40
~4 o 00000079 002356
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0000
0079
002356
002357
DOCUMENT INVENTORY LIST - FOSMAf
SMO CaseEPA Contract No. :DOCUMENT CONTROL #CASE-REGION-SUFFIX
of Samples__ of
60$
0 0 7-
DOCUH£KT TYPE1 S»ct>ap_ I/( Narrative)
Section I j/ (Q.C. Summary)Section Il l/Sample Oata for 5MO
^Traffic ReportsOne-entry for each Sample
Section IV/Ub Oetection LimitsInitial Calibration Oata Form VI
'VOA Continuing Calibration Oata Farm VIIInitial Calibration Oata Form VI
Continuing Calibration Oata Form VIIPesticide Oata Summary Forms VI I I -X
VGA Initial Cal ibrat ion Raw OataContinuing Cal ibrat ion Raw Oata
SNA Initial Cal ibrat ion Raw OataContinuing Calibration Raw Oata
Pesticide Raw OataRaw Calibration Oata
PAGE NUMBERS
8FB Raw Calibration OataMethod Blank OataMatrix Spike Oata
Matrix Spike Duplicate Oata
Airbil l/Shipping ManifestId Chain-of-Custody Document
Sample Receipt FormSection VIJAab
GC Injection Log PagesGC/HS Inj act ion lag Pages
002358
DOCUMENT INVENTORY CHECKL ISTPAGE 1 OF 3
SMU Case No . :£PA Contract No . : Q I ~
Date:No. of Samples
Document Type,Case F i l e Document Inventory List
Section 1: (Narrat ive )
Section 2: SPRS (Form II ) SummaryMS/MSO (Form II I ) SummarySB (Form IV) SummaryDFTPP (Form V) SummaryBFB (Form V) Summary
Section 3: Sample Data (for each sample)
Organ ic Analys i s Data Sheet (4 pages)VGA RICVGA Ouantitat ion Report (HSL )VOA Quantitatlon Sapor t ^non-HSL)vbA SpectraSNA mShA Quantitatlon Report (HSL)BHA QauntUatlon Report (non-HSL)^A spect'raPest i c i d e/PCB Chrotnatograms
Present
L^
L^
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&~~
is-I**-
.&Zis*^L^
\S*~i^£/-
Absent
002359
DOCUMENT INVENTORY CHECKL IST2 OF 3
3MO Case M o . : .56? 3EPA Contract No , : 69- £ /
Date:No. of Samples
Document Type
Section 4: Lab Detection LimitsInitial Cal ibrat ion Data(Form VI)
in order: VGA, SNAContinuing Calibration Data(Form V I I )
in order: VGA, SNAPesticide Evaluation Standards Summary(Form VI I I )
Pesticide/PCB Standards Summary(Form IX)
Pesticide/PCs Identification(Form X)
VGA Initial Calibration Raw DataBK4 Initial Cal ibrat ion Raw DataVGA Continuing Calibration Raw Data8NA Continuing Calibration Raw DataPesticide Evaluation Standards Data(A, 8, and C)
Pesticide Individual Standard Mix Data(A or B)
Present
L^
I/
IS
IS
is-</(7iSISISL/
I/
Absent
002360
DOCUMENT INVENTORY CHECKL ISTPAGE 3 OF 3
SMO Case No . :EPA Contract No. :
Date:No. of Samples
Section
Document Type Present Absent
5: DFTPP Raw Data8FB Raw DataMetnod Blank DataMatr ix Spike DataMatr i x Spike Dupl i cate Data
Section 6: Traffic ReportAiro i l 1 /Shipping ManifestField Chain-of -Custody DocumentSample Receipt Form
Section 7: Lab Notebook Pages - PreparationGC Injection Log PagesGC/MS Injection Log Pages
* If absent, indicate reason for absence.
