone 0.089 0.093 0.091 0.092 0.093 0.097 0.090 0.092 2.806
1,1-Dichloroethene 0.473 0.457 0.486 0.517 0.521 0.518 0.495 0.494 0.495 4.648
Tert-Butyl Alcohol 0.023 0.027 0.027 0.028 0.031 0.032 0.028 11.816
Dimethyl Sulfide 0.287 0.297 0.340 0.336 0.357 0.356 0.352 0.351 0.334 8.216
Iodomethane 0.013 0.079 0.141 0.251 0.276 0.290 0.298 0.192 59.519 0.998
Methyl acetate 0.215 0.241 0.249 0.254 0.256 0.266 0.247 7.124
Methylene Chloride 0.335 0.334 0.310 0.314 0.305 0.293 0.302 0.313 5.038
Carbon Disulfide 0.710 0.770 0.789 0.834 0.806 0.757 0.688 0.765 6.757
Acrylonitrile 0.094 0.114 0.118 0.119 0.129 0.131 0.126 0.119 10.729
Methyl Tert Butyl Ether 0.745 0.695 0.766 0.793 0.821 0.803 0.773 0.768 0.771 5.035
trans-1,2-Dichloroethene 0.246 0.236 0.270 0.276 0.288 0.287 0.276 0.287 0.271 7.185
n-Hexane 0.407 0.430 0.467 0.476 0.471 0.467 0.453 6.165
Diisopropyl ether 1.117 1.264 1.233 1.203 1.164 1.017 0.915 1.130 11.071
Vinyl Acetate 0.479 0.533 0.487 0.517 0.535 0.472 0.424 0.492 8.019
1,1-Dichloroethane 0.640 0.593 0.611 0.604 0.645 0.631 0.596 0.577 0.612 3.958
Ethyl-Tert-Butyl ether 0.964 1.097 1.071 1.046 1.027 0.914 0.834 0.993 9.488
2-Butanone 0.137 0.139 0.143 0.147 0.152 0.157 0.155 0.147 5.313
Propionitrile 0.034 0.041 0.043 0.044 0.045 0.047 0.050 0.043 11.768
2,2-Dichloropropane 0.423 0.369 0.405 0.392 0.420 0.417 0.395 0.398 0.402 4.470
cis-1,2-Dichloroethene 0.316 0.262 0.294 0.319 0.332 0.328 0.315 0.320 0.311 7.292
Chloroform 0.668 0.681 0.536 0.542 0.526 0.550 0.525 0.494 0.481 0.556 12.730
1-Bromopropane 0.040 0.054 0.061 0.060 0.058 0.061 0.059 0.056 13.246
Bromochloromethane 0.129 0.172 0.187 0.196 0.199 0.196 0.192 0.198 0.184 12.931
Tetrahydrofuran 0.158 0.115 0.106 0.104 0.106 0.106 0.108 0.115 16.890 0.999
Dibromofluoromethane 0.280 0.262 0.272 0.271 0.260 0.269 3.091
1,1,1-Trichloroethane 0.415 0.399 0.423 0.462 0.483 0.485 0.463 0.464 0.449 7.243
Cyclohexane 0.581 0.524 0.578 0.607 0.650 0.644 0.623 0.599 0.540 0.594 7.282
1,1-Dichloropropene 0.331 0.335 0.357 0.372 0.408 0.407 0.386 0.387 0.373 7.978
Carbon Tetrachloride 0.304 0.349 0.379 0.396 0.420 0.430 0.409 0.410 0.387 10.874
Tert-Amyl-Methyl ether 0.714 0.837 0.823 0.816 0.803 0.73 0.677 0.77142 8.15202
1,2-Dichloroethane-d4 0.363 0.317 0.338 0.335 0.317 0.33379 5.69157
1,2-Dichloroethane 0.442 0.419 0.47 0.476 0.478 0.468 0.436 0.423 0.45135 5.33453
Benzene 1.156 1.084 1.179 1.185 1.199 1.141 1.011 0.878 1.104 10.0158
Trichloroethene 0.226 0.251 0.301 0.301 0.325 0.317 0.301 0.309 0.29146 11.7841
Methylcyclohexane 0.477 0.383 0.443 0.467 0.507 0.501 0.477 0.464 0.423 0.46019 8.49006
1,2-Dichloropropane 0.313 0.286 0.342 0.342 0.369 0.363 0.345 0.352 0.33917 8.04796
1,4-Dioxane 0.002 0.003 0.003 0.003 0.003 0.003 0.00293 13.9596
Bromodichloromethane 0.343 0.298 0.345 0.37 0.408 0.403 0.393 0.389 0.36867 10.1709
Dibromomethane 0.12 0.153 0.171 0.163 0.188 0.182 0.176 0.183 0.16712 13.2633
2-Chloroethyl Vinyl Ether 0.14 0.162 0.18 0.202 0.21 0.215 0.22 0.208 0.19218 14.9182
4-Methyl-2-Pentanone 0.099 0.116 0.122 0.127 0.138 0.133 0.12257 11.2898
cis-1,3-Dichloropropene 0.334 0.303 0.37 0.402 0.455 0.472 0.45 0.443 0.40378 15.4416 0.999
Dimethyl Disulfide 0.147 0.173 0.237 0.271 0.28 0.288 0.269 0.23782 23.5484 0.999
Chlorobenzene-d5 ISTD
Toluene-d8 1.507 1.348 1.404 1.335 1.146 1.34813 9.77146
Toluene 2.389 1.827 1.753 1.819 1.767 1.658 1.41 1.80307 16.3818 0.991
Ethyl Methacrylate 0.303 0.369 0.419 0.482 0.512 0.503 0.484 0.461 0.44178 16.5839 0.998
trans-1,3-Dichloropropene 0.496 0.468 0.517 0.577 0.593 0.574 0.53 0.53644 8.70041
1,1,2-Trichloroethane 0.319 0.306 0.337 0.349 0.367 0.361 0.35 0.342 0.34131 5.95867
2-Hexanone 0.257 0.302 0.314 0.319 0.323 0.318 0.30532 8.13831
1,3-Dichloropropane 0.632 0.563 0.598 0.616 0.627 0.611 0.573 0.539 0.59471 5.61804
Tetrachloroethene 0.237 0.276 0.301 0.34 0.35 0.354 0.336 0.331 0.31574 13.0405
Dibromochloromethane 0.302 0.303 0.328 0.364 0.422 0.438 0.419 0.416 0.37379 15.2048 0.999
1,2-Dibromoethane 0.218 0.277 0.297 0.323 0.336 0.338 0.324 0.324 0.30457 13.3219
1-Chlorohexane 0.435 0.368 0.42 0.471 0.528 0.54 0.528 0.493 0.454 0.47077 12.2378
Chlorobenzene 1.06 1.029 1.093 1.095 1.14 1.091 0.982 0.852 1.04267 8.68375
1,1,1,2-Tetrachloroethane 0.333 0.343 0.376 0.375 0.422 0.428 0.418 0.412 0.38822 9.55907
Ethylbenzene 0.49 0.553 0.573 0.617 0.631 0.597 0.568 0.5756 8.15775
m-,p-Xylene 0.624 0.61 0.662 0.73 0.738 0.723 0.635 0.52 0.6552 11.3677
o-Xylene 0.611 0.542 0.601 0.714 0.734 0.742 0.699 0.654 0.66201 10.9201
Styrene 0.915 0.841 0.944 1.039 1.186 1.213 1.116 0.962 1.02697 13.0703
Bromoform 0.169 0.221 0.229 0.278 0.299 0.304 0.316 0.25955 20.9192 0.999
Isopropylbenzene 1.54 1.47 1.654 1.773 1.858 1.79 1.534 1.228 1.60558 12.8593
1,4-Dichlorobenzene-d4 ISTD
1,1,2,2-Tetrachloroethane 0.602 0.603 0.738 0.784 0.799 0.755 0.759 0.712 0.71899 10.6759
p-Bromofluorobenzene 0.94 0.932 0.941 0.959 0.874 0.92914 3.499
1,2,3-Trichloropropane 0.192 0.203 0.227 0.25 0.237 0.238 0.241 0.22684 9.47455
trans-1,4-Dichloro-2-Butene 0.145 0.197 0.252 0.276 0.273 0.283 0.283 0.259 0.24598 20.0146 0.998
R^2
Page 84
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
n-Propylbenzene 3.443 3.25 3.731 4.084 4.255 3.72 3.078 3.6516 11.7041
Bromobenzene 0.765 0.798 0.769 0.857 0.913 0.978 0.915 0.884 0.825 0.85586 8.52037
1,3,5-Trimethylbenzene 2.528 2.343 2.64 2.841 3.025 2.723 2.375 1.866 2.54273 14.0286
2-Chlorotoluene 2.677 2.489 2.82 2.937 3.017 2.639 2.322 1.813 2.58925 14.9669
4-Chlorotoluene 1.945 1.885 2.066 2.17 2.308 2.123 1.844 1.421 1.97015 13.7289
a-Methylstyrene 1.273 1.545 1.523 1.47 1.247 1.119 1.36309 12.7744
tert-Butylbenzene 0.452 0.537 0.622 0.676 0.646 0.63 0.606 0.59568 12.8233
1,2,4-Trimethylbenzene 2.375 2.721 2.996 3.128 2.834 2.449 2.75056 10.8088
sec-Butylbenzene 2.835 3.307 3.628 3.804 3.444 2.938 3.32593 11.4512
p-Isopropyltoluene 2.257 2.755 2.988 3.212 2.941 2.558 2.7853 12.2258
1,3-Dichlorobenzene 1.381 1.452 1.581 1.675 1.801 1.669 1.574 1.332 1.5582 10.2657
1,4-Dichlorobenzene 1.654 1.501 1.619 1.747 1.774 1.655 1.555 1.316 1.60264 9.16319
n-Butylbenzene 2.011 2.347 2.567 2.939 2.747 2.426 2.50625 12.9532
1,2-Dichlorobenzene 1.749 1.667 1.454 1.685 1.649 1.757 1.617 1.532 1.299 1.60101 9.3155
1,2-Dibromo-3-Chloropropane 0.092 0.133 0.151 0.154 0.157 0.168 0.14243 19.0803 0.999
1,2,4-Trichlorobenzene 0.9 0.961 1.064 1.102 1.251 1.175 1.143 1.07 1.08325 10.4409
Hexachlorobutadiene 0.336 0.503 0.513 0.584 0.642 0.617 0.623 0.616 0.55426 18.444 1
Naphthalene 2.035 1.958 2.204 2.525 2.772 2.535 2.227 1.831 2.26105 14.3669
1,2,3-Trichlorobenzene 0.922 0.878 0.94 1.027 1.136 1.237 1.159 1.103 1.065 1.05185 11.4386
Thu May 18 10:46:55 2017
Page 85
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Calibration Table Report
Method: A9FOOWT.M
Title: A9-FOO Water SOP:MSV01 04-12-17 HPMS8
Last Calibration: Thu Apr 13 16:40:13 2017
Curve: WG609829
Calibration Files
5 20 50 100 200 300 400 5008M418916.D 8M418917.D 8M418918.D 8M418919.D 8M418920.D 8M418921.D 8M418922.D 8M418923.D
Compound Avg %RSD
I Fluorobenzene ISTDT Acetonitrile 0.013 0.012 0.013 0.013 0.012 0.013 0.013 0.013 3.572T 3-Chloro-1-propene 0.312 0.315 0.327 0.337 0.346 0.341 0.344 0.341 0.333 3.984T 2-Chloro-1,3-butadiene 0.285 0.299 0.317 0.330 0.340 0.336 0.337 0.336 0.322 6.267T Ethyl Acetate 0.099 0.101 0.098 0.101 0.108 0.103 0.106 0.109 0.103 4.045T Methacrylonitrile 0.052 0.059 0.057 0.059 0.064 0.061 0.063 0.065 0.060 7.025T Isobutyl Alcohol 0.003 0.004 0.004 0.004 0.005 0.005 0.004 12.096T 1-Butanol 0.000 0.000T Methyl methacrylate 0.096 0.101 0.103 0.107 0.116 0.112 0.116 0.121 0.109 7.922T 2-Nitropropane 0.027 0.028 0.031 0.034 0.034 0.035 0.037 0.032 11.358I Chlorobenzene-d5 ISTDI 1,4-Dichlorobenzene-d4 ISTDT Cyclohexanone 0.006 0.006 0.007 0.008 0.007 0.008 0.009 0.007 13.841
Mon Apr 17 15:45:45 2017
Page 86
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Calibration Table ReportMethod: 8260WT.MTitle: Method 8260B/624 WTR-SOP:OVLMSV01 04-17-17 HPMS8Last Calibration: Tue Apr 18 08:45:38 2017Curve: WG610410Calibration Files
0.3 0.4 1 2 5 20 50 100 200 3008M419002.D 8M419003.D 8M419004.D 8M419005.D 8M419006.D 8M419007.D 8M419008.D 8M419009.D 8M419010.D 8M419011.D
Compound Avg %RSD Linear Quad
I Fluorobenzene ISTDT Dichlorodifluoromethane 0.313 0.289 0.277 0.384 0.370 0.362 0.373 0.338 13.019P Chloromethane 0.456 0.440 0.417 0.437 0.403 0.401 0.407 0.423 5.087C Vinyl Chloride 0.426 0.430 0.414 0.394 0.429 0.389 0.367 0.347 0.399 7.750T 1,3-Butadiene 0.273 0.246 0.164 0.130 0.118 0.112 0.174 39.828 1.000
T Bromomethane 0.064 0.068 0.074 0.124 0.149 0.181 0.110 44.154 1.001
T Chloroethane 0.162 0.163 0.173 0.171 0.183 0.177 0.180 0.186 0.174 5.074T Trichlorofluoromethane 0.393 0.462 0.411 0.420 0.452 0.436 0.437 0.459 0.434 5.614T Diethyl ether 0.159 0.160 0.163 0.158 0.160 0.167 0.176 0.163 3.861T Isoprene 0.316 0.325 0.346 0.353 0.353 0.366 0.343 5.533T Acrolein 0.022 0.023 0.021 0.022 0.024 0.024 0.023 4.706T 1,1,2-Trichloro-1,2,2-Trifluoroethane 0.251 0.228 0.237 0.253 0.250 0.252 0.261 0.247 4.440T Acetone 0.036 0.033 0.036 0.037 0.034 0.035 0.035 4.082C 1,1-Dichloroethene 0.331 0.366 0.344 0.349 0.377 0.371 0.376 0.383 0.362 5.154T Tert-Butyl Alcohol 0.010 0.012 0.011 0.011 0.011 0.013 0.011 10.980T Dimethyl Sulfide 0.232 0.226 0.240 0.246 0.249 0.255 0.241 4.476T Iodomethane 0.026 0.067 0.121 0.154 0.164 0.116 0.108 48.714 NO CALT Methyl acetate 0.099 0.091 0.097 0.098 0.093 0.100 0.096 3.655T Methylene Chloride 0.271 0.245 0.249 0.263 0.258 0.264 0.272 0.260 3.943T Carbon Disulfide 0.794 0.744 0.746 0.729 0.763 0.767 0.766 0.713 0.753 3.339T Acrylonitrile 0.043 0.045 0.049 0.049 0.053 0.054 0.049 0.049 8.214T Methyl Tert Butyl Ether 0.495 0.474 0.502 0.530 0.528 0.543 0.517 0.513 4.642T trans-1,2-Dichloroethene 0.342 0.345 0.349 0.334 0.360 0.353 0.363 0.373 0.352 3.537T n-Hexane 0.301 0.278 0.290 0.295 0.300 0.301 0.294 2.997T Diisopropyl ether 0.776 0.794 0.805 0.792 0.783 0.801 0.768 0.788 1.708T Vinyl Acetate 0.353 0.350 0.359 0.366 0.348 0.345 0.354 2.233P 1,1-Dichloroethane 0.405 0.460 0.437 0.441 0.474 0.462 0.473 0.476 0.453 5.418T Ethyl-Tert-Butyl ether 0.651 0.652 0.684 0.667 0.669 0.693 0.679 0.671 2.398T 2-Butanone 0.053 0.052 0.056 0.058 0.053 0.059 0.055 5.073T Propionitrile 0.015 0.016 0.018 0.017 0.017 0.018 0.019 0.017 7.523T 2,2-Dichloropropane 0.336 0.387 0.384 0.373 0.399 0.387 0.396 0.399 0.383 5.430T cis-1,2-Dichloroethene 0.263 0.287 0.282 0.286 0.300 0.296 0.305 0.311 0.291 5.182C Chloroform 0.619 0.539 0.514 0.499 0.459 0.479 0.467 0.473 0.471 0.502 10.092T 1-Bromopropane 0.057 0.053 0.055 0.056 0.057 0.059 0.061 0.061 0.057 5.096T Bromochloromethane 0.118 0.150 0.156 0.160 0.167 0.167 0.170 0.168 0.157 11.011T Tetrahydrofuran 0.039 0.035 0.038 0.036 0.038 0.040 0.039 0.038 4.497S Dibromofluoromethane 0.251 0.244 0.261 0.272 0.265 0.269 0.273 0.262 4.105T 1,1,1-Trichloroethane 0.337 0.406 0.380 0.394 0.426 0.420 0.431 0.450 0.405 8.684T Cyclohexane 0.371 0.358 0.372 0.358 0.379 0.389 0.403 0.391 0.377 4.255T 1,1-Dichloropropene 0.354 0.340 0.337 0.363 0.353 0.359 0.371 0.354 3.449T Tert-Amyl-Methyl ether 0.568 0.579 0.618 0.598 0.602 0.629 0.609 0.600 3.552T Carbon Tetrachloride 0.288 0.38 0.359 0.363 0.404 0.394 0.41 0.411 0.3759 10.8547S 1,2-Dichloroethane-d4 0.215 0.219 0.227 0.237 0.23 0.224 0.235 0.2267 3.56551T Heptane 0 0T 1,2-Dichloroethane 0.247 0.28 0.273 0.279 0.298 0.293 0.305 0.299 0.284 6.56007T Benzene 1.013 1.058 1.034 1.013 1.082 1.044 1.045 0.975 1.0328 3.16185T Trichloroethene 0.28 0.291 0.275 0.274 0.294 0.29 0.302 0.315 0.2901 4.79714T Methylcyclohexane 0.371 0.369 0.386 0.392 0.4 0.402 0.3867 3.65443C 1,2-Dichloropropane 0.235 0.244 0.249 0.243 0.257 0.256 0.264 0.269 0.2522 4.51345T Bromodichloromethane 0.273 0.313 0.319 0.319 0.35 0.347 0.359 0.361 0.3301 9.09766T 1,4-Dioxane 0.001 0.001 0.002 0.002 0.002 0.0014 8.93532T Dibromomethane 0.101 0.125 0.129 0.129 0.138 0.136 0.14 0.14 0.1298 9.96462T 2-Chloroethyl Vinyl Ether 0.091 0.101 0.106 0.114 0.116 0.114 0.122 0.1091 9.65313T 4-Methyl-2-Pentanone 0.042 0.045 0.05 0.051 0.049 0.055 0.0489 9.48763T cis-1,3-Dichloropropene 0.303 0.354 0.349 0.364 0.401 0.404 0.417 0.416 0.3759 10.7244
Page 87
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
T Dimethyl Disulfide 0.133 0.169 0.201 0.215 0.226 0.237 0.1968 19.8258 0.998
I Chlorobenzene-d5 ISTDS Toluene-d8 1.126 1.107 1.183 1.185 1.136 1.123 1.136 1.1423 2.63592C Toluene 1.276 1.435 1.421 1.416 1.507 1.432 1.412 1.234 1.3916 6.46773T Ethyl Methacrylate 0.208 0.222 0.252 0.262 0.287 0.29 0.277 0.303 0.2625 12.7656T Paraldehyde 0 0T trans-1,3-Dichloropropene 0.367 0.363 0.389 0.421 0.422 0.44 0.423 0.4036 7.59969T 1,1,2-Trichloroethane 0.21 0.235 0.224 0.228 0.239 0.229 0.237 0.23 0.2289 4.06629T 2-Hexanone 0.048 0.053 0.058 0.06 0.054 0.063 0.0562 9.63322T 1,3-Dichloropropane 0.353 0.405 0.372 0.373 0.41 0.397 0.403 0.383 0.387 5.15702T Tetrachloroethene 0.245 0.284 0.279 0.285 0.31 0.295 0.312 0.328 0.2923 8.65757T Dibromochloromethane 0.232 0.267 0.271 0.289 0.315 0.318 0.333 0.328 0.2942 12.052T 1,2-Dibromoethane 0.188 0.209 0.218 0.222 0.242 0.236 0.241 0.233 0.2236 8.21869T 1-Chlorohexane 0.385 0.44 0.423 0.428 0.44 0.451 0.457 0.466 0.472 0.4403 5.99946P Chlorobenzene 1.008 0.965 0.972 0.936 1.008 0.988 1.042 1.006 0.9906 3.29062T 1,1,1,2-Tetrachloroethane 0.303 0.316 0.32 0.335 0.379 0.385 0.423 0.3515 12.6454C Ethylbenzene 0.467 0.5 0.532 0.513 0.574 0.568 0.62 0.665 0.5548 11.7603T m-,p-Xylene 0.572 0.637 0.62 0.627 0.689 0.677 0.694 0.623 0.6425 6.46237T o-Xylene 0.611 0.592 0.623 0.665 0.648 0.68 0.703 0.6459 6.13337T Styrene 0.814 0.93 0.929 0.995 1.114 1.111 1.142 1.067 1.0127 11.3997P Bromoform 0.125 0.142 0.163 0.191 0.196 0.207 0.207 0.176 18.66 0.999
T Isopropylbenzene 1.463 1.551 1.54 1.592 1.678 1.613 1.576 1.361 1.5466 6.28276I 1,4-Dichlorobenzene-d4 ISTDP 1,1,2,2-Tetrachloroethane 0.385 0.493 0.455 0.465 0.508 0.494 0.502 0.472 0.4717 8.42371S p-Bromofluorobenzene 0.897 0.839 0.876 0.891 0.86 0.878 0.935 0.8823 3.42248T 1,2,3-Trichloropropane 0.117 0.127 0.131 0.143 0.144 0.146 0.138 0.1352 7.82469T trans-1,4-Dichloro-2-Butene 0.058 0.065 0.085 0.109 0.122 0.115 0.114 0.116 0.0978 25.7933 1.000
T n-Propylbenzene 3.478 3.723 3.692 3.608 3.807 3.577 3.383 2.726 3.4991 9.72861T Bromobenzene 0.752 0.696 0.839 0.81 0.813 0.857 0.845 0.872 0.896 0.8199 7.58093T 1,3,5-Trimethylbenzene 2.467 2.514 2.525 2.506 2.737 2.623 2.589 2.306 2.5336 4.94471T 2-Chlorotoluene 2.674 2.623 2.305 2.553 2.347 2.198 2.2 2.21 2.3888 8.30021T 4-Chlorotoluene 1.995 2.135 2.439 1.867 2.369 2.326 2.308 1.784 2.1528 11.4607T a-Methylstyrene 1.296 1.355 1.455 1.517 1.498 1.401 1.4204 6.02416T tert-Butylbenzene 0.52 0.555 0.528 0.588 0.571 0.601 0.653 0.5736 7.96677T 1,2,4-Trimethylbenzene 2.284 2.607 2.62 2.578 2.817 2.742 2.701 2.343 2.5866 7.19751T sec-Butylbenzene 3.278 3.292 3.183 3.429 3.252 3.145 2.633 3.1733 8.03336T p-Isopropyltoluene 2.64 2.605 2.626 2.913 2.796 2.737 2.387 2.6721 6.23483T 1,3-Dichlorobenzene 1.502 1.596 1.568 1.535 1.665 1.625 1.642 1.581 1.5891 3.4371T 1,4-Dichlorobenzene 1.772 1.622 1.643 1.594 1.517 1.637 1.592 1.618 1.545 1.6156 4.45875T n-Butylbenzene 2.426 2.337 2.245 2.632 2.542 2.483 2.184 2.407 6.69686T 1,2-Dichlorobenzene 1.368 1.185 1.488 1.397 1.379 1.46 1.438 1.454 1.396 1.396 6.36818T 1,2-Dibromo-3-Chloropropane 0.073 0.072 0.076 0.079 0.083 0.077 0.0768 5.09915T 1,2,4-Trichlorobenzene 0.864 0.92 0.882 0.852 0.952 0.983 1.022 1.044 0.9399 7.72424T Hexachlorobutadiene 0.405 0.427 0.426 0.402 0.449 0.44 0.456 0.493 0.4374 6.74711T Naphthalene 1.353 1.273 1.232 1.251 1.396 1.436 1.465 1.339 1.3431 6.41915T 1,2,3-Trichlorobenzene 0.796 0.766 0.75 0.705 0.691 0.802 0.821 0.847 0.847 0.7805 7.29917
Tue Apr 18 12:15:24 2017
Page 88
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Calibration Table Report
Method: A9FOOSL.M
Title: FOO/APPIX SOIL 02/20/2017 SOP: OVL MSV01
Last Calibration: Tue Feb 21 15:27:36 2017
Curve: WG603526
Calibration Files
5 20 50 100 200 300 400 500 R^29M978918.D 9M978919.D 9M978920.D 9M978921.D 9M978922.D 9M978923.D 9M978924.D 9M978925.D
Compound Avg %RSD Linear
Fluorobenzene ISTD
Acetonitrile 0.045 0.047 0.047 0.049 0.046 0.049 0.046 0.047 3.144
3-Chloro-1-propene 0.438 0.493 0.514 0.528 0.521 0.484 0.489 0.467 0.492 6.091
2-Chloro-1,3-butadiene 0.383 0.447 0.470 0.490 0.481 0.448 0.457 0.435 0.451 7.360
Ethyl Acetate 0.305 0.314 0.329 0.323 0.306 0.316 0.305 0.314 3.020
Methacrylonitrile 0.103 0.111 0.116 0.121 0.122 0.117 0.122 0.117 0.116 5.609
Isobutyl Alcohol 0.019 0.019 0.017 0.020 0.021 0.020 0.022 0.023 0.020 8.963
1-Butanol 0.006 0.009 0.010 0.010 0.012 0.012 0.010 22.774 0.992
Methyl methacrylate 0.228 0.257 0.284 0.299 0.296 0.281 0.286 0.275 0.276 8.390
2-Nitropropane 0.057 0.060 0.077 0.086 0.089 0.087 0.094 0.092 0.080 17.823 0.998
Chlorobenzene-d5 ISTD
