ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Sacramento880 Riverside ParkwayWest Sacramento, CA 95605Tel: (916)373-5600
TestAmerica Job ID: 320-4398-1Client Project/Site: Stringfellow Acid Project
For:CH2M Hill Constructors, Inc.3 Hutton Centre DriveSuite 200Santa Ana, California 92707
Attn: Emily Keene
Authorized for release by:10/30/2013 4:36:34 PMDavid Alltucker, Project Manager I(916)[email protected]
Designee for
Jill Kellmann, Project Manager II(916)[email protected]
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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SDMS DOCID#1142026
Table of Contents
Client: CH2M Hill Constructors, Inc.Project/Site: Stringfellow Acid Project
TestAmerica Job ID: 320-4398-1
Page 2 of 53TestAmerica Sacramento
10/30/2013
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
Isotope Dilution Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
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Definitions/GlossaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
F MS/MSD Recovery and/or RPD exceeds the control limits
GC Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
F MS/MSD Recovery and/or RPD exceeds the control limits
HPLC/IC
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
LCMS
Qualifier Description
* Isotope Dilution analyte exceeds control limits
Qualifier
F MS/MSD Recovery and/or RPD exceeds the control limits
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
I Ion Ratio outside of limits, value is EMPC.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Sacramento
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Case NarrativeClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4398-1
Project/Site: Stringfellow Acid Project
Job ID: 320-4398-1
Laboratory: TestAmerica Sacramento
Narrative
Job Narrative
320-4398-1
Receipt
The samples were received on 10/3/2013 9:10 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 0.5º C.
GC/MS VOA
Method(s) 8260B/CA_LUFTMS: The matrix spike (MS) recovery for analytical batch 27356 was just outside the lower control limit. The
associated laboratory control sample (LCS) recovery met acceptance criteria. Samples are asociated with extraction batch numbers
26834 (4421) and 26711 (4398).
No other analytical or quality issues were noted.
GC/MS Semi VOA
Method(s) GCMSMS_NDMA: Isotope dilution analyte (IDA) recovery for the following samples were outside acceptance limits: (320-4314-2
MS), (320-4314-2 MSD), (MB 320-27254/1-A). No corrective action was performed per the laboratory's standard operating procedure
since the recovery was above 10% and the signal to noise criteria was met.
Method(s) GCMSMS_NDMA: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for prep batch 27254 (analytical batch 27724)
were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria.
No other analytical or quality issues were noted.
HPLC
No analytical or quality issues were noted.
GC Semi VOA
Method(s) 8015B: The matrix spike / matrix spike duplicate (MS/MSD) percent recoveries and %RPD for prep batch 27322 (analytical batch
27666) were outside control limits. This is possibly attributed to sample preparation.
No other analytical or quality issues were noted.
LCMS
No analytical or quality issues were noted.
General Chemistry
Method(s) 9056: ICV for nitrite fro batch 27899 was spiked 25 ul of stocking reagent WC-NO2-1000_00022 instead of the usual 20ul. The
spiked concentration was corrected in the LIMs in order to report correctly in the raw data.
Method(s) Moisture: For percent moisture results less than ten percent, the RPD does not apply. The percent solid results are used to
calculate the RPD instead. The RPD for the percent solid results for the following samples: (320-4398-3 DU), EPAZ5S10CS13
(320-4398-3) in batch #27040 are within acceptable control limits.
No other analytical or quality issues were noted.
Organic Prep
Method(s) 3510C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
batch 27099 for method 8015B_DRO-aqueous.
Method(s) 3510C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
batch 27145 for method NDMA-aqueous.
No other analytical or quality issues were noted.
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Case NarrativeClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4398-1
Project/Site: Stringfellow Acid Project
Job ID: 320-4398-1 (Continued)
Laboratory: TestAmerica Sacramento (Continued)
I certify that this data package is in compliance with the terms and conditions of the contract and Statement of Work both technically and for
completeness, for other than the condition(s) detailed above. Release of the data contained in this hardcopy data package and in the
computer-readable data submitted has been authorized by the Quality Assurance Manager or his/her designee, as verified by the following
signature.
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Detection SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5S10CS03 Lab Sample ID: 320-4398-1
☼Diesel Range Organics (C10-C24)
RL
1.0 mg/Kg
MDL
0.30
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA18.4 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble11.5 J 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble12.8 9056
☼Sulfate 5.0 mg/Kg0.24 Soluble13.4 J 9056
☼Perchlorate 1.0 ug/Kg0.15 Total/NA10.91 J 6850
Client Sample ID: EPAZ5S10BS03 Lab Sample ID: 320-4398-2
☼Diesel Range Organics (C10-C24)
RL
0.99 mg/Kg
MDL
0.30
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA13.2 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble10.95 J 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble10.27 9056
☼Perchlorate 0.99 ug/Kg0.15 Total/NA10.22 J I 6850
Client Sample ID: EPAZ5S10CS13 Lab Sample ID: 320-4398-3
☼Diesel Range Organics (C10-C24)
RL
1.0 mg/Kg
MDL
0.30
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA13.8 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble11.3 J 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble13.2 9056
☼Sulfate 5.0 mg/Kg0.24 Soluble13.2 J 9056
☼Perchlorate 0.99 ug/Kg0.15 Total/NA10.91 J 6850
Client Sample ID: EPAZ5S29BS3 Lab Sample ID: 320-4398-4
No Detections.
Client Sample ID: EPAZ5S29BS00 Lab Sample ID: 320-4398-5
☼Diesel Range Organics (C10-C24)
RL
0.99 mg/Kg
MDL
0.30
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.6 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble10.95 J 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble11.8 9056
☼Sulfate 5.0 mg/Kg0.24 Soluble15.7 9056
☼Perchlorate 0.97 ug/Kg0.15 Total/NA12.1 6850
Client Sample ID: EPAZ5S29BS03 Lab Sample ID: 320-4398-6
☼Gasoline Range Organics (GRO)
-C7-C12
RL
0.52 mg/Kg
MDL
0.052
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.072 8260B/CA_LUFT
MS☼Diesel Range Organics (C10-C24) 0.99 mg/Kg0.30 Total/NA10.44 J 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble12.2 J 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble10.74 9056
☼Sulfate 5.0 mg/Kg0.24 Soluble11.5 J 9056
Client Sample ID: EPAZ5S29BS08 Lab Sample ID: 320-4398-7
☼Gasoline Range Organics (GRO)
-C7-C12
RL
0.52 mg/Kg
MDL
0.052
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.071 8260B/CA_LUFT
MS
TestAmerica Sacramento
This Detection Summary does not include radiochemical test results.
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Detection SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5S29BS08 (Continued) Lab Sample ID: 320-4398-7
☼Diesel Range Organics (C10-C24)
RL
1.0 mg/Kg
MDL
0.31
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.46 8015B
☼Fluoride 2.6 mg/Kg0.31 Soluble11.3 J 9056
☼Nitrate 0.26 mg/Kg0.11 Soluble10.55 9056
☼Sulfate 5.1 mg/Kg0.25 Soluble11.3 J 9056
☼Perchlorate 0.99 ug/Kg0.15 Total/NA10.20 J 6850
Client Sample ID: EPAZ5S29CS00 Lab Sample ID: 320-4398-8
☼Diesel Range Organics (C10-C24)
RL
0.99 mg/Kg
MDL
0.30
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.0 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble10.68 J 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble10.40 9056
☼Sulfate 5.0 mg/Kg0.24 Soluble12.5 J 9056
☼Perchlorate 0.98 ug/Kg0.15 Total/NA10.52 J 6850
Client Sample ID: EPAZ5S29CS03 Lab Sample ID: 320-4398-9
☼Diesel Range Organics (C10-C24)
RL
1.0 mg/Kg
MDL
0.30
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.55 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble10.71 J 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble10.40 9056
☼Sulfate 5.0 mg/Kg0.24 Soluble11.3 J 9056
☼Perchlorate 1.0 ug/Kg0.15 Total/NA10.17 J 6850
Client Sample ID: EPAZ5S29CS08 Lab Sample ID: 320-4398-10
☼Gasoline Range Organics (GRO)
-C7-C12
RL
0.47 mg/Kg
MDL
0.047
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.073 8260B/CA_LUFT
MS☼Diesel Range Organics (C10-C24) 1.0 mg/Kg0.30 Total/NA10.39 J 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble10.91 J 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble10.37 9056
☼Sulfate 5.1 mg/Kg0.24 Soluble11.3 J 9056
Client Sample ID: EPAZ5S29CS18 Lab Sample ID: 320-4398-11
☼Gasoline Range Organics (GRO)
-C7-C12
RL
0.46 mg/Kg
MDL
0.046
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.060 8260B/CA_LUFT
MS☼Diesel Range Organics (C10-C24) 1.0 mg/Kg0.31 Total/NA10.48 J 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble10.85 J 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble10.36 9056
☼Sulfate 5.1 mg/Kg0.24 Soluble11.1 J 9056
TestAmerica Sacramento
This Detection Summary does not include radiochemical test results.
