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CERCLA Immediate Removal Project Kane and Lombard Streets Drumsite Baltimore, Maryland Sampling Reference Notebook
CERCLA Immediate Removal Project
Kane and Lombard Streets DrumsiteBaltimore, Maryland
Sampling Reference Notebook
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3 AIR MOXIICRV:G PSGCRA:-; ?CR
The ".-.;-.> & ?.' .'•• jr-i •; : t e j-.>.'::.-La ,-3 po: . nr: al rhreat of or;; ->1c vapor .•="" - 'is
and the iirpact of such rc-1-vasi-ts on off-site arr.ns. The presence of pTt^nt^a] ly
?.-=r°e ^ r-;pt3 ties of o-_;--~n'c v-T.-'.^J.; .._;.:i',= ri als on-si; e, the p1v>si onl. ':'-.;? •••••> r-; . - ; • < • 3
of the site (se:ii-buried s.ur.'!ace d.-:.-s) and the sensitive popular.:, on •./;.•• •'..• . . . '^ 'S
?.rc"jnd the site (school, residennial .--.•-tss, hospitals) create a p.-cd fur ; .pi t-n.trit •'. :a
•n •.:•;; e^sjve air-'.-or: tcring prcgri^ .f•:,'•?":§ cn-slte operations. .
"-1?v i's an oijclii'-e of an «ir- oDijitoring program which >:-s ?cL-n <.'.. ..''-. ]'..••..]
en axa^sble information to address the characteristics of the site in cu :•' !.T.. Jr
= v,culd be ;.-oi-ed that feVt-n for a given set of physical parameters (f ont-i.-nin-nts,
cc'-.-centratJORS etc) air rionitoring protocols are largely dtp- rV.-vit en t3:nc- .-iriont
conditions ]J!-.e Lo^perature, wind speed, wind diiection a.id other related factors.
Therefore, the air monitoring program outlined in the ensuring paragraphs should
be considered a guide, tailored to the site specific needs as far as possible, but
its implementation should be evaluated on the specific site conditions at the time
in question.
The proposed air-monitoring project is divided into 2 major portions as
follows:
1) Real time Air Monitoring
2) Personnel Pump Air Monitoring (time weighted average)
1) Real Ti~ie Air Mom'.tor j.ng
'i'he rlD (F>."ie Ton * ::cf' on ~-Rt-:.'Ctur) .-nnd/or T.' D (Phot oi onn'i.-j i i.- a Dctontor)
•'• <-:> '-- .".its :,-••'31 be usnd for on-site .\nd off-site opitorir-g. '"'ff-l1 0^^ jring
' • - • - . - . - • •;-, .-• ._• }-_j~fp c- 3r_t _ • „ • . . . -i. =;.- ' ' V.? -"' •; - •'-. 'vj
' ! o ',.Li:ir :•:...- ..y; : . . - j - "or - . . - ' ; • - § centirr.;ry.:s air ; c.; •.: ;r._:s.
\ >' '•.•:• "' ?. •; i r.:'. •-.:', t '~~.il "~a •:-;?• d en-site ccnfinucusly for air 'acnitorj.n^
:'n vhe work ar^a.
A rlD/r'lD instr-..:.. .ii: shall be vised for peri-ieter air nonitbring. As irdjc.ite
jn Vr tflch'T.ent #1 ,'iir '.ncnitcriDg s'lotions have b«nn ^st^bf: :• chad at the
peri'-'.rier. During active site cp&raticjjs (A ._...c.val of ur•—..=;, .-icv^-^nt -^>f
soils/fruits., etc.) continuous air ijonii-oi ir;g vill be prcv?red aronid rhe
ri:ii'. -it er. Duvirg ;:.~y oiiner si'e op^r.-iiicn '.-Vere cVru.':s , :- .•;" s , .-f'c. fa
•..•ct "...•:'.:.§ handled, pi-riodi c periaeters air soaitoring v/iJl be ._•:•.••.: i -d, A
perimeter run will be nsade every 2 to 3 hours. One (1) perimeter air
:i)0ni foring run shall be conducted before co—jnencement of work and after site
has been secured on a daily basis.
A] 5=0, wn^n site operations-are .in progress crd r-~e activity :.s cccuri^g on t'r.e
^— adjacent ballfie3ds, the_perimeter air monitoring will concentrate in those areas.