Cyclohexanone 0.018 0.022 0.025 0.028 0.026 0.029 0.027 0.025 15.974 0.997
1,4-Dichlorobenzene-d4 ISTD
Tue Feb 21 15:37:39 2017
Page 89
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Calibration Table Report
Method: 8260SL.M
Title: 8260(B) SOP: OVL MSV01 SOIL 05/23/17 HPMS9
Last Calibration: Tue May 23 15:17:14 2017
Curve: WG615237
Calibration Files
0.5 1 2 5 20 50 100 200 3009M980432.D 9M980433.D 9M980434.D 9M980435.D 9M980436.D 9M980437.D 9M980438.D 9M980439.D 9M980440.D
Compound Avg %RSD Linear Quadratic
Fluorobenzene ISTD
Dichlorodifluoromethane 0.246 0.284 0.295 0.259 0.274 0.313 0.273 0.278 8.030
Chloromethane 0.378 0.340 0.282 0.300 0.359 0.338 0.333 10.813
Vinyl Chloride 0.184 0.241 0.260 0.207 0.215 0.228 0.201 0.219 11.773
1,3-Butadiene 0.145 0.162 0.144 0.114 0.113 0.102 0.107 0.127 18.242 0.996
Bromomethane 0.232 0.222 0.174 0.165 0.178 0.154 0.188 16.940 0.995
Chloroethane 0.185 0.193 0.175 0.169 0.199 0.170 0.182 6.849
Trichlorofluoromethane 0.335 0.409 0.412 0.383 0.388 0.445 0.404 0.397 8.572
Diethyl ether 0.294 0.286 0.249 0.243 0.296 0.291 0.277 8.617
Isoprene 0.338 0.363 0.334 0.344 0.391 0.360 0.355 5.983
Acrolein 0.049 0.059 0.059 0.053 0.057 0.065 0.067 0.058 11.013
1,1,2-Trichloro-1,2,2-Trifluoroethane 0.226 0.240 0.220 0.222 0.256 0.232 0.233 5.829
Acetone 0.222 0.159 0.143 0.150 0.133 0.140 0.158 20.777 0.998
1,1-Dichloroethene 0.349 0.408 0.425 0.400 0.410 0.465 0.424 0.412 8.467
Tert-Butyl Alcohol 0.058 0.054 0.051 0.050 0.067 0.056 12.119
Dimethyl Sulfide 0.217 0.268 0.292 0.265 0.274 0.320 0.284 0.274 11.429
Iodomethane 0.119 0.127 0.174 0.242 0.231 0.265 0.193 32.107 0.998
Methyl acetate 0.316 0.368 0.364 0.328 0.328 0.361 0.331 0.342 6.193
Methylene Chloride 0.299 0.280 0.244 0.246 0.286 0.253 0.268 8.765
Carbon Disulfide 0.818 0.746 0.770 0.702 0.719 0.831 0.734 0.760 6.453
Acrylonitrile 0.128 0.153 0.154 0.138 0.147 0.168 0.184 0.153 12.173
Methyl Tert Butyl Ether 0.597 0.772 0.788 0.711 0.725 0.839 0.743 0.739 10.283
trans-1,2-Dichloroethene 0.326 0.410 0.414 0.385 0.393 0.448 0.404 0.397 9.398
n-Hexane 0.429 0.487 0.464 0.460 0.527 0.478 0.474 6.906
Diisopropyl ether 1.261 1.248 1.050 1.028 1.240 1.196 1.170 8.911
Vinyl Acetate 0.439 0.514 0.599 0.692 0.630 0.675 0.592 16.497 0.998
1,1-Dichloroethane 0.443 0.517 0.523 0.477 0.481 0.552 0.491 0.498 7.221
Ethyl-Tert-Butyl ether 1.052 1.028 0.886 0.866 1.051 1.034 0.986 8.735
2-Butanone 0.175 0.185 0.185 0.219 0.198 0.223 0.197 10.014
Propionitrile 0.051 0.059 0.057 0.056 0.070 0.074 0.061 14.877
2,2-Dichloropropane 0.300 0.356 0.366 0.344 0.351 0.411 0.375 0.357 9.436
cis-1,2-Dichloroethene 0.203 0.265 0.282 0.253 0.258 0.306 0.273 0.263 12.141
Chloroform 0.380 0.445 0.465 0.413 0.419 0.486 0.430 0.434 8.101
1-Bromopropane 0.039 0.047 0.045 0.046 0.055 0.050 0.054 0.048 11.120
Bromochloromethane 0.133 0.160 0.171 0.163 0.168 0.190 0.174 0.165 10.435
Tetrahydrofuran 0.164 0.151 0.137 0.136 0.147 0.157 0.149 7.460
Dibromofluoromethane 0.254 0.233 0.272 0.276 0.265 0.260 6.617
1,1,1-Trichloroethane 0.280 0.354 0.393 0.365 0.373 0.434 0.392 0.370 12.824
Cyclohexane 0.414 0.527 0.573 0.506 0.524 0.599 0.538 0.526 11.115
1,1-Dichloropropene 0.313 0.334 0.307 0.321 0.364 0.330 0.328 6.203
Tert-Amyl-Methyl ether 0.820 0.791 0.683 0.671 0.821 0.813 0.766 9.180
Carbon Tetrachloride 0.29289 0.31699 0.31213 0.33031 0.38971 0.3567 0.33312 10.4727
1,2-Dichloroethane-d4 0.31654 0.30847 0.34609 0.3364 0.32331 0.32616 4.63933
Heptane 0 0
1,2-Dichloroethane 0.33803 0.39852 0.40195 0.37996 0.38536 0.43986 0.39241 0.39087 7.76385
Benzene 0.80698 1.02836 1.02298 0.90895 0.92283 1.05233 0.90638 0.94983 9.29021
Trichloroethene 0.2249 0.28315 0.26996 0.2542 0.25942 0.29412 0.26134 0.26387 8.4207
Methylcyclohexane 0.43492 0.43679 0.42091 0.42381 0.48719 0.43852 0.44036 5.46016
1,2-Dichloropropane 0.22658 0.28187 0.2923 0.265 0.27568 0.32378 0.28712 0.27891 10.5668
1,4-Dioxane 0.00375 0.00403 0.00433 0.00452 0.00613 0.00633 0.00485 22.7665 0.998
Bromodichloromethane 0.28256 0.30468 0.30429 0.32033 0.38465 0.34655 0.32384 11.286
Dibromomethane 0.12277 0.1591 0.17751 0.16793 0.17202 0.2019 0.18104 0.1689 14.3914
2-Chloroethyl Vinyl Ether 0.13982 0.15845 0.17486 0.20617 0.18595 0.17305 14.6866
4-Methyl-2-Pentanone 0.10503 0.12528 0.13869 0.165 0.15182 0.17334 0.14319 17.8216 0.995
cis-1,3-Dichloropropene 0.32308 0.35447 0.35942 0.37785 0.44285 0.40028 0.37632 11.0204
Dimethyl Disulfide 0.25819 0.3577 0.37088 0.42953 0.52232 0.48353 0.49731 0.41707 22.5325 0.997
Chlorobenzene-d5 ISTD
Toluene-d8 1.32931 1.24766 1.36447 1.35272 1.18812 1.29646 5.8473
Toluene 1.12084 1.40035 1.54236 1.39327 1.362 1.55253 1.28612 1.37964 10.7922
Ethyl Methacrylate 0.34883 0.42389 0.44038 0.53408 0.48562 0.44656 15.5504 0.996
trans-1,3-Dichloropropene 0.36313 0.4583 0.46041 0.48183 0.58154 0.51451 0.47662 15.1144 0.995
1,1,2-Trichloroethane 0.22386 0.31286 0.33003 0.30784 0.31162 0.35655 0.31582 0.30837 13.2509
2-Hexanone 0.17065 0.33435 0.37135 0.48319 0.44361 0.50745 0.3851 32.1752 0.994
1,3-Dichloropropane 0.39544 0.51188 0.55413 0.51824 0.50892 0.59434 0.52009 0.51472 11.8183
Tetrachloroethene 0.24255 0.30066 0.32772 0.29019 0.2877 0.3347 0.29646 0.29714 10.1676
Dibromochloromethane 0.32723 0.33426 0.35311 0.36651 0.44137 0.39798 0.37008 11.6417
1,2-Dibromoethane 0.27496 0.3186 0.30635 0.32155 0.3685 0.33173 0.32028 9.5817
1-Chlorohexane 0.41418 0.46131 0.43155 0.43453 0.50377 0.45558 0.45015 6.9634
Chlorobenzene 0.88602 1.00258 1.08815 0.91569 0.9081 1.03953 0.87681 0.95956 8.67873
1,1,1,2-Tetrachloroethane 0.28684 0.33494 0.35481 0.3426 0.33769 0.39976 0.35625 0.3447 9.74074
Ethylbenzene 0.42796 0.52747 0.55239 0.49735 0.48604 0.56148 0.48774 0.50578 9.056
m-,p-Xylene 0.57238 0.52979 0.63877 0.69325 0.60511 0.59691 0.67843 0.56858 0.6104 9.22583
o-Xylene 0.48537 0.60436 0.64412 0.58265 0.5869 0.68063 0.5883 0.59605 10.184
Styrene 0.88222 1.01973 0.98335 0.99506 1.17911 1.00088 1.01006 9.50003
Bromoform 0.2468 0.26527 0.28042 0.351 0.32651 0.294 14.7714
Isopropylbenzene 1.35585 1.64249 1.67087 1.53129 1.51217 1.74054 1.4314 1.55494 8.81943
1,4-Dichlorobenzene-d4 ISTD
1,1,2,2-Tetrachloroethane 0.6242 0.81549 0.91406 0.90654 0.91148 1.02423 0.91847 0.8735 14.3627
p-Bromofluorobenzene 0.9478 0.92808 1.00358 0.91328 0.90529 0.93961 4.17774
1,2,3-Trichloropropane 0.26603 0.276 0.28125 0.27356 0.30345 0.28176 0.28034 4.52994
R^2
Page 90
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
trans-1,4-Dichloro-2-Butene 0.28278 0.3263 0.32882 0.39115 0.36223 0.33826 12.0828
n-Propylbenzene 3.03086 3.79165 4.03741 3.8251 3.52438 3.54164 2.91559 3.5238 11.8124
Bromobenzene 0.66226 0.8893 0.96298 0.8797 0.82324 0.87194 0.80221 0.84166 11.2124
1,3,5-Trimethylbenzene 2.17574 2.63707 2.86163 2.71343 2.49525 2.60622 2.26692 2.53661 9.60965
2-Chlorotoluene 2.13547 2.53777 2.80859 2.53254 2.4266 2.44126 2.17898 2.43732 9.40052
4-Chlorotoluene 2.00505 2.43818 2.37165 2.14992 1.838 2.01616 1.7285 2.07821 12.5789
a-Methylstyrene 1.35882 1.33081 1.30477 1.46901 1.32745 1.35817 4.77603
tert-Butylbenzene 0.66487 0.59944 0.55648 0.59297 0.54628 0.59201 7.88621
1,2,4-Trimethylbenzene 2.04957 2.86539 3.02888 2.79016 2.54896 2.71197 2.31826 2.61617 12.9265
sec-Butylbenzene 3.23905 3.62962 3.74038 3.55307 3.25781 3.38054 2.83017 3.37581 9.04278
p-Isopropyltoluene 2.509 3.10151 2.99414 2.91784 2.72192 2.92459 2.46968 2.80552 8.70289
1,3-Dichlorobenzene 1.50758 1.78058 1.84751 1.67405 1.56993 1.76979 1.53827 1.66967 8.01523
1,4-Dichlorobenzene 1.74699 1.92089 1.86064 1.68979 1.5968 1.83807 1.56085 1.74486 7.82671
n-Butylbenzene 2.22913 2.79862 2.89925 2.71706 2.59446 2.88759 2.4027 2.64697 9.58809
1,2-Dichlorobenzene 1.38048 1.72247 1.76431 1.62853 1.58237 1.91125 1.53986 1.64704 10.4079
1,2-Dibromo-3-Chloropropane 0.21621 0.23382 0.26844 0.30963 0.25254 0.25613 13.9658
1,2,4-Trichlorobenzene 1.06977 1.26451 1.30441 1.14806 1.24191 1.44339 1.13132 1.22905 10.2124
Hexachlorobutadiene 0.50283 0.59177 0.66688 0.60293 0.6322 0.77368 0.60822 0.6255 13.1682
Naphthalene 2.7944 3.32504 3.44532 3.28651 3.60003 3.81264 2.70881 3.28182 12.2994
1,2,3-Trichlorobenzene 1.10949 1.32469 1.31658 1.15583 1.28929 1.43286 1.11821 1.24956 9.85405
Wed May 24 12:57:24 2017
Page 91
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/26/2017 14:28Version 1.5Report generated
5309110PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
Analyte Expected Found* Exceeds
%D Limit %D
RF
11M18011
WG612759
Instrument ID:HPMS11
File ID:
Run Date:05/04/2017
Run Time:00:00
Analyst:FJB
ICal Workgroup:
8260BMethod:
L17051231Login Number: WG612759-10Sample ID:
03-MAY-17HPMS11 -Cal ID:
QUCLUnits
QC Key:STD
Page 92
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/26/2017 14:28Version 1.5Report generated
5309110PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
Chloroform
1,1-Dichloroethene
Vinyl Chloride
Chloromethane
1,1,2,2-Tetrachloroethane
1,1-Dichloroethane
Bromoform
Chlorobenzene
Benzene
Carbon Tetrachloride
1,2-Dichloroethane
2-Butanone
Tetrachloroethene
Trichloroethene
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
SPCC
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
18.3
18.4
21.6
22.3
19.6
19.1
16.5
20.9
20.5
20.2
19.6
19.4
21.4
21.9
0.508
0.455
0.467
0.617
0.704
0.586
0.246
1.09
1.13
0.392
0.443
0.143
0.338
0.319
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
8.60
8.00
8.20
11.5
2.10
4.30
17.6
4.40
2.30
1.20
1.90
2.80
6.90
9.30
Analyte Expected Found
* Exceeds
%D
Limit %D
RF
11M18442
WG614378
Instrument ID:HPMS11
File ID:
Run Date:05/16/2017
Run Time:18:14
Analyst:ADC
ICal Workgroup:
8260BMethod:
L17051231Login Number: WG614378-12Sample ID:
16-MAY-17HPMS11 -Cal ID:
QUCL20
20
20
20
20
20
20
20
20
20
20
20
20
20
Units
QC Key:STD
Page 93
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/26/2017 14:28Version 1.5Report generated
5309110PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
Analyte Expected Found* Exceeds
%D Limit %D
RF
8M418926
WG609829
Instrument ID:HPMS8
File ID:
Run Date:04/12/2017
Run Time:16:10
Analyst:TMB
ICal Workgroup:
8260BMethod:
L17051231Login Number: WG609829-10Sample ID:
12-APR-17HPMS8 -Cal ID:
QUCLUnits
QC Key:STD
Page 94
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/26/2017 14:28Version 1.5Report generated
5309110PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
Chloroform
1,1-Dichloroethene
Vinyl Chloride
Bromoform
1,1-Dichloroethane
1,1,2,2-Tetrachloroethane
Chloromethane
Chlorobenzene
Benzene
Carbon Tetrachloride
1,2-Dichloroethane
2-Butanone
Tetrachloroethene
Trichloroethene
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
SPCC
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
44.7
47.0
45.4
42.9
47.6
45.7
48.6
47.2
47.6
50.2
47.2
43.5
50.6
47.5
0.449
0.340
0.363
0.175
0.432
0.431
0.411
0.934
0.983
0.377
0.268
0.0479
0.296
0.276
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10.6
6.00
9.20
14.2
4.80
8.60
2.80
5.70
4.90
0.300
5.50
13.1
1.20
5.00
Analyte Expected Found
* Exceeds
%D
Limit %D
RF
8M419014
WG610410
Instrument ID:HPMS8
File ID:
Run Date:04/17/2017
Run Time:19:53
Analyst:TMB
ICal Workgroup:
8260BMethod:
L17051231Login Number: WG610410-12Sample ID:
17-APR-17HPMS8 -Cal ID:
QUCL20
20
20
20
20
20
20
20
20
20
20
20
20
20
Units
QC Key:STD
Page 95
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/26/2017 14:28Version 1.5Report generated
5308759PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
Analyte Expected Found* Exceeds
%D Limit %D
RF
9M978927
WG603526
Instrument ID:HPMS9
File ID:
Run Date:02/21/2017
Run Time:01:23
Analyst:ADC
ICal Workgroup:
8260BMethod:
L17051231Login Number: WG603526-09Sample ID:
21-FEB-17HPMS9 -Cal ID:
QUCLUnits
QC Key:STD
Page 96
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/26/2017 14:28Version 1.5Report generated
5308759PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
Chloroform
1,1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
Toluene
Vinyl Chloride
Bromoform
Chlorobenzene
Chloromethane
1,1-Dichloroethane
1,1,2,2-Tetrachloroethane
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromomethane
2-Butanone
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon Disulfide
Carbon Tetrachloride
Dibromochloromethane
Chloroethane
2-Chloroethyl Vinyl Ether
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,2-Dichloroethane
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,3-Dichloropropane
2,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
CCC
CCC
CCC
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
SPCC
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
21.3
21.5
21.3
22.0
22.4
22.6
17.7
21.7
24.9
20.6
21.4
17.9
21.9
22.6
21.3
20.3
28.6
19.4
23.4
23.0
23.1
15.6
21.5
19.4
22.2
20.6
20.1
26.2
18.9
21.5
21.1
22.1
22.3
22.2
32.8
21.2
21.9
21.6
22.5
21.6
22.7
20.0
0.463
0.442
0.298
0.556
1.54
0.247
0.261
1.04
0.414
0.512
0.934
0.144
1.04
0.949
0.176
0.329
0.240
0.191
3.09
3.88
0.684
0.593
0.358
0.359
0.202
0.178
2.45
2.72
0.242
0.344
0.178
1.82
1.86
1.94
0.455
0.414
0.288
0.428
0.578
0.387
0.428
0.510
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
6.60
7.50
6.70
9.90
11.8
12.8
11.3
8.40
24.4
2.80
6.90
10.5
9.40
12.8
6.40
1.60
43.0
3.20
16.8
14.9
15.5
22.0
7.40
3.10
11.1
3.00
0.400
31.0
5.40
7.30
5.60
10.6
11.5
11.2
63.9
5.80
9.50
7.80
12.3
8.20
13.7
0
Analyte Expected Found %DRF
9M980442
WG615237
Instrument ID:HPMS9
File ID:
Run Date:05/23/2017
Run Time:15:46
Analyst:ADC
ICal Workgroup:
8260BMethod:
L17051231Login Number: WG615237-11Sample ID:
23-MAY-17HPMS9 -Cal ID:
Q
*
*
*
*
*
UCL20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Units
QC Key:STD
Page 97
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/26/2017 14:28Version 1.5Report generated
5308759PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
1,1-Dichloropropene
2-Hexanone
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
4-Methyl-2-Pentanone
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Tetrachloroethene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl Acetate
o-Xylene
m-,p-Xylene
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
40.0
22.1
17.0
21.8
21.6
23.1
19.4
21.6
22.9
24.3
21.9
21.4
22.5
22.4
22.9
22.9
21.5
21.9
21.3
21.4
23.9
23.4
24.6
22.8
45.3
0.362
0.309
0.681
1.68
3.25
0.137
0.289
3.75
4.28
1.10
0.368
0.335
1.40
1.41
0.424
0.332
0.289
0.422
0.301
3.13
2.97
0.740
0.680
0.691
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
10.3
14.9
8.80
7.90
15.7
3.00
8.00
14.4
21.3
9.40
6.80
12.7
11.8
14.7
14.5
7.60
9.30
6.30
7.20
19.7
17.0
22.8
14.0
13.1
Analyte Expected Found
* Exceeds
%D
Limit %D
RF
9M980442
WG615237
Instrument ID:HPMS9
File ID:
Run Date:05/23/2017
Run Time:15:46
Analyst:ADC
ICal Workgroup:
8260BMethod:
L17051231Login Number: WG615237-11Sample ID:
23-MAY-17HPMS9 -Cal ID:
Q
*
*
UCL20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Units
QC Key:STD
Page 98
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
INTERNAL STANDARD AREA SUMMARY(COMPARED TO CCV)
INTERNAL_STD - Modified 03/06/2008
05/26/2017 14:28Report generated5309113PDF File ID:
Microbac Laboratories Inc.
L17051231-03
L17051231-05
L17051231-07
L17051231-09
L17051231-11
L17051231-13
WG615095-01
WG615282-01
WG615282-02
WG615282-03
DL01
DL01
DL01
DL01
DL01
DL01
DL01
01
01
01
1 2 3
120312 229454 333775
117025 219558 318324
111321 213585 310490
111638 216952 314074
110236 217936 316529
112674 216605 311211
108085 213852 304757
119737 245509 352411
138533 255705 360756
141367 254883 357421
164010 287882 396075WG615277-02
328020 575764 792150
82005 143941 198038
Upper Limit
Lower Limit
Sample Number Dilution Tag
10.0
10.0
10.0
10.0
10.0
10.0
10.0
1.00
1.00
1.00
NA
NA
NA
NA
NA
NA
1
2
3
-
-
-
1,4-Dichlorobenzene-d4
Chlorobenzene-d5
Fluorobenzene
WG615277-02CCV Number:
HPMS11Instrument ID:
L17051231Login Number:
TCLPMatrix:WG615282Workgroup (AAB#):
Underline = Response outside limits
HPMS11CAL ID:
IS- IS- IS-
IS-
IS-
IS-
-16-MAY-17
Page 99
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
INTERNAL STANDARD AREA SUMMARY(COMPARED TO CCV)
INTERNAL_STD - Modified 03/06/2008
05/26/2017 14:28Report generated5309113PDF File ID:
Microbac Laboratories Inc.
L17051231-01
WG615278-01
WG615405-01
WG615405-02
WG615405-03
WG615405-04
DL01
DL01
01
01
01
01
1 2 3
290931 588362 720960
225844 459348 566858
275456 564667 695797
307106 595987 732592
318801 615097 750399
238600 496486 615842
318339 604742 745295WG615404-02
636678 1209484 1490590
159170 302371 372648
Upper Limit
Lower Limit
Sample Number Dilution Tag
10.0
10.0
1.00
1.00
1.00
1.00
NA
NA
NA
NA
NA
NA
1
2
3
-
-
-
1,4-Dichlorobenzene-d4
Chlorobenzene-d5
Fluorobenzene
WG615404-02CCV Number:
HPMS8Instrument ID:
L17051231Login Number:
TCLPMatrix:WG615405Workgroup (AAB#):
Underline = Response outside limits
HPMS8CAL ID:
IS- IS- IS-
IS-
IS-
IS-
-17-APR-17
Page 100
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
INTERNAL STANDARD AREA SUMMARY(COMPARED TO CCV)
INTERNAL_STD - Modified 03/06/2008
05/26/2017 14:29Report generated5308761PDF File ID:
Microbac Laboratories Inc.