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Client Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4398-1Client Sample ID: EPAZ5S10CS03Matrix: SolidDate Collected: 10/02/13 09:50
Percent Solids: 98.7Date Received: 10/03/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND 0.59 0.059 mg/Kg ☼ 10/03/13 17:27 10/11/13 20:00 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 91 70 - 131 10/03/13 17:27 10/11/13 20:00 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 8.4 1.0 0.30 mg/Kg ☼ 10/11/13 10:11 10/16/13 20:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 106 63 - 141 10/11/13 10:11 10/16/13 20:12 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 1.5 J 2.5 0.30 mg/Kg ☼ 10/17/13 16:02 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/17/13 16:02 1☼Nitrate 2.8
5.0 0.24 mg/Kg 10/17/13 16:02 1☼Sulfate 3.4 J
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate 0.91 J 1.0 0.15 ug/Kg ☼ 10/11/13 07:23 10/18/13 23:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.89 ug/Kg ☼ 10/10/13 09:18 10/14/13 21:35 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 91 70 - 130 10/10/13 09:18 10/14/13 21:35 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 4.7 0.71 ug/Kg ☼ 10/10/13 13:38 10/17/13 03:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 55 50 - 150 10/10/13 13:38 10/17/13 03:25 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
Lab Sample ID: 320-4398-2Client Sample ID: EPAZ5S10BS03Matrix: SolidDate Collected: 10/02/13 08:40
Percent Solids: 99.4Date Received: 10/03/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND 0.59 0.059 mg/Kg ☼ 10/03/13 17:27 10/11/13 20:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 93 70 - 131 10/03/13 17:27 10/11/13 20:25 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 3.2 0.99 0.30 mg/Kg ☼ 10/11/13 10:11 10/16/13 20:43 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Sacramento
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Client Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4398-2Client Sample ID: EPAZ5S10BS03Matrix: SolidDate Collected: 10/02/13 08:40
Percent Solids: 99.4Date Received: 10/03/13 09:10
o-Terphenyl (Surr) 100 63 - 141 10/11/13 10:11 10/16/13 20:43 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 0.95 J 2.5 0.30 mg/Kg ☼ 10/17/13 16:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/17/13 16:14 1☼Nitrate 0.27
5.0 0.24 mg/Kg 10/17/13 16:14 1☼Sulfate ND
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate 0.22 J I 0.99 0.15 ug/Kg ☼ 10/11/13 07:23 10/18/13 23:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.88 ug/Kg ☼ 10/10/13 09:18 10/14/13 21:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 88 70 - 130 10/10/13 09:18 10/14/13 21:52 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 4.9 0.75 ug/Kg ☼ 10/10/13 13:38 10/17/13 04:59 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 63 50 - 150 10/10/13 13:38 10/17/13 04:59 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
Lab Sample ID: 320-4398-3Client Sample ID: EPAZ5S10CS13Matrix: SolidDate Collected: 10/02/13 09:55
Percent Solids: 99.6Date Received: 10/03/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND 0.54 0.054 mg/Kg ☼ 10/03/13 17:27 10/11/13 20:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 90 70 - 131 10/03/13 17:27 10/11/13 20:49 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 3.8 1.0 0.30 mg/Kg ☼ 10/11/13 10:11 10/16/13 21:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 105 63 - 141 10/11/13 10:11 10/16/13 21:13 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 1.3 J 2.5 0.30 mg/Kg ☼ 10/17/13 16:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/17/13 16:25 1☼Nitrate 3.2
5.0 0.24 mg/Kg 10/17/13 16:25 1☼Sulfate 3.2 J
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate 0.91 J 0.99 0.15 ug/Kg ☼ 10/11/13 07:23 10/18/13 23:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Sacramento
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Client Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4398-3Client Sample ID: EPAZ5S10CS13Matrix: SolidDate Collected: 10/02/13 09:55
Percent Solids: 99.6Date Received: 10/03/13 09:10
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.88 ug/Kg ☼ 10/10/13 09:18 10/14/13 22:10 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 105 70 - 130 10/10/13 09:18 10/14/13 22:10 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 5.0 0.76 ug/Kg ☼ 10/10/13 13:38 10/17/13 05:23 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 51 50 - 150 10/10/13 13:38 10/17/13 05:23 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
Lab Sample ID: 320-4398-4Client Sample ID: EPAZ5S29BS3Matrix: WaterDate Collected: 10/02/13 13:30
Date Received: 10/03/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND 50 15 ug/L 10/10/13 14:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 96 73 - 115 10/10/13 14:41 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics [C10-C28] ND 47 15 ug/L 10/09/13 10:20 10/17/13 07:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 102 56 - 145 10/09/13 10:20 10/17/13 07:18 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 9056 - Anions, Ion ChromatographyRL MDL
Fluoride ND 0.50 0.059 mg/L 10/03/13 12:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.050 0.022 mg/L 10/03/13 12:14 1Nitrate ND
1.0 0.049 mg/L 10/03/13 12:14 1Sulfate ND
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate ND 0.50 0.082 ug/L 10/08/13 10:00 10/11/13 11:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 1.0 0.097 ug/L 10/08/13 14:47 10/10/13 23:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 100 63 - 123 10/08/13 14:47 10/10/13 23:41 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 1.9 0.37 ng/L 10/09/13 14:56 10/18/13 21:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 50 25 - 150 10/09/13 14:56 10/18/13 21:14 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4398-5Client Sample ID: EPAZ5S29BS00Matrix: SolidDate Collected: 10/02/13 11:35
Percent Solids: 100.0Date Received: 10/03/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND 0.54 0.054 mg/Kg ☼ 10/03/13 17:27 10/11/13 21:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 90 70 - 131 10/03/13 17:27 10/11/13 21:13 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 1.6 0.99 0.30 mg/Kg ☼ 10/11/13 10:11 10/16/13 21:43 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 100 63 - 141 10/11/13 10:11 10/16/13 21:43 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 0.95 J 2.5 0.30 mg/Kg ☼ 10/17/13 16:37 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/17/13 16:37 1☼Nitrate 1.8
5.0 0.24 mg/Kg 10/17/13 16:37 1☼Sulfate 5.7
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate 2.1 0.97 0.15 ug/Kg ☼ 10/11/13 07:23 10/19/13 00:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.88 ug/Kg ☼ 10/10/13 09:18 10/14/13 22:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 98 70 - 130 10/10/13 09:18 10/14/13 22:27 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 4.9 0.75 ug/Kg ☼ 10/10/13 13:38 10/17/13 05:47 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 67 50 - 150 10/10/13 13:38 10/17/13 05:47 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
Lab Sample ID: 320-4398-6Client Sample ID: EPAZ5S29BS03Matrix: SolidDate Collected: 10/02/13 11:55
Percent Solids: 98.8Date Received: 10/03/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
0.072 J 0.52 0.052 mg/Kg ☼ 10/03/13 17:27 10/11/13 21:38 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 94 70 - 131 10/03/13 17:27 10/11/13 21:38 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 0.44 J 0.99 0.30 mg/Kg ☼ 10/11/13 10:11 10/16/13 23:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Sacramento
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Client Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4398-6Client Sample ID: EPAZ5S29BS03Matrix: SolidDate Collected: 10/02/13 11:55
Percent Solids: 98.8Date Received: 10/03/13 09:10
o-Terphenyl (Surr) 91 63 - 141 10/11/13 10:11 10/16/13 23:45 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 2.2 J 2.5 0.30 mg/Kg ☼ 10/17/13 16:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/17/13 16:48 1☼Nitrate 0.74
5.0 0.24 mg/Kg 10/17/13 16:48 1☼Sulfate 1.5 J
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate ND I 0.99 0.15 ug/Kg ☼ 10/11/13 07:23 10/19/13 00:23 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.88 ug/Kg ☼ 10/10/13 09:18 10/14/13 22:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 96 70 - 130 10/10/13 09:18 10/14/13 22:45 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 4.9 0.75 ug/Kg ☼ 10/10/13 13:38 10/17/13 06:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 84 50 - 150 10/10/13 13:38 10/17/13 06:11 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
Lab Sample ID: 320-4398-7Client Sample ID: EPAZ5S29BS08Matrix: SolidDate Collected: 10/02/13 12:05
Percent Solids: 96.9Date Received: 10/03/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
0.071 J 0.52 0.052 mg/Kg ☼ 10/03/13 17:27 10/11/13 22:02 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 97 70 - 131 10/03/13 17:27 10/11/13 22:02 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 0.46 J 1.0 0.31 mg/Kg ☼ 10/11/13 10:11 10/17/13 00:15 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 99 63 - 141 10/11/13 10:11 10/17/13 00:15 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 1.3 J 2.6 0.31 mg/Kg ☼ 10/17/13 17:00 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.26 0.11 mg/Kg 10/17/13 17:00 1☼Nitrate 0.55
5.1 0.25 mg/Kg 10/17/13 17:00 1☼Sulfate 1.3 J
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate 0.20 J 0.99 0.15 ug/Kg ☼ 10/11/13 07:23 10/19/13 00:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Sacramento
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Client Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4398-7Client Sample ID: EPAZ5S29BS08Matrix: SolidDate Collected: 10/02/13 12:05
Percent Solids: 96.9Date Received: 10/03/13 09:10
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.90 ug/Kg ☼ 10/10/13 09:18 10/11/13 09:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 71 70 - 130 10/10/13 09:18 10/11/13 09:21 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 5.0 0.76 ug/Kg ☼ 10/10/13 13:38 10/17/13 06:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 54 50 - 150 10/10/13 13:38 10/17/13 06:34 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