{/L/ISt/iy\yis7
- -i/-- .isL^L/LS\Sis
002361
Science Applications international CorporabonApri l 17 , 1986
USEPA - REGION VIEnvironmental Services D iv i s i o n6608 Hornwood Dr.Montcrey Park Plaza, Bldg C.Houston, Texas 77074Attn: W i l l i am LangleySubject: EPA Contract 68-01 -6851Dear Mr. Langley:Enclosed please find a copy of the data report for SMO Case 5636 whichincludes 4 soi l samples plus assoc iated QC determinat ions .Although no signif icant problems were encountered in analyses of thesesamples several factors are noteworthy. «"-ij^es or tneseThe only problems encountered relative to surrogate spike recoveriesoccurred in the volati le fraction. The dS-toluene reEoverlei wire s l lqhtf jhigh re lat ive to contract acceptance windows. These samples were notreanalyzed to confirm sample - derived effects because the initial anaTvSerepresent dupl icate measurements, thus negating the need for conflrStlOTThe matrix spike recoveries for the volati le fraction were qood withoutexcept ion . The matr ix sp ike recoveries for extractable anal jtes weretypically good exh ib i t ing a total of four 8NA and two pestic ide outliersThe matrix s p lke precis ion/accuracy determinations were all we?l with inI 1 Eli 1 \f o *
yt°A t0 i?6 ??t?d.was the Presence of the tentatively ident if ied comoound4-hydroxy-4-methy1-2-pentanon e , a common reaction product ?n Swextract systems. Sample data has been appropriately noted with "B"qual if iers in the body of the data report.Don' t hesitate to contact me at ( 6 1 9 ) 4 5 6 - 7 4 6 9 should you have any quest ionsconcerning this data report. y ^uest 1ons
Sincerely,J
Lisa J. Pe^fersonSystem Project Manager/IshEnclosureDivision of Applied Environmental Sciences, 476 Prospect Street. La Joila. California 92037 (6/9J 456-7462:•>:>:& S.4.-C O'tiros Altnn}i<r,(,ut> Cr.icaqo. Dayton Uonce/ H,;.ifs^«, Loa Angeles Od» H,dg» OrM-irfo S*" Luega. S,m franc'Sco Tucson «n,t Was^,f,atari Ut.
002362
SOIL SURROGATE PERCENT RECOVERY SUMMARY__ Contract Laboratory „ ^5fti<Li______________ Contract No.
1MAurtcM.
FDOO"?
- - - - - - - - - - VOLATltfc
TQbMM-Q*
Ul-im
1cr»- 1 * 11
-VOLATILE - - - - - - - - - - - - [ PtSTiClO(
-»»
K~:Zb_-
"75
:?5?4 ~
__H'i _
FCH^ftMfL • -0»
/VA
VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS'*AQVISQRY LIMITS ONLY
"fct ^ _ _
Voia tiles: out of _'£— out af.? out *f _IZ
S.4,6.73
'5h::.
CMtOAIMOitll
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; outside of QCof OC Umtsof OC timts
r/as
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002363
SOIL MATRIX SPIKE /MATRIX SPIKE DUPLICATE RECOVERY5636 _______ Contractor ___SBL£ _______ Contract No. ~ ° ! '
Medium L»v*t
FRACTION
VOASMO
SAMPLE NO.moos
SAMPLE WO.
ACIDSMO
SAMPLE WO.
P£STSMQSAMPLE NO.
COMPOUND
TolueneSenren*
2.4Pyreoe
•P&troKKji-f*- PropytotnJCT*
Phenol
4- CWoro-3- Methyfphanol
AkfrtnDwttrin
4.4'-ODT
CONC. SPIKEADDED
OOIOOmoo
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SAMPLERESULTOooooocoooo&.o£Loooo0
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R22212921734738382'473SSO33SO503143384S
VALU6S ARE OUTSIDE CC LIMITS.
ERY5917262-1376G-133&913966-143810731 - 13728-8935-14?41-12628-1041/ 10920902510226-1031 1 18446-127•IS- 13034 13231-13442-13923134
RPO: VOAf. Qutttdff QC limit*oulsict* QC
QC limit»outucto QC limits
RECOVERV;B/M O^x __mif Of Jj .;ACIO-Scooiol JjQ;PEST „ 3. oul of .(,&:
c Mmft*oulikte QC IimiiioutiKt* QC ilmilt
QC limitl
FORM 7 / M S
002364
Case No. Contractor R I G Contract No. .L>O °
M1B110
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FORM IV 7/85
002365
• »C/ *S TUNING AND
CASEINST 1C " - INN1LA6 1C D^"APR7CATA RELEASE AOTHORIfED
«t/E
30
127
275365441442443
12
LABORATORY 5A ICSENS DATE 04/07/86CALI DATE 03/29/86
BV :.Srri; .. Z-***^**-*^ ~**f^+*~
SEWS TIMEANALVST
-6851II 38 00CO
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Q-" MASS 1982% 0? MASS 69
60%THAN
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VALUE INVALVE IN
PARENTHESIS IS '/. Ovc MASS 69PA»ENDH£SIS IS V. 0? MASS 442
688
* 3 280 00
45 420. 38
49 170 00
100 006 19
£0 111 . 557 49
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( 17 57) 2
SAMPLE 10 LAB ID DATE OF ANALYSIS TIME of ANALYSIS
4- 1 - ia.ioqSOPPM5TD BNRSTD 80 J±J^S£DBNftSThlfeH . H - 7 - 15.