L17051231-02
L17051231-04
L17051231-06
L17051231-08
L17051231-10
L17051231-12
L17051231-14
WG615221-02
WG615221-03
WG615352-01
WG615352-02
01
01
01
01
01
01
01
01
01
01
01
1 2 3
183633 522816 830438
196549 494619 765999
210820 493003 732999
227405 560554 846320
149494 443488 726347
172098 449942 708037
294074 601340 861697
200812 483425 735399
217876 531450 816934
312747 634941 887685
280863 553971 778891
299797 575431 784465WG615237-07
599594 1150862 1568930
149899 287716 392233
Upper Limit
Lower Limit
Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
NA
NA
NA
NA
NA
NA
1
2
3
-
-
-
1,4-Dichlorobenzene-d4
Chlorobenzene-d5
Fluorobenzene
WG615237-07CCV Number:
HPMS9Instrument ID:
L17051231Login Number:
SOLIDMatrix:WG615352Workgroup (AAB#):
Underline = Response outside limits
HPMS9CAL ID:
IS- IS- IS-
IS-
IS-
IS-
-23-MAY-17
Page 101
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
INTERNAL STANDARD RETENTION TIME SUMMARY(COMPARED TO CCV)
INTERNAL_STD_RT - Modified 03/06/2008
05/26/2017 14:28Report generated5309115PDF File ID:
Microbac Laboratories Inc.
L17051231-03
L17051231-05
L17051231-07
L17051231-09
L17051231-11
L17051231-13
WG615095-01
WG615282-01
WG615282-02
WG615282-03
DL01
DL01
DL01
DL01
DL01
DL01
DL01
01
01
01
1 2 3
16.94 14.12 10.49
16.94 14.12 10.49
16.94 14.12 10.49
16.94 14.12 10.49
16.94 14.12 10.49
16.94 14.12 10.49
16.94 14.12 10.49
16.94 14.12 10.49
16.94 14.12 10.49
16.94 14.12 10.49
16.94 14.12 10.49WG615277-02
17.44 14.62 10.99
16.44 13.62 9.99
Upper Limit
Lower Limit
Sample Number Dilution Tag
10.0
10.0
10.0
10.0
10.0
10.0
10.0
1.00
1.00
1.00
NA
NA
NA
NA
NA
NA
1
2
3
-
-
-
1,4-Dichlorobenzene-d4
Chlorobenzene-d5
Fluorobenzene
WG615277-02CCV Number:
HPMS11Instrument ID:
L17051231Login Number:
TCLPMatrix:WG615282Workgroup (AAB#):
Underline = Response outside limits
IS- IS- IS-
IS-
IS-
IS-
HPMS11CAL ID: -16-MAY-17
Page 102
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
INTERNAL STANDARD RETENTION TIME SUMMARY(COMPARED TO CCV)
INTERNAL_STD_RT - Modified 03/06/2008
05/26/2017 14:28Report generated5309115PDF File ID:
Microbac Laboratories Inc.
L17051231-01
WG615278-01
WG615405-01
WG615405-02
WG615405-03
WG615405-04
DL01
DL01
01
01
01
01
1 2 3
17.82 14.79 10.91
17.82 14.79 10.92
17.82 14.79 10.91
17.82 14.79 10.92
17.81 14.79 10.92
17.82 14.79 10.91
17.82 14.79 10.92WG615404-02
18.32 15.29 11.42
17.32 14.29 10.42
Upper Limit
Lower Limit
Sample Number Dilution Tag
10.0
10.0
1.00
1.00
1.00
1.00
NA
NA
NA
NA
NA
NA
1
2
3
-
-
-
1,4-Dichlorobenzene-d4
Chlorobenzene-d5
Fluorobenzene
WG615404-02CCV Number:
HPMS8Instrument ID:
L17051231Login Number:
TCLPMatrix:WG615405Workgroup (AAB#):
Underline = Response outside limits
IS- IS- IS-
IS-
IS-
IS-
HPMS8CAL ID: -17-APR-17
Page 103
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
INTERNAL STANDARD RETENTION TIME SUMMARY(COMPARED TO CCV)
INTERNAL_STD_RT - Modified 03/06/2008
05/26/2017 14:29Report generated5308763PDF File ID:
Microbac Laboratories Inc.
L17051231-02
L17051231-04
L17051231-06
L17051231-08
L17051231-10
L17051231-12
L17051231-14
WG615221-02
WG615221-03
WG615352-01
WG615352-02
01
01
01
01
01
01
01
01
01
01
01
1 2 3
17.63 14.6 10.73
17.64 14.61 10.73
17.64 14.61 10.73
17.64 14.61 10.73
17.63 14.6 10.74
17.63 14.61 10.73
17.63 14.6 10.73
17.64 14.61 10.73
17.63 14.61 10.73
17.64 14.61 10.73
17.64 14.61 10.73
17.63 14.61 10.73WG615237-07
18.13 15.11 11.23
17.13 14.11 10.23
Upper Limit
Lower Limit
Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
NA
NA
NA
NA
NA
NA
1
2
3
-
-
-
1,4-Dichlorobenzene-d4
Chlorobenzene-d5
Fluorobenzene
WG615237-07CCV Number:
HPMS9Instrument ID:
L17051231Login Number:
SOLIDMatrix:WG615352Workgroup (AAB#):
Underline = Response outside limits
IS- IS- IS-
IS-
IS-
IS-
HPMS9CAL ID: -23-MAY-17
Page 104
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:80588
Page: 1
Approved: February 24, 2017
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HPMS9
ADC
8260
022017
NA
MSV01 24
Internal Standard:
CCV:
Surrogate Standard:
LCS: MS/MSD:
Workgroups:
STD80448
STD80322
STD80112
STD80191 STD80191
WG603477, WG603526
Column 1 ID: Column 2 ID:RTX502.2 NA
Method: SOP: Rev:5035/ 5030B/ 5030C PAT01 19
9M978905
9M978906
9M978907
9M978908
9M978909
9M978910
9M978911
9M978912
9M978913
9M978914
9M978915
9M978916
9M978917
9M978918
9M978919
9M978920
9M978921
9M978922
9M978923
9M978924
9M978925
9M978926
9M978927
9M978928
WG603477-01 BFB 50ng 8260
RINSE
WG603477-02 0.5ug/L STD 8260
WG603477-03 1.0ug/L STD 8260
WG603477-04 2.0ug/L STD 8260
WG603477-05 5.0ug/L STD 8260
WG603477-06 20.0ug/L STD 8260
WG603477-07 50.0ug/L STD 8260
WG603477-08 100.0ug/L STD 8260
WG603477-09 200.0ug/L STD 8260
WG603477-10 300.0ug/L STD 8260
RINSE
WG603477-11 50.0ug/L STD 8260
WG603526-01 5ug/kg A9FOO
WG603526-02 20ug/kg A9FOO
WG603526-03 50ug/kg A9FOO
WG603526-04 100ug/kg A9FOO
WG603526-05 200ug/kg A9FOO
WG603526-06 300ug/kg A9FOO
WG603526-07 400ug/kg A9FOO
WG603526-08 500ug/kg A9FOO
RINSE
WG603526-09 100ug/kg A9FOO ALT SRC
mix 2 check
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
STD79950
STD80322
STD80322
STD80322
STD80322
STD80322
STD80322
STD80322
STD80322
STD80322
STD80191
STD80557
STD80557
STD80557
STD80557
STD80557
STD80557
STD80557
STD80557
STD80470
STD80470
02/20/17 14:09
02/20/17 14:34
02/20/17 15:05
02/20/17 15:36
02/20/17 16:07
02/20/17 16:38
02/20/17 17:10
02/20/17 17:41
02/20/17 18:12
02/20/17 18:44
02/20/17 19:15
02/20/17 19:46
02/20/17 20:17
02/20/17 20:48
02/20/17 21:19
02/20/17 21:50
02/20/17 22:21
02/20/17 22:51
02/20/17 23:21
02/20/17 23:52
02/21/17 00:22
02/21/17 00:53
02/21/17 01:23
02/21/17 12:39
File ID Sample Information Dil Reference Date/TimeMat
7
1
7
7
7
7
7
7
7
7
7
1
7
7
7
7
7
7
7
7
7
7
7
7
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
pH
Comments:
Maintenance Log ID:
Page 105
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:81580
Page: 1
Approved: April 18, 2017
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HPMS8
TMB
8260B
041217
NA
MSV01/OVAP MSV01 24/0
Internal Standard:
CCV:
Surrogate Standard:
LCS: MS/MSD:
Workgroups:
STD81235
STD81397
STD81235
STD81404 NA
WG609829
Column 1 ID: Column 2 ID:RTX502.2 NA
Method: SOP: Rev:5030B/5030C/5035A PAT01/OVAP PAT01 18/1
Method: SOP: Rev:624 MSV10 15
8M418914
8M418915
8M418916
8M418917
8M418918
8M418919
8M418920
8M418921
8M418922
8M418923
8M418924
8M418925
8M418926
8M418927
8M418928
WG609829-01 50ng BFB STD 8260
RINSE
WG609829-02 5ug/L STD A9/FOO
WG609829-03 20ug/L STD A9/FOO
WG609829-04 50ug/L STD A9/FOO
WG609829-05 100ug/L STD A9/FOO
WG609829-06 200ug/L STD A9/FOO
WG609829-07 300ug/L STD A9/FOO
WG609829-08 400ug/L STD A9/FOO
WG609829-09 500ug/L STD A9/FOO
RINSE
RINSE
WG609829-10 100ug/L ALT SRC STD A9/FO
WG609948-01 50ug/L CCV STD 8260
RINSE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
STD80989
STD80989
STD81397
STD81397
STD81397
STD81397
STD81397
STD81397
STD81397
STD81397
STD81404
STD81377
04/12/17 10:17
04/12/17 10:42
04/12/17 11:11
04/12/17 11:40
04/12/17 12:10
04/12/17 12:41
04/12/17 13:10
04/12/17 13:40
04/12/17 14:10
04/12/17 14:39
04/12/17 15:09
04/12/17 15:39
04/12/17 16:10
04/12/17 16:39
04/12/17 17:09
File ID Sample Information Dil Reference Date/TimeMat
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
pH
Comments:
Maintenance Log ID: 54128
Page 106
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:81593
Page: 1
Approved: April 20, 2017
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HPMS8
TMB
8260B
041717
NA
MSV01/OVAP MSV01 24/0
Internal Standard:
CCV:
Surrogate Standard:
LCS: MS/MSD:
Workgroups:
STD81235
STD81447
STD81235
STD81461 NA
WG610410
2
3
4
X
X
Comments
Seq. Rerun Dil. AnalytesReason
Column 1 ID: Column 2 ID:RTX502.2 NA
Method: SOP: Rev:5030B/5030C/5035A PAT01 18/1
Method: SOP: Rev:624 MSV10 15
8M418996
8M418997
8M418998
8M418999
8M419000
8M419001
8M419002
8M419003
8M419004
8M419005
8M419006
8M419007
8M419008
8M419009
8M419010
8M419011
8M419012
8M419013
8M419014
8M419015
WG610373-01 50ng BFB STD 8260
WG610373-02 50ug/L CCV STD 8260
WG610373-02 50ug/L CCV STD 8260
WG000000-01 100ug/L A9 CCV STD 8260
WG610410-01 50ng BFB STD 8260
RINSE
WG610410-02 0.3ug/L STD 8260
WG610410-03 0.4ug/L STD 8260
WG610410-04 1ug/L STD 8260
WG610410-05 2ug/L STD 8260
WG610410-06 5ug/L STD 8260
WG610410-07 20ug/L STD 8260
WG610410-08 50ug/L STD 8260
WG610410-09 100ug/L STD 8260
WG610410-10 200ug/L STD 8260
WG610410-11 300ug/L STD 8260
RINSE
RINSE
WG610410-12 50ug/L ALT SRC STD 8260
RINSE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
STD80989
STD81375
STD81375
STD81397
STD80989
STD81447
STD81447
STD81447
STD81447
STD81447
STD81447
STD81447
STD81447
STD81447
STD81447
STD81461
04/17/17 09:44
04/17/17 10:10
04/17/17 10:42
04/17/17 11:13
04/17/17 12:58
04/17/17 13:21
04/17/17 13:51
04/17/17 14:25
04/17/17 14:55
04/17/17 15:25
04/17/17 15:54
04/17/17 16:24
04/17/17 16:54
04/17/17 17:23
04/17/17 17:54
04/17/17 18:24
04/17/17 18:53
04/17/17 19:23
04/17/17 19:53
04/17/17 20:23
File ID Sample Information Dil Reference Date/TimeMat
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
pH
Bromomethane was low, DNR.
Bromomethane and iodomethane were low, DNR.
Not needed, DNR.
Comments:
8M418997
8M418998
8M418999
File ID:
File ID:
File ID:
Maintenance Log ID: 54132
Page 107
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:81984
Page: 1
Approved: May 09, 2017
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HPMS11
ADC
8260
050317
NA
MSV01, OVAP MSV01 24,0
Internal Standard:
CCV:
Surrogate Standard:
LCS: MS/MSD:
Workgroups:
STD81442
STD81698/STD81708
STD81441
STD81656/STD81640 NA
WG612363 WG612759
14 X
Comments
Seq. Rerun Dil. AnalytesReason
Column 1 ID: Column 2 ID:RTX502.2 NA
Method: SOP: Rev:5035/ 5030B/ 5030C PAT01, OVAP PAT01 18,1
Method: SOP: Rev:624 MSV10 15
11M17986
11M17987
11M17988
11M17989
11M17990
11M17991
11M17992
11M17993
11M17994
11M17995
11M17996
11M17997
11M17998
11M17999
11M18000
11M18001
11M18002
11M18003
11M18004
11M18005
11M18006
11M18007
11M18008
11M18009
11M18010
11M18011
WG612363-01 50ng BFB STD 8260
RINSE
WG612363-02 .3ug/L CCV ICAL 8260
WG612363-03 .4ug/L CCV ICAL 8260
WG612363-04 1ug/L CCV ICAL 8260
WG612363-05 2ug/L CCV ICAL 8260
WG612363-06 5ug/L CCV ICAL 8260
WG612363-07 20ug/L CCV ICAL 8260
WG612363-08 50ug/L CCV ICAL 8260
WG612363-09 100ug/L CCV ICAL 8260
WG612363-10 200ug/L CCV ICAL 8260
WG612363-11 300ug/L CCV ICAL 8260
RINSE
WG612363-12 50ug/L ICV 8260
WG612363-12 20ug/L ICV 8260
WG612759-01 BFB 50ng A9FOO
WG612759-02 5ug/L STD A9FOO
WG612759-03 20ug/L STD A9FOO
WG612759-04 50ug/L STD A9FOO
WG612759-05 100ug/L STD A9FOO
WG612759-06 200ug/L STD A9FOO
WG612759-07 300ug/L STD A9FOO
WG612759-08 400ug/L STD A9FOO
WG612759-09 500ug/L STD A9FOO
RINSE
WG612759-10 100ug/L STD A9FOO
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
STD81491
STD81698
STD81698
STD81698
STD81698
STD81698
STD81698
STD81698
STD81698
STD81698
STD81698
STD81656
STD81656
STD81491
STD81708
STD81708
STD81708
STD81708
STD81708
STD81708
STD81708
STD81708
STD81640
05/03/17 10:28
05/03/17 10:52
05/03/17 11:21
05/03/17 11:50
05/03/17 12:19
05/03/17 12:48
05/03/17 13:17
05/03/17 13:46
05/03/17 14:15
05/03/17 14:44
05/03/17 15:13
05/03/17 15:42
05/03/17 16:11
05/03/17 16:40
05/03/17 17:47
05/03/17 19:14
05/03/17 19:42
05/03/17 20:10
05/03/17 20:39
05/03/17 21:08
05/03/17 21:36
05/03/17 22:05
05/03/17 22:34
05/03/17 23:02
05/03/17 23:31
05/04/17 00:00
File ID Sample Information Dil Reference Date/TimeMat
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
pH
WG612363-12 ICV had multiple failures. RR at 20ppb.
Comments:
11M17999File ID:
Maintenance Log ID:
Page 108
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:82278
Page: 1
Approved: May 22, 2017
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HPMS11
ADC
8260B
051617
NA
MSV01/OVAP MSV01 24/0
Internal Standard:
CCV:
Surrogate Standard:
LCS: MS/MSD:
Workgroups:
STD81876
STD81698
STD81877
STD81861 STD81861
WG614378 (ICAL)
Column 1 ID: Column 2 ID:RTX502.2 NA
Method: SOP: Rev:5030B/5030C/5035A PAT01/OVAP PAT01 18/1
Method: SOP: Rev:624 MSV10 15
11M18429
11M18430
11M18431
11M18432
11M18433
11M18434
11M18435
11M18436
11M18437
11M18438
11M18439
11M18440
11M18441
11M18442
WG614378-01 BFB 50ng 8260
RINSE
WG614378-02 0.3ug/L CCV 8260
WG614378-03 0.4ug/L CCV 8260
WG614378-04 1.0ug/L CCV 8260
WG614378-05 2.0ug/L CCV 8260
WG614378-06 5.0ug/L CCV 8260
WG614378-07 20.0ug/L CCV 8260
WG614378-08 50.0ug/L CCV 8260
WG614378-09 100.0ug/L CCV 8260
WG614378-10 200.0ug/L CCV 8260
WG614378-11 300.0ug/L CCV 8260
RINSE
WG614378-12 20.0ug/L ALT 8260
1
1
1
1
1
1
1
1
1
1
1
1
1
1
STD81491
STD81880
STD81880
STD81880
STD81880
STD81880
STD81880
STD81880
STD81880
STD81880
STD81880
STD81880
STD81881
05/16/17 12:01
05/16/17 12:25
05/16/17 12:54
05/16/17 13:23
05/16/17 13:52
05/16/17 14:21
05/16/17 14:50
05/16/17 15:20
05/16/17 15:49
05/16/17 16:18
05/16/17 16:47
05/16/17 17:16
05/16/17 17:45
05/16/17 18:14
File ID Sample Information Dil Reference Date/TimeMat
1
1
1
1
1
1
1
1
1
1
1
1
1
1
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
pH
Comments:
Maintenance Log ID:
Page 109
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:82377
Page: 1
Approved: May 26, 2017
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HPMS9
ADC
8260
052317
NA
MSV01,OVAP MSV01 24,0
Internal Standard:
CCV:
Surrogate Standard:
LCS: MS/MSD:
Workgroups:
STD81876
STD81880
STD81877
STD81881 STD81881
WG615352
20
Comments
Seq. Rerun Dil. AnalytesReason
Column 1 ID: Column 2 ID:RTX502.2 NA
Method: SOP: Rev:5035/ 5030B/ 5030C PAT01, OVAP PAT01 19, 0
9M980430
9M980431
9M980432
9M980433
9M980434
9M980435
9M980436
9M980437
9M980438
9M980439
9M980440
9M980441
9M980442
9M980443
9M980444
9M980445
9M980446
9M980447
9M980448
9M980449
9M980450
9M980451
9M980452
9M980453
9M980454
9M980455
9M980456
9M980457
WG615237-01 50ng BFB
RINSE
WG615237-02 0.5ug/kg STD8260
WG615237-03 1.0ug/kg STD8260
WG615237-04 2.0ug/kg STD8260
WG615237-05 5.0ug/kg STD8260
WG615237-06 20.0ug/kg STD8260
WG615237-07 50.0ug/kg STD8260
WG615237-08 100.0ug/kg STD8260
WG615237-09 200.0ug/kg STD8260
WG615237-10 300.0ug/kg STD8260
RINSE
WG615237-11 20.0ug/kg ALT8260
RINSE
WG615352-01 BLK 8260
WG615352-02 20ug/kg LCS 8260
L17051231-04 A 826-SPE
L17051231-06 A 826-SPE
L17051231-08 A 826-SPE
L17051231-10 A 826-SPE
L17051231-12 A 826-SPE
L17051231-14 A 826-SPE
WG615221-01 L17051231-02 A 826-SPE
WG615221-02 MS A 826-SPE
WG615221-03 MSD A 826-SPE
RINSE
RINSE
TEST CCV
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
STD81491
STD81880
STD81880
STD81880
STD81880
STD81880
STD81880
STD81880
STD81880
STD81880
STD81880
STD81881
STD81881
STD81881
STD81881
STD81881
STD81881
05/23/17 09:48
05/23/17 10:17
05/23/17 10:46
05/23/17 11:16
05/23/17 11:46
05/23/17 12:17
05/23/17 12:47
05/23/17 13:16
05/23/17 13:47
05/23/17 14:16
05/23/17 14:46
05/23/17 15:16
05/23/17 15:46
05/23/17 16:16
05/23/17 16:46
05/23/17 17:16
05/23/17 17:46
05/23/17 18:16
05/23/17 18:47
05/23/17 19:17
05/23/17 19:47
05/23/17 20:17
05/23/17 20:47
05/23/17 21:17
05/23/17 21:47
05/23/17 22:17
05/23/17 22:47
05/24/17 08:46
File ID Sample Information Dil Reference Date/TimeMat
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
pH
Comments:
9M980449File ID:
Maintenance Log ID:
Page 110
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:82377
Page: 2
Approved: May 26, 2017
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HPMS9
ADC
8260
052317
NA
MSV01,OVAP MSV01 24,0
Internal Standard:
CCV:
Surrogate Standard:
LCS: MS/MSD:
Workgroups:
STD81876
STD81880
STD81877
STD81881 STD81881
WG615352
Comments
Seq. Rerun Dil. AnalytesReason
Column 1 ID: Column 2 ID:RTX502.2 NA
Method: SOP: Rev:5035/ 5030B/ 5030C PAT01, OVAP PAT01 19, 0
L17051231-10 ISTD and SSTD failure are obvious SMI as is evident in lower ISTD response in other samples with similar HC.
Comments:
Maintenance Log ID:
Page 111
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:82361
Page: 1
Approved: May 26, 2017
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HPMS11
TMB
8260
052317
NA
MSV01, OVAP MSV01 24,0
Internal Standard:
CCV:
Surrogate Standard:
LCS: MS/MSD:
Workgroups:
STD82876
STD81983, STD81708
STD82877
STD82009, STD81742 STD82009
WG615282, WEG615296
Column 1 ID: Column 2 ID:RTX502.2 NA
Method: SOP: Rev:624 MSV10 10
Method: SOP: Rev:5035, 5030B, 5030C PAT01, OVAP PAT01 19,0
11M18562
11M18563
11M18564
11M18566
11M18567
11M18568
11M18569
11M18570
11M18571
11M18572
11M18575
11M18576
11M18577
11M18578
11M18579
11M18580
11M18581
11M18582
11M18583
11M18584
11M18585
11M18586
11M18587
11M18588
11M18589
11M18590
11M18591
11M18592
11M18593
11M18594
11M18595
11M18596
11M18597
11M18598
WG615277-01 50ng BFB STD 8260
WG615277-01 50ng BFB STD 8260
WG615277-02 50ug/L CCV STD 8260
WG615279-01 100ug/L CCV 826-A9
WG615282-01 BLANK 8260
WG615282-02 20ug/L LCS 8260
WG615282-03 20ug/L LCS2 8260
WG615282-04 20ug/L LCS A9 8260
WG615282-05 20ug/L LCS2 A9 8260
L17051074-01 C 00 2X 826-SPE
L17051074-03 C 00 5X 826-SPE
L17051074-01 C 00 2X 826-SPE
L17051074-05 C 00 2X 826-SPE
L17051231-01 10X AF 826-TC
L17051231-03 10X AF 826-TC
L17051231-05 10X AF 826-TC
L17051231-07 10X AF 826-TC
L17051231-09 10X AF 826-TC
L17051231-11 10X AF 826-TC
L17051231-13 10X AF 826-TC
L17051242-01 A TB 826-A9-SPE
L17051179-03 B A1 826-A9-SPE
L17050625-02 B 826-VAP2
L17051242-02 A 826-A9-SPE
L17051242-03 A 826-A9-SPE
L17051242-05 A ER 826-A9-SPE
RINSE
WG615296-01 20ug/L LCS 624
WG615296-02 20ug/L LCS 624
RINSE
WG615296-03 BLANK 624
L17051246-01 A 624-SPE
L17051272-01 A 624
L17051272-02 A 624
1
1
1
1
1
1
1
1
1
2
5
2
2
10
10
10
10
10
10
10
1
1
1
1
1
1
1
1
1
1
1
1
1
1
STD81972
STD81972
STD81983
STD81708
STD82009
STD82009
STD81742
STD81742
STD82009
STD82009
05/23/17 11:51
05/23/17 12:03
05/23/17 12:27
05/23/17 13:08
05/23/17 13:37
05/23/17 14:06
05/23/17 14:35
05/23/17 15:04
05/23/17 15:33
05/23/17 16:02
05/23/17 16:35
05/23/17 17:27
05/23/17 17:56
05/23/17 18:25
05/23/17 18:54
05/23/17 19:23
05/23/17 19:52
05/23/17 20:20
05/23/17 20:49
05/23/17 21:18
05/23/17 21:47
05/23/17 22:16
05/23/17 22:45
05/23/17 23:14
05/23/17 23:43
05/24/17 00:12
05/24/17 00:41
05/24/17 01:10
05/24/17 01:39
05/24/17 02:08
05/24/17 02:37
05/24/17 03:06
05/24/17 03:34
05/24/17 04:03
File ID Sample Information Dil Reference Date/TimeMat
1
1
1
1
1
1
1
1
1
1
1
1
1
17
17
17
17
17
17
17
1
1
1
1
1
1
1
2
2
2
2
2
2
2
NA
NA
NA
NA
NA
NA
NA
NA
NA
<2
<2
<2
<2
NA
NA
NA
NA
NA
NA
NA
<2
<2
<2
<2
<2
<2
NA
NA
NA
NA
NA
<2
6
5
pH
Comments:
Maintenance Log ID:
Page 112
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:82361
Page: 2
Approved: May 26, 2017
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HPMS11
TMB
8260
052317
NA
MSV01, OVAP MSV01 24,0
Internal Standard:
CCV:
Surrogate Standard:
LCS: MS/MSD:
Workgroups:
STD82876
STD81983, STD81708
STD82877
STD82009, STD81742 STD82009
WG615282, WEG615296
10
23
26 X
Comments
Seq. Rerun Dil. Analytes
Missed Tune
Reason
Column 1 ID: Column 2 ID:RTX502.2 NA
Method: SOP: Rev:624 MSV10 10
Method: SOP: Rev:5035, 5030B, 5030C PAT01, OVAP PAT01 19,0
11M18599
11M18600
11M18601
11M18602
11M18603
11M18604
RINSE
L17051151-01 B 00 2X 624-SPE
CCV
RINSE
RINSE
WG615095-01 FBLK 10X AF 826-TC
1
2
1
1
1
10
05/24/17 04:32
05/24/17 05:02
05/24/17 05:31
05/24/17 06:01
05/24/17 06:30
05/24/17 06:59
File ID Sample Information Dil Reference Date/TimeMat
2
2
1
1
1
17
NA
<2
NA
NA
NA
NA
pH
L17051074-01 SOFTWARE ERROR, RERUN VIAL IMMEDIATELY.
