...Analyte or Test PA DEP PA DEP Cleanup Actual Variation Actual Variation Parameter Units Limit...

Boucher & James, Inc.

Consulting Engineers Project:

1456 Ferry Road, Building 500 Job #:

Doylestown, PA 18901 Prep.By:

(215) 345-9400 Date:

For Conceptual Purposes: All Locations Approximate

JPH

177229E

Confirmation Environmental Testing St. Anthony's Church Property

4/30/2018

Sample Locations April 18, 2018

New Garden Township, Chester County, PA

N

Legend

- Soil Sample

- Water Sample

W1

W2

S1

S2

W2

S1

Scale

0' 600'

SUMMARY OF SAMPLING RESULTS - SOIL

SAINT ANTHONY IN THE HILLS SITE

Samples Collected on: 4/18/2018

Sample 177229E-S1 Sample 177229E-S2

Analyte or Test PA DEP PA DEP Cleanup Actual Variation Actual Variation

Parameter Units Limit Criteria Result From Limit Result From Limit

Benzo (a) Anthracene ug/kg (ppb) 6,000 Direct Contact 350 Acceptable 260 Acceptable

Benzo (a) Pyrene ug/kg (ppb) 5,800 Direct Contact 430 Acceptable 270 Acceptable

Benzo (b) Fluoranthene ug/kg (ppb) 3,500 Direct Contact 720 Acceptable 400 Acceptable

Benzo(g,h,i)Perylene ug/kg (ppb) 13,000,000 Direct Contact 370 Acceptable 200 Acceptable

Benzo(k)fluoranthene ug/kg (ppb) 4,000 Direct Contact 260 Acceptable 160 Acceptable

Chrysene ug/kg (ppb) 35,000 Direct Contact 500 Acceptable 360 Acceptable

Dibenz(a,h)anthracene ug/kg (ppb) 1,000 Direct Contact 96 Acceptable 38 Acceptable

Fluoranthene ug/kg (ppb) 8,800,000 Direct Contact 770 Acceptable 460 Acceptable

Indeno(1,2,3-cd)Pyrene ug/kg (ppb) 3,500 Direct Contact 310 Acceptable 190 Acceptable

Phenanthrene ug/kg (ppb) 66,000,000 Direct Contact 300 Acceptable 190 Acceptable

Pyrene ug/kg (ppb) 6,600,000 Direct Contact 670 Acceptable 460 Acceptable

Acenaphthylene ug/kg (ppb) 13,000,000 Direct Contact ND Acceptable 42 Acceptable

Acetone ug/kg (ppb) 10,000,000 Direct Contact 6.8 Acceptable ND Acceptable

Methylene Chloride ug/kg (ppb) 1,300,000 Direct Contact 0.64 Acceptable 0.26 Acceptable

Aroclor 1254 ug/kg (ppb) 4,400 Direct Contact 170 Acceptable ND Acceptable

Lead (Total) ug/kg (ppb) 500,000 Direct Contact 39,200 Acceptable 20,600 Acceptable

Arsenic ug/kg (ppb) 12,000 Direct Contact 2,900 Acceptable 3,700 Acceptable

Barium ug/kg (ppb) 44,000,000 Direct Contact 111,000 Acceptable 175,000 Acceptable

Cadmium ug/kg (ppb) 110,000 Direct Contact 2,000 Acceptable ND Acceptable

Chromium ug/kg (ppb) 190,000,000 Direct Contact 39,200 Acceptable 40,700 Acceptable

Mercury ug/kg (ppb) 35,000 Direct Contact 14 Acceptable 29 Acceptable

ND=Not Detected Within Lower

Detection Limit of Equipment

(See Lab Reports for L.D.L.)

Maintenance Garage Festival Grounds

SUMMARY OF SAMPLING RESULTS - WATER

SAINT ANTHONY IN THE HILLS

Samples Collected on: 4/18/2018

Sample 177299E-W1 Sample 177229E-W2

Analyte or Test PA DEP PA DEP Cleanup Actual Variation Actual Variation

Parameter Units Limit Criteria* Result From Limit Result From Limit

Nitrate as N ug/L (ppb) 10 Resid. Aquifer 2.28 Acceptable 0.10 Acceptable

Chloride ug/L (ppb) 250 Resid. Aquifer 51.3 Acceptable 63.6 Acceptable

Barium ug/L (ppb) 2,000 Resid. Aquifer 60.1 Acceptable 62.9 Acceptable

Cadmium ug/L (ppb) 5 Resid. Aquifer ND Acceptable 1.3 Acceptable

Lead ug/L (ppb) 5 Resid. Aquifer 0.39 Acceptable 12.2 Exceeds Limit

Chloroform ug/L (ppb) 80 Resid. Aquifer 0.38 Acceptable ND Acceptable

N-Nitrosodimethylamine ug/L (ppb) 0.0014 Resid. Aquifer ND Acceptable 1.1 Exceeds Limit

pH Resid. Aquifer 7.0 5.6

ND=Not Detected Within Lower

Detection Limit of Equipment

(See Lab Reports for L.D.L.)

Central Well (#6) Northeast Well (#9)

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Edison777 New Durham RoadEdison, NJ 08817Tel: (732)549-3900

TestAmerica Job ID: 460-154197-1Client Project/Site: SAITH

For:Boucher & James Inc1456 Ferry RoadBuilding 500Doylestown, Pennsylvania 18901

Attn: Phil Getty

Authorized for release by:5/2/2018 11:03:28 PM

Jannel Franklin, Manager of Project Management Assistants(732)[email protected]

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents

Client: Boucher & James IncProject/Site: SAITH

TestAmerica Job ID: 460-154197-1

Page 2 of 34TestAmerica Edison

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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

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Definitions/GlossaryTestAmerica Job ID: 460-154197-1Client: Boucher & James Inc

Project/Site: SAITH

Qualifiers

GC/MS VOA

Qualifier Description

U Indicates the analyte was analyzed for but not detected.

Qualifier

* LCS or LCSD is outside acceptance limits.

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

GC/MS VOA TICs


J Indicates an Estimated Value for TICs

Qualifier

N This flag indicates the presumptive evidence of a compound.

GC/MS Semi VOA



Qualifier


GC/MS Semi VOA TICs


J Indicates an Estimated Value for TICs

Qualifier

N This flag indicates the presumptive evidence of a compound.

GC Semi VOA



Qualifier

* LCS or LCSD is outside acceptance limits.

* RPD of the LCS and LCSD exceeds the control limits

HPLC/IC


D Sample results are obtained from a dilution; the surrogate or matrix spike recoveries reported are calculated from diluted samples.

Qualifier


F1 MS and/or MSD Recovery is outside acceptance limits.

Metals



Qualifier


General Chemistry


HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.

Qualifier

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains No Free Liquid

DER Duplicate Error Ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL Detection Limit (DoD/DOE)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision Level Concentration (Radiochemistry)

EDL Estimated Detection Limit (Dioxin)

LOD Limit of Detection (DoD/DOE)

LOQ Limit of Quantitation (DoD/DOE)

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Definitions/GlossaryTestAmerica Job ID: 460-154197-1Client: Boucher & James Inc

Project/Site: SAITH

Glossary (Continued)

These commonly used abbreviations may or may not be present in this report.

MDA Minimum Detectable Activity (Radiochemistry)

Abbreviation

MDC Minimum Detectable Concentration (Radiochemistry)

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not Detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative Error Ratio (Radiochemistry)

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Case NarrativeClient: Boucher & James Inc TestAmerica Job ID: 460-154197-1Project/Site: SAITH

Job ID: 460-154197-1

Laboratory: TestAmerica Edison

Narrative

Job Narrative460-154197-1

Comments

No additional comments.

Receipt

The samples were received on 4/18/2018 12:24 PM; the samples arrived in good condition, properly preserved and, where required, on

ice. The temperatures of the 2 coolers at receipt time were 2.4º C and 3.4º C.

GC/MS VOA Method(s) 8260C: The continuing calibration verification (CCV) analyzed in batch 460-513199 was outside the method criteria for the

following analytes: Chloromethane and Dichlorodifluoromethane. A CCV standard at or below the reporting limit (RL) was analyzed with

the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analytes are considered estimated.

Method(s) 8260C: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for analytical batch 460-513199 recovered outside control limits for the following analyte: Dichlorodifluoromethane. This analyte was not detected in the

associated samples; therefore, the data have been reported.

Method(s) 8260C: The laboratory control sample duplicate (LCSD) for analytical batch 460-513220 recovered outside control limits for the following analyte: 1,1,2,2-Tetrachloroethane. This analyte was biased high in the LCSD and was not detected in the associated samples; therefore, the data have been reported.

Method(s) 8260C: The continuing calibration verification (CCV) analyzed in batch 460-513775 was outside the method criteria for the following analyte: Dichlorodifluoromethane. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected

analyte is considered estimated.

Method(s) 8260C: The laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for analytical batch 460-513775 recovered outside control limits for the following analyte: Dichlorodifluoromethane.

Method(s) 8260C: The following sample had a peak at 7.98 min that is a GC carryover; therefore, it was not reported.177229E-S2 (460-154197-2)

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GC/MS Semi VOA

Method(s) 8270D: The continuing calibration verification (CCV) associated with batch 460-512568 recovered above the upper control limit for < Benzo[g,h,i]perylene, Dibenz(a,h)anthracene, Di-n-octyl phthalate and Indeno[1,2,3-cd]pyrene>. The samples associated with this

CCV were non-detects for the affected analytes; therefore, the data have been reported. The following sample is impacted: (CCVIS

460-512568/2).

Method(s) 8270D: The continuing calibration verification (CCV) associated with batch 460-513246 recovered above the upper control limit

for < 4-Nitrophenol>. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. The following sample is impacted: (CCVIS 460-513246/2).


GC Semi VOA Method(s) 300.0: The following samples were diluted to bring the concentration of target analytes within the calibration range:

177229E-W1 (460-154197-3), 177229E-W2 (460-154197-4), (460-154197-D-4 DU), (460-154197-D-4 MS) and (460-154197-D-4 MSD) at 23.0, 23.0, 23.0, 23.0 and 23.0. Elevated reporting limits (RLs) are provided.

Method(s) 8081B: The following sample required a mercury clean-up, via EPA Method 3660A, to reduce matrix interferences caused by

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Case NarrativeClient: Boucher & James Inc TestAmerica Job ID: 460-154197-1Project/Site: SAITH

Job ID: 460-154197-1 (Continued)

Laboratory: TestAmerica Edison (Continued)

sulfur: 177229E-W2 (460-154197-4). The reagent lot number used was: SLBT8543.

