Appendix D - Geotechnical Report€¦ · ATTN: ERIC CHUNG FINAL Report Date: 25-AUG-15 14:35 (MT)...

Appendix D - Geotechnical Report

[This report shall not be reproduced except in full without the written authority of the Laboratory.]

18-AUG-15

Lab Work Order #: L1659064

Date Received:CHUNG AND VANDER DOELEN

311 VICTORIA ST. N.KITCHENER ON N2H 5E1

ATTN: ERIC CHUNGFINAL 25-AUG-15 14:35 (MT)Report Date:

Version:

Certificate of Analysis

ALS CANADA LTD Part of the ALS Group A Campbell Brothers Limited Company

____________________________________________

Mary-Lynn PiresAccount Manager

ADDRESS: 60 Northland Road, Unit 1, Waterloo, ON N2V 2B8 Canada | Phone: +1 519 886 6910 | Fax: +1 519 886 9047

Client Phone: 519-742-8979

G15100Job Reference: G15100Project P.O. #:

14-461973, 14-461974C of C Numbers:Legal Site Desc:

Result

25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed

Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)

L1659064 CONTD....2Page of

G15100ANALYTICAL GUIDELINE REPORT

Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:

Guideline Limits

#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)

* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.

18

L1659064-1

L1659064-2

BH1-1

BH1-2

D. FONDEVILLA on 21-JUL-15


Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

#1

#1

#2

#2

Physical Tests

Leachable Anions & Nutrients

Anions and Nutrients

Cyanides

Saturated Paste Extractables

Metals

Speciated Metals

Physical Tests

Polycyclic Aromatic Hydrocarbons

Conductivity% MoisturepH

Chloride

Sulphate

Cyanide, Weak Acid Diss

SARCalcium (Ca)Magnesium (Mg)Sodium (Na)

Antimony (Sb)Arsenic (As)Barium (Ba)Beryllium (Be)Boron (B)Boron (B), Hot Water Ext.Cadmium (Cd)Chromium (Cr)Cobalt (Co)Copper (Cu)Lead (Pb)Mercury (Hg)Molybdenum (Mo)Nickel (Ni)Selenium (Se)Silver (Ag)Thallium (Tl)Uranium (U)Vanadium (V)Zinc (Zn)

Chromium, Hexavalent

% Moisture

Acenaphthene

0.1573.558.03

24.4

20

<0.050

0.5412.12.27.8

<1.01.88.2

<0.50<5.0<0.10<0.5010.02.36.05.6

0.0061<1.04.3

<1.0<0.20<0.50<1.028.721.7

0.23

9.66

<0.050

0.00400.100.10

5.0

20

0.050

0.101.01.01.0

1.01.01.00.505.00.100.501.01.01.01.0

0.00501.01.01.00.200.501.01.05.0

0.20

0.10

0.050

mS/cm%

pH units

ug/g

mg/kg

ug/g

SARmg/Lmg/Lmg/L

ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g

ug/g

%

ug/g

20-AUG-1519-AUG-1519-AUG-15

25-AUG-15

24-AUG-15

19-AUG-15

20-AUG-1520-AUG-1520-AUG-1520-AUG-15

20-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-15

20-AUG-15

19-AUG-15

24-AUG-15

1.4 1.4

0.051 0.051

12 12

40 5018 18670 6708 10

120 1202 2

1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340

8 10

21 29

Result






Guideline Limits



18

L1659064-2

L1659064-3

BH1-2

BH2-1



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

#1

#1

#2

#2


Polychlorinated Biphenyls

Physical Tests

Cyanides


Metals

AcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenzo(ah)anthraceneFluorantheneFluoreneIndeno(1,2,3-cd)pyrene1+2-Methylnaphthalenes1-Methylnaphthalene2-MethylnaphthaleneNaphthalenePhenanthrenePyreneSurrogate: 2-FluorobiphenylSurrogate: p-Terphenyl d14

Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260Total PCBsSurrogate: d14-Terphenyl




Antimony (Sb)Arsenic (As)Barium (Ba)

<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.042<0.030<0.030<0.050<0.050<0.05091.691.1

<0.010<0.010<0.010<0.010<0.02096.2

0.1534.818.07

<0.050

0.2510.76.14.1

<1.02.712.9

0.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0420.0300.0300.0500.0500.050

50-14050-140

0.0100.0100.0100.0100.020

60-140

0.00400.100.10

0.050

0.101.01.01.0

1.01.01.0

ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g%%

ug/gug/gug/gug/gug/g%

mS/cm%

pH units

ug/g

SARmg/Lmg/Lmg/L

ug/gug/gug/g


22-AUG-1522-AUG-1522-AUG-1522-AUG-1522-AUG-1522-AUG-15

20-AUG-1519-AUG-1519-AUG-15

19-AUG-15

20-AUG-1520-AUG-1520-AUG-1520-AUG-15

20-AUG-1520-AUG-1520-AUG-15

0.15 0.170.67 0.740.96 0.960.3 0.30.96 0.969.6 9.60.96 0.969.6 9.60.1 0.19.6 9.662 69

0.76 0.9530 4230 4230 429.6 2812 1696 96

1.1 1.1

1.4 1.4

0.051 0.051

12 12

40 5018 18670 670

Result






Guideline Limits



18

L1659064-3

L1659064-4

BH2-1

BH2-2



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

#1

#1

#2

#2

Metals

Speciated Metals

Physical Tests


Beryllium (Be)Boron (B)Boron (B), Hot Water Ext.Cadmium (Cd)Chromium (Cr)Cobalt (Co)Copper (Cu)Lead (Pb)Mercury (Hg)Molybdenum (Mo)Nickel (Ni)Selenium (Se)Silver (Ag)Thallium (Tl)Uranium (U)Vanadium (V)Zinc (Zn)