L17050625-02 NOT NEEDED DNR.
L17051242-05 DNR
Comments:
11M18572
11M18587
11M18590
File ID:
File ID:
File ID:
Maintenance Log ID:
Page 113
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:82387
Page: 1
Approved: May 26, 2017
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HPMS8
TMB
8260B
052417
NA
MSV01/OVAP MSV01 24/0
Internal Standard:
CCV:
Surrogate Standard:
LCS: MS/MSD:
Workgroups:
STD81815
STD81983
STD81815
STD82009 STD82009
WG615405
Comments
Seq. Rerun Dil. AnalytesReason
Column 1 ID: Column 2 ID:RTX502.2 NA
Method: SOP: Rev:5030B/5030C/5035A PAT01/OVAP PAT01 18/1
Method: SOP: Rev:624 MSV10 15
8M419868
8M419869
8M419870
8M419871
8M419872
8M419873
8M419874
8M419875
8M419876
8M419877
8M419878
8M419879
8M419880
8M419881
8M419882
8M419883
8M419884
8M419885
8M419886
8M419887
8M419888
8M419889
8M419890
8M419891
8M419892
8M419893
8M419894
8M419895
8M419896
8M419897
WG615404-01 50ng BFB STD 8260
WG615404-02 50ug/L CCV STD 8260
WG000000-01 100ug/L A9 CCV STD 8260
WG615405-01 VBLK0524 BLANK STD 826
WG615405-02 20ug/L LCS STD 8260
WG615405-03 20ug/L LCS2 STD 8260
L17051231-01 B 10X 826-TC
L17051257-01 A 10X 826-TC
L17051257-02 A 10X 826-TC
L17051284-10 A 826-LOW
L17051284-11 A 826-LOW
L17051307-01 A 10X 826-TC
L17051310-03 A TB 826-BETX
L17051310-01 A 826-BETX
L17051311-01 A 826-BETX
L17051312-01 A 826-BETX
WG615405-04 VBLK0524 BLANK STD 624
L17051284-01 B 624-SPE
L17051284-02 B 624-SPE
L17051284-03 B 624-SPE
L17051284-04 B 624-SPE
L17051284-05 B 624-SPE
L17051284-06 B 624-SPE
L17051284-07 B 624-SPE
L17051284-08 B 624-SPE
L17051284-09 B 624-SPE
WG615278-01 A FBLK 10X 826-TC
WG615405-06 A MS 1257-01 10X 826-TC
CCV
RINSE
1
1
1
1
1
1
10
10
10
1
1
10
1
1
1
1
1
1
1
1
1
1
1
1
1
1
10
10
1
1
STD81972
STD81983
STD81708
STD82009
STD82009
STD82009
05/24/17 11:36
05/24/17 11:59
05/24/17 12:28
05/24/17 12:57
05/24/17 13:25
05/24/17 13:53
05/24/17 14:22
05/24/17 14:50
05/24/17 15:19
05/24/17 15:49
05/24/17 16:17
05/24/17 16:46
05/24/17 17:14
05/24/17 17:42
05/24/17 18:11
05/24/17 18:39
05/24/17 19:08
05/24/17 19:36
05/24/17 20:05
05/24/17 20:33
05/24/17 21:02
05/24/17 21:30
05/24/17 21:59
05/24/17 22:29
05/24/17 22:57
05/24/17 23:26
05/24/17 23:54
05/25/17 00:23
05/25/17 00:51
05/25/17 01:21
File ID Sample Information Dil Reference Date/TimeMat
1
1
1
1
1
1
17
1
17
2
2
17
1
1
1
1
2
2
2
2
2
2
2
2
2
2
17
17
1
1
NA
NA
NA
NA
NA
NA
5
5
5
<2
<2
5
<2
<2
<2
<2
NA
<2
<2
<2
<2
<2
<2
<2
<2
<2
4
NA
NA
NA
pH
Comments:
Maintenance Log ID: 54187
Page 114
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:82387
Page: 2
Approved: May 26, 2017
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HPMS8
TMB
8260B
052417
NA
MSV01/OVAP MSV01 24/0
Internal Standard:
CCV:
Surrogate Standard:
LCS: MS/MSD:
Workgroups:
STD81815
STD81983
STD81815
STD82009 STD82009
WG615405
3
Comments
Seq. Rerun Dil. AnalytesReason
Column 1 ID: Column 2 ID:RTX502.2 NA
Method: SOP: Rev:5030B/5030C/5035A PAT01/OVAP PAT01 18/1
Method: SOP: Rev:624 MSV10 15
Not needed, DNR.
Comments:
8M419870File ID:
Maintenance Log ID: 54187
Page 115
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
VOA Preparation/Preservation/Extraction Log
VOA_EXT - Modified 05/22/2008 PDF ID:Report generated: 05/23/2017 09:29
Microbac Laboratories Inc.
5305888
WG615221
Run Date:05/23/2017 09:14
Analyst:JSTBatch #:
L17051231-02
L17051231-04
L17051231-06
L17051231-08
L17051231-10
L17051231-12
L17051231-14
WG615221-01
WG615221-02
WG615221-03
SAMPLE # Fraction
A
A
A
A
A
A
A
A
A
A
Preserved
5.16
5.00
4.98
5.04
5.18
5.17
5.07
5.16
5.17
5.06
50.0
45.2
49.0
26.5
41.6
56.8
1.96
50.0
50.0
50.0
Sample Wt Water
5
5
5
5
5
5
5
5
5
5
Method:5030B/5030C/5035
PCT-S Tare Wt Total Wt
05/23/17 09:14
05/23/17 09:15
05/23/17 09:20
05/23/17 09:22
05/23/17 09:23
05/23/17 09:25
05/23/17 09:28
05/23/17 09:15
05/23/17 09:15
05/23/17 09:16
Collected
05/19/17 13:24
05/19/17 15:00
05/19/17 14:45
05/19/17 15:30
05/19/17 16:18
05/19/17 16:30
05/19/17 17:12
MeOH CommentsVt
5
5
5
5
5
5
5
5
5
5
Comments:1 = improperly sealed cap2 = preserved out of hold
3 = effervesced4 = preserved with NaHSO4
5 = preserved by freezing6 = preserved in field
Analyst:
COA19469
COA18552
Purge and trap methanol
Purified Lab Sand Lot #
Product:8260
Page 116
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Page 117
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Page 118
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
05/17/2017 10:07Report generated5297722PDF File ID:
Microbac Laboratories Inc.
METHOD BLANK SUMMARY
Report Name: BLANK_SUMMARY
14G67536
05/16/17 11:21
05/16/17 14:27
WG614544
WG614301-01
HP14
Blank File ID:
Prep Date:
Analyzed Date:
Work Group:
Blank Sample ID:
Instrument ID:
8015CMethod:
LJHAnalyst:
L17050904Login Number:
LCS
LCS2
17-0751 IR MUD 54 RETURN
17-0751 IR MUD SILO
17-0751 IR MUD WE RECLAIM PIT
17-0751 IR MUD BREAKOUT
17-0751 IR MUD GRID C1-D1
WG614301-02
WG614301-03
L17050904-03
L17050904-01
L17050904-04
L17050904-05
L17050904-02
14G67537
14G67538
14G67540
14G67541
14G67542
14G67543
14G67544
05/16/17 15:06
05/16/17 15:45
05/16/17 17:04
05/16/17 17:43
05/16/17 18:22
05/16/17 19:02
05/16/17 19:41
This Method Blank Applies To The Following Samples:
Client ID Lab Sample ID Lab File ID Time Analyzed TAG
01
01
01
01
01
01
01
Page 119
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac Laboratories Inc.
METHOD BLANK REPORT
Report Name:BLANK
PDF ID: 5297723
17-MAY-2017 10:07
o-Terphenyl
Octacosane
69.6
62.6
Surrogates % Recovery Surrogate Limits
43
25
-
-
136
162
Qualifier
PASS
PASS
Analytes Concentration Dilution Qualifier
Diesel Range (C10-C28) 12500 10000 J3900
ND Analyte Not detected at or above reporting limit
* |Analyte concentration| > RL
14G67536
WG614544
Instrument ID:HP14
File ID:
Prep Date:05/16/17 11:21
Run Date:05/16/17 14:27
Analyst:LJH
Workgroup (AAB#): ug/kgUnits:
8015CMethod:
SoilMatrix:
L17050904Login Number: WG614301-01Sample ID:
09-MAY-17Cal ID: HP14-OT900917Contract #:
3546Prep Method:
MDL RL
MDL
RL
Method Detection Limit
Reporting/Practical Quantitation Limit
Page 120
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
LCS_LCS2 - Modified 03/06/2008
05/17/2017 10:07Report generated:5297724PDF File ID:
LABORATORY CONTROL SAMPLE (LCS)
Microbac Laboratories Inc.
Diesel Range (C10-C28)
LCS LCS2
4.13137000 143000
Analytes %RPD
250000 250000
Found FoundKnown Known
54.9 57.2
% REC % REC
26
RPDLmt
%RecLimits
35 120-
Q
Sample ID:
Sample ID:
WG614301-02
WG614301-03
LCS
LCS2
14G67537
14G67538
File ID:
File ID:
o-Terphenyl
Octacosane
LCS LCS2
69.7 73.4
68.2 74.9
Surogates% Recovery % Recovery
Surrogate Limits
43
25
136
162
-
-
Qualifier
PASS
PASS
Run Date:
Run Date:
05/16/2017 15:06
05/16/2017 15:45
WG614544
Instrument ID:HP14
Analyst:LJH
Workgroup (AAB#): ug/kgUnits:
8015CMethod:SoilMatrix:
L17050904Login Number: 3546Prep Method:
* EXCEEDS %REC LIMIT
# EXCEEDS RPD LIMIT
STDQC Key: STD81195Lot #:
Page 121
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
SURROGATES - Modified 03/06/2008
05/17/2017 10:07Report generated:5297728PDF File ID:
SURROGATE STANDARDS
Microbac Laboratories Inc.
L17050904-01
L17050904-02
L17050904-03
L17050904-04
L17050904-05
WG614301-01
WG614301-02
WG614301-03
01
01
01
01
01
01
01
01
1 2Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1
2
-
-
o-Terphenyl
Octacosane
8015Method:
HP14Instrument Id:
L17050904Login Number:
SoilMatrix:WG614544Workgroup (AAB#):
Underline = Result out of surrogate limits
26.2 36.2
12.6 9.41
53.4 52.3
30.9 30.4
39.5 34.6
69.6 62.6
69.7 68.2
73.4 74.9
43
25
-
-
136
162
Surrogates Surrogate Limits
DL = surrogate diluted out
HP14CAL ID: -09-MAY-17
ND = surrogate not detected
Page 122
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac Laboratories Inc.
METHOD BLANK REPORT
Report Name:BLANK
PDF ID: 5308023
25-MAY-2017 09:27
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
p-Terphenyl-d14
Phenol-d5
105
85.6
72.2
88.2
97.5
74.0
Surrogates % Recovery Surrogate Limits
19
30
25
23
18
24
-
-
-
-
-
-
122
115
121
120
137
113
Qualifier
PASS
PASS
PASS
PASS
PASS
PASS
Analytes Concentration Dilution Qualifier
Chrysene
Di-N-Butylphthalate
Di-n-octylphthalate
Dibenzo(a,h)Anthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Diphenylamine/n-Nitrosodiphenylamine
N-Nitrosodipropylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
82.5
82.5
82.5
82.5
82.5
82.5
82.5
82.5
82.5
82.5
82.5
375
82.5
82.5
82.5
82.5
82.5
82.5
82.5
412
82.5
82.5
82.5
165
165
165
165
165
165
165
165
165
165
165
750
165
165
165
165
165
165
165
825
165
165
165
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
82.5
82.5
82.5
82.5
82.5
82.5
82.5
82.5
82.5
82.5
82.5
375
82.5
82.5
82.5
82.5
82.5
82.5
82.5
412
82.5
82.5
82.5
ND Analyte Not detected at or above reporting limit
* |Analyte concentration| > RL
12M62299
WG615227
Instrument ID:HPMS12
File ID:
Prep Date:05/22/17 11:48
Run Date:05/23/17 11:25
Analyst:SCB
Workgroup (AAB#): ug/kgUnits:
8270CMethod:
SoilMatrix:
L17051231Login Number: WG615091-01Sample ID:
10-APR-17Cal ID:HPMS12-OT900917Contract #:
3546Prep Method:
MDL RL
MDL
RL
Method Detection Limit
Reporting/Practical Quantitation Limit
Page 123
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/17/2017 10:07Report generated5297727PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
Diesel Range (C10-C28) 1000000 1040000 53300 4.46
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
14G67546
WG614544
Instrument ID:HP14
File ID:
Run Date:05/16/2017
Run Time:20:59
Analyst:LJH
Workgroup (AAB#):
8015CMethod:
L17050904Login Number: WG614359-02Sample ID:
09-MAY-17HP14 -Cal ID:
UNITS
ug/kg
UCL20
STDQC Key:
WATERMatrix:
Page 124
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Response Factor Report HP14
Method : C:\MSDCHEM\1\METHODS\DROQUANT.M (Chemstation Integrator) Title : SOP:GCS02 8015B/C/D DRO ICAL 05/09/17 Last Update : Tue May 09 14:01:47 2017 WG613451 Calibration Files 10k =14G67512.D 5000 =14G67513.D 2500 =14G67514.D 1000 =14G67515.D 500 =14G67516.D 100 =14G67517.D
Compound 10k 5000 2500 1000 500 100 Avg %RSD -------------------------------------------------------------------------- 1) h Diesel Range (C1 4.697 4.957 4.498 4.973 5.404 6.089 5.103 E4 11.19 2) s O-Terphenyl 5.179 5.829 5.070 5.462 5.901 5.320 5.460 E4 6.25 3) s Octacosane 3.011 4.001 3.424 3.684 3.921 3.732 3.629 E4 10.02 -------------------------------------------------------------------------- (#) = Out of Range
DROQUANT.M Tue May 09 14:42:19 2017
Page 125
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
LCS - Modified 03/06/2008
05/26/2017 14:28Report generated:5308758PDF File ID:
LABORATORY CONTROL SAMPLE (LCS)
Microbac Laboratories Inc.
9M980445
WG615352
Instrument ID:HPMS9
File ID:
Run Date:05/23/2017
Run Time:17:16
Analyst:ADC
Workgroup (AAB#): ug/kgUnits:
5030B/5030C/503Prep Method:
SoilMatrix:
L17051231Login Number:
Analytes Expected Found LCS Limits Q% Rec
Dibromofluoromethane
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
105
103
108
109
Surrogates % Recovery Surrogate Limits
80
80
81
74
-
-
-
-
120
120
117
121
Qualifier
PASS
PASS
PASS
PASS
WG615352-02Sample ID:
23-MAY-17Cal ID: HPMS9-STDQC Key:
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
4-Methyl-2-pentanone
Methylene chloride
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
o-Xylene
m-,p-Xylene
65
68
72
47
74
50
72
74
71
55
72
77
60
65
70
60
72
48
65
75
74
10
45
70
70
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
40.0
21.5
21.4
22.2
20.6
23.2
25.7
23.6
22.4
22.2
23.2
22.1
23.0
23.7
22.8
22.2
23.3
21.4
21.2
23.4
23.4
23.2
25.9
25.7
22.9
45.5
108
107
111
103
116
129
118
112
111
116
110
115
119
114
111
117
107
106
117
117
116
130
129
115
114
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
135
129
128
146
128
146
136
130
137
130
130
126
135
130
135
125
126
154
130
132
133
150
140
130
130
8260BMethod:
* EXCEEDS %REC LIMIT
Lot#:STD81766
Page 126
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
LCS_LCS2 - Modified 03/06/2008
05/26/2017 14:28Report generated:5309109PDF File ID:
LABORATORY CONTROL SAMPLE (LCS)
Microbac Laboratories Inc.
1,1-Dichloroethene
1,2-Dichloroethane
Methyl Ethyl Ketone
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
LCS LCS2
4.01
1.54
5.32
2.70
2.37
2.22
2.08
0.870
1.31
0.804
20.1 20.9
20.8 21.1
18.6 19.6
21.1 21.6
20.4 20.9
21.2 21.7
18.9 19.3
21.4 21.6
20.6 20.8
21.8 22.0
Analytes %RPD
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
Found FoundKnown Known
100 105
104 105
93.0 98.1
105 108
102 105
106 108
94.3 96.3
107 108
103 104
109 110
% REC % REC
20
20
20
20
20
20
20
20
20
20
RPDLmt
%RecLimits
80
80
10
80
65
80
80
80
80
50
132
129
170
121
140
120
125
124
122
170
-
-
-
-
-
-
-
-
-
-
Q
Sample ID:
Sample ID:
WG615282-02
WG615282-03
LCS
LCS2
11M18568
11M18569
File ID:
File ID:
1,2-Dichloroethane-d4
Dibromofluoromethane
4-Bromofluorobenzene
Toluene-d8
LCS LCS2
105 107
101 106
106 106
107 108
Surogates% Recovery % Recovery
Surrogate Limits
80
86
86
88
120
118
115
110
-
-
-
-
Qualifier
PASS
PASS
PASS
PASS
Run Date:
Run Date:
05/23/2017 14:06
05/23/2017 14:35
WG615282
Instrument ID:HPMS11
Analyst:TMB/JDS
Workgroup (AAB#): ug/LUnits:
8260BMethod:TCLP LeachMatrix:
L17051231Login Number: 5030B/5030C/503Prep Method:
* EXCEEDS %REC LIMIT
# EXCEEDS RPD LIMIT
STDQC Key: STD82009Lot #:
Page 127
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
SURROGATES - Modified 03/06/2008
05/25/2017 09:29Report generated:5308033PDF File ID:
SURROGATE STANDARDS
Microbac Laboratories Inc.