Method(s) 8082A: The laboratory control sample duplicate (LCSD) for preparation batch 460-512708 and analytical batch 460-513329

recovered outside control limits for the following analytes: Aroclor 1016 and Aroclor 1260. These analytes were biased high in the LCSD

and were not detected in the associated samples; therefore, the data have been reported.

Method(s) 8082A: The RPD of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for batch preparation batch 460-512708 and analytical batch 460-513329 recovered outside control limits for the following analytes Aroclor 1016 and Aroclor

1260.

Method(s) 8082A: The laboratory control sample duplicate (LCSD) recovered outside control limits for the surrogate and spike but LCS

recovered within control limits. The data have been qualified and reported. (LCSD 460-512708/3-A)

Method(s) 8151A: The closing continuing calibration verification (CCVC) associated with batch 513952 recovered above the upper control

limit for many analytes. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.

Method(s) 8151A: The laboratory control sample duplicate (LCSD) for 513872 recovered outside control limits for the following analytes: Silvex (2,4,5-TP) on the secondary column. These analytes were biased high in the LCSD and were not detected in the associated samples; therefore, the data have been reported.


Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

General Chemistry

No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Organic Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

VOA Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.


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Client Sample ResultsTestAmerica Job ID: 460-154197-1Client: Boucher & James Inc

Project/Site: SAITH

Lab Sample ID: 460-154197-1Client Sample ID: 177229E-S1Matrix: SolidDate Collected: 04/18/18 10:50

Percent Solids: 73.8Date Received: 04/18/18 12:24

Method: 8260C - Volatile Organic Compounds by GC/MSRL MDL

1,1,1-Trichloroethane 0.30 U 1.3 0.30 ug/Kg ☼ 04/19/18 00:20 04/23/18 03:39 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

1.3 0.28 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼1,1,2,2-Tetrachloroethane 0.28 U

1.3 0.39 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼1,1,2-Trichloro-1,2,2-trifluoroethane 0.39 U

1.3 0.23 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼1,1,2-Trichloroethane 0.23 U

1.3 0.27 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼1,1-Dichloroethane 0.27 U

1.3 0.29 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼1,1-Dichloroethene 0.29 U

1.3 0.24 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼1,2,3-Trichlorobenzene 0.24 U


1.3 0.60 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼1,2-Dibromo-3-Chloropropane 0.60 U

1.3 0.19 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼1,2-Dichlorobenzene 0.19 U


1.3 0.55 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼1,2-Dichloropropane 0.55 U



26 12 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼1,4-Dioxane 12 U

6.5 1.4 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼2-Butanone (MEK) 1.4 U

6.5 1.0 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼2-Hexanone 1.0 U

6.5 0.87 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼4-Methyl-2-pentanone (MIBK) 0.87 U

6.5 4.9 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Acetone 6.8

1.3 0.34 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Benzene 0.34 U

1.3 0.55 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Bromoform 0.55 U

1.3 0.62 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Bromomethane 0.62 U

1.3 0.35 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Carbon disulfide 0.35 U

1.3 0.24 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Carbon tetrachloride 0.24 U

1.3 0.23 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Chlorobenzene 0.23 U

1.3 0.37 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Chlorobromomethane 0.37 U

1.3 0.25 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Chlorodibromomethane 0.25 U

1.3 0.68 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Chloroethane 0.68 U

1.3 0.42 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Chloroform 0.42 U

1.3 0.57 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Chloromethane 0.57 U

1.3 0.20 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼cis-1,2-Dichloroethene 0.20 U

1.3 0.36 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼cis-1,3-Dichloropropene 0.36 U

1.3 0.29 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Cyclohexane 0.29 U

1.3 0.34 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Dichlorobromomethane 0.34 U

1.3 0.44 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Dichlorodifluoromethane 0.44 U *

1.3 0.26 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Ethylbenzene 0.26 U

1.3 0.23 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Ethylene Dibromide 0.23 U

1.3 0.16 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Isopropylbenzene 0.16 U

6.5 5.6 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Methyl acetate 5.6 U

1.3 0.16 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Methyl tert-butyl ether 0.16 U

1.3 0.21 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Methylcyclohexane 0.21 U

1.3 0.21 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Methylene Chloride 0.64 J

1.3 0.23 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼m-Xylene & p-Xylene 0.23 U

1.3 0.12 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼o-Xylene 0.12 U

1.3 0.16 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Styrene 0.16 U

1.3 0.19 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Tetrachloroethene 0.19 U

1.3 0.82 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Toluene 0.82 U

1.3 0.32 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼trans-1,2-Dichloroethene 0.32 U

1.3 0.35 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼trans-1,3-Dichloropropene 0.35 U

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Project/Site: SAITH



Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)RL MDL

Trichloroethene 0.19 U 1.3 0.19 ug/Kg ☼ 04/19/18 00:20 04/23/18 03:39 1


1.3 0.53 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Trichlorofluoromethane 0.53 U

1.3 0.71 ug/Kg 04/19/18 00:20 04/23/18 03:39 1☼Vinyl chloride 0.71 U

Butane, 2-methyl- 19 J N ug/Kg ☼ 2.30 78-78-4 04/19/18 00:20 04/23/18 03:39 1

Tentatively Identified Compound Dil FacAnalyzedPreparedUnit DQualifierEst. Result CAS No.RT

☼ 104/23/18 03:3904/19/18 00:20JUnknown alkane 8.1 ug/Kg 2.50

☼ 104/23/18 03:3904/19/18 00:20J NCyclopentane 287-92-3300 ug/Kg 3.35

1,2-Dichloroethane-d4 (Surr) 104 78 - 135 04/19/18 00:20 04/23/18 03:39 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

4-Bromofluorobenzene 102 04/19/18 00:20 04/23/18 03:39 167 - 126

Dibromofluoromethane (Surr) 105 04/19/18 00:20 04/23/18 03:39 161 - 149

Toluene-d8 (Surr) 99 04/19/18 00:20 04/23/18 03:39 173 - 121

Method: 8270D - Semivolatile Organic Compounds (GC/MS)RL MDL

1,1'-Biphenyl 12 U 890 12 ug/Kg ☼ 04/21/18 07:17 04/23/18 17:04 2


890 12 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼1,2,4,5-Tetrachlorobenzene 12 U

890 19 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼1,4-Dichlorobenzene 19 U

890 16 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼2,2'-oxybis[1-chloropropane] 16 U

890 61 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼2,3,4,6-Tetrachlorophenol 61 U

890 30 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼2,4,5-Trichlorophenol 30 U


360 19 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼2,4-Dichlorophenol 19 U

890 39 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼2,4-Dimethylphenol 39 U

720 440 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼2,4-Dinitrophenol 440 U

180 45 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼2,4-Dinitrotoluene 45 U


890 41 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼2-Chloronaphthalene 41 U

890 13 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼2-Chlorophenol 13 U

890 11 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼2-Methylnaphthalene 11 U

890 14 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼2-Methylphenol 14 U

890 33 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼2-Nitroaniline 33 U

890 29 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼2-Nitrophenol 29 U

890 15 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼3 & 4 Methylphenol 15 U

360 140 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼3,3'-Dichlorobenzidine 140 U


720 150 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼4,6-Dinitro-2-methylphenol 150 U

890 12 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼4-Bromophenyl phenyl ether 12 U

890 15 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼4-Chloro-3-methylphenol 15 U

890 63 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼4-Chloroaniline 63 U

890 14 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼4-Chlorophenyl phenyl ether 14 U




890 65 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Acenaphthene 65 U

890 9.3 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Acenaphthylene 9.3 U

890 14 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Acetophenone 14 U

890 10 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Anthracene 10 U

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Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL

Atrazine 23 U 360 23 ug/Kg ☼ 04/21/18 07:17 04/23/18 17:04 2


890 39 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Benzaldehyde 39 U

89 31 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Benzo[a]anthracene 350

89 24 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Benzo[a]pyrene 430

89 23 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Benzo[b]fluoranthene 720

890 26 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Benzo[g,h,i]perylene 370 J

89 18 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Benzo[k]fluoranthene 260

890 31 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Bis(2-chloroethoxy)methane 31 U

89 11 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Bis(2-chloroethyl)ether 11 U

890 47 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Bis(2-ethylhexyl) phthalate 47 U

890 42 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Butyl benzyl phthalate 42 U

890 54 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Caprolactam 54 U

890 10 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Carbazole 10 U

890 15 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Chrysene 500 J

89 39 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Dibenz(a,h)anthracene 96

890 13 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Dibenzofuran 13 U

890 13 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Diethyl phthalate 13 U

890 11 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Dimethyl phthalate 11 U

890 160 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Di-n-butyl phthalate 160 U

890 47 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Di-n-octyl phthalate 47 U

890 12 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Fluoranthene 770 J

890 12 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Fluorene 12 U

89 13 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Hexachlorobenzene 13 U

180 19 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Hexachlorobutadiene 19 U

890 79 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Hexachlorocyclopentadiene 79 U

89 14 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Hexachloroethane 14 U

89 35 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Indeno[1,2,3-cd]pyrene 310

360 24 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Isophorone 24 U

890 15 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Naphthalene 15 U

89 22 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Nitrobenzene 22 U

89 14 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼N-Nitrosodi-n-propylamine 14 U

890 17 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼N-Nitrosodiphenylamine 17 U

720 180 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Pentachlorophenol 180 U

890 16 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Phenanthrene 300 J

890 13 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Phenol 13 U

890 22 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Pyrene 670 J

890 49 ug/Kg 04/21/18 07:17 04/23/18 17:04 2☼Pyridine 49 U

Heneicosane 2400 J N ug/Kg ☼ 12.76 629-94-7 04/21/18 07:17 04/23/18 17:04 2


☼ 204/23/18 17:0404/21/18 07:17JUnknown 2400 ug/Kg 13.91

☼ 204/23/18 17:0404/21/18 07:17JUnknown 2000 ug/Kg 14.58

☼ 204/23/18 17:0404/21/18 07:17JUnknown 980 ug/Kg 16.17

2,4,6-Tribromophenol (Surr) 59 10 - 103 04/21/18 07:17 04/23/18 17:04 2


2-Fluorobiphenyl 61 04/21/18 07:17 04/23/18 17:04 238 - 95

2-Fluorophenol (Surr) 55 04/21/18 07:17 04/23/18 17:04 225 - 92

Nitrobenzene-d5 (Surr) 58 04/21/18 07:17 04/23/18 17:04 237 - 94

Phenol-d5 (Surr) 57 04/21/18 07:17 04/23/18 17:04 232 - 91

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Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)