Finally the frequency and extent of the real-time air monitoring program shall
be adjusted based on day to day operations and the history of daily operation as
the removal action progresses.
In case of a release, detected by the on-site monitors, the ;perimeter
jaonitoring will be stepped up and any plume leaving the hot zone areas will be#
tracked.
The data from the perimeter monitoring will be recorded in a tabulated format
on standard forms. (See Attachment //2) .
2) Personnel Pu-irp Air Monitoring (time weighted average)
This c;3t«£cry of air rioniioring shall be conducted using pc.-sorne..! air monitoring
••••.v.t>s (e.g. Gjllians, ~ ':\A~) and tbe'ssir/pl.ing ijedia will lie .opropri nt Fly chor-en from
b.: <: '. :•...'.. -.-d ~n a cssii by ca:~s. basis. .•""•• 2 -•: ;1 y: ;-'^l_,*
- analysis by the nb»crb ::; de of the t-:nax ,-r;>i rhr/.-e sr.-i.vi v. -'.-.is to b-i,_ .„ ^_m,
performed by tbe ;;ubi]e stj'uo jab 'for Yc^Li^ .;:;;:_:~:',cs ,
— tinslysis of c&rtc.n w'.-'bds u^tmg .."r.x.:I'5 l^/' .• ... cd "o r^e ,""- ' - ' (j vv a .
P""^vr;'e "^c-b conLrJ-c'.-'-d cut L..r~';0ri r_p\CS.
Prior to the implementation of the regular air voni toring prc^r.":. :n.'cl'-" g
•pe: ~c.r-r.sl .pu-.rsj b;-,':e3 j.ne dava : -^cs ro be ;1ave1 oped. _Tv.:s •.•::!! be J--.-?. .?s :.:"" •::
1) Zs-.ab.lish FID/?JD readings en-sire and off-site (at ;•.: e p-.ri- -s .,-r
station) prior to conruencen/ent of any active on-sile cp;:-nations
(moving of drum, soil etc.)
2) Establish baseline data using personnel pu~ps usirg r.-r^on tubes/
tenax/3 stage tubes at ten air monitoring stations, ~s ^vrwn in
—• Attachment T/3. The tubes sent to an outside lab will be analyzed ^^
using PCAM 127 and the tenax/3 stage tubes to be analyzed according to the
established protocol'for the state mobile lab.
The regular air monitoring program using personnel pumps will involve 6 stations
(See Attachment //A) . The flow rates and total volume will nominally be the same as
those established for the baseline monitoring. However, site conditions (operations,
temp, wind direction, and speed) will dictate the actual flow rates on a case by case
basis.
The regular frequency of sampling x ill be as follows;
o Once a day using the tenax/3-stage tubes and analyses by the state mobile lab.
o Once evnry week using carbon tubes to be analy?.ed by PCA.M 127.
Q-.nliny Assurance/Quality Control (QA/QC) procedures will be a'ppr 7 ::-r lately
ir-r? i- en ted. All p':~ps along virh .the tubes will be calibrated uncer the sa~>e
ccr.jitions. For on- site analytics! work, b!,;.-.'-.s and/or specifically prc-p^red
tubes (exposed ro ur.kc'.m substances 3r.d ]ocv.-n ccncantr:.;':; .. ;-.s will ba .- " J'c-d . i o -'-3
ss-ples to be ansl^ed for QA/QC •p-'jr.po.s s) . A'rro back- to- r-rck c.s-'pli. g (v--.;:-g a
set of ten ax tubes/3 stage rubas and carbon v.:l. es at the same tir-e) will >= /'-i"""
f"cni -ci-.Tie to t:r-e. This deci;:icn- vrill be ...r-de on caily ?i'a •. ; fj-2t: --?; .
Tn sidition to flie above i;:st rv~ent oriant^d sir :-."C'/:J i -;ring r ;' --£ ~ : "*• > -_-—•-..-
t'r. fco:.-&ti cal nodels will also be developed for a set of nc filial v.i.nd ;.;d \ ,-.:.. ,i.r ;i'.-r -3
conditions and a representative organic compound on-site. This activity will be
performed by the Environmental Response Team (ERT) and the -information will assist -
the OSC and technical staff on-site to assess theoretical ranges of aerial impact
-' during a release.
