02/14/2013 Calvin Yang Invoice Central Valley Regional Water … · 2017-10-26 · Magnesium EPA...

Central Valley Regional Water Quality Control Boar

Rancho Cordova, CA 95670

11020 Sun Center Drive, Suite 200

Stephane Maupas For PM Staff

Project Manager

Thank you for selecting BSK Associates for your analytical testing needs . We have prepared this

report in response to your request for analytical services. Enclosed are the results of analyses for

samples received by the laboratory on 01/31/2013 09:40.

If additional clarification of any information is required, please contact your Client Services

Representative, PM Staff at (800) 877-8310 or (559) 497-2888.

BSK ASSOCIATES

02/14/2013

Dear Calvin Yang,

A3A2257

Calvin Yang Invoice

A303834

1414 Stanislaus Street Fresno, CA 93706 (559) 497-2888 FAX (559) 485-6935 www.bsklabs.com

An Employee-Owned Company | Analytical Testing | Construction Observation

Environmental Engineering | Geotechnical Engineering | Materials Testing

A3A2257 FINAL 02142013 1632

Page 1 of 59

Case Narrative

02/14/2013

Work Order Information

Client Name:

Client Code: centr4730


Work Order: A3A2257

Project: Evaluation WQ in Ag Dominated Water Bodies

Submitted by: Calvin Yang

ONTRACShipped by:

COC Number:

TAT: 10

PO #: 11-123-555

Sample Receipt Conditions

Cooler #2 0.6Cooler: Temp. ºC:

Containers Intact

COC/Labels Agree

Received On Wet Ice

Packing Material - Bubble Wrap

Packing Material - Foam

Sample(s) were received in temperature range.

Initial receipt at BSK-SAC

Default Cooler 0.9Cooler: Temp. ºC:

Containers Intact

COC/Labels Agree

Received On Wet Ice

Packing Material - Bubble Wrap

Packing Material - Foam

Sample(s) were received in temperature range.

Initial receipt at BSK-SAC

Report Manager Report Format

Calvin Yang Final.rpt




A3A2257 FINAL 02142013 1632

Page 2 of 59

Certificate of Analysis


Report Issue Date:Received Date:

Received Time:11020 Sun Center Drive, Suite 200


02/14/2013 16:32Calvin Yang01/31/2013

09:40

CCY130130-10Sample Description:

Lab Sample ID:

Sample Date: 01/30/2013 07:46 Sampled by: Calvin Yang

Matrix: Surface WaterSample Type: Grab

A3A2257-01

General Chemistry

ResultAnalyte RL Prepared AnalyzedRL

MultUnitsMethod Batch Qual

0.10 mg/LAmmonia as N SM

4500-NH3 G

02/05/13 02/07/13A301269* B1.1ND 1

1.0 mg/LChloride EPA 300.0 01/31/13 01/31/13A3011671.3 1

1.0 umhos/cmConductivity @ 25C SM 2510 B 01/31/13 01/31/13A30118489 1

0.10 mg/LFluoride SM 4500-F C 02/06/13 02/06/13A301347ND 1

0.22 mg/LNitrate as N EPA 300.0 01/31/13 13:29 01/31/13 13:29A301167ND 1

2.0 ug/LPerchlorate EPA 314.0 02/06/13 02/06/13A301364ND 1

2.0 mg/LSulfate as SO4 EPA 300.0 01/31/13 01/31/13A301167ND 1

5.0 mg/LTotal Dissolved Solids SM 2540C 02/01/13 02/05/13A30119758 1

Metals



5.0 ug/LAluminum EPA 200.8

DRC

02/06/13 02/07/13A301342* 56 1

5.0 ug/LAluminum - Dissolved (1) EPA 200.8

DRC

02/07/13 02/12/13A301406* ND 1

0.50 ug/LAntimony EPA 200.8

DRC

02/06/13 02/07/13A301342* ND 1

0.10 ug/LArsenic EPA 200.8

DRC

02/06/13 02/08/13A301342* 0.35 1

0.10 ug/LArsenic - Dissolved (1) EPA 200.8

DRC

02/07/13 02/08/13A301406* 0.33 1

1.0 ug/LBarium EPA 200.8

DRC

02/06/13 02/07/13A301342* 5.6 1

0.50 ug/LBeryllium EPA 200.8

DRC

02/06/13 02/07/13A301342* ND 1

10 ug/LBoron EPA 200.8 02/04/13 02/12/13A301233* 19 1

0.25 ug/LCadmium EPA 200.8

DRC

02/06/13 02/08/13A301342* ND 1

0.10 mg/LCalcium EPA 200.7 02/04/13 02/07/13A3012339.0 1

0.50 ug/LChromium EPA 200.8

DRC

02/06/13 02/07/13A301342* ND 1

0.50 ug/LCopper EPA 200.8

DRC

02/06/13 02/07/13A301342* 0.53 1

0.41 mg/LHardness as CaCO3 SM 2340B 40

10 ug/LIron EPA 200.8

DRC

02/06/13 02/07/13A301342* 73 1

10 ug/LIron - Dissolved (1) EPA 200.8

DRC

02/07/13 02/12/13A301406* ND 1




A3A2257 FINAL 02142013 1632

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02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-01

Metals



0.10 ug/LLead EPA 200.8

DRC

02/06/13 02/07/13A301342* ND 1

0.10 mg/LMagnesium EPA 200.7 02/04/13 02/07/13A3012334.3 1

1.0 ug/LManganese EPA 200.8

DRC

02/06/13 02/07/13A301342* 8.8 1

1.0 ug/LManganese - Dissolved (1) EPA 200.8

DRC

02/07/13 02/12/13A301406* 3.4 1

0.20 ug/LMercury EPA 200.8 02/04/13 02/12/13A301233ND 1

1.0 ug/LNickel EPA 200.8

DRC

02/06/13 02/07/13A301342* ND 1

1.0 ug/LSelenium EPA 200.8

DRC

02/06/13 02/07/13A301342* ND 1

1.0 ug/LSilver EPA 200.8

DRC

02/11/13 02/12/13A301500* ND 1

1.0 mg/LSodium EPA 200.7 02/04/13 02/07/13A3012333.2 1

1.0 ug/LThallium EPA 200.8

DRC

02/06/13 02/07/13A301342* ND 1

5.0 ug/LZinc EPA 200.8

DRC

02/06/13 02/07/13A301342* ND 1




A3A2257 FINAL 02142013 1632

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02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-02

General Chemistry




4500-NH3 G

02/11/13 02/11/13A301517* ND 1



0.10 mg/LFluoride SM 4500-F C 02/06/13 02/06/13A3013470.14 1

0.22 mg/LNitrate as N EPA 300.0 01/31/13 13:38 01/31/13 13:38A3011670.93 1


2.0 mg/LSulfate as SO4 EPA 300.0 01/31/13 01/31/13A30116714 1


Metals




DRC

02/07/13 02/07/13A301404* 2600 1


DRC

02/07/13 02/12/13A301406* 6.7 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/08/13A301404* 4.1 1


DRC

02/07/13 02/08/13A301406* 2.8 1


DRC

02/07/13 02/07/13A301404* 130 1


DRC

02/07/13 02/07/13A301404* ND 1

10 ug/LBoron EPA 200.8 02/04/13 02/12/13A301233* 31 1


DRC

02/07/13 02/08/13A301404* ND 1

0.10 mg/LCalcium EPA 200.7 02/04/13 02/07/13A30123339 1


DRC

02/07/13 02/07/13A301404* 6.5 1


DRC

02/07/13 02/07/13A301404* 7.2 1



DRC

02/07/13 02/07/13A301404* 2700 1


DRC

02/07/13 02/12/13A301406* 21 1




A3A2257 FINAL 02142013 1632

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02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-02

Metals




DRC

02/07/13 02/12/13A301404* 0.91 1

0.10 mg/LMagnesium EPA 200.7 02/04/13 02/07/13A30123328 1


DRC

02/07/13 02/07/13A301404* 350 1


DRC

02/07/13 02/12/13A301406* 120 1



DRC

02/07/13 02/07/13A301404* 8.1 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1

1.0 mg/LSodium EPA 200.7 02/04/13 02/07/13A30123320 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* 6.7 1




A3A2257 FINAL 02142013 1632

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02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:


Matrix: Waste WaterSample Type: Grab

A3A2257-03

General Chemistry




4500-NH3 G

02/05/13 02/07/13A301269* B1.35.4 1

1.0 mg/LChloride EPA 300.0 01/31/13 01/31/13A30116732 1




10 ug/LPerchlorate EPA 314.0 02/07/13 02/07/13A301483 DL01ND 5



Metals




DRC

02/07/13 02/07/13A301404* 12 1


DRC

02/07/13 02/12/13A301406* 5.4 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/08/13A301404* 4.2 1


DRC

02/07/13 02/08/13A301406* 3.4 1


DRC

02/07/13 02/07/13A301404* 79 1


DRC

02/07/13 02/07/13A301404* ND 1

10 ug/LBoron EPA 200.8 02/04/13 02/12/13A301233* 82 1


DRC

02/07/13 02/08/13A301404* ND 1

0.10 mg/LCalcium EPA 200.7 02/04/13 02/07/13A30123344 1


DRC

02/07/13 02/07/13A301404* 2.0 1


DRC

02/07/13 02/07/13A301404* 2.8 1



DRC

02/07/13 02/07/13A301404* 990 1


DRC

02/07/13 02/12/13A301406* 75 1




A3A2257 FINAL 02142013 1632

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02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-03

Metals




DRC

02/07/13 02/12/13A301404* ND 1



DRC

02/07/13 02/07/13A301404* 37 1


DRC

02/07/13 02/12/13A301406* 25 1



DRC

02/07/13 02/07/13A301404* 1.9 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1

1.0 mg/LSodium EPA 200.7 02/04/13 02/07/13A30123345 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1

Organics



Volatile Organics (Standard List) by GC-MS

0.50 ug/L1,1,1,2-Tetrachloroethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/L1,1,1-Trichloroethane EPA 8260B 01/31/13 02/01/13A301200* ND 1


5.0 ug/L1,1,2-Trichloro-1,2,2-trifluoroethane EPA 8260B 01/31/13 02/01/13A301200* ND 1


0.50 ug/L1,1-Dichloroethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/L1,1-Dichloroethene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/L1,1-Dichloropropene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/L1,2,3-Trichlorobenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/L1,2,3-Trichloropropane EPA 8260B 01/31/13 02/01/13A301200* ND 1


5.0 ug/L1,2,4-Trimethylbenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/L1,2-Dibromoethane (EDB) EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/L1,2-Dichlorobenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1


0.50 ug/L1,2-Dichloropropane EPA 8260B 01/31/13 02/01/13A301200* ND 1




A3A2257 FINAL 02142013 1632

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02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-03