Terphenyl-d14 (Surr) 59 24 - 109 04/21/18 07:17 04/23/18 17:04 2


Method: 8081B - Organochlorine Pesticides (GC)RL MDL

4,4'-DDD 1.5 U 9.1 1.5 ug/Kg ☼ 04/19/18 22:17 04/20/18 16:04 1


9.1 1.1 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼4,4'-DDE 1.1 U

9.1 1.7 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼4,4'-DDT 1.7 U

9.1 1.4 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼Aldrin 1.4 U

2.7 0.92 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼alpha-BHC 0.92 U

2.7 1.0 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼beta-BHC 1.0 U

2.7 0.55 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼delta-BHC 0.55 U

2.7 1.2 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼Dieldrin 1.2 U

9.1 1.4 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼Endosulfan I 1.4 U

9.1 2.3 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼Endosulfan II 2.3 U

9.1 1.1 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼Endosulfan sulfate 1.1 U

9.1 1.3 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼Endrin 1.3 U

9.1 2.1 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼Endrin aldehyde 2.1 U

9.1 1.8 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼Endrin ketone 1.8 U

2.7 0.84 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼gamma-BHC (Lindane) 0.84 U

9.1 1.1 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼Heptachlor 1.1 U

9.1 1.4 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼Heptachlor epoxide 1.4 U

9.1 2.1 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼Methoxychlor 2.1 U

91 33 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼Toxaphene 33 U

91 22 ug/Kg 04/19/18 22:17 04/20/18 16:04 1☼Chlordane (technical) 22 U

DCB Decachlorobiphenyl 97 69 - 150 04/19/18 22:17 04/20/18 16:04 1


DCB Decachlorobiphenyl 88 04/19/18 22:17 04/20/18 16:04 169 - 150

Tetrachloro-m-xylene 95 04/19/18 22:17 04/20/18 16:04 174 - 150


Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyRL MDL

Aroclor 1016 12 U 91 12 ug/Kg ☼ 04/19/18 22:27 04/20/18 22:42 1


91 12 ug/Kg 04/19/18 22:27 04/20/18 22:42 1☼Aroclor 1221 12 U

91 12 ug/Kg 04/19/18 22:27 04/20/18 22:42 1☼Aroclor 1232 12 U

91 12 ug/Kg 04/19/18 22:27 04/20/18 22:42 1☼Aroclor 1242 12 U

91 12 ug/Kg 04/19/18 22:27 04/20/18 22:42 1☼Aroclor 1248 12 U

91 12 ug/Kg 04/19/18 22:27 04/20/18 22:42 1☼Aroclor 1254 170

91 12 ug/Kg 04/19/18 22:27 04/20/18 22:42 1☼Aroclor 1260 12 U

91 12 ug/Kg 04/19/18 22:27 04/20/18 22:42 1☼Aroclor-1262 12 U

91 12 ug/Kg 04/19/18 22:27 04/20/18 22:42 1☼Aroclor 1268 12 U

91 12 ug/Kg 04/19/18 22:27 04/20/18 22:42 1☼Polychlorinated biphenyls, Total 170




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Method: 8151A - Herbicides (GC)RL MDL

2,4-D 11 U 45 11 ug/Kg ☼ 04/23/18 20:56 04/24/18 09:05 1


45 15 ug/Kg 04/23/18 20:56 04/24/18 09:05 1☼Silvex (2,4,5-TP) 15 U

45 11 ug/Kg 04/23/18 20:56 04/24/18 09:05 1☼2,4,5-T 11 U

2,4-Dichlorophenylacetic acid 142 80 - 150 04/23/18 20:56 04/24/18 09:05 1


2,4-Dichlorophenylacetic acid 126 04/23/18 20:56 04/24/18 09:05 180 - 150

Method: 6020A - Metals (ICP/MS)RL MDL

Arsenic 2.9 1.3 0.42 mg/Kg ☼ 04/26/18 04:27 04/26/18 15:51 20


2.6 0.87 mg/Kg 04/26/18 04:27 04/26/18 15:51 20☼Barium 111

1.3 0.44 mg/Kg 04/26/18 04:27 04/26/18 15:51 20☼Cadmium 2.0

2.6 0.79 mg/Kg 04/26/18 04:27 04/26/18 15:51 20☼Chromium 47.2

0.79 0.25 mg/Kg 04/26/18 04:27 04/26/18 15:51 20☼Lead 39.2

6.6 0.38 mg/Kg 04/26/18 04:27 04/26/18 15:51 20☼Selenium 0.38 U

1.3 0.81 mg/Kg 04/26/18 04:27 04/26/18 15:51 20☼Silver 0.81 U

Method: 7471B - Mercury (CVAA)RL MDL

Mercury 0.014 J 0.021 0.013 mg/Kg ☼ 04/20/18 04:46 04/20/18 09:46 1


General ChemistryRL MDL

Percent Moisture 26.2 1.0 1.0 % 04/19/18 12:36 1


1.0 1.0 % 04/19/18 12:36 1Percent Solids 73.8




1,1,1-Trichloroethane 0.34 U 1.5 0.34 ug/Kg ☼ 04/19/18 00:20 04/25/18 01:55 1


1.5 0.32 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼1,1,2,2-Tetrachloroethane 0.32 U

1.5 0.45 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼1,1,2-Trichloro-1,2,2-trifluoroethane 0.45 U

1.5 0.26 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼1,1,2-Trichloroethane 0.26 U


1.5 0.33 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼1,1-Dichloroethene 0.33 U



1.5 0.68 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼1,2-Dibromo-3-Chloropropane 0.68 U



1.5 0.63 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼1,2-Dichloropropane 0.63 U



30 14 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼1,4-Dioxane 14 U

7.4 1.6 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼2-Butanone (MEK) 1.6 U

7.4 1.2 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼2-Hexanone 1.2 U

7.4 0.98 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼4-Methyl-2-pentanone (MIBK) 0.98 U

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Acetone 5.6 U 7.4 5.6 ug/Kg ☼ 04/19/18 00:20 04/25/18 01:55 1


1.5 0.38 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Benzene 0.38 U

1.5 0.63 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Bromoform 0.63 U

1.5 0.70 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Bromomethane 0.70 U

1.5 0.39 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Carbon disulfide 0.39 U

1.5 0.27 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Carbon tetrachloride 0.27 U

1.5 0.26 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Chlorobenzene 0.26 U

1.5 0.42 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Chlorobromomethane 0.42 U

1.5 0.29 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Chlorodibromomethane 0.29 U

1.5 0.77 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Chloroethane 0.77 U

1.5 0.47 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Chloroform 0.47 U

1.5 0.64 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Chloromethane 0.64 U

1.5 0.22 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼cis-1,2-Dichloroethene 0.22 U

1.5 0.40 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼cis-1,3-Dichloropropene 0.40 U

1.5 0.33 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Cyclohexane 0.33 U

1.5 0.38 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Dichlorobromomethane 0.38 U

1.5 0.50 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Dichlorodifluoromethane 0.50 U *

1.5 0.29 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Ethylbenzene 0.29 U

1.5 0.27 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Ethylene Dibromide 0.27 U

1.5 0.19 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Isopropylbenzene 0.19 U

7.4 6.4 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Methyl acetate 6.4 U

1.5 0.18 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Methyl tert-butyl ether 0.18 U

1.5 0.24 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Methylcyclohexane 0.24 U

1.5 0.24 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Methylene Chloride 0.26 J

1.5 0.26 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼m-Xylene & p-Xylene 0.26 U

1.5 0.14 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼o-Xylene 0.14 U

1.5 0.18 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Styrene 0.18 U

1.5 0.21 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Tetrachloroethene 0.21 U

1.5 0.92 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Toluene 0.92 U

1.5 0.36 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼trans-1,2-Dichloroethene 0.36 U

1.5 0.39 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼trans-1,3-Dichloropropene 0.39 U

1.5 0.21 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Trichloroethene 0.21 U

1.5 0.60 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Trichlorofluoromethane 0.60 U

1.5 0.81 ug/Kg 04/19/18 00:20 04/25/18 01:55 1☼Vinyl chloride 0.81 U

Tentatively Identified Compound None ug/Kg ☼ 04/19/18 00:20 04/25/18 01:55 1


1,2-Dichloroethane-d4 (Surr) 92 78 - 135 04/19/18 00:20 04/25/18 01:55 1


4-Bromofluorobenzene 85 04/19/18 00:20 04/25/18 01:55 167 - 126

Dibromofluoromethane (Surr) 92 04/19/18 00:20 04/25/18 01:55 161 - 149

Toluene-d8 (Surr) 87 04/19/18 00:20 04/25/18 01:55 173 - 121


1,1'-Biphenyl 12 U 880 12 ug/Kg ☼ 04/21/18 07:17 04/23/18 17:27 2


880 11 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼1,2,4,5-Tetrachlorobenzene 11 U

880 18 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼1,4-Dichlorobenzene 18 U

880 16 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼2,2'-oxybis[1-chloropropane] 16 U

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2,3,4,6-Tetrachlorophenol 59 U 880 59 ug/Kg ☼ 04/21/18 07:17 04/23/18 17:27 2




350 19 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼2,4-Dichlorophenol 19 U

880 39 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼2,4-Dimethylphenol 39 U

710 430 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼2,4-Dinitrophenol 430 U



880 41 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼2-Chloronaphthalene 41 U

880 12 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼2-Chlorophenol 12 U

880 11 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼2-Methylnaphthalene 11 U




880 15 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼3 & 4 Methylphenol 15 U

350 130 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼3,3'-Dichlorobenzidine 130 U


710 140 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼4,6-Dinitro-2-methylphenol 140 U

880 11 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼4-Bromophenyl phenyl ether 11 U

880 15 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼4-Chloro-3-methylphenol 15 U

880 61 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼4-Chloroaniline 61 U

880 14 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼4-Chlorophenyl phenyl ether 14 U




880 64 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Acenaphthene 64 U

880 9.1 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Acenaphthylene 42 J

880 14 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Acetophenone 14 U

880 9.8 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Anthracene 9.8 U

350 22 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Atrazine 22 U

880 38 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Benzaldehyde 38 U

88 31 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Benzo[a]anthracene 260

88 23 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Benzo[a]pyrene 270

88 23 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Benzo[b]fluoranthene 400

880 26 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Benzo[g,h,i]perylene 200 J

88 17 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Benzo[k]fluoranthene 160

880 30 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Bis(2-chloroethoxy)methane 30 U

88 11 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Bis(2-chloroethyl)ether 11 U

880 46 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Bis(2-ethylhexyl) phthalate 46 U

880 41 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Butyl benzyl phthalate 41 U

880 53 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Caprolactam 53 U

880 10 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Carbazole 10 U

880 15 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Chrysene 360 J

88 38 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Dibenz(a,h)anthracene 38 J