L17051231-02
L17051231-04
L17051231-06
L17051231-08
L17051231-10
L17051231-12
L17051231-14
WG615091-01
WG615091-02
01
01
01
01
01
01
01
01
01
1 2 3 4 5 6Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1
2
3
4
5
6
-
-
-
-
-
-
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
p-Terphenyl-d14
Phenol-d5
8270Method:
HPMS12Instrument Id:
L17051231Login Number:
SoilMatrix:WG615227Workgroup (AAB#):
Underline = Result out of surrogate limits
101 77.8 67.6 86.7 92.1 69.3
85.5 84.2 69.3 89.2 80.3 67.6
91.0 83.7 66.8 86.5 76.4 65.4
83.4 81.7 62.9 84.5 75.9 62.2
70.9 57.1 45.1 60.2 79.1 43.6
87.9 82.1 62.5 88.7 77.3 59.8
54.9 64.3 46.1 72.5 68.3 49.0
105 85.6 72.2 88.2 97.5 74.0
84.5 79.7 68.6 81.7 80.9 67.7
19
30
25
23
18
24
-
-
-
-
-
-
122
115
121
120
137
113
Surrogates Surrogate Limits
DL = surrogate diluted out
HPMS12CAL ID: -10-APR-17
ND = surrogate not detected
Page 128
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/25/2017 09:26Report generated5309623PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
2,4-Dichlorophenol
2-Nitrophenol
4-Chloro-3-Methylphenol
Acenaphthene
Benzo[a]pyrene
Di-n-Octyl Phthalate
Fluoranthene
Diphenylamine/n-Nitrosodiphenylamine
Phenol
1,4-Dichlorobenzene
Hexachlorobutadiene
Pentachlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrophenol
4-Nitrophenol
Hexachlorocyclopentadiene
n-Nitrosodipropylamine
2-Methylphenol
3-,4-Methylphenol
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pyridine
2,4,5-Trichlorophenol
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
51100
52000
53200
48200
50200
47200
50600
48100
48100
48000
57600
49000
49200
61500
51500
64100
43500
44100
47100
50900
52100
47000
52200
46100
48700
0.280
0.204
0.316
1.25
1.10
1.62
1.15
0.653
1.60
1.47
0.166
0.126
0.386
0.180
0.446
0.279
0.634
0.939
1.35
0.455
0.209
0.555
0.357
1.54
0.391
2.11
3.91
6.32
3.66
0.347
5.63
1.11
3.89
3.76
4.04
15.2
1.94
1.57
22.9
3.04
28.3
13.1
11.9
5.72
1.80
4.28
6.00
4.46
7.73
2.50
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
12M62316
WG615400
Instrument ID:HPMS12
File ID:
Run Date:05/24/2017
Run Time:10:05
Analyst:MES
Workgroup (AAB#):
8270CMethod:
L17051231Login Number: WG615388-02Sample ID:
10-APR-17HPMS12 -Cal ID:
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UCL20
20
20
20
20
20
20
20
20
20
20
20
20
40
40
40
40
40
40
40
40
40
40
40
40
STDQC Key:
WATERMatrix:
Page 129
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/25/2017 09:28Report generated5308031PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
1,4-Dichlorobenzene
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2-Nitrophenol
4-Chloro-3-Methylphenol
Acenaphthene
Benzo[a]pyrene
Di-n-Octyl Phthalate
Fluoranthene
Hexachlorobutadiene
Diphenylamine/n-Nitrosodiphenylamine
Pentachlorophenol
Phenol
2,4-Dinitrophenol
4-Nitrophenol
Hexachlorocyclopentadiene
n-Nitrosodipropylamine
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
2,4,5-Trichlorophenol
2,4-Dimethylphenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitroaniline
3,3'-Dichlorobenzidine
3-,4-Methylphenol
3-Nitroaniline
4,6-Dinitro-2-Methylphenol
4-Bromophenyl Phenyl Ether
4-Chloroaniline
4-Chlorophenyl Phenyl Ether
4-Nitroaniline
Acenaphthylene
Anthracene
Benzo[a]anthracene
Benzo[b]fluoranthene
Benzo[ghi]perylene
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
49200
50300
49800
50900
53300
47200
51300
47400
50400
56800
48800
50400
48700
64700
53700
59200
40200
50900
47900
50100
49000
47300
50200
49000
47700
50800
50700
45900
53000
51000
50300
47900
59500
52200
53300
49900
48500
46800
48800
48600
48800
52200
1.51
0.395
0.273
0.200
0.316
1.23
1.12
1.63
1.15
0.164
0.663
0.130
1.62
0.190
0.465
0.257
0.595
0.305
1.36
1.56
0.393
0.325
0.448
0.341
1.25
1.54
0.714
0.978
0.377
0.421
1.44
0.411
0.130
0.204
0.115
0.630
0.388
2.00
1.14
1.19
1.22
1.02
1.65
0.588
0.389
1.71
6.53
5.67
2.55
5.26
0.827
13.6
2.39
0.738
2.53
29.4
7.31
18.3
19.7
1.88
4.18
0.244
2.07
5.33
0.306
1.94
4.58
1.59
1.48
8.13
5.97
1.92
0.606
4.17
19.0
4.43
6.68
0.224
2.99
6.49
2.32
2.76
2.39
4.35
Analyte Expected Found Q%DRF
12M62298
WG615227
Instrument ID:HPMS12
File ID:
Run Date:05/23/2017
Run Time:10:50
Analyst:SCB
Workgroup (AAB#):
8270CMethod:
L17051231Login Number: WG615240-02Sample ID:
10-APR-17HPMS12 -Cal ID:
UNITS
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
UCL20
20
20
20
20
20
20
20
20
20
20
20
20
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
STDQC Key:
WATERMatrix:
Page 130
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/25/2017 09:28Report generated5308031PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
Benzo[k]fluoranthene
Benzoic Acid
Benzyl Alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
bis(2-Ethylhexyl)phthalate
Butyl Benzyl Phthalate
Chrysene
Di-n-Butyl Phthalate
Dibenz[ah]anthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluorene
Hexachlorobenzene
Hexachloroethane
Indeno[1,2,3-cd]pyrene
Isophorone
Naphthalene
Nitrobenzene
Phenanthrene
Pyrene
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
45400
33100
49600
40700
45700
49600
47400
43200
48400
49000
55200
47600
49000
49200
49200
53800
51400
53400
48400
49100
49700
48700
47300
0.991
0.151
0.948
0.392
0.843
1.47
0.920
0.585
1.07
1.38
1.05
1.70
1.48
1.42
1.35
0.216
0.607
1.24
0.606
1.07
0.340
1.10
1.28
9.13
33.7
0.830
18.6
8.51
0.722
5.24
13.6
3.26
2.05
10.3
4.72
1.97
1.63
1.58
7.50
2.75
6.90
3.26
1.86
0.625
2.56
5.31
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
12M62298
WG615227
Instrument ID:HPMS12
File ID:
Run Date:05/23/2017
Run Time:10:50
Analyst:SCB
Workgroup (AAB#):
8270CMethod:
L17051231Login Number: WG615240-02Sample ID:
10-APR-17HPMS12 -Cal ID:
UNITS
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
UCL40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
STDQC Key:
WATERMatrix:
Page 131
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/25/2017 09:25Version 1.5Report generated
5309621PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
1,4-Dichlorobenzene
Hexachlorobutadiene
Pentachlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrophenol
Hexachlorocyclopentadiene
4-Nitrophenol
n-Nitrosodipropylamine
2-Methylphenol
3-,4-Methylphenol
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pyridine
2,4,5-Trichlorophenol
CCC
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
49900
55900
63000
50800
59200
61400
53000
57900
50400
51600
52500
49400
49500
53400
53400
49200
1.53
0.161
0.162
0.398
0.172
0.267
0.459
0.790
1.07
1.47
0.469
0.198
0.585
0.366
1.78
0.395
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
0.300
11.9
26.1
1.60
18.4
22.8
6.00
15.7
0.900
3.20
4.90
1.30
1.00
6.90
6.80
1.60
Analyte Expected Found
* Exceeds
%D
Limit %D
RF
12M61777
WG609563
Instrument ID:HPMS12
File ID:
Run Date:04/10/2017
Run Time:21:31
Analyst:SCB
ICal Workgroup:
8270CMethod:
L17051231Login Number: WG609563-11Sample ID:
10-APR-17HPMS12 -Cal ID:
QUCL30
30
40
30
40
40
40
30
30
30
30
30
30
30
30
30
Units
QC Key:STD
Page 132
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/25/2017 09:28Version 1.5Report generated
5308029PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
1,4-Dichlorobenzene
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2-Nitrophenol
4-Chloro-3-Methylphenol
Acenaphthene
Benzo[a]pyrene
Di-n-Octyl Phthalate
Fluoranthene
Hexachlorobutadiene
Diphenylamine/n-Nitrosodiphenylamine
Pentachlorophenol
Phenol
2,4-Dinitrophenol
4-Nitrophenol
Hexachlorocyclopentadiene
n-Nitrosodipropylamine
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
2,4,5-Trichlorophenol
2,4-Dimethylphenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitroaniline
3-,4-Methylphenol
3-Nitroaniline
4,6-Dinitro-2-Methylphenol
4-Bromophenyl Phenyl Ether
4-Chloroaniline
4-Chlorophenyl Phenyl Ether
4-Nitroaniline
Acenaphthylene
Anthracene
Benzo[a]anthracene
Benzo[b]fluoranthene
Benzo[ghi]perylene
Benzo[k]fluoranthene
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
49900
50800
50900
51800
49900
54800
50100
52800
49600
55900
50600
63000
54300
59200
53000
61400
57900
48700
50300
51600
49200
51000
52500
52000
57000
52600
48200
50400
54800
51600
51900
55500
50600
50700
51300
51400
49800
48500
48600
48600
50700
49700
1.53
0.398
0.279
0.204
0.296
1.42
1.10
1.82
1.13
0.161
0.687
0.162
1.81
0.172
0.459
0.267
0.790
0.291
1.43
1.60
0.395
0.350
0.469
0.361
1.49
1.59
0.678
1.07
0.389
1.47
0.445
0.121
0.197
0.110
0.648
0.410
2.13
1.13
1.19
1.21
0.993
1.09
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
0.300
1.60
1.90
3.70
0.300
9.50
0.300
5.70
0.800
11.9
1.10
26.1
8.50
18.4
6.00
22.8
15.7
2.60
0.600
3.30
1.60
2.00
4.90
3.90
13.9
5.20
3.70
0.900
9.50
3.20
3.90
11.0
1.20
1.40
2.50
2.70
0.400
3.00
2.80
2.80
1.50
0.500
Analyte Expected Found %DRF
12M61777
WG609563
Instrument ID:HPMS12
File ID:
Run Date:04/10/2017
Run Time:21:31
Analyst:SCB
ICal Workgroup:
8270CMethod:
L17051231Login Number: WG609563-11Sample ID:
10-APR-17HPMS12 -Cal ID:
QUCL30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Units
QC Key:STD
Page 133
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/25/2017 09:28Version 1.5Report generated
5308029PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
Benzoic Acid
Benzyl Alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
bis(2-Ethylhexyl)phthalate
Butyl Benzyl Phthalate
Chrysene
Di-n-Butyl Phthalate
Dibenz[ah]anthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluorene
Hexachlorobenzene
Hexachloroethane
Indeno[1,2,3-cd]pyrene
Isophorone
Naphthalene
Nitrobenzene
Phenanthrene
Pyrene
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
47200
51300
51400
52000
50800
54000
51000
50600
52700
49900
50600
52800
52300
52600
49400
49500
49100
51400
50000
53400
48700
48200
0.232
0.981
0.474
0.957
1.51
1.05
0.690
1.12
1.49
0.953
1.80
1.59
1.51
1.44
0.198
0.585
1.14
0.644
1.09
0.366
1.10
1.31
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
5.70
2.50
2.70
3.90
1.50
7.90
2.00
1.10
5.40
0.200
1.30
5.50
4.60
5.20
1.30
1.00
1.70
2.80
0
6.90
2.60
3.60
Analyte Expected Found
* Exceeds
%D
Limit %D
RF
12M61777
WG609563
Instrument ID:HPMS12
File ID:
Run Date:04/10/2017
Run Time:21:31
Analyst:SCB
ICal Workgroup:
8270CMethod:
L17051231Login Number: WG609563-11Sample ID:
10-APR-17HPMS12 -Cal ID:
QUCL30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Units
QC Key:STD
Page 134
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/25/2017 09:28Version 1.5Report generated
5308029PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
3,3'-Dichlorobenzidine 50000 53400 0.441ug/L 6.80
Analyte Expected Found
* Exceeds
%D
Limit %D
RF
12M61779
WG609563
Instrument ID:HPMS12
File ID:
Run Date:04/10/2017
Run Time:22:36
Analyst:SCB
ICal Workgroup:
8270CMethod:
L17051231Login Number: WG609563-13Sample ID:
10-APR-17HPMS12 -Cal ID:
QUCL30
Units
QC Key:STD
Page 135
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
INTERNAL STANDARD AREA SUMMARY(COMPARED TO CCV)
INTERNAL_STD - Modified 03/06/2008
05/25/2017 09:26Report generated5309624PDF File ID:
Microbac Laboratories Inc.
L17051231-01
L17051231-03
L17051231-05
L17051231-07
L17051231-09
L17051231-11
L17051231-13
WG615097-01
WG615097-02
WG615216-01
WG615216-02
01
01
01
01
01
01
01
01
01
01
01
1 2 3 4 5 6
99379 185096 299893 368338 292656 314410
100414 164426 305392 369646 284088 312476
101237 168295 299488 337884 291478 326419
101050 166928 314177 333596 287340 315427
103302 187260 301163 382759 293979 345239
102788 170112 319126 371740 291431 323009
102941 185878 301302 380841 289977 343511
104843 191921 310692 390373 303833 358289
104813 174002 318860 344942 304969 324813
108833 187407 315435 396011 322065 359979
102537 181219 295395 362752 299904 327491
118542 206426 354369 405282 359204 380634WG615388-02
237084 412852 708738 810564 718408 761268
59271 103213 177185 202641 179602 190317
Upper Limit
Lower Limit
Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
NA
NA
NA
NA
NA
NA
1
2
3
4
5
6
-
-
-
-
-
-
1,4-Dichlorobenzene-d4
Acenaphthene-d10
Chrysene-d12
Naphthalene-d8
Perylene-d12
Phenanthrene-d10
WG615388-02CCV Number:
HPMS12Instrument ID:
L17051231Login Number:
TCLPMatrix:WG615400Workgroup (AAB#):
Underline = Response outside limits
HPMS12CAL ID:
IS- IS- IS- IS- IS- IS-
IS-
IS-
IS-
IS-
IS-
IS-
-10-APR-17
Page 136
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
INTERNAL STANDARD AREA SUMMARY(COMPARED TO CCV)
INTERNAL_STD - Modified 03/06/2008
05/25/2017 09:29Report generated5308032PDF File ID:
Microbac Laboratories Inc.
L17051231-02
L17051231-04
L17051231-06
L17051231-08
L17051231-10
L17051231-12
L17051231-14
WG615091-01
WG615091-02
WG615091-04
WG615091-05
01
01
01
01
01
01
01
01
01
01
01
1 2 3 4 5 6
101407 186165 298269 383844 304512 342200
104196 189493 325826 387870 310151 352205
98204 186958 311427 380478 308097 338839
105419 188682 309876 387587 322218 339647
106267 192777 326550 393519 323697 324841
104638 188174 311919 384487 304487 335235
101947 185256 300791 377915 298286 340457
102238 186655 302139 380370 297124 339873
102517 186096 303270 377713 309601 347719
99388 174511 287191 351610 278235 323738
99333 161886 295386 363889 275328 308800
162142 316083 529986 633707 530132 578472WG615240-02
324284 632166 1059972 1267414 1060264 1156944
81071 158042 264993 316854 265066 289236
Upper Limit
Lower Limit
Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
NA
NA
NA
NA
NA
NA
1
2
3
4
5
6
-
-
-
-
-
-
1,4-Dichlorobenzene-d4
Acenaphthene-d10
Chrysene-d12
Naphthalene-D8
Perylene-d12
Phenanthrene-d10
WG615240-02CCV Number:
HPMS12Instrument ID:
L17051231Login Number:
SOLIDMatrix:WG615227Workgroup (AAB#):
Underline = Response outside limits
HPMS12CAL ID:
IS- IS- IS- IS- IS- IS-
IS-
IS-
IS-
IS-
IS-
IS-
-10-APR-17
Page 137
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
INTERNAL STANDARD RETENTION TIME SUMMARY(COMPARED TO CCV)
INTERNAL_STD_RT - Modified 03/06/2008
05/25/2017 09:26Report generated5309635PDF File ID:
Microbac Laboratories Inc.
L17051231-01
L17051231-03
L17051231-05
L17051231-07
L17051231-09
L17051231-11
L17051231-13
WG615097-01
WG615097-02
WG615216-01
WG615216-02
01
01
01
01
01
01
01
01
01
01
01
1 2 3 4 5 6
7.823 10.927 16.237 9.116 19.079 12.54
7.823 10.927 16.237 9.116 19.079 12.54
7.823 10.927 16.237 9.116 19.074 12.54
7.823 10.927 16.237 9.116 19.074 12.54
7.823 10.927 16.237 9.116 19.079 12.54
7.823 10.927 16.237 9.116 19.079 12.54
7.823 10.927 16.237 9.116 19.079 12.54
7.823 10.927 16.237 9.116 19.079 12.54
7.823 10.927 16.237 9.116 19.074 12.54
7.829 10.932 16.243 9.121 19.085 12.546
7.823 10.927 16.243 9.116 19.085 12.546
7.82 10.93 16.24 9.12 19.08 12.55WG615388-02
8.32 11.43 16.74 9.62 19.58 13.05
7.32 10.43 15.74 8.62 18.58 12.05
Upper Limit
Lower Limit
Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
NA
NA
NA
NA
NA
NA
1
2
3
4
5
6
-
-
-
-
-
-
1,4-Dichlorobenzene-d4
Acenaphthene-d10
Chrysene-d12
Naphthalene-d8
Perylene-d12
Phenanthrene-d10
WG615388-02CCV Number:
HPMS12Instrument ID:
L17051231Login Number:
TCLPMatrix:WG615400Workgroup (AAB#):
Underline = Response outside limits
IS- IS- IS- IS- IS- IS-
IS-
IS-
IS-
IS-
IS-
IS-
HPMS12CAL ID: -10-APR-17
Page 138
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
INTERNAL STANDARD RETENTION TIME SUMMARY(COMPARED TO CCV)
INTERNAL_STD_RT - Modified 03/06/2008
05/25/2017 09:29Report generated5308036PDF File ID:
Microbac Laboratories Inc.
L17051231-02
L17051231-04
L17051231-06
L17051231-08
L17051231-10
L17051231-12
L17051231-14
WG615091-01
WG615091-02
WG615091-04
WG615091-05
01
01
01
01
01
01
01
01
01
01
01
1 2 3 4 5 6
7.823 10.927 16.237 9.116 19.074 12.54
7.823 10.927 16.237 9.116 19.074 12.54
7.823 10.927 16.237 9.116 19.074 12.54
7.823 10.927 16.237 9.116 19.074 12.54
7.823 10.927 16.232 9.116 19.074 12.54
7.823 10.927 16.237 9.116 19.079 12.54
7.823 10.927 16.232 9.116 19.074 12.54
7.823 10.927 16.237 9.116 19.079 12.54
7.823 10.927 16.237 9.116 19.079 12.54
7.823 10.927 16.242 9.116 19.079 12.54
7.823 10.927 16.243 9.116 19.079 12.54
7.83 10.93 16.25 9.12 19.09 12.55WG615240-02
8.33 11.43 16.75 9.62 19.59 13.05
7.33 10.43 15.75 8.62 18.59 12.05
Upper Limit
Lower Limit
Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
NA
NA
NA
NA
NA
NA
1
2
3
4
5
6
-
-
-
-
-
-
1,4-Dichlorobenzene-d4
Acenaphthene-d10
Chrysene-d12
Naphthalene-D8
Perylene-d12
Phenanthrene-d10
WG615240-02CCV Number:
HPMS12Instrument ID:
L17051231Login Number:
SOLIDMatrix:WG615227Workgroup (AAB#):
Underline = Response outside limits
IS- IS- IS- IS- IS- IS-
IS-
IS-
IS-
IS-
IS-
IS-
HPMS12CAL ID: -10-APR-17
Page 139
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:81488
Page: 1 Approved: 12-APR-17
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HPMS12
SCB
8270C/D
041017
NA
MSS01 28
Column 1 ID: Column 2 ID:RXI-5MS NA
Method: SOP: Rev:OVAP MSS01 0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
12M61763
12M61764
12M61765
12M61766
12M61767
12M61768
12M61769
12M61770
12M61771
12M61772
12M61773
12M61774
12M61775
12M61776
12M61777
12M61778
12M61779
12M61780
12M61781
12M61782
12M61783
12M61784
12M61785
12M61786
12M61787
12M61788
RINSE W/IS
WG609563-01 50PPM DFTPP STD
WG609563-02 50PPM 8270 STD
WG609563-01 50PPM DFTPP STD
WG609563-01 50PPM DFTPP STD
WG609563-02 50PPM 8270 STD
WG609563-03 1PPM 8270 STD
WG609563-04 3PPM 8270 STD
WG609563-05 10PPM 8270 STD
WG609563-06 15PPM 8270 STD
WG609563-07 25PPM 8270 STD
WG609563-08 80PPM 8270 STD
WG609563-09 100PPM 8270 STD
WG609563-10 120PPM 8270 STD
WG609563-11 50PPM 8270 ALT SRC
WG609563-12 50PPM 1,4-DIOX ALT SRC
WG609563-13 50PPM MP,A9,BEN ALT SRC
WG609604-01 50PPM TCL/A-TERP STD
WG609604-02 3PPM TCL/A-TERP STD
WG609604-03 10PPM TCL/A-TERP STD
WG609604-04 25PPM TCL/A-TERP STD
WG609604-05 80PPM TCL/A-TERP STD
WG609604-06 100PPM TCL/A-TERP STD
WG609604-07 200PPM TCL/A-TERP STD
WG609604-08 50PPM TCL/A-TERP ALT SRC
BAKE OUT
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
STD80383
STD79533
STD80383
STD80383
STD79533
STD79533
STD79533
STD79533
STD79533
STD79533
STD79533
STD79533
STD79533
STD81294
STD79236
STD79746
STD81291
STD81291
STD81291
STD81291
STD81291
STD81291
STD81291
STD81289
04/10/17 13:58
04/10/17 14:32
04/10/17 14:51
04/10/17 15:33
04/10/17 16:14
04/10/17 16:33
04/10/17 17:06
04/10/17 17:39
04/10/17 18:12
04/10/17 18:46
04/10/17 19:19
04/10/17 19:52
04/10/17 20:25
04/10/17 20:59
04/10/17 21:31
04/10/17 22:04
04/10/17 22:36
04/10/17 23:09
04/10/17 23:42
04/11/17 00:14
04/11/17 00:47
04/11/17 01:20
04/11/17 01:52
04/11/17 02:25
04/11/17 02:57
04/11/17 03:30
Seq. File ID Sample Information Dil Reference Date/TimeMat
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
COA19575Internal STD: Surrogate STD: NA
Comments:
WG609563, WG609604Workgroups:
2
3
WG609563-01 50PPM DFTPP STD DNR
WG609563-02 50PPM 8270 STD raised the voltage by 50, DNR
Comments
Seq. Rerun Dil. AnalytesReason
Maintenance Log ID:
Calibration STD
Syringe Filter Lot#:
STD79533, 81291CCV STD: LCS STD: MS/MSD STD:
Eluent ID#:
Page 140
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:81488
Page: 2 Approved: 12-APR-17
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HPMS12
SCB
8270C/D
041017
NA
MSS01 28
Column 1 ID: Column 2 ID:RXI-5MS NA
Method: SOP: Rev:OVAP MSS01 0
COA19575Internal STD: Surrogate STD: NA
WG609563, WG609604Workgroups:
4
WG609563-01 50PPM DFTPP STD has an ion failure, DNR
Comments
Seq. Rerun Dil. AnalytesReason
Maintenance Log ID: Syringe Filter Lot#:
STD79533, 81291CCV STD: LCS STD:
Eluent ID#:
Page 141
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID:82369
Page: 1 Approved: 24-MAY-17
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
HPMS12
SCB
8270C/D
052317
MES
MSS01 28
Column 1 ID: Column 2 ID:RXI-5MS NA
Method: SOP: Rev:OVAP MSS01 0
1
2
3
4
5
6
7
8
9
10
11
19
13
14
15
16
17
18
12M62296
12M62297
12M62298
12M62299
12M62300
12M62301
12M62302
12M62303
12M62304
12M62305
12M62306
12M62307
12M62308
12M62309
12M62310
12M62311
12M62312
12M62313
WG615240-01 50PPM DFTPP STD
WG615240-01 50PPM DFTPP STD
WG615240-02 50PPM 8270 STD
WG615091-01 BLANK 5/22
WG615091-02 LCS 5/22
L17051231-14
L17051231-04
L17051231-08
L17051231-06
L17051231-10
L17051231-12
L17051231-02 REF
WG615091-04 MS
WG615091-05 MSD
BAKE OUT
BAKE OUT
BAKE OUT
BAKE OUT
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
STD80383
STD80383
STD79533
SOIL
SOIL
SOIL
SOIL
SOIL
SOIL
SOIL
SOIL
SOIL
SOIL
SOIL
05/23/17 10:01
05/23/17 10:32
05/23/17 10:50
05/23/17 11:25
05/23/17 11:58
05/23/17 12:31
05/23/17 13:03
05/23/17 13:36
05/23/17 14:10
05/23/17 14:43
05/23/17 15:16
05/23/17 15:49
05/23/17 16:22
05/23/17 16:55
05/23/17 17:28
05/23/17 18:01
05/23/17 18:34
05/23/17 19:07
Seq. File ID Sample Information Dil Reference Date/TimeMat
1
1
1
7
7
7
7
7
7
7
7
7
7
7
1
1
1
1
COA19575Internal STD: Surrogate STD: NA
Comments:
WG615227Workgroups:
1
4
13
14
X
DFTPP, ion ratio failed.
WG615091-01 BLANK 5/22 benzoic acid is >MDL, but <RL. The associated samples are non-detect for this analyte.
WG615091-04 MS: 2 analytes failed low.
WG615091-05 MSD: 2 analytes failed low.
Comments
Seq. Rerun Dil. AnalytesReason
Maintenance Log ID:
Calibration STD
Syringe Filter Lot#:
STD79533CCV STD: LCS STD: MS/MSD STD:
Eluent ID#:
Page 142
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/26/2017 14:28Version 1.5Report generated
5309110PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
Chloroform
1,1-Dichloroethene
Vinyl Chloride
Chloromethane
1,1,2,2-Tetrachloroethane
1,1-Dichloroethane
Bromoform
Chlorobenzene
Benzene
Carbon Tetrachloride
1,2-Dichloroethane
2-Butanone
Tetrachloroethene
Trichloroethene
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
SPCC
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
18.3
18.4
21.6
22.3
19.6
19.1
16.5
20.9
20.5
20.2
19.6
19.4
21.4
21.9
0.508
0.455
0.467
0.617
0.704
0.586
0.246
1.09
1.13
0.392
0.443
0.143
0.338
0.319
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
8.60
8.00
8.20
11.5
2.10
4.30
17.6
4.40
2.30
1.20
1.90
2.80
6.90
9.30
Analyte Expected Found
* Exceeds
%D
Limit %D
RF
11M18442
WG614378
Instrument ID:HPMS11
File ID:
Run Date:05/16/2017
Run Time:18:14
Analyst:ADC
ICal Workgroup:
8260BMethod:
L17051231Login Number: WG614378-12Sample ID:
16-MAY-17HPMS11 -Cal ID:
QUCL20
20
20
20
20
20
20
20
20
20
20
20
20
20
Units
QC Key:STD
Page 143
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Page 144
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/26/2017 14:28Version 1.5Report generated
5308759PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
1,1-Dichloropropene
2-Hexanone
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
4-Methyl-2-Pentanone
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Tetrachloroethene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl Acetate
o-Xylene
m-,p-Xylene
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
40.0
22.1
17.0
21.8
21.6
23.1
19.4
21.6
22.9
24.3
21.9
21.4
22.5
22.4
22.9
22.9
21.5
21.9
21.3
21.4
23.9
23.4
24.6
22.8
45.3
0.362
0.309
0.681
1.68
3.25
0.137
0.289
3.75
4.28
1.10
0.368
0.335
1.40
1.41
0.424
0.332
0.289
0.422
0.301
3.13
2.97
0.740
0.680
0.691
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
10.3
14.9
8.80
7.90
15.7
3.00
8.00
14.4
21.3
9.40
6.80
12.7
11.8
14.7
14.5
7.60
9.30
6.30
7.20
19.7
17.0
22.8
14.0
13.1
Analyte Expected Found
* Exceeds
%D
Limit %D
RF
9M980442
WG615237
Instrument ID:HPMS9
File ID:
Run Date:05/23/2017
Run Time:15:46
Analyst:ADC
ICal Workgroup:
8260BMethod:
L17051231Login Number: WG615237-11Sample ID:
23-MAY-17HPMS9 -Cal ID:
Q
*
*
UCL20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Units
QC Key:STD
Page 145
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
INTERNAL STANDARD AREA SUMMARY(COMPARED TO CCV)
INTERNAL_STD - Modified 03/06/2008
05/26/2017 14:28Report generated5309113PDF File ID:
Microbac Laboratories Inc.
L17051231-03
L17051231-05
L17051231-07
L17051231-09
L17051231-11
L17051231-13
WG615095-01
WG615282-01
WG615282-02
WG615282-03
DL01
DL01
DL01
DL01
DL01
DL01
DL01
01
01
01
1 2 3
120312 229454 333775
117025 219558 318324
111321 213585 310490
111638 216952 314074
110236 217936 316529
112674 216605 311211
108085 213852 304757
119737 245509 352411
138533 255705 360756
141367 254883 357421
164010 287882 396075WG615277-02
328020 575764 792150
82005 143941 198038
Upper Limit
Lower Limit
Sample Number Dilution Tag
10.0
10.0
10.0
10.0
10.0
10.0
10.0
1.00
1.00
1.00
NA
NA
NA
NA
NA
NA
1
2
3
-
-
-
1,4-Dichlorobenzene-d4
Chlorobenzene-d5
Fluorobenzene
WG615277-02CCV Number:
HPMS11Instrument ID:
L17051231Login Number:
TCLPMatrix:WG615282Workgroup (AAB#):
Underline = Response outside limits
HPMS11CAL ID:
IS- IS- IS-
IS-
IS-
IS-
-16-MAY-17
Page 146
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Inorganic QA/QC
Page 147
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
05/17/2017 10:07Report generated5297722PDF File ID:
Microbac Laboratories Inc.