Organics









20 ug/L2-Butanone EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/L2-Chlorotoluene EPA 8260B 01/31/13 02/01/13A301200* ND 1

20 ug/L2-Hexanone EPA 8260B 01/31/13 02/01/13A301200* ND 1


20 ug/L4-Methyl-2-pentanone EPA 8260B 01/31/13 02/01/13A301200* ND 1

20 ug/LAcetone EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LBenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LBromobenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/LBromochloromethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LBromodichloromethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LBromoform EPA 8260B 01/31/13 02/01/13A301200* ND 1

1.0 ug/LBromomethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

50 ug/LCarbon disulfide EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LCarbon Tetrachloride EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LChlorobenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LChloroethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LChloroform EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LChloromethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/Lcis-1,2-Dichloroethene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/Lcis-1,3-Dichloropropene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LDibromochloromethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/LDibromochloropropane (DBCP) EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LDibromomethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

1.0 ug/LDichlorodifluoromethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LDichloromethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LEthylbenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/LHexachlorobutadiene EPA 8260B 01/31/13 02/01/13A301200* ND 1

50 ug/LHexachloroethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

50 ug/LIodomethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/LIsopropylbenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/Lm,p-Xylenes EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LMethyl-t-butyl ether EPA 8260B 01/31/13 02/01/13A301200* ND 1




A3A2257 FINAL 02142013 1632

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02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-03

Organics




5.0 ug/LNaphthalene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/Ln-Butylbenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/Ln-Propylbenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/Lo-Xylene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/Lp-Isopropyltoluene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/Lsec-Butylbenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/LStyrene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/Ltert-Butylbenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LTetrachloroethene (PCE) EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LToluene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/Ltrans-1,2-Dichloroethene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/Ltrans-1,3-Dichloropropene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LTrichloroethene (TCE) EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LTrichlorofluoromethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LVinyl Chloride EPA 8260B 01/31/13 02/01/13A301200* ND 1

Surrogate: 1,2-Dichloroethane-d4 Acceptable range: 70-130 %116 %EPA 8260B

Surrogate: Bromofluorobenzene Acceptable range: 70-130 %100 %EPA 8260B

Surrogate: Toluene-d8 Acceptable range: 70-130 %96 %EPA 8260B

0.50 ug/LTotal Xylenes, EPA 8260B* ND




A3A2257 FINAL 02142013 1632

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02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-04

General Chemistry




4500-NH3 G

02/05/13 02/07/13A301269* B1.32.4 1








Metals




DRC

02/07/13 02/07/13A301404* 1300 1


DRC

02/07/13 02/12/13A301406* ND 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/08/13A301404* 3.9 1


DRC

02/07/13 02/08/13A301406* 3.2 1


DRC

02/07/13 02/07/13A301404* 110 1


DRC

02/07/13 02/07/13A301404* ND 1

10 ug/LBoron EPA 200.8 02/04/13 02/12/13A301233* 49 1


DRC

02/07/13 02/08/13A301404* ND 1

0.10 mg/LCalcium EPA 200.7 02/04/13 02/07/13A30123342 1


DRC

02/07/13 02/07/13A301404* 4.0 1


DRC

02/07/13 02/07/13A301404* 4.9 1



DRC

02/07/13 02/07/13A301404* 1800 1


DRC

02/07/13 02/12/13A301406* 41 1




A3A2257 FINAL 02142013 1632

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02/14/2013 16:32Calvin Yang01/31/2013

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Lab Sample ID:



A3A2257-04

Metals




DRC

02/07/13 02/12/13A301404* 0.53 1



DRC

02/07/13 02/07/13A301404* 200 1


DRC

02/07/13 02/12/13A301406* 1.5 1



DRC

02/07/13 02/07/13A301404* 5.2 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1

1.0 mg/LSodium EPA 200.7 02/04/13 02/07/13A30123330 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* 5.4 1

Organics







5.0 ug/L1,1,2-Trichloro-1,2,2-trifluoroethane EPA 8260B 01/31/13 02/01/13A301200* ND 1



0.50 ug/L1,1-Dichloroethene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/L1,1-Dichloropropene EPA 8260B 01/31/13 02/01/13A301200* ND 1


5.0 ug/L1,2,3-Trichloropropane EPA 8260B 01/31/13 02/01/13A301200* ND 1



0.50 ug/L1,2-Dibromoethane (EDB) EPA 8260B 01/31/13 02/01/13A301200* ND 1







A3A2257 FINAL 02142013 1632

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Lab Sample ID:



A3A2257-04

Organics









20 ug/L2-Butanone EPA 8260B 01/31/13 02/01/13A301200* ND 1


20 ug/L2-Hexanone EPA 8260B 01/31/13 02/01/13A301200* ND 1


20 ug/L4-Methyl-2-pentanone EPA 8260B 01/31/13 02/01/13A301200* ND 1

20 ug/LAcetone EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LBenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LBromobenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/LBromochloromethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LBromodichloromethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LBromoform EPA 8260B 01/31/13 02/01/13A301200* ND 1

1.0 ug/LBromomethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

50 ug/LCarbon disulfide EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LCarbon Tetrachloride EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LChlorobenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LChloroethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LChloroform EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LChloromethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/Lcis-1,2-Dichloroethene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/Lcis-1,3-Dichloropropene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LDibromochloromethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/LDibromochloropropane (DBCP) EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LDibromomethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

1.0 ug/LDichlorodifluoromethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LDichloromethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LEthylbenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/LHexachlorobutadiene EPA 8260B 01/31/13 02/01/13A301200* ND 1

50 ug/LHexachloroethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

50 ug/LIodomethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/LIsopropylbenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/Lm,p-Xylenes EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LMethyl-t-butyl ether EPA 8260B 01/31/13 02/01/13A301200* ND 1




A3A2257 FINAL 02142013 1632

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Lab Sample ID:



A3A2257-04

Organics




5.0 ug/LNaphthalene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/Ln-Butylbenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/Ln-Propylbenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/Lo-Xylene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/Lp-Isopropyltoluene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/Lsec-Butylbenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/LStyrene EPA 8260B 01/31/13 02/01/13A301200* ND 1

5.0 ug/Ltert-Butylbenzene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LTetrachloroethene (PCE) EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LToluene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/Ltrans-1,2-Dichloroethene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/Ltrans-1,3-Dichloropropene EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LTrichloroethene (TCE) EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LTrichlorofluoromethane EPA 8260B 01/31/13 02/01/13A301200* ND 1

0.50 ug/LVinyl Chloride EPA 8260B 01/31/13 02/01/13A301200* ND 1

Surrogate: 1,2-Dichloroethane-d4 Acceptable range: 70-130 %109 %EPA 8260B

Surrogate: Bromofluorobenzene Acceptable range: 70-130 %101 %EPA 8260B

Surrogate: Toluene-d8 Acceptable range: 70-130 %100 %EPA 8260B

0.50 ug/LTotal Xylenes, EPA 8260B* ND




A3A2257 FINAL 02142013 1632

Page 14 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-05

General Chemistry




4500-NH3 G

02/05/13 02/07/13A301269* B1.1ND 1






2.0 mg/LSulfate as SO4 EPA 300.0 01/31/13 01/31/13A3011676.0 1


Metals




DRC

02/07/13 02/07/13A301404* 1700 1


DRC

02/07/13 02/12/13A301406* 18 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/08/13A301404* 2.8 1


DRC

02/07/13 02/08/13A301406* 1.6 1


DRC

02/07/13 02/07/13A301404* 110 1


DRC

02/07/13 02/07/13A301404* ND 1

10 ug/LBoron EPA 200.8 02/04/13 02/12/13A301233* 18 1


DRC

02/07/13 02/08/13A301404* ND 1

0.10 mg/LCalcium EPA 200.7 02/04/13 02/07/13A30123321 1


DRC

02/07/13 02/07/13A301404* 4.0 1


DRC

02/07/13 02/07/13A301404* 6.0 1



DRC

02/07/13 02/07/13A301404* 3500 10


DRC

02/07/13 02/12/13A301406* 240 1




A3A2257 FINAL 02142013 1632

Page 15 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-05

Metals




DRC

02/07/13 02/12/13A301404* 0.91 1



DRC

02/07/13 02/07/13A301404* 150 1


DRC

02/07/13 02/12/13A301406* 1.6 1



DRC

02/07/13 02/07/13A301404* 7.7 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1

1.0 mg/LSodium EPA 200.7 02/04/13 02/07/13A30123311 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* 5.9 1




A3A2257 FINAL 02142013 1632

Page 16 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-06

General Chemistry




4500-NH3 G

02/11/13 02/11/13A301517* 0.11 1








Metals




DRC

02/07/13 02/07/13A301404* 2700 1


DRC

02/07/13 02/12/13A301406* 5.0 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/08/13A301404* 5.8 1


DRC

02/07/13 02/08/13A301406* 4.5 1


DRC

02/07/13 02/07/13A301404* 120 1


DRC

02/07/13 02/07/13A301404* ND 1

10 ug/LBoron EPA 200.8 02/04/13 02/12/13A301233* 29 1


DRC

02/07/13 02/08/13A301404* ND 1

0.10 mg/LCalcium EPA 200.7 02/04/13 02/07/13A30123334 1


DRC

02/07/13 02/07/13A301404* 6.0 1


DRC

02/07/13 02/07/13A301404* 5.3 1



DRC

02/07/13 02/07/13A301404* 2900 1


DRC

02/07/13 02/12/13A301406* 28 1




A3A2257 FINAL 02142013 1632

Page 17 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-06

Metals




DRC

02/07/13 02/12/13A301404* 0.86 1



DRC

02/07/13 02/07/13A301404* 150 1


DRC

02/07/13 02/12/13A301406* ND 1



DRC

02/07/13 02/07/13A301404* 7.8 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1

1.0 mg/LSodium EPA 200.7 02/04/13 02/07/13A30123314 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* 7.2 1




A3A2257 FINAL 02142013 1632

Page 18 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-07

General Chemistry




4500-NH3 G

02/11/13 02/11/13A301517* ND 1








Metals




DRC

02/07/13 02/07/13A301404* 1200 1


DRC

02/07/13 02/12/13A301406* 8.3 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/08/13A301404* 3.0 1


DRC

02/07/13 02/08/13A301406* 2.1 1


DRC

02/07/13 02/07/13A301404* 59 1


DRC

02/07/13 02/07/13A301404* ND 1

10 ug/LBoron EPA 200.8 02/04/13 02/12/13A301233* 35 1


DRC

02/07/13 02/08/13A301404* ND 1

0.10 mg/LCalcium EPA 200.7 02/04/13 02/07/13A30123321 1


DRC

02/07/13 02/07/13A301404* 2.9 1


DRC

02/07/13 02/07/13A301404* 3.3 1



DRC

02/07/13 02/07/13A301404* 1700 1


DRC

02/07/13 02/12/13A301406* 72 1




A3A2257 FINAL 02142013 1632

Page 19 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-07

Metals




DRC

02/07/13 02/12/13A301404* 0.48 1



DRC

02/07/13 02/07/13A301404* 74 1


DRC

02/07/13 02/12/13A301406* 2.4 1



DRC

02/07/13 02/07/13A301404* 4.8 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1