880 12 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Dibenzofuran 12 U

880 13 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Diethyl phthalate 13 U

880 11 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Dimethyl phthalate 11 U

880 150 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Di-n-butyl phthalate 150 U

880 46 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Di-n-octyl phthalate 46 U

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Fluoranthene 460 J 880 11 ug/Kg ☼ 04/21/18 07:17 04/23/18 17:27 2


880 12 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Fluorene 12 U

88 13 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Hexachlorobenzene 13 U

180 19 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Hexachlorobutadiene 19 U

880 77 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Hexachlorocyclopentadiene 77 U

88 14 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Hexachloroethane 14 U

88 34 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Indeno[1,2,3-cd]pyrene 190

350 23 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Isophorone 23 U

880 15 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Naphthalene 15 U

88 21 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Nitrobenzene 21 U

88 14 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼N-Nitrosodi-n-propylamine 14 U

880 17 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼N-Nitrosodiphenylamine 17 U

710 180 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Pentachlorophenol 180 U

880 15 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Phenanthrene 190 J

880 13 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Phenol 13 U

880 22 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Pyrene 460 J

880 48 ug/Kg 04/21/18 07:17 04/23/18 17:27 2☼Pyridine 48 U

Unknown 1100 J ug/Kg ☼ 11.25 04/21/18 07:17 04/23/18 17:27 2


☼ 204/23/18 17:2704/21/18 07:17JUnknown 750 ug/Kg 11.45

☼ 204/23/18 17:2704/21/18 07:17JUnknown 990 ug/Kg 12.36

☼ 204/23/18 17:2704/21/18 07:17J NOctadecanal 638-66-4860 ug/Kg 12.50

☼ 204/23/18 17:2704/21/18 07:17J NTridecane, 7-propyl- 55045-09-52600 ug/Kg 12.76

☼ 204/23/18 17:2704/21/18 07:17JUnknown 1200 ug/Kg 12.96

☼ 204/23/18 17:2704/21/18 07:17JUnknown 880 ug/Kg 13.47



2-Fluorobiphenyl 60 04/21/18 07:17 04/23/18 17:27 238 - 95



Phenol-d5 (Surr) 56 04/21/18 07:17 04/23/18 17:27 232 - 91

Terphenyl-d14 (Surr) 54 04/21/18 07:17 04/23/18 17:27 224 - 109


4,4'-DDD 1.5 U 8.9 1.5 ug/Kg ☼ 04/19/18 22:17 04/20/18 16:17 1


8.9 1.0 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼4,4'-DDE 1.0 U

8.9 1.6 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼4,4'-DDT 1.6 U

8.9 1.3 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼Aldrin 1.3 U

2.7 0.90 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼alpha-BHC 0.90 U

2.7 1.0 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼beta-BHC 1.0 U

2.7 0.54 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼delta-BHC 0.54 U

2.7 1.2 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼Dieldrin 1.2 U

8.9 1.4 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼Endosulfan I 1.4 U

8.9 2.3 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼Endosulfan II 2.3 U

8.9 1.1 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼Endosulfan sulfate 1.1 U

8.9 1.3 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼Endrin 1.3 U

8.9 2.1 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼Endrin aldehyde 2.1 U

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Method: 8081B - Organochlorine Pesticides (GC) (Continued)RL MDL

Endrin ketone 1.7 U 8.9 1.7 ug/Kg ☼ 04/19/18 22:17 04/20/18 16:17 1


2.7 0.82 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼gamma-BHC (Lindane) 0.82 U

8.9 1.0 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼Heptachlor 1.0 U

8.9 1.3 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼Heptachlor epoxide 1.3 U

8.9 2.0 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼Methoxychlor 2.0 U

89 32 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼Toxaphene 32 U

89 21 ug/Kg 04/19/18 22:17 04/20/18 16:17 1☼Chlordane (technical) 21 U







Aroclor 1016 12 U 89 12 ug/Kg ☼ 04/19/18 22:27 04/20/18 22:59 1


89 12 ug/Kg 04/19/18 22:27 04/20/18 22:59 1☼Aroclor 1221 12 U

89 12 ug/Kg 04/19/18 22:27 04/20/18 22:59 1☼Aroclor 1232 12 U

89 12 ug/Kg 04/19/18 22:27 04/20/18 22:59 1☼Aroclor 1242 12 U

89 12 ug/Kg 04/19/18 22:27 04/20/18 22:59 1☼Aroclor 1248 12 U

89 12 ug/Kg 04/19/18 22:27 04/20/18 22:59 1☼Aroclor 1254 12 U

89 12 ug/Kg 04/19/18 22:27 04/20/18 22:59 1☼Aroclor 1260 12 U

89 12 ug/Kg 04/19/18 22:27 04/20/18 22:59 1☼Aroclor-1262 12 U

89 12 ug/Kg 04/19/18 22:27 04/20/18 22:59 1☼Aroclor 1268 12 U

89 12 ug/Kg 04/19/18 22:27 04/20/18 22:59 1☼Polychlorinated biphenyls, Total 12 U





2,4-D 10 U 44 10 ug/Kg ☼ 04/23/18 20:56 04/24/18 09:20 1


44 15 ug/Kg 04/23/18 20:56 04/24/18 09:20 1☼Silvex (2,4,5-TP) 15 U

44 10 ug/Kg 04/23/18 20:56 04/24/18 09:20 1☼2,4,5-T 10 U





Arsenic 3.7 1.3 0.41 mg/Kg ☼ 04/26/18 04:27 04/26/18 15:54 20


2.5 0.84 mg/Kg 04/26/18 04:27 04/26/18 15:54 20☼Barium 175

1.3 0.42 mg/Kg 04/26/18 04:27 04/26/18 15:54 20☼Cadmium 0.42 U

2.5 0.76 mg/Kg 04/26/18 04:27 04/26/18 15:54 20☼Chromium 40.7

0.76 0.24 mg/Kg 04/26/18 04:27 04/26/18 15:54 20☼Lead 20.6

6.3 0.37 mg/Kg 04/26/18 04:27 04/26/18 15:54 20☼Selenium 0.37 U

1.3 0.78 mg/Kg 04/26/18 04:27 04/26/18 15:54 20☼Silver 0.78 U

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Method: 7471B - Mercury (CVAA)RL MDL

Mercury 0.029 0.022 0.013 mg/Kg ☼ 04/20/18 04:46 04/20/18 09:48 1



Percent Moisture 24.7 1.0 1.0 % 04/19/18 12:36 1


1.0 1.0 % 04/19/18 12:36 1Percent Solids 75.3

Lab Sample ID: 460-154197-3Client Sample ID: 177229E-W1Matrix: WaterDate Collected: 04/18/18 09:25

Date Received: 04/18/18 12:24


1,1,1-Trichloroethane 0.28 U 1.0 0.28 ug/L 04/23/18 04:12 1


1.0 0.19 ug/L 04/23/18 04:12 11,1,2,2-Tetrachloroethane 0.19 U *

1.0 0.34 ug/L 04/23/18 04:12 11,1,2-Trichloro-1,2,2-trifluoroethane 0.34 U

1.0 0.080 ug/L 04/23/18 04:12 11,1,2-Trichloroethane 0.080 U

1.0 0.24 ug/L 04/23/18 04:12 11,1-Dichloroethane 0.24 U

1.0 0.34 ug/L 04/23/18 04:12 11,1-Dichloroethene 0.34 U

1.0 0.35 ug/L 04/23/18 04:12 11,2,3-Trichlorobenzene 0.35 U


1.0 0.23 ug/L 04/23/18 04:12 11,2-Dibromo-3-Chloropropane 0.23 U

1.0 0.22 ug/L 04/23/18 04:12 11,2-Dichlorobenzene 0.22 U


1.0 0.18 ug/L 04/23/18 04:12 11,2-Dichloropropane 0.18 U



50 8.7 ug/L 04/23/18 04:12 11,4-Dioxane 8.7 U

5.0 2.2 ug/L 04/23/18 04:12 12-Butanone (MEK) 2.2 U

5.0 0.72 ug/L 04/23/18 04:12 12-Hexanone 0.72 U

5.0 0.63 ug/L 04/23/18 04:12 14-Methyl-2-pentanone (MIBK) 0.63 U

5.0 1.1 ug/L 04/23/18 04:12 1Acetone 1.1 U

1.0 0.090 ug/L 04/23/18 04:12 1Benzene 0.090 U

1.0 0.18 ug/L 04/23/18 04:12 1Bromoform 0.18 U

1.0 0.18 ug/L 04/23/18 04:12 1Bromomethane 0.18 U

1.0 0.22 ug/L 04/23/18 04:12 1Carbon disulfide 0.22 U

1.0 0.33 ug/L 04/23/18 04:12 1Carbon tetrachloride 0.33 U

1.0 0.24 ug/L 04/23/18 04:12 1Chlorobenzene 0.24 U

1.0 0.30 ug/L 04/23/18 04:12 1Chlorobromomethane 0.30 U

1.0 0.22 ug/L 04/23/18 04:12 1Chlorodibromomethane 0.22 U

1.0 0.37 ug/L 04/23/18 04:12 1Chloroethane 0.37 U

1.0 0.22 ug/L 04/23/18 04:12 1Chloroform 0.22 U

1.0 0.22 ug/L 04/23/18 04:12 1Chloromethane 0.22 U

1.0 0.26 ug/L 04/23/18 04:12 1cis-1,2-Dichloroethene 0.26 U

1.0 0.16 ug/L 04/23/18 04:12 1cis-1,3-Dichloropropene 0.16 U

1.0 0.26 ug/L 04/23/18 04:12 1Cyclohexane 0.26 U

1.0 0.15 ug/L 04/23/18 04:12 1Dichlorobromomethane 0.15 U

1.0 0.14 ug/L 04/23/18 04:12 1Dichlorodifluoromethane 0.14 U

1.0 0.30 ug/L 04/23/18 04:12 1Ethylbenzene 0.30 U

1.0 0.19 ug/L 04/23/18 04:12 1Ethylene Dibromide 0.19 U

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Isopropylbenzene 0.32 U 1.0 0.32 ug/L 04/23/18 04:12 1