FORM V 7/85
002366
1T--Z T JA
FORM V 7/85
002367
Cm No.inscrumtnt ID FlNNIJUb 10 BMflfijO
TUNING AND MASS CL IBRAT IONBromofluorob«nz*M (BFB)
S^IC. —————— _ Contract NoTim* 1 = QO
ContractorDate 3- 10-86Data Release Authorized By:
ION ABUNDANCE CRITfiMtA
SO75
9596173174175176177
15.0 • 40.0% of the baie peak30.0 • 60.0% of the bate peakBase peak. 100% relative abundance50 • 9.0% of the bate peekLeu than 1 .0% of the bau oeakGreater then 50.0% of the ban peekS.O 9.0% of man 174Greater than 95.0%, but teas than f 01 0% of m«i 1745.0 -9.0% of rruu 176
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THIS PERFORMANCE TUNE APPLIES TO fHE FOLLOWINGSAMPLES. BLANKS AND STANDARDS. Value m ptftnthtm if % mjti 174in 0trtnth«m n i?G.
SAMPLE ID LAS 10 DATE OF ANALYSIS TIME OF ANALYSIS
svSV5QQ«*• i. • 3*^^ 3=AQ-^
FORM V 7/85
002368
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LABORATOifSENS BA1ECALI DATE
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VAL'JE IN PASENTMESIS ISVALVE IN PARENTHESIS IS
174MASS 176
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78.4
79
266300757168523414
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TMIS PES50SMANCEAND STANDARDS
*JNE APPL IES f'.HE FOLLOWING SAMPLES* SLANKS,
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P8 S
BLANKDOCS
"BOOS
LAS IDSMAS17SVHAS 1 SLKMAfll"7
760053V76008GV7600 1QV76002QV760O4QV76006GV76007QV760O3GVA
DATEANALYZED
03/ 17/8603/ 17/860 3 / 1 7 / 8 603/ 17/8603/17/3603/ 17/3603/ 17/8603/ 17/8603/ 17/8603/ 17/8603/ 17/86
TIMEANALYZED
3Q
10101 1121315161713
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: 07: 0056: 00
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002369
O. Box-am HVTlScEmplc : i'i^nKi^3i"3-v..^ -55V^--fcffi: 557^90 -;: .;-^:
Case Number:
Sample Site Name/Code:
© SAMPLE CONCENTRATION(Check One)
Low ConcentrationMedium Concentration
SAMPLE MATRIX(Check One)
__Water__1 Soil/Sediment
Ship To:
Attn:
TransferShip To:
(D Regional Office:Sampling Personnel:
(Name}
(Phone)Sampling Date:
(Begin) .End)
© For each sample collected specify numberof containers used and mark volume levelon each bottle.
Water(Extract able)Water(VOA)
5) flipping Information
Name of Gamer
Date Shipped:
Airbill Number:
Soil/Sediment(Extffactable)Soil/Sediment(VOA)Other
Sample Description___ Surf ace Water __ Mixed Media__ Ground Water __ Solids__ Leachate __ Other (specify)
Qg) Special Handling Instructions:(e.g., safety precautions, hazardous nature}
Number o:Container;
ApproximateTotal Volume
@ Analysis Lab:Rec'd by: ________Date Rec'd: _______Sample ConditionOn Receipt (e.g., broken, noice, Cham-of-Custody,etc.)