1.0 mg/LSodium EPA 200.7 02/04/13 02/07/13A30123315 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1




A3A2257 FINAL 02142013 1632

Page 20 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-08

General Chemistry




4500-NH3 G

02/05/13 02/07/13A301269* B1.35.6 1




A3A2257 FINAL 02142013 1632

Page 21 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-09

General Chemistry




4500-NH3 G

02/11/13 02/11/13A301517* ND 1




A3A2257 FINAL 02142013 1632

Page 22 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-10

General Chemistry






0.44 mg/LNitrate as N EPA 300.0 01/31/13 14:51 01/31/13 14:51A30116713 2




Metals




DRC

02/07/13 02/07/13A301404* 34 1


DRC

02/07/13 02/12/13A301406* ND 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/08/13A301404* 24 1


DRC

02/07/13 02/08/13A301406* 24 1


DRC

02/07/13 02/07/13A301404* 28 1


DRC

02/07/13 02/07/13A301404* ND 1

10 ug/LBoron EPA 200.8 02/04/13 02/12/13A301233* 120 1


DRC

02/07/13 02/08/13A301404* ND 1

0.10 mg/LCalcium EPA 200.7 02/04/13 02/07/13A30123341 1


DRC

02/07/13 02/07/13A301404* 0.81 1


DRC

02/07/13 02/07/13A301404* 2.6 1



DRC

02/07/13 02/07/13A301404* 16 1


DRC

02/07/13 02/12/13A301406* ND 1


DRC

02/07/13 02/12/13A301404* ND 1





A3A2257 FINAL 02142013 1632

Page 23 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-10

Metals




DRC

02/07/13 02/07/13A301404* 1.7 1


DRC

02/07/13 02/12/13A301406* 1.5 1



DRC

02/07/13 02/07/13A301404* 2.2 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1

1.0 mg/LSodium EPA 200.7 02/04/13 02/07/13A30123358 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* 25 1




A3A2257 FINAL 02142013 1632

Page 24 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-11

General Chemistry






0.44 mg/LNitrate as N EPA 300.0 01/31/13 15:00 01/31/13 15:00A30116711 2




Metals




DRC

02/07/13 02/07/13A301404* 38 1


DRC

02/07/13 02/12/13A301406* ND 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/08/13A301404* 19 1


DRC

02/07/13 02/08/13A301406* 19 1


DRC

02/07/13 02/07/13A301404* 48 1


DRC

02/07/13 02/07/13A301404* ND 1

10 ug/LBoron EPA 200.8 02/04/13 02/12/13A301233* 110 1


DRC

02/07/13 02/08/13A301404* ND 1

0.10 mg/LCalcium EPA 200.7 02/04/13 02/07/13A30123349 1


DRC

02/07/13 02/07/13A301404* 1.1 1


DRC

02/07/13 02/07/13A301404* 2.2 1



DRC

02/07/13 02/07/13A301404* 39 1


DRC

02/07/13 02/12/13A301406* ND 1


DRC

02/07/13 02/12/13A301404* ND 1





A3A2257 FINAL 02142013 1632

Page 25 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-11

Metals




DRC

02/07/13 02/07/13A301404* 29 1


DRC

02/07/13 02/12/13A301406* 9.3 1



DRC

02/07/13 02/07/13A301404* 2.5 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1

1.0 mg/LSodium EPA 200.7 02/04/13 02/07/13A30123353 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* 19 1




A3A2257 FINAL 02142013 1632

Page 26 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-12

General Chemistry










Metals




DRC

02/07/13 02/07/13A301404* 26 1


DRC

02/07/13 02/12/13A301406* ND 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/08/13A301404* 4.2 1


DRC

02/07/13 02/08/13A301406* 4.1 1


DRC

02/07/13 02/07/13A301404* 110 1


DRC

02/07/13 02/07/13A301404* ND 1

10 ug/LBoron EPA 200.8 02/04/13 02/12/13A301233* 53 1


DRC

02/07/13 02/08/13A301404* ND 1

0.10 mg/LCalcium EPA 200.7 02/04/13 02/07/13A30123371 1


DRC

02/07/13 02/07/13A301404* 1.9 1


DRC

02/07/13 02/07/13A301404* 1.2 1



DRC

02/07/13 02/07/13A301404* 69 1


DRC

02/07/13 02/12/13A301406* ND 1


DRC

02/07/13 02/12/13A301404* ND 1





A3A2257 FINAL 02142013 1632

Page 27 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-12

Metals




DRC

02/07/13 02/07/13A301404* 98 1


DRC

02/07/13 02/12/13A301406* 15 1



DRC

02/07/13 02/07/13A301404* 2.6 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1

1.0 mg/LSodium EPA 200.7 02/04/13 02/07/13A30123335 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1




A3A2257 FINAL 02142013 1632

Page 28 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-13

General Chemistry










Metals




DRC

02/07/13 02/07/13A301404* 1000 1


DRC

02/07/13 02/12/13A301406* 8.3 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/08/13A301404* 3.1 1


DRC

02/07/13 02/08/13A301406* 2.1 1


DRC

02/07/13 02/07/13A301404* 60 1


DRC

02/07/13 02/07/13A301404* ND 1

10 ug/LBoron EPA 200.8 02/04/13 02/12/13A301233* 35 1


DRC

02/07/13 02/08/13A301404* ND 1

0.10 mg/LCalcium EPA 200.7 02/04/13 02/07/13A30123321 1


DRC

02/07/13 02/07/13A301404* 2.5 1


DRC

02/07/13 02/07/13A301404* 3.1 1



DRC

02/07/13 02/07/13A301404* 1500 1


DRC

02/07/13 02/12/13A301406* 61 1


DRC

02/07/13 02/12/13A301404* 0.43 1





A3A2257 FINAL 02142013 1632

Page 29 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-13

Metals




DRC

02/07/13 02/07/13A301404* 63 1


DRC

02/07/13 02/12/13A301406* ND 1



DRC

02/07/13 02/07/13A301404* 4.6 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1

1.0 mg/LSodium EPA 200.7 02/04/13 02/07/13A30123315 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1




A3A2257 FINAL 02142013 1632

Page 30 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-14

General Chemistry










Metals



50 ug/LAluminum EPA 200.8

DRC

02/07/13 02/07/13A301404* 3100 10


DRC

02/07/13 02/12/13A301406* 7.8 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/08/13A301404* 7.5 1


DRC

02/07/13 02/08/13A301406* 6.1 1


DRC

02/07/13 02/07/13A301404* 96 1


DRC

02/07/13 02/07/13A301404* ND 1

10 ug/LBoron EPA 200.8 02/04/13 02/12/13A301233* 51 1


DRC

02/07/13 02/08/13A301404* ND 1

0.10 mg/LCalcium EPA 200.7 02/04/13 02/07/13A30123336 1


DRC

02/07/13 02/07/13A301404* 6.7 1


DRC

02/07/13 02/07/13A301404* 5.5 1



DRC

02/07/13 02/07/13A301404* 3400 10


DRC

02/07/13 02/12/13A301406* 13 1


DRC

02/07/13 02/12/13A301404* 1.3 1





A3A2257 FINAL 02142013 1632

Page 31 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-14

Metals




DRC

02/07/13 02/07/13A301404* 110 1


DRC

02/07/13 02/12/13A301406* 1.9 1



DRC

02/07/13 02/07/13A301404* 7.5 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1

1.0 mg/LSodium EPA 200.7 02/04/13 02/07/13A30123319 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* 9.1 1




A3A2257 FINAL 02142013 1632

Page 32 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-15

General Chemistry










Metals




DRC

02/07/13 02/07/13A301404* 1700 1


DRC

02/07/13 02/12/13A301406* 9.0 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/08/13A301404* 4.1 1


DRC

02/07/13 02/08/13A301406* 2.9 1


DRC

02/07/13 02/07/13A301404* 71 1


DRC

02/07/13 02/07/13A301404* ND 1

10 ug/LBoron EPA 200.8 02/04/13 02/12/13A301233* 41 1


DRC

02/07/13 02/08/13A301404* ND 1

0.10 mg/LCalcium EPA 200.7 02/04/13 02/07/13A30123325 1


DRC

02/07/13 02/07/13A301404* 4.0 1


DRC

02/07/13 02/07/13A301404* 4.1 1



DRC

02/07/13 02/07/13A301404* 2200 1


DRC

02/07/13 02/12/13A301406* 36 1


DRC

02/07/13 02/12/13A301404* 0.79 1





A3A2257 FINAL 02142013 1632

Page 33 of 59






02/14/2013 16:32Calvin Yang01/31/2013

09:40


Lab Sample ID:



A3A2257-15

Metals




DRC

02/07/13 02/07/13A301404* 94 1


DRC

02/07/13 02/12/13A301406* ND 1



DRC

02/07/13 02/07/13A301404* 5.8 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* ND 1