5.0 0.58 ug/L 04/23/18 04:12 1Methyl acetate 0.58 U

1.0 0.13 ug/L 04/23/18 04:12 1Methyl tert-butyl ether 0.13 U

1.0 0.22 ug/L 04/23/18 04:12 1Methylcyclohexane 0.22 U

1.0 0.21 ug/L 04/23/18 04:12 1Methylene Chloride 0.21 U

1.0 0.28 ug/L 04/23/18 04:12 1m-Xylene & p-Xylene 0.28 U

1.0 0.32 ug/L 04/23/18 04:12 1o-Xylene 0.32 U

1.0 0.17 ug/L 04/23/18 04:12 1Styrene 0.17 U

1.0 0.12 ug/L 04/23/18 04:12 1Tetrachloroethene 0.12 U

1.0 0.25 ug/L 04/23/18 04:12 1Toluene 0.25 U

1.0 0.18 ug/L 04/23/18 04:12 1trans-1,2-Dichloroethene 0.18 U

1.0 0.19 ug/L 04/23/18 04:12 1trans-1,3-Dichloropropene 0.19 U

1.0 0.22 ug/L 04/23/18 04:12 1Trichloroethene 0.22 U

1.0 0.15 ug/L 04/23/18 04:12 1Trichlorofluoromethane 0.15 U

1.0 0.060 ug/L 04/23/18 04:12 1Vinyl chloride 0.060 U

Tentatively Identified Compound None ug/L 04/23/18 04:12 1


1,2-Dichloroethane-d4 (Surr) 110 74 - 132 04/23/18 04:12 1


4-Bromofluorobenzene 91 04/23/18 04:12 177 - 124

Dibromofluoromethane (Surr) 100 04/23/18 04:12 172 - 131

Toluene-d8 (Surr) 102 04/23/18 04:12 180 - 120

Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL

Benzo[a]anthracene 0.016 U 0.050 0.016 ug/L 04/19/18 15:58 04/20/18 08:56 1


0.050 0.022 ug/L 04/19/18 15:58 04/20/18 08:56 1Benzo[a]pyrene 0.022 U

0.050 0.024 ug/L 04/19/18 15:58 04/20/18 08:56 1Benzo[b]fluoranthene 0.024 U

0.030 0.026 ug/L 04/19/18 15:58 04/20/18 08:56 1Bis(2-chloroethyl)ether 0.026 U

0.020 0.013 ug/L 04/19/18 15:58 04/20/18 08:56 1Hexachlorobenzene 0.013 U

0.20 0.12 ug/L 04/19/18 15:58 04/20/18 08:56 1N-Nitrosodimethylamine 0.12 U

0.20 0.15 ug/L 04/19/18 15:58 04/20/18 08:56 1Pentachlorophenol 0.15 U


1,1'-Biphenyl 1.2 U 10 1.2 ug/L 04/19/18 15:58 04/20/18 05:57 1


10 1.2 ug/L 04/19/18 15:58 04/20/18 05:57 11,2,4,5-Tetrachlorobenzene 1.2 U

10 1.3 ug/L 04/19/18 15:58 04/20/18 05:57 11,4-Dichlorobenzene 1.3 U

10 0.63 ug/L 04/19/18 15:58 04/20/18 05:57 12,2'-oxybis[1-chloropropane] 0.63 U

10 0.75 ug/L 04/19/18 15:58 04/20/18 05:57 12,3,4,6-Tetrachlorophenol 0.75 U

10 0.28 ug/L 04/19/18 15:58 04/20/18 05:57 12,4,5-Trichlorophenol 0.28 U


10 0.42 ug/L 04/19/18 15:58 04/20/18 05:57 12,4-Dichlorophenol 0.42 U

10 0.24 ug/L 04/19/18 15:58 04/20/18 05:57 12,4-Dimethylphenol 0.24 U

20 14 ug/L 04/19/18 15:58 04/20/18 05:57 12,4-Dinitrophenol 14 U

2.0 1.0 ug/L 04/19/18 15:58 04/20/18 05:57 12,4-Dinitrotoluene 1.0 U


10 1.2 ug/L 04/19/18 15:58 04/20/18 05:57 12-Chloronaphthalene 1.2 U

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2-Chlorophenol 0.38 U 10 0.38 ug/L 04/19/18 15:58 04/20/18 05:57 1


10 1.1 ug/L 04/19/18 15:58 04/20/18 05:57 12-Methylnaphthalene 1.1 U

10 0.26 ug/L 04/19/18 15:58 04/20/18 05:57 12-Methylphenol 0.26 U

10 0.47 ug/L 04/19/18 15:58 04/20/18 05:57 12-Nitroaniline 0.47 U

10 0.75 ug/L 04/19/18 15:58 04/20/18 05:57 12-Nitrophenol 0.75 U

10 0.24 ug/L 04/19/18 15:58 04/20/18 05:57 13 & 4 Methylphenol 0.24 U

10 1.4 ug/L 04/19/18 15:58 04/20/18 05:57 13,3'-Dichlorobenzidine 1.4 U


20 13 ug/L 04/19/18 15:58 04/20/18 05:57 14,6-Dinitro-2-methylphenol 13 U

10 0.75 ug/L 04/19/18 15:58 04/20/18 05:57 14-Bromophenyl phenyl ether 0.75 U

10 0.58 ug/L 04/19/18 15:58 04/20/18 05:57 14-Chloro-3-methylphenol 0.58 U

10 1.9 ug/L 04/19/18 15:58 04/20/18 05:57 14-Chloroaniline 1.9 U

10 1.3 ug/L 04/19/18 15:58 04/20/18 05:57 14-Chlorophenyl phenyl ether 1.3 U




10 1.1 ug/L 04/19/18 15:58 04/20/18 05:57 1Acenaphthene 1.1 U

10 0.82 ug/L 04/19/18 15:58 04/20/18 05:57 1Acenaphthylene 0.82 U

10 0.79 ug/L 04/19/18 15:58 04/20/18 05:57 1Acetophenone 0.79 U

10 0.63 ug/L 04/19/18 15:58 04/20/18 05:57 1Anthracene 0.63 U

2.0 1.3 ug/L 04/19/18 15:58 04/20/18 05:57 1Atrazine 1.3 U

10 0.59 ug/L 04/19/18 15:58 04/20/18 05:57 1Benzaldehyde 0.59 U

10 1.4 ug/L 04/19/18 15:58 04/20/18 05:57 1Benzo[g,h,i]perylene 1.4 U

1.0 0.67 ug/L 04/19/18 15:58 04/20/18 05:57 1Benzo[k]fluoranthene 0.67 U

10 0.24 ug/L 04/19/18 15:58 04/20/18 05:57 1Bis(2-chloroethoxy)methane 0.24 U

2.0 1.7 ug/L 04/19/18 15:58 04/20/18 05:57 1Bis(2-ethylhexyl) phthalate 1.7 U

10 0.85 ug/L 04/19/18 15:58 04/20/18 05:57 1Butyl benzyl phthalate 0.85 U

10 0.68 ug/L 04/19/18 15:58 04/20/18 05:57 1Caprolactam 0.68 U

10 0.68 ug/L 04/19/18 15:58 04/20/18 05:57 1Carbazole 0.68 U

2.0 0.91 ug/L 04/19/18 15:58 04/20/18 05:57 1Chrysene 0.91 U

1.0 0.72 ug/L 04/19/18 15:58 04/20/18 05:57 1Dibenz(a,h)anthracene 0.72 U

10 1.1 ug/L 04/19/18 15:58 04/20/18 05:57 1Dibenzofuran 1.1 U

10 0.98 ug/L 04/19/18 15:58 04/20/18 05:57 1Diethyl phthalate 0.98 U

10 0.77 ug/L 04/19/18 15:58 04/20/18 05:57 1Dimethyl phthalate 0.77 U

10 0.84 ug/L 04/19/18 15:58 04/20/18 05:57 1Di-n-butyl phthalate 0.84 U

10 4.8 ug/L 04/19/18 15:58 04/20/18 05:57 1Di-n-octyl phthalate 4.8 U

10 0.84 ug/L 04/19/18 15:58 04/20/18 05:57 1Fluoranthene 0.84 U

10 0.91 ug/L 04/19/18 15:58 04/20/18 05:57 1Fluorene 0.91 U

1.0 0.78 ug/L 04/19/18 15:58 04/20/18 05:57 1Hexachlorobutadiene 0.78 U

10 1.7 ug/L 04/19/18 15:58 04/20/18 05:57 1Hexachlorocyclopentadiene 1.7 U

2.0 1.2 ug/L 04/19/18 15:58 04/20/18 05:57 1Hexachloroethane 1.2 U

2.0 1.3 ug/L 04/19/18 15:58 04/20/18 05:57 1Indeno[1,2,3-cd]pyrene 1.3 U

10 0.80 ug/L 04/19/18 15:58 04/20/18 05:57 1Isophorone 0.80 U

10 1.1 ug/L 04/19/18 15:58 04/20/18 05:57 1Naphthalene 1.1 U

1.0 0.57 ug/L 04/19/18 15:58 04/20/18 05:57 1Nitrobenzene 0.57 U

1.0 0.43 ug/L 04/19/18 15:58 04/20/18 05:57 1N-Nitrosodi-n-propylamine 0.43 U

10 0.89 ug/L 04/19/18 15:58 04/20/18 05:57 1N-Nitrosodiphenylamine 0.89 U

10 0.58 ug/L 04/19/18 15:58 04/20/18 05:57 1Phenanthrene 0.58 U

10 0.29 ug/L 04/19/18 15:58 04/20/18 05:57 1Phenol 0.29 U

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Pyrene 1.6 U 10 1.6 ug/L 04/19/18 15:58 04/20/18 05:57 1