% Moisture

AcenaphtheneAcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenzo(ah)anthraceneFluorantheneFluoreneIndeno(1,2,3-cd)pyrene1+2-Methylnaphthalenes1-Methylnaphthalene2-MethylnaphthaleneNaphthalenePhenanthrenePyrene

<0.506.5

<0.10<0.507.62.510.48.3

0.0059<1.05.4

<1.0<0.20<0.50<1.015.144.3

<0.20

6.73

<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.042<0.030<0.030<0.050<0.050<0.050

0.505.00.100.501.01.01.01.0

0.00501.01.01.00.200.501.01.05.0

0.20

0.10

0.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0420.0300.0300.0500.0500.050

ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g

ug/g

%

ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g

20-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-15

20-AUG-15

19-AUG-15

24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15

8 10120 1202 2

1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340

8 10

21 290.15 0.170.67 0.740.96 0.960.3 0.30.96 0.969.6 9.60.96 0.969.6 9.60.1 0.19.6 9.662 69

0.76 0.9530 4230 4230 429.6 2812 1696 96

Result






Guideline Limits



18

L1659064-4

L1659064-5

BH2-2

BH3-1



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

#1

#1

#2

#2



Physical Tests

Cyanides


Metals

Speciated Metals

Surrogate: 2-FluorobiphenylSurrogate: p-Terphenyl d14






89.889.1

<0.010<0.010<0.010<0.010<0.02096.0

0.1418.108.16

<0.050

0.327.75.94.8

<1.01.914.7

<0.505.4

<0.10<0.506.92.16.410.4

0.0051<1.04.1

<1.0<0.20<0.50<1.014.339.7

50-14050-140

0.0100.0100.0100.0100.020

60-140

0.00400.100.10

0.050

0.101.01.01.0

1.01.01.00.505.00.100.501.01.01.01.0

0.00501.01.01.00.200.501.01.05.0

%%


mS/cm%

pH units

ug/g

SARmg/Lmg/Lmg/L


24-AUG-1524-AUG-15


20-AUG-1519-AUG-1519-AUG-15

19-AUG-15

20-AUG-1520-AUG-1520-AUG-1520-AUG-15


1.1 1.1

1.4 1.4

0.051 0.051

12 12

40 5018 18670 6708 10

120 1202 2

1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340

Result






Guideline Limits



18

L1659064-5

L1659064-6

L1659064-7

BH3-1

BH3-2

BH4-2




Sampled By:

Sampled By:

Sampled By:

SOIL

SOIL

SOIL

Matrix:

Matrix:

Matrix:

#1

#1

#1

#2

#2

#2

Speciated Metals

Physical Tests



Physical Tests

Cyanides


% Moisture

AcenaphtheneAcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenzo(ah)anthraceneFluorantheneFluoreneIndeno(1,2,3-cd)pyrene1+2-Methylnaphthalenes1-Methylnaphthalene2-MethylnaphthaleneNaphthalenePhenanthrenePyreneSurrogate: 2-FluorobiphenylSurrogate: p-Terphenyl d14



<0.20

3.15

<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.042<0.030<0.030<0.050<0.050<0.05091.590.7

<0.010<0.010<0.010<0.010<0.02099.4

0.3700.298.14

0.20

0.10

0.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0420.0300.0300.0500.0500.050

50-14050-140

0.0100.0100.0100.0100.020

60-140

0.00400.100.10

ug/g

%

ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g%%


mS/cm%

pH units

20-AUG-15

19-AUG-15

24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15


20-AUG-1519-AUG-1519-AUG-15

8 10

21 290.15 0.170.67 0.740.96 0.960.3 0.30.96 0.969.6 9.60.96 0.969.6 9.60.1 0.19.6 9.662 69

0.76 0.9530 4230 4230 429.6 2812 1696 96

1.1 1.1

1.4 1.4

Result






Guideline Limits



18

L1659064-7

L1659064-8

BH4-2

BH5-1



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

#1

#1

#2

#2

Cyanides


Metals

Speciated Metals

Physical Tests

Cyanides


Metals








<0.050

4.4721.61.479.4

<1.02.318.4

<0.50<5.0<0.10<0.509.12.76.45.8

0.0142<1.06.0

<1.0<0.20<0.50<1.017.829.7

0.28

0.2671.008.23

<0.050

1.6448.25.945.2

0.050

0.101.01.01.0

1.01.01.00.505.00.100.501.01.01.01.0

0.00501.01.01.00.200.501.01.05.0

0.20

0.00400.100.10

0.050

0.101.01.01.0

ug/g

SARmg/Lmg/Lmg/L


ug/g

mS/cm%

pH units

ug/g

SARmg/Lmg/Lmg/L

19-AUG-15

20-AUG-1520-AUG-1520-AUG-1520-AUG-15


20-AUG-15

20-AUG-1519-AUG-1519-AUG-15

19-AUG-15

20-AUG-1520-AUG-1520-AUG-1520-AUG-15

0.051 0.051

12 12

40 5018 18670 6708 10

120 1202 2

1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340

8 10

1.4 1.4

0.051 0.051

12 12

Result






Guideline Limits



18

L1659064-8 BH5-1D. FONDEVILLA on 21-JUL-15Sampled By:SOILMatrix: #1 #2

Metals

Speciated Metals





<1.02.917.2

<0.507.90.13

<0.508.62.57.710.2

0.0123<1.05.7

<1.0<0.20<0.50<1.015.544.2

0.21

<0.050<0.050<0.050<0.050<0.0500.051

<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.042<0.030<0.030<0.050<0.050<0.05090.590.2