Sample Location
LABHLECOPY
002370
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002371
QRGANICS ANALYSIS DATA SHCET SAMPLE #: 5D005i-ABQRATGRY SAICLABORATORY ID: 76001GMATRIX: SOILDATA RELEASE AUTHORIZED SV: Efl
CASE tt/SAS #: 5636QC SEPORT ft: S*34-CONTRACT #: -6851DATE DECEIVED:
SEMIVOLATILE COMPOUNDS (PAGE 1)LEVEL:DATE EXT/P9EP:DATE ANALYZED:SPL—>EXTRA€T:PM:7. MOISTURE:7. MOISTURE (DECANTED)STANDARD ID.SENSITIVITY ID:UNITS:
CAS #
OW04/08/8630. 05G: 1M1.Wt21- 1 1NASTDAP88
GPC CLEANyp _YES J^NOSEPARATORY EXTRACTION H
EXTRACTION ' '
1081 1 195
5411061009595
39638106621
67987888
10565-1 1 1120-120-9 1 -
106-87-59-91-77-88^95-91-88-
13 1 -208-99-83-51 -
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51-6-50-1-48-7-32-9-44-3-64-7-72-1-95-3-59-1~"75~5-67-9-85-0-91-1-33-2-82-1-20-3-47-8-68-3-50-7-57-6-47-4-06-2-95-4-58-7-74-4-1 1-3~9&-809-232-928-502-764-9
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002372
ORGANICS ANALYSIS DATA SHEET SAMPLE ?DOC5LABORATORY: SAICLABORATORY ID: 760010MATR IX : SOILDATA RELEASE AyTHORIZED BY
CASE #/SAS #: 5636QC REPORT #: &***CONTRACT #: -6851DATE RECEIVED:
SEMIVOLATILE COMPOUNDS <PAGE 2)
04/OS/8630. 05C: 1ML
LEVEL: LOWDATE EKT/PREP:DATE ANALYZED:SPL—>EXTRA€T:PH:X MOISTURE: 21. 11X MOISTURE (DECANTED): NASTANDARD ID: STDAPR8SENSITIVITY ID: BfAPRSUWITS: UG/KG
CAS #
QPC CLEANUPSEPARATORVCONTINUOUS
_YES J_NOEXTRACTION __YESEXTRACTION ' ' YES
121606
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S61011 18
8785
12084
206129859156
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Cas« NoOrganics Analysis Data Sh««t(Page 4)Tentatively Identified Compounds
CASWumkor Compound Mam* MT Of SunMum**f
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002377
ORGANICS ANALYSIS 0ATA •SAMftE * fD006SAIC
LABWATOSV 1C 760020sor*.DATA RELEASE AUTHORIZED fly
CASE »/SA8 • • 5636QC RC?o*r » aatCONTRACT » -685IDATE RECEIVED
COWOfNDS (*ACE 1)LOUCXT/P9EP
DATE ANAL Vf ED-- >EXTRACT
X MOISTWC < DEC ANTED)STANDARD IDSENSITIVITY ID:UNITS
CAS »100-95-21 1 1 -44-493-57-8
541-73-1106-46-7100-51-695-5O-J93-48-7
39638-32-91O6-44-5621-64-767-72-198-93-378-59-I38-73-5
103-67-965-83-0
1 1 1 -91 - 1120-33-2120-82-191-20-3
106-47-887-68*339-3O-791-57-677-47-488-O6-293-93-49t-3«-7S8-74-4
131-1 1-32OS-96-B99-O9-283-32-951-28-5
100-02-7132-64-9
04/06/8630. 640.Ttt18 9NASTDAfRSDfA^ffBUO/KO
0 IS< 2-CMLOOOETHVV. )fcT>«R
CLCAM^ _ VE8EITKACTIOW
CONTINUOUS EXTRACTION VES
1. 4-DlCHVOROBENrENEaENE^L ALCOHOLi. 2-Diem.gffoaENZENE
N-NI TROSQD I *RQ*»U VAHINEWEXACWLOROETHANCISOPHORONE2-NITRO^WENOL2* 4-f lENZOIC ACIDB I8< 2-CM.OftOCTHOX V )2. 4-DlCXLQ*Q?HCNQL1. 2, 4-TR! CWLQRGflENtENENAPMTWAUENt4-CWVOROANILINtHEX ACXLOROflOT AD I ENS
Hi X A€>tt.Q*OC VCLOf CNT AD I ENE2* 4, 6-2. 4,2-CMLOfiONAfHTXALENEDIMETWVi. PHTMALATE3-NITROANILINEACfNAPWTMCNE2. 4-DtNITflOfHENCH,4-NITfiOPMCNOi.
