Appendix D - Geotechnical Report
[This report shall not be reproduced except in full without the written authority of the Laboratory.]
18-AUG-15
Lab Work Order #: L1659064
Date Received:CHUNG AND VANDER DOELEN
311 VICTORIA ST. N.KITCHENER ON N2H 5E1
ATTN: ERIC CHUNGFINAL 25-AUG-15 14:35 (MT)Report Date:
Version:
Certificate of Analysis
ALS CANADA LTD Part of the ALS Group A Campbell Brothers Limited Company
____________________________________________
Mary-Lynn PiresAccount Manager
ADDRESS: 60 Northland Road, Unit 1, Waterloo, ON N2V 2B8 Canada | Phone: +1 519 886 6910 | Fax: +1 519 886 9047
Client Phone: 519-742-8979
G15100Job Reference: G15100Project P.O. #:
14-461973, 14-461974C of C Numbers:Legal Site Desc:
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....2Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-1
L1659064-2
BH1-1
BH1-2
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
Sampled By:
Sampled By:
SOIL
SOIL
Matrix:
Matrix:
#1
#1
#2
#2
Physical Tests
Leachable Anions & Nutrients
Anions and Nutrients
Cyanides
Saturated Paste Extractables
Metals
Speciated Metals
Physical Tests
Polycyclic Aromatic Hydrocarbons
Conductivity% MoisturepH
Chloride
Sulphate
Cyanide, Weak Acid Diss
SARCalcium (Ca)Magnesium (Mg)Sodium (Na)
Antimony (Sb)Arsenic (As)Barium (Ba)Beryllium (Be)Boron (B)Boron (B), Hot Water Ext.Cadmium (Cd)Chromium (Cr)Cobalt (Co)Copper (Cu)Lead (Pb)Mercury (Hg)Molybdenum (Mo)Nickel (Ni)Selenium (Se)Silver (Ag)Thallium (Tl)Uranium (U)Vanadium (V)Zinc (Zn)
Chromium, Hexavalent
% Moisture
Acenaphthene
0.1573.558.03
24.4
20
<0.050
0.5412.12.27.8
<1.01.88.2
<0.50<5.0<0.10<0.5010.02.36.05.6
0.0061<1.04.3
<1.0<0.20<0.50<1.028.721.7
0.23
9.66
<0.050
0.00400.100.10
5.0
20
0.050
0.101.01.01.0
1.01.01.00.505.00.100.501.01.01.01.0
0.00501.01.01.00.200.501.01.05.0
0.20
0.10
0.050
mS/cm%
pH units
ug/g
mg/kg
ug/g
SARmg/Lmg/Lmg/L
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g
ug/g
%
ug/g
20-AUG-1519-AUG-1519-AUG-15
25-AUG-15
24-AUG-15
19-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-15
19-AUG-15
24-AUG-15
1.4 1.4
0.051 0.051
12 12
40 5018 18670 6708 10
120 1202 2
1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340
8 10
21 29
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....3Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-2
L1659064-3
BH1-2
BH2-1
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
Sampled By:
Sampled By:
SOIL
SOIL
Matrix:
Matrix:
#1
#1
#2
#2
Polycyclic Aromatic Hydrocarbons
Polychlorinated Biphenyls
Physical Tests
Cyanides
Saturated Paste Extractables
Metals
AcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenzo(ah)anthraceneFluorantheneFluoreneIndeno(1,2,3-cd)pyrene1+2-Methylnaphthalenes1-Methylnaphthalene2-MethylnaphthaleneNaphthalenePhenanthrenePyreneSurrogate: 2-FluorobiphenylSurrogate: p-Terphenyl d14
Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260Total PCBsSurrogate: d14-Terphenyl
Conductivity% MoisturepH
Cyanide, Weak Acid Diss
SARCalcium (Ca)Magnesium (Mg)Sodium (Na)
Antimony (Sb)Arsenic (As)Barium (Ba)
<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.042<0.030<0.030<0.050<0.050<0.05091.691.1
<0.010<0.010<0.010<0.010<0.02096.2
0.1534.818.07
<0.050
0.2510.76.14.1
<1.02.712.9
0.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0420.0300.0300.0500.0500.050
50-14050-140
0.0100.0100.0100.0100.020
60-140
0.00400.100.10
0.050
0.101.01.01.0
1.01.01.0
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g%%
ug/gug/gug/gug/gug/g%
mS/cm%
pH units
ug/g
SARmg/Lmg/Lmg/L
ug/gug/gug/g
24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15
22-AUG-1522-AUG-1522-AUG-1522-AUG-1522-AUG-1522-AUG-15
20-AUG-1519-AUG-1519-AUG-15
19-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-1520-AUG-1520-AUG-15
0.15 0.170.67 0.740.96 0.960.3 0.30.96 0.969.6 9.60.96 0.969.6 9.60.1 0.19.6 9.662 69
0.76 0.9530 4230 4230 429.6 2812 1696 96
1.1 1.1
1.4 1.4
0.051 0.051
12 12
40 5018 18670 670
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....4Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-3
L1659064-4
BH2-1
BH2-2
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
Sampled By:
Sampled By:
SOIL
SOIL
Matrix:
Matrix:
#1
#1
#2
#2
Metals
Speciated Metals
Physical Tests
Polycyclic Aromatic Hydrocarbons
Beryllium (Be)Boron (B)Boron (B), Hot Water Ext.Cadmium (Cd)Chromium (Cr)Cobalt (Co)Copper (Cu)Lead (Pb)Mercury (Hg)Molybdenum (Mo)Nickel (Ni)Selenium (Se)Silver (Ag)Thallium (Tl)Uranium (U)Vanadium (V)Zinc (Zn)
Chromium, Hexavalent
% Moisture
AcenaphtheneAcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenzo(ah)anthraceneFluorantheneFluoreneIndeno(1,2,3-cd)pyrene1+2-Methylnaphthalenes1-Methylnaphthalene2-MethylnaphthaleneNaphthalenePhenanthrenePyrene
<0.506.5
<0.10<0.507.62.510.48.3
0.0059<1.05.4
<1.0<0.20<0.50<1.015.144.3
<0.20
6.73
<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.042<0.030<0.030<0.050<0.050<0.050
0.505.00.100.501.01.01.01.0
0.00501.01.01.00.200.501.01.05.0
0.20
0.10
0.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0420.0300.0300.0500.0500.050
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g
ug/g
%
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g
20-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-15
19-AUG-15
24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15
8 10120 1202 2
1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340
8 10
21 290.15 0.170.67 0.740.96 0.960.3 0.30.96 0.969.6 9.60.96 0.969.6 9.60.1 0.19.6 9.662 69
0.76 0.9530 4230 4230 429.6 2812 1696 96
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....5Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-4
L1659064-5
BH2-2
BH3-1
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
Sampled By:
Sampled By:
SOIL
SOIL
Matrix:
Matrix:
#1
#1
#2
#2
Polycyclic Aromatic Hydrocarbons
Polychlorinated Biphenyls
Physical Tests
Cyanides
Saturated Paste Extractables
Metals
Speciated Metals
Surrogate: 2-FluorobiphenylSurrogate: p-Terphenyl d14
Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260Total PCBsSurrogate: d14-Terphenyl
Conductivity% MoisturepH
Cyanide, Weak Acid Diss
SARCalcium (Ca)Magnesium (Mg)Sodium (Na)
Antimony (Sb)Arsenic (As)Barium (Ba)Beryllium (Be)Boron (B)Boron (B), Hot Water Ext.Cadmium (Cd)Chromium (Cr)Cobalt (Co)Copper (Cu)Lead (Pb)Mercury (Hg)Molybdenum (Mo)Nickel (Ni)Selenium (Se)Silver (Ag)Thallium (Tl)Uranium (U)Vanadium (V)Zinc (Zn)
89.889.1
<0.010<0.010<0.010<0.010<0.02096.0
0.1418.108.16
<0.050
0.327.75.94.8
<1.01.914.7
<0.505.4
<0.10<0.506.92.16.410.4
0.0051<1.04.1
<1.0<0.20<0.50<1.014.339.7
50-14050-140
0.0100.0100.0100.0100.020
60-140
0.00400.100.10
0.050
0.101.01.01.0
1.01.01.00.505.00.100.501.01.01.01.0
0.00501.01.01.00.200.501.01.05.0
%%
ug/gug/gug/gug/gug/g%
mS/cm%
pH units
ug/g
SARmg/Lmg/Lmg/L
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g
24-AUG-1524-AUG-15
22-AUG-1522-AUG-1522-AUG-1522-AUG-1522-AUG-1522-AUG-15
20-AUG-1519-AUG-1519-AUG-15
19-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-15
1.1 1.1
1.4 1.4
0.051 0.051
12 12
40 5018 18670 6708 10
120 1202 2
1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....6Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-5
L1659064-6
L1659064-7
BH3-1
BH3-2
BH4-2
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
Sampled By:
Sampled By:
Sampled By:
SOIL
SOIL
SOIL
Matrix:
Matrix:
Matrix:
#1
#1
#1
#2
#2
#2
Speciated Metals
Physical Tests
Polycyclic Aromatic Hydrocarbons
Polychlorinated Biphenyls
Physical Tests
Cyanides
Chromium, Hexavalent
% Moisture
AcenaphtheneAcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenzo(ah)anthraceneFluorantheneFluoreneIndeno(1,2,3-cd)pyrene1+2-Methylnaphthalenes1-Methylnaphthalene2-MethylnaphthaleneNaphthalenePhenanthrenePyreneSurrogate: 2-FluorobiphenylSurrogate: p-Terphenyl d14
Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260Total PCBsSurrogate: d14-Terphenyl
Conductivity% MoisturepH
<0.20
3.15
<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.042<0.030<0.030<0.050<0.050<0.05091.590.7
<0.010<0.010<0.010<0.010<0.02099.4
0.3700.298.14
0.20
0.10
0.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0420.0300.0300.0500.0500.050
50-14050-140
0.0100.0100.0100.0100.020
60-140
0.00400.100.10
ug/g
%
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g%%
ug/gug/gug/gug/gug/g%
mS/cm%
pH units
20-AUG-15
19-AUG-15
24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15
22-AUG-1522-AUG-1522-AUG-1522-AUG-1522-AUG-1522-AUG-15
20-AUG-1519-AUG-1519-AUG-15
8 10
21 290.15 0.170.67 0.740.96 0.960.3 0.30.96 0.969.6 9.60.96 0.969.6 9.60.1 0.19.6 9.662 69
0.76 0.9530 4230 4230 429.6 2812 1696 96
1.1 1.1
1.4 1.4
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....7Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-7
L1659064-8
BH4-2
BH5-1
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
Sampled By:
Sampled By:
SOIL
SOIL
Matrix:
Matrix:
#1
#1
#2
#2
Cyanides
Saturated Paste Extractables
Metals
Speciated Metals
Physical Tests
Cyanides
Saturated Paste Extractables
Metals
Cyanide, Weak Acid Diss
SARCalcium (Ca)Magnesium (Mg)Sodium (Na)
Antimony (Sb)Arsenic (As)Barium (Ba)Beryllium (Be)Boron (B)Boron (B), Hot Water Ext.Cadmium (Cd)Chromium (Cr)Cobalt (Co)Copper (Cu)Lead (Pb)Mercury (Hg)Molybdenum (Mo)Nickel (Ni)Selenium (Se)Silver (Ag)Thallium (Tl)Uranium (U)Vanadium (V)Zinc (Zn)
Chromium, Hexavalent
Conductivity% MoisturepH
Cyanide, Weak Acid Diss
SARCalcium (Ca)Magnesium (Mg)Sodium (Na)
<0.050
4.4721.61.479.4
<1.02.318.4
<0.50<5.0<0.10<0.509.12.76.45.8
0.0142<1.06.0
<1.0<0.20<0.50<1.017.829.7
0.28
0.2671.008.23
<0.050
1.6448.25.945.2
0.050
0.101.01.01.0
1.01.01.00.505.00.100.501.01.01.01.0
0.00501.01.01.00.200.501.01.05.0
0.20
0.00400.100.10
0.050
0.101.01.01.0
ug/g
SARmg/Lmg/Lmg/L
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g
ug/g
mS/cm%
pH units
ug/g
SARmg/Lmg/Lmg/L
19-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-15
20-AUG-1519-AUG-1519-AUG-15
19-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-15
0.051 0.051
12 12
40 5018 18670 6708 10
120 1202 2
1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340
8 10
1.4 1.4
0.051 0.051
12 12
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....8Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-8 BH5-1D. FONDEVILLA on 21-JUL-15Sampled By:SOILMatrix: #1 #2
Metals
Speciated Metals
Polycyclic Aromatic Hydrocarbons
Antimony (Sb)Arsenic (As)Barium (Ba)Beryllium (Be)Boron (B)Boron (B), Hot Water Ext.Cadmium (Cd)Chromium (Cr)Cobalt (Co)Copper (Cu)Lead (Pb)Mercury (Hg)Molybdenum (Mo)Nickel (Ni)Selenium (Se)Silver (Ag)Thallium (Tl)Uranium (U)Vanadium (V)Zinc (Zn)
Chromium, Hexavalent
AcenaphtheneAcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenzo(ah)anthraceneFluorantheneFluoreneIndeno(1,2,3-cd)pyrene1+2-Methylnaphthalenes1-Methylnaphthalene2-MethylnaphthaleneNaphthalenePhenanthrenePyreneSurrogate: 2-FluorobiphenylSurrogate: p-Terphenyl d14
<1.02.917.2
<0.507.90.13
<0.508.62.57.710.2
0.0123<1.05.7
<1.0<0.20<0.50<1.015.544.2
0.21
<0.050<0.050<0.050<0.050<0.0500.051
<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.042<0.030<0.030<0.050<0.050<0.05090.590.2
1.01.01.00.505.00.100.501.01.01.01.0
0.00501.01.01.00.200.501.01.05.0
0.20
0.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0420.0300.0300.0500.0500.050
50-14050-140
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g
ug/g
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g%%
20-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-15