Responsibilities
The real time perimeter air monitoring will be implemented by state personnel
with technical assistance from the TATs.
The real time on-site air monitoring will be performed by ERGS personnel under
supervision of the OSC.
The personnel pump air monitoring program will be implemented by the TATs with* .
analytical assistance from, the on-site air lab and the private lab cent/acted
through ERCS.
Theoretical air modeling will be performed by ERT.
All technical data rc-opilation and cvaluat ion will be performed by the TATs.
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On ::ay ?r 19-34 th3 Air £..-_?.G---.-e:it J5f :-.i.riist;at 1:.:' s .r'obile Air "cr: it or ing Liberal: cry (.-L.U-IL) .-as ;„;.jl ry =rdas in. en-site facility f^r *.*. =/;tif ic&tIon of •".-7 -tSJor^Hnic cc-.\ c^nds. '-'ith -.'•.•: r-;;sl£tzncis of _;i •_.-. '..'.3site generator, tasting ---as conducted an av-ra-2 ofei£ht hours per c%y,s-ery ^y, f: TJ: /;y 7 -o
fund site because of t'ra dvpi~g of a ^-r^e :. " r •--cf .fatal drums filled with unknown, possibly t^xic,
.2. Trsts and K2'-v.~c- ol o~y
oc.i-prised of t-o co?."~~ns,' two detectors, two ?-;-s of] tiaps, ana t-.o gas chrc,:atcg,raphs with integrators.
This system also affords some versatility in testingzsthcds. The primary functioning mode is that of anambient air tester where,with the aid of a sampling
' cane, ambient air is pulled through two collecting'• traps for 20 minutes and eventually desorbed onto the• column. This method was not used.
A second method uses the side-arm desorbers, part of ^Pthe Envirochem units. The three-stage sorption tubes(tenar,ambersorb,charcoal) were removed for remoteadsorption, using a handheld pump, and then thermallydesorbed by the unit for column analysis. A slightadaptation of the above method was also used on thosetenax tubes ordinarily desorbed through the Foxboroportable unit. This was done by simply attachingthe Pczboro vent-out to the Envirochem trap-adsorp-tion transfer line. This was accomplished with littledifficulty but presented contamination problems fromcarryover at low levels.
The third method made use of the Envirochem purge-and-trap mode. A 1:10 dilution of soil-to-distilledwater or a 100 solution of sample water "as usad to
: fill the purging vial. Carrier gas was biitblodthrough the mixture or solution for eleven ^inut^s,trapped, and then sent to column.
.An often used qualitative technique of taking hrsd-space was also employed with sr^s srco-ss. G-.rj--.-iii !y,a 1 jil or 5 :sl satpla -as drsxn-crf by .^jvi.vje '--.-a in j----::-donto the traps, d-sorbed, and analysed.
i-.-^-r: r:=n s t * •-?<:--! iz.3t :' rn -_--s J ". e by i.-j,-.;L:ng c:-,e (i; ul of a .25 -g/^1v _. I iti'e or5":i.c_s .-ScrE-dard •-.••to a puvnp-ev =-c x_^t ed .=r.beri;-rb or tin ax scrWnt•_.ba. 7".;e tube vis then thermally desorb-d onuo both tr'-.s 6nd held a totaof 12 .ir-jjies.. After trap c^jrpt ion and transfer to colu-r.n a -^r.perst^re-vrogr.--. • :.-ed SO-- :ir ute run vas initiated. '^calibration followed. Th:.s..standardization was done prior to tach run of sorbent tube sets.
pijrge-snd-t rap st. sndsrdi zai. : on •-•33 conducted by injecting JO ul of .1 .25'- =1, , — L V C j. o C 1 . c C / & - r- 1 C 5 S: - -~ - - i -' C v- n L O I -j u ru a. O ;. -j 1 3 C 1 i .' «.- C - cr L c T .; /• J ^ i c ni:sir:g a 10 ml al^c/jot of t'"ac solution as a pur^eeble. Ire s^sricsrj i.spurged for 11 -uii'-jtss, trip;:ed, desorbed, .-nd ihen re .V; L- ssd to col\.r:n..Standardization was done prior to each run of purge-and-tt ap sets.