Lab Sample ID: 320-4398-8Client Sample ID: EPAZ5S29CS00Matrix: SolidDate Collected: 10/02/13 11:05
Percent Solids: 100.0Date Received: 10/03/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND 0.59 0.059 mg/Kg ☼ 10/03/13 17:27 10/11/13 22:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 93 70 - 131 10/03/13 17:27 10/11/13 22:26 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 1.0 0.99 0.30 mg/Kg ☼ 10/11/13 10:11 10/17/13 00:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 108 63 - 141 10/11/13 10:11 10/17/13 00:45 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 0.68 J 2.5 0.30 mg/Kg ☼ 10/17/13 17:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/17/13 17:11 1☼Nitrate 0.40
5.0 0.24 mg/Kg 10/17/13 17:11 1☼Sulfate 2.5 J
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate 0.52 J 0.98 0.15 ug/Kg ☼ 10/11/13 07:23 10/19/13 00:57 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.88 ug/Kg ☼ 10/10/13 09:18 10/11/13 09:39 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 70 70 - 130 10/10/13 09:18 10/11/13 09:39 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 4.9 0.75 ug/Kg ☼ 10/10/13 13:38 10/17/13 06:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 50 50 - 150 10/10/13 13:38 10/17/13 06:58 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4398-9Client Sample ID: EPAZ5S29CS03Matrix: SolidDate Collected: 10/02/13 11:10
Percent Solids: 99.7Date Received: 10/03/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND 0.54 0.054 mg/Kg ☼ 10/03/13 17:27 10/11/13 22:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 95 70 - 131 10/03/13 17:27 10/11/13 22:50 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 0.55 J 1.0 0.30 mg/Kg ☼ 10/11/13 10:11 10/17/13 01:15 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 87 63 - 141 10/11/13 10:11 10/17/13 01:15 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 0.71 J 2.5 0.30 mg/Kg ☼ 10/17/13 17:23 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/17/13 17:23 1☼Nitrate 0.40
5.0 0.24 mg/Kg 10/17/13 17:23 1☼Sulfate 1.3 J
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate 0.17 J 1.0 0.15 ug/Kg ☼ 10/11/13 07:23 10/19/13 01:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 9.9 0.87 ug/Kg ☼ 10/10/13 09:18 10/11/13 10:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 77 70 - 130 10/10/13 09:18 10/11/13 10:14 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 4.9 0.74 ug/Kg ☼ 10/10/13 13:38 10/17/13 07:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 72 50 - 150 10/10/13 13:38 10/17/13 07:21 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
Lab Sample ID: 320-4398-10Client Sample ID: EPAZ5S29CS08Matrix: SolidDate Collected: 10/02/13 11:15
Percent Solids: 97.9Date Received: 10/03/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
0.073 J 0.47 0.047 mg/Kg ☼ 10/03/13 17:27 10/11/13 23:15 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 93 70 - 131 10/03/13 17:27 10/11/13 23:15 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 0.39 J 1.0 0.30 mg/Kg ☼ 10/11/13 10:11 10/17/13 01:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Sacramento
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Client Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4398-10Client Sample ID: EPAZ5S29CS08Matrix: SolidDate Collected: 10/02/13 11:15
Percent Solids: 97.9Date Received: 10/03/13 09:10
o-Terphenyl (Surr) 101 63 - 141 10/11/13 10:11 10/17/13 01:45 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 0.91 J 2.5 0.30 mg/Kg ☼ 10/17/13 17:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/17/13 17:34 1☼Nitrate 0.37
5.1 0.24 mg/Kg 10/17/13 17:34 1☼Sulfate 1.3 J
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate ND 1.0 0.15 ug/Kg ☼ 10/11/13 07:23 10/19/13 01:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.89 ug/Kg ☼ 10/10/13 09:18 10/11/13 10:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 85 70 - 130 10/10/13 09:18 10/11/13 10:32 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 5.1 0.78 ug/Kg ☼ 10/10/13 13:38 10/17/13 07:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 67 50 - 150 10/10/13 13:38 10/17/13 07:45 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
Lab Sample ID: 320-4398-11Client Sample ID: EPAZ5S29CS18Matrix: SolidDate Collected: 10/02/13 11:20
Percent Solids: 97.8Date Received: 10/03/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
0.060 J 0.46 0.046 mg/Kg ☼ 10/03/13 17:27 10/14/13 23:20 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 92 70 - 131 10/03/13 17:27 10/14/13 23:20 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 0.48 J 1.0 0.31 mg/Kg ☼ 10/11/13 10:11 10/17/13 02:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 94 63 - 141 10/11/13 10:11 10/17/13 02:16 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 0.85 J 2.5 0.30 mg/Kg ☼ 10/17/13 17:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/17/13 17:46 1☼Nitrate 0.36
5.1 0.24 mg/Kg 10/17/13 17:46 1☼Sulfate 1.1 J
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate ND I 1.0 0.15 ug/Kg ☼ 10/11/13 07:23 10/19/13 01:47 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4398-11Client Sample ID: EPAZ5S29CS18Matrix: SolidDate Collected: 10/02/13 11:20
Percent Solids: 97.8Date Received: 10/03/13 09:10
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.89 ug/Kg ☼ 10/10/13 09:18 10/11/13 10:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 87 70 - 130 10/10/13 09:18 10/11/13 10:49 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 4.9 0.75 ug/Kg ☼ 10/10/13 13:38 10/17/13 08:09 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 60 50 - 150 10/10/13 13:38 10/17/13 08:09 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Surrogate SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSPrep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (70-131)
BFB
91320-4398-1
Percent Surrogate Recovery (Acceptance Limits)
EPAZ5S10CS03
93320-4398-2 EPAZ5S10BS03
90320-4398-3 EPAZ5S10CS13
90320-4398-5 EPAZ5S29BS00
94320-4398-6 EPAZ5S29BS03
97320-4398-7 EPAZ5S29BS08
93320-4398-8 EPAZ5S29CS00
95320-4398-9 EPAZ5S29CS03
93320-4398-10 EPAZ5S29CS08
92320-4398-11 EPAZ5S29CS18
91320-4421-A-3-A MS Matrix Spike
90320-4421-A-3-B MSD Matrix Spike Duplicate
91320-4452-A-11-A MS Matrix Spike
91320-4452-A-11-B MSD Matrix Spike Duplicate
89LCS 320-27356/7 Lab Control Sample
94LCS 320-27514/15 Lab Control Sample
89MB 320-27356/11 Method Blank
93MB 320-27514/23 Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene (Surr)
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSPrep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (73-115)
BFB
96320-4398-4
Percent Surrogate Recovery (Acceptance Limits)
EPAZ5S29BS3
99LCS 320-27229/15 Lab Control Sample
100LCSD 320-27229/16 Lab Control Sample Dup
95MB 320-27229/7 Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene (Surr)
Method: 8015B - Diesel Range Organics (DRO) (GC)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (63-141)
OTPH1
106320-4398-1
Percent Surrogate Recovery (Acceptance Limits)
EPAZ5S10CS03
100320-4398-2 EPAZ5S10BS03
105320-4398-3 EPAZ5S10CS13
100320-4398-5 EPAZ5S29BS00
91320-4398-6 EPAZ5S29BS03
99320-4398-7 EPAZ5S29BS08
108320-4398-8 EPAZ5S29CS00
87320-4398-9 EPAZ5S29CS03
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Surrogate SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 8015B - Diesel Range Organics (DRO) (GC) (Continued)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (63-141)
OTPH1
101320-4398-10
Percent Surrogate Recovery (Acceptance Limits)
EPAZ5S29CS08
94320-4398-11 EPAZ5S29CS18
69320-4421-F-3-H MS Matrix Spike
110320-4421-F-3-I MSD Matrix Spike Duplicate
97LCS 320-27322/2-A Lab Control Sample
95MB 320-27322/1-A Method Blank
Surrogate Legend
OTPH = o-Terphenyl (Surr)
Method: 8015B - Diesel Range Organics (DRO) (GC)Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (56-145)
OTPH1
102320-4398-4
Percent Surrogate Recovery (Acceptance Limits)
EPAZ5S29BS3
95LCS 320-27099/2-A Lab Control Sample
98MB 320-27099/1-A Method Blank
Surrogate Legend
OTPH = o-Terphenyl (Surr)
Method: 8321A - Benzene Sulfonic Acids (LCMS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (70-130)
4-Bromobenzenesulfonic Acid
91320-4398-1
Percent Surrogate Recovery (Acceptance Limits)
EPAZ5S10CS03
88320-4398-2 EPAZ5S10BS03
105320-4398-3 EPAZ5S10CS13
98320-4398-5 EPAZ5S29BS00
96320-4398-6 EPAZ5S29BS03
71320-4398-7 EPAZ5S29BS08
70320-4398-8 EPAZ5S29CS00
77320-4398-9 EPAZ5S29CS03
85320-4398-10 EPAZ5S29CS08
87320-4398-11 EPAZ5S29CS18
89320-4421-F-3-B MS Matrix Spike
92320-4421-F-3-C MSD Matrix Spike Duplicate
71LCS 320-27199/2-A Lab Control Sample
109MB 320-27199/1-A Method Blank
Surrogate Legend
4-Bromobenzenesulfonic Acid = 4-Bromobenzenesulfonic Acid
TestAmerica Sacramento
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Surrogate SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 8321A - Benzene Sulfonic Acids (LCMS)Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (63-123)
4-Bromobenzenesulfonic Acid
100320-4398-4
Percent Surrogate Recovery (Acceptance Limits)
EPAZ5S29BS3
98320-4421-H-6-C MS Matrix Spike
103320-4421-H-6-D MSD Matrix Spike Duplicate
102LCS 320-27056/2-A Lab Control Sample
99MB 320-27056/1-A Method Blank
Surrogate Legend
4-Bromobenzenesulfonic Acid = 4-Bromobenzenesulfonic Acid
TestAmerica Sacramento
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Isotope Dilution SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSPrep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (50-150)
NDMA
41 *320-4314-E-2-F MS
Percent Isotope Dilution Recovery (Acceptance Limits)
Matrix Spike
45 *320-4314-E-2-G MSD Matrix Spike Duplicate
55320-4398-1 EPAZ5S10CS03
63320-4398-2 EPAZ5S10BS03
51320-4398-3 EPAZ5S10CS13
67320-4398-5 EPAZ5S29BS00
84320-4398-6 EPAZ5S29BS03
54320-4398-7 EPAZ5S29BS08
50320-4398-8 EPAZ5S29CS00
72320-4398-9 EPAZ5S29CS03
67320-4398-10 EPAZ5S29CS08
60320-4398-11 EPAZ5S29CS18
64LCS 320-27254/2-A Lab Control Sample
47 *MB 320-27254/1-A Method Blank
Surrogate Legend
NDMA = N-Nitrosodimethylamine-d6
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSPrep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (25-150)
NDMA
50320-4398-4
Percent Isotope Dilution Recovery (Acceptance Limits)
EPAZ5S29BS3
60LCS 320-27145/2-A Lab Control Sample
66MB 320-27145/1-A Method Blank
Surrogate Legend
NDMA = N-Nitrosodimethylamine-d6
TestAmerica Sacramento