1.0 mg/LSodium EPA 200.7 02/04/13 02/07/13A30123317 1


DRC

02/07/13 02/07/13A301404* ND 1


DRC

02/07/13 02/07/13A301404* 6.2 1




A3A2257 FINAL 02142013 1632

Page 34 of 59

General Chemistry Quality Control Report

Analyte Result Units Level

Spike

Result %REC Limits RPD Limit QualRL

Source %REC RPD Date

Analyzed

Batch: A301167 Prepared: 01/31/2013Analyst: AJT

Blank (A301167-BLK1) EPA 300.0 - Quality Control

Chloride ND mg/L1.0 01/31/13

Nitrate as N ND mg/L0.22 01/31/13

Sulfate as SO4 ND mg/L2.0 01/31/13

Blank Spike (A301167-BS1) EPA 300.0 - Quality Control

90-110101Chloride 5051 mg/L1.0 01/31/13

90-110101Nitrate as N 1111 mg/L0.22 01/31/13

90-110101Sulfate as SO4 5051 mg/L2.0 01/31/13

Blank Spike Dup (A301167-BSD1) EPA 300.0 - Quality Control

2090-110100 2Chloride 5050 mg/L1.0 01/31/13

2090-11099 2Nitrate as N 1111 mg/L0.22 01/31/13

2090-110100 2Sulfate as SO4 5050 mg/L2.0 01/31/13

Source: A3A2241-01Matrix Spike (A301167-MS1) EPA 300.0 - Quality Control

80-12098Chloride 100100 mg/L2.0 4.9 01/31/13

80-12099Nitrate as N 2325 mg/L0.44 2.3 01/31/13

80-12099Sulfate as SO4 100110 mg/L4.0 8.3 01/31/13


80-12096Chloride 100100 mg/L2.0 5.2 01/31/13

80-12097Nitrate as N 2322 mg/L0.44 ND 01/31/13

80-12097Sulfate as SO4 100100 mg/L4.0 5.3 01/31/13

Source: A3A2241-01Matrix Spike Dup (A301167-MSD1) EPA 300.0 - Quality Control

2080-12097 1Chloride 100100 mg/L2.0 4.9 01/31/13

2080-12098 1Nitrate as N 2324 mg/L0.44 2.3 01/31/13

2080-12098 1Sulfate as SO4 100110 mg/L4.0 8.3 01/31/13


2080-12094 2Chloride 100100 mg/L2.0 5.2 01/31/13

2080-12096 1Nitrate as N 2322 mg/L0.44 ND 01/31/13

2080-12095 2Sulfate as SO4 100100 mg/L4.0 5.3 01/31/13



Chloride ND mg/L1.0 01/31/13

Nitrate as N ND mg/L0.22 01/31/13

Sulfate as SO4 ND mg/L2.0 01/31/13


90-11096Chloride 5048 mg/L1.0 01/31/13

90-11098Nitrate as N 1111 mg/L0.22 01/31/13

90-11098Sulfate as SO4 5049 mg/L2.0 01/31/13


2090-11098 1Chloride 5049 mg/L1.0 01/31/13




A3A2257 FINAL 02142013 1632

Page 35 of 59



Spike



Analyzed



2090-11099 1Nitrate as N 1111 mg/L0.22 01/31/13

2090-11099 1Sulfate as SO4 5049 mg/L2.0 01/31/13


80-12097Chloride 100120 mg/L2.0 25 01/31/13

80-12098Nitrate as N 2323 mg/L0.44 0.44 01/31/13

80-12098Sulfate as SO4 100170 mg/L4.0 68 01/31/13


80-12096Chloride 100160 mg/L2.0 68 01/31/13

80-12099Nitrate as N 2324 mg/L0.44 1.5 01/31/13

80-12097Sulfate as SO4 100180 mg/L4.0 81 01/31/13


2080-12098 1Chloride 100120 mg/L2.0 25 01/31/13

2080-12099 1Nitrate as N 2323 mg/L0.44 0.44 01/31/13

2080-12098 0Sulfate as SO4 100170 mg/L4.0 68 01/31/13


2080-12096 0Chloride 100160 mg/L2.0 68 01/31/13

2080-12099 0Nitrate as N 2324 mg/L0.44 1.5 01/31/13

2080-12097 0Sulfate as SO4 100180 mg/L4.0 81 01/31/13

Batch: A301184 Prepared: 01/31/2013Analyst: CEG

Blank (A301184-BLK1) SM 2510 B - Quality Control

Conductivity @ 25C ND umhos/cm1.0 01/31/13

Source: A3A2257-12Duplicate (A301184-DUP1) SM 2510 B - Quality Control

201Conductivity @ 25C 830 umhos/cm1.0 830 01/31/13

Source: A3A2304-03Duplicate (A301184-DUP2) SM 2510 B - Quality Control

201Conductivity @ 25C 220 umhos/cm1.0 220 01/31/13

Batch: A301197 Prepared: 02/01/2013Analyst: DEH

Blank (A301197-BLK1) SM 2540C - Quality Control

Total Dissolved Solids ND mg/L5.0 02/05/13

Blank (A301197-BLK2) SM 2540C - Quality Control

Total Dissolved Solids ND mg/L5.0 02/05/13

Source: A3A2249-02Duplicate (A301197-DUP1) SM 2540C - Quality Control

201Total Dissolved Solids 620 mg/L5.0 620 02/05/13

Source: A3A2257-11Duplicate (A301197-DUP2) SM 2540C - Quality Control

201Total Dissolved Solids 490 mg/L5.0 500 02/05/13




A3A2257 FINAL 02142013 1632

Page 36 of 59



Spike



Analyzed

Batch: A301269 Prepared: 02/05/2013Analyst: KKC

Blank (A301269-BLK1) SM 4500-NH3 G - Quality Control

B1.0Ammonia as N 0.10 mg/L0.10 02/07/13


Ammonia as N ND mg/L0.10 02/07/13

Blank Spike (A301269-BS1) SM 4500-NH3 G - Quality Control

80-12098Ammonia as N 109.8 mg/L0.10 02/07/13


80-12096Ammonia as N 109.6 mg/L0.10 02/07/13

Blank Spike Dup (A301269-BSD1) SM 4500-NH3 G - Quality Control

2080-12096 1Ammonia as N 109.6 mg/L0.10 02/07/13


2080-12098 2Ammonia as N 109.8 mg/L0.10 02/07/13

Source: A3A2257-05Matrix Spike (A301269-MS2) SM 4500-NH3 G - Quality Control

80-12095Ammonia as N 109.5 mg/L0.10 ND 02/07/13

Source: A3A2257-05Matrix Spike Dup (A301269-MSD2) SM 4500-NH3 G - Quality Control

2080-12096 1Ammonia as N 109.6 mg/L0.10 ND 02/07/13

Batch: A301347 Prepared: 02/06/2013Analyst: SAB

Blank (A301347-BLK1) SM 4500-F C - Quality Control

Fluoride ND mg/L0.10 02/06/13

Blank Spike (A301347-BS1) SM 4500-F C - Quality Control

90-110101Fluoride 1.01.0 mg/L0.10 02/06/13

Blank Spike Dup (A301347-BSD1) SM 4500-F C - Quality Control

2090-110101 0Fluoride 1.01.0 mg/L0.10 02/06/13

Source: A3B0139-01Matrix Spike (A301347-MS1) SM 4500-F C - Quality Control

80-120100Fluoride 1.01.4 mg/L0.10 0.40 02/06/13

Source: A3A2224-19Matrix Spike (A301347-MS2) SM 4500-F C - Quality Control

80-120102Fluoride 1.01.4 mg/L0.10 0.42 02/06/13

Source: A3B0139-01Matrix Spike Dup (A301347-MSD1) SM 4500-F C - Quality Control

2080-120101 1Fluoride 1.01.4 mg/L0.10 0.40 02/06/13

Source: A3A2224-19Matrix Spike Dup (A301347-MSD2) SM 4500-F C - Quality Control

2080-120105 2Fluoride 1.01.5 mg/L0.10 0.42 02/06/13






A3A2257 FINAL 02142013 1632

Page 37 of 59



Spike



Analyzed



Fluoride ND mg/L0.10 02/06/13

Blank Spike (A301357-BS1) SM 4500-F C - Quality Control

90-110101Fluoride 1.01.0 mg/L0.10 02/06/13

Blank Spike Dup (A301357-BSD1) SM 4500-F C - Quality Control

2090-110102 0Fluoride 1.01.0 mg/L0.10 02/06/13

Source: A3A2257-05Matrix Spike (A301357-MS1) SM 4500-F C - Quality Control

80-120100Fluoride 1.01.1 mg/L0.10 0.10 02/06/13

Source: A3B0022-01Matrix Spike (A301357-MS2) SM 4500-F C - Quality Control

80-120102Fluoride 1.01.5 mg/L0.10 0.48 02/06/13

Source: A3A2257-05Matrix Spike Dup (A301357-MSD1) SM 4500-F C - Quality Control

2080-120102 2Fluoride 1.01.1 mg/L0.10 0.10 02/06/13

Source: A3B0022-01Matrix Spike Dup (A301357-MSD2) SM 4500-F C - Quality Control

2080-120103 1Fluoride 1.01.5 mg/L0.10 0.48 02/06/13

Batch: A301364 Prepared: 02/06/2013Analyst: RCN


Perchlorate ND ug/L2.0 02/06/13


85-11597Perchlorate 2524 ug/L2.0 02/06/13


1585-11596 1Perchlorate 2524 ug/L2.0 02/06/13

Source: A3B0136-03Matrix Spike (A301364-MS2) EPA 314.0 - Quality Control

80-120108Perchlorate 7.58.1 ug/L2.0 ND 02/07/13

Source: A3B0136-03Matrix Spike Dup (A301364-MSD2) EPA 314.0 - Quality Control

15 MS0580-12089 19Perchlorate 7.56.7 ug/L2.0 ND 02/07/13



Perchlorate ND ug/L2.0 02/07/13


85-115102Perchlorate 2525 ug/L2.0 02/07/13


1585-11597 4Perchlorate 2524 ug/L2.0 02/07/13




A3A2257 FINAL 02142013 1632

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Spike



Analyzed



80-12095Perchlorate 1514 ug/L2.0 ND 02/07/13


1580-12092 3Perchlorate 1514 ug/L2.0 ND 02/07/13

Batch: A301517 Prepared: 02/11/2013Analyst: KKC


Ammonia as N ND mg/L0.10 02/11/13


80-120103Ammonia as N 1010 mg/L0.10 02/11/13


2080-120104 1Ammonia as N 1010 mg/L0.10 02/11/13

Source: A3B0279-02Matrix Spike (A301517-MS1) SM 4500-NH3 G - Quality Control

80-12095Ammonia as N 1013 mg/L0.10 3.4 02/11/13

Source: A3B0448-02Matrix Spike (A301517-MS2) SM 4500-NH3 G - Quality Control

80-120100Ammonia as N 1010 mg/L0.10 0.16 02/11/13

Source: A3B0279-02Matrix Spike Dup (A301517-MSD1) SM 4500-NH3 G - Quality Control

2080-12091 3Ammonia as N 1012 mg/L0.10 3.4 02/11/13

Source: A3B0448-02Matrix Spike Dup (A301517-MSD2) SM 4500-NH3 G - Quality Control