Hc<sd-s-pcce analysis st «:.J.£i-di i^Li on -as conducLe_d Lhrc jgh ^t i v .3 -^ <~.~- 3 r s c r. "" o 3 5 -^ 1 ? • ^ '" "^ s ^ *~^ " ° c t *' c 'i o a ? c c 1 1 • '.' c — -' - - j - .t. ^ - - - - ' -^ .The .-..--.".pie was held en trap for at Jeas± six (6) ninut.es, desorbed, andr - ' r c :--.2 d to column. T*~e c£ 1 :'.br*r:"on vas retained in cc-.z-pu-tef :,iu-:;oi-y c, drecalibrated to accosroodate any changes in oven temperature programming.
4. Results and Conclusions
The nearest approximation to ambient air testing was deviior. st ratsd by thatdata derived from the sorbent tube testing in which tubes attached to band-held pumps were placed at designated points concentric to groundsource-zero.Air samples were drawn through the tubes for an average of 1 hour and thentested. The results of the sampling are given in the accompanying tables.Some samples were at or below the detectable levels for the chlorinatedorganic compounds. Most samples were non-detectable for any chlorinatedcompounds. Volatile compounds listed were at or below levels ordinarilyfound in ambient airs previously tested close to both residential andindustrialized areas; some results from these areas having reached levels ashigh as 50 ppb in some cases, especially as related to specific compoundssuch as pentane, hexane, benzene, toluene and the xylenes. Low part perbillion levels of these compounds are generally associated with gasolineusage in automobiles and contribute greatly to background detectables.
Methods showing elevated levels were those which depended on close-sourceanalyses, methods such as purge-and-trap and head-space analysis. Themaximum ranges on these resulted in 200 to 300 ppb levels.
True anbient air testing would have resulted in even lower levels th.-sn thosefound for the close-to-ground sorbent tube tests. Dispersion dynamics at 12feet above ground level are more fluid than what sorbent t;;bes allow.
In su-r-Tiary, the sfnpling program at the Kane & Lor-ibard site has shown no3'vcls of uTnbient air pollution that are outside the levels norr-.a! ly fiv--nd inthe urban ;-nd suburbsn areas we have measured to date.
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PROJECT 18?8-E16
:REL::;;:;ARY AIR SASPL: ~::''LTs
NO COMPOUNDS WERE DETECTED t.EOVE THE STATED Lii»17 OF DETECT'JCN (LOO) FCR-THE PRIORITY S.-.:'.r«.ES.
OHM'' Station 'f.'o. £nd 5es_cri r-tion
Ici2'3-02 STA 01 Kiddle SHe (in drjrr. ores) I.":-.--."1.
' lS^'8-04 STA 02B Middle Site (in dri;nj area) C.ZQ vo/1
1 3528-11 STA 10 Middle East Side (off site) 0.^0 ug/1
= ppt
i £ .i ?\
I~C. •=•:•-- L----/:i '.:-.-.-.rJvia-.v A.Brua/l t;dA!!anlic Park. Thc>c'--e. \'J C5C;S.' \ •—" '?.-.- '. *- •• 'jp ' r." ri•.•'••.•/ '•'. =""-i,"a/- • c
__\ ,~:.c-e: i£C'2; S'2-2^29 f-'J £00-7.22-0 89 -
June 6, 1934
CLIENT: O.K. :<ATE?. LSP.O. Bex 551Fivsdlsy, OH 458^0-0551
CAP3CS TVHES
XITHOD OFA:;AJLYSIS: NIOSH Method P&CAM 127
DATESSAILED: May 19, 3 984 May 25, 1984 & Msy 76, 1?34
DATERECEIVED: May 30, 1984
SAXPLESCOLLECTED BY: CLIENT
ANALYSISPERIOD: May 30, 1984 thru June 5, 1984
ANALYSIS NO: A6626 thru • A6636
ANALYTICAL L/V30RATORY TESTING
All inf crration regarding these samples i.e.; sc--up]e dales, t rl' e, ~.t?t ?'--'d ofc :>] ] fr-ct icn, vhere the client or clients' representative perfcnj^d the £.-~7iecollection etc., is as reported to us by the client. GC/MS : aw c;ta is stc-;edfrr a ;.-r:r.'i of thirty (20) cays. P'r-^se c:cr.i*rt ;.he : .-'.c siory ^
;•-, - -.r ->f v.:--<.s r ^ u r t if a l - . n c r r •••-,: i :>d rf i -Lr.a :s , , ; .' r ,(
t
J '
;} CLIENT:__ ROY F. VESTQN ______ ANALYSIS NO:____*. . .