24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15
40 5018 18670 6708 10
120 1202 2
1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340
8 10
21 290.15 0.170.67 0.740.96 0.960.3 0.30.96 0.969.6 9.60.96 0.969.6 9.60.1 0.19.6 9.662 69
0.76 0.9530 4230 4230 429.6 2812 1696 96
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....9Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-9
L1659064-10
BH6-2
BH7-2
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
Sampled By:
Sampled By:
SOIL
SOIL
Matrix:
Matrix:
#1
#1
#2
#2
Physical Tests
Cyanides
Saturated Paste Extractables
Metals
Speciated Metals
Physical Tests
Leachable Anions & Nutrients
Anions and Nutrients
Conductivity% MoisturepH
Cyanide, Weak Acid Diss
SARCalcium (Ca)Magnesium (Mg)Sodium (Na)
Antimony (Sb)Arsenic (As)Barium (Ba)Beryllium (Be)Boron (B)Boron (B), Hot Water Ext.Cadmium (Cd)Chromium (Cr)Cobalt (Co)Copper (Cu)Lead (Pb)Mercury (Hg)Molybdenum (Mo)Nickel (Ni)Selenium (Se)Silver (Ag)Thallium (Tl)Uranium (U)Vanadium (V)Zinc (Zn)
Chromium, Hexavalent
Conductivity% MoisturepH
Chloride
Sulphate
0.1247.177.96
<0.050
0.7822.42.814.8
<1.01.810.9
<0.505.2
<0.10<0.507.42.16.26.6
<0.0050<1.04.1
<1.0<0.20<0.50<1.015.238.9
0.21
0.23314.07.57
48.3
<20
0.00400.100.10
0.050
0.101.01.01.0
1.01.01.00.505.00.100.501.01.01.01.0
0.00501.01.01.00.200.501.01.05.0
0.20
0.00400.100.10
5.0
20
mS/cm%
pH units
ug/g
SARmg/Lmg/Lmg/L
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g
ug/g
mS/cm%
pH units
ug/g
mg/kg
20-AUG-1519-AUG-1519-AUG-15
19-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-15
20-AUG-1519-AUG-1519-AUG-15
25-AUG-15
24-AUG-15
1.4 1.4
0.051 0.051
12 12
40 5018 18670 6708 10
120 1202 2
1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340
8 10
1.4 1.4
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....10Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-10
L1659064-11
BH7-2
BH8-1
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
Sampled By:
Sampled By:
SOIL
SOIL
Matrix:
Matrix:
#1
#1
#2
#2
Cyanides
Saturated Paste Extractables
Metals
Speciated Metals
Physical Tests
Cyanides
Saturated Paste Extractables
Metals
Cyanide, Weak Acid Diss
SARCalcium (Ca)Magnesium (Mg)Sodium (Na)
Antimony (Sb)Arsenic (As)Barium (Ba)Beryllium (Be)Boron (B)Boron (B), Hot Water Ext.Cadmium (Cd)Chromium (Cr)Cobalt (Co)Copper (Cu)Lead (Pb)Mercury (Hg)Molybdenum (Mo)Nickel (Ni)Selenium (Se)Silver (Ag)Thallium (Tl)Uranium (U)Vanadium (V)Zinc (Zn)
Chromium, Hexavalent
Conductivity% MoisturepH
Cyanide, Weak Acid Diss
SARCalcium (Ca)Magnesium (Mg)Sodium (Na)
<0.050
2.0519.42.135.5
<1.03.023.5
<0.505.70.42
<0.5010.63.08.318.1
0.0231<1.05.8
<1.0<0.20<0.50<1.022.340.6
<0.20
0.1753.858.11
<0.050
0.6510.73.99.8
0.050
0.101.01.01.0
1.01.01.00.505.00.100.501.01.01.01.0
0.00501.01.01.00.200.501.01.05.0
0.20
0.00400.100.10
0.050
0.101.01.01.0
ug/g
SARmg/Lmg/Lmg/L
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g
ug/g
mS/cm%
pH units
ug/g
SARmg/Lmg/Lmg/L
19-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-15
20-AUG-1519-AUG-1519-AUG-15
19-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-15
0.051 0.051
12 12
40 5018 18670 6708 10
120 1202 2
1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340
8 10
1.4 1.4
0.051 0.051
12 12
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....11Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-11
L1659064-12
BH8-1
BH8-2
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
Sampled By:
Sampled By:
SOIL
SOIL
Matrix:
Matrix:
#1
#1
#2
#2
Metals
Speciated Metals
Physical Tests
Polycyclic Aromatic Hydrocarbons
Antimony (Sb)Arsenic (As)Barium (Ba)Beryllium (Be)Boron (B)Boron (B), Hot Water Ext.Cadmium (Cd)Chromium (Cr)Cobalt (Co)Copper (Cu)Lead (Pb)Mercury (Hg)Molybdenum (Mo)Nickel (Ni)Selenium (Se)Silver (Ag)Thallium (Tl)Uranium (U)Vanadium (V)Zinc (Zn)
Chromium, Hexavalent
% Moisture
AcenaphtheneAcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenzo(ah)anthraceneFluorantheneFluoreneIndeno(1,2,3-cd)pyrene1+2-Methylnaphthalenes1-Methylnaphthalene2-Methylnaphthalene
<1.03.015.2
<0.507.1
<0.10<0.508.22.810.513.7
0.0100<1.05.8
<1.0<0.20<0.50<1.015.157.3
<0.20
12.3
<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.042<0.030<0.030
1.01.01.00.505.00.100.501.01.01.01.0
0.00501.01.01.00.200.501.01.05.0
0.20
0.10
0.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0420.0300.030
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g
ug/g
%
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g
20-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-15
19-AUG-15
24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15
40 5018 18670 6708 10
120 1202 2
1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340
8 10
21 290.15 0.170.67 0.740.96 0.960.3 0.30.96 0.969.6 9.60.96 0.969.6 9.60.1 0.19.6 9.662 69
0.76 0.9530 4230 4230 42
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....12Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-12
L1659064-13
BH8-2
BH9-1
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
Sampled By:
Sampled By:
SOIL
SOIL
Matrix:
Matrix:
#1
#1
#2
#2
Polycyclic Aromatic Hydrocarbons
Physical Tests
Leachable Anions & Nutrients
Anions and Nutrients
Cyanides
Saturated Paste Extractables
Metals
NaphthalenePhenanthrenePyreneSurrogate: 2-FluorobiphenylSurrogate: p-Terphenyl d14
Conductivity% MoisturepH
Chloride
Sulphate
Cyanide, Weak Acid Diss
SARCalcium (Ca)Magnesium (Mg)Sodium (Na)
Antimony (Sb)Arsenic (As)Barium (Ba)Beryllium (Be)Boron (B)Boron (B), Hot Water Ext.Cadmium (Cd)Chromium (Cr)Cobalt (Co)Copper (Cu)Lead (Pb)Mercury (Hg)Molybdenum (Mo)Nickel (Ni)Selenium (Se)Silver (Ag)Thallium (Tl)Uranium (U)Vanadium (V)Zinc (Zn)
<0.050<0.050<0.05091.590.3