10 1.9 ug/L 04/19/18 15:58 04/20/18 05:57 1Pyridine 1.9 U

Tentatively Identified Compound None ug/L 04/19/18 15:58 04/20/18 05:57 1




2-Fluorobiphenyl 92 04/19/18 15:58 04/20/18 05:57 145 - 107



Phenol-d5 (Surr) 33 04/19/18 15:58 04/20/18 05:57 114 - 39

Terphenyl-d14 (Surr) 102 04/19/18 15:58 04/20/18 05:57 140 - 148


4,4'-DDD 0.0060 U 0.020 0.0060 ug/L 04/20/18 08:14 04/23/18 12:35 1


0.020 0.0020 ug/L 04/20/18 08:14 04/23/18 12:35 14,4'-DDE 0.0020 U

0.020 0.0040 ug/L 04/20/18 08:14 04/23/18 12:35 14,4'-DDT 0.0040 U

0.020 0.0030 ug/L 04/20/18 08:14 04/23/18 12:35 1Aldrin 0.0030 U

0.020 0.0070 ug/L 04/20/18 08:14 04/23/18 12:35 1alpha-BHC 0.0070 U

0.020 0.0040 ug/L 04/20/18 08:14 04/23/18 12:35 1beta-BHC 0.0040 U

0.50 0.055 ug/L 04/20/18 08:14 04/23/18 12:35 1Chlordane (technical) 0.055 U

0.020 0.0050 ug/L 04/20/18 08:14 04/23/18 12:35 1delta-BHC 0.0050 U

0.020 0.0030 ug/L 04/20/18 08:14 04/23/18 12:35 1Dieldrin 0.0030 U

0.020 0.0020 ug/L 04/20/18 08:14 04/23/18 12:35 1Endosulfan I 0.0020 U

0.020 0.0040 ug/L 04/20/18 08:14 04/23/18 12:35 1Endosulfan II 0.0040 U

0.020 0.0060 ug/L 04/20/18 08:14 04/23/18 12:35 1Endosulfan sulfate 0.0060 U

0.020 0.0040 ug/L 04/20/18 08:14 04/23/18 12:35 1Endrin 0.0040 U

0.020 0.0080 ug/L 04/20/18 08:14 04/23/18 12:35 1Endrin aldehyde 0.0080 U

0.020 0.0080 ug/L 04/20/18 08:14 04/23/18 12:35 1Endrin ketone 0.0080 U

0.020 0.012 ug/L 04/20/18 08:14 04/23/18 12:35 1gamma-BHC (Lindane) 0.012 U

0.020 0.0030 ug/L 04/20/18 08:14 04/23/18 12:35 1Heptachlor 0.0030 U

0.020 0.0050 ug/L 04/20/18 08:14 04/23/18 12:35 1Heptachlor epoxide 0.0050 U

0.020 0.0040 ug/L 04/20/18 08:14 04/23/18 12:35 1Methoxychlor 0.0040 U

0.50 0.11 ug/L 04/20/18 08:14 04/23/18 12:35 1Toxaphene 0.11 U







Aroclor 1016 0.10 U * 0.40 0.10 ug/L 04/20/18 08:20 04/23/18 15:56 1


0.40 0.10 ug/L 04/20/18 08:20 04/23/18 15:56 1Aroclor 1221 0.10 U

0.40 0.10 ug/L 04/20/18 08:20 04/23/18 15:56 1Aroclor 1232 0.10 U

0.40 0.10 ug/L 04/20/18 08:20 04/23/18 15:56 1Aroclor 1242 0.10 U

0.40 0.10 ug/L 04/20/18 08:20 04/23/18 15:56 1Aroclor 1248 0.10 U

0.40 0.099 ug/L 04/20/18 08:20 04/23/18 15:56 1Aroclor 1254 0.099 U

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Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)RL MDL

Aroclor 1260 0.099 U * 0.40 0.099 ug/L 04/20/18 08:20 04/23/18 15:56 1


0.40 0.099 ug/L 04/20/18 08:20 04/23/18 15:56 1Aroclor-1262 0.099 U

0.40 0.099 ug/L 04/20/18 08:20 04/23/18 15:56 1Aroclor 1268 0.099 U

0.40 0.10 ug/L 04/20/18 08:20 04/23/18 15:56 1Polychlorinated biphenyls, Total 0.10 U





2,4-D 0.13 U 1.2 0.13 ug/L 04/24/18 22:31 04/25/18 11:34 1


1.2 0.11 ug/L 04/24/18 22:31 04/25/18 11:34 1Silvex (2,4,5-TP) 0.11 U

1.2 0.12 ug/L 04/24/18 22:31 04/25/18 11:34 12,4,5-T 0.12 U




Method: 300.0 - Anions, Ion ChromatographyRL MDL

Nitrate as N 2.28 0.10 0.016 mg/L 04/20/18 04:13 1


0.12 0.019 mg/L 04/20/18 04:13 1Nitrite as N 0.019 U

Method: 300.0 - Anions, Ion Chromatography - DLRL MDL

Chloride 51.3 D 2.76 1.79 mg/L 04/20/18 07:40 23



Silver 1.4 U 2.0 1.4 ug/L 04/23/18 09:58 04/24/18 18:37 2


2.0 0.77 ug/L 04/23/18 09:58 04/24/18 18:37 2Arsenic 0.77 U

4.0 1.1 ug/L 04/23/18 09:58 04/24/18 18:37 2Barium 60.1

2.0 0.61 ug/L 04/23/18 09:58 04/24/18 18:37 2Cadmium 0.61 U

4.0 1.3 ug/L 04/23/18 09:58 04/24/18 18:37 2Chromium 1.3 U

1.2 0.37 ug/L 04/23/18 09:58 04/24/18 18:37 2Lead 0.39 J

10.0 0.69 ug/L 04/23/18 09:58 04/24/18 18:37 2Selenium 0.69 U

Method: 7470A - Mercury (CVAA)RL MDL

Mercury 0.12 U 0.20 0.12 ug/L 04/23/18 12:30 04/23/18 14:20 1



pH 7.0 HF SU 04/24/18 12:31 1


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1,1,1-Trichloroethane 0.28 U 1.0 0.28 ug/L 04/23/18 04:36 1


1.0 0.19 ug/L 04/23/18 04:36 11,1,2,2-Tetrachloroethane 0.19 U *

1.0 0.34 ug/L 04/23/18 04:36 11,1,2-Trichloro-1,2,2-trifluoroethane 0.34 U

1.0 0.080 ug/L 04/23/18 04:36 11,1,2-Trichloroethane 0.080 U


1.0 0.34 ug/L 04/23/18 04:36 11,1-Dichloroethene 0.34 U



1.0 0.23 ug/L 04/23/18 04:36 11,2-Dibromo-3-Chloropropane 0.23 U



1.0 0.18 ug/L 04/23/18 04:36 11,2-Dichloropropane 0.18 U



50 8.7 ug/L 04/23/18 04:36 11,4-Dioxane 8.7 U

5.0 2.2 ug/L 04/23/18 04:36 12-Butanone (MEK) 2.2 U

5.0 0.72 ug/L 04/23/18 04:36 12-Hexanone 0.72 U

5.0 0.63 ug/L 04/23/18 04:36 14-Methyl-2-pentanone (MIBK) 0.63 U

5.0 1.1 ug/L 04/23/18 04:36 1Acetone 1.1 U

1.0 0.090 ug/L 04/23/18 04:36 1Benzene 0.090 U

1.0 0.18 ug/L 04/23/18 04:36 1Bromoform 0.18 U

1.0 0.18 ug/L 04/23/18 04:36 1Bromomethane 0.18 U

1.0 0.22 ug/L 04/23/18 04:36 1Carbon disulfide 0.22 U

1.0 0.33 ug/L 04/23/18 04:36 1Carbon tetrachloride 0.33 U

1.0 0.24 ug/L 04/23/18 04:36 1Chlorobenzene 0.24 U

1.0 0.30 ug/L 04/23/18 04:36 1Chlorobromomethane 0.30 U

1.0 0.22 ug/L 04/23/18 04:36 1Chlorodibromomethane 0.22 U

1.0 0.37 ug/L 04/23/18 04:36 1Chloroethane 0.37 U

1.0 0.22 ug/L 04/23/18 04:36 1Chloroform 0.38 J

1.0 0.22 ug/L 04/23/18 04:36 1Chloromethane 0.22 U

1.0 0.26 ug/L 04/23/18 04:36 1cis-1,2-Dichloroethene 0.26 U

1.0 0.16 ug/L 04/23/18 04:36 1cis-1,3-Dichloropropene 0.16 U

1.0 0.26 ug/L 04/23/18 04:36 1Cyclohexane 0.26 U

1.0 0.15 ug/L 04/23/18 04:36 1Dichlorobromomethane 0.15 U

1.0 0.14 ug/L 04/23/18 04:36 1Dichlorodifluoromethane 0.14 U

1.0 0.30 ug/L 04/23/18 04:36 1Ethylbenzene 0.30 U

1.0 0.19 ug/L 04/23/18 04:36 1Ethylene Dibromide 0.19 U

1.0 0.32 ug/L 04/23/18 04:36 1Isopropylbenzene 0.32 U

5.0 0.58 ug/L 04/23/18 04:36 1Methyl acetate 0.58 U

1.0 0.13 ug/L 04/23/18 04:36 1Methyl tert-butyl ether 0.13 U

1.0 0.22 ug/L 04/23/18 04:36 1Methylcyclohexane 0.22 U

1.0 0.21 ug/L 04/23/18 04:36 1Methylene Chloride 0.21 U

1.0 0.28 ug/L 04/23/18 04:36 1m-Xylene & p-Xylene 0.28 U

1.0 0.32 ug/L 04/23/18 04:36 1o-Xylene 0.32 U

1.0 0.17 ug/L 04/23/18 04:36 1Styrene 0.17 U

1.0 0.12 ug/L 04/23/18 04:36 1Tetrachloroethene 0.12 U

1.0 0.25 ug/L 04/23/18 04:36 1Toluene 0.25 U

1.0 0.18 ug/L 04/23/18 04:36 1trans-1,2-Dichloroethene 0.18 U

1.0 0.19 ug/L 04/23/18 04:36 1trans-1,3-Dichloropropene 0.19 U

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Trichloroethene 0.22 U 1.0 0.22 ug/L 04/23/18 04:36 1