CLIENT I.D.:_____519-E1___________ CHAR.T NO:_____TO N.
-l VOLATILE ORGANIC COMPOUNDS
] NIO£H ?f,CAM 127
-T DETECTION] PAP-A-METER . LEVEL (ul/1) RESULT (..I/.1.)
. re—ere <O.OI 0.07
5 Chloroforn -cO.Ol N.D.
a 1 ,2-Bich3 oroethsne <0.01 ?^.D.
j • Methlyene Chloride <0.01 N.D.
1,1,2,2-Tetrachloroethane <0.01 N.D.
Tetrachloroethene <0.01 N.D.
1,1,1-Trichloroethane <0.01 N.D.
1,1,2-Trichloroethane *0.01 N.D..
T;-i\:h3oroethane <0.01 N.D.
Toluene <0.01 0.42
Acetone *0.01 N.D.
p-Dioxane <0.01 N.D.
Methyl ethyl Ketone <0.01 N.D.
Styrene <0-01 »-D.Xylenes (Total) <0.01 N.D.
VOLUME (liters) 60
1
flRU00725
CL' :.::
1
7i
CL;E:.T I.D.: 2---jn< 519-EO • . • CHART NO.: F?J; :coS2
vnT--.TIT.E ORGANIC COMPOU'.'DS
N'lOSK P&CAM 127
DETECTION (ng/tuba)LLMIT - E£'..'1TS
Benzene <10 N.D.
Chloroform . <10 •' N'.D.
' 1 ,2-D:c:-5lcrr.-i'-.<r,e <30 S'.D.
Xeiihylene chloride <10 27
r I.1,2,2-Tetrschloroethane <10 N.D.
Tetrachloroethene <10 N.D.
1,1,1-Trichloroethane <10 N.D.
1.1,2-Tricbloroetr.ane <10 N.D.
— Trichloroerhene <10 N'.D.
~i ^ Toluene <10 N.D.4Acetone <10 N.D.
I p-Dioxane <10 N.D.Methyl ethyl Ketone <10 N.D.
^" Styrene <10 N.D.
Xylenes(Total) <10 N.D.
VOLUME N.A.
RRU00726
CLir;- I. P.: 519-52__.________ CHART NO:_____F^N:__10535
"' •' VOLATILE ORGANIC CC;-.?CiJ • . N10SH PtCAH 127
PARA/iETER LEVEL (' 1/D AIEULT
E^nrer.e • .' <0.01 '",C3Chloroforn <0.01 N'.D.
j 1,2-Dichloroethane <0.01 N.D..4 Methlyene Chloride <0.01 N.D.
1,1,2,2-Tetrachloroetbane <0.01 N.D.
J Tetrachlcroethene ' <0.01 N.D.1,1,1-Trichloroethane <0.01 N.D.
1 ,1,2-Trichloroethane " <0.01 N.D.Trichloroethsne <-0.01 N.D.
Toluene <0.01 0.11
Acetone <0.01 N.D.p-Dioxane <0.01 N.D.
Methyl ethyl Ketone <0.01 N.D.
Styrene <0.01 N.D.
Xylenes (Total) cO.Ol N.D.
VOLUME (liters) 60
ARI*00727
j
ci;:.rr:__gyY•__?. %ZS:'CK_______ . ANALYSIS N9:_
CLI£NT I.D.: 519-E3 ' CHART NO:
T\ VOLATILE ORGANIC COMPOUNDS
I KJOSH P'-rCAM 327i .
DETECTIONI P.A.RA-METER LEVEL (ul/l) RESULT (ul/1)i
• rfrn-.ene ^0.01' ' 0.07<I Chloroform <0.01 N.D. •
1,2-Dichloroethane <0.01 . . N.D. I
i Methlyene Chloride <0.01 N.D.
1 , 1 , 2,2-Tetrachl oroethane <0.01 N.D.
Tetrachloroethene <0.01 N.D.
- 1 , 1 , 1-Trichloroethane <0.01 N D.
1 , 1 , 2-TrichloroeLhane <0.01 N.D.
Tr ichloroeL'nane <0.01 N.D.
1 Toluene <0.01 0.07
Acetone <0.01 N.D.p-Dioxane <0.01 N.D.