0.21710.77.72
12.6
<20
<0.050
<0.1025.74.52.1
<1.03.842.2
<0.50<5.00.23
<0.5013.54.38.512.6
0.0276<1.08.8
<1.0<0.20<0.50<1.026.549.5
0.0500.0500.050
50-14050-140
0.00400.100.10
5.0
20
0.050
0.101.01.01.0
1.01.01.00.505.00.100.501.01.01.01.0
0.00501.01.01.00.200.501.01.05.0
ug/gug/gug/g%%
mS/cm%
pH units
ug/g
mg/kg
ug/g
SARmg/Lmg/Lmg/L
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g
24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15
20-AUG-1519-AUG-1519-AUG-15
25-AUG-15
24-AUG-15
19-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-15
9.6 2812 1696 96
1.4 1.4
0.051 0.051
12 12
40 5018 18670 6708 10
120 1202 2
1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....13Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-13
L1659064-14
L1659064-15
BH9-1
BH9-2
BH10-2
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
Sampled By:
Sampled By:
Sampled By:
SOIL
SOIL
SOIL
Matrix:
Matrix:
Matrix:
#1
#1
#1
#2
#2
#2
Speciated Metals
Physical Tests
Polycyclic Aromatic Hydrocarbons
Polychlorinated Biphenyls
Physical Tests
Saturated Paste Extractables
Chromium, Hexavalent
% Moisture
AcenaphtheneAcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenzo(ah)anthraceneFluorantheneFluoreneIndeno(1,2,3-cd)pyrene1+2-Methylnaphthalenes1-Methylnaphthalene2-MethylnaphthaleneNaphthalenePhenanthrenePyreneSurrogate: 2-FluorobiphenylSurrogate: p-Terphenyl d14
Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260Total PCBsSurrogate: d14-Terphenyl
pH
SARCalcium (Ca)
<0.20
5.68
<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.042<0.030<0.030<0.050<0.050<0.05091.589.3
<0.010<0.010<0.010<0.010<0.02097.9
8.03
0.2113.2
0.20
0.10
0.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0500.0420.0300.0300.0500.0500.050
50-14050-140
0.0100.0100.0100.0100.020
60-140
0.10
0.101.0
ug/g
%
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g%%
ug/gug/gug/gug/gug/g%
pH units
SARmg/L
20-AUG-15
19-AUG-15
24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15
22-AUG-1522-AUG-1522-AUG-1522-AUG-1522-AUG-1522-AUG-15
19-AUG-15
20-AUG-1520-AUG-15
8 10
21 290.15 0.170.67 0.740.96 0.960.3 0.30.96 0.969.6 9.60.96 0.969.6 9.60.1 0.19.6 9.662 69
0.76 0.9530 4230 4230 429.6 2812 1696 96
1.1 1.1
12 12
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....14Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-15
L1659064-16
L1659064-17
BH10-2
BH11-1
BH12-1
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
Sampled By:
Sampled By:
Sampled By:
SOIL
SOIL
SOIL
Matrix:
Matrix:
Matrix:
#1
#1
#1
#2
#2
#2
Saturated Paste Extractables
Physical Tests
Cyanides
Saturated Paste Extractables
Metals
Speciated Metals
Physical Tests
Magnesium (Mg)Sodium (Na)
Conductivity% MoisturepH
Cyanide, Weak Acid Diss
SARCalcium (Ca)Magnesium (Mg)Sodium (Na)
Antimony (Sb)Arsenic (As)Barium (Ba)Beryllium (Be)Boron (B)Boron (B), Hot Water Ext.Cadmium (Cd)Chromium (Cr)Cobalt (Co)Copper (Cu)Lead (Pb)Mercury (Hg)Molybdenum (Mo)Nickel (Ni)Selenium (Se)Silver (Ag)Thallium (Tl)Uranium (U)Vanadium (V)Zinc (Zn)
Chromium, Hexavalent
3.73.4
0.16112.47.34
<0.050
<0.1019.54.01.3
<1.04.955.1
<0.505.50.17
<0.5018.55.49.912.2
0.0393<1.012.1<1.0<0.20<0.50<1.038.857.7
<0.20
1.01.0
0.00400.100.10
0.050
0.101.01.01.0
1.01.01.00.505.00.100.501.01.01.01.0
0.00501.01.01.00.200.501.01.05.0
0.20
mg/Lmg/L
mS/cm%
pH units
ug/g
SARmg/Lmg/Lmg/L
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g
ug/g
20-AUG-1520-AUG-15
20-AUG-1519-AUG-1519-AUG-15
19-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-15
1.4 1.4
0.051 0.051
12 12
40 5018 18670 6708 10
120 1202 2
1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340
8 10
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....15Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-17
L1659064-18
BH12-1
BH12-2
D. FONDEVILLA on 21-JUL-15
D. FONDEVILLA on 21-JUL-15
Sampled By:
Sampled By:
SOIL
SOIL
Matrix:
Matrix:
#1
#1
#2
#2
Physical Tests
Cyanides
Saturated Paste Extractables
Metals
Speciated Metals
Physical Tests
Polycyclic Aromatic Hydrocarbons
Conductivity% MoisturepH
Cyanide, Weak Acid Diss
SARCalcium (Ca)Magnesium (Mg)Sodium (Na)
Antimony (Sb)Arsenic (As)Barium (Ba)Beryllium (Be)Boron (B)Boron (B), Hot Water Ext.Cadmium (Cd)Chromium (Cr)Cobalt (Co)Copper (Cu)Lead (Pb)Mercury (Hg)Molybdenum (Mo)Nickel (Ni)Selenium (Se)Silver (Ag)Thallium (Tl)Uranium (U)Vanadium (V)Zinc (Zn)
Chromium, Hexavalent
% Moisture
AcenaphtheneAcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyrene
0.12815.57.56
<0.050
<0.1016.05.21.3
<1.02.721.7
<0.50<5.00.13
<0.5011.72.75.85.8
0.0139<1.06.3
<1.0<0.20<0.50<1.022.126.7
0.21
6.83
<0.050<0.050<0.050<0.050<0.050
0.00400.100.10
0.050
0.101.01.01.0
1.01.01.00.505.00.100.501.01.01.01.0
0.00501.01.01.00.200.501.01.05.0
0.20
0.10
0.0500.0500.0500.0500.050
mS/cm%
pH units
ug/g
SARmg/Lmg/Lmg/L
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g
ug/g
%
ug/gug/gug/gug/gug/g
20-AUG-1519-AUG-1519-AUG-15
19-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-1520-AUG-15
20-AUG-15
19-AUG-15
24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15
1.4 1.4
0.051 0.051
12 12
40 5018 18670 6708 10
120 1202 2
1.9 1.9160 16080 100230 300120 1203.9 2040 40270 3405.5 5.540 503.3 3.333 3386 86340 340
8 10
21 290.15 0.170.67 0.740.96 0.960.3 0.3
Result
25-AUG-15 14:35 (MT)Sample DetailsGrouping Analyte D.L. UnitsQualifier Analyzed
Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - T2-ICC-Soil (Coarse/Fine)
L1659064 CONTD....16Page of
G15100ANALYTICAL GUIDELINE REPORT
Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied:
Guideline Limits
#1: T2-Soil-Ind/Com/Commu Property Use (Coarse) #2: T2-Soil-Ind/Com/Commu Property Use (Fine)
* ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.