2080-12099 1Ammonia as N 1010 mg/L0.10 0.16 02/11/13




A3A2257 FINAL 02142013 1632

Page 39 of 59

Metals Quality Control Report


Spike



Analyzed

Batch: A301233 Prepared: 02/04/2013Analyst: NRE


Calcium ND mg/L0.10 02/07/13

Magnesium ND mg/L0.10 02/07/13

Sodium ND mg/L1.0 02/07/13


85-11598Calcium 109.8 mg/L0.10 02/07/13

85-11599Magnesium 109.9 mg/L0.10 02/07/13

85-115102Sodium 1010 mg/L1.0 02/07/13


2085-11599 0Calcium 109.9 mg/L0.10 02/07/13

2085-11598 0Magnesium 109.8 mg/L0.10 02/07/13

2085-115102 0Sodium 1010 mg/L1.0 02/07/13


70-130101Calcium 1019 mg/L0.10 9.0 02/07/13

70-13099Magnesium 1014 mg/L0.10 4.3 02/07/13

70-130102Sodium 1013 mg/L1.0 3.2 02/07/13


70-130102Calcium 1031 mg/L0.10 21 02/07/13

70-130100Magnesium 1024 mg/L0.10 14 02/07/13

70-130101Sodium 1025 mg/L1.0 15 02/07/13


2070-130100 1Calcium 1019 mg/L0.10 9.0 02/07/13

2070-130100 0Magnesium 1014 mg/L0.10 4.3 02/07/13

2070-130101 0Sodium 1013 mg/L1.0 3.2 02/07/13


2070-130105 1Calcium 1031 mg/L0.10 21 02/07/13

2070-130101 0Magnesium 1024 mg/L0.10 14 02/07/13

2070-130103 1Sodium 1025 mg/L1.0 15 02/07/13


Boron ND ug/L10 02/12/13

Mercury ND ug/L0.20 02/12/13


85-115100Boron 600600 ug/L10 02/12/13

85-11593Mercury 5.04.7 ug/L0.20 02/12/13


2085-115101 1Boron 600600 ug/L10 02/12/13

2085-11595 2Mercury 5.04.8 ug/L0.20 02/12/13


70-130100Boron 600620 ug/L10 19 02/12/13




A3A2257 FINAL 02142013 1632

Page 40 of 59



Spike



Analyzed

Batch: A301233 Prepared: 02/04/2013Analyst: MAS


70-130102Mercury 5.05.1 ug/L0.20 ND 02/12/13


70-130100Boron 600630 ug/L10 35 02/12/13

70-13095Mercury 5.04.7 ug/L0.20 ND 02/12/13


2070-130100 0Boron 600620 ug/L10 19 02/12/13

2070-13099 2Mercury 5.05.0 ug/L0.20 ND 02/12/13


2070-13098 2Boron 600620 ug/L10 35 02/12/13

2070-130103 8Mercury 5.05.1 ug/L0.20 ND 02/12/13

Batch: A301342 Prepared: 02/06/2013Analyst: PSK

Blank (A301342-BLK1) EPA 200.8 DRC - Quality Control

Aluminum ND ug/L5.0 02/07/13

Antimony ND ug/L0.50 02/07/13

Barium ND ug/L1.0 02/07/13

Beryllium ND ug/L0.50 02/07/13

Chromium ND ug/L0.50 02/07/13

Copper ND ug/L0.50 02/07/13

Iron ND ug/L10 02/07/13

Lead ND ug/L0.10 02/07/13

Manganese ND ug/L1.0 02/07/13

Nickel ND ug/L1.0 02/07/13

Selenium ND ug/L1.0 02/07/13

Thallium ND ug/L1.0 02/07/13

Zinc ND ug/L5.0 02/07/13


Arsenic ND ug/L0.10 02/08/13

Cadmium ND ug/L0.25 02/08/13

Blank Spike (A301342-BS1) EPA 200.8 DRC - Quality Control

85-115102Aluminum 5051 ug/L5.0 02/07/13

85-115100Antimony 5050 ug/L0.50 02/07/13

85-115102Barium 5051 ug/L1.0 02/07/13

85-11592Beryllium 5046 ug/L0.50 02/07/13

85-11599Chromium 5050 ug/L0.50 02/07/13

85-11599Copper 5049 ug/L0.50 02/07/13

85-11598Iron 5049 ug/L10 02/07/13

85-115101Lead 5050 ug/L0.10 02/07/13

85-11599Manganese 5050 ug/L1.0 02/07/13

85-11599Nickel 5049 ug/L1.0 02/07/13

85-11589Selenium 5044 ug/L1.0 02/07/13

85-115100Thallium 5050 ug/L1.0 02/07/13




A3A2257 FINAL 02142013 1632

Page 41 of 59



Spike



Analyzed



85-11596Zinc 5048 ug/L5.0 02/07/13


85-11598Arsenic 5049 ug/L0.10 02/08/13

85-11592Cadmium 5046 ug/L0.25 02/08/13

Blank Spike Dup (A301342-BSD1) EPA 200.8 DRC - Quality Control

2085-115102 1Aluminum 5051 ug/L5.0 02/07/13

2085-115102 2Antimony 5051 ug/L0.50 02/07/13

2085-115103 1Barium 5051 ug/L1.0 02/07/13

2085-11593 2Beryllium 5047 ug/L0.50 02/07/13

2085-115101 2Chromium 5051 ug/L0.50 02/07/13

2085-115101 2Copper 5050 ug/L0.50 02/07/13

2085-11599 1Iron 5050 ug/L10 02/07/13

2085-115103 2Lead 5051 ug/L0.10 02/07/13

2085-115100 1Manganese 5050 ug/L1.0 02/07/13

2085-11599 1Nickel 5050 ug/L1.0 02/07/13

2085-11592 3Selenium 5046 ug/L1.0 02/07/13

2085-115103 3Thallium 5051 ug/L1.0 02/07/13

2085-11597 1Zinc 5048 ug/L5.0 02/07/13


2085-11599 1Arsenic 5050 ug/L0.10 02/08/13

2085-11591 1Cadmium 5045 ug/L0.25 02/08/13

Source: A3A2224-10Matrix Spike (A301342-MS1) EPA 200.8 DRC - Quality Control

70-130103Aluminum 5051 ug/L5.0 ND 02/07/13

70-130101Antimony 5051 ug/L0.50 ND 02/07/13

70-130103Barium 5051 ug/L1.0 ND 02/07/13

70-13091Beryllium 5045 ug/L0.50 ND 02/07/13

70-130100Chromium 5050 ug/L0.50 ND 02/07/13

70-130100Copper 5050 ug/L0.50 ND 02/07/13

70-13099Iron 5049 ug/L10 ND 02/07/13

70-130102Lead 5051 ug/L0.10 ND 02/07/13

70-130100Manganese 5050 ug/L1.0 ND 02/07/13

70-13099Nickel 5050 ug/L1.0 ND 02/07/13

70-13088Selenium 5044 ug/L1.0 ND 02/07/13

70-130102Thallium 5051 ug/L1.0 ND 02/07/13

70-13088Zinc 5047 ug/L5.0 ND 02/07/13


MS0170-130168Aluminum 50 High510 ug/L5.0 430 02/07/13

70-130102Antimony 5051 ug/L0.50 ND 02/07/13

70-130105Arsenic 5054 ug/L0.10 1.9 02/08/13

70-130105Barium 50130 ug/L1.0 79 02/07/13

70-130104Beryllium 5052 ug/L0.50 ND 02/07/13

70-13090Cadmium 5045 ug/L0.25 ND 02/08/13

70-130105Chromium 5055 ug/L0.50 2.4 02/07/13




A3A2257 FINAL 02142013 1632

Page 42 of 59



Spike



Analyzed



70-13089Copper 5047 ug/L0.50 2.4 02/07/13

70-130121Iron 50650 ug/L10 590 02/07/13

70-130105Lead 5053 ug/L0.10 0.21 02/07/13

70-13098Manganese 5092 ug/L1.0 43 02/07/13

70-13097Nickel 5051 ug/L1.0 2.8 02/07/13

70-13093Selenium 5047 ug/L1.0 ND 02/07/13

70-130106Thallium 5053 ug/L1.0 ND 02/07/13

70-13087Zinc 5049 ug/L5.0 5.7 02/07/13


70-130100Arsenic 5050 ug/L0.10 ND 02/08/13

70-13090Cadmium 5045 ug/L0.25 ND 02/08/13

Source: A3A2224-10Matrix Spike Dup (A301342-MSD1) EPA 200.8 DRC - Quality Control