1.0 0.15 ug/L 04/23/18 04:36 1Trichlorofluoromethane 0.15 U

1.0 0.060 ug/L 04/23/18 04:36 1Vinyl chloride 0.060 U

Tentatively Identified Compound None ug/L 04/23/18 04:36 1


1,2-Dichloroethane-d4 (Surr) 113 74 - 132 04/23/18 04:36 1


4-Bromofluorobenzene 88 04/23/18 04:36 177 - 124

Dibromofluoromethane (Surr) 97 04/23/18 04:36 172 - 131

Toluene-d8 (Surr) 105 04/23/18 04:36 180 - 120

Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL

Benzo[a]anthracene 0.016 U 0.050 0.016 ug/L 04/19/18 15:58 04/20/18 03:22 1


0.050 0.022 ug/L 04/19/18 15:58 04/20/18 03:22 1Benzo[a]pyrene 0.022 U

0.050 0.024 ug/L 04/19/18 15:58 04/20/18 03:22 1Benzo[b]fluoranthene 0.024 U

0.030 0.026 ug/L 04/19/18 15:58 04/20/18 03:22 1Bis(2-chloroethyl)ether 0.026 U

0.020 0.013 ug/L 04/19/18 15:58 04/20/18 03:22 1Hexachlorobenzene 0.013 U

0.20 0.12 ug/L 04/19/18 15:58 04/20/18 03:22 1N-Nitrosodimethylamine 1.1

0.20 0.15 ug/L 04/19/18 15:58 04/20/18 03:22 1Pentachlorophenol 0.15 U


1,1'-Biphenyl 1.2 U 10 1.2 ug/L 04/19/18 15:58 04/20/18 06:18 1


10 1.2 ug/L 04/19/18 15:58 04/20/18 06:18 11,2,4,5-Tetrachlorobenzene 1.2 U

10 1.3 ug/L 04/19/18 15:58 04/20/18 06:18 11,4-Dichlorobenzene 1.3 U

10 0.63 ug/L 04/19/18 15:58 04/20/18 06:18 12,2'-oxybis[1-chloropropane] 0.63 U

10 0.75 ug/L 04/19/18 15:58 04/20/18 06:18 12,3,4,6-Tetrachlorophenol 0.75 U



10 0.42 ug/L 04/19/18 15:58 04/20/18 06:18 12,4-Dichlorophenol 0.42 U

10 0.24 ug/L 04/19/18 15:58 04/20/18 06:18 12,4-Dimethylphenol 0.24 U

20 14 ug/L 04/19/18 15:58 04/20/18 06:18 12,4-Dinitrophenol 14 U



10 1.2 ug/L 04/19/18 15:58 04/20/18 06:18 12-Chloronaphthalene 1.2 U

10 0.38 ug/L 04/19/18 15:58 04/20/18 06:18 12-Chlorophenol 0.38 U

10 1.1 ug/L 04/19/18 15:58 04/20/18 06:18 12-Methylnaphthalene 1.1 U




10 0.24 ug/L 04/19/18 15:58 04/20/18 06:18 13 & 4 Methylphenol 0.24 U

10 1.4 ug/L 04/19/18 15:58 04/20/18 06:18 13,3'-Dichlorobenzidine 1.4 U


20 13 ug/L 04/19/18 15:58 04/20/18 06:18 14,6-Dinitro-2-methylphenol 13 U

10 0.75 ug/L 04/19/18 15:58 04/20/18 06:18 14-Bromophenyl phenyl ether 0.75 U

10 0.58 ug/L 04/19/18 15:58 04/20/18 06:18 14-Chloro-3-methylphenol 0.58 U

10 1.9 ug/L 04/19/18 15:58 04/20/18 06:18 14-Chloroaniline 1.9 U

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4-Chlorophenyl phenyl ether 1.3 U 10 1.3 ug/L 04/19/18 15:58 04/20/18 06:18 1





10 1.1 ug/L 04/19/18 15:58 04/20/18 06:18 1Acenaphthene 1.1 U

10 0.82 ug/L 04/19/18 15:58 04/20/18 06:18 1Acenaphthylene 0.82 U

10 0.79 ug/L 04/19/18 15:58 04/20/18 06:18 1Acetophenone 0.79 U

10 0.63 ug/L 04/19/18 15:58 04/20/18 06:18 1Anthracene 0.63 U

2.0 1.3 ug/L 04/19/18 15:58 04/20/18 06:18 1Atrazine 1.3 U

10 0.59 ug/L 04/19/18 15:58 04/20/18 06:18 1Benzaldehyde 0.59 U

10 1.4 ug/L 04/19/18 15:58 04/20/18 06:18 1Benzo[g,h,i]perylene 1.4 U

1.0 0.67 ug/L 04/19/18 15:58 04/20/18 06:18 1Benzo[k]fluoranthene 0.67 U

10 0.24 ug/L 04/19/18 15:58 04/20/18 06:18 1Bis(2-chloroethoxy)methane 0.24 U

2.0 1.7 ug/L 04/19/18 15:58 04/20/18 06:18 1Bis(2-ethylhexyl) phthalate 1.7 U

10 0.85 ug/L 04/19/18 15:58 04/20/18 06:18 1Butyl benzyl phthalate 0.85 U

10 0.68 ug/L 04/19/18 15:58 04/20/18 06:18 1Caprolactam 0.68 U

10 0.68 ug/L 04/19/18 15:58 04/20/18 06:18 1Carbazole 0.68 U

2.0 0.91 ug/L 04/19/18 15:58 04/20/18 06:18 1Chrysene 0.91 U

1.0 0.72 ug/L 04/19/18 15:58 04/20/18 06:18 1Dibenz(a,h)anthracene 0.72 U

10 1.1 ug/L 04/19/18 15:58 04/20/18 06:18 1Dibenzofuran 1.1 U

10 0.98 ug/L 04/19/18 15:58 04/20/18 06:18 1Diethyl phthalate 0.98 U

10 0.77 ug/L 04/19/18 15:58 04/20/18 06:18 1Dimethyl phthalate 0.77 U

10 0.84 ug/L 04/19/18 15:58 04/20/18 06:18 1Di-n-butyl phthalate 0.84 U

10 4.8 ug/L 04/19/18 15:58 04/20/18 06:18 1Di-n-octyl phthalate 4.8 U

10 0.84 ug/L 04/19/18 15:58 04/20/18 06:18 1Fluoranthene 0.84 U

10 0.91 ug/L 04/19/18 15:58 04/20/18 06:18 1Fluorene 0.91 U

1.0 0.78 ug/L 04/19/18 15:58 04/20/18 06:18 1Hexachlorobutadiene 0.78 U

10 1.7 ug/L 04/19/18 15:58 04/20/18 06:18 1Hexachlorocyclopentadiene 1.7 U

2.0 1.2 ug/L 04/19/18 15:58 04/20/18 06:18 1Hexachloroethane 1.2 U

2.0 1.3 ug/L 04/19/18 15:58 04/20/18 06:18 1Indeno[1,2,3-cd]pyrene 1.3 U

10 0.80 ug/L 04/19/18 15:58 04/20/18 06:18 1Isophorone 0.80 U

10 1.1 ug/L 04/19/18 15:58 04/20/18 06:18 1Naphthalene 1.1 U

1.0 0.57 ug/L 04/19/18 15:58 04/20/18 06:18 1Nitrobenzene 0.57 U

1.0 0.43 ug/L 04/19/18 15:58 04/20/18 06:18 1N-Nitrosodi-n-propylamine 0.43 U

10 0.89 ug/L 04/19/18 15:58 04/20/18 06:18 1N-Nitrosodiphenylamine 0.89 U

10 0.58 ug/L 04/19/18 15:58 04/20/18 06:18 1Phenanthrene 0.58 U

10 0.29 ug/L 04/19/18 15:58 04/20/18 06:18 1Phenol 0.29 U

10 1.6 ug/L 04/19/18 15:58 04/20/18 06:18 1Pyrene 1.6 U

10 1.9 ug/L 04/19/18 15:58 04/20/18 06:18 1Pyridine 1.9 U

Formamide, N,N-dimethyl- 7.5 J N ug/L 2.40 68-12-2 04/19/18 15:58 04/20/18 06:18 1


104/20/18 06:1804/19/18 15:58J NUrea, tetramethyl- 632-22-443 ug/L 4.21

104/20/18 06:1804/19/18 15:58JUnknown 34 ug/L 6.40

104/20/18 06:1804/19/18 15:58JUnknown 13 ug/L 7.45

104/20/18 06:1804/19/18 15:58JUnknown 31 ug/L 7.67

104/20/18 06:1804/19/18 15:58JUnknown 43 ug/L 9.62

104/20/18 06:1804/19/18 15:58J NPhenol, 4,4'-(1-methylethylidene)bis- 80-05-77.0 ug/L 10.17

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2-Fluorobiphenyl 93 04/19/18 15:58 04/20/18 06:18 145 - 107



Phenol-d5 (Surr) 33 04/19/18 15:58 04/20/18 06:18 114 - 39

Terphenyl-d14 (Surr) 101 04/19/18 15:58 04/20/18 06:18 140 - 148


4,4'-DDD 0.0060 U 0.020 0.0060 ug/L 04/20/18 08:14 04/23/18 13:04 1


0.020 0.0020 ug/L 04/20/18 08:14 04/23/18 13:04 14,4'-DDE 0.0020 U

0.020 0.0040 ug/L 04/20/18 08:14 04/23/18 13:04 14,4'-DDT 0.0040 U

0.020 0.0030 ug/L 04/20/18 08:14 04/23/18 13:04 1Aldrin 0.0030 U

0.020 0.0070 ug/L 04/20/18 08:14 04/23/18 13:04 1alpha-BHC 0.0070 U

0.020 0.0040 ug/L 04/20/18 08:14 04/23/18 13:04 1beta-BHC 0.0040 U

0.50 0.055 ug/L 04/20/18 08:14 04/23/18 13:04 1Chlordane (technical) 0.055 U

0.020 0.0050 ug/L 04/20/18 08:14 04/23/18 13:04 1delta-BHC 0.0050 U

0.020 0.0030 ug/L 04/20/18 08:14 04/23/18 13:04 1Dieldrin 0.0030 U

0.020 0.0020 ug/L 04/20/18 08:14 04/23/18 13:04 1Endosulfan I 0.0020 U

0.020 0.0040 ug/L 04/20/18 08:14 04/23/18 13:04 1Endosulfan II 0.0040 U

0.020 0.0060 ug/L 04/20/18 08:14 04/23/18 13:04 1Endosulfan sulfate 0.0060 U

0.020 0.0040 ug/L 04/20/18 08:14 04/23/18 13:04 1Endrin 0.0040 U

0.020 0.0080 ug/L 04/20/18 08:14 04/23/18 13:04 1Endrin aldehyde 0.0080 U

0.020 0.0080 ug/L 04/20/18 08:14 04/23/18 13:04 1Endrin ketone 0.0080 U

0.020 0.012 ug/L 04/20/18 08:14 04/23/18 13:04 1gamma-BHC (Lindane) 0.012 U

0.020 0.0030 ug/L 04/20/18 08:14 04/23/18 13:04 1Heptachlor 0.0030 U

0.020 0.0050 ug/L 04/20/18 08:14 04/23/18 13:04 1Heptachlor epoxide 0.0050 U

0.020 0.0040 ug/L 04/20/18 08:14 04/23/18 13:04 1Methoxychlor 0.0040 U

0.50 0.11 ug/L 04/20/18 08:14 04/23/18 13:04 1Toxaphene 0.11 U







Aroclor 1016 0.10 U * 0.40 0.10 ug/L 04/20/18 08:20 04/23/18 16:14 1


0.40 0.10 ug/L 04/20/18 08:20 04/23/18 16:14 1Aroclor 1221 0.10 U

0.40 0.10 ug/L 04/20/18 08:20 04/23/18 16:14 1Aroclor 1232 0.10 U

0.40 0.10 ug/L 04/20/18 08:20 04/23/18 16:14 1Aroclor 1242 0.10 U

0.40 0.10 ug/L 04/20/18 08:20 04/23/18 16:14 1Aroclor 1248 0.10 U

0.40 0.099 ug/L 04/20/18 08:20 04/23/18 16:14 1Aroclor 1254 0.099 U

0.40 0.099 ug/L 04/20/18 08:20 04/23/18 16:14 1Aroclor 1260 0.099 U *

0.40 0.099 ug/L 04/20/18 08:20 04/23/18 16:14 1Aroclor-1262 0.099 U

0.40 0.099 ug/L 04/20/18 08:20 04/23/18 16:14 1Aroclor 1268 0.099 U

0.40 0.10 ug/L 04/20/18 08:20 04/23/18 16:14 1Polychlorinated biphenyls, Total 0.10 U