Methyl ethyl Ketone <0.01 N.D.
Styrene <0.01 N.D.Xylenes (Total) <0.01 N.D.
VOLUME- (liters) 24
RRU00728
V.' CLI£ST:____?.OY r. "-'ESTCN_________ ANALYSIS NO:______-15\Q_
I
CLIENT I.D.: 5:5-0- _______ CHART NO: FRN: I0b87————————^————————
' ?' } ' VOLATILE 03GAS'1C CCMPr'JNDS
N 7 C £ K ? frC AM 1 2 7
DETECTIONI PARA-METER LEVEL (ng/tube) RESULTt
- r£n7.e-.? ...._„. .. • < 10 N.D.
•i Ch 1 o r o f ona *}Q N.D.1,2-Dichloroethane <10 N.D.
j Methlyene Chloride <10 26
1,1,2,2-Tetrachlorcethane <10 N.D.
j Tetrachloroethene <10 N.D.
1 . 1,1-Trichl oroet'--r:e - < 10 N.D.
1''—' 1,1.2-Trichloroecr.ane <10 N.D.i
Trichloroethane <10 N.D.
•| Toluene <10 N.D.
Acetone <10 N.D.! p - D i o x a n e <10 N.D.
Merhyl ethyl Ketone <10 N.D.
. St^rene <10 N.D.
: Xylenes (Total) OO N.D.
! ' " '{ VOLUME (liters) N.A.
CLIENT: -C!Y F. '--:- 'CS ANALYSIS NO:
i
CLIENT I.P.: 525-?A__________ CHART NO: FRN: 10SE:3
ij VOLATILE ORGANIC COMPOUNDS
3 . NICSH ?C.AM 127
DETECTIONPARAMETER LEVEL(ul/1) RESULT (ul/D
5er.2.er>e <0.01 O.G8
Chlcrofora <0.01 N.D.1,2-Dichlcroethane <0.01 N.D.
Methlyene Chloride <0.01 N.D.
1,1,2,2-Tetrachloroethane <0.01 N.D.
Tetrachloroethene <0.01 N.D.
J , 1,1-Trichloroethane <0.01 N.D.
1 ,1 , 2-Trichloroethane <0.01 N.D.
Trichloroethane <0.01 N.D.
Toluene <0.01 N.D.
-cetone <0.01 N.D.
p-Dioxane <0.01 N.D.
Methyl ethyl Ketone <0.01 N.D.
Styrene <0.01 N.D.
Xylenes (Total) < 0.01 N.D.
VOLUME (liters) 60
00730
2 9
l
CLIENT: ?GY r. VESTGN ANALYSIS NO:
CLIENT I.D.: 525-2A _______ CHART NO: F?.N: 1C539
VOLATILE ORGANIC CCM?CU>-TDS
TQSH P C.AM 127
T DETECTIONI PAP.AMETER LEVEL (ul/1) RESULT (ul/1)
• "enrer-e «c0.01 N'.D.
Chloroform <0.01 N.D.1 ,2-Dichloroethane <0.01 N.D.
3 Mechlyene Chloride C0.01 0.101 ,1 ,2,2-Tetrachloioethane <0.01 N.D.
'. * Tetrachloroethene <:0.01 N.D.
1 ,! , 1-Trichloroetbane <f0.01 N.D.\1 ,1,2-Trichloroethane <0.01 N.D.
Trichloroethane <0.01 N.D.
Toluene <0.01 N.D.Acetone <0.01 N.D.
1 p-Dioxane <0.01 N.D.
' Methyl ethyl Ketone <0.01 N.D.
j Styrene <0.01 N.D.
i Xylenes (Total) <-0.01 N.D.
1 VOLUME (liters) 45
»i
AR!*0073t
:LIENT:____;OY p. WZSTCN_____ ANALYSIS NO:
CLIENT I.P.: 525-3A__________. CHART NO:_____F?.N: ?059Q*
-t\
I VOLATILE ORGANIC COMPOUNDS
MOSH PkCAM 3275t»
DETECTIONI PARA-METER LEVEL (ul/1) RESULT (ul/l)4
, E-er.zer-e <0.01 sj.r,.
Chloroform <0.01 N.D.1,2-Dichloroethane <0.01 v n
j Meuhlyene Chloride <0.01 N.D.