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QC Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS
Client Sample ID: Matrix SpikeLab Sample ID: 320-4421-A-3-A MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27356 Prep Batch: 26834
Gasoline Range Organics (GRO)
-C7-C12
ND 1.01 0.744 F mg/Kg 74 79 - 123☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
4-Bromofluorobenzene (Surr) 70 - 131
Surrogate
91
MS MS
Qualifier Limits%Recovery
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-4421-A-3-B MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27356 Prep Batch: 26834
Gasoline Range Organics (GRO)
-C7-C12
ND 1.03 0.853 mg/Kg 83 79 - 123 14 30☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
4-Bromofluorobenzene (Surr) 70 - 131
Surrogate
90
MSD MSD
Qualifier Limits%Recovery
Client Sample ID: Matrix SpikeLab Sample ID: 320-4452-A-11-A MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27514 Prep Batch: 27074
Gasoline Range Organics (GRO)
-C7-C12
0.055 J 0.914 0.985 mg/Kg 102 79 - 123☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
4-Bromofluorobenzene (Surr) 70 - 131
Surrogate
91
MS MS
Qualifier Limits%Recovery
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-4452-A-11-B MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27514 Prep Batch: 27074
Gasoline Range Organics (GRO)
-C7-C12
0.055 J 0.946 0.868 mg/Kg 86 79 - 123 13 30☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
4-Bromofluorobenzene (Surr) 70 - 131
Surrogate
91
MSD MSD
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 320-27229/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27229
RL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND 50 15 ug/L 10/10/13 13:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
TestAmerica Sacramento
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QC Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 320-27229/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27229
4-Bromofluorobenzene (Surr) 95 73 - 115 10/10/13 13:55 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-27229/15
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27229
Gasoline Range Organics (GRO)
-C7-C12
500 542 ug/L 108 78 - 118
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4-Bromofluorobenzene (Surr) 73 - 115
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 320-27229/16
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27229
Gasoline Range Organics (GRO)
-C7-C12
500 529 ug/L 106 78 - 118 2 23
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
4-Bromofluorobenzene (Surr) 73 - 115
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 320-27356/11
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27356
RL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND 0.50 0.050 mg/Kg 10/11/13 19:12 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
4-Bromofluorobenzene (Surr) 89 70 - 131 10/11/13 19:12 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-27356/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27356
Gasoline Range Organics (GRO)
-C7-C12
1.00 0.983 mg/Kg 98 79 - 123
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4-Bromofluorobenzene (Surr) 70 - 131
Surrogate
89
LCS LCS
Qualifier Limits%Recovery
TestAmerica Sacramento
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QC Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 320-27514/23
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27514
RL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND 0.50 0.050 mg/Kg 10/14/13 22:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
4-Bromofluorobenzene (Surr) 93 70 - 131 10/14/13 22:34 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-27514/15
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27514
Gasoline Range Organics (GRO)
-C7-C12
1.00 1.02 mg/Kg 102 79 - 123
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4-Bromofluorobenzene (Surr) 70 - 131
Surrogate
94
LCS LCS
Qualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 320-27099/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27666 Prep Batch: 27099
RL MDL
Diesel Range Organics [C10-C28] ND 50 16 ug/L 10/09/13 10:20 10/17/13 06:18 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
o-Terphenyl (Surr) 98 56 - 145 10/17/13 06:18 1
MB MB
Surrogate
10/09/13 10:20
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-27099/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27666 Prep Batch: 27099
Diesel Range Organics
[C10-C28]
300 269 ug/L 90 53 - 123
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
o-Terphenyl (Surr) 56 - 145
Surrogate
95
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 320-27322/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27666 Prep Batch: 27322
RL MDL
Diesel Range Organics (C10-C24) ND 1.0 0.30 mg/Kg 10/11/13 10:11 10/16/13 15:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
TestAmerica Sacramento
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QC Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 8015B - Diesel Range Organics (DRO) (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 320-27322/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27666 Prep Batch: 27322
o-Terphenyl (Surr) 95 63 - 141 10/16/13 15:05 1
MB MB
Surrogate
10/11/13 10:11
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-27322/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27666 Prep Batch: 27322
Diesel Range Organics
(C10-C24)
10.0 9.51 mg/Kg 95 67 - 113
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
o-Terphenyl (Surr) 63 - 141
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Matrix SpikeLab Sample ID: 320-4421-F-3-H MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27666 Prep Batch: 27322
Diesel Range Organics
(C10-C24)
3.5 10.0 7.52 F mg/Kg 40 67 - 113☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
o-Terphenyl (Surr) 63 - 141
Surrogate
69
MS MS
Qualifier Limits%Recovery
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-4421-F-3-I MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27666 Prep Batch: 27322
Diesel Range Organics
(C10-C24)
3.5 9.97 11.9 F mg/Kg 85 67 - 113 45 30☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
o-Terphenyl (Surr) 63 - 141
Surrogate
110
MSD MSD
Qualifier Limits%Recovery
Method: 9056 - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 320-26700/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 26700
RL MDL
Fluoride ND 0.50 0.059 mg/L 10/03/13 11:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.0491.0 mg/L 10/03/13 11:51 1Sulfate
TestAmerica Sacramento
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QC Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 9056 - Anions, Ion Chromatography (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-26700/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 26700
Fluoride 7.50 7.32 mg/L 98 90 - 110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Sulfate 7.50 7.14 mg/L 95 90 - 110
Client Sample ID: EPAZ5S29BS3Lab Sample ID: 320-4398-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 26700
Fluoride ND 5.00 5.25 mg/L 105 90 - 110
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Sulfate ND 5.00 5.20 mg/L 104 90 - 110
Client Sample ID: EPAZ5S29BS3Lab Sample ID: 320-4398-4 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 26700
Fluoride ND 5.00 4.93 mg/L 99 90 - 110 6 10
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Sulfate ND 5.00 4.92 mg/L 98 90 - 110 6 10
Client Sample ID: Method BlankLab Sample ID: MB 320-26701/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 26701
RL MDL
Nitrate ND 0.050 0.022 mg/L 10/03/13 11:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-26701/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 26701
Nitrate 1.88 1.73 mg/L 92 90 - 110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: EPAZ5S29BS3Lab Sample ID: 320-4398-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 26701
Nitrate ND 1.00 1.05 mg/L 105 90 - 110
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: EPAZ5S29BS3Lab Sample ID: 320-4398-4 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 26701
Nitrate ND 1.00 1.00 mg/L 100 90 - 110 5 10
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 9056 - Anions, Ion Chromatography (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 320-27468/1-A
Matrix: Solid Prep Type: Soluble
Analysis Batch: 27899
RL MDL
Nitrate ND 0.25 0.11 mg/Kg 10/17/13 13:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-27468/2-A
Matrix: Solid Prep Type: Soluble
Analysis Batch: 27899
Nitrate 5.00 4.91 mg/Kg 98 85 - 115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 320-4421-E-3-D MS
Matrix: Solid Prep Type: Soluble
Analysis Batch: 27899
Nitrate 2.1 5.03 6.94 mg/Kg 97 85 - 115☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-4421-E-3-E MSD
Matrix: Solid Prep Type: Soluble
Analysis Batch: 27899
Nitrate 2.1 5.03 6.95 mg/Kg 97 85 - 115 0 15☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: DuplicateLab Sample ID: 320-4421-E-3-C DU
Matrix: Solid Prep Type: Soluble
Analysis Batch: 27899
Nitrate 2.1 1.99 mg/Kg 4 15☼
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 320-27468/1-A
Matrix: Solid Prep Type: Soluble
Analysis Batch: 27900
RL MDL
Fluoride ND 2.5 0.30 mg/Kg 10/17/13 13:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.245.0 mg/Kg 10/17/13 13:44 1Sulfate
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-27468/2-A
Matrix: Solid Prep Type: Soluble
Analysis Batch: 27900
Fluoride 25.0 23.7 mg/Kg 95 85 - 115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Sulfate 25.0 23.9 mg/Kg 96 85 - 115
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QC Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 9056 - Anions, Ion Chromatography (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 320-4421-E-3-D MS
Matrix: Solid Prep Type: Soluble
Analysis Batch: 27900
Fluoride 1.9 J 25.1 26.0 mg/Kg 96 85 - 115☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Sulfate 21 25.1 44.4 mg/Kg 94 85 - 115☼
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-4421-E-3-E MSD
Matrix: Solid Prep Type: Soluble
Analysis Batch: 27900
Fluoride 1.9 J 25.1 25.8 mg/Kg 95 85 - 115 1 15☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Sulfate 21 25.1 44.2 mg/Kg 93 85 - 115 1 15☼
Client Sample ID: DuplicateLab Sample ID: 320-4421-E-3-C DU
Matrix: Solid Prep Type: Soluble
Analysis Batch: 27900
Fluoride 1.9 J 1.91 J mg/Kg 1 15☼
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Sulfate 21 21.0 mg/Kg 2 15☼