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Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)




2,4-D 0.13 U 1.2 0.13 ug/L 04/24/18 22:31 04/25/18 11:49 1


1.2 0.11 ug/L 04/24/18 22:31 04/25/18 11:49 1Silvex (2,4,5-TP) 0.11 U

1.2 0.12 ug/L 04/24/18 22:31 04/25/18 11:49 12,4,5-T 0.12 U




Method: 300.0 - Anions, Ion ChromatographyRL MDL

Nitrate as N 0.10 0.10 0.016 mg/L 04/20/18 04:29 1


0.12 0.019 mg/L 04/20/18 04:29 1Nitrite as N 0.019 U F1

Method: 300.0 - Anions, Ion Chromatography - DLRL MDL

Chloride 63.6 D F1 2.76 1.79 mg/L 04/20/18 07:55 23



Silver 1.4 U 2.0 1.4 ug/L 04/23/18 09:58 04/24/18 18:39 2


2.0 0.77 ug/L 04/23/18 09:58 04/24/18 18:39 2Arsenic 0.77 U

4.0 1.1 ug/L 04/23/18 09:58 04/24/18 18:39 2Barium 62.9

2.0 0.61 ug/L 04/23/18 09:58 04/24/18 18:39 2Cadmium 1.3 J

4.0 1.3 ug/L 04/23/18 09:58 04/24/18 18:39 2Chromium 1.3 U

1.2 0.37 ug/L 04/23/18 09:58 04/24/18 18:39 2Lead 12.2

10.0 0.69 ug/L 04/23/18 09:58 04/24/18 18:39 2Selenium 0.69 U

Method: 7470A - Mercury (CVAA)RL MDL

Mercury 0.12 U 0.20 0.12 ug/L 04/23/18 12:30 04/23/18 14:22 1



pH 5.6 HF SU 04/24/18 12:34 1


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Lab ChronicleClient: Boucher & James Inc TestAmerica Job ID: 460-154197-1Project/Site: SAITH

Client Sample ID: 177229E-S1 Lab Sample ID: 460-154197-1Matrix: SolidDate Collected: 04/18/18 10:50


Analysis Moisture 04/19/18 12:36 BJP1 512413 TAL EDI

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



Prep 5035 04/19/18 00:20 AVM512235 TAL EDI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8260C 1 513199 04/23/18 03:39 AAT TAL EDITotal/NA

Prep 3546 512975 04/21/18 07:17 ANM TAL EDITotal/NA

Analysis 8270D 2 513246 04/23/18 17:04 DAN TAL EDITotal/NA

Prep 3546 512562 04/19/18 22:17 ARA TAL EDITotal/NA

Analysis 8081B 1 512794 04/20/18 16:04 SAK TAL EDITotal/NA


Analysis 8082A 1 512820 04/20/18 22:42 JXZ TAL EDITotal/NA

Prep 8151A 513518 04/23/18 20:56 JMS TAL EDITotal/NA

Analysis 8151A 1 513637 04/24/18 09:05 SAK TAL EDITotal/NA

Prep 3050B 514229 04/26/18 04:27 TLA TAL EDITotal/NA

Analysis 6020A 20 514435 04/26/18 15:51 PHP TAL EDITotal/NA

Prep 7471B 512630 04/20/18 04:46 TJS TAL EDITotal/NA

Analysis 7471B 1 512760 04/20/18 09:46 TJS TAL EDITotal/NA



Analysis Moisture 04/19/18 12:36 BJP1 512413 TAL EDI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



Prep 5035 04/19/18 00:20 AVM512235 TAL EDI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8260C 1 513775 04/25/18 01:55 MZS TAL EDITotal/NA

Prep 3546 512975 04/21/18 07:17 ANM TAL EDITotal/NA





Analysis 8082A 1 512820 04/20/18 22:59 JXZ TAL EDITotal/NA

Prep 8151A 513518 04/23/18 20:56 JMS TAL EDITotal/NA

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Analysis 8151A 04/24/18 09:20 SAK1 513637 TAL EDI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Prep 3050B 514229 04/26/18 04:27 TLA TAL EDITotal/NA


Prep 7471B 512630 04/20/18 04:46 TJS TAL EDITotal/NA

Analysis 7471B 1 512760 04/20/18 09:48 TJS TAL EDITotal/NA

Client Sample ID: 177229E-W1 Lab Sample ID: 460-154197-3Matrix: WaterDate Collected: 04/18/18 09:25


Analysis 8260C 04/23/18 04:12 MZS1 513220 TAL EDI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Prep 3510C 512456 04/19/18 15:58 MIS TAL EDITotal/NA



Analysis 8270D SIM 1 512603 04/20/18 08:56 DAN TAL EDITotal/NA

Prep 3510C 512703 04/20/18 08:14 ANM TAL EDITotal/NA



Analysis 8082A 1 513329 04/23/18 15:56 CDC TAL EDITotal/NA

Prep 8151A 513872 04/24/18 22:31 AFR TAL EDITotal/NA


Analysis 300.0 1 512532 04/20/18 04:13 MJA TAL EDITotal/NA

Analysis 300.0 DL 23 512531 04/20/18 07:40 MJA TAL EDITotal/NA

Prep 3010A 513348 04/23/18 09:58 QZY TAL EDITotal/NA


Prep 7470A 513378 04/23/18 12:30 RBS TAL EDITotal/NA

Analysis 7470A 1 513425 04/23/18 14:20 RBS TAL EDITotal/NA

Analysis 9040C 1 513772 04/24/18 12:31 YAH TAL EDITotal/NA



Analysis 8260C 04/23/18 04:36 MZS1 513220 TAL EDI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Analysis 8270D SIM 1 512603 04/20/18 03:22 DAN TAL EDITotal/NA




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Analysis 8082A 04/23/18 16:14 CDC1 513329 TAL EDI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Prep 8151A 513872 04/24/18 22:31 AFR TAL EDITotal/NA


Analysis 300.0 1 512532 04/20/18 04:29 MJA TAL EDITotal/NA

Analysis 300.0 DL 23 512531 04/20/18 07:55 MJA TAL EDITotal/NA

Prep 3010A 513348 04/23/18 09:58 QZY TAL EDITotal/NA


Prep 7470A 513378 04/23/18 12:30 RBS TAL EDITotal/NA

Analysis 7470A 1 513425 04/23/18 14:22 RBS TAL EDITotal/NA

Analysis 9040C 1 513772 04/24/18 12:34 YAH TAL EDITotal/NA

Laboratory References:

TAL EDI = TestAmerica Edison, 777 New Durham Road, Edison, NJ 08817, TEL (732)549-3900

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Accreditation/Certification SummaryClient: Boucher & James Inc TestAmerica Job ID: 460-154197-1Project/Site: SAITH

Laboratory: TestAmerica EdisonUnless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.

Authority Program EPA Region Identification Number Expiration Date

Pennsylvania 68-005223NELAP 02-28-19

Analysis Method Prep Method Matrix Analyte

The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:

8082A 3510C Water Aroclor 1016








8082A 3510C Water Aroclor-1262

8082A 3510C Water Polychlorinated biphenyls, Total

8082A 3546 Solid Polychlorinated biphenyls, Total

8260C Water cis-1,2-Dichloroethene

8270D 3510C Water 4-Methylphenol

8270D 3546 Solid 4-Methylphenol

8270D SIM 3510C Water Bis(2-chloroethyl)ether

Moisture Solid Percent Moisture

Moisture Solid Percent Solids

TestAmerica Edison

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Method SummaryTestAmerica Job ID: 460-154197-1Client: Boucher & James Inc

Project/Site: SAITH

Method Method Description LaboratoryProtocol

SW8468260C Volatile Organic Compounds by GC/MS TAL EDI

SW8468270D Semivolatile Organic Compounds (GC/MS) TAL EDI

SW8468270D SIM Semivolatile Organic Compounds (GC/MS SIM) TAL EDI

SW8468081B Organochlorine Pesticides (GC) TAL EDI

SW8468082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL EDI

SW8468151A Herbicides (GC) TAL EDI

MCAWW300.0 Anions, Ion Chromatography TAL EDI

SW8466020A Metals (ICP/MS) TAL EDI

SW8467470A Mercury (CVAA) TAL EDI

SW8467471B Mercury (CVAA) TAL EDI

SW8469040C pH TAL EDI

EPAMoisture Percent Moisture TAL EDI

SW8463010A Preparation, Total Metals TAL EDI

SW8463050B Preparation, Metals TAL EDI

SW8463510C Liquid-Liquid Extraction (Separatory Funnel) TAL EDI

SW8463546 Microwave Extraction TAL EDI

SW8465030C Purge and Trap TAL EDI

SW8465035 Closed System Purge and Trap TAL EDI

SW8467470A Preparation, Mercury TAL EDI

SW8467471B Preparation, Mercury TAL EDI

SW8468151A Extraction (Herbicides) TAL EDI

Protocol References:

EPA = US Environmental Protection Agency

MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL EDI = TestAmerica Edison, 777 New Durham Road, Edison, NJ 08817, TEL (732)549-3900

TestAmerica Edison

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Sample SummaryTestAmerica Job ID: 460-154197-1Client: Boucher & James Inc

Project/Site: SAITH

Lab Sample ID Client Sample ID ReceivedCollectedMatrix

460-154197-1 177229E-S1 Solid 04/18/18 10:50 04/18/18 12:24

460-154197-2 177229E-S2 Solid 04/18/18 11:05 04/18/18 12:24

460-154197-3 177229E-W1 Water 04/18/18 09:25 04/18/18 12:24

460-154197-4 177229E-W2 Water 04/18/18 10:27 04/18/18 12:24

TestAmerica Edison

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Login Sample Receipt Checklist

Client: Boucher & James Inc Job Number: 460-154197-1

Login Number: 154197

Question Answer Comment

Creator: Gilmore, Julie L

List Source: TestAmerica Edison

List Number: 1

N/ARadioactivity wasn't checked or is </= background as measured by a survey meter.

N/AThe cooler's custody seal, if present, is intact.

N/ASample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable. IR KOP#1 2.4, 3.4

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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