CONCmmmm
400 U40O V400 y400 y400 y400 y400 y400 y400 y400. y400. y4<x> y400 y4004OO.400 y
200040040O.4004OO400. y400. y400400400 y400 y2000 y400. y2000 y400 y400. y2000. y400. y2000. y2000. y400 y
002378
ORGANies A^AL^SIS DATA SHEET SAMPLE #' "DQ06LABORATORY SA2CLABORATORY ID 760020MATRIX SOILDATA RELEASE AUTHORIZED
CASE «/SA6 * 5636oc REPORT # aKCONTRACT tt: -6851DATE DECEIVED
SEMIVOLATILE COMPOUNDS (PAOC 2)LEVEL.DATE EKT/PRfP:DATE ANALYZED3PL-- >EITRACTPH:% HOISTORE
LOW04/08/8630 640: I ML
OPC CLEANOPSEPAHAfCmv EITHACTION HCONTINUOUS EITKACT10N
STAWDAUD ID3CNSITIVITVWITS
CAS
18 7NASTDAP68C/O/KC
2. 4-2,6-DINlTaQTQl.yENEDICTHVL PMTMAkATC
PWEWVL ETHER
4, 6-DINITRQ-2-««TMn.PHCNQLN-NITROSOD1PHCNVLAM1ME4-8ROMOPHENYL PHENVL ETHERHEXACHLGfiOBENIENEPCbfTACHLOROPHCNOL
121- 14-2606-20-284-66-2
7009-72-386-73-7
tOO-Ot-6934-52-186-30-6
101-99-3110-74-I87-86-989-01-8
120-12-784-74-2
2O6-44-0129-OO-085-68-791-94-156-55-3
1 17-8 1 -7218-O1-9117-84-0209-99-2207-08-950-32-8
193-39-S53-70-3
191-24-2RESULTS ARE REPORTED ON A DRV WEIGHT BASIS
ANTHRACENEDI-W-avTYL PHTHALATE'LUOHANTWENEPVRENEBtlTYL 0ENZVL PHTHALATE3, 3'-DieHLC*08ENriDIN£BCNZO ( A ) ANTHRACENE6 1 8(2-ETHVLMEXVL) PHTHALATECWVSEWEOI-N-OCTYL PHTHALATEflEUf 0 ( B ) 'LUOft ANTHENE8ENZO ( K ) f LUORANTHCNEINOENO( 1. 2, 3-DIflENfO<A,
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2000. U400 U400 U400 04OO. U400 U400 yBOO U400. U
I 32400. y4OO U400. U400. U400 U400 U400 y4OO. U
002379
FD-OOs
Organ i cs Analysis Data Shvet(Page 3)
Pesticide/PCBs
0«*te C. tr •;}'_ ted /r r epare-j - olO - 86Hw^b — — — «_ - «_ -
HASNumber ug/kg
L^Lf 'J- .1idrji:l._J_t acn1 or £l± 9.
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AC2S.lor - 1 2 4 ZArou 1 or ^_1I4BAro^i or-1 2ti4Aroc 1 or— I Z'6O
190
'/ ' i -- volume o<- e:--, tract i ^ . i e c ' -^d *. ul •Vs - Valume of water dx tracted f m l >Ws = Weight o-f sample extracted ig»Vt = Voltu-ne of total extract (ul )
or Ws 24 .8 000O
002380
Case NoOrganic* Analysis Data Shaat
Sample Num, — . »I - ' JJC00 r
fc
Tentatively Identified Compounds
CAfl Compound AT or Scankg;
.VA4-T
ist71C.If
2123.
24
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Form t.i»en 0 7 85
002381
US ENVE8ONMENTW ffiNCTflWISampled
OltoAJWC^^T) Case Number:
Sample Site Name/Code:
SAMPLE ODNCENTRATION(Check One)
Low ConcentrationMedium Concentration
SAIvE'LE MATRIX(Check One)
„__. Water—Jl Soil/Sediment
Ship To:
Attn:HMHHTransferShip To:
© Regional Office:Sampling Personnel:
(Name)
(PhonetSampling Date:
© For each sample collected specify numberof containers used and mark volume levelon each bottle.
Number ofContainersWater(Extractable)
(Begin) (End)Water(VGA)
ApproximateTotal Volume
@ Analysis Lab:Rec'd by: ________Date Hec'd: ______Sample Conditionon Receipt (e.g., broken, noice, Chain-of-Custody, etc.)
2) Shipping Information
Name of Carrier
Date Shipped:
Airbill Number:
Soil/Sediment(Ixtracfcable)Sofl/Sedlment(VGA)
Sample Description___ Surf ace Water__ Ground Water_. Leachate
Sample LocationMixed MediaSSoiidsOther (specify)
® Special Handling Instructions:(e.g., safety precautions, hazardous nature)
LABnLECOPV
002382
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002383
QRSANICS ANALYSIS DATA SHEET SAMPLE #: ~DOQ75AIC
LABORATORY ID: 76003QHAT8IX : SOILSATA RELEASE AUTHORIZED
CASE tf/SAS #: 5636QC REPORT #: £&3k—fe ~0t>&—CONTRACT #: -6851DATE RECEIVED 3/*@e/86o
SEMIV0LATILE COMPOUNDS (PAQE 1)LEVEL:DATE EXT/PSEP:DATE ANALYZED:SPL— >EKTflACT:PH:'/; MOISTURE:V. MOISTURE (DECANTED)STANDARD ID:
GPC CLEANUP VE8 \t__NQLOW4/8/86 SEPARATQRY EXTRACTION04/08/86 CONTINUOUS EXTRACTION30. 771G : 1MLS, 7.623. 37NA
.YESYES
SENSITIVITY ID: &FAPR8UNITS: US/KG
CAS #108-95-2 PHENOL1 1 1 -44-4 B IS ( 2-CHLQSQETH VL ) ETHER95-57-8 2-CHLOROPMENOL
541-73-1 1, 3-BICHLOaOBENfENE106-46-7 1, 4-DICWLOSOSENZENE1OO-51-6 fiENZVL ALCOHOL95-50-1 i> 2-BICHLQRQBEN2ENE95-48-7 2-METHVLPWENDL
39638-32-9 BIS(2-CHL0SOISOPROPVL) ETHER106-44-5 4-METMYLPWENQL621-64-7 N-NITRQSQDIPSQPLVAMINE
67-72- 1 HEKACHL080ETHANE9S-95-3 NITROBENZENE78-59- 1 I SOPMORONE88-75-5 2-NITRQPHENOV.