2070-130102 0Aluminum 5051 ug/L5.0 ND 02/07/13

2070-130101 0Antimony 5051 ug/L0.50 ND 02/07/13

2070-130102 0Barium 5051 ug/L1.0 ND 02/07/13

2070-13089 2Beryllium 5045 ug/L0.50 ND 02/07/13

2070-130100 1Chromium 5050 ug/L0.50 ND 02/07/13

2070-130100 0Copper 5050 ug/L0.50 ND 02/07/13

2070-130102 3Iron 5051 ug/L10 ND 02/07/13

2070-130102 0Lead 5051 ug/L0.10 ND 02/07/13

2070-130100 0Manganese 5050 ug/L1.0 ND 02/07/13

2070-13098 1Nickel 5049 ug/L1.0 ND 02/07/13

2070-13087 2Selenium 5043 ug/L1.0 ND 02/07/13

2070-130103 1Thallium 5051 ug/L1.0 ND 02/07/13

2070-13088 0Zinc 5047 ug/L5.0 ND 02/07/13


20 MS0170-130143 2Aluminum 50 High500 ug/L5.0 430 02/07/13

2070-130101 1Antimony 5051 ug/L0.50 ND 02/07/13

2070-130105 1Arsenic 5054 ug/L0.10 1.9 02/08/13

2070-130100 2Barium 50130 ug/L1.0 79 02/07/13

2070-130103 1Beryllium 5052 ug/L0.50 ND 02/07/13

2070-13092 2Cadmium 5046 ug/L0.25 ND 02/08/13

2070-130104 1Chromium 5054 ug/L0.50 2.4 02/07/13

2070-13089 0Copper 5047 ug/L0.50 2.4 02/07/13

2070-13092 2Iron 50640 ug/L10 590 02/07/13

2070-130105 1Lead 5053 ug/L0.10 0.21 02/07/13

2070-13095 2Manganese 5090 ug/L1.0 43 02/07/13

2070-13095 2Nickel 5050 ug/L1.0 2.8 02/07/13

2070-13093 1Selenium 5046 ug/L1.0 ND 02/07/13

2070-130105 1Thallium 5053 ug/L1.0 ND 02/07/13

2070-13086 1Zinc 5049 ug/L5.0 5.7 02/07/13


2070-13099 1Arsenic 5049 ug/L0.10 ND 02/08/13

2070-13090 0Cadmium 5045 ug/L0.25 ND 02/08/13




A3A2257 FINAL 02142013 1632

Page 43 of 59



Spike



Analyzed




Aluminum ND ug/L5.0 02/07/13

Antimony ND ug/L0.50 02/07/13

Barium ND ug/L1.0 02/07/13

Beryllium ND ug/L0.50 02/07/13

Chromium ND ug/L0.50 02/07/13

Copper ND ug/L0.50 02/07/13

Iron ND ug/L10 02/07/13

Lead ND ug/L0.10 02/07/13

Manganese ND ug/L1.0 02/07/13

Nickel ND ug/L1.0 02/07/13

Selenium ND ug/L1.0 02/07/13

Silver ND ug/L1.0 02/07/13

Thallium ND ug/L1.0 02/07/13

Zinc ND ug/L5.0 02/07/13


Arsenic ND ug/L0.10 02/08/13

Cadmium ND ug/L0.25 02/08/13


85-115113Aluminum 5057 ug/L5.0 02/07/13

85-115104Antimony 5052 ug/L0.50 02/07/13

85-115106Barium 5053 ug/L1.0 02/07/13

85-115113Beryllium 5057 ug/L0.50 02/07/13

85-115108Chromium 5054 ug/L0.50 02/07/13

85-115101Copper 5051 ug/L0.50 02/07/13

85-115106Iron 5053 ug/L10 02/07/13

85-115103Lead 5052 ug/L0.10 02/07/13

85-115106Manganese 5053 ug/L1.0 02/07/13

85-115107Nickel 5054 ug/L1.0 02/07/13

85-11596Selenium 5048 ug/L1.0 02/07/13

BS0685-115213Silver 50 High110 ug/L1.0 02/07/13

85-115102Thallium 5051 ug/L1.0 02/07/13

85-11599Zinc 5050 ug/L5.0 02/07/13


85-115102Arsenic 5051 ug/L0.10 02/08/13

85-11592Cadmium 5046 ug/L0.25 02/08/13


2085-115112 1Aluminum 5056 ug/L5.0 02/07/13

2085-115103 1Antimony 5051 ug/L0.50 02/07/13

2085-115105 1Barium 5052 ug/L1.0 02/07/13

2085-115112 1Beryllium 5056 ug/L0.50 02/07/13

2085-115107 1Chromium 5053 ug/L0.50 02/07/13




A3A2257 FINAL 02142013 1632

Page 44 of 59



Spike



Analyzed



2085-115100 1Copper 5050 ug/L0.50 02/07/13

2085-115105 1Iron 5053 ug/L10 02/07/13

2085-115103 0Lead 5052 ug/L0.10 02/07/13

2085-115106 0Manganese 5053 ug/L1.0 02/07/13

2085-115106 1Nickel 5053 ug/L1.0 02/07/13

2085-11597 2Selenium 5049 ug/L1.0 02/07/13

20 BS0685-115213 0Silver 50 High110 ug/L1.0 02/07/13

2085-115103 0Thallium 5051 ug/L1.0 02/07/13

2085-11599 1Zinc 5049 ug/L5.0 02/07/13


2085-115108 6Arsenic 5054 ug/L0.10 02/08/13

2085-11589 4Cadmium 5045 ug/L0.25 02/08/13


70-130112Aluminum 5082 ug/L5.0 26 02/07/13

70-130105Antimony 5053 ug/L0.50 ND 02/07/13

70-130102Barium 50160 ug/L1.0 110 02/07/13

70-13095Beryllium 5048 ug/L0.50 ND 02/07/13

70-130101Chromium 5052 ug/L0.50 1.9 02/07/13

70-13088Copper 5045 ug/L0.50 1.2 02/07/13

70-130110Iron 50120 ug/L10 69 02/07/13

70-130111Lead 5056 ug/L0.10 ND 02/07/13

70-130100Manganese 50150 ug/L1.0 98 02/07/13

70-13094Nickel 5050 ug/L1.0 2.6 02/07/13

70-13088Selenium 5044 ug/L1.0 ND 02/07/13

MS0870-130202Silver 50 High100 ug/L1.0 ND 02/07/13

70-130108Thallium 5054 ug/L1.0 ND 02/07/13

70-13089Zinc 5045 ug/L5.0 ND 02/07/13

Source: A3B0022-01Matrix Spike (A301404-MS2) EPA 200.8 DRC - Quality Control

MS0170-130135Aluminum 50 High3900 ug/L5.0 3800 02/07/13

70-130102Antimony 5051 ug/L0.50 ND 02/07/13

70-130107Barium 50200 ug/L1.0 140 02/07/13

70-130103Beryllium 5051 ug/L0.50 ND 02/07/13

70-130103Chromium 5059 ug/L0.50 8.1 02/07/13

70-13086Copper 5047 ug/L0.50 4.1 02/07/13

MS0170-130378Iron 50 High4700 ug/L10 4500 02/07/13

70-130108Lead 5055 ug/L0.10 1.1 02/07/13

70-130119Manganese 50420 ug/L1.0 360 02/07/13

70-13096Nickel 5059 ug/L1.0 11 02/07/13

70-13092Selenium 5046 ug/L1.0 ND 02/07/13

MS0870-130195Silver 50 High97 ug/L1.0 ND 02/07/13

70-130109Thallium 5055 ug/L1.0 ND 02/07/13

70-13082Zinc 5051 ug/L5.0 9.9 02/07/13


70-130105Arsenic 5057 ug/L0.10 4.2 02/08/13




A3A2257 FINAL 02142013 1632

Page 45 of 59



Spike



Analyzed



70-13090Cadmium 5045 ug/L0.25 ND 02/08/13

Source: A3B0022-01Matrix Spike (A301404-MS4) EPA 200.8 DRC - Quality Control

70-130110Arsenic 5060 ug/L0.10 4.9 02/08/13

70-13087Cadmium 5044 ug/L0.25 ND 02/08/13


2070-130112 0Aluminum 5082 ug/L5.0 26 02/07/13

2070-130104 1Antimony 5052 ug/L0.50 ND 02/07/13

2070-130104 1Barium 50160 ug/L1.0 110 02/07/13

2070-130101 5Beryllium 5050 ug/L0.50 ND 02/07/13

2070-130103 2Chromium 5054 ug/L0.50 1.9 02/07/13

2070-13088 0Copper 5045 ug/L0.50 1.2 02/07/13

2070-130109 0Iron 50120 ug/L10 69 02/07/13

2070-130108 3Lead 5054 ug/L0.10 ND 02/07/13

2070-130103 1Manganese 50150 ug/L1.0 98 02/07/13

2070-13096 2Nickel 5050 ug/L1.0 2.6 02/07/13

2070-13092 4Selenium 5046 ug/L1.0 ND 02/07/13

20 MS0870-130197 3Silver 50 High99 ug/L1.0 ND 02/07/13

2070-130109 0Thallium 5054 ug/L1.0 ND 02/07/13

2070-13089 1Zinc 5044 ug/L5.0 ND 02/07/13

Source: A3B0022-01Matrix Spike Dup (A301404-MSD2) EPA 200.8 DRC - Quality Control

20 MS0270-13048 1Aluminum 50 Low3800 ug/L5.0 3800 02/07/13

2070-130101 0Antimony 5051 ug/L0.50 ND 02/07/13

2070-130104 1Barium 50200 ug/L1.0 140 02/07/13

2070-130102 1Beryllium 5051 ug/L0.50 ND 02/07/13

2070-130103 0Chromium 5059 ug/L0.50 8.1 02/07/13

2070-13086 0Copper 5047 ug/L0.50 4.1 02/07/13

20 MS0170-130256 1Iron 50 High4600 ug/L10 4500 02/07/13

2070-130109 1Lead 5056 ug/L0.10 1.1 02/07/13

2070-130117 0Manganese 50420 ug/L1.0 360 02/07/13

2070-13097 1Nickel 5059 ug/L1.0 11 02/07/13

2070-13092 1Selenium 5046 ug/L1.0 ND 02/07/13

20 MS0870-130196 1Silver 50 High98 ug/L1.0 ND 02/07/13

2070-130110 1Thallium 5055 ug/L1.0 ND 02/07/13

2070-13082 0Zinc 5051 ug/L5.0 9.9 02/07/13


2070-130105 0Arsenic 5057 ug/L0.10 4.2 02/08/13

2070-13089 1Cadmium 5044 ug/L0.25 ND 02/08/13

Source: A3B0022-01Matrix Spike Dup (A301404-MSD4) EPA 200.8 DRC - Quality Control