Method: 6850 - Perchlorate by LC/MS or LC/MS/MS
Client Sample ID: Method BlankLab Sample ID: MB 320-27018/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27233 Prep Batch: 27018
RL MDL
Perchlorate ND 0.50 0.082 ug/L 10/08/13 10:00 10/11/13 06:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-27018/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27233 Prep Batch: 27018
Perchlorate 5.00 4.96 ug/L 99 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 320-4264-H-3-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27233 Prep Batch: 27018
Perchlorate ND 5.00 4.96 ug/L 99 80 - 120
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-4264-H-3-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27233 Prep Batch: 27018
Perchlorate ND 5.00 4.85 ug/L 97 80 - 120 2 15
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 6850 - Perchlorate by LC/MS or LC/MS/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 320-27299/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27864 Prep Batch: 27299
RL MDL
Perchlorate ND 1.0 0.15 ug/Kg 10/11/13 07:23 10/18/13 22:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-27299/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27864 Prep Batch: 27299
Perchlorate 50.0 55.6 ug/Kg 111 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 320-4421-F-3-E MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27864 Prep Batch: 27299
Perchlorate 1.7 49.6 56.1 ug/Kg 110 80 - 120☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-4421-F-3-F MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27864 Prep Batch: 27299
Perchlorate 1.7 50.1 57.3 ug/Kg 111 80 - 120 2 15☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 8321A - Benzene Sulfonic Acids (LCMS)
Client Sample ID: Method BlankLab Sample ID: MB 320-27056/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27272 Prep Batch: 27056
RL MDL
p-CBSA ND 1.0 0.097 ug/L 10/08/13 14:47 10/10/13 21:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
4-Bromobenzenesulfonic Acid 99 63 - 123 10/10/13 21:03 1
MB MB
Surrogate
10/08/13 14:47
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-27056/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27272 Prep Batch: 27056
p-CBSA 5.00 5.20 ug/L 104 60 - 127
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4-Bromobenzenesulfonic Acid 63 - 123
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
TestAmerica Sacramento
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QC Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 8321A - Benzene Sulfonic Acids (LCMS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 320-4421-H-6-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27272 Prep Batch: 27056
p-CBSA ND 5.00 5.60 ug/L 112 60 - 127
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
4-Bromobenzenesulfonic Acid 63 - 123
Surrogate
98
MS MS
Qualifier Limits%Recovery
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-4421-H-6-D MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27272 Prep Batch: 27056
p-CBSA ND 5.00 5.34 ug/L 107 60 - 127 5 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
4-Bromobenzenesulfonic Acid 63 - 123
Surrogate
103
MSD MSD
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 320-27199/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27512 Prep Batch: 27199
RL MDL
p-CBSA ND 10 0.88 ug/Kg 10/10/13 09:18 10/14/13 21:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
4-Bromobenzenesulfonic Acid 109 70 - 130 10/14/13 21:17 1
MB MB
Surrogate
10/10/13 09:18
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-27199/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27272 Prep Batch: 27199
p-CBSA 50.0 52.3 ug/Kg 105 70 - 130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4-Bromobenzenesulfonic Acid 70 - 130
Surrogate
71
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Matrix SpikeLab Sample ID: 320-4421-F-3-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27272 Prep Batch: 27199
p-CBSA ND 50.4 48.7 ug/Kg 97 70 - 130☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
4-Bromobenzenesulfonic Acid 70 - 130
Surrogate
89
MS MS
Qualifier Limits%Recovery
TestAmerica Sacramento
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QC Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 8321A - Benzene Sulfonic Acids (LCMS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-4421-F-3-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27272 Prep Batch: 27199
p-CBSA ND 49.9 44.7 ug/Kg 89 70 - 130 9 30☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
4-Bromobenzenesulfonic Acid 70 - 130
Surrogate
92
MSD MSD
Qualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MS
Client Sample ID: Method BlankLab Sample ID: MB 320-27145/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27918 Prep Batch: 27145
RL MDL
N-Nitrosodimethylamine ND 2.0 0.39 ng/L 10/09/13 14:56 10/18/13 18:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
N-Nitrosodimethylamine-d6 66 25 - 150 10/18/13 18:05 1
MB MB
Isotope Dilution
10/09/13 14:56
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-27145/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 27918 Prep Batch: 27145
N-Nitrosodimethylamine 20.0 23.1 ng/L 115 58 - 150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
N-Nitrosodimethylamine-d6 25 - 150
Isotope Dilution
60
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 320-27254/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27724 Prep Batch: 27254
RL MDL
N-Nitrosodimethylamine ND 5.0 0.76 ug/Kg 10/10/13 13:38 10/16/13 21:54 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
N-Nitrosodimethylamine-d6 47 * 50 - 150 10/16/13 21:54 1
MB MB
Isotope Dilution
10/10/13 13:38
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-27254/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27724 Prep Batch: 27254
N-Nitrosodimethylamine 2.50 3.14 J ug/Kg 126 70 - 130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
N-Nitrosodimethylamine-d6 50 - 150
Isotope Dilution
64
LCS LCS
Qualifier Limits%Recovery
TestAmerica Sacramento
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QC Sample ResultsTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MS (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 320-4314-E-2-F MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27724 Prep Batch: 27254
N-Nitrosodimethylamine ND 2.35 4.63 J F ug/Kg 197 70 - 130☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
N-Nitrosodimethylamine-d6 * 50 - 150
Isotope Dilution
41
MS MS
Qualifier Limits%Recovery
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-4314-E-2-G MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 27724 Prep Batch: 27254
N-Nitrosodimethylamine ND 2.54 4.21 J F ug/Kg 165 70 - 130 9 35☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
N-Nitrosodimethylamine-d6 * 50 - 150
Isotope Dilution
45
MSD MSD
Qualifier Limits%Recovery
TestAmerica Sacramento
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QC Association SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
GC/MS VOA
Prep Batch: 26711
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035320-4398-1 EPAZ5S10CS03 Total/NA
Solid 5035320-4398-2 EPAZ5S10BS03 Total/NA
Solid 5035320-4398-3 EPAZ5S10CS13 Total/NA
Solid 5035320-4398-5 EPAZ5S29BS00 Total/NA
Solid 5035320-4398-6 EPAZ5S29BS03 Total/NA
Solid 5035320-4398-7 EPAZ5S29BS08 Total/NA
Solid 5035320-4398-8 EPAZ5S29CS00 Total/NA
Solid 5035320-4398-9 EPAZ5S29CS03 Total/NA
Solid 5035320-4398-10 EPAZ5S29CS08 Total/NA
Solid 5035320-4398-11 EPAZ5S29CS18 Total/NA
Prep Batch: 26834
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035320-4421-A-3-A MS Matrix Spike Total/NA
Solid 5035320-4421-A-3-B MSD Matrix Spike Duplicate Total/NA
Prep Batch: 27074
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035320-4452-A-11-A MS Matrix Spike Total/NA
Solid 5035320-4452-A-11-B MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 27229
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B/CA_LUFT
MS
320-4398-4 EPAZ5S29BS3 Total/NA
Water 8260B/CA_LUFT
MS
LCS 320-27229/15 Lab Control Sample Total/NA
Water 8260B/CA_LUFT
MS
LCSD 320-27229/16 Lab Control Sample Dup Total/NA
Water 8260B/CA_LUFT
MS
MB 320-27229/7 Method Blank Total/NA
Analysis Batch: 27356
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B/CA_LUFT
MS
26711320-4398-1 EPAZ5S10CS03 Total/NA
Solid 8260B/CA_LUFT
MS
26711320-4398-2 EPAZ5S10BS03 Total/NA
Solid 8260B/CA_LUFT
MS
26711320-4398-3 EPAZ5S10CS13 Total/NA
Solid 8260B/CA_LUFT
MS
26711320-4398-5 EPAZ5S29BS00 Total/NA
Solid 8260B/CA_LUFT
MS
26711320-4398-6 EPAZ5S29BS03 Total/NA
Solid 8260B/CA_LUFT
MS
26711320-4398-7 EPAZ5S29BS08 Total/NA
Solid 8260B/CA_LUFT
MS
26711320-4398-8 EPAZ5S29CS00 Total/NA
Solid 8260B/CA_LUFT
MS
26711320-4398-9 EPAZ5S29CS03 Total/NA
Solid 8260B/CA_LUFT
MS
26711320-4398-10 EPAZ5S29CS08 Total/NA
Solid 8260B/CA_LUFT
MS
26834320-4421-A-3-A MS Matrix Spike Total/NA
TestAmerica Sacramento
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QC Association SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
GC/MS VOA (Continued)
Analysis Batch: 27356 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B/CA_LUFT
MS
26834320-4421-A-3-B MSD Matrix Spike Duplicate Total/NA
Solid 8260B/CA_LUFT
MS
LCS 320-27356/7 Lab Control Sample Total/NA
Solid 8260B/CA_LUFT
MS
MB 320-27356/11 Method Blank Total/NA
Analysis Batch: 27514
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B/CA_LUFT
MS
26711320-4398-11 EPAZ5S29CS18 Total/NA
Solid 8260B/CA_LUFT
MS
27074320-4452-A-11-A MS Matrix Spike Total/NA
Solid 8260B/CA_LUFT
MS
27074320-4452-A-11-B MSD Matrix Spike Duplicate Total/NA
Solid 8260B/CA_LUFT
MS
LCS 320-27514/15 Lab Control Sample Total/NA
Solid 8260B/CA_LUFT
MS
MB 320-27514/23 Method Blank Total/NA
GC Semi VOA
Prep Batch: 27099
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C320-4398-4 EPAZ5S29BS3 Total/NA
Water 3510CLCS 320-27099/2-A Lab Control Sample Total/NA
Water 3510CMB 320-27099/1-A Method Blank Total/NA
Prep Batch: 27322
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550B320-4398-1 EPAZ5S10CS03 Total/NA
Solid 3550B320-4398-2 EPAZ5S10BS03 Total/NA
Solid 3550B320-4398-3 EPAZ5S10CS13 Total/NA
Solid 3550B320-4398-5 EPAZ5S29BS00 Total/NA
Solid 3550B320-4398-6 EPAZ5S29BS03 Total/NA
Solid 3550B320-4398-7 EPAZ5S29BS08 Total/NA
Solid 3550B320-4398-8 EPAZ5S29CS00 Total/NA
Solid 3550B320-4398-9 EPAZ5S29CS03 Total/NA
Solid 3550B320-4398-10 EPAZ5S29CS08 Total/NA