18
L1659064-18 BH12-2D. FONDEVILLA on 21-JUL-15Sampled By:SOILMatrix: #1 #2
Polycyclic Aromatic Hydrocarbons
Benzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenzo(ah)anthraceneFluorantheneFluoreneIndeno(1,2,3-cd)pyrene1+2-Methylnaphthalenes1-Methylnaphthalene2-MethylnaphthaleneNaphthalenePhenanthrenePyreneSurrogate: 2-FluorobiphenylSurrogate: p-Terphenyl d14
<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.050<0.042<0.030<0.030<0.050<0.050<0.05087.185.7
0.0500.0500.0500.0500.0500.0500.0500.0500.0420.0300.0300.0500.0500.050
50-14050-140
ug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/gug/g%%
24-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-1524-AUG-15
0.96 0.969.6 9.60.96 0.969.6 9.60.1 0.19.6 9.662 69
0.76 0.9530 4230 4230 429.6 2812 1696 96
Reference Information
G15100 L1659064 CONTD....17Page of
25-AUG-15 14:35 (MT)
B-HWS-R511-WT
CL-R511-WT
CN-WAD-R511-WT
CR-CR6-IC-WT
EC-R511-WT
HG-200.2-CVAA-WT
MET-200.2-CCMS-WT
METHYLNAPS-CALC-WTMOISTURE-WTPAH-511-WT
Boron-HWE-O.Reg 153/04 (July2011)
Chloride-O.Reg 153/04 (July 2011)
Cyanide (WAD)-O.Reg 153/04 (July 2011)
Hexavalent Chromium in Soil
Conductivity-O.Reg 153/04 (July2011)
Mercury in Soil by CVAAS
Metals in Soil by CRC ICPMS
ABN-Calculated Parameters% MoisturePAH-O.Reg 153/04 (July 2011)
A dried solid sample is extracted with calcium chloride, the sample undergoes a heating process. After cooling the sample is filtered and analyzed by ICP/OES.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
5 grams of dried soil is mixed with 10 grams of distilled water for a minimum of 30 minutes. The extract is filtered and analyzed by ion chromatography.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
The sample is extracted with a strong base for 16 hours, and then filtered. The filtrate is then distilled where the cyanide is converted to cyanogen chloride by reacting with chloramine-T, the cyanogen chloride then reacts with a combination of barbituric acid and isonicotinic acid to form a highly colored complex.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
This analysis is carried out using procedures adapted from "Test Methods for Evaluating Solid Waste" SW-846, Method 7199, published by the United States Environmental Protection Agency (EPA). The procedure involves analysis for chromium (VI) by ion chromatography using diphenylcarbazide in asulphuric acid solution.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
A representative subsample is tumbled with de-ionized (DI) water. The ratio of water to soil is 2:1 v/w. After tumbling the sample is then analyzed by a conductivity meter.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
Soil samples are digested with nitric and hydrochloric acids, followed by analysis by CVAAS.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
Soil samples are digested with nitric and hydrochloric acids, followed by analysis by CRC ICPMS.
Method Limitation: This method is not a total digestion technique. It is a very strong acid digestion that is intended to dissolve those metals that may be environmentally available. This method does not dissolve all silicate materials and may result in a partial extraction. depending on the sample matrix,for some metals, including, but not limited to Al, Ba, Be, Cr, Sr, Ti, Tl, and V.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported).
A representative sub-sample of soil is fortified with deuterium-labelled surrogates and a mechanical shaking techniqueis used to extract the sample with a mixture of methanol and toluene. The extracts are concentrated and analyzed by GC/MS. Depending on the analytical GC/MS column used benzo(j)fluoranthene may chromatographically co-elute with benzo(b)fluoranthene or benzo(k)fluoranthene.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported).
Methods Listed (if applicable):
ALS Test Code Test Description
Soil
Soil
Soil
Soil
Soil
Soil
Soil
SoilSoilSoil
HW EXTR, EPA 6010B
EPA 300.0
MOE 3015/APHA 4500CN I-WAD
SW846 3060A/7199
MOEE E3138
EPA 200.2/1631E (mod)
EPA 200.2/6020A (mod)
SW846 8270Gravimetric: Oven DriedSW846 3510/8270
Method Reference*** Matrix
18
Reference Information
G15100 L1659064 CONTD....18Page of
25-AUG-15 14:35 (MT)
PCB-511-WT
PH-R511-WT
SAR-R511-WT
SO4-WT
PCB-O.Reg 153/04 (July 2011)
pH-O.Reg 153/04 (July 2011)
SAR-O.Reg 153/04 (July 2011)
Sulphate
An aliquot of a solid sample is extracted with a solvent, extract is cleaned up and analyzed on the GC/MS.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
A minimum 10g portion of the sample is extracted with 20mL of 0.01M calcium chloride solution by shaking for at least 30 minutes. The aqueous layer isseparated from the soil and then analyzed using a pH meter and electrode.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
A dried, disaggregated solid sample is extracted with deionized water, the aqueous extract is separated from the solid, acidified and then analyzed usinga ICP/OES.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
Soil
Soil
Soil
Soil
SW846 3510/8082
MOEE E3137A
SW846 6010C
EPA 300.0
*** ALS test methods may incorporate modifications from specified reference methods to improve performance.
GLOSSARY OF REPORT TERMS
Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there.mg/kg - milligrams per kilogram based on dry weight of samplemg/kg wwt - milligrams per kilogram based on wet weight of samplemg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/L - unit of concentration based on volume, parts per million.< - Less than.D.L. - The reporting limit.N/A - Result not available. Refer to qualifier code and definition for explanation.
Test results reported relate only to the samples as received by the laboratory.UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION.Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.
Application of guidelines is provided "as is" without warranty of any kind, either expressed or implied, including, but not limited to fitness for a particular purpose, or non-infringement. ALS assumes no responsibility for errors or omissions in the information.
The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:
Chain of Custody numbers:
14-461973 14-461974
Laboratory Definition Code Laboratory Location Laboratory Definition Code Laboratory Location
WT ALS ENVIRONMENTAL - WATERLOO, ONTARIO, CANADA
18
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Client:
Contact:
CHUNG AND VANDER DOELEN311 VICTORIA ST. N. KITCHENER ON N2H 5E1ERIC CHUNG
Report Date: 25-AUG-15Workorder: L1659064
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
B-HWS-R511-WT
CL-R511-WT
CN-WAD-R511-WT
CR-CR6-IC-WT
Soil
Soil
Soil
Soil
R3250233
R3253204
R3250333
R3250845
Batch
Batch
Batch
Batch
DUP
IRM
MB
MS
DUP
LCS
MB
MS
DUP
LCS
MB
MS
CRM
DUP
LCS
MB
WG2153319-3
WG2153319-2
WG2153319-1
WG2153319-4
WG2156410-2
WG2156410-3
WG2156410-1
WG2156410-4
WG2152328-3
WG2152328-2
WG2152328-1
WG2152328-4
WG2151850-4
WG2151850-3
WG2151850-2
WG2151850-1
L1658681-3
SALINITY_SOIL4
L1658681-3
L1659064-13
L1659064-13
L1658720-11
L1658720-11
WT-SQC012
L1657369-5
Boron (B), Hot Water Ext.