METHOD BLANK SUMMARY
Report Name: BLANK_SUMMARY
14G67536
05/16/17 11:21
05/16/17 14:27
WG614544
WG614301-01
HP14
Blank File ID:
Prep Date:
Analyzed Date:
Work Group:
Blank Sample ID:
Instrument ID:
8015CMethod:
LJHAnalyst:
L17050904Login Number:
LCS
LCS2
17-0751 IR MUD 54 RETURN
17-0751 IR MUD SILO
17-0751 IR MUD WE RECLAIM PIT
17-0751 IR MUD BREAKOUT
17-0751 IR MUD GRID C1-D1
WG614301-02
WG614301-03
L17050904-03
L17050904-01
L17050904-04
L17050904-05
L17050904-02
14G67537
14G67538
14G67540
14G67541
14G67542
14G67543
14G67544
05/16/17 15:06
05/16/17 15:45
05/16/17 17:04
05/16/17 17:43
05/16/17 18:22
05/16/17 19:02
05/16/17 19:41
This Method Blank Applies To The Following Samples:
Client ID Lab Sample ID Lab File ID Time Analyzed TAG
01
01
01
01
01
01
01
Page 148
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac Laboratories Inc.
METHOD BLANK REPORT
Report Name:BLANK
PDF ID: 5297723
17-MAY-2017 10:07
o-Terphenyl
Octacosane
69.6
62.6
Surrogates % Recovery Surrogate Limits
43
25
-
-
136
162
Qualifier
PASS
PASS
Analytes Concentration Dilution Qualifier
Diesel Range (C10-C28) 12500 10000 J3900
ND Analyte Not detected at or above reporting limit
* |Analyte concentration| > RL
14G67536
WG614544
Instrument ID:HP14
File ID:
Prep Date:05/16/17 11:21
Run Date:05/16/17 14:27
Analyst:LJH
Workgroup (AAB#): ug/kgUnits:
8015CMethod:
SoilMatrix:
L17050904Login Number: WG614301-01Sample ID:
09-MAY-17Cal ID: HP14-OT900917Contract #:
3546Prep Method:
MDL RL
MDL
RL
Method Detection Limit
Reporting/Practical Quantitation Limit
Page 149
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
LCS_LCS2 - Modified 03/06/2008
05/17/2017 10:07Report generated:5297724PDF File ID:
LABORATORY CONTROL SAMPLE (LCS)
Microbac Laboratories Inc.
Diesel Range (C10-C28)
LCS LCS2
4.13137000 143000
Analytes %RPD
250000 250000
Found FoundKnown Known
54.9 57.2
% REC % REC
26
RPDLmt
%RecLimits
35 120-
Q
Sample ID:
Sample ID:
WG614301-02
WG614301-03
LCS
LCS2
14G67537
14G67538
File ID:
File ID:
o-Terphenyl
Octacosane
LCS LCS2
69.7 73.4
68.2 74.9
Surogates% Recovery % Recovery
Surrogate Limits
43
25
136
162
-
-
Qualifier
PASS
PASS
Run Date:
Run Date:
05/16/2017 15:06
05/16/2017 15:45
WG614544
Instrument ID:HP14
Analyst:LJH
Workgroup (AAB#): ug/kgUnits:
8015CMethod:SoilMatrix:
L17050904Login Number: 3546Prep Method:
* EXCEEDS %REC LIMIT
# EXCEEDS RPD LIMIT
STDQC Key: STD81195Lot #:
Page 150
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
SURROGATES - Modified 03/06/2008
05/17/2017 10:07Report generated:5297728PDF File ID:
SURROGATE STANDARDS
Microbac Laboratories Inc.
L17050904-01
L17050904-02
L17050904-03
L17050904-04
L17050904-05
WG614301-01
WG614301-02
WG614301-03
01
01
01
01
01
01
01
01
1 2Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1
2
-
-
o-Terphenyl
Octacosane
8015Method:
HP14Instrument Id:
L17050904Login Number:
SoilMatrix:WG614544Workgroup (AAB#):
Underline = Result out of surrogate limits
26.2 36.2
12.6 9.41
53.4 52.3
30.9 30.4
39.5 34.6
69.6 62.6
69.7 68.2
73.4 74.9
43
25
-
-
136
162
Surrogates Surrogate Limits
DL = surrogate diluted out
HP14CAL ID: -09-MAY-17
ND = surrogate not detected
Page 151
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/17/2017 10:07Report generated5297727PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
Diesel Range (C10-C28) 1000000 1000000 51200 0.384
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
14G67535
WG614544
Instrument ID:HP14
File ID:
Run Date:05/16/2017
Run Time:09:32
Analyst:LJH
Workgroup (AAB#):
8015CMethod:
L17050904Login Number: WG614359-01Sample ID:
09-MAY-17HP14 -Cal ID:
UNITS
ug/kg
UCL20
STDQC Key:
WATERMatrix:
Page 152
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/17/2017 10:07Report generated5297727PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
Diesel Range (C10-C28) 1000000 1040000 53300 4.46
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
14G67546
WG614544
Instrument ID:HP14
File ID:
Run Date:05/16/2017
Run Time:20:59
Analyst:LJH
Workgroup (AAB#):
8015CMethod:
L17050904Login Number: WG614359-02Sample ID:
09-MAY-17HP14 -Cal ID:
UNITS
ug/kg
UCL20
STDQC Key:
WATERMatrix:
Page 153
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/24/2017 11:14Report generated5308574PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
0.400
1.00
0.0500
0.500
0.500
0.400
0.400
0.398
1.01
0.0503
0.506
0.504
0.407
0.405
99.5
101
101
101
101
102
101
90 - 110
90 - 110
90 - 110
90 - 110
90 - 110
90 - 110
90 - 110
Analyte Expected Found Q
* Exceeds
LIMITS
Criteria LIMITS
%REC
T4.052317.165324
WG615308
Instrument ID:ICP-THERMO4
File ID:
Run Date:05/23/2017
Run Time:16:53
Analyst:KKB
Workgroup (AAB#):
6010BMethod:
L17051231Login Number: WG615438-14Sample ID:
23-MAY-17ICP-TH -Cal ID:
UNITS
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
STDQC Key:
WATERMatrix:
Page 154
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/24/2017 11:14Report generated5308574PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
0.400
1.00
0.0500
0.500
0.500
0.400
0.400
0.397
1.01
0.0508
0.506
0.511
0.402
0.402
99.2
101
102
101
102
100
100
90 - 110
90 - 110
90 - 110
90 - 110
90 - 110
90 - 110
90 - 110
Analyte Expected Found Q
* Exceeds
LIMITS
Criteria LIMITS
%REC
T4.052317.171908
WG615308
Instrument ID:ICP-THERMO4
File ID:
Run Date:05/23/2017
Run Time:17:19
Analyst:KKB
Workgroup (AAB#):
6010BMethod:
L17051231Login Number: WG615438-16Sample ID:
23-MAY-17ICP-TH -Cal ID:
UNITS
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
STDQC Key:
WATERMatrix:
Page 155
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCB - Modified 03/05/2008
05/24/2017 11:14Report generated5308575PDF File ID:
CONTINUING CALIBRATION BLANK (CCB)
Microbac Laboratories Inc.
Analytes MDL RDL Concentration Qualifier
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
0.0500
0.00500
0.00500
0.0100
0.0500
0.0400
0.00500
0.100
0.0100
0.0100
0.0200
0.100
0.0800
0.0100
0.0500
0.00500
0.00500
0.0100
0.0500
0.0400
0.00500
T4.052317.144628
WG615308
Instrument ID:ICP-THERMO4
File ID:
Run Date:05/23/2017
Run Time:14:46
Analyst:KKB
Workgroup (AAB#):
mg/LUnits:
6010BMethod:
L17051231Login Number: WG615438-11Sample ID:
U
U
U
U
U
U
U
U = Result is less than MDL.F = Result is between MDL and RL.
23-MAY-17ICP-TH -Cal ID:
* = Result is above RL.
WATERMatrix: QAPP:STD
Page 156
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCB - Modified 03/05/2008
05/24/2017 11:14Report generated5308575PDF File ID:
CONTINUING CALIBRATION BLANK (CCB)
Microbac Laboratories Inc.
Analytes MDL RDL Concentration Qualifier
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
0.0500
0.00500
0.00500
0.0100
0.0500
0.0400
0.00500
0.100
0.0100
0.0100
0.0200
0.100
0.0800
0.0100
0.0500
0.00500
0.00500
0.0100
0.0500
0.0400
0.00500
T4.052317.161307
WG615308
Instrument ID:ICP-THERMO4
File ID:
Run Date:05/23/2017
Run Time:16:13
Analyst:KKB
Workgroup (AAB#):
mg/LUnits:
6010BMethod:
L17051231Login Number: WG615438-13Sample ID:
U
U
U
U
U
U
U
U = Result is less than MDL.F = Result is between MDL and RL.
23-MAY-17ICP-TH -Cal ID:
* = Result is above RL.
WATERMatrix: QAPP:STD
Page 157
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/17/2017 10:07Version 1.5Report generated
5297726PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
Diesel Range (C10-C28) 1000000 1040000 53300ug/L 4.40
Analyte Expected Found
* Exceeds
%D
Limit %D
RF
14G67518
WG613451
Instrument ID:HP14
File ID:
Run Date:05/09/2017
Run Time:14:09
Analyst:LJH
ICal Workgroup:
8015CMethod:
L17050904Login Number: WG613451-07Sample ID:
09-MAY-17HP14 -Cal ID:
QUCL20
Units
QC Key:STD
Page 158
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
LCS_LCS2 - Modified 03/06/2008
05/26/2017 14:28Report generated:5309109PDF File ID:
LABORATORY CONTROL SAMPLE (LCS)
Microbac Laboratories Inc.
1,1-Dichloroethene
1,2-Dichloroethane
Methyl Ethyl Ketone
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
LCS LCS2
4.01
1.54
5.32
2.70
2.37
2.22
2.08
0.870
1.31
0.804
20.1 20.9
20.8 21.1
18.6 19.6
21.1 21.6
20.4 20.9
21.2 21.7
18.9 19.3
21.4 21.6
20.6 20.8
21.8 22.0
Analytes %RPD
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
Found FoundKnown Known
100 105
104 105
93.0 98.1
105 108
102 105
106 108
94.3 96.3
107 108
103 104
109 110
% REC % REC
20
20
20
20
20
20
20
20
20
20
RPDLmt
%RecLimits
80
80
10
80
65
80
80
80
80
50
132
129
170
121
140
120
125
124
122
170
-
-
-
-
-
-
-
-
-
-
Q
Sample ID:
Sample ID:
WG615282-02
WG615282-03
LCS
LCS2
11M18568
11M18569
File ID:
File ID:
1,2-Dichloroethane-d4
Dibromofluoromethane
4-Bromofluorobenzene
Toluene-d8
LCS LCS2
105 107
101 106
106 106
107 108
Surogates% Recovery % Recovery
Surrogate Limits
80
86
86
88
120
118
115
110
-
-
-
-
Qualifier
PASS
PASS
PASS
PASS
Run Date:
Run Date:
05/23/2017 14:06
05/23/2017 14:35
WG615282
Instrument ID:HPMS11
Analyst:TMB/JDS
Workgroup (AAB#): ug/LUnits:
8260BMethod:TCLP LeachMatrix:
L17051231Login Number: 5030B/5030C/503Prep Method:
* EXCEEDS %REC LIMIT
# EXCEEDS RPD LIMIT
STDQC Key: STD82009Lot #:
Page 159
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
SURROGATES - Modified 03/06/2008
05/25/2017 09:29Report generated:5308033PDF File ID:
SURROGATE STANDARDS
Microbac Laboratories Inc.
L17051231-02
L17051231-04
L17051231-06
L17051231-08
L17051231-10
L17051231-12
L17051231-14
WG615091-01
WG615091-02
01
01
01
01
01
01
01
01
01
1 2 3 4 5 6Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1
2
3
4
5
6
-
-
-
-
-
-
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
p-Terphenyl-d14
Phenol-d5
8270Method:
HPMS12Instrument Id:
L17051231Login Number:
SoilMatrix:WG615227Workgroup (AAB#):
Underline = Result out of surrogate limits
101 77.8 67.6 86.7 92.1 69.3
85.5 84.2 69.3 89.2 80.3 67.6
91.0 83.7 66.8 86.5 76.4 65.4
83.4 81.7 62.9 84.5 75.9 62.2
70.9 57.1 45.1 60.2 79.1 43.6
87.9 82.1 62.5 88.7 77.3 59.8
54.9 64.3 46.1 72.5 68.3 49.0
105 85.6 72.2 88.2 97.5 74.0
84.5 79.7 68.6 81.7 80.9 67.7
19
30
25
23
18
24
-
-
-
-
-
-
122
115
121
120
137
113
Surrogates Surrogate Limits
DL = surrogate diluted out
HPMS12CAL ID: -10-APR-17
ND = surrogate not detected
Page 160
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/25/2017 09:26Report generated5309623PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
2,4-Dichlorophenol
2-Nitrophenol
4-Chloro-3-Methylphenol
Acenaphthene
Benzo[a]pyrene
Di-n-Octyl Phthalate
Fluoranthene
Diphenylamine/n-Nitrosodiphenylamine
Phenol
1,4-Dichlorobenzene
Hexachlorobutadiene
Pentachlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrophenol
4-Nitrophenol
Hexachlorocyclopentadiene
n-Nitrosodipropylamine
2-Methylphenol
3-,4-Methylphenol
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pyridine
2,4,5-Trichlorophenol
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
51100
52000
53200
48200
50200
47200
50600
48100
48100
48000
57600
49000
49200
61500
51500
64100
43500
44100
47100
50900
52100
47000
52200
46100
48700
0.280
0.204
0.316
1.25
1.10
1.62
1.15
0.653
1.60
1.47
0.166
0.126
0.386
0.180
0.446
0.279
0.634
0.939
1.35
0.455
0.209
0.555
0.357
1.54
0.391
2.11
3.91
6.32
3.66
0.347
5.63
1.11
3.89
3.76
4.04
15.2
1.94
1.57
22.9
3.04
28.3
13.1
11.9
5.72
1.80
4.28
6.00
4.46
7.73
2.50
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
12M62316
WG615400
Instrument ID:HPMS12
File ID:
Run Date:05/24/2017
Run Time:10:05
Analyst:MES
Workgroup (AAB#):
8270CMethod:
L17051231Login Number: WG615388-02Sample ID:
10-APR-17HPMS12 -Cal ID:
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UCL20
20
20
20
20
20
20
20
20
20
20
20
20
40
40
40
40
40
40
40
40
40
40
40
40
STDQC Key:
WATERMatrix:
Page 161
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/25/2017 09:28Report generated5308031PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
1,4-Dichlorobenzene
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2-Nitrophenol
4-Chloro-3-Methylphenol
Acenaphthene
Benzo[a]pyrene
Di-n-Octyl Phthalate
Fluoranthene
Hexachlorobutadiene
Diphenylamine/n-Nitrosodiphenylamine
Pentachlorophenol
Phenol
2,4-Dinitrophenol
4-Nitrophenol
Hexachlorocyclopentadiene
n-Nitrosodipropylamine
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
2,4,5-Trichlorophenol
2,4-Dimethylphenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitroaniline
3,3'-Dichlorobenzidine
3-,4-Methylphenol
3-Nitroaniline
4,6-Dinitro-2-Methylphenol
4-Bromophenyl Phenyl Ether
4-Chloroaniline
4-Chlorophenyl Phenyl Ether
4-Nitroaniline
Acenaphthylene
Anthracene
Benzo[a]anthracene
Benzo[b]fluoranthene
Benzo[ghi]perylene
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
49200
50300
49800
50900
53300
47200
51300
47400
50400
56800
48800
50400
48700
64700
53700
59200
40200
50900
47900
50100
49000
47300
50200
49000
47700
50800
50700
45900
53000
51000
50300
47900
59500
52200
53300
49900
48500
46800
48800
48600
48800
52200
1.51
0.395
0.273
0.200
0.316
1.23
1.12
1.63
1.15
0.164
0.663
0.130
1.62
0.190
0.465
0.257
0.595
0.305
1.36
1.56
0.393
0.325
0.448
0.341
1.25
1.54
0.714
0.978
0.377
0.421
1.44
0.411
0.130
0.204
0.115
0.630
0.388
2.00
1.14
1.19
1.22
1.02
1.65
0.588
0.389
1.71
6.53
5.67
2.55
5.26
0.827
13.6
2.39
0.738
2.53
29.4
7.31
18.3
19.7
1.88
4.18
0.244
2.07
5.33
0.306
1.94
4.58
1.59
1.48
8.13
5.97
1.92
0.606
4.17
19.0
4.43
6.68
0.224
2.99
6.49
2.32
2.76
2.39
4.35
Analyte Expected Found Q%DRF
12M62298
WG615227
Instrument ID:HPMS12
File ID:
Run Date:05/23/2017
Run Time:10:50
Analyst:SCB
Workgroup (AAB#):
8270CMethod:
L17051231Login Number: WG615240-02Sample ID:
10-APR-17HPMS12 -Cal ID:
UNITS
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
UCL20
20
20
20
20
20
20
20
20
20
20
20
20
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
STDQC Key:
WATERMatrix:
Page 162
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/25/2017 09:28Report generated5308031PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
Benzo[k]fluoranthene
Benzoic Acid
Benzyl Alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
bis(2-Ethylhexyl)phthalate
Butyl Benzyl Phthalate
Chrysene
Di-n-Butyl Phthalate
Dibenz[ah]anthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluorene
Hexachlorobenzene
Hexachloroethane
Indeno[1,2,3-cd]pyrene
Isophorone
Naphthalene
Nitrobenzene
Phenanthrene
Pyrene
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
45400
33100
49600
40700
45700
49600
47400
43200
48400
49000
55200
47600
49000
49200
49200
53800
51400
53400
48400
49100
49700
48700
47300
0.991
0.151
0.948
0.392
0.843
1.47
0.920
0.585
1.07
1.38
1.05
1.70
1.48
1.42
1.35
0.216
0.607
1.24
0.606
1.07
0.340
1.10
1.28
9.13
33.7
0.830
18.6
8.51
0.722
5.24
13.6
3.26
2.05
10.3
4.72
1.97
1.63
1.58
7.50
2.75
6.90
3.26
1.86
0.625
2.56
5.31
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
12M62298
WG615227
Instrument ID:HPMS12
File ID:
Run Date:05/23/2017
Run Time:10:50
Analyst:SCB
Workgroup (AAB#):
8270CMethod:
L17051231Login Number: WG615240-02Sample ID:
10-APR-17HPMS12 -Cal ID:
UNITS
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
UCL40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
STDQC Key:
WATERMatrix:
Page 163
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/26/2017 14:28Report generated5309112PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
1,2-Dichloropropane
Ethylbenzene
Toluene
Chloroform
1,1-Dichloroethene
Vinyl Chloride
1,1,2,2-Tetrachloroethane
1,1-Dichloroethane
Bromoform
Chloromethane
Chlorobenzene
Benzene
Carbon Tetrachloride
1,2-Dichloroethane
2-Butanone
Tetrachloroethene
Trichloroethene
CCC
CCC
CCC
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
SPCC
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.3
50.7
50.2
44.2
48.3
49.4
49.5
48.2
43.4
42.2
48.8
48.1
51.7
47.2
43.9
51.9
48.1
0.341
0.584
1.54
0.491
0.478
0.427
0.712
0.590
0.265
0.467
1.02
1.06
0.401
0.426
0.129
0.328
0.281
0.611
1.40
0.480
11.7
3.46
1.17
0.938
3.68
13.3
15.6
2.34
3.78
3.46
5.66
12.2
3.84
3.72
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
11M18564
WG615282
Instrument ID:HPMS11
File ID:
Run Date:05/23/2017
Run Time:12:27
Analyst:TMB
Workgroup (AAB#):
8260BMethod:
L17051231Login Number: WG615277-02Sample ID:
16-MAY-17HPMS11 -Cal ID:
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UCL20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
STDQC Key:
WATERMatrix:
Page 164
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/26/2017 14:28Report generated5309112PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
Analyte Expected Found Q* Exceeds
%D Criteria %D
RF
11M18566
WG615282
Instrument ID:HPMS11
File ID:
Run Date:05/23/2017
Run Time:13:08
Analyst:TMB/JDS
Workgroup (AAB#):
8260BMethod:
L17051231Login Number: WG615279-01Sample ID:
03-MAY-17HPMS11 -Cal ID:
UNITS UCL
STDQC Key:
WATERMatrix:
Page 165
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/26/2017 14:28Report generated5309112PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
1,2-Dichloropropane
Ethylbenzene
Toluene
Chloroform
1,1-Dichloroethene
Vinyl Chloride
1,1,2,2-Tetrachloroethane
1,1-Dichloroethane
Bromoform
Chloromethane
Chlorobenzene
Benzene
Carbon Tetrachloride
1,2-Dichloroethane
2-Butanone
Tetrachloroethene
Trichloroethene
CCC
CCC
CCC
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
SPCC
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
53.4
55.2
55.5
49.9
57.2
59.8
45.7
56.1
43.6
60.1
52.2
55.3
59.1
50.8
42.3
56.0
54.8
0.269
0.613
1.54
0.501
0.414
0.478
0.432
0.509
0.177
0.509
1.04
1.14
0.445
0.288
0.0467
0.327
0.318
*
6.72
10.5
10.9
0.218
14.5
19.7
8.51
12.2
12.9
20.2
4.49
10.6
18.3
1.53
15.3
12.0
9.51
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
8M419869
WG615405
Instrument ID:HPMS8
File ID:
Run Date:05/24/2017
Run Time:11:59
Analyst:TMB
Workgroup (AAB#):
8260BMethod:
L17051231Login Number: WG615404-02Sample ID:
17-APR-17HPMS8 -Cal ID:
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UCL20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
STDQC Key:
WATERMatrix:
Page 166
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/25/2017 09:25Version 1.5Report generated
5309621PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
1,4-Dichlorobenzene
Hexachlorobutadiene
Pentachlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrophenol
Hexachlorocyclopentadiene
4-Nitrophenol
n-Nitrosodipropylamine
2-Methylphenol
3-,4-Methylphenol
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pyridine
2,4,5-Trichlorophenol
CCC
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
49900
55900
63000
50800
59200
61400
53000
57900
50400
51600
52500
49400
49500
53400
53400
49200
1.53
0.161
0.162
0.398
0.172
0.267
0.459
0.790
1.07
1.47
0.469
0.198
0.585
0.366
1.78
0.395
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
0.300
11.9
26.1
1.60
18.4
22.8
6.00
15.7
0.900
3.20
4.90
1.30
1.00
6.90
6.80
1.60
Analyte Expected Found
* Exceeds
%D
Limit %D
RF
12M61777
WG609563
Instrument ID:HPMS12
File ID:
Run Date:04/10/2017
Run Time:21:31
Analyst:SCB
ICal Workgroup:
8270CMethod:
L17051231Login Number: WG609563-11Sample ID:
10-APR-17HPMS12 -Cal ID:
QUCL30
30
40
30
40
40
40
30
30
30
30
30
30
30
30
30
Units
QC Key:STD
Page 167
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CORR_FACTORS - Modified 03/05/2008
05/24/2017 11:13Report generated:5308569PDF File ID:
INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Microbac Laboratories Inc.