Solid 3550B320-4398-11 EPAZ5S29CS18 Total/NA
Solid 3550B320-4421-F-3-H MS Matrix Spike Total/NA
Solid 3550B320-4421-F-3-I MSD Matrix Spike Duplicate Total/NA
Solid 3550BLCS 320-27322/2-A Lab Control Sample Total/NA
Solid 3550BMB 320-27322/1-A Method Blank Total/NA
Analysis Batch: 27666
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015B 27322320-4398-1 EPAZ5S10CS03 Total/NA
Solid 8015B 27322320-4398-2 EPAZ5S10BS03 Total/NA
Solid 8015B 27322320-4398-3 EPAZ5S10CS13 Total/NA
Water 8015B 27099320-4398-4 EPAZ5S29BS3 Total/NA
Solid 8015B 27322320-4398-5 EPAZ5S29BS00 Total/NA
TestAmerica Sacramento
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QC Association SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
GC Semi VOA (Continued)
Analysis Batch: 27666 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015B 27322320-4398-6 EPAZ5S29BS03 Total/NA
Solid 8015B 27322320-4398-7 EPAZ5S29BS08 Total/NA
Solid 8015B 27322320-4398-8 EPAZ5S29CS00 Total/NA
Solid 8015B 27322320-4398-9 EPAZ5S29CS03 Total/NA
Solid 8015B 27322320-4398-10 EPAZ5S29CS08 Total/NA
Solid 8015B 27322320-4398-11 EPAZ5S29CS18 Total/NA
Solid 8015B 27322320-4421-F-3-H MS Matrix Spike Total/NA
Solid 8015B 27322320-4421-F-3-I MSD Matrix Spike Duplicate Total/NA
Water 8015B 27099LCS 320-27099/2-A Lab Control Sample Total/NA
Solid 8015B 27322LCS 320-27322/2-A Lab Control Sample Total/NA
Water 8015B 27099MB 320-27099/1-A Method Blank Total/NA
Solid 8015B 27322MB 320-27322/1-A Method Blank Total/NA
HPLC/IC
Analysis Batch: 26700
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9056320-4398-4 EPAZ5S29BS3 Total/NA
Water 9056320-4398-4 MS EPAZ5S29BS3 Total/NA
Water 9056320-4398-4 MSD EPAZ5S29BS3 Total/NA
Water 9056LCS 320-26700/4 Lab Control Sample Total/NA
Water 9056MB 320-26700/3 Method Blank Total/NA
Analysis Batch: 26701
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9056320-4398-4 EPAZ5S29BS3 Total/NA
Water 9056320-4398-4 MS EPAZ5S29BS3 Total/NA
Water 9056320-4398-4 MSD EPAZ5S29BS3 Total/NA
Water 9056LCS 320-26701/4 Lab Control Sample Total/NA
Water 9056MB 320-26701/3 Method Blank Total/NA
Leach Batch: 27468
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid DI Leach320-4398-1 EPAZ5S10CS03 Soluble
Solid DI Leach320-4398-2 EPAZ5S10BS03 Soluble
Solid DI Leach320-4398-3 EPAZ5S10CS13 Soluble
Solid DI Leach320-4398-5 EPAZ5S29BS00 Soluble
Solid DI Leach320-4398-6 EPAZ5S29BS03 Soluble
Solid DI Leach320-4398-7 EPAZ5S29BS08 Soluble
Solid DI Leach320-4398-8 EPAZ5S29CS00 Soluble
Solid DI Leach320-4398-9 EPAZ5S29CS03 Soluble
Solid DI Leach320-4398-10 EPAZ5S29CS08 Soluble
Solid DI Leach320-4398-11 EPAZ5S29CS18 Soluble
Solid DI Leach320-4421-E-3-C DU Duplicate Soluble
Solid DI Leach320-4421-E-3-D MS Matrix Spike Soluble
Solid DI Leach320-4421-E-3-E MSD Matrix Spike Duplicate Soluble
Solid DI LeachLCS 320-27468/2-A Lab Control Sample Soluble
Solid DI LeachMB 320-27468/1-A Method Blank Soluble
TestAmerica Sacramento
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QC Association SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
HPLC/IC (Continued)
Analysis Batch: 27899
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9056 27468320-4398-1 EPAZ5S10CS03 Soluble
Solid 9056 27468320-4398-2 EPAZ5S10BS03 Soluble
Solid 9056 27468320-4398-3 EPAZ5S10CS13 Soluble
Solid 9056 27468320-4398-5 EPAZ5S29BS00 Soluble
Solid 9056 27468320-4398-6 EPAZ5S29BS03 Soluble
Solid 9056 27468320-4398-7 EPAZ5S29BS08 Soluble
Solid 9056 27468320-4398-8 EPAZ5S29CS00 Soluble
Solid 9056 27468320-4398-9 EPAZ5S29CS03 Soluble
Solid 9056 27468320-4398-10 EPAZ5S29CS08 Soluble
Solid 9056 27468320-4398-11 EPAZ5S29CS18 Soluble
Solid 9056 27468320-4421-E-3-C DU Duplicate Soluble
Solid 9056 27468320-4421-E-3-D MS Matrix Spike Soluble
Solid 9056 27468320-4421-E-3-E MSD Matrix Spike Duplicate Soluble
Solid 9056 27468LCS 320-27468/2-A Lab Control Sample Soluble
Solid 9056 27468MB 320-27468/1-A Method Blank Soluble
Analysis Batch: 27900
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9056 27468320-4398-1 EPAZ5S10CS03 Soluble
Solid 9056 27468320-4398-2 EPAZ5S10BS03 Soluble
Solid 9056 27468320-4398-3 EPAZ5S10CS13 Soluble
Solid 9056 27468320-4398-5 EPAZ5S29BS00 Soluble
Solid 9056 27468320-4398-6 EPAZ5S29BS03 Soluble
Solid 9056 27468320-4398-7 EPAZ5S29BS08 Soluble
Solid 9056 27468320-4398-8 EPAZ5S29CS00 Soluble
Solid 9056 27468320-4398-9 EPAZ5S29CS03 Soluble
Solid 9056 27468320-4398-10 EPAZ5S29CS08 Soluble
Solid 9056 27468320-4398-11 EPAZ5S29CS18 Soluble
Solid 9056 27468320-4421-E-3-C DU Duplicate Soluble
Solid 9056 27468320-4421-E-3-D MS Matrix Spike Soluble
Solid 9056 27468320-4421-E-3-E MSD Matrix Spike Duplicate Soluble
Solid 9056 27468LCS 320-27468/2-A Lab Control Sample Soluble
Solid 9056 27468MB 320-27468/1-A Method Blank Soluble
LCMS
Prep Batch: 27018
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Filtration320-4264-H-3-B MS Matrix Spike Total/NA
Water Filtration320-4264-H-3-C MSD Matrix Spike Duplicate Total/NA
Water Filtration320-4398-4 EPAZ5S29BS3 Total/NA
Water FiltrationLCS 320-27018/2-A Lab Control Sample Total/NA
Water FiltrationMB 320-27018/1-A Method Blank Total/NA
Prep Batch: 27056
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Filtration320-4398-4 EPAZ5S29BS3 Total/NA
Water Filtration320-4421-H-6-C MS Matrix Spike Total/NA
Water Filtration320-4421-H-6-D MSD Matrix Spike Duplicate Total/NA
Water FiltrationLCS 320-27056/2-A Lab Control Sample Total/NA
TestAmerica Sacramento
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QC Association SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
LCMS (Continued)
Prep Batch: 27056 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water FiltrationMB 320-27056/1-A Method Blank Total/NA
Prep Batch: 27145
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C320-4398-4 EPAZ5S29BS3 Total/NA
Water 3510CLCS 320-27145/2-A Lab Control Sample Total/NA
Water 3510CMB 320-27145/1-A Method Blank Total/NA
Prep Batch: 27199
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid SHAKE320-4398-1 EPAZ5S10CS03 Total/NA
Solid SHAKE320-4398-2 EPAZ5S10BS03 Total/NA
Solid SHAKE320-4398-3 EPAZ5S10CS13 Total/NA
Solid SHAKE320-4398-5 EPAZ5S29BS00 Total/NA
Solid SHAKE320-4398-6 EPAZ5S29BS03 Total/NA
Solid SHAKE320-4398-7 EPAZ5S29BS08 Total/NA
Solid SHAKE320-4398-8 EPAZ5S29CS00 Total/NA
Solid SHAKE320-4398-9 EPAZ5S29CS03 Total/NA
Solid SHAKE320-4398-10 EPAZ5S29CS08 Total/NA
Solid SHAKE320-4398-11 EPAZ5S29CS18 Total/NA
Solid SHAKE320-4421-F-3-B MS Matrix Spike Total/NA
Solid SHAKE320-4421-F-3-C MSD Matrix Spike Duplicate Total/NA
Solid SHAKELCS 320-27199/2-A Lab Control Sample Total/NA
Solid SHAKEMB 320-27199/1-A Method Blank Total/NA
Analysis Batch: 27233
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6850 27018320-4264-H-3-B MS Matrix Spike Total/NA
Water 6850 27018320-4264-H-3-C MSD Matrix Spike Duplicate Total/NA
Water 6850 27018320-4398-4 EPAZ5S29BS3 Total/NA
Water 6850 27018LCS 320-27018/2-A Lab Control Sample Total/NA
Water 6850 27018MB 320-27018/1-A Method Blank Total/NA
Prep Batch: 27254
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550B320-4314-E-2-F MS Matrix Spike Total/NA
Solid 3550B320-4314-E-2-G MSD Matrix Spike Duplicate Total/NA
Solid 3550B320-4398-1 EPAZ5S10CS03 Total/NA
Solid 3550B320-4398-2 EPAZ5S10BS03 Total/NA
Solid 3550B320-4398-3 EPAZ5S10CS13 Total/NA
Solid 3550B320-4398-5 EPAZ5S29BS00 Total/NA
Solid 3550B320-4398-6 EPAZ5S29BS03 Total/NA
Solid 3550B320-4398-7 EPAZ5S29BS08 Total/NA
Solid 3550B320-4398-8 EPAZ5S29CS00 Total/NA
Solid 3550B320-4398-9 EPAZ5S29CS03 Total/NA
Solid 3550B320-4398-10 EPAZ5S29CS08 Total/NA
Solid 3550B320-4398-11 EPAZ5S29CS18 Total/NA
Solid 3550BLCS 320-27254/2-A Lab Control Sample Total/NA
Solid 3550BMB 320-27254/1-A Method Blank Total/NA
TestAmerica Sacramento
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QC Association SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
LCMS (Continued)
Analysis Batch: 27272
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8321A 27056320-4398-4 EPAZ5S29BS3 Total/NA
Solid 8321A 27199320-4398-7 EPAZ5S29BS08 Total/NA
Solid 8321A 27199320-4398-8 EPAZ5S29CS00 Total/NA
Solid 8321A 27199320-4398-9 EPAZ5S29CS03 Total/NA
Solid 8321A 27199320-4398-10 EPAZ5S29CS08 Total/NA
Solid 8321A 27199320-4398-11 EPAZ5S29CS18 Total/NA
Solid 8321A 27199320-4421-F-3-B MS Matrix Spike Total/NA
Solid 8321A 27199320-4421-F-3-C MSD Matrix Spike Duplicate Total/NA
Water 8321A 27056320-4421-H-6-C MS Matrix Spike Total/NA
Water 8321A 27056320-4421-H-6-D MSD Matrix Spike Duplicate Total/NA
Water 8321A 27056LCS 320-27056/2-A Lab Control Sample Total/NA
Solid 8321A 27199LCS 320-27199/2-A Lab Control Sample Total/NA
Water 8321A 27056MB 320-27056/1-A Method Blank Total/NA
Prep Batch: 27299
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid SHAKE320-4398-1 EPAZ5S10CS03 Total/NA
Solid SHAKE320-4398-2 EPAZ5S10BS03 Total/NA
Solid SHAKE320-4398-3 EPAZ5S10CS13 Total/NA
Solid SHAKE320-4398-5 EPAZ5S29BS00 Total/NA
Solid SHAKE320-4398-6 EPAZ5S29BS03 Total/NA
Solid SHAKE320-4398-7 EPAZ5S29BS08 Total/NA
Solid SHAKE320-4398-8 EPAZ5S29CS00 Total/NA
Solid SHAKE320-4398-9 EPAZ5S29CS03 Total/NA
Solid SHAKE320-4398-10 EPAZ5S29CS08 Total/NA
Solid SHAKE320-4398-11 EPAZ5S29CS18 Total/NA
Solid SHAKE320-4421-F-3-E MS Matrix Spike Total/NA
Solid SHAKE320-4421-F-3-F MSD Matrix Spike Duplicate Total/NA
Solid SHAKELCS 320-27299/2-A Lab Control Sample Total/NA
Solid SHAKEMB 320-27299/1-A Method Blank Total/NA
Analysis Batch: 27512
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8321A 27199320-4398-1 EPAZ5S10CS03 Total/NA
Solid 8321A 27199320-4398-2 EPAZ5S10BS03 Total/NA
Solid 8321A 27199320-4398-3 EPAZ5S10CS13 Total/NA
Solid 8321A 27199320-4398-5 EPAZ5S29BS00 Total/NA
Solid 8321A 27199320-4398-6 EPAZ5S29BS03 Total/NA
Solid 8321A 27199MB 320-27199/1-A Method Blank Total/NA
Analysis Batch: 27724
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid GCMSMS_NDM
A
27254320-4314-E-2-F MS Matrix Spike Total/NA
Solid GCMSMS_NDM
A
27254320-4314-E-2-G MSD Matrix Spike Duplicate Total/NA
Solid GCMSMS_NDM
A
27254320-4398-1 EPAZ5S10CS03 Total/NA
Solid GCMSMS_NDM
A
27254320-4398-2 EPAZ5S10BS03 Total/NA
Solid GCMSMS_NDM
A
27254320-4398-3 EPAZ5S10CS13 Total/NA
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QC Association SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
LCMS (Continued)
Analysis Batch: 27724 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid GCMSMS_NDM