Boron (B), Hot Water Ext.
Boron (B), Hot Water Ext.
Boron (B), Hot Water Ext.
Chloride
Chloride
Chloride
Chloride
Cyanide, Weak Acid Diss
Cyanide, Weak Acid Diss
Cyanide, Weak Acid Diss
Cyanide, Weak Acid Diss
Chromium, Hexavalent
Chromium, Hexavalent
Chromium, Hexavalent
0.74
108.9
<0.10
N/A
12.7
104.3
<5.0
105.2
<0.050
87.7
<0.050
95.8
90.8
<0.20
97.6
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
25-AUG-15
25-AUG-15
25-AUG-15
25-AUG-15
19-AUG-15
19-AUG-15
19-AUG-15
19-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
10
0.5
N/A
N/A
40
30
35
35
70-130
-
70-130
70-130
80-120
70-130
70-130
80-120
ug/g
%
ug/g
%
ug/g
%
ug/g
%
ug/g
%
ug/g
%
%
ug/g
%
MS-B
0.82
12.6
<0.050
<0.20
0.1
5
0.05
RPD-NA
RPD-NA
14
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Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
CR-CR6-IC-WT
EC-R511-WT
HG-200.2-CVAA-WT
MET-200.2-CCMS-WT
Soil
Soil
Soil
Soil
R3250845
R3250061
R3250160
R3250163
R3251020
Batch
Batch
Batch
Batch
Batch
MB
DUP
LCS
LCS
MB
CRM
DUP
LCS
MB
CRM
DUP
LCS
MB
CRM
WG2151850-1
WG2153325-4
WG2153494-2
WG2153494-3
WG2153325-1
WG2153332-2
WG2153332-6
WG2153332-4
WG2153332-1
WG2153335-2
WG2153335-6
WG2153335-4
WG2153335-1
WG2153332-2
WG2153325-3
WT-CANMET-TILL1
WG2153332-5
WT-CANMET-TILL1
WG2153335-5
WT-CANMET-TILL1
Chromium, Hexavalent
Conductivity
Conductivity
Conductivity
Conductivity
Mercury (Hg)
Mercury (Hg)
Mercury (Hg)
Mercury (Hg)
Mercury (Hg)
Mercury (Hg)
Mercury (Hg)
Mercury (Hg)
Antimony (Sb)
Arsenic (As)
<0.20
0.125
98.9
101.5
<0.0040
94.8
<0.0050
102.0
<0.0050
95.5
0.0062
100.0
<0.0050
99.1
109.8
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
2.4
N/A
6.0
20
40
40
90-110
90-110
70-130
80-120
70-130
80-120
70-130
70-130
ug/g
mS/cm
%
%
mS/cm
%
ug/g
%
mg/kg
%
ug/g
%
mg/kg
%
%
0.128
<0.0050
0.0059
0.2
0.044
0.005
0.005
RPD-NA
14
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Report Date: 25-AUG-15Workorder: L1659064
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil
R3251020BatchCRM
DUP
WG2153332-2
WG2153332-6
WT-CANMET-TILL1
WG2153332-5
Barium (Ba)
Beryllium (Be)
Cadmium (Cd)
Chromium (Cr)
Cobalt (Co)
Copper (Cu)
Lead (Pb)
Molybdenum (Mo)
Nickel (Ni)
Selenium (Se)
Silver (Ag)
Thallium (Tl)
Uranium (U)
Vanadium (V)
Zinc (Zn)
Antimony (Sb)
Arsenic (As)
Barium (Ba)
Beryllium (Be)
Boron (B)
Cadmium (Cd)
Chromium (Cr)
Cobalt (Co)
Copper (Cu)
Lead (Pb)
Molybdenum (Mo)
Nickel (Ni)
Selenium (Se)
Silver (Ag)
Thallium (Tl)
Uranium (U)
Vanadium (V)
103.9
102.6
97.2
113.5
106.5
101.5
91.9
101.7
107.5
89.3
96.8
103.0
106.9
116.0
105.7
<0.10
1.11
9.57
<0.10
<5.0
0.024
4.44
1.68
1.82
3.58
0.43
2.95
<0.20
<0.10
<0.050
0.240
9.11
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
N/A
8.5
14
N/A
N/A
N/A
2.4
6.4
2.4
0.8
0.24
3.5
N/A
N/A
N/A
6.6
9.0
30
30
40
30
30
30
30
30
30
40
2
30
30
40
30
30
30
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
<1.0
1.0
8.3
<0.50
<5.0
<0.50
4.3
1.6
1.9
3.6
<1.0
2.8
<1.0
<0.20
<0.50
<1.0
8.3
RPD-NA
RPD-NA
RPD-NA
RPD-NA
J
RPD-NA
RPD-NA
RPD-NA
14
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Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil
R3251020BatchDUP
LCS
MB
WG2153332-6
WG2153332-3
WG2153332-1
WG2153332-5Zinc (Zn)
Antimony (Sb)
Arsenic (As)
Barium (Ba)
Beryllium (Be)
Boron (B)
Cadmium (Cd)
Chromium (Cr)
Cobalt (Co)
Copper (Cu)
Lead (Pb)
Molybdenum (Mo)
Nickel (Ni)
Selenium (Se)
Silver (Ag)
Thallium (Tl)
Uranium (U)
Vanadium (V)
Zinc (Zn)
Antimony (Sb)
Arsenic (As)
Barium (Ba)
Beryllium (Be)
Boron (B)
Cadmium (Cd)
Chromium (Cr)
Cobalt (Co)
Copper (Cu)
Lead (Pb)
Molybdenum (Mo)
Nickel (Ni)
Selenium (Se)
10.2
102.1
96.3
96.4
98.5
96.4
91.3
94.1
94.6
92.8
100.9
102.0
94.7
94.6
97.2
94.6
95.0
96.5
99.4
<0.10
<0.10
<0.50
<0.10
<5.0
<0.020
<0.50
<0.10
<0.50
<0.50
<0.10
<0.50
<0.20
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
17 30
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
ug/g
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
8.6
0.1
0.1
0.5
0.1
5
0.02
0.5
0.1
0.5
0.5
0.1
0.5
0.2
14
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Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil
R3251020
R3251092
Batch
Batch
MB
CRM
DUP
WG2153332-1
WG2153335-2
WG2153335-6
WT-CANMET-TILL1
WG2153335-5
Silver (Ag)
Thallium (Tl)
Uranium (U)
Vanadium (V)
Zinc (Zn)
Antimony (Sb)
Arsenic (As)
Barium (Ba)
Beryllium (Be)
Cadmium (Cd)
Chromium (Cr)
Cobalt (Co)
Copper (Cu)
Lead (Pb)
Molybdenum (Mo)
Nickel (Ni)
Selenium (Se)
Silver (Ag)
Thallium (Tl)
Uranium (U)
Vanadium (V)
Zinc (Zn)
Antimony (Sb)
Arsenic (As)
Barium (Ba)
Beryllium (Be)
Boron (B)
Cadmium (Cd)
Chromium (Cr)
Cobalt (Co)
Copper (Cu)
<0.10
<0.050
<0.050
<0.20
<2.0
98.6
102.7
99.7
87.2
92.8
103.5
101.0
97.0
92.8
97.5
101.4
89.7
96.1
95.1
111.9
106.3
97.5
<0.10
2.41
12.3
0.13
5.8
0.140
7.25
2.41
9.57
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
N/A
13
4.4
11
11
12
4.4
4.9
8.8
30
30
40
30
30
30
30
30
30
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
<1.0
2.7
12.9
<0.50
6.5
<0.50
7.6
2.5
10.4
0.1
0.05
0.05
0.2
2
RPD-NA
14
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CHUNG AND VANDER DOELEN311 VICTORIA ST. N. KITCHENER ON N2H 5E1ERIC CHUNG
