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020832

TSSTINO MO CCRTIFICATION

VP/OTJt V Of V

Juia M, 1911

TECHNICAL REPORTfor

Vlar & CompanyUSEPA Contract Laboratory Program

Sample Management Office300 N. Lee Street

Alexandria, VA 22314

ENVIRONMCNTAL TfSTINO intf CERTIFICATION CORPORATION

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020S:rj• 28« RARITAN CENTER PARKWAV • EDISON, NJ 00(37 (201) HS-ttOO

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39 E4723-C942240 E4724-C942341 E4726-C942542 E4727-C942643 E4728-C942744 A1254 STD9.045 A1248 STD3.046 E4729-C942847 E4730-C942948 E4731-C943049 E4732-C943150 E4733-C943251 E4734-C943352 E4744-C943453 E4745-C943454 E4746-C943655 A1242 STD5.056 A1232 STD5.057 A1221 STD5.058 A1016 STD5.059 PEST ST01.060 /E

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,00, ,0000, ,0000,00, ,0000, ,0000.00, ,0000, ,0000.00, ,0000, ,1)000,00, ,0000, ,1)000,00, .0000, ,0000.00, ,0000, ,0000.00, ,0000, ,0000,00, .0000, ,0000.00, ,0000, ,0000.00, ,0000, ,0000.00, ,0000, ,0000,00, .0000, ,0900.00, ,0000, ,0000,00, ,0000, ,0000.00, ,0000, ,0000,00, ,0000, 1,0400,

58, P030I iIH, R0301 iIH, 1,00, 1,0000, 1,000059, P0302 lIH, R0302 lIH, 1,00, 1,0000, 1,0900

5H6

\ 1

riflY 29, 193* 14:33< SEQUENCE! D2640P OH CRN 13

CHflNNEL 1

< SUBSEOUENCE 1

METHOD4 IFBP'I

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Conpound No, 37Conpound Nann TetrachloroethyleneBean Nunben 526Retention Tine, 21,57 nin.Area, 64272Concentrationi 176,65 ng

i

mi >sinBpk b 9

666*

(60*

460*'*

260*•

S HIS Rrv. E Data BMfFul

39 (E

)S yL L f. 1 r ..,1 4* i'a

l spectra of the HJS data Sea639,68

94X" ' ' 121 ' ' ' ' ' 1*1 ' ' ' ' ' 211

n 839rlitS'm

40

46

Ml

404)

Fill >C22Bpk Rb 21

2686IH

2666*

1BOO*

1600*

SOO*

31 BC174ZVJP,lZlSHRS.ori:Tlri« T4^

(S46 V

" f. 4-iT r1' 41 81

5RnPLE,BClr4ZV5P,VDH FRHC Sea8«,T7

/ ia2 yk / fT 126 ' 1(8 ' 288

n 6B9• in,

40

46

•46

0

W

D <a Filn >C2?.31iiUi'iann BC1742VBP,1215HR8,«CMi»c, ETC SAMPLE,BC1742VBP,VOA FRACTION,S/lfl/B4,10UL

Conpeund Noi 36Connound Nanei TolueneBean Nunben S59Retention Tine, 28.77 nin.Ariai 137710Concentration' 182.20 ng

1567 1 '\I21037

1)

O 2sh•Isa

File >9Bf!'p* /j..y.

60Ba/.

(66*

466*1

266*

*

9*4

U48

Rev

(

\-r*

, E Data laseFuil spectra of the NBS data je4nttoi.ot

16

86 l"

, i. ] U-^' e'0 ' 120 ' IH ' 268

1209

?66'.41

M6

•20

I)•s,n

.pi%bfc8106*

260*

166*

*

Si*l

J

742VSPf121EHRS,eCi;TC SH"PLE,BC174IVSP,VOH FRRC Sc«21 ,2(

1

ni

IIf

•* 180 ,„\ ( 133 x1

, .1. _J. .. 1 . /

n 628•in,rlBO

46

46

M6

•26•

•A• -m- • • • • • -rt- • • i • • -,2, ••'••!„ • 266

Data FiJe, >C?23tnUlNanei 8C1742VBP,1215HRB,«CMite. ETC BAMPLE,BC1742WSP,VOA FRACTION,S/1B/B4,1PUL

Conpound Not 39Conpound Nanei 2-HexanoniBean Nunben 520Retention Tinei 21.26 nin.Areai 19865Concentrationi 146.16 ng

1568 0 038

rill >DMnil*866*

(II*

406*

2860;

S HBS t99

16

fil

*il

HH

E Data BaseFull spectra of the NBS data Scan1174.11

i

'/' 166,' 162

88 121 ' IH' ' 210 ' 248

1274Bin,:«e40

40

M»

Aea

Fill >C2231 BC174ZV.SP(1216MR5,«CnC SH"PLEfBC174ZVSP,V0R FRHC Scan 400Ipk Rb 6167 JP 19.71 ain.

666»

466*

306*

266*

I860

' ' ' ' 4

•

1 " >Mrl ... 1 '," "> '!' "x

rioe40•

40•10••20

. ., . . _rt . ., ...J(. .... . iw . ... .itt • - , . - JW -

Data File* )C2231,,U1Nann QC1742VBP,1215HRB,«CNilei ETC SAMPLE,BC1742ySP,VQA FRACTION,5/ifl/B4,10UL

Canpound No, 40Conpound Nanei 4-Methyl-S-pentanoneBean Nunbin 460Retention Tlnn 19.71 nin.Ariai 28194Concentration, 171,27 ng

1570

Fill >9IRS NBS Rfv. C Data Baqaujii spectra of the NBS data scan 1616

itV ' ' ' ' ' '1M 281

1)g.I17J

Fill >C22Bpk Rb 11

1666*

866*

(86*

468*

266*

61

\L.,ri

* ' •„• • • • • • •*• • ' l

26,36

119 133 *'t 177 \/ / . N ^ i

n 763nln.

46

40

MO0

•20

' i*6' ' ' ' ' ' '168 ' ' ' ' 286 '

Data Filei >C223J,,U1Nann BC1742VBP,1215HRB,ICHlaci ETC SAMPLE,BC1742V8P,VOA FRACTION,5/lB/B4,10UL

Cenpound Noi 41Conpound Nanei BtunneBean Nunben 703Retention Tinn 28,36 nin.Areai 77766Concentrationi 183.42 ng

02104°

1571 "M

880*

Flle >DBMS' NIJ Rev. E Data BaaeFull spectra of the HIS data Scan U7(Bpk «bM9999 •" i676,06 in

66

MO' \ S1 77 I280* T ( 7 J lita

I_____Ui_————2U.

u

W

Fill >C22Bpk Rb 19

1260*

660*

400*

*

31 BC174ZVSP,1Z1SHRS,|133

«1 7841 ? ,'

' ' "4^ ™ * 'lit

CETC JHFIPLE,BC174ZVSP(VOH FRRC SCI

>"

1 2671 133 177 \

;.|l( / . / . L.... .M ..... .M ..... .24a.

n 707•in.

40

46

•28

Data File i >C223inUlNanei qCl?42VBP,121SHRB,OCHi«ci ETC SAMPLE,flC1742V8P,VOA FRACTION,S/1B/B4,10UL

Conpound No, 42Conpound Nanei ortho-XyleneBean Nunber, 707Retention Tine, 26.52 nln.Areai 82603Concentration) 136.88 ng

021041tftf35

1572

saTK

I

File >Dlf•>k iW

666*

6680J

468*

288*

*

S NBS Rev. E Data Its*!99

/ ?l,?r*<xflllt

1

J1

spectra of the HIS data sc*n1679.00

66

166

lit ' IH' ' 266

1(79Bin.rlBB

i6840LM0

•

«

•ag>I03

Fill >C2231 BC174ZVSP.1216HRS,eCETC SHnPLE(BC174ZVSP.VDR FRHC Scan 723Bpk Ab CB6B6 V 29.14 »in.

2668*

266U*

1666*

1666*-.

668*'

61 77\ X..l.Jl.JL.

166

J*'l •••^•"1 ."eVj"'.

/

.„ 147 267133 * "S.'; • ' ' i

riee•

40•

40•

i41•20

lie ' ' ' ' ' lie ' ' ' ' 286*§» Data File, >C223inUl

Nane < QC1742VBP,121SHRB ,ICMi»c, ETC SAMPLE,QC1742VBP,VOA FRACTION,5/18/64,iOUL

Conpound No, 43Cenpeund Nanei neta-and-para-XyleneRean Nunbin 723Retention Tine, 29.14 nln.Ariai 177739Concentrationi 307.31 ng

021042

1573 "Tw

________ Totol Ion ChromatogromFit* \C33ie tH.tmtf In

OData Fill> >E2219nU3Nann 50PPM BTDMi»c, 50PPM STD B/N/A FRACTION,5/23/84,*E BTL434

Id File) i XFBENTitle, IFB P.E,QUANT ID FILE...,MHC..B31114La«t Calibration' 640522 12,48Operator IDi UU992Bdaunt Tim i B40523 07,56

021043O • G *1

1574 »6

F1J« >E22Bpk Rb 20

M600>1(606-

24806-2286*C8N8-1060*

1(60*

1460*12*0t

010*(60*460*260*

19 ceppn STB MPPH STB B/N s492 6.

" 7 '?/ 7il,.,l ,1,1 W ' 4»" ' «Y ' W ' '»' (V

66

74tf,WfW,,y,,,,,,tf,,l.

dn sse,

'•

*'

70

hi58M0

i98

«0

•10

4

Data File. >E22i9,,U3Nane> SOPPH BTbMilei SIPPH STD B/N/A FRACTION,5/23/84,OE B1L034

Conpound Net VConpound Nann PhenolBean Nunbtin 550Retention Ti*e. 3,86 nin.Aria i 12F.y94Concentration, 49.Bl UC/ML

O 71575

Fill >E2219 WPPH STD BBPPH STD ,„ B/H Scan 669Bpk Rb 24166 7 9.03 pjjji,

B4M8-

226«6

26606;tAAftfttmwmw

16000-

14666

1266ft

1601*

800*

•Oil;

4080-

26B* 49

63

1

,

,

126

!B 61 rto 010 91 180 ill it 8

;i»o

•98

«

T«

46

«e

M0

•90

«0

11

Data Filei >E2219<>U3Nanei 50PPM 6TDHiaci SOPPH 6TD B/N/A FRACTION,5/23/84,OE BTL034

Conpound Not 4Conpound Nanei bit<E-Chloroethyl) etherBean Nunberi 569Ritemtien Tinei 9.03 nln,Ariai 93921Concentration! 49.42 UC/hL

021045

1576 . %%

File >E2219 W"» STD HPPR STfl ,VN /jBpk flb 26911 *

C8M*>i

nil*

KM*

1480*

1200*

16608

680*

600*

400*

see*»

in76

60

61 1

(0" '

86

OB' ' " ' " ' it a" ' 120 ' 140I

n (28A'e1'

10

i*1;fO

I"*•

M6

•30

«0

•<B

A

Data File, >E2219nU3Nanei SOPPrt 3TOHlaci SOPPH 6TD U/N/A FRACTION,5/23/04,« BTL«34

Conpound No> 6Ctnpound Mane, 1,4-DichloribenieneBean Nunbiri 62URetention Tinei 9.57 nin,Ariai 83391Concentration, 52.SB UC/ML

021046

o , ' V--G°1577 t«

o

Fill >E2219 MPPrBpk Ab C1044

2060*

I860*

1666*'

1460*

1266*

1666*

666*

668*

486*

261*

1 STD UOPPM STD I'M ,oCcllSj

7»>

61

68

1»••!'" ft

163

l|...iMl .)......... |.~

X.

1 61 ' 7B ' 1

/ «

66

1 I'llMIIII •II 1 9

)0r

an 722ur1048

|?e

•«e

«e

•46

•38

«•

r,-- ,- -ie|--.- --

Data File. >E22i9nU3Nanei SOPPM STD

SOPPM BTD B/N/A FRACTION, 5/23/84, OE BTL034

Conpound No, 12Conpound Nann 2-MethylphenolBean Nunbin 722Ret in t ion Tine, 10.44 nin.Aria > 82435Concentration, 53.29 UC/ML

021047

O - ' c^Gt1578 *

1

. ___ ._.. yi W7Bpk Rb 16360 16 6 ejn,File X2219 BiPPM STD BBPPH STBRb 10;

3000*2860*M80*2480*2260*2860*1860ft1(00*1466ft1260*1680ft800*660*4808-

77

61

43 I I t?

ll,,,,,ll|•16

200H

68

79

90

'iio'

40

40

M6

«0

Data Filli >b2219,.U3Nane, SOPPM STDMite, 50HPM STD B/N/A FRACTION,5/23/B4,OE BTL»34

Conpound Not 13Conpound Nanei 4-MethylphenclBean Nunbin 767Retention Tine, 10.B5 nin.Areai 130474Cencintratiom 53.60 UU/ML

021048

1579 ^

O

Fill >£2219 WPPrl STD WPrTSTD B/N .*,„ 1026Bpk flb 63764 . Il5« oiin.

(666*6660ft6266*4880*4468*4666ft3666*9266*2680*2406I- c482000*1666ft

i

1266*866*

20«e<H Lje

1266H B|63 7« 77 rr!6

466*p ...,.......,..............,......,.............

46

40

Data File, >E2219i>U3Nanei SOPPM 6TDMist, SOPPM 81D 6/N/A FRACTION,S/23/B4,«E BTL»34

Conpound Not 22Conpound Nanei NaphthaleneBean Nunberi 1026Retention Tine, 13,22 nln,Ariai 2B0037Concentrationi 50.10 UC/ML

021049

1580

o

o

)

1It(jl

File >E2219 B»ppripk Rb tl

•AttAslCWolP

1666*

1668*

1406*•

1288ft•

180i|ft

••••>•WiT

668ft

460*

206*

400

[

41sI, 1

STD 6BPPM STD

77X.

61' 6*

I, .,11,

7 '

t67»'M Jean 933

U

183

„ \

:• 12,3

122X

i

1

rrll»'

•96

•40

>6

40

40

46

48

48

r

' ' '60 ' 70 8B 9V 'l80 ' ' lie ' 120

Data Fill i >E2219nU3Nann SOPPM STD •Mitei 5DPPN STD B/N/A FRACTION,5/23/B4,»E BTL034

Conpound Noi 27Conpound Nann 2,4-DinethylphenolBean Nunben 933Retention Tine, 12.37 nin,Ariai 93553Concentration. 44.40 UC/ML

.,021050»$ ..Q - V-

». **1581 v

./—Hia»

;| S S S S 2 ':* 1582

File >E2219 WPPfl STD WPP« 5TP ,«BPK AD MCM12000-

4III8-

4480ft

4666ft

8MM-

9260ft•AAAAEvvev

t460t

2660*

1666*

1260ft

686*

466*

*

65

' (6 '