105-67-9 2. 4-DIMETHVLPWENOL65-85-0 6EHZQ1C ACID
1 1 1 -9 1 - 1 BIS<2-CHL08OETWOKV)METHANE120-33-2 2, 4-DICHLOROPWENOL120-82-1 1, 2, 4-T£I€M4.0R0B£NZ£NE9 1 -20-3 NAPHTHALENE
1 06-47-8 4-CHL0SQAN I L I N£87-68-3 HEKACHLOROflUTABIENE59-50-7 4-CHLORO-3-METHYLPM£NOL91-57-6 2-HETHYLNAPWTHALENE77-47-4 HEXACMLOROCVCLCPENTAtlENEf^C3 Mimf\f*. VB ^ ^J A JL __M^^l3 f & faJt ^^iflf^fl t*llPM/*>tOw vw «t <C* *t t O * K A %* P»i*.W*» wT^rtSbl* t/Af95-95-4 2, 4, 5-TRICMkORQPHENOL9 1 - 58-7 2-C WL.080WAPHTHALENES0-74-4 2-NITROANILIWE
131- 1 1 -3 DIMETHYL PWTWALATE208-96-8 ACENAPHTHYLENE
99-09-2 3-NITROANILINE83-32-9 ACENAPWTHENE51-28-5 2» 4-DINITROPHENOL
100-02-7 4-NITRQPHENQL132-64-9 DlfiENZOFURAN
CQtiZ
400. U400. U400. U400. U400. U400. U400. U400. U400. U400. U400. U400. U400. U400. U400, U400. U
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002384
ORGAN ICS ANALYSIS DATA SiHEETLABORATORYMATRIX : SOILBATA RELEA?€ AUTHORIZED SY:
SAIC;: 76003Q
SAMPLE #: FD007CASE tt/SAS #: 5636Q€ REPORT #: -SbBfe-fe-CONTRACT #: -6851PATE RECEIVED: 3/«fr/86
SEMIVOLATILE COMPOUNDS (PAGE £>LEVEL.DATEDATE ANALYZEDSPL—>£XTRACTPW:V. MOISTURE:y. MOISTURE <DECANTED)STANDARD ID:SENSITIVITY IDUNITS:
CAS «
LOW4/8/8604/00/8630 771G; 1ML5". ."K,23. 37NASTDAPR8
GPC CLEANUP _VES \__NOSEPARATORY EXTRACTION
EXTRACTION : YESYES
UG/HG
121- 14-2 2, 4-DINITROTOLUENE606-20-2 2,6-DINITROTOLUENE84-66-2 BIETMYL PHTWALATE
7005-72-3 4-CHLOROPHENVL PHENYL ETHER86-73-7 FLUQSENE
100-O1-6 4-HITRQANILINE534-52-1 4,6-DINITRO-2-METWVLPHENOL86-3O-6 N-NITROSODIPHENVLAMINE
101-55-3 4-fiROMOPHENYL PHENYL ETHER118-74-1 HEKACHLOROSENZENE87-86-5 PENTACHLOROPHENQL85-oi-8 PHENANTHRENEi 20-I 2-7 ANTHRACENE84-74-2 DI-N-fiUTYL PHTHALAVE
206-44-0 FLUORANTHENE129-OO-O PYfiENE85-68-7 8UTYL BENZYL PHTHALATE91-94-1 3. 3'-DICHLO80BENZIDINE56-55-3 SENZO(A)ANTHRACENE
1 17-81 -7 8IS<2-ETHVLHEKVL)PMTHALATE218-01-9 CHRYSENE1 17-84-0 DI-N-OCTYL PHTHALATE205-99-2 8SNZO < fi)FLUQgANTHENE207-O8-9 8ENZO < K)FLUORANTHENE
50-32-Q 8SNZO<A)PYRENE193-39-5 INDEN0U* 2, 3-CD)PYRENE53-7O-3 D18ENZO<A, M)ANTHRACEN£
191-24-2 8ENZO(GHI)PERYLENERESULTS ARE REPORTED HN A DRY WEIGHT flASIS.