1.01.01.00.505.00.100.501.01.01.01.0

0.00501.01.01.00.200.501.01.05.0

0.20

0.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0420.0300.0300.0500.0500.050

50-14050-140


ug/g



20-AUG-15


40 5018 18670 6708 10

120 1202 2

1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340

8 10

21 290.15 0.170.67 0.740.96 0.960.3 0.30.96 0.969.6 9.60.96 0.969.6 9.60.1 0.19.6 9.662 69

0.76 0.9530 4230 4230 429.6 2812 1696 96

Result






Guideline Limits



18

L1659064-9

L1659064-10

BH6-2

BH7-2



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

#1

#1

#2

#2

Physical Tests

Cyanides


Metals

Speciated Metals

Physical Tests









Chloride

Sulphate

0.1247.177.96

<0.050

0.7822.42.814.8

<1.01.810.9

<0.505.2

<0.10<0.507.42.16.26.6

<0.0050<1.04.1

<1.0<0.20<0.50<1.015.238.9

0.21

0.23314.07.57

48.3

<20

0.00400.100.10

0.050

0.101.01.01.0

1.01.01.00.505.00.100.501.01.01.01.0

0.00501.01.01.00.200.501.01.05.0

0.20

0.00400.100.10

5.0

20

mS/cm%

pH units

ug/g

SARmg/Lmg/Lmg/L


ug/g

mS/cm%

pH units

ug/g

mg/kg

20-AUG-1519-AUG-1519-AUG-15

19-AUG-15

20-AUG-1520-AUG-1520-AUG-1520-AUG-15


20-AUG-15

20-AUG-1519-AUG-1519-AUG-15

25-AUG-15

24-AUG-15

1.4 1.4

0.051 0.051

12 12

40 5018 18670 6708 10

120 1202 2

1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340

8 10

1.4 1.4

Result






Guideline Limits



18

L1659064-10

L1659064-11

BH7-2

BH8-1



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

#1

#1

#2

#2

Cyanides


Metals

Speciated Metals

Physical Tests

Cyanides


Metals








<0.050

2.0519.42.135.5

<1.03.023.5

<0.505.70.42

<0.5010.63.08.318.1

0.0231<1.05.8

<1.0<0.20<0.50<1.022.340.6

<0.20

0.1753.858.11

<0.050

0.6510.73.99.8

0.050

0.101.01.01.0

1.01.01.00.505.00.100.501.01.01.01.0

0.00501.01.01.00.200.501.01.05.0

0.20

0.00400.100.10

0.050

0.101.01.01.0

ug/g

SARmg/Lmg/Lmg/L


ug/g

mS/cm%

pH units

ug/g

SARmg/Lmg/Lmg/L

19-AUG-15

20-AUG-1520-AUG-1520-AUG-1520-AUG-15


20-AUG-15

20-AUG-1519-AUG-1519-AUG-15

19-AUG-15

20-AUG-1520-AUG-1520-AUG-1520-AUG-15

0.051 0.051

12 12

40 5018 18670 6708 10

120 1202 2

1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340

8 10

1.4 1.4

0.051 0.051

12 12

Result






Guideline Limits



18

L1659064-11

L1659064-12

BH8-1

BH8-2



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

#1

#1

#2

#2

Metals

Speciated Metals

Physical Tests




% Moisture

AcenaphtheneAcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenzo(ah)anthraceneFluorantheneFluoreneIndeno(1,2,3-cd)pyrene1+2-Methylnaphthalenes1-Methylnaphthalene2-Methylnaphthalene

<1.03.015.2

<0.507.1

<0.10<0.508.22.810.513.7

0.0100<1.05.8

<1.0<0.20<0.50<1.015.157.3

<0.20

12.3

<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.042<0.030<0.030

1.01.01.00.505.00.100.501.01.01.01.0

0.00501.01.01.00.200.501.01.05.0

0.20

0.10

0.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0420.0300.030


ug/g

%

ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g


20-AUG-15

19-AUG-15

24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15

40 5018 18670 6708 10

120 1202 2

1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340

8 10

21 290.15 0.170.67 0.740.96 0.960.3 0.30.96 0.969.6 9.60.96 0.969.6 9.60.1 0.19.6 9.662 69

0.76 0.9530 4230 4230 42

Result






Guideline Limits



18

L1659064-12

L1659064-13

BH8-2

BH9-1



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

#1

#1

#2

#2


Physical Tests



Cyanides


Metals

NaphthalenePhenanthrenePyreneSurrogate: 2-FluorobiphenylSurrogate: p-Terphenyl d14