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
BORON
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
LITHIUM
MAGNESIUM
MANGANESE
MOLYBDENUM
NICKEL
PHOSPHORUS
POTASSIUM
SELENIUM
SILICON
SILVER
SODIUM
STRONTIUM
THALLIUM
TIN
TITANIUM
VANADIUM
ZINC
ZIRCONIUM
Analyte
308.20
206.80
189.00
455.40
313.10
249.60
228.80
422.60
267.70
228.60
224.70
261.10
220.30
670.70
279.10
257.60
202.00
231.60
214.90
766.40
196.10
212.40
328.10
589.50
407.70
190.80
189.90
337.20
292.40
206.20
339.10
Wave Length
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
ZR
Insturment ID:
Date:
Method:ICP-THERMO4
01/04/2017
6010B
Login Number:L17051231
Page 168
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/25/2017 09:28Version 1.5Report generated
5308029PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
Benzoic Acid
Benzyl Alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
bis(2-Ethylhexyl)phthalate
Butyl Benzyl Phthalate
Chrysene
Di-n-Butyl Phthalate
Dibenz[ah]anthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluorene
Hexachlorobenzene
Hexachloroethane
Indeno[1,2,3-cd]pyrene
Isophorone
Naphthalene
Nitrobenzene
Phenanthrene
Pyrene
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
47200
51300
51400
52000
50800
54000
51000
50600
52700
49900
50600
52800
52300
52600
49400
49500
49100
51400
50000
53400
48700
48200
0.232
0.981
0.474
0.957
1.51
1.05
0.690
1.12
1.49
0.953
1.80
1.59
1.51
1.44
0.198
0.585
1.14
0.644
1.09
0.366
1.10
1.31
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
5.70
2.50
2.70
3.90
1.50
7.90
2.00
1.10
5.40
0.200
1.30
5.50
4.60
5.20
1.30
1.00
1.70
2.80
0
6.90
2.60
3.60
Analyte Expected Found
* Exceeds
%D
Limit %D
RF
12M61777
WG609563
Instrument ID:HPMS12
File ID:
Run Date:04/10/2017
Run Time:21:31
Analyst:SCB
ICal Workgroup:
8270CMethod:
L17051231Login Number: WG609563-11Sample ID:
10-APR-17HPMS12 -Cal ID:
QUCL30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Units
QC Key:STD
Page 169
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID: 82374
Page: 1 Approved: May 24, 2017
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
ICP-THERMO4
KKB
200.7/6010B/6010C
052317T4.1R.TXT
N/A
ME600G 8
Calibration Std:
ICSA:
ICV Std:
ICSAB:
Post Spike:
Workgroups:
STD81957
STD81649
STD81979
STD81939
STD81528
615308,615115,615271,615275
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
T4.052317.141017
T4.052317.141400
T4.052317.141743
T4.052317.142128
T4.052317.142455
T4.052317.142822
T4.052317.143152
T4.052317.143535
T4.052317.143920
T4.052317.144300
T4.052317.144628
T4.052317.153305
T4.052317.153648
T4.052317.154016
T4.052317.154400
T4.052317.154743
T4.052317.155127
T4.052317.155507
T4.052317.155847
T4.052317.160229
T4.052317.160557
T4.052317.160939
T4.052317.161307
T4.052317.161653
T4.052317.162035
T4.052317.162415
T4.052317.162755
T4.052317.163134
T4.052317.163503
T4.052317.163831
T4.052317.164215
T4.052317.164558
T4.052317.164940
T4.052317.165324
WG615438-01
WG615438-02
WG615438-03
WG615438-04
WG615438-05
WG615438-06
WG615438-07
WG615438-08
WG615438-09
WG615438-10
WG615438-11
WG615215-02
WG615215-03
WG615014-01
WG615014-02
WG615014-03
L17051122-01
L17051160-01
L17051161-01
WG615308-01
WG615308-02
WG615438-12
WG615438-13
L17051162-01
L17051167-01
L17051167-02
WG615215-01
WG615215-04
WG615215-05
L17051170-01
L17051170-02
L17051231-01
L17051231-03
WG615438-14
Calibration Point
Calibration Point
Calibration Point
Calibration Point
Calibration Point
Initial Calibration Verification
Initial Calib Blank
Interference Check
Interference Check
CCV
CCB
Method/Prep Blank
Laboratory Control S
Fluid Blank 1
Fluid Blank 1
Fluid Blank 2
\#1 CELLAR DIRT
AWV 10 BAGS
SAPA 7 BAGS
Post Digestion Spike
Serial Dilution
CCV
CCB
KAISER 9 BAGS
WPAFB-SA-101
WPAFB-SA-102
Reference Sample
Matrix Spike
Matrix Spike Duplica
5/8 WASTE DRUM \#1
5/8 WASTE DRUM \#2
17-0751 OSG DISPOSAL PI
17-0751 IR MUD ORIGINAL
CCV
5/50
5/50
5/50
5/50
5/50
5/50
5/50
5/50
5/50
5/50
5/50
5/50
5/50
5/50
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
1
1
1
1
1
L17051161-01
L17051161-01
L17051167-03
L17051167-03
L17051167-03
05/23/17 14:10
05/23/17 14:14
05/23/17 14:17
05/23/17 14:21
05/23/17 14:24
05/23/17 14:28
05/23/17 14:31
05/23/17 14:35
05/23/17 14:39
05/23/17 14:43
05/23/17 14:46
05/23/17 15:33
05/23/17 15:36
05/23/17 15:40
05/23/17 15:44
05/23/17 15:47
05/23/17 15:51
05/23/17 15:55
05/23/17 15:58
05/23/17 16:02
05/23/17 16:05
05/23/17 16:09
05/23/17 16:13
05/23/17 16:16
05/23/17 16:20
05/23/17 16:24
05/23/17 16:27
05/23/17 16:31
05/23/17 16:35
05/23/17 16:38
05/23/17 16:42
05/23/17 16:45
05/23/17 16:49
05/23/17 16:53
Seq. File ID Sample ID Prep Dil Reference Date/Time
Comments:
Maintenance Log ID:
Int. Std: RGT39282
CCV: STD81717 COA19158LLCCV: Tuning Sol :
Stannous : Hydroxylamine :
Page 170
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
INTERNAL STANDARD AREA SUMMARY(COMPARED TO CCV)
INTERNAL_STD - Modified 03/06/2008
05/25/2017 09:26Report generated5309624PDF File ID:
Microbac Laboratories Inc.
L17051231-01
L17051231-03
L17051231-05
L17051231-07
L17051231-09
L17051231-11
L17051231-13
WG615097-01
WG615097-02
WG615216-01
WG615216-02
01
01
01
01
01
01
01
01
01
01
01
1 2 3 4 5 6
99379 185096 299893 368338 292656 314410
100414 164426 305392 369646 284088 312476
101237 168295 299488 337884 291478 326419
101050 166928 314177 333596 287340 315427
103302 187260 301163 382759 293979 345239
102788 170112 319126 371740 291431 323009
102941 185878 301302 380841 289977 343511
104843 191921 310692 390373 303833 358289
104813 174002 318860 344942 304969 324813
108833 187407 315435 396011 322065 359979
102537 181219 295395 362752 299904 327491
118542 206426 354369 405282 359204 380634WG615388-02
237084 412852 708738 810564 718408 761268
59271 103213 177185 202641 179602 190317
Upper Limit
Lower Limit
Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
NA
NA
NA
NA
NA
NA
1
2
3
4
5
6
-
-
-
-
-
-
1,4-Dichlorobenzene-d4
Acenaphthene-d10
Chrysene-d12
Naphthalene-d8
Perylene-d12
Phenanthrene-d10
WG615388-02CCV Number:
HPMS12Instrument ID:
L17051231Login Number:
TCLPMatrix:WG615400Workgroup (AAB#):
Underline = Response outside limits
HPMS12CAL ID:
IS- IS- IS- IS- IS- IS-
IS-
IS-
IS-
IS-
IS-
IS-
-10-APR-17
Page 171
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Calibration Table Report
Method: 8260WT.M
Title: 8260B/624 (SOP: OVL MSV01) Water 051617 HPMS11
Last Calibration: Wed May 17 12:46:08 2017
Curve: WG614378
Calibration Files
0.3 0.4 1 2 5 20 50 100 200 30011M18431.D 11M18432.D 11M18433.D 11M18434.D 11M18435.D 11M18436.D 11M18437.D 11M18438.D 11M18439.D 11M18440.D
Compound Avg %RSD Linear Quadratic
Fluorobenzene ISTD
Dichlorodifluoromethane 0.317 0.353 0.357 0.424 0.407 0.378 0.368 0.372 9.541
Chloromethane 0.560 0.639 0.584 0.630 0.536 0.486 0.439 0.553 13.227
Vinyl Chloride 0.498 0.417 0.470 0.439 0.478 0.442 0.375 0.336 0.432 12.564
1,3-Butadiene 0.343 0.282 0.295 0.228 0.162 0.153 0.130 0.227 36.032 1.002
Bromomethane 0.207 0.210 0.206 0.193 0.198 0.204 0.219 0.205 4.082
Chloroethane 0.219 0.239 0.241 0.249 0.245 0.237 0.248 0.240 4.259
Trichlorofluoromethane 0.441 0.417 0.471 0.462 0.480 0.472 0.439 0.448 0.454 4.729
Diethyl ether 0.273 0.297 0.290 0.286 0.284 0.278 0.284 0.285 2.761
Isoprene 0.305 0.365 0.389 0.401 0.441 0.443 0.441 0.439 0.403 12.220
Acrolein 0.029 0.040 0.038 0.039 0.040 0.042 0.042 0.039 11.129
1,1,2-Trichloro-1,2,2-Trifluoroethane 0.195 0.234 0.242 0.249 0.253 0.241 0.255 0.239 8.688
Acetone 0.089 0.093 0.091 0.092 0.093 0.097 0.090 0.092 2.806
1,1-Dichloroethene 0.473 0.457 0.486 0.517 0.521 0.518 0.495 0.494 0.495 4.648
Tert-Butyl Alcohol 0.023 0.027 0.027 0.028 0.031 0.032 0.028 11.816
Dimethyl Sulfide 0.287 0.297 0.340 0.336 0.357 0.356 0.352 0.351 0.334 8.216
Iodomethane 0.013 0.079 0.141 0.251 0.276 0.290 0.298 0.192 59.519 0.998
Methyl acetate 0.215 0.241 0.249 0.254 0.256 0.266 0.247 7.124
Methylene Chloride 0.335 0.334 0.310 0.314 0.305 0.293 0.302 0.313 5.038
Carbon Disulfide 0.710 0.770 0.789 0.834 0.806 0.757 0.688 0.765 6.757
Acrylonitrile 0.094 0.114 0.118 0.119 0.129 0.131 0.126 0.119 10.729
Methyl Tert Butyl Ether 0.745 0.695 0.766 0.793 0.821 0.803 0.773 0.768 0.771 5.035
trans-1,2-Dichloroethene 0.246 0.236 0.270 0.276 0.288 0.287 0.276 0.287 0.271 7.185
n-Hexane 0.407 0.430 0.467 0.476 0.471 0.467 0.453 6.165
Diisopropyl ether 1.117 1.264 1.233 1.203 1.164 1.017 0.915 1.130 11.071
Vinyl Acetate 0.479 0.533 0.487 0.517 0.535 0.472 0.424 0.492 8.019
1,1-Dichloroethane 0.640 0.593 0.611 0.604 0.645 0.631 0.596 0.577 0.612 3.958
Ethyl-Tert-Butyl ether 0.964 1.097 1.071 1.046 1.027 0.914 0.834 0.993 9.488
2-Butanone 0.137 0.139 0.143 0.147 0.152 0.157 0.155 0.147 5.313
Propionitrile 0.034 0.041 0.043 0.044 0.045 0.047 0.050 0.043 11.768
2,2-Dichloropropane 0.423 0.369 0.405 0.392 0.420 0.417 0.395 0.398 0.402 4.470
cis-1,2-Dichloroethene 0.316 0.262 0.294 0.319 0.332 0.328 0.315 0.320 0.311 7.292
Chloroform 0.668 0.681 0.536 0.542 0.526 0.550 0.525 0.494 0.481 0.556 12.730
1-Bromopropane 0.040 0.054 0.061 0.060 0.058 0.061 0.059 0.056 13.246
Bromochloromethane 0.129 0.172 0.187 0.196 0.199 0.196 0.192 0.198 0.184 12.931
Tetrahydrofuran 0.158 0.115 0.106 0.104 0.106 0.106 0.108 0.115 16.890 0.999
Dibromofluoromethane 0.280 0.262 0.272 0.271 0.260 0.269 3.091
1,1,1-Trichloroethane 0.415 0.399 0.423 0.462 0.483 0.485 0.463 0.464 0.449 7.243
Cyclohexane 0.581 0.524 0.578 0.607 0.650 0.644 0.623 0.599 0.540 0.594 7.282
1,1-Dichloropropene 0.331 0.335 0.357 0.372 0.408 0.407 0.386 0.387 0.373 7.978
Carbon Tetrachloride 0.304 0.349 0.379 0.396 0.420 0.430 0.409 0.410 0.387 10.874
Tert-Amyl-Methyl ether 0.714 0.837 0.823 0.816 0.803 0.73 0.677 0.77142 8.15202
1,2-Dichloroethane-d4 0.363 0.317 0.338 0.335 0.317 0.33379 5.69157
1,2-Dichloroethane 0.442 0.419 0.47 0.476 0.478 0.468 0.436 0.423 0.45135 5.33453
Benzene 1.156 1.084 1.179 1.185 1.199 1.141 1.011 0.878 1.104 10.0158
Trichloroethene 0.226 0.251 0.301 0.301 0.325 0.317 0.301 0.309 0.29146 11.7841
Methylcyclohexane 0.477 0.383 0.443 0.467 0.507 0.501 0.477 0.464 0.423 0.46019 8.49006
1,2-Dichloropropane 0.313 0.286 0.342 0.342 0.369 0.363 0.345 0.352 0.33917 8.04796
1,4-Dioxane 0.002 0.003 0.003 0.003 0.003 0.003 0.00293 13.9596
Bromodichloromethane 0.343 0.298 0.345 0.37 0.408 0.403 0.393 0.389 0.36867 10.1709
Dibromomethane 0.12 0.153 0.171 0.163 0.188 0.182 0.176 0.183 0.16712 13.2633
2-Chloroethyl Vinyl Ether 0.14 0.162 0.18 0.202 0.21 0.215 0.22 0.208 0.19218 14.9182
4-Methyl-2-Pentanone 0.099 0.116 0.122 0.127 0.138 0.133 0.12257 11.2898
cis-1,3-Dichloropropene 0.334 0.303 0.37 0.402 0.455 0.472 0.45 0.443 0.40378 15.4416 0.999
Dimethyl Disulfide 0.147 0.173 0.237 0.271 0.28 0.288 0.269 0.23782 23.5484 0.999
Chlorobenzene-d5 ISTD
Toluene-d8 1.507 1.348 1.404 1.335 1.146 1.34813 9.77146
Toluene 2.389 1.827 1.753 1.819 1.767 1.658 1.41 1.80307 16.3818 0.991
Ethyl Methacrylate 0.303 0.369 0.419 0.482 0.512 0.503 0.484 0.461 0.44178 16.5839 0.998
trans-1,3-Dichloropropene 0.496 0.468 0.517 0.577 0.593 0.574 0.53 0.53644 8.70041
1,1,2-Trichloroethane 0.319 0.306 0.337 0.349 0.367 0.361 0.35 0.342 0.34131 5.95867
2-Hexanone 0.257 0.302 0.314 0.319 0.323 0.318 0.30532 8.13831
1,3-Dichloropropane 0.632 0.563 0.598 0.616 0.627 0.611 0.573 0.539 0.59471 5.61804
Tetrachloroethene 0.237 0.276 0.301 0.34 0.35 0.354 0.336 0.331 0.31574 13.0405
Dibromochloromethane 0.302 0.303 0.328 0.364 0.422 0.438 0.419 0.416 0.37379 15.2048 0.999
1,2-Dibromoethane 0.218 0.277 0.297 0.323 0.336 0.338 0.324 0.324 0.30457 13.3219
1-Chlorohexane 0.435 0.368 0.42 0.471 0.528 0.54 0.528 0.493 0.454 0.47077 12.2378
Chlorobenzene 1.06 1.029 1.093 1.095 1.14 1.091 0.982 0.852 1.04267 8.68375
1,1,1,2-Tetrachloroethane 0.333 0.343 0.376 0.375 0.422 0.428 0.418 0.412 0.38822 9.55907
Ethylbenzene 0.49 0.553 0.573 0.617 0.631 0.597 0.568 0.5756 8.15775
m-,p-Xylene 0.624 0.61 0.662 0.73 0.738 0.723 0.635 0.52 0.6552 11.3677
o-Xylene 0.611 0.542 0.601 0.714 0.734 0.742 0.699 0.654 0.66201 10.9201
Styrene 0.915 0.841 0.944 1.039 1.186 1.213 1.116 0.962 1.02697 13.0703
Bromoform 0.169 0.221 0.229 0.278 0.299 0.304 0.316 0.25955 20.9192 0.999
Isopropylbenzene 1.54 1.47 1.654 1.773 1.858 1.79 1.534 1.228 1.60558 12.8593
1,4-Dichlorobenzene-d4 ISTD
1,1,2,2-Tetrachloroethane 0.602 0.603 0.738 0.784 0.799 0.755 0.759 0.712 0.71899 10.6759
p-Bromofluorobenzene 0.94 0.932 0.941 0.959 0.874 0.92914 3.499
1,2,3-Trichloropropane 0.192 0.203 0.227 0.25 0.237 0.238 0.241 0.22684 9.47455
trans-1,4-Dichloro-2-Butene 0.145 0.197 0.252 0.276 0.273 0.283 0.283 0.259 0.24598 20.0146 0.998
R^2
Page 172
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
n-Propylbenzene 3.443 3.25 3.731 4.084 4.255 3.72 3.078 3.6516 11.7041
Bromobenzene 0.765 0.798 0.769 0.857 0.913 0.978 0.915 0.884 0.825 0.85586 8.52037
1,3,5-Trimethylbenzene 2.528 2.343 2.64 2.841 3.025 2.723 2.375 1.866 2.54273 14.0286
2-Chlorotoluene 2.677 2.489 2.82 2.937 3.017 2.639 2.322 1.813 2.58925 14.9669
4-Chlorotoluene 1.945 1.885 2.066 2.17 2.308 2.123 1.844 1.421 1.97015 13.7289
a-Methylstyrene 1.273 1.545 1.523 1.47 1.247 1.119 1.36309 12.7744
tert-Butylbenzene 0.452 0.537 0.622 0.676 0.646 0.63 0.606 0.59568 12.8233
1,2,4-Trimethylbenzene 2.375 2.721 2.996 3.128 2.834 2.449 2.75056 10.8088
sec-Butylbenzene 2.835 3.307 3.628 3.804 3.444 2.938 3.32593 11.4512
p-Isopropyltoluene 2.257 2.755 2.988 3.212 2.941 2.558 2.7853 12.2258
1,3-Dichlorobenzene 1.381 1.452 1.581 1.675 1.801 1.669 1.574 1.332 1.5582 10.2657
1,4-Dichlorobenzene 1.654 1.501 1.619 1.747 1.774 1.655 1.555 1.316 1.60264 9.16319
n-Butylbenzene 2.011 2.347 2.567 2.939 2.747 2.426 2.50625 12.9532
1,2-Dichlorobenzene 1.749 1.667 1.454 1.685 1.649 1.757 1.617 1.532 1.299 1.60101 9.3155
1,2-Dibromo-3-Chloropropane 0.092 0.133 0.151 0.154 0.157 0.168 0.14243 19.0803 0.999
1,2,4-Trichlorobenzene 0.9 0.961 1.064 1.102 1.251 1.175 1.143 1.07 1.08325 10.4409
Hexachlorobutadiene 0.336 0.503 0.513 0.584 0.642 0.617 0.623 0.616 0.55426 18.444 1
Naphthalene 2.035 1.958 2.204 2.525 2.772 2.535 2.227 1.831 2.26105 14.3669
1,2,3-Trichlorobenzene 0.922 0.878 0.94 1.027 1.136 1.237 1.159 1.103 1.065 1.05185 11.4386
Thu May 18 10:46:55 2017
Page 173
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Calibration Table Report
Method: A9FOOWT.M
Title: A9-FOO Water SOP:MSV01 04-12-17 HPMS8
Last Calibration: Thu Apr 13 16:40:13 2017
Curve: WG609829
Calibration Files
5 20 50 100 200 300 400 5008M418916.D 8M418917.D 8M418918.D 8M418919.D 8M418920.D 8M418921.D 8M418922.D 8M418923.D
Compound Avg %RSD
I Fluorobenzene ISTDT Acetonitrile 0.013 0.012 0.013 0.013 0.012 0.013 0.013 0.013 3.572T 3-Chloro-1-propene 0.312 0.315 0.327 0.337 0.346 0.341 0.344 0.341 0.333 3.984T 2-Chloro-1,3-butadiene 0.285 0.299 0.317 0.330 0.340 0.336 0.337 0.336 0.322 6.267T Ethyl Acetate 0.099 0.101 0.098 0.101 0.108 0.103 0.106 0.109 0.103 4.045T Methacrylonitrile 0.052 0.059 0.057 0.059 0.064 0.061 0.063 0.065 0.060 7.025T Isobutyl Alcohol 0.003 0.004 0.004 0.004 0.005 0.005 0.004 12.096T 1-Butanol 0.000 0.000T Methyl methacrylate 0.096 0.101 0.103 0.107 0.116 0.112 0.116 0.121 0.109 7.922T 2-Nitropropane 0.027 0.028 0.031 0.034 0.034 0.035 0.037 0.032 11.358I Chlorobenzene-d5 ISTDI 1,4-Dichlorobenzene-d4 ISTDT Cyclohexanone 0.006 0.006 0.007 0.008 0.007 0.008 0.009 0.007 13.841
Mon Apr 17 15:45:45 2017
Page 174
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Page 175
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
05/17/2017 10:07Report generated5297722PDF File ID:
Microbac Laboratories Inc.
METHOD BLANK SUMMARY
Report Name: BLANK_SUMMARY
14G67536
05/16/17 11:21
05/16/17 14:27
WG614544
WG614301-01
HP14
Blank File ID:
Prep Date:
Analyzed Date:
Work Group:
Blank Sample ID:
Instrument ID:
8015CMethod:
LJHAnalyst:
L17050904Login Number:
LCS
LCS2
17-0751 IR MUD 54 RETURN
17-0751 IR MUD SILO
17-0751 IR MUD WE RECLAIM PIT
17-0751 IR MUD BREAKOUT
17-0751 IR MUD GRID C1-D1
WG614301-02
WG614301-03
L17050904-03
L17050904-01
L17050904-04
L17050904-05
L17050904-02
14G67537
14G67538
14G67540
14G67541
14G67542
14G67543
14G67544
05/16/17 15:06
05/16/17 15:45
05/16/17 17:04
05/16/17 17:43
05/16/17 18:22
05/16/17 19:02
05/16/17 19:41
This Method Blank Applies To The Following Samples:
Client ID Lab Sample ID Lab File ID Time Analyzed TAG
01
01
01
01
01
01
01
Page 176
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Microbac Laboratories Inc.
METHOD BLANK REPORT
Report Name:BLANK
PDF ID: 5297723
17-MAY-2017 10:07
o-Terphenyl
Octacosane
69.6
62.6
Surrogates % Recovery Surrogate Limits
43
25
-
-
136
162
Qualifier
PASS
PASS
Analytes Concentration Dilution Qualifier
Diesel Range (C10-C28) 12500 10000 J3900
ND Analyte Not detected at or above reporting limit
* |Analyte concentration| > RL
14G67536
WG614544
Instrument ID:HP14
File ID:
Prep Date:05/16/17 11:21
Run Date:05/16/17 14:27
Analyst:LJH
Workgroup (AAB#): ug/kgUnits:
8015CMethod:
SoilMatrix:
L17050904Login Number: WG614301-01Sample ID:
09-MAY-17Cal ID: HP14-OT900917Contract #:
3546Prep Method:
MDL RL
MDL
RL
Method Detection Limit
Reporting/Practical Quantitation Limit
Page 177
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
LCS_LCS2 - Modified 03/06/2008
05/17/2017 10:07Report generated:5297724PDF File ID:
LABORATORY CONTROL SAMPLE (LCS)
Microbac Laboratories Inc.
Diesel Range (C10-C28)
LCS LCS2
4.13137000 143000
Analytes %RPD
250000 250000
Found FoundKnown Known
54.9 57.2
% REC % REC
26
RPDLmt
%RecLimits
35 120-
Q
Sample ID:
Sample ID:
WG614301-02
WG614301-03
LCS
LCS2
14G67537
14G67538
File ID:
File ID:
o-Terphenyl
Octacosane
LCS LCS2
69.7 73.4
68.2 74.9
Surogates% Recovery % Recovery
Surrogate Limits
43
25
136
162
-
-
Qualifier
PASS
PASS
Run Date:
Run Date:
05/16/2017 15:06
05/16/2017 15:45
WG614544
Instrument ID:HP14
Analyst:LJH
Workgroup (AAB#): ug/kgUnits:
8015CMethod:SoilMatrix:
L17050904Login Number: 3546Prep Method:
* EXCEEDS %REC LIMIT
# EXCEEDS RPD LIMIT
STDQC Key: STD81195Lot #:
Page 178
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
SURROGATES - Modified 03/06/2008
05/17/2017 10:07Report generated:5297728PDF File ID:
SURROGATE STANDARDS
Microbac Laboratories Inc.