A
27254320-4398-5 EPAZ5S29BS00 Total/NA
Solid GCMSMS_NDM
A
27254320-4398-6 EPAZ5S29BS03 Total/NA
Solid GCMSMS_NDM
A
27254320-4398-7 EPAZ5S29BS08 Total/NA
Solid GCMSMS_NDM
A
27254320-4398-8 EPAZ5S29CS00 Total/NA
Solid GCMSMS_NDM
A
27254320-4398-9 EPAZ5S29CS03 Total/NA
Solid GCMSMS_NDM
A
27254320-4398-10 EPAZ5S29CS08 Total/NA
Solid GCMSMS_NDM
A
27254320-4398-11 EPAZ5S29CS18 Total/NA
Solid GCMSMS_NDM
A
27254LCS 320-27254/2-A Lab Control Sample Total/NA
Solid GCMSMS_NDM
A
27254MB 320-27254/1-A Method Blank Total/NA
Analysis Batch: 27864
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6850 27299320-4398-1 EPAZ5S10CS03 Total/NA
Solid 6850 27299320-4398-2 EPAZ5S10BS03 Total/NA
Solid 6850 27299320-4398-3 EPAZ5S10CS13 Total/NA
Solid 6850 27299320-4398-5 EPAZ5S29BS00 Total/NA
Solid 6850 27299320-4398-6 EPAZ5S29BS03 Total/NA
Solid 6850 27299320-4398-7 EPAZ5S29BS08 Total/NA
Solid 6850 27299320-4398-8 EPAZ5S29CS00 Total/NA
Solid 6850 27299320-4398-9 EPAZ5S29CS03 Total/NA
Solid 6850 27299320-4398-10 EPAZ5S29CS08 Total/NA
Solid 6850 27299320-4398-11 EPAZ5S29CS18 Total/NA
Solid 6850 27299320-4421-F-3-E MS Matrix Spike Total/NA
Solid 6850 27299320-4421-F-3-F MSD Matrix Spike Duplicate Total/NA
Solid 6850 27299LCS 320-27299/2-A Lab Control Sample Total/NA
Solid 6850 27299MB 320-27299/1-A Method Blank Total/NA
Analysis Batch: 27918
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water GCMSMS_NDM
A
27145320-4398-4 EPAZ5S29BS3 Total/NA
Water GCMSMS_NDM
A
27145LCS 320-27145/2-A Lab Control Sample Total/NA
Water GCMSMS_NDM
A
27145MB 320-27145/1-A Method Blank Total/NA
General Chemistry
Analysis Batch: 27040
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D 2216320-4398-1 EPAZ5S10CS03 Total/NA
Solid D 2216320-4398-2 EPAZ5S10BS03 Total/NA
Solid D 2216320-4398-3 EPAZ5S10CS13 Total/NA
Solid D 2216320-4398-3 DU EPAZ5S10CS13 Total/NA
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QC Association SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
General Chemistry (Continued)
Analysis Batch: 27045
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D 2216320-4398-5 EPAZ5S29BS00 Total/NA
Solid D 2216320-4398-6 EPAZ5S29BS03 Total/NA
Solid D 2216320-4398-7 EPAZ5S29BS08 Total/NA
Solid D 2216320-4398-8 EPAZ5S29CS00 Total/NA
Solid D 2216320-4398-9 EPAZ5S29CS03 Total/NA
Solid D 2216320-4398-10 EPAZ5S29CS08 Total/NA
Solid D 2216320-4398-11 EPAZ5S29CS18 Total/NA
Solid D 2216320-4404-A-4 DU Duplicate Total/NA
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Lab ChronicleClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4398-1
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5S10CS03 Lab Sample ID: 320-4398-1Matrix: SolidDate Collected: 10/02/13 09:50
Percent Solids: 98.7Date Received: 10/03/13 09:10
Prep 5035 KSS10/03/13 17:27 TAL SAC26711
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.26 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 27356 10/11/13 20:00 WLS TAL SACTotal/NA 4.26 g 5 mL
Prep 3550B 27322 10/11/13 10:11 GDB TAL SACTotal/NA 30.48 g 3 mL
Analysis 8015B 1 27666 10/16/13 20:12 UFB TAL SACTotal/NA 30.48 g 3 mL
Analysis 9056 1 27899 10/17/13 16:02 LW1 TAL SACSoluble 5 mL 5 mL
Leach DI Leach 27468 10/16/13 14:30 LW1 TAL SACSoluble 10.09 g 50 mL
Analysis 9056 1 27900 10/17/13 16:02 LW1 TAL SACSoluble 5 mL
Prep SHAKE 27199 10/10/13 09:18 HJA TAL SACTotal/NA 9.98 g 100 mL
Analysis 8321A 1 27512 10/14/13 21:35 NSS TAL SACTotal/NA 9.98 g 100 mL
Prep 3550B 27254 10/10/13 13:38 GDB TAL SACTotal/NA 10.78 g 0.5 mL
Analysis GCMSMS_NDMA 1 27724 10/17/13 03:25 VMN TAL SACTotal/NA 10.78 g 0.5 mL
Prep SHAKE 27299 10/11/13 07:23 HJA TAL SACTotal/NA 3.04 g 10.00 mL
Analysis 6850 1 27864 10/18/13 23:16 NSS TAL SACTotal/NA 3.04 g 10.00 mL
Analysis D 2216 1 27040 10/08/13 12:02 BH TAL SACTotal/NA
Client Sample ID: EPAZ5S10BS03 Lab Sample ID: 320-4398-2Matrix: SolidDate Collected: 10/02/13 08:40
Percent Solids: 99.4Date Received: 10/03/13 09:10
Prep 5035 KSS10/03/13 17:27 TAL SAC26711
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.28 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 27356 10/11/13 20:25 WLS TAL SACTotal/NA 4.28 g 5 mL
Prep 3550B 27322 10/11/13 10:11 GDB TAL SACTotal/NA 30.59 g 3 mL
Analysis 8015B 1 27666 10/16/13 20:43 UFB TAL SACTotal/NA 30.59 g 3 mL
Leach DI Leach 27468 10/16/13 14:30 LW1 TAL SACSoluble 10.09 g 50 mL
Analysis 9056 1 27899 10/17/13 16:14 LW1 TAL SACSoluble 5 mL 5 mL
Analysis 9056 1 27900 10/17/13 16:14 LW1 TAL SACSoluble 5 mL
Prep SHAKE 27199 10/10/13 09:18 HJA TAL SACTotal/NA 10.08 g 100 mL
Analysis 8321A 1 27512 10/14/13 21:52 NSS TAL SACTotal/NA 10.08 g 100 mL
Prep 3550B 27254 10/10/13 13:38 GDB TAL SACTotal/NA 10.24 g 0.5 mL
Analysis GCMSMS_NDMA 1 27724 10/17/13 04:59 VMN TAL SACTotal/NA 10.24 g 0.5 mL
Prep SHAKE 27299 10/11/13 07:23 HJA TAL SACTotal/NA 3.05 g 10.00 mL
Analysis 6850 1 27864 10/18/13 23:33 NSS TAL SACTotal/NA 3.05 g 10.00 mL
Analysis D 2216 1 27040 10/08/13 12:02 BH TAL SACTotal/NA
Client Sample ID: EPAZ5S10CS13 Lab Sample ID: 320-4398-3Matrix: SolidDate Collected: 10/02/13 09:55
Percent Solids: 99.6Date Received: 10/03/13 09:10
Prep 5035 KSS10/03/13 17:27 TAL SAC26711
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.61 g 5 mL
TestAmerica Sacramento
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Lab ChronicleClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4398-1
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5S10CS13 Lab Sample ID: 320-4398-3Matrix: SolidDate Collected: 10/02/13 09:55
Percent Solids: 99.6Date Received: 10/03/13 09:10
Analysis 8260B/CA_LUFTM
S
WLS10/11/13 20:491 TAL SAC27356
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.61 g 5 mL
Prep 3550B 27322 10/11/13 10:11 GDB TAL SACTotal/NA 30.06 g 3 mL
Analysis 8015B 1 27666 10/16/13 21:13 UFB TAL SACTotal/NA 30.06 g 3 mL
Leach DI Leach 27468 10/16/13 14:30 LW1 TAL SACSoluble 10.01 g 50 mL
Analysis 9056 1 27899 10/17/13 16:25 LW1 TAL SACSoluble 5 mL 5 mL
Analysis 9056 1 27900 10/17/13 16:25 LW1 TAL SACSoluble 5 mL
Prep SHAKE 27199 10/10/13 09:18 HJA TAL SACTotal/NA 10.00 g 100 mL
Analysis 8321A 1 27512 10/14/13 22:10 NSS TAL SACTotal/NA 10.00 g 100 mL
Prep 3550B 27254 10/10/13 13:38 GDB TAL SACTotal/NA 10.07 g 0.5 mL
Analysis GCMSMS_NDMA 1 27724 10/17/13 05:23 VMN TAL SACTotal/NA 10.07 g 0.5 mL
Prep SHAKE 27299 10/11/13 07:23 HJA TAL SACTotal/NA 3.03 g 10.00 mL
Analysis 6850 1 27864 10/18/13 23:50 NSS TAL SACTotal/NA 3.03 g 10.00 mL
Analysis D 2216 1 27040 10/08/13 12:02 BH TAL SACTotal/NA
Client Sample ID: EPAZ5S29BS3 Lab Sample ID: 320-4398-4Matrix: WaterDate Collected: 10/02/13 13:30
Date Received: 10/03/13 09:10
Analysis 8260B/CA_LUFTM
S
MEO10/10/13 14:411 TAL SAC27229
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 50 mL 50 mL
Prep 3510C 27099 10/09/13 10:20 LRH TAL SACTotal/NA 1055 mL 3 mL
Analysis 8015B 1 27666 10/17/13 07:18 UFB TAL SACTotal/NA 1055 mL 3 mL
Analysis 9056 1 26700 10/03/13 12:14 LW1 TAL SACTotal/NA 5 mL
Analysis 9056 1 26701 10/03/13 12:14 LW1 TAL SACTotal/NA 5 mL
Prep Filtration 27018 10/08/13 10:00 HJA TAL SACTotal/NA 4.00 mL 4.00 mL
Analysis 6850 1 27233 10/11/13 11:13 NSS TAL SACTotal/NA 4.00 mL 4.00 mL
Prep Filtration 27056 10/08/13 14:47 HJA TAL SACTotal/NA 10.00 mL 10.00 mL
Analysis 8321A 1 27272 10/10/13 23:41 NSS TAL SACTotal/NA 10.00 mL 10.00 mL
Prep 3510C 27145 10/09/13 14:56 LRH TAL SACTotal/NA 1050.7 mL 0.5 mL
Analysis GCMSMS_NDMA 1 27918 10/18/13 21:14 VMN TAL SACTotal/NA 1050.7 mL 0.5 mL
Client Sample ID: EPAZ5S29BS00 Lab Sample ID: 320-4398-5Matrix: SolidDate Collected: 10/02/13 11:35
Percent Solids: 100.0Date Received: 10/03/13 09:10
Prep 5035 KSS10/03/13 17:27 TAL SAC26711
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.65 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 27356 10/11/13 21:13 WLS TAL SACTotal/NA 4.65 g 5 mL
Prep 3550B 27322 10/11/13 10:11 GDB TAL SACTotal/NA 30.35 g 3 mL
Analysis 8015B 1 27666 10/16/13 21:43 UFB TAL SACTotal/NA 30.35 g 3 mL
Leach DI Leach 27468 10/16/13 14:30 LW1 TAL SACSoluble 10.02 g 50 mL
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Lab ChronicleClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4398-1
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5S29BS00 Lab Sample ID: 320-4398-5Matrix: SolidDate Collected: 10/02/13 11:35
Percent Solids: 100.0Date Received: 10/03/13 09:10
Analysis 9056 LW110/17/13 16:371 TAL SAC27899
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Soluble 5 mL 5 mL
Analysis 9056 1 27900 10/17/13 16:37 LW1 TAL SACSoluble 5 mL
Prep SHAKE 27199 10/10/13 09:18 HJA TAL SACTotal/NA 10.04 g 100 mL
Analysis 8321A 1 27512 10/14/13 22:27 NSS TAL SACTotal/NA 10.04 g 100 mL
Prep 3550B 27254 10/10/13 13:38 GDB TAL SACTotal/NA 10.12 g 0.5 mL
Analysis GCMSMS_NDMA 1 27724 10/17/13 05:47 VMN TAL SACTotal/NA 10.12 g 0.5 mL
Prep SHAKE 27299 10/11/13 07:23 HJA TAL SACTotal/NA 3.09 g 10.00 mL
Analysis 6850 1 27864 10/19/13 00:06 NSS TAL SACTotal/NA 3.09 g 10.00 mL
Analysis D 2216 1 27045 10/08/13 13:27 BH TAL SACTotal/NA
Client Sample ID: EPAZ5S29BS03 Lab Sample ID: 320-4398-6Matrix: SolidDate Collected: 10/02/13 11:55
Percent Solids: 98.8Date Received: 10/03/13 09:10
Prep 5035 KSS10/03/13 17:27 TAL SAC26711
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.86 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 27356 10/11/13 21:38 WLS TAL SACTotal/NA 4.86 g 5 mL
Prep 3550B 27322 10/11/13 10:11 GDB TAL SACTotal/NA 30.60 g 3 mL
Analysis 8015B 1 27666 10/16/13 23:45 UFB TAL SACTotal/NA 30.60 g 3 mL
Analysis 9056 1 27899 10/17/13 16:48 LW1 TAL SACSoluble 5 mL 5 mL
Leach DI Leach 27468 10/16/13 14:30 LW1 TAL SACSoluble 10.11 g 50 mL
Analysis 9056 1 27900 10/17/13 16:48 LW1 TAL SACSoluble 5 mL
Prep SHAKE 27199 10/10/13 09:18 HJA TAL SACTotal/NA 10.10 g 100 mL
Analysis 8321A 1 27512 10/14/13 22:45 NSS TAL SACTotal/NA 10.10 g 100 mL
Prep 3550B 27254 10/10/13 13:38 GDB TAL SACTotal/NA 10.30 g 0.5 mL
Analysis GCMSMS_NDMA 1 27724 10/17/13 06:11 VMN TAL SACTotal/NA 10.30 g 0.5 mL
Prep SHAKE 27299 10/11/13 07:23 HJA TAL SACTotal/NA 3.06 g 10.00 mL
Analysis 6850 1 27864 10/19/13 00:23 NSS TAL SACTotal/NA 3.06 g 10.00 mL
Analysis D 2216 1 27045 10/08/13 13:27 BH TAL SACTotal/NA
Client Sample ID: EPAZ5S29BS08 Lab Sample ID: 320-4398-7Matrix: SolidDate Collected: 10/02/13 12:05
Percent Solids: 96.9Date Received: 10/03/13 09:10
Prep 5035 KSS10/03/13 17:27 TAL SAC26711