Chloride

Sulphate




<0.050<0.050<0.05091.590.3

0.21710.77.72

12.6

<20

<0.050

<0.1025.74.52.1

<1.03.842.2

<0.50<5.00.23

<0.5013.54.38.512.6

0.0276<1.08.8

<1.0<0.20<0.50<1.026.549.5

0.0500.0500.050

50-14050-140

0.00400.100.10

5.0

20

0.050

0.101.01.01.0

1.01.01.00.505.00.100.501.01.01.01.0

0.00501.01.01.00.200.501.01.05.0

ug/gug/gug/g%%

mS/cm%

pH units

ug/g

mg/kg

ug/g

SARmg/Lmg/Lmg/L


24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15

20-AUG-1519-AUG-1519-AUG-15

25-AUG-15

24-AUG-15

19-AUG-15

20-AUG-1520-AUG-1520-AUG-1520-AUG-15


9.6 2812 1696 96

1.4 1.4

0.051 0.051

12 12

40 5018 18670 6708 10

120 1202 2

1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340

Result






Guideline Limits



18

L1659064-13

L1659064-14

L1659064-15

BH9-1

BH9-2

BH10-2




Sampled By:

Sampled By:

Sampled By:

SOIL

SOIL

SOIL

Matrix:

Matrix:

Matrix:

#1

#1

#1

#2

#2

#2

Speciated Metals

Physical Tests



Physical Tests



% Moisture



pH

SARCalcium (Ca)

<0.20

5.68

<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.042<0.030<0.030<0.050<0.050<0.05091.589.3

<0.010<0.010<0.010<0.010<0.02097.9

8.03

0.2113.2

0.20

0.10

0.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0420.0300.0300.0500.0500.050

50-14050-140

0.0100.0100.0100.0100.020

60-140

0.10

0.101.0

ug/g

%



pH units

SARmg/L

20-AUG-15

19-AUG-15



19-AUG-15

20-AUG-1520-AUG-15

8 10

21 290.15 0.170.67 0.740.96 0.960.3 0.30.96 0.969.6 9.60.96 0.969.6 9.60.1 0.19.6 9.662 69

0.76 0.9530 4230 4230 429.6 2812 1696 96

1.1 1.1

12 12

Result






Guideline Limits



18

L1659064-15

L1659064-16

L1659064-17

BH10-2

BH11-1

BH12-1




Sampled By:

Sampled By:

Sampled By:

SOIL

SOIL

SOIL

Matrix:

Matrix:

Matrix:

#1

#1

#1

#2

#2

#2


Physical Tests

Cyanides


Metals

Speciated Metals

Physical Tests

Magnesium (Mg)Sodium (Na)






3.73.4

0.16112.47.34

<0.050

<0.1019.54.01.3

<1.04.955.1

<0.505.50.17

<0.5018.55.49.912.2

0.0393<1.012.1<1.0<0.20<0.50<1.038.857.7

<0.20

1.01.0

0.00400.100.10

0.050

0.101.01.01.0

1.01.01.00.505.00.100.501.01.01.01.0

0.00501.01.01.00.200.501.01.05.0

0.20

mg/Lmg/L

mS/cm%

pH units

ug/g

SARmg/Lmg/Lmg/L


ug/g

20-AUG-1520-AUG-15

20-AUG-1519-AUG-1519-AUG-15

19-AUG-15

20-AUG-1520-AUG-1520-AUG-1520-AUG-15


20-AUG-15

1.4 1.4

0.051 0.051

12 12

40 5018 18670 6708 10

120 1202 2

1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340

8 10

Result






Guideline Limits



18

L1659064-17

L1659064-18

BH12-1

BH12-2



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

#1

#1

#2

#2

Physical Tests

Cyanides


Metals

Speciated Metals

Physical Tests







% Moisture

AcenaphtheneAcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyrene

0.12815.57.56

<0.050

<0.1016.05.21.3

<1.02.721.7

<0.50<5.00.13

<0.5011.72.75.85.8

0.0139<1.06.3

<1.0<0.20<0.50<1.022.126.7

0.21

6.83

<0.050<0.050<0.050<0.050<0.050

0.00400.100.10

0.050

0.101.01.01.0

1.01.01.00.505.00.100.501.01.01.01.0

0.00501.01.01.00.200.501.01.05.0

0.20

0.10

0.0500.0500.0500.0500.050

mS/cm%

pH units

ug/g

SARmg/Lmg/Lmg/L


ug/g

%

ug/gug/gug/gug/gug/g

20-AUG-1519-AUG-1519-AUG-15

19-AUG-15

20-AUG-1520-AUG-1520-AUG-1520-AUG-15


20-AUG-15

19-AUG-15

24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15

1.4 1.4

0.051 0.051

12 12

40 5018 18670 6708 10

120 1202 2

1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340

8 10

21 290.15 0.170.67 0.740.96 0.960.3 0.3

Result






Guideline Limits



18

L1659064-18 BH12-2D. FONDEVILLA on 21-JUL-15Sampled By:SOILMatrix: #1 #2


Benzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenzo(ah)anthraceneFluorantheneFluoreneIndeno(1,2,3-cd)pyrene1+2-Methylnaphthalenes1-Methylnaphthalene2-MethylnaphthaleneNaphthalenePhenanthrenePyreneSurrogate: 2-FluorobiphenylSurrogate: p-Terphenyl d14

<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.042<0.030<0.030<0.050<0.050<0.05087.185.7

0.0500.0500.0500.0500.0500.0500.0500.0500.0420.0300.0300.0500.0500.050

50-14050-140

ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g%%

24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15

0.96 0.969.6 9.60.96 0.969.6 9.60.1 0.19.6 9.662 69

0.76 0.9530 4230 4230 429.6 2812 1696 96

Reference Information

G15100 L1659064 CONTD....17Page of

25-AUG-15 14:35 (MT)

B-HWS-R511-WT

CL-R511-WT

CN-WAD-R511-WT

CR-CR6-IC-WT

EC-R511-WT

HG-200.2-CVAA-WT

MET-200.2-CCMS-WT

METHYLNAPS-CALC-WTMOISTURE-WTPAH-511-WT

Boron-HWE-O.Reg 153/04 (July2011)

Chloride-O.Reg 153/04 (July 2011)

Cyanide (WAD)-O.Reg 153/04 (July 2011)

Hexavalent Chromium in Soil

Conductivity-O.Reg 153/04 (July2011)

Mercury in Soil by CVAAS

Metals in Soil by CRC ICPMS

ABN-Calculated Parameters% MoisturePAH-O.Reg 153/04 (July 2011)

A dried solid sample is extracted with calcium chloride, the sample undergoes a heating process. After cooling the sample is filtered and analyzed by ICP/OES.

Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).

5 grams of dried soil is mixed with 10 grams of distilled water for a minimum of 30 minutes. The extract is filtered and analyzed by ion chromatography.


The sample is extracted with a strong base for 16 hours, and then filtered. The filtrate is then distilled where the cyanide is converted to cyanogen chloride by reacting with chloramine-T, the cyanogen chloride then reacts with a combination of barbituric acid and isonicotinic acid to form a highly colored complex.


This analysis is carried out using procedures adapted from "Test Methods for Evaluating Solid Waste" SW-846, Method 7199, published by the United States Environmental Protection Agency (EPA). The procedure involves analysis for chromium (VI) by ion chromatography using diphenylcarbazide in asulphuric acid solution.


A representative subsample is tumbled with de-ionized (DI) water. The ratio of water to soil is 2:1 v/w. After tumbling the sample is then analyzed by a conductivity meter.


Soil samples are digested with nitric and hydrochloric acids, followed by analysis by CVAAS.


Soil samples are digested with nitric and hydrochloric acids, followed by analysis by CRC ICPMS.

Method Limitation: This method is not a total digestion technique. It is a very strong acid digestion that is intended to dissolve those metals that may be environmentally available. This method does not dissolve all silicate materials and may result in a partial extraction. depending on the sample matrix,for some metals, including, but not limited to Al, Ba, Be, Cr, Sr, Ti, Tl, and V.

Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported).

A representative sub-sample of soil is fortified with deuterium-labelled surrogates and a mechanical shaking techniqueis used to extract the sample with a mixture of methanol and toluene. The extracts are concentrated and analyzed by GC/MS. Depending on the analytical GC/MS column used benzo(j)fluoranthene may chromatographically co-elute with benzo(b)fluoranthene or benzo(k)fluoranthene.

Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported).

Methods Listed (if applicable):

ALS Test Code Test Description

Soil

Soil

Soil

Soil

Soil

Soil

Soil

SoilSoilSoil

HW EXTR, EPA 6010B

EPA 300.0

MOE 3015/APHA 4500CN I-WAD

SW846 3060A/7199

MOEE E3138

EPA 200.2/1631E (mod)

EPA 200.2/6020A (mod)

SW846 8270Gravimetric: Oven DriedSW846 3510/8270

Method Reference*** Matrix

18

Reference Information

G15100 L1659064 CONTD....18Page of

25-AUG-15 14:35 (MT)

PCB-511-WT

PH-R511-WT

SAR-R511-WT

SO4-WT

PCB-O.Reg 153/04 (July 2011)

pH-O.Reg 153/04 (July 2011)

SAR-O.Reg 153/04 (July 2011)

Sulphate

An aliquot of a solid sample is extracted with a solvent, extract is cleaned up and analyzed on the GC/MS.


A minimum 10g portion of the sample is extracted with 20mL of 0.01M calcium chloride solution by shaking for at least 30 minutes. The aqueous layer isseparated from the soil and then analyzed using a pH meter and electrode.


A dried, disaggregated solid sample is extracted with deionized water, the aqueous extract is separated from the solid, acidified and then analyzed usinga ICP/OES.


Soil

Soil

Soil

Soil

SW846 3510/8082

MOEE E3137A

SW846 6010C

EPA 300.0

*** ALS test methods may incorporate modifications from specified reference methods to improve performance.

GLOSSARY OF REPORT TERMS

Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there.mg/kg - milligrams per kilogram based on dry weight of samplemg/kg wwt - milligrams per kilogram based on wet weight of samplemg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/L - unit of concentration based on volume, parts per million.< - Less than.D.L. - The reporting limit.N/A - Result not available. Refer to qualifier code and definition for explanation.

Test results reported relate only to the samples as received by the laboratory.UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION.Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.

Application of guidelines is provided "as is" without warranty of any kind, either expressed or implied, including, but not limited to fitness for a particular purpose, or non-infringement. ALS assumes no responsibility for errors or omissions in the information.

The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:

Chain of Custody numbers:

14-461973 14-461974

Laboratory Definition Code Laboratory Location Laboratory Definition Code Laboratory Location

WT ALS ENVIRONMENTAL - WATERLOO, ONTARIO, CANADA

18

Quality Control ReportPage 1 of

Client:

Contact:

CHUNG AND VANDER DOELEN311 VICTORIA ST. N. KITCHENER ON N2H 5E1ERIC CHUNG

Report Date: 25-AUG-15Workorder: L1659064

Test Matrix Reference Result Qualifier Units RPD Limit Analyzed

B-HWS-R511-WT

CL-R511-WT

CN-WAD-R511-WT

CR-CR6-IC-WT

Soil

Soil

Soil

Soil

R3250233

R3253204

R3250333

R3250845

Batch

Batch

Batch

Batch

DUP

IRM

MB

MS

DUP

LCS

MB

MS

DUP

LCS

MB

MS

CRM

DUP

LCS

MB

WG2153319-3

WG2153319-2

WG2153319-1

WG2153319-4

WG2156410-2

WG2156410-3

WG2156410-1

WG2156410-4

WG2152328-3

WG2152328-2

WG2152328-1

WG2152328-4

WG2151850-4

WG2151850-3

WG2151850-2

WG2151850-1

L1658681-3

SALINITY_SOIL4

L1658681-3

L1659064-13

L1659064-13

L1658720-11

L1658720-11

WT-SQC012

L1657369-5

Boron (B), Hot Water Ext.