Report Date: 25-AUG-15Workorder: L1659064
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil
R3251092BatchDUP
LCS
MB
WG2153335-6
WG2153335-3
WG2153335-1
WG2153335-5Lead (Pb)
Molybdenum (Mo)
Nickel (Ni)
Selenium (Se)
Silver (Ag)
Thallium (Tl)
Uranium (U)
Vanadium (V)
Zinc (Zn)
Antimony (Sb)
Arsenic (As)
Barium (Ba)
Beryllium (Be)
Boron (B)
Cadmium (Cd)
Chromium (Cr)
Cobalt (Co)
Copper (Cu)
Lead (Pb)
Molybdenum (Mo)
Nickel (Ni)
Selenium (Se)
Silver (Ag)
Thallium (Tl)
Uranium (U)
Vanadium (V)
Zinc (Zn)
Antimony (Sb)
Arsenic (As)
Barium (Ba)
Beryllium (Be)
Boron (B)
7.66
0.29
5.06
<0.20
<0.10
<0.050
0.417
14.3
44.5
110.6
104.8
105.3
93.9
92.5
106.2
103.8
105.4
103.5
109.0
107.6
104.6
105.9
103.6
104.4
105.8
106.0
98.4
<0.10
<0.10
<0.50
<0.10
<5.0
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
7.6
13
5.8
N/A
N/A
N/A
9.3
5.5
0.3
40
40
30
30
40
30
30
30
30
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
8.3
<1.0
5.4
<1.0
<0.20
<0.50
<1.0
15.1
44.3
0.1
0.1
0.5
0.1
5
RPD-NA
RPD-NA
RPD-NA
14
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CHUNG AND VANDER DOELEN311 VICTORIA ST. N. KITCHENER ON N2H 5E1ERIC CHUNG
Report Date: 25-AUG-15Workorder: L1659064
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT
MOISTURE-WT
PAH-511-WT
Soil
Soil
Soil
R3251092
R3249043
R3252258
Batch
Batch
Batch
MB
DUP
LCS
MB
DUP
WG2153335-1
WG2152114-3
WG2152114-2
WG2152114-1
WG2151969-5
L1659055-7
WG2151969-4
Cadmium (Cd)
Chromium (Cr)
Cobalt (Co)
Copper (Cu)
Lead (Pb)
Molybdenum (Mo)
Nickel (Ni)
Selenium (Se)
Silver (Ag)
Thallium (Tl)
Uranium (U)
Vanadium (V)
Zinc (Zn)
% Moisture
% Moisture
% Moisture
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
<0.020
<0.50
<0.10
<0.50
<0.50
<0.10
<0.50
<0.20
<0.10
<0.050
<0.050
<0.20
<2.0
9.07
98.0
<0.10
<0.030
<0.030
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
19-AUG-15
19-AUG-15
19-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
6.3
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
20
40
40
40
40
40
40
40
40
40
40
90-110
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
9.66
<0.030
<0.030
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
0.02
0.5
0.1
0.5
0.5
0.1
0.5
0.2
0.1
0.05
0.05
0.2
2
0.1
RPD-NA
RPD-NA
RPD-NA
RPD-NA
RPD-NA
RPD-NA
RPD-NA
RPD-NA
RPD-NA
RPD-NA
14
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CHUNG AND VANDER DOELEN311 VICTORIA ST. N. KITCHENER ON N2H 5E1ERIC CHUNG
Report Date: 25-AUG-15Workorder: L1659064
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Soil
R3252258BatchDUP
IRM
LCS
WG2151969-5
WG2151969-3
WG2151969-2
WG2151969-4
ALS PAH1 RM
Chrysene
Dibenzo(ah)anthracene
Fluoranthene
Fluorene
Indeno(1,2,3-cd)pyrene
Naphthalene
Phenanthrene
Pyrene
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Chrysene
Dibenzo(ah)anthracene
Fluoranthene
Fluorene
Indeno(1,2,3-cd)pyrene
Naphthalene
Phenanthrene
Pyrene
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
95.3
101.3
69.9
111.9
67.3
104.4
92.9
110.1
100.4
76.7
119.1
121.4
110.3
71.2
94.3
96.0
103.1
108.2
87.9
89.0
90.9
91.1
91.3
89.0
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
40
40
40
40
40
40
40
40
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
RPD-NA
RPD-NA
RPD-NA
RPD-NA
RPD-NA
RPD-NA
RPD-NA
RPD-NA
14
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Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT
PCB-511-WT
Soil
Soil
R3252258BatchLCS
MB
WG2151969-2
WG2151969-1
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Chrysene
Dibenzo(ah)anthracene
Fluoranthene
Fluorene
Indeno(1,2,3-cd)pyrene
Naphthalene
Phenanthrene
Pyrene
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Chrysene
Dibenzo(ah)anthracene
Fluoranthene
Fluorene
Indeno(1,2,3-cd)pyrene
Naphthalene
Phenanthrene
Pyrene
Surrogate: 2-Fluorobiphenyl
Surrogate: p-Terphenyl d14
92.4
88.5
77.5
89.2
93.7
80.8
89.7
91.9
79.1
89.7
89.6
95.4
<0.030
<0.030
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
<0.050
89.5
88.0
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
50-140
%
%
%
%
%
%
%
%
%
%
%
%
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
%
%
0.03
0.03
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
50-140
50-140
14
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CHUNG AND VANDER DOELEN311 VICTORIA ST. N. KITCHENER ON N2H 5E1ERIC CHUNG
Report Date: 25-AUG-15Workorder: L1659064
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PCB-511-WT
PH-R511-WT
SAR-R511-WT
Soil
Soil
Soil
R3251604
R3249319
R3250269
Batch
Batch
Batch
DUP
LCS
MB
MS
DUP
LCS
DUP
IRM
WG2151969-5
WG2151969-2
WG2151969-1
WG2151969-6
WG2151989-1
WG2152535-3
WG2153325-4
WG2153325-2
WG2151969-4
WG2151969-4
L1657369-11
WG2153325-3
WT SAR1
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Surrogate: d14-Terphenyl
Aroclor 1242
Aroclor 1254
Aroclor 1260
pH
pH
Calcium (Ca)
Sodium (Na)
Magnesium (Mg)
Calcium (Ca)
Sodium (Na)
Magnesium (Mg)
<0.010
<0.010
<0.010
<0.010
108.6
94.7
100.4
110.0
<0.010
<0.010
<0.010
<0.010
100.5
107.7
101.3
111.5
7.69
7.03
16.0
1.3
5.2
97.9
99.5
96.1
22-AUG-15
22-AUG-15
22-AUG-15
22-AUG-15
22-AUG-15
22-AUG-15
22-AUG-15
22-AUG-15
22-AUG-15
22-AUG-15
22-AUG-15
22-AUG-15