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.96 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 27356 10/11/13 22:02 WLS TAL SACTotal/NA 4.96 g 5 mL
Prep 3550B 27322 10/11/13 10:11 GDB TAL SACTotal/NA 30.02 g 3 mL
Analysis 8015B 1 27666 10/17/13 00:15 UFB TAL SACTotal/NA 30.02 g 3 mL
Analysis 9056 1 27899 10/17/13 17:00 LW1 TAL SACSoluble 5 mL 5 mL
Leach DI Leach 27468 10/16/13 14:30 LW1 TAL SACSoluble 10.10 g 50 mL
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Lab ChronicleClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4398-1
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5S29BS08 Lab Sample ID: 320-4398-7Matrix: SolidDate Collected: 10/02/13 12:05
Percent Solids: 96.9Date Received: 10/03/13 09:10
Analysis 9056 LW110/17/13 17:001 TAL SAC27900
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Soluble 5 mL
Prep SHAKE 27199 10/10/13 09:18 HJA TAL SACTotal/NA 10.11 g 100 mL
Analysis 8321A 1 27272 10/11/13 09:21 NSS TAL SACTotal/NA 10.11 g 100 mL
Prep 3550B 27254 10/10/13 13:38 GDB TAL SACTotal/NA 10.30 g 0.5 mL
Analysis GCMSMS_NDMA 1 27724 10/17/13 06:34 VMN TAL SACTotal/NA 10.30 g 0.5 mL
Prep SHAKE 27299 10/11/13 07:23 HJA TAL SACTotal/NA 3.12 g 10.00 mL
Analysis 6850 1 27864 10/19/13 00:40 NSS TAL SACTotal/NA 3.12 g 10.00 mL
Analysis D 2216 1 27045 10/08/13 13:27 BH TAL SACTotal/NA
Client Sample ID: EPAZ5S29CS00 Lab Sample ID: 320-4398-8Matrix: SolidDate Collected: 10/02/13 11:05
Percent Solids: 100.0Date Received: 10/03/13 09:10
Prep 5035 KSS10/03/13 17:27 TAL SAC26711
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.21 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 27356 10/11/13 22:26 WLS TAL SACTotal/NA 4.21 g 5 mL
Prep 3550B 27322 10/11/13 10:11 GDB TAL SACTotal/NA 30.40 g 3 mL
Analysis 8015B 1 27666 10/17/13 00:45 UFB TAL SACTotal/NA 30.40 g 3 mL
Leach DI Leach 27468 10/16/13 14:30 LW1 TAL SACSoluble 10.03 g 50 mL
Analysis 9056 1 27899 10/17/13 17:11 LW1 TAL SACSoluble 5 mL 5 mL
Analysis 9056 1 27900 10/17/13 17:11 LW1 TAL SACSoluble 5 mL
Prep SHAKE 27199 10/10/13 09:18 HJA TAL SACTotal/NA 10.03 g 100 mL
Analysis 8321A 1 27272 10/11/13 09:39 NSS TAL SACTotal/NA 10.03 g 100 mL
Prep 3550B 27254 10/10/13 13:38 GDB TAL SACTotal/NA 10.19 g 0.5 mL
Analysis GCMSMS_NDMA 1 27724 10/17/13 06:58 VMN TAL SACTotal/NA 10.19 g 0.5 mL
Prep SHAKE 27299 10/11/13 07:23 HJA TAL SACTotal/NA 3.05 g 10.00 mL
Analysis 6850 1 27864 10/19/13 00:57 NSS TAL SACTotal/NA 3.05 g 10.00 mL
Analysis D 2216 1 27045 10/08/13 13:27 BH TAL SACTotal/NA
Client Sample ID: EPAZ5S29CS03 Lab Sample ID: 320-4398-9Matrix: SolidDate Collected: 10/02/13 11:10
Percent Solids: 99.7Date Received: 10/03/13 09:10
Prep 5035 KSS10/03/13 17:27 TAL SAC26711
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.66 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 27356 10/11/13 22:50 WLS TAL SACTotal/NA 4.66 g 5 mL
Prep 3550B 27322 10/11/13 10:11 GDB TAL SACTotal/NA 29.95 g 3 mL
Analysis 8015B 1 27666 10/17/13 01:15 UFB TAL SACTotal/NA 29.95 g 3 mL
Analysis 9056 1 27899 10/17/13 17:23 LW1 TAL SACSoluble 5 mL 5 mL
Leach DI Leach 27468 10/16/13 14:30 LW1 TAL SACSoluble 10.12 g 50 mL
Analysis 9056 1 27900 10/17/13 17:23 LW1 TAL SACSoluble 5 mL 1.0 mL
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Lab ChronicleClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4398-1
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5S29CS03 Lab Sample ID: 320-4398-9Matrix: SolidDate Collected: 10/02/13 11:10
Percent Solids: 99.7Date Received: 10/03/13 09:10
Prep SHAKE HJA10/10/13 09:18 TAL SAC27199
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10.11 g 100 mL
Analysis 8321A 1 27272 10/11/13 10:14 NSS TAL SACTotal/NA 10.11 g 100 mL
Prep 3550B 27254 10/10/13 13:38 GDB TAL SACTotal/NA 10.27 g 0.5 mL
Analysis GCMSMS_NDMA 1 27724 10/17/13 07:21 VMN TAL SACTotal/NA 10.27 g 0.5 mL
Prep SHAKE 27299 10/11/13 07:23 HJA TAL SACTotal/NA 3.01 g 10.00 mL
Analysis 6850 1 27864 10/19/13 01:13 NSS TAL SACTotal/NA 3.01 g 10.00 mL
Analysis D 2216 1 27045 10/08/13 13:27 BH TAL SACTotal/NA
Client Sample ID: EPAZ5S29CS08 Lab Sample ID: 320-4398-10Matrix: SolidDate Collected: 10/02/13 11:15
Percent Solids: 97.9Date Received: 10/03/13 09:10
Prep 5035 KSS10/03/13 17:27 TAL SAC26711
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.48 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 27356 10/11/13 23:15 WLS TAL SACTotal/NA 5.48 g 5 mL
Prep 3550B 27322 10/11/13 10:11 GDB TAL SACTotal/NA 30.53 g 3 mL
Analysis 8015B 1 27666 10/17/13 01:45 UFB TAL SACTotal/NA 30.53 g 3 mL
Leach DI Leach 27468 10/16/13 14:30 LW1 TAL SACSoluble 10.09 g 50 mL
Analysis 9056 1 27899 10/17/13 17:34 LW1 TAL SACSoluble 5 mL 5 mL
Analysis 9056 1 27900 10/17/13 17:34 LW1 TAL SACSoluble 5 mL
Prep SHAKE 27199 10/10/13 09:18 HJA TAL SACTotal/NA 10.09 g 100 mL
Analysis 8321A 1 27272 10/11/13 10:32 NSS TAL SACTotal/NA 10.09 g 100 mL
Prep 3550B 27254 10/10/13 13:38 GDB TAL SACTotal/NA 9.97 g 0.5 mL
Analysis GCMSMS_NDMA 1 27724 10/17/13 07:45 VMN TAL SACTotal/NA 9.97 g 0.5 mL
Prep SHAKE 27299 10/11/13 07:23 HJA TAL SACTotal/NA 3.06 g 10.00 mL
Analysis 6850 1 27864 10/19/13 01:30 NSS TAL SACTotal/NA 3.06 g 10.00 mL
Analysis D 2216 1 27045 10/08/13 13:27 BH TAL SACTotal/NA
Client Sample ID: EPAZ5S29CS18 Lab Sample ID: 320-4398-11Matrix: SolidDate Collected: 10/02/13 11:20
Percent Solids: 97.8Date Received: 10/03/13 09:10
Prep 5035 KSS10/03/13 17:27 TAL SAC26711
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.5 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 27514 10/14/13 23:20 WLS TAL SACTotal/NA 5.5 g 5 mL
Prep 3550B 27322 10/11/13 10:11 GDB TAL SACTotal/NA 30.18 g 3 mL
Analysis 8015B 1 27666 10/17/13 02:16 UFB TAL SACTotal/NA 30.18 g 3 mL
Leach DI Leach 27468 10/16/13 14:30 LW1 TAL SACSoluble 10.07 g 50 mL
Analysis 9056 1 27899 10/17/13 17:46 LW1 TAL SACSoluble 5 mL 5 mL
Analysis 9056 1 27900 10/17/13 17:46 LW1 TAL SACSoluble 5 mL
Prep SHAKE 27199 10/10/13 09:18 HJA TAL SACTotal/NA 10.07 g 100 mL
Analysis 8321A 1 27272 10/11/13 10:49 NSS TAL SACTotal/NA 10.07 g 100 mL
TestAmerica Sacramento
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Lab ChronicleClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4398-1
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5S29CS18 Lab Sample ID: 320-4398-11Matrix: SolidDate Collected: 10/02/13 11:20
Percent Solids: 97.8Date Received: 10/03/13 09:10
Prep 3550B GDB10/10/13 13:38 TAL SAC27254
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10.41 g 0.5 mL
Analysis GCMSMS_NDMA 1 27724 10/17/13 08:09 VMN TAL SACTotal/NA 10.41 g 0.5 mL
Prep SHAKE 27299 10/11/13 07:23 HJA TAL SACTotal/NA 3.03 g 10.00 mL
Analysis 6850 1 27864 10/19/13 01:47 NSS TAL SACTotal/NA 3.03 g 10.00 mL
Analysis D 2216 1 27045 10/08/13 13:27 BH TAL SACTotal/NA
Laboratory References:
TAL SAC = TestAmerica Sacramento, 880 Riverside Parkway, West Sacramento, CA 95605, TEL (916)373-5600
TestAmerica Sacramento
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Certification SummaryClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4398-1
Project/Site: Stringfellow Acid Project
Laboratory: TestAmerica SacramentoAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
A2LA NE-OS-22-13A2LA 01-31-14
A2LA DoD ELAP 2928-01 01-31-14
Alaska (UST) State Program 10 UST-055 12-18-13
Arizona State Program 9 AZ0708 08-11-14
Arkansas DEQ State Program 6 88-0691 06-17-14
California NELAP 9 1119CA 01-31-14
Connecticut State Program 1 PH-0691 06-30-15
Florida NELAP 4 E87570 06-30-14
Guam State Program 9 N/A 08-31-14
Hawaii State Program 9 N/A 01-31-14
Illinois NELAP 5 200060 03-17-14
Kansas NELAP 7 E-10375 10-31-13
Louisiana NELAP 6 30612 06-30-14
Michigan State Program 5 9947 01-31-14
Nebraska State Program 7 NE-OS-22-13 01-31-14
Nevada State Program 9 CA44 07-31-14
New Jersey NELAP 2 CA005 06-30-14
New York NELAP 2 11666 04-01-14
Northern Mariana Islands State Program 9 MP0007 02-01-14
Oregon NELAP 10 CA200005 03-28-14
Pennsylvania NELAP 3 68-01272 03-31-14
South Carolina State Program 4 87014 06-30-14
Texas NELAP 6 T104704399-08-TX 05-31-14
US Fish & Wildlife Federal LE148388-0 12-31-13
USDA Federal P330-11-00436 12-30-14
USEPA UCMR Federal 1 CA00044 11-06-14
Utah NELAP 8 QUAN1 01-31-14
Washington State Program 10 C581 05-05-14
West Virginia State Program 3 9930C 12-31-13
Wyoming State Program 8 8TMS-Q 01-31-14
TestAmerica Sacramento
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Method SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method Method Description LaboratoryProtocol
SW8468260B/CA_LUFTM
S
Volatile Organic Compounds by GC/MS TAL SAC
SW8468015B Diesel Range Organics (DRO) (GC) TAL SAC
SW8469056 Anions, Ion Chromatography TAL SAC
EPA6850 Perchlorate by LC/MS or LC/MS/MS TAL SAC
SW8468321A Benzene Sulfonic Acids (LCMS) TAL SAC
TestAmerica SOPGCMSMS_NDMA Nitrosamines by Isotope Dilution and GC/CI/MS/MS TAL SAC
ASTMD 2216 Percent Moisture TAL SAC
Protocol References:
ASTM = ASTM International
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
TestAmerica SOP = TestAmerica, Inc., Standard Operating Procedure
Laboratory References:
TAL SAC = TestAmerica Sacramento, 880 Riverside Parkway, West Sacramento, CA 95605, TEL (916)373-5600
TestAmerica Sacramento
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Sample SummaryTestAmerica Job ID: 320-4398-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
320-4398-1 EPAZ5S10CS03 Solid 10/02/13 09:50 10/03/13 09:10
320-4398-2 EPAZ5S10BS03 Solid 10/02/13 08:40 10/03/13 09:10
320-4398-3 EPAZ5S10CS13 Solid 10/02/13 09:55 10/03/13 09:10
320-4398-4 EPAZ5S29BS3 Water 10/02/13 13:30 10/03/13 09:10
320-4398-5 EPAZ5S29BS00 Solid 10/02/13 11:35 10/03/13 09:10
320-4398-6 EPAZ5S29BS03 Solid 10/02/13 11:55 10/03/13 09:10
320-4398-7 EPAZ5S29BS08 Solid 10/02/13 12:05 10/03/13 09:10
320-4398-8 EPAZ5S29CS00 Solid 10/02/13 11:05 10/03/13 09:10
320-4398-9 EPAZ5S29CS03 Solid 10/02/13 11:10 10/03/13 09:10
320-4398-10 EPAZ5S29CS08 Solid 10/02/13 11:15 10/03/13 09:10
320-4398-11 EPAZ5S29CS18 Solid 10/02/13 11:20 10/03/13 09:10
TestAmerica Sacramento
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Login Sample Receipt Checklist
Client: CH2M Hill Constructors, Inc. Job Number: 320-4398-1
Login Number: 4398
Question Answer Comment
Creator: Hytrek, Cheryl
List Source: TestAmerica Sacramento
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
N/AIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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