CONC40O. U400. U400. U
U
510O.400. U
002385
Organ!cs Analysis Data Sheet(Page 3)
Pesticid«/PCB*
CASNumber gq/kq
. .a-Hl tC ' L i ^i-Jan.j -1 ' . .
rU d r i ng {' C h pp i . i
59-98-8 -t-an I
1- T- .*. 1 --o j"
Pi el dr in__4 4" -jJDf ___"_ Er>cK L n____ _^ndo 5Lilig 0;_1 J4
LLL'Iii~ ''Jzt.i 1 l'-* i""J6--^^4^s "- :1 -"?
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- volume o+ extract in tec tod iot- . - j l tjine -j* w-jter -3x t r^c tea • -n i~ We igh t ."jf sample *?x tr-«»c ted 'LJ= Volume of total extract J t ., '. )
,1 4
002386
C*«f No —• i
Organic* Analysts Data Shot{Pag* 4)TantativtJy ldantifi«d Compounds
1. Pin 8 ? 85
002387
'ROTECTION AGENCY HWI Sample . .
ORGANICS TRAFFIC REPbRT:D ;
0 COM Number:iSample Site Name/Coda:
i!
© Regional Offcce __ ..Sampling Personnel
i' < Name >
f^Phone)Sampling Data:
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NameofCamerii Date Shipped1
Airbill Number
© SAMPLEC(C
Low). __ Medi
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ONCENTRATirheck One >
ConcentrationumConcantrati
UTRDCDn»*
ediment
© For each sample collected «|of containers uaad and mark on each bottle.
Number ofContainersWater(Retractable)Water(VOA)Soli/Sediment(EsctTftctabia)Son/Sediment(VGA)Other
@ Sample Deecription_ Surface Water Muted MediaGro»jnd Water SobdsLaachate Other (specify)
ON © Ship To:
onAttn
TransferShip To:
jecrfy numberrolume level
ApproximateTotal Volume
_
(0) AnalynaLab:Rnn'dhy-DAt* R* d-Sample ConditionOn ReCOlpt |* g , broken, ncice, Chaansf -Custody, etc.)
D Sample Location
© Special Handling Instructions:(e.g., safety precautions, hazardous nature)
LABniZCQPY
J55-1 <7-r^>&
002388
: A ; C•ifcv;* A* :*» : t- r e - . - •
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108- 10- 1127- 18-4ioa-sa-3103-90-7100-4J-4100-42-5495-47-6
03/i r/14NA
ID: £ £NS !T [ v iT v IP
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610666
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106
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002389
MQANICS ANALYSIS CATA SXET3A1C
TD 76OO4Q*ACHI)r SOIL
RELEASE
LEVEL
CASE 0/8A8 0' Jft3*COMttlACr 0 -6851DACE DECEIVED
0VCOHfOUNM (fAOE 1)
LOWDATE3fL— ;E l tT ( »ACTfHV. MOISTO*E' : HOISTOflE -DECANTED *STAWAffD IDSENS IT IV ITV ID'JNITB
CAS •
O4/08/8630 995C4, if14 12NA
CLEAMt* xrfAcriot* HVEBCONTINUUM EIC0ACCION I" VES
108-95
5411 0610O9595
39638104621
679878
10565
1 1 11 2O12091
1068759917788959188
13J208
998351
100132
95-244-457-873-146-751-650-148-732-944-564-772- t95-359-175-567-985-09 1 - 133-282-120-347-868-35O-757-647-406-295-458-774-4U-396-8O9-232-928-502-764-9
06/KOCOWC
B 18(2-
1 . 4-DIOft.OflOBCNftNCBINtVL ALCOHOLi. 2-OKMLW00CWICWC
2, 4-sthioic ACID2, 4-1. 2, 4-NAfXTMALENE4-CHLOKOANILINE>*E X ACHLO«OBOT Afi I EN£
*£ K ACWIQflOC V CLWENTAD I ENE2. 4, 6-2, 4. 5-2-MITROANILINE
fMTMALATE3-NITftQANlLtNEACENAfMTMENE2. 4-DINITRWHE4-HITROfHENOL
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2000400
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002390
3)*GANICS ANALVSI5 DATA SH€ET SAMPLESAXC CASE ft/SAS ft
TO*V ID '6O040HATRIIC SOIL
DATA RELEASE AyrHOHIfED flr ' l^f: ' ' • •
COG8
CCWftACr ft: -6891DATE RECEIVED "'
.EVfiV.DAfEDATE
SEMIVOLATILE CQWOyNDS (PAOE 2)CLEANW _
'DECANTED)
EXTffACTION04/08/86 CONTINUOUS EXTRACTION30 9930 im.14 12NA
VES
ID IDCAS ftmmmmm
12 1 - 14 -2606-20-284-66-2
7003-72-366-73-7
100-01-6334-32-186-30-6
101-33-3118-74-187-86-383-01-8
12O-12-784-74-2
206-44-0129-OO-O33—68—791-94- i36-33-3
1 17-81 -7218-01-91i 7-84-0203-99-2207-08-9
30-32-8193-39-533-7O-3
191-24-2ftESUlTS AfiE
uo/xo2. 4-DXNirftOrOLWENE2. 6-DXNir*0r0V.UENEDIErHVL fHCHALAfC4-CMLO*OfMENVL PMENVL
CONC
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400 yeoo yI 38.