2070-130110 0Arsenic 5060 ug/L0.10 4.9 02/08/13

2070-13087 0Cadmium 5043 ug/L0.25 ND 02/08/13





A3A2257 FINAL 02142013 1632

Page 46 of 59



Spike



Analyzed



Arsenic - Dissolved (1) ND ug/L0.10 02/08/13


Aluminum - Dissolved (1) ND ug/L5.0 02/12/13

Iron - Dissolved (1) ND ug/L10 02/12/13

Manganese - Dissolved (1) ND ug/L1.0 02/12/13


85-11599Arsenic - Dissolved (1) 5050 ug/L0.10 02/08/13


85-115108Aluminum - Dissolved (1) 5054 ug/L5.0 02/12/13

85-115106Iron - Dissolved (1) 5053 ug/L10 02/12/13

85-11599Manganese - Dissolved (1) 5049 ug/L1.0 02/12/13


2085-115100 1Arsenic - Dissolved (1) 5050 ug/L0.10 02/08/13


2085-115109 1Aluminum - Dissolved (1) 5054 ug/L5.0 02/12/13

2085-115103 3Iron - Dissolved (1) 5052 ug/L10 02/12/13

2085-115100 1Manganese - Dissolved (1) 5050 ug/L1.0 02/12/13


70-130101Arsenic - Dissolved (1) 5051 ug/L0.10 0.33 02/08/13


70-130106Arsenic - Dissolved (1) 5055 ug/L0.10 1.9 02/08/13


70-130107Aluminum - Dissolved (1) 5058 ug/L5.0 ND 02/12/13

70-130103Iron - Dissolved (1) 5060 ug/L10 ND 02/12/13

70-13097Manganese - Dissolved (1) 5052 ug/L1.0 3.4 02/12/13


70-130109Aluminum - Dissolved (1) 5065 ug/L5.0 10 02/12/13

70-130104Iron - Dissolved (1) 5066 ug/L10 14 02/12/13

70-13094Manganese - Dissolved (1) 5048 ug/L1.0 ND 02/12/13


2070-130101 0Arsenic - Dissolved (1) 5051 ug/L0.10 0.33 02/08/13


2070-130104 2Arsenic - Dissolved (1) 5054 ug/L0.10 1.9 02/08/13


2070-130102 5Aluminum - Dissolved (1) 5055 ug/L5.0 ND 02/12/13

2070-130102 1Iron - Dissolved (1) 5060 ug/L10 ND 02/12/13




A3A2257 FINAL 02142013 1632

Page 47 of 59



Spike



Analyzed



2070-13097 0Manganese - Dissolved (1) 5052 ug/L1.0 3.4 02/12/13


2070-130105 3Aluminum - Dissolved (1) 5063 ug/L5.0 10 02/12/13

2070-13099 4Iron - Dissolved (1) 5063 ug/L10 14 02/12/13

2070-13094 0Manganese - Dissolved (1) 5048 ug/L1.0 ND 02/12/13



Silver ND ug/L1.0 02/12/13


85-115101Silver 5050 ug/L1.0 02/12/13


2085-115100 1Silver 5050 ug/L1.0 02/12/13


70-13092Silver 5046 ug/L1.0 ND 02/12/13


70-13094Silver 5047 ug/L1.0 ND 02/12/13


2070-13092 0Silver 5046 ug/L1.0 ND 02/12/13


2070-13092 2Silver 5046 ug/L1.0 ND 02/12/13




A3A2257 FINAL 02142013 1632

Page 48 of 59

Organics Quality Control Report


Spike



Analyzed

Batch: A301200 Prepared: 01/31/2013Analyst: AMN

Blank (A301200-BLK1) EPA 8260B - Quality Control

1,1,1,2-Tetrachloroethane ND ug/L0.50 01/31/13

1,1,1-Trichloroethane ND ug/L0.50 01/31/13

1,1,2,2-Tetrachloroethane ND ug/L0.50 01/31/13

1,1,2-Trichloro-1,2,2-trifluoroethane ND ug/L5.0 01/31/13

1,1,2-Trichloroethane ND ug/L0.50 01/31/13

1,1-Dichloroethane ND ug/L0.50 01/31/13

1,1-Dichloroethene ND ug/L0.50 01/31/13

1,1-Dichloropropene ND ug/L5.0 01/31/13

1,2,3-Trichlorobenzene ND ug/L5.0 01/31/13

1,2,3-Trichloropropane ND ug/L5.0 01/31/13

1,2,4-Trichlorobenzene ND ug/L5.0 01/31/13

1,2,4-Trimethylbenzene ND ug/L5.0 01/31/13

1,2-Dibromoethane (EDB) ND ug/L0.50 01/31/13

1,2-Dichlorobenzene ND ug/L0.50 01/31/13

1,2-Dichloroethane ND ug/L0.50 01/31/13

1,2-Dichloropropane ND ug/L0.50 01/31/13

1,3,5-Trimethylbenzene ND ug/L5.0 01/31/13





2-Butanone ND ug/L20 01/31/13

2-Chlorotoluene ND ug/L5.0 01/31/13

2-Hexanone ND ug/L20 01/31/13

4-Chlorotoluene ND ug/L5.0 01/31/13

4-Methyl-2-pentanone ND ug/L20 01/31/13

Acetone ND ug/L20 01/31/13

Benzene ND ug/L0.50 01/31/13

Bromobenzene ND ug/L0.50 01/31/13

Bromochloromethane ND ug/L5.0 01/31/13

Bromodichloromethane ND ug/L0.50 01/31/13

Bromoform ND ug/L0.50 01/31/13

Bromomethane ND ug/L1.0 01/31/13

Carbon disulfide ND ug/L50 01/31/13

Carbon Tetrachloride ND ug/L0.50 01/31/13

Chlorobenzene ND ug/L0.50 01/31/13

Chloroethane ND ug/L0.50 01/31/13

Chloroform ND ug/L0.50 01/31/13

Chloromethane ND ug/L0.50 01/31/13

cis-1,2-Dichloroethene ND ug/L0.50 01/31/13

cis-1,3-Dichloropropene ND ug/L0.50 01/31/13

Dibromochloromethane ND ug/L0.50 01/31/13

Dibromochloropropane (DBCP) ND ug/L5.0 01/31/13

Dibromomethane ND ug/L0.50 01/31/13

Dichlorodifluoromethane ND ug/L1.0 01/31/13

Dichloromethane ND ug/L0.50 01/31/13

Ethylbenzene ND ug/L0.50 01/31/13




A3A2257 FINAL 02142013 1632

Page 49 of 59



Spike



Analyzed


Blank (A301200-BLK1) EPA 8260B - Quality Control

Hexachlorobutadiene ND ug/L5.0 01/31/13

Hexachloroethane ND ug/L50 01/31/13

Iodomethane ND ug/L50 01/31/13

Isopropylbenzene ND ug/L5.0 01/31/13

m,p-Xylenes ND ug/L0.50 01/31/13

Methyl-t-butyl ether ND ug/L0.50 01/31/13

Naphthalene ND ug/L5.0 01/31/13

n-Butylbenzene ND ug/L5.0 01/31/13

n-Propylbenzene ND ug/L5.0 01/31/13

o-Xylene ND ug/L0.50 01/31/13

p-Isopropyltoluene ND ug/L5.0 01/31/13

sec-Butylbenzene ND ug/L5.0 01/31/13

Styrene ND ug/L5.0 01/31/13

tert-Butylbenzene ND ug/L5.0 01/31/13

Tetrachloroethene (PCE) ND ug/L0.50 01/31/13

Toluene ND ug/L0.50 01/31/13

trans-1,2-Dichloroethene ND ug/L0.50 01/31/13

trans-1,3-Dichloropropene ND ug/L0.50 01/31/13

Trichloroethene (TCE) ND ug/L0.50 01/31/13

Trichlorofluoromethane ND ug/L0.50 01/31/13

Vinyl Chloride ND ug/L0.50 01/31/13

70-130Surrogate: 1,2-Dichloroethane-d4 10410 10 01/31/13

70-130Surrogate: Bromofluorobenzene 10010 10 01/31/13

70-130Surrogate: Toluene-d8 999.9 10 01/31/13

Blank Spike (A301200-BS1) EPA 8260B - Quality Control

78-1271041,1,1,2-Tetrachloroethane 1010 ug/L0.50 01/31/13

71-132981,1,1-Trichloroethane 109.8 ug/L0.50 01/31/13

72-1301071,1,2,2-Tetrachloroethane 1011 ug/L0.50 01/31/13

68-144941,1,2-Trichloro-1,2,2-trifluoroethane 109.4 ug/L5.0 01/31/13

79-1231021,1,2-Trichloroethane 1010 ug/L0.50 01/31/13

69-1291061,1-Dichloroethane 1011 ug/L0.50 01/31/13

72-133981,1-Dichloroethene 109.8 ug/L0.50 01/31/13

73-130991,1-Dichloropropene 109.9 ug/L5.0 01/31/13

53-1871311,2,3-Trichlorobenzene 1013 ug/L5.0 01/31/13

74-1291051,2,3-Trichloropropane 1011 ug/L5.0 01/31/13

85-1391161,2,4-Trichlorobenzene 1012 ug/L5.0 01/31/13

79-1251051,2,4-Trimethylbenzene 1011 ug/L5.0 01/31/13

76-1281031,2-Dibromoethane (EDB) 1010 ug/L0.50 01/31/13

84-1261051,2-Dichlorobenzene 1010 ug/L0.50 01/31/13

66-1271081,2-Dichloroethane 1011 ug/L0.50 01/31/13

74-1251031,2-Dichloropropane 1010 ug/L0.50 01/31/13

79-1281051,3,5-Trimethylbenzene 1011 ug/L5.0 01/31/13


79-1181081,3-Dichloropropane 1011 ug/L5.0 01/31/13


69-133962,2-Dichloropropane 109.6 ug/L5.0 01/31/13




A3A2257 FINAL 02142013 1632

Page 50 of 59



Spike



Analyzed



50-1421162-Butanone 1012 ug/L20 01/31/13

79-1261052-Chlorotoluene 1010 ug/L5.0 01/31/13

56-1431192-Hexanone 1012 ug/L20 01/31/13

76-1241044-Chlorotoluene 1010 ug/L5.0 01/31/13

61-1311174-Methyl-2-pentanone 1012 ug/L20 01/31/13

10-198138Acetone 1014 ug/L20 01/31/13

75-126100Benzene 1010 ug/L0.50 01/31/13

75-125105Bromobenzene 1010 ug/L0.50 01/31/13

66-127111Bromochloromethane 1011 ug/L5.0 01/31/13

71-13194Bromodichloromethane 109.4 ug/L0.50 01/31/13

74-141104Bromoform 1010 ug/L0.50 01/31/13

41-17987Bromomethane 108.7 ug/L1.0 01/31/13

67-14098Carbon disulfide 109.8 ug/L50 01/31/13

69-14097Carbon Tetrachloride 109.7 ug/L0.50 01/31/13

81-126100Chlorobenzene 1010 ug/L0.50 01/31/13

62-130117Chloroethane 1012 ug/L0.50 01/31/13

72-12894Chloroform 109.4 ug/L0.50 01/31/13

50-13898Chloromethane 109.8 ug/L0.50 01/31/13

70-126104cis-1,2-Dichloroethene 1010 ug/L0.50 01/31/13

74-12688cis-1,3-Dichloropropene 108.8 ug/L0.50 01/31/13

76-133103Dibromochloromethane 1010 ug/L0.50 01/31/13

63-141104Dibromochloropropane (DBCP) 1010 ug/L5.0 01/31/13

74-127103Dibromomethane 1010 ug/L0.50 01/31/13

59-13597Dichlorodifluoromethane 109.7 ug/L1.0 01/31/13

68-133107Dichloromethane 1011 ug/L0.50 01/31/13

82-123102Ethylbenzene 1010 ug/L0.50 01/31/13

61-204131Hexachlorobutadiene 1013 ug/L5.0 01/31/13

78-145100Hexachloroethane 1010 ug/L50 01/31/13

35-169138Iodomethane 1014 ug/L50 01/31/13

77-131107Isopropylbenzene 1011 ug/L5.0 01/31/13

79-126102m,p-Xylenes 2020 ug/L0.50 01/31/13

73-124101Methyl-t-butyl ether 2020 ug/L0.50 01/31/13

57-168129Naphthalene 1013 ug/L5.0 01/31/13

80-130105n-Butylbenzene 1011 ug/L5.0 01/31/13

77-132107n-Propylbenzene 1011 ug/L5.0 01/31/13

79-127107o-Xylene 1011 ug/L0.50 01/31/13

83-127107p-Isopropyltoluene 1011 ug/L5.0 01/31/13

79-131108sec-Butylbenzene 1011 ug/L5.0 01/31/13

80-129101Styrene 1010 ug/L5.0 01/31/13

73-137103tert-Butylbenzene 1010 ug/L5.0 01/31/13

70-149129Tetrachloroethene (PCE) 1013 ug/L0.50 01/31/13

78-12497Toluene 109.7 ug/L0.50 01/31/13

70-127103trans-1,2-Dichloroethene 1010 ug/L0.50 01/31/13

69-126104trans-1,3-Dichloropropene 1010 ug/L0.50 01/31/13

79-133108Trichloroethene (TCE) 1011 ug/L0.50 01/31/13

61-13798Trichlorofluoromethane 109.8 ug/L0.50 01/31/13

62-13797Vinyl Chloride 109.7 ug/L0.50 01/31/13




A3A2257 FINAL 02142013 1632

Page 51 of 59



Spike



Analyzed



70-130Surrogate: 1,2-Dichloroethane-d4 969.6 10 01/31/13


70-130Surrogate: Toluene-d8 10210 10 01/31/13

Blank Spike Dup (A301200-BSD1) EPA 8260B - Quality Control

3078-127107 31,1,1,2-Tetrachloroethane 1011 ug/L0.50 01/31/13