Chloride

Chloride

Chloride

Chloride








0.74

108.9

<0.10

N/A

12.7

104.3

<5.0

105.2

<0.050

87.7

<0.050

95.8

90.8

<0.20

97.6

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

25-AUG-15

25-AUG-15

25-AUG-15

25-AUG-15

19-AUG-15

19-AUG-15

19-AUG-15

19-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

10

0.5

N/A

N/A

40

30

35

35

70-130

-

70-130

70-130

80-120

70-130

70-130

80-120

ug/g

%

ug/g

%

ug/g

%

ug/g

%

ug/g

%

ug/g

%

%

ug/g

%

MS-B

0.82

12.6

<0.050

<0.20

0.1

5

0.05

RPD-NA

RPD-NA

14


Client:

Contact:




CR-CR6-IC-WT

EC-R511-WT

HG-200.2-CVAA-WT

MET-200.2-CCMS-WT

Soil

Soil

Soil

Soil

R3250845

R3250061

R3250160

R3250163

R3251020

Batch

Batch

Batch

Batch

Batch

MB

DUP

LCS

LCS

MB

CRM

DUP

LCS

MB

CRM

DUP

LCS

MB

CRM

WG2151850-1

WG2153325-4

WG2153494-2

WG2153494-3

WG2153325-1

WG2153332-2

WG2153332-6

WG2153332-4

WG2153332-1

WG2153335-2

WG2153335-6

WG2153335-4

WG2153335-1

WG2153332-2

WG2153325-3

WT-CANMET-TILL1

WG2153332-5

WT-CANMET-TILL1

WG2153335-5

WT-CANMET-TILL1


Conductivity

Conductivity

Conductivity

Conductivity

Mercury (Hg)

Mercury (Hg)

Mercury (Hg)

Mercury (Hg)

Mercury (Hg)

Mercury (Hg)

Mercury (Hg)

Mercury (Hg)

Antimony (Sb)

Arsenic (As)

<0.20

0.125

98.9

101.5

<0.0040

94.8

<0.0050

102.0

<0.0050

95.5

0.0062

100.0

<0.0050

99.1

109.8

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

2.4

N/A

6.0

20

40

40

90-110

90-110

70-130

80-120

70-130

80-120

70-130

70-130

ug/g

mS/cm

%

%

mS/cm

%

ug/g

%

mg/kg

%

ug/g

%

mg/kg

%

%

0.128

<0.0050

0.0059

0.2

0.044

0.005

0.005

RPD-NA

14


Client:

Contact:




MET-200.2-CCMS-WT Soil

R3251020BatchCRM

DUP

WG2153332-2

WG2153332-6

WT-CANMET-TILL1

WG2153332-5

Barium (Ba)

Beryllium (Be)

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

103.9

102.6

97.2

113.5

106.5

101.5

91.9

101.7

107.5

89.3

96.8

103.0

106.9

116.0

105.7

<0.10

1.11

9.57

<0.10

<5.0

0.024

4.44

1.68

1.82

3.58

0.43

2.95

<0.20

<0.10

<0.050

0.240

9.11

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

N/A

8.5

14

N/A

N/A

N/A

2.4

6.4

2.4

0.8

0.24

3.5

N/A

N/A

N/A

6.6

9.0

30

30

40

30

30

30

30

30

30

40

2

30

30

40

30

30

30

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

<1.0

1.0

8.3

<0.50

<5.0

<0.50

4.3

1.6

1.9

3.6

<1.0

2.8

<1.0

<0.20

<0.50

<1.0

8.3

RPD-NA

RPD-NA

RPD-NA

RPD-NA

J

RPD-NA

RPD-NA

RPD-NA

14


Client:

Contact:





R3251020BatchDUP

LCS

MB

WG2153332-6

WG2153332-3

WG2153332-1

WG2153332-5Zinc (Zn)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

10.2

102.1

96.3

96.4

98.5

96.4

91.3

94.1

94.6

92.8

100.9

102.0

94.7

94.6

97.2

94.6

95.0

96.5

99.4

<0.10

<0.10

<0.50

<0.10

<5.0

<0.020

<0.50

<0.10

<0.50

<0.50

<0.10

<0.50

<0.20

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

17 30

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

ug/g

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

8.6

0.1

0.1

0.5

0.1

5

0.02

0.5

0.1

0.5

0.5

0.1

0.5

0.2

14


Client:

Contact:





R3251020

R3251092

Batch

Batch

MB

CRM

DUP

WG2153332-1

WG2153335-2

WG2153335-6

WT-CANMET-TILL1

WG2153335-5

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

<0.10

<0.050

<0.050

<0.20

<2.0

98.6

102.7

99.7

87.2

92.8

103.5

101.0

97.0

92.8

97.5

101.4

89.7

96.1

95.1

111.9

106.3

97.5

<0.10

2.41

12.3

0.13

5.8

0.140

7.25

2.41

9.57

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

N/A

13

4.4

11

11

12

4.4

4.9

8.8

30

30

40

30

30

30

30

30

30

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

<1.0

2.7

12.9

<0.50

6.5

<0.50

7.6

2.5

10.4

0.1

0.05

0.05

0.2

2

RPD-NA

14


Client:

Contact:





R3251092BatchDUP

LCS

MB

WG2153335-6

WG2153335-3

WG2153335-1

WG2153335-5Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)

7.66

0.29

5.06

<0.20

<0.10

<0.050

0.417

14.3

44.5

110.6

104.8

105.3

93.9

92.5

106.2

103.8

105.4

103.5

109.0

107.6

104.6

105.9

103.6

104.4

105.8

106.0

98.4

<0.10

<0.10

<0.50

<0.10

<5.0

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

7.6

13

5.8

N/A

N/A

N/A

9.3

5.5

0.3

40

40

30

30

40

30

30

30

30

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

8.3

<1.0

5.4

<1.0

<0.20

<0.50

<1.0

15.1

44.3

0.1

0.1

0.5

0.1

5

RPD-NA

RPD-NA

RPD-NA

14


Client:

Contact:




MET-200.2-CCMS-WT

MOISTURE-WT

PAH-511-WT

Soil

Soil

Soil

R3251092

R3249043

R3252258

Batch

Batch

Batch

MB

DUP

LCS

MB

DUP

WG2153335-1

WG2152114-3

WG2152114-2

WG2152114-1

WG2151969-5

L1659055-7

WG2151969-4

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

% Moisture

% Moisture

% Moisture

1-Methylnaphthalene

2-Methylnaphthalene

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene

Benzo(b)fluoranthene

Benzo(g,h,i)perylene

Benzo(k)fluoranthene

<0.020

<0.50

<0.10

<0.50

<0.50

<0.10

<0.50

<0.20

<0.10

<0.050

<0.050

<0.20

<2.0

9.07

98.0

<0.10

<0.030

<0.030

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

19-AUG-15

19-AUG-15

19-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

6.3

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

20

40

40

40

40

40

40

40

40

40

40

90-110

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

%

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

9.66

<0.030

<0.030

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

0.02

0.5

0.1

0.5

0.5

0.1

0.5

0.2

0.1

0.05

0.05

0.2

2

0.1

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

14


Client:

Contact:




PAH-511-WT Soil

R3252258BatchDUP

IRM

LCS

WG2151969-5

WG2151969-3

WG2151969-2

WG2151969-4

ALS PAH1 RM

Chrysene

Dibenzo(ah)anthracene

Fluoranthene

Fluorene

Indeno(1,2,3-cd)pyrene

Naphthalene

Phenanthrene

Pyrene

1-Methylnaphthalene

2-Methylnaphthalene

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

1-Methylnaphthalene

2-Methylnaphthalene

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

95.3

101.3

69.9

111.9

67.3

104.4

92.9

110.1

100.4

76.7

119.1

121.4

110.3

71.2

94.3

96.0

103.1

108.2

87.9

89.0

90.9

91.1

91.3

89.0

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

40

40

40

40

40

40

40

40

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

14


Client:

Contact:




PAH-511-WT

PCB-511-WT

Soil

Soil

R3252258BatchLCS

MB

WG2151969-2

WG2151969-1

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

1-Methylnaphthalene

2-Methylnaphthalene

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

Surrogate: 2-Fluorobiphenyl

Surrogate: p-Terphenyl d14

92.4

88.5

77.5

89.2

93.7

80.8

89.7

91.9

79.1

89.7

89.6

95.4

<0.030

<0.030

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

89.5

88.0

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

%

%

%

%

%

%

%

%

%

%

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

0.03

0.03

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

50-140

50-140

14


Client:

Contact:




PCB-511-WT

PH-R511-WT

SAR-R511-WT

Soil

Soil

Soil

R3251604

R3249319

R3250269

Batch

Batch

Batch

DUP

LCS

MB

MS

DUP

LCS

DUP

IRM

WG2151969-5

WG2151969-2

WG2151969-1

WG2151969-6

WG2151989-1

WG2152535-3

WG2153325-4

WG2153325-2

WG2151969-4

WG2151969-4

L1657369-11

WG2153325-3

WT SAR1

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Surrogate: d14-Terphenyl

Aroclor 1242

Aroclor 1254

Aroclor 1260

pH

pH

Calcium (Ca)

Sodium (Na)

Magnesium (Mg)

Calcium (Ca)

Sodium (Na)

Magnesium (Mg)

<0.010

<0.010

<0.010

<0.010

108.6

94.7

100.4

110.0

<0.010

<0.010

<0.010

<0.010

100.5

107.7

101.3

111.5

7.69

7.03

16.0

1.3

5.2

97.9

99.5

96.1

22-AUG-15

22-AUG-15

22-AUG-15

22-AUG-15

22-AUG-15

22-AUG-15

22-AUG-15

22-AUG-15

22-AUG-15

22-AUG-15

22-AUG-15

22-AUG-15

22-AUG-15

22-AUG-15

22-AUG-15

22-AUG-15

19-AUG-15

19-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

20-AUG-15

N/A

N/A

N/A

N/A

0.03

4.4

2.3

4.8

40

40

40

40

0.3

40

40

40

60-140

60-140

60-140

60-140

60-140

60-140

60-140

6.7-7.3

70-130

70-130

70-130

ug/g

ug/g

ug/g

ug/g

%

%

%

%

ug/g

ug/g

ug/g

ug/g

%

%

%

%

pH units

pH units

mg/L

mg/L

mg/L

%

%

%

<0.010

<0.010

<0.010

<0.010

7.66

15.4

1.4

5.0

0.01

0.01

0.01

0.01

60-140

RPD-NA

RPD-NA

RPD-NA

RPD-NA

J

14


Client:

Contact:




SAR-R511-WT

SO4-WT

Soil

Soil

R3250269

R3253204

Batch

Batch

MB

CRM

DUP

LCS

MB

WG2153325-1

WG2155832-5

WG2155832-4

WG2155832-2

WG2155832-1

AN-CRM-WT

L1659064-1

Calcium (Ca)

Sodium (Na)

Magnesium (Mg)

Sulphate

Sulphate

Sulphate

Sulphate

<1.0

<1.0

<1.0

116.2

<20

104.7

<20

20-AUG-15

20-AUG-15

20-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

24-AUG-15

N/A 30

70-130

70-130

mg/L

mg/L

mg/L

%

mg/kg

%

mg/kg

20

1

1

1

20

RPD-NA

14

Quality Control Report

Page 12 of


Sample Parameter Qualifier Definitions:

Description Qualifier

J

MS-B

RPD-NA

Duplicate results and limits are expressed in terms of absolute difference.

Matrix Spike recovery could not be accurately calculated due to high analyte background in sample.

Relative Percent Difference Not Available due to result(s) being less than detection limit.

Limit ALS Control Limit (Data Quality Objectives)DUP DuplicateRPD Relative Percent DifferenceN/A Not AvailableLCS Laboratory Control SampleSRM Standard Reference MaterialMS Matrix SpikeMSD Matrix Spike DuplicateADE Average Desorption EfficiencyMB Method BlankIRM Internal Reference MaterialCRM Certified Reference MaterialCCV Continuing Calibration VerificationCVS Calibration Verification StandardLCSD Laboratory Control Sample Duplicate

Legend:

Client:

Contact:


14


Page 13 of


ALS Product Description Sample

ID Sampling Date Date Processed Rec. HT Actual HT

Physical Tests


Cyanides


123456789

1011121314161718

11013

135789

1011131617

2468

121418

21-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-15

21-JUL-1521-JUL-1521-JUL-15

21-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-15

21-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-15

19-AUG-15 16:1719-AUG-15 16:1819-AUG-15 16:1919-AUG-15 16:2019-AUG-15 16:2119-AUG-15 16:2219-AUG-15 16:2319-AUG-15 16:2419-AUG-15 16:2519-AUG-15 16:2619-AUG-15 16:2719-AUG-15 16:2819-AUG-15 16:2919-AUG-15 16:3019-AUG-15 16:3119-AUG-15 16:3219-AUG-15 16:33

25-AUG-15 01:3425-AUG-15 01:3525-AUG-15 01:36

18-AUG-15 19:4318-AUG-15 19:4418-AUG-15 19:4518-AUG-15 19:4618-AUG-15 19:4718-AUG-15 19:4818-AUG-15 19:4918-AUG-15 19:5018-AUG-15 19:5118-AUG-15 19:5218-AUG-15 19:53

18-AUG-15 16:1818-AUG-15 16:1918-AUG-15 16:2018-AUG-15 16:2118-AUG-15 16:2218-AUG-15 16:2318-AUG-15 16:24

1414141414141414141414141414141414

303030

1414141414141414141414

14141414141414

2929292929292929292929292929292929

353535

2828282828282828282828

28282828282828

% Moisture

Chloride-O.Reg 153/04 (July 2011)

Cyanide (WAD)-O.Reg 153/04 (July 2011)

PAH-O.Reg 153/04 (July 2011)

EHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTR

EHTEHTEHT

EHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTR

EHTREHTREHTREHTREHTREHTREHTR

Qualifier

Legend & Qualifier Definitions:

Hold Time Exceedances:

Units

daysdaysdaysdaysdaysdaysdaysdaysdaysdaysdaysdaysdaysdaysdaysdaysdays

daysdaysdays

daysdaysdaysdaysdaysdaysdaysdaysdaysdaysdays

daysdaysdaysdaysdaysdaysdays

EHTR-FM: EHTR: EHTL: EHT: Rec. HT:

Exceeded ALS recommended hold time prior to sample receipt. Field Measurement recommended.Exceeded ALS recommended hold time prior to sample receipt.Exceeded ALS recommended hold time prior to analysis. Sample was received less than 24 hours prior to expiry.Exceeded ALS recommended hold time prior to analysis.ALS recommended hold time (see units).

Client:

Contact:


14


Page 14 of


The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against pre-determined data quality objectives to provide confidence in the accuracy of associated test results.

Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order.

Notes*:Where actual sampling date is not provided to ALS, the date (& time) of receipt is used for calculation purposes.Where actual sampling time is not provided to ALS, the earlier of 12 noon on the sampling date or the time (& date) of receipt isused for calculation purposes. Samples for L1659064 were received on 18-AUG-15 12:00.

ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal governmentrequirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by theUS EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS.

Client:

Contact:


14

Date post:	22-Sep-2020
Category:	Documents
Upload:	others
View:	2 times
Download:	0 times

Appendix D - Geotechnical Report€¦ · ATTN: ERIC CHUNG FINAL Report Date: 25-AUG-15 14:35 (MT)...

Documents