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400 y400. y400 y400 y400 y400. y400 y400. y
002391
5.J i .
Organic* Analysis Data Shevt3)
•^ .,- f f + i- , -,,- ! :.)!,• • • I. t f » • _ * £c; : ' ~p,ir.; - ,-iri.i i , ;• -jtf
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Vi « ^oU.'rrw? of extract i r , - e c t ^ d ' ( . • , ! •Vs - volume of water extracted <ml ' 'Ws ~ Weight o-f tampl 'g ex t rac t ed >g :
Vt - Vol Li.-ne of total e ; tract 'ul >
002392
Ca«*Organic* Analysis Data Sh««t
(Pag* 4)T«ntativ»lv Idantifiad Compounds
> (. (
o
002393
of EnforcementCHAIN OF CUSTODY RECORD Flnit Inttrrutional Bldg., 1201 fc'm St.
___ Date, Texas 75270PROJ NO PROJECT NAME
SAMPLER
SI A NO OATE IMC&-
STATION LOCATION
NO
OF
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REMARKS
*4o etc 09 SV y- 3_..3"
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£ T?^FDoo 7 t -
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Date / Time
Date /Time
Date / Time
Received by f. Relinquished by f^
Received by t$><i>wure) Relinquithec4 by {St
Received fot Laboratory b Date /Time
r~~- Origin*! AccofDomm Shipment Copy to Coo'dinajo' f t»ld
Date / Time
Date /Time
Received by:
Received by:
Remaiks
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002394
SAI DOCUMENT CONTROL LOG: SAMPLE RECEIPT AND LOG-IN
SAMPLE CUSTODIAN SIGNATURE: DOCUMENT CONTROL HO.: 56e>36-(*> .-CIRCLE THE APPROPRIATE RESPONSE:
1. Custody Seal
2. Cha1n-of-Custody3. Sample TagsSample Tag Numbers4. SHQ Forws
"->_fit/absentact/not Intactresent/absent
rit /absentIfsted
5MO/SAS CASE
AIRBILL HIW3ER: J/OQ/j'€?2.6
chain-of-cystody SHIPPER:
DATERECEIVED
7 ^ -s j i f c-?- ./r ft* - ' *t* - / J 5fc
TIMERECEIVED
/(^CVI,Y
^Ji.0 rfi/£jtf A»
EPA/5MOOiAIN-Of-CUSTOOYRECORDBUMBCR$-^4T$ 77»J-6, - 770?L 77*5
SHG S/WLEKUmER
f^.C^Z .r4-.M&ra oo7ro co$
MO. oruOHTAINERSRECEIVED
:?53J
CORRESPONDINGSA!LABNUMBER .
97Ki*?//20p7t«?^10*£K?J^^)?Jfe^V^?^
— - — •• • — -• » —
SA! CHA1N-OF-CUST00YRECORD NO.sa.« S7-DVMT,< S7 -C*/liALw %? • &(£*3« %? O^
DOES INFORMATION WC*^TOOY RECWS,
TRAFFIC KEPCmTS W©SAHPl£ TAGS AGREE?
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REMARKS:amiTioi OF SAMPLEsmp*ENT, ETC. Hwl- - -OK H^limNeHKnOKcf i Hiit- isS®
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002395