22-AUG-15
22-AUG-15
22-AUG-15
22-AUG-15
19-AUG-15
19-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
20-AUG-15
N/A
N/A
N/A
N/A
0.03
4.4
2.3
4.8
40
40
40
40
0.3
40
40
40
60-140
60-140
60-140
60-140
60-140
60-140
60-140
6.7-7.3
70-130
70-130
70-130
ug/g
ug/g
ug/g
ug/g
%
%
%
%
ug/g
ug/g
ug/g
ug/g
%
%
%
%
pH units
pH units
mg/L
mg/L
mg/L
%
%
%
<0.010
<0.010
<0.010
<0.010
7.66
15.4
1.4
5.0
0.01
0.01
0.01
0.01
60-140
RPD-NA
RPD-NA
RPD-NA
RPD-NA
J
14
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CHUNG AND VANDER DOELEN311 VICTORIA ST. N. KITCHENER ON N2H 5E1ERIC CHUNG
Report Date: 25-AUG-15Workorder: L1659064
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
SAR-R511-WT
SO4-WT
Soil
Soil
R3250269
R3253204
Batch
Batch
MB
CRM
DUP
LCS
MB
WG2153325-1
WG2155832-5
WG2155832-4
WG2155832-2
WG2155832-1
AN-CRM-WT
L1659064-1
Calcium (Ca)
Sodium (Na)
Magnesium (Mg)
Sulphate
Sulphate
Sulphate
Sulphate
<1.0
<1.0
<1.0
116.2
<20
104.7
<20
20-AUG-15
20-AUG-15
20-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
24-AUG-15
N/A 30
70-130
70-130
mg/L
mg/L
mg/L
%
mg/kg
%
mg/kg
20
1
1
1
20
RPD-NA
14
Quality Control Report
Page 12 of
Report Date: 25-AUG-15Workorder: L1659064
Sample Parameter Qualifier Definitions:
Description Qualifier
J
MS-B
RPD-NA
Duplicate results and limits are expressed in terms of absolute difference.
Matrix Spike recovery could not be accurately calculated due to high analyte background in sample.
Relative Percent Difference Not Available due to result(s) being less than detection limit.
Limit ALS Control Limit (Data Quality Objectives)DUP DuplicateRPD Relative Percent DifferenceN/A Not AvailableLCS Laboratory Control SampleSRM Standard Reference MaterialMS Matrix SpikeMSD Matrix Spike DuplicateADE Average Desorption EfficiencyMB Method BlankIRM Internal Reference MaterialCRM Certified Reference MaterialCCV Continuing Calibration VerificationCVS Calibration Verification StandardLCSD Laboratory Control Sample Duplicate
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Report Date: 25-AUG-15Workorder: L1659064
ALS Product Description Sample
ID Sampling Date Date Processed Rec. HT Actual HT
Physical Tests
Leachable Anions & Nutrients
Cyanides
Polycyclic Aromatic Hydrocarbons
123456789
1011121314161718
11013
135789
1011131617
2468
121418
21-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-15
21-JUL-1521-JUL-1521-JUL-15
21-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-15
21-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-1521-JUL-15
19-AUG-15 16:1719-AUG-15 16:1819-AUG-15 16:1919-AUG-15 16:2019-AUG-15 16:2119-AUG-15 16:2219-AUG-15 16:2319-AUG-15 16:2419-AUG-15 16:2519-AUG-15 16:2619-AUG-15 16:2719-AUG-15 16:2819-AUG-15 16:2919-AUG-15 16:3019-AUG-15 16:3119-AUG-15 16:3219-AUG-15 16:33
25-AUG-15 01:3425-AUG-15 01:3525-AUG-15 01:36
18-AUG-15 19:4318-AUG-15 19:4418-AUG-15 19:4518-AUG-15 19:4618-AUG-15 19:4718-AUG-15 19:4818-AUG-15 19:4918-AUG-15 19:5018-AUG-15 19:5118-AUG-15 19:5218-AUG-15 19:53
18-AUG-15 16:1818-AUG-15 16:1918-AUG-15 16:2018-AUG-15 16:2118-AUG-15 16:2218-AUG-15 16:2318-AUG-15 16:24
1414141414141414141414141414141414
303030
1414141414141414141414
14141414141414
2929292929292929292929292929292929
353535
2828282828282828282828
28282828282828
% Moisture
Chloride-O.Reg 153/04 (July 2011)
Cyanide (WAD)-O.Reg 153/04 (July 2011)
PAH-O.Reg 153/04 (July 2011)
EHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTR
EHTEHTEHT
EHTREHTREHTREHTREHTREHTREHTREHTREHTREHTREHTR
EHTREHTREHTREHTREHTREHTREHTR
Qualifier
Legend & Qualifier Definitions:
Hold Time Exceedances:
Units
daysdaysdaysdaysdaysdaysdaysdaysdaysdaysdaysdaysdaysdaysdaysdaysdays
daysdaysdays
daysdaysdaysdaysdaysdaysdaysdaysdaysdaysdays
daysdaysdaysdaysdaysdaysdays
EHTR-FM: EHTR: EHTL: EHT: Rec. HT:
Exceeded ALS recommended hold time prior to sample receipt. Field Measurement recommended.Exceeded ALS recommended hold time prior to sample receipt.Exceeded ALS recommended hold time prior to analysis. Sample was received less than 24 hours prior to expiry.Exceeded ALS recommended hold time prior to analysis.ALS recommended hold time (see units).
Client:
Contact:
CHUNG AND VANDER DOELEN311 VICTORIA ST. N. KITCHENER ON N2H 5E1ERIC CHUNG
14
Quality Control Report
Page 14 of
Report Date: 25-AUG-15Workorder: L1659064
The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against pre-determined data quality objectives to provide confidence in the accuracy of associated test results.
Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order.
Notes*:Where actual sampling date is not provided to ALS, the date (& time) of receipt is used for calculation purposes.Where actual sampling time is not provided to ALS, the earlier of 12 noon on the sampling date or the time (& date) of receipt isused for calculation purposes. Samples for L1659064 were received on 18-AUG-15 12:00.
ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal governmentrequirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by theUS EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS.
Client:
Contact:
CHUNG AND VANDER DOELEN311 VICTORIA ST. N. KITCHENER ON N2H 5E1ERIC CHUNG
14