1,1,2,2-Tetrachloroethane <0.01 N D»»
.) • Tetrachloroethene <0.01 N.D.
1,1,1-Trichl oroefhane <0.01 >. n
! L.-.' 1,1,2-Trichloroethane • <0.01 N.D.
]Trichlcroethane <0.01 N.D.
• Toluene «0.01 N.D...^Acetone <0.01 N.D.
p-Dioxane <0.01 N.D.Methyl ethyl Ketone <0.01 N.D.
Styrene <0.01 N.D.Xylenes (Total) <0.01 N.D.
VOLUME (liters) 45
"> CLIENT: . ?."t F. %ES7CX___________ ANALYSIS NO:.•
' CLIENT I . D . : 5 2 5 - 0 C H A . R T NO:_____FRN; -C591
• *tj VOLATILE CRCANTC COMPOUNDS
j NICSH P&CA.M 127J
DETECTION| PARAMETER LEVEL (r.g/tube) RESULT (rg/r.be)4
_ Benzene . <; 10 . N'.D.
j • Chloroform <10 N.D.1,2-Dichloroethaae . <10 N.D.
j Merhlyer.e Chloride < 10 N.D.
1 ,1,2,2-Tetrachloroethane - .. <10 N.D.
Tetrachloroethene <10 N.D.
1,1,1-Trichloroethane <10 N.D.
) 1,1,2-Trichloroethane <10 N.D.Trichloroethane OQ N.D.
Toluene <10 N.D.Ac«»rone <10 N.D.
p-Dioxane <10 N.D.
Methyl ethyl Ketone <10 N.D.
Styr-'-,p <10 N.D.
Xylenes (Total) <10 N.D.
, . ..VOLUME (liters) N.R.
J
1
ARt(00733
CLIENT: ROY F. -"STC-NT' ' CLIENT I.D.: ' 525-1A CHART NO: F~.N: 10592
VOLATILE ORGANIC COMPOUNDS
NIOSH P&CAM 127
DETECTIONPARAMETER LEVEL (ul/1) RESULT (ul/1)
ene <.0.01 N.D.
/ Chlorcform <0.01 • N.D.
1 , 2-D::chIoioethane <0.01 N.D.\] Methlyene Chloride <0.01 N.D.
1,1 ,2,2-Tetrachloroethane - - •• '<0.01 N.D.
! Tetrachloroethene rf'O.Ol N.D.1 , 1,1-Trichloroethane <0.01 N.D.
? (^ ' 1,1,2-Trichloroethane <0.01 N.D.-
Trichloroethane <0.01 N.D.
~* Toluene <0.01 N.D.
* Acetone <0.01 N.D.I p-Dioxane <0.01 N.D.•i Methyl ethyl Ketone 0.01 N.D.
Styrene 0.01 N.D.J . Xylenes (Total) <0.01 N.D.
' VOLUME (liters) 45
00731;
ANALYSIS NO:
CLIENT I. P.: 526-3A __________ _ • CHART NO: ________ pp.*; ; IG;93
VOLATILE OHGAJvlC COMPOUNDS
AM 127
DETECTIONPARAMETER LEVEL (ul/1) RESULT (ul/1)
r-ai'^cr.e «r. 0.01 N.D.
Chloroform «s.0.01 N.D.
1 ,2-Dic'nloroechane <0.01 N.D.
.Methlyene Chloride cO.Ol N.D.1 , 1 ,2,2-Tetrachloroethane <0.01 N.D.
Tetrachlcrcethene ' <0.01 N.D.
1 , 1,1-Trichloroetbane <UD.01 N.D.1 , 1 ,2-Trichloroethane <-0.01 N.D.
Trichloroethane <0.01 N.D.
Toluene <0.01 N.D.
Acetone <0.01 N.D.
p-Dioxane <0.01 N.D.
Methyl ethyl Ketone <0.01 N.D.
Styrene <0.01 N.D.
Xylenes (Total) <.0.01 N.D.
VOLUME (liters) 45
NOTES AND CCh._ENTS
N:D. = N'on Detectable1 ' ' -
-..j N.A. • Non Applicable
-, N.R. s Not Requested4
i '•
T
i
1
- 4
I
•*jl
1
i
j
Thomas F.^Cullen, Jr. ', ILaboratory Director/Organics Divisioi I
DEP CERTIFICATION NO: 08153