L17050904-01
L17050904-02
L17050904-03
L17050904-04
L17050904-05
WG614301-01
WG614301-02
WG614301-03
01
01
01
01
01
01
01
01
1 2Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1
2
-
-
o-Terphenyl
Octacosane
8015Method:
HP14Instrument Id:
L17050904Login Number:
SoilMatrix:WG614544Workgroup (AAB#):
Underline = Result out of surrogate limits
26.2 36.2
12.6 9.41
53.4 52.3
30.9 30.4
39.5 34.6
69.6 62.6
69.7 68.2
73.4 74.9
43
25
-
-
136
162
Surrogates Surrogate Limits
DL = surrogate diluted out
HP14CAL ID: -09-MAY-17
ND = surrogate not detected
Page 179
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/17/2017 10:07Report generated5297727PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
Diesel Range (C10-C28) 1000000 1000000 51200 0.384
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
14G67535
WG614544
Instrument ID:HP14
File ID:
Run Date:05/16/2017
Run Time:09:32
Analyst:LJH
Workgroup (AAB#):
8015CMethod:
L17050904Login Number: WG614359-01Sample ID:
09-MAY-17HP14 -Cal ID:
UNITS
ug/kg
UCL20
STDQC Key:
WATERMatrix:
Page 180
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/17/2017 10:07Report generated5297727PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
Diesel Range (C10-C28) 1000000 1040000 53300 4.46
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
14G67546
WG614544
Instrument ID:HP14
File ID:
Run Date:05/16/2017
Run Time:20:59
Analyst:LJH
Workgroup (AAB#):
8015CMethod:
L17050904Login Number: WG614359-02Sample ID:
09-MAY-17HP14 -Cal ID:
UNITS
ug/kg
UCL20
STDQC Key:
WATERMatrix:
Page 181
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/24/2017 11:14Report generated5308574PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
0.400
1.00
0.0500
0.500
0.500
0.400
0.400
0.398
1.01
0.0503
0.506
0.504
0.407
0.405
99.5
101
101
101
101
102
101
90 - 110
90 - 110
90 - 110
90 - 110
90 - 110
90 - 110
90 - 110
Analyte Expected Found Q
* Exceeds
LIMITS
Criteria LIMITS
%REC
T4.052317.165324
WG615308
Instrument ID:ICP-THERMO4
File ID:
Run Date:05/23/2017
Run Time:16:53
Analyst:KKB
Workgroup (AAB#):
6010BMethod:
L17051231Login Number: WG615438-14Sample ID:
23-MAY-17ICP-TH -Cal ID:
UNITS
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
STDQC Key:
WATERMatrix:
Page 182
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/24/2017 11:14Report generated5308574PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
0.400
1.00
0.0500
0.500
0.500
0.400
0.400
0.397
1.01
0.0508
0.506
0.511
0.402
0.402
99.2
101
102
101
102
100
100
90 - 110
90 - 110
90 - 110
90 - 110
90 - 110
90 - 110
90 - 110
Analyte Expected Found Q
* Exceeds
LIMITS
Criteria LIMITS
%REC
T4.052317.171908
WG615308
Instrument ID:ICP-THERMO4
File ID:
Run Date:05/23/2017
Run Time:17:19
Analyst:KKB
Workgroup (AAB#):
6010BMethod:
L17051231Login Number: WG615438-16Sample ID:
23-MAY-17ICP-TH -Cal ID:
UNITS
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
STDQC Key:
WATERMatrix:
Page 183
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCB - Modified 03/05/2008
05/24/2017 11:14Report generated5308575PDF File ID:
CONTINUING CALIBRATION BLANK (CCB)
Microbac Laboratories Inc.
Analytes MDL RDL Concentration Qualifier
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
0.0500
0.00500
0.00500
0.0100
0.0500
0.0400
0.00500
0.100
0.0100
0.0100
0.0200
0.100
0.0800
0.0100
0.0500
0.00500
0.00500
0.0100
0.0500
0.0400
0.00500
T4.052317.144628
WG615308
Instrument ID:ICP-THERMO4
File ID:
Run Date:05/23/2017
Run Time:14:46
Analyst:KKB
Workgroup (AAB#):
mg/LUnits:
6010BMethod:
L17051231Login Number: WG615438-11Sample ID:
U
U
U
U
U
U
U
U = Result is less than MDL.F = Result is between MDL and RL.
23-MAY-17ICP-TH -Cal ID:
* = Result is above RL.
WATERMatrix: QAPP:STD
Page 184
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCB - Modified 03/05/2008
05/24/2017 11:14Report generated5308575PDF File ID:
CONTINUING CALIBRATION BLANK (CCB)
Microbac Laboratories Inc.
Analytes MDL RDL Concentration Qualifier
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
0.0500
0.00500
0.00500
0.0100
0.0500
0.0400
0.00500
0.100
0.0100
0.0100
0.0200
0.100
0.0800
0.0100
0.0500
0.00500
0.00500
0.0100
0.0500
0.0400
0.00500
T4.052317.161307
WG615308
Instrument ID:ICP-THERMO4
File ID:
Run Date:05/23/2017
Run Time:16:13
Analyst:KKB
Workgroup (AAB#):
mg/LUnits:
6010BMethod:
L17051231Login Number: WG615438-13Sample ID:
U
U
U
U
U
U
U
U = Result is less than MDL.F = Result is between MDL and RL.
23-MAY-17ICP-TH -Cal ID:
* = Result is above RL.
WATERMatrix: QAPP:STD
Page 185
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/17/2017 10:07Version 1.5Report generated
5297726PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
Diesel Range (C10-C28) 1000000 1040000 53300ug/L 4.40
Analyte Expected Found
* Exceeds
%D
Limit %D
RF
14G67518
WG613451
Instrument ID:HP14
File ID:
Run Date:05/09/2017
Run Time:14:09
Analyst:LJH
ICal Workgroup:
8015CMethod:
L17050904Login Number: WG613451-07Sample ID:
09-MAY-17HP14 -Cal ID:
QUCL20
Units
QC Key:STD
Page 186
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
LCS_LCS2 - Modified 03/06/2008
05/26/2017 14:28Report generated:5309109PDF File ID:
LABORATORY CONTROL SAMPLE (LCS)
Microbac Laboratories Inc.
1,1-Dichloroethene
1,2-Dichloroethane
Methyl Ethyl Ketone
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
LCS LCS2
4.01
1.54
5.32
2.70
2.37
2.22
2.08
0.870
1.31
0.804
20.1 20.9
20.8 21.1
18.6 19.6
21.1 21.6
20.4 20.9
21.2 21.7
18.9 19.3
21.4 21.6
20.6 20.8
21.8 22.0
Analytes %RPD
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
20.0 20.0
Found FoundKnown Known
100 105
104 105
93.0 98.1
105 108
102 105
106 108
94.3 96.3
107 108
103 104
109 110
% REC % REC
20
20
20
20
20
20
20
20
20
20
RPDLmt
%RecLimits
80
80
10
80
65
80
80
80
80
50
132
129
170
121
140
120
125
124
122
170
-
-
-
-
-
-
-
-
-
-
Q
Sample ID:
Sample ID:
WG615282-02
WG615282-03
LCS
LCS2
11M18568
11M18569
File ID:
File ID:
1,2-Dichloroethane-d4
Dibromofluoromethane
4-Bromofluorobenzene
Toluene-d8
LCS LCS2
105 107
101 106
106 106
107 108
Surogates% Recovery % Recovery
Surrogate Limits
80
86
86
88
120
118
115
110
-
-
-
-
Qualifier
PASS
PASS
PASS
PASS
Run Date:
Run Date:
05/23/2017 14:06
05/23/2017 14:35
WG615282
Instrument ID:HPMS11
Analyst:TMB/JDS
Workgroup (AAB#): ug/LUnits:
8260BMethod:TCLP LeachMatrix:
L17051231Login Number: 5030B/5030C/503Prep Method:
* EXCEEDS %REC LIMIT
# EXCEEDS RPD LIMIT
STDQC Key: STD82009Lot #:
Page 187
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
SURROGATES - Modified 03/06/2008
05/25/2017 09:29Report generated:5308033PDF File ID:
SURROGATE STANDARDS
Microbac Laboratories Inc.
L17051231-02
L17051231-04
L17051231-06
L17051231-08
L17051231-10
L17051231-12
L17051231-14
WG615091-01
WG615091-02
01
01
01
01
01
01
01
01
01
1 2 3 4 5 6Sample Number Dilution Tag
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1
2
3
4
5
6
-
-
-
-
-
-
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
p-Terphenyl-d14
Phenol-d5
8270Method:
HPMS12Instrument Id:
L17051231Login Number:
SoilMatrix:WG615227Workgroup (AAB#):
Underline = Result out of surrogate limits
101 77.8 67.6 86.7 92.1 69.3
85.5 84.2 69.3 89.2 80.3 67.6
91.0 83.7 66.8 86.5 76.4 65.4
83.4 81.7 62.9 84.5 75.9 62.2
70.9 57.1 45.1 60.2 79.1 43.6
87.9 82.1 62.5 88.7 77.3 59.8
54.9 64.3 46.1 72.5 68.3 49.0
105 85.6 72.2 88.2 97.5 74.0
84.5 79.7 68.6 81.7 80.9 67.7
19
30
25
23
18
24
-
-
-
-
-
-
122
115
121
120
137
113
Surrogates Surrogate Limits
DL = surrogate diluted out
HPMS12CAL ID: -10-APR-17
ND = surrogate not detected
Page 188
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
CCV - Modified 03/05/2008
05/25/2017 09:26Report generated5309623PDF File ID:
CONTINUING CALIBRATION VERIFICATION (CCV)
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
2,4-Dichlorophenol
2-Nitrophenol
4-Chloro-3-Methylphenol
Acenaphthene
Benzo[a]pyrene
Di-n-Octyl Phthalate
Fluoranthene
Diphenylamine/n-Nitrosodiphenylamine
Phenol
1,4-Dichlorobenzene
Hexachlorobutadiene
Pentachlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrophenol
4-Nitrophenol
Hexachlorocyclopentadiene
n-Nitrosodipropylamine
2-Methylphenol
3-,4-Methylphenol
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pyridine
2,4,5-Trichlorophenol
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
51100
52000
53200
48200
50200
47200
50600
48100
48100
48000
57600
49000
49200
61500
51500
64100
43500
44100
47100
50900
52100
47000
52200
46100
48700
0.280
0.204
0.316
1.25
1.10
1.62
1.15
0.653
1.60
1.47
0.166
0.126
0.386
0.180
0.446
0.279
0.634
0.939
1.35
0.455
0.209
0.555
0.357
1.54
0.391
2.11
3.91
6.32
3.66
0.347
5.63
1.11
3.89
3.76
4.04
15.2
1.94
1.57
22.9
3.04
28.3
13.1
11.9
5.72
1.80
4.28
6.00
4.46
7.73
2.50
Analyte Expected Found Q
* Exceeds
%D
Criteria %D
RF
12M62316
WG615400
Instrument ID:HPMS12
File ID:
Run Date:05/24/2017
Run Time:10:05
Analyst:MES
Workgroup (AAB#):
8270CMethod:
L17051231Login Number: WG615388-02Sample ID:
10-APR-17HPMS12 -Cal ID:
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UCL20
20
20
20
20
20
20
20
20
20
20
20
20
40
40
40
40
40
40
40
40
40
40
40
40
STDQC Key:
WATERMatrix:
Page 189
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Instrument Run Log
Run Log ID: 82367
Page: 2 Approved: May 24, 2017
Microbac Laboratories Inc.
Instrument:
Analyst1:
Method:
Dataset:
Analyst2:
SOP: Rev:
CVAA1
LSJ
7470A/245.1
052317C.CSV
N/A
404 17
Calibration Std:
ICSA:
ICV Std:
ICSAB:
Post Spike:
Workgroups:
STD82023
N/A
STD82017
N/A
STD82023
615228
35
36
37
38
39
40
41
42
M7.052317.155351
M7.052317.155624
M7.052317.155857
M7.052317.160130
M7.052317.160401
M7.052317.160631
M7.052317.160904
M7.052317.161135
L17051231-03
L17051231-05
L17051231-07
L17051231-09
L17051231-11
L17051231-13
WG615387-15
WG615387-16
17-0751 IR MUD ORIGINAL
17-0751 IR MUD SILO
17-0751 IR MUD GRID A3 NE
17-0751 WEST BOREHOLE
17-0751 WEST RECLAIMER
17-0751 EAST RECLAIMER
CCV
CCB
4/40
4/40
4/40
4/40
4/40
4/40
1
1
1
1
1
1
1
1
05/23/17 15:53
05/23/17 15:56
05/23/17 15:58
05/23/17 16:01
05/23/17 16:04
05/23/17 16:06
05/23/17 16:09
05/23/17 16:11
Seq. File ID Sample ID Prep Dil Reference Date/Time
Comments:
Maintenance Log ID:
Int. Std:
CCV: LLCCV: Tuning Sol :
RGT39471 Stannous : RGT39469Hydroxylamine :
Page 190
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Page 191
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
ALT - Modified 09/06/2007
05/25/2017 09:25Version 1.5Report generated
5309621PDF File ID:
ALTERNATE SOURCE CALIBRATION REPORT
Microbac Laboratories Inc.
CCC Calibration Check CompoundsSPCC System Performance Check Compounds
1,4-Dichlorobenzene
Hexachlorobutadiene
Pentachlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrophenol
Hexachlorocyclopentadiene
4-Nitrophenol
n-Nitrosodipropylamine
2-Methylphenol
3-,4-Methylphenol
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pyridine
2,4,5-Trichlorophenol
CCC
CCC
CCC
CCC
SPCC
SPCC
SPCC
SPCC
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
49900
55900
63000
50800
59200
61400
53000
57900
50400
51600
52500
49400
49500
53400
53400
49200
1.53
0.161
0.162
0.398
0.172
0.267
0.459
0.790
1.07
1.47
0.469
0.198
0.585
0.366
1.78
0.395
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
0.300
11.9
26.1
1.60
18.4
22.8
6.00
15.7
0.900
3.20
4.90
1.30
1.00
6.90
6.80
1.60
Analyte Expected Found
* Exceeds
%D
Limit %D
RF
12M61777
WG609563
Instrument ID:HPMS12
File ID:
Run Date:04/10/2017
Run Time:21:31
Analyst:SCB
ICal Workgroup:
8270CMethod:
L17051231Login Number: WG609563-11Sample ID:
10-APR-17HPMS12 -Cal ID:
QUCL30
30
40
30
40
40
40
30
30
30
30
30
30
30
30
30
Units
QC Key:STD
Page 192
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Page 193
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Page 194
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Internal Chain of Custody Report
Login:
Account:
Project:
Samples:
Due Date:
L17051231
2755
2755.044
14
24-MAY-2017
A1 - Sample Archive (COLD)A2 - Sample Archive (AMBIENT)F1 - Volatiles Freezer in LoginV1 - Volatiles Refrigerator in LoginW1 - Walkin Cooler in Login
Microbac Laboratories Inc.
L17051231-01
L17051231-02
L17051231-02
L17051231-03
L17051231-04
911918
911919
911920
911921
911922
Samplenum
Samplenum
Samplenum
Samplenum
Samplenum
Container ID
Container ID
Container ID
Container ID
Container ID
1
1
1
1
1
Bottle:
Bottle:
Bottle:
Bottle:
Bottle:
1
2
3
1
2
1
2
3
4
1
2
3
1
2
LOGIN
PREP
STORE
LOGIN
ANALYZ
LOGIN
PREP
PREP
STORE
LOGIN
PREP
STORE
LOGIN
ANALYZ
COOLER
W1
TCL
COOLER
V1
COOLER
W1
EXT
DIG
COOLER
W1
TCL
COOLER
V1
W1
TCL
A2
V1
ORG4
W1
EXT
DIG
A2
W1
TCL
A2
V1
ORG4
22-MAY-2017 10:46
22-MAY-2017 11:26
22-MAY-2017 15:43
22-MAY-2017 10:46
22-MAY-2017 10:57
22-MAY-2017 10:46
22-MAY-2017 11:53
22-MAY-2017 14:59
22-MAY-2017 16:26
22-MAY-2017 10:46
22-MAY-2017 11:26
22-MAY-2017 15:43
22-MAY-2017 10:46
22-MAY-2017 10:57
CLS
BNB
BRG
CLS
JDS
CLS
CPD
ZTB
CLS
CLS
BNB
BRG
CLS
JDS
BRG
BNB
CLS
CLS
JDH
AC
BRG
BNB
CLS
Seq.
Seq.
Seq.
Seq.
Seq.
Purpose
Purpose
Purpose
Purpose
Purpose
From
From
From
From
From
To
To
To
To
To
Date/Time
Date/Time
Date/Time
Date/Time
Date/Time
Accept
Accept
Accept
Accept
Accept
Relinquish
Relinquish
Relinquish
Relinquish
Relinquish
Products
Products
Products
Products
Products
TC-EX
8260
8270
TC-EX
8260
pH
pH
pH
pH
pH
Page 195
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Internal Chain of Custody Report
Login:
Account:
Project:
Samples:
Due Date:
L17051231
2755
2755.044
14
24-MAY-2017
A1 - Sample Archive (COLD)A2 - Sample Archive (AMBIENT)F1 - Volatiles Freezer in LoginV1 - Volatiles Refrigerator in LoginW1 - Walkin Cooler in Login
Microbac Laboratories Inc.
L17051231-04
L17051231-05
L17051231-06
L17051231-06
911923
911924
911925
911926
Samplenum
Samplenum
Samplenum
Samplenum
Container ID
Container ID
Container ID
Container ID
1
1
1
1
Bottle:
Bottle:
Bottle:
Bottle:
1
2
3
4
1
2
3
1
2
1
2
3
4
LOGIN
PREP
PREP
STORE
LOGIN
PREP
STORE
LOGIN
ANALYZ
LOGIN
PREP
PREP
STORE
COOLER
W1
EXT
DIG
COOLER
W1
TCL
COOLER
V1
COOLER
W1
EXT
DIG
W1
EXT
DIG
A2
W1
TCL
A2
V1
ORG4
W1
EXT
DIG
A2
22-MAY-2017 10:46
22-MAY-2017 11:53
22-MAY-2017 14:59
22-MAY-2017 16:26
22-MAY-2017 10:46
22-MAY-2017 11:26
22-MAY-2017 15:42
22-MAY-2017 10:46
22-MAY-2017 10:57
22-MAY-2017 10:46
22-MAY-2017 11:55
22-MAY-2017 14:59
22-MAY-2017 16:26
CLS
CPD
ZTB
CLS
CLS
BNB
BRG
CLS
JDS
CLS
CPD
ZTB
CLS
CLS
JDH
AC
BRG
BNB
CLS
CLS
JDH
AC
Seq.
Seq.
Seq.
Seq.
Purpose
Purpose
Purpose
Purpose
From
From
From
From
To
To
To
To
Date/Time
Date/Time
Date/Time
Date/Time
Accept
Accept
Accept
Accept
Relinquish
Relinquish
Relinquish
Relinquish
Products
Products
Products
Products
8270
TC-EX
8260
8270
pH
pH
pH
pH
Page 196
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Internal Chain of Custody Report
Login:
Account:
Project:
Samples:
Due Date:
L17051231
2755
2755.044
14
24-MAY-2017
A1 - Sample Archive (COLD)A2 - Sample Archive (AMBIENT)F1 - Volatiles Freezer in LoginV1 - Volatiles Refrigerator in LoginW1 - Walkin Cooler in Login
Microbac Laboratories Inc.
L17051231-07
L17051231-08
L17051231-08
L17051231-09
L17051231-10
911927
911928
911929
911930
911931
Samplenum
Samplenum
Samplenum
Samplenum
Samplenum
Container ID
Container ID
Container ID
Container ID
Container ID
1
1
1
1
1
Bottle:
Bottle:
Bottle:
Bottle:
Bottle:
1
2
3
1
2
1
2
3
4
1
2
3
1
2
LOGIN
PREP
STORE
LOGIN
ANALYZ
LOGIN
PREP
PREP
STORE
LOGIN
PREP
STORE
LOGIN
ANALYZ
COOLER
W1
TCL
COOLER
V1
COOLER
W1
EXT
DIG
COOLER
W1
TCL
COOLER
V1
W1
TCL
A2
V1
ORG4
W1
EXT
DIG
A2
W1
TCL
A2
V1
ORG4
22-MAY-2017 10:46
22-MAY-2017 11:26
22-MAY-2017 15:43
22-MAY-2017 10:46
22-MAY-2017 10:57
22-MAY-2017 10:46
22-MAY-2017 11:53
22-MAY-2017 14:59
22-MAY-2017 16:25
22-MAY-2017 10:46
22-MAY-2017 11:26
22-MAY-2017 15:42
22-MAY-2017 10:46
22-MAY-2017 10:57
CLS
BNB
BRG
CLS
JDS
CLS
CPD
ZTB
CLS
CLS
BNB
BRG
CLS
JDS
BRG
BNB
CLS
CLS
JDH
AC
BRG
BNB
CLS
Seq.
Seq.
Seq.
Seq.
Seq.
Purpose
Purpose
Purpose
Purpose
Purpose
From
From
From
From
From
To
To
To
To
To
Date/Time
Date/Time
Date/Time
Date/Time
Date/Time
Accept
Accept
Accept
Accept
Accept
Relinquish
Relinquish
Relinquish
Relinquish
Relinquish
Products
Products
Products
Products
Products
TC-EX
8260
8270
TC-EX
8260
pH
pH
pH
pH
pH
Page 197
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Internal Chain of Custody Report
Login:
Account:
Project:
Samples:
Due Date:
L17051231
2755
2755.044
14
24-MAY-2017
A1 - Sample Archive (COLD)A2 - Sample Archive (AMBIENT)F1 - Volatiles Freezer in LoginV1 - Volatiles Refrigerator in LoginW1 - Walkin Cooler in Login
Microbac Laboratories Inc.
L17051231-10
L17051231-11
L17051231-12
L17051231-12
911932
911933
911934
911935
Samplenum
Samplenum
Samplenum
Samplenum
Container ID
Container ID
Container ID
Container ID
1
1
1
1
Bottle:
Bottle:
Bottle:
Bottle:
1
2
3
4
1
2
3
1
2
1
2
3
4
LOGIN
PREP
PREP
STORE
LOGIN
PREP
STORE
LOGIN
ANALYZ
LOGIN
PREP
PREP
STORE
COOLER
W1
EXT
DIG
COOLER
W1
TCL
COOLER
V1
COOLER
W1
EXT
DIG
W1
EXT
DIG
A2
W1
TCL
A2
V1
ORG4
W1
EXT
DIG
A2
22-MAY-2017 10:46
22-MAY-2017 11:53
22-MAY-2017 14:59
22-MAY-2017 16:25
22-MAY-2017 10:46
22-MAY-2017 11:26
22-MAY-2017 15:42
22-MAY-2017 10:46
22-MAY-2017 10:57
22-MAY-2017 10:46
22-MAY-2017 11:53
22-MAY-2017 14:59
22-MAY-2017 16:25
CLS
CPD
ZTB
CLS
CLS
BNB
BRG
CLS
JDS
CLS
CPD
ZTB
CLS
CLS
JDH
AC
BRG
BNB
CLS
CLS
JDH
AC
Seq.
Seq.
Seq.
Seq.
Purpose
Purpose
Purpose
Purpose
From
From
From
From
To
To
To
To
Date/Time
Date/Time
Date/Time
Date/Time
Accept
Accept
Accept
Accept
Relinquish
Relinquish
Relinquish
Relinquish
Products
Products
Products
Products
8270
TC-EX
8260
8270
pH
pH
pH
pH
Page 198
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Internal Chain of Custody Report
Login:
Account:
Project:
Samples:
Due Date:
L17051231
2755
2755.044
14
24-MAY-2017
A1 - Sample Archive (COLD)A2 - Sample Archive (AMBIENT)F1 - Volatiles Freezer in LoginV1 - Volatiles Refrigerator in LoginW1 - Walkin Cooler in Login
Microbac Laboratories Inc.
L17051231-13
L17051231-14
L17051231-14
911936
911937
911938
Samplenum
Samplenum
Samplenum
Container ID
Container ID
Container ID
1
1
1
Bottle:
Bottle:
Bottle:
1
2
3
1
2
1
2
3
4
LOGIN
PREP
STORE
LOGIN
ANALYZ
LOGIN
PREP
PREP
STORE
COOLER
W1
TCL
COOLER
V1
COOLER
W1
EXT
DIG
W1
TCL
A2
V1
ORG4
W1
EXT
DIG
A2
22-MAY-2017 10:46
22-MAY-2017 11:26
22-MAY-2017 15:43
22-MAY-2017 10:46
22-MAY-2017 10:57
22-MAY-2017 10:46
22-MAY-2017 11:53
22-MAY-2017 14:59
22-MAY-2017 16:25
CLS
BNB
BRG
CLS
JDS
CLS
CPD
ZTB
CLS
BRG
BNB
CLS
CLS
JDH
AC
Seq.
Seq.
Seq.
Purpose
Purpose
Purpose
From
From
From
To
To
To
Date/Time
Date/Time
Date/Time
Accept
Accept
Accept
Relinquish
Relinquish
Relinquish
Products
Products
Products
TC-EX
8260
8270
pH
pH
pH
Page 199
L17051231 / Revision: 0 / 199 total pages Generated: 05/30/2017 08:34
20170605-4006 FERC PDF (Unofficial) 06/05/2017
Document Content(s)
EPAemail.DOCX.........................................................1-2
DRO Results.PDF.......................................................3-29
Totals and TCLP Results prelim.PDF....................................30-94
Totals and TCLP Results Final.PDF.....................................95-293
20170605-4006 FERC PDF (Unofficial) 06/05/2017