3071-13296 11,1,1-Trichloroethane 109.6 ug/L0.50 01/31/13

3072-130111 41,1,2,2-Tetrachloroethane 1011 ug/L0.50 01/31/13

3068-14495 11,1,2-Trichloro-1,2,2-trifluoroethane 109.5 ug/L5.0 01/31/13

3079-123107 41,1,2-Trichloroethane 1011 ug/L0.50 01/31/13

3069-129105 11,1-Dichloroethane 1011 ug/L0.50 01/31/13

3072-133101 41,1-Dichloroethene 1010 ug/L0.50 01/31/13

3073-130103 41,1-Dichloropropene 1010 ug/L5.0 01/31/13

3053-187131 01,2,3-Trichlorobenzene 1013 ug/L5.0 01/31/13

3074-129115 91,2,3-Trichloropropane 1012 ug/L5.0 01/31/13

3085-139120 31,2,4-Trichlorobenzene 1012 ug/L5.0 01/31/13

3079-125107 21,2,4-Trimethylbenzene 1011 ug/L5.0 01/31/13

3076-128108 41,2-Dibromoethane (EDB) 1011 ug/L0.50 01/31/13

3084-126107 11,2-Dichlorobenzene 1011 ug/L0.50 01/31/13

3066-127107 01,2-Dichloroethane 1011 ug/L0.50 01/31/13

3074-125104 11,2-Dichloropropane 1010 ug/L0.50 01/31/13

3079-128107 21,3,5-Trimethylbenzene 1011 ug/L5.0 01/31/13


3079-118112 41,3-Dichloropropane 1011 ug/L5.0 01/31/13


3069-13399 22,2-Dichloropropane 109.9 ug/L5.0 01/31/13

3050-142103 132-Butanone 1010 ug/L20 01/31/13

3079-126106 12-Chlorotoluene 1011 ug/L5.0 01/31/13

3056-143110 82-Hexanone 1011 ug/L20 01/31/13

3076-124103 04-Chlorotoluene 1010 ug/L5.0 01/31/13

3061-131120 24-Methyl-2-pentanone 1012 ug/L20 01/31/13

3010-198109 24Acetone 1011 ug/L20 01/31/13

3075-126103 3Benzene 1010 ug/L0.50 01/31/13

3075-125108 3Bromobenzene 1011 ug/L0.50 01/31/13

3066-127105 5Bromochloromethane 1011 ug/L5.0 01/31/13

3071-13193 2Bromodichloromethane 109.3 ug/L0.50 01/31/13

3074-141106 2Bromoform 1011 ug/L0.50 01/31/13

3041-17994 8Bromomethane 109.4 ug/L1.0 01/31/13

3067-140101 3Carbon disulfide 1010 ug/L50 01/31/13

3069-14098 1Carbon Tetrachloride 109.8 ug/L0.50 01/31/13

3081-126103 3Chlorobenzene 1010 ug/L0.50 01/31/13

3062-130104 12Chloroethane 1010 ug/L0.50 01/31/13

3072-12896 2Chloroform 109.6 ug/L0.50 01/31/13

3050-13896 1Chloromethane 109.6 ug/L0.50 01/31/13

3070-126105 0cis-1,2-Dichloroethene 1010 ug/L0.50 01/31/13

3074-12692 4cis-1,3-Dichloropropene 109.2 ug/L0.50 01/31/13

3076-133101 2Dibromochloromethane 1010 ug/L0.50 01/31/13




A3A2257 FINAL 02142013 1632

Page 52 of 59



Spike



Analyzed


Blank Spike Dup (A301200-BSD1) EPA 8260B - Quality Control

3063-141112 7Dibromochloropropane (DBCP) 1011 ug/L5.0 01/31/13

3074-127103 1Dibromomethane 1010 ug/L0.50 01/31/13

3059-135100 3Dichlorodifluoromethane 1010 ug/L1.0 01/31/13

3068-133109 2Dichloromethane 1011 ug/L0.50 01/31/13

3082-123104 3Ethylbenzene 1010 ug/L0.50 01/31/13

3061-204124 6Hexachlorobutadiene 1012 ug/L5.0 01/31/13

3078-14599 0Hexachloroethane 109.9 ug/L50 01/31/13

3035-169147 6Iodomethane 1015 ug/L50 01/31/13

3077-131108 1Isopropylbenzene 1011 ug/L5.0 01/31/13

3079-126105 3m,p-Xylenes 2021 ug/L0.50 01/31/13

3073-124103 2Methyl-t-butyl ether 2021 ug/L0.50 01/31/13

3057-168135 4Naphthalene 1013 ug/L5.0 01/31/13

3080-130112 6n-Butylbenzene 1011 ug/L5.0 01/31/13

3077-132108 0n-Propylbenzene 1011 ug/L5.0 01/31/13

3079-127109 1o-Xylene 1011 ug/L0.50 01/31/13

3083-127108 0p-Isopropyltoluene 1011 ug/L5.0 01/31/13

3079-131107 1sec-Butylbenzene 1011 ug/L5.0 01/31/13

3080-129105 3Styrene 1010 ug/L5.0 01/31/13

3073-137108 5tert-Butylbenzene 1011 ug/L5.0 01/31/13

3070-149114 12Tetrachloroethene (PCE) 1011 ug/L0.50 01/31/13

3078-124101 4Toluene 1010 ug/L0.50 01/31/13

3070-127105 2trans-1,2-Dichloroethene 1011 ug/L0.50 01/31/13

3069-126105 0trans-1,3-Dichloropropene 1010 ug/L0.50 01/31/13

3079-133108 1Trichloroethene (TCE) 1011 ug/L0.50 01/31/13

3061-137103 5Trichlorofluoromethane 1010 ug/L0.50 01/31/13

3062-13797 0Vinyl Chloride 109.7 ug/L0.50 01/31/13

70-130Surrogate: 1,2-Dichloroethane-d4 10010 10 01/31/13


70-130Surrogate: Toluene-d8 10110 10 01/31/13




A3A2257 FINAL 02142013 1632

Page 53 of 59

Certificate of Analysis 02/14/2013

Notes:

· The Chain of Custody document and Sample Integrity Sheet are part of the analytical report.

· Any remaining sample(s) for testing will be disposed of one month from the final report date unless other arrangements are made in

advance.

· Sample(s) received, prepared, and analyzed within the method specified criteria unless otherwise noted within this report.

· The results relate only to the samples analyzed in accordance with test(s) requested by the client on the Chain of Custody document. Any

analytical quality control exceptions to method criteria that are to be considered when evaluating these results have been flagged and are

defined in the data qualifiers section.

· All results are expressed on wet weight basis unless otherwise specified.

· All positive results for EPA Methods 504.1, 502.2, and 524.2 require the analysis of a Field Reagent Blank (FRB) to confirm that the results

are not a contamination error from field sampling steps. If Field Reagent Blanks were not submitted with the samples, this method

requirement has not been performed.

· Results contained in this analytical report must be reproduced in its entirety.

· Samples collected by BSK Analytical Laboratories were collected in accordance with the BSK Sampling and Collection Standard Operating

Procedures.

· BSK Analytical Laboratories certifies that the test results contained in this report meet all requirements of the NELAC Standards for

applicable certified drinking water chemistry analyses unless qualified or noted in the Case Narrative.

· Analytical data contained in this report may be used for regulatory purposes to meet the requirements of the Federal or State drinking water,

wastewater, and hazardous waste programs.

· J-value is equivalent to DNQ (Detected, not quantified) which is a trace value. A trace value is an analyte detected between the MDL and the

laboratory reporting limit. This result is of an unknown data quality and is only qualitative (estimated). Baseline noise, calibration curve

extrapolation below the lowest calibrator, method blank detections, and integration artifacts can all produce apparent DNQ values, which

contribute to the un-reliability of these values.

· (1) - Residual chlorine and pH analysis have a 15 minute holding time for both drinking and waste water samples as defined by the EPA and

40 CFR 136. Waste water and ground water (monitoring well) samples must be field filtered to meet the 15 minute holding time for dissolved

metals.

· * - This is not a NELAP accredited analyte.

· Summations of analytes (i.e. Total Trihalomethanes) may appear to add individual amounts incorrectly, due to rounding of analyte values

occurring before or after the total value is calculated, as well as rounding of the total value.

· (2) The digestion used to produce this result deviated from EPA 200.2 by excluding hydrochloric acid in order to produce acceptable

recoveries for affected metals.

· (2C) Result reported from secondary analytical column.

· RL Multiplier is the factor used to adjust the reporting limit (RL) due to variations in sample preparation procedures and dilutions required for

matrix interferences.

Certifications:

State of California - CDPH - ELAP

State of California - CDPH - SAC ELAP

State of California - CDPH - NELAP

State of Nevada - NDEP

State of Hawaii - DOH

1180

2435

04227CA

CA000792009A

04227CA

Please refer to our website for a copy of our Accredited Fields of Testing for each certificattion.

Definitions and Flags for Data Qualifiers

mg/L: Milligrams/Liter (ppm)

mg/Kg: Milligrams/Kilogram (ppm)

µg/L: Micrograms/Liter (ppb)

µg/Kg: Micrograms/Kilogram (ppb)

%: Percent Recovered (surrogates)

M: Method Detection Limit

RL: Reporting Limit

:DL x Dilution

ND: None Detected at RL

pCi/L: Picocuries per Liter

NR: Non-Reportable

MDA95: Min. Detected Activity

MPN: Most Probable Number

CFU: Colony Forming Unit

Absent: Less than 1 CFU/100mLs

Present: 1 or more CFU/100mLs

RL Mult: RL Multiplier

MS08 Recovery for matrix spike was biased high; associated samples were ND.

MS05 MS/MSD RPD exceeded the method acceptance limit. Recovery met acceptance criteria.




A3A2257 FINAL 02142013 1632

Page 54 of 59

Certificate of Analysis 02/14/2013

MS02 Matrix spike recovery was low; the associated blank spike recovery was acceptable.

MS01 Matrix spike recovery was high; the associated blank spike recovery was acceptable.

DL01 Sample required dilution due to matrix or high concentration of non-target analyte.

BS06 Blank spike recovery for this analyte was biased high; associated samples were ND.

B1.3 Analyte detected in associated method blank. Reanalysis was not attempted because the reported result was >10x that

found in the blank. Sample result may be, in part, attributable to ambient laboratory background.

B1.1 Analyte detected in associated method blank. No material impact on reported result as sample is ND for this parameter.

B1.0 Analyte present in method blank above reporting limit.




A3A2257 FINAL 02142013 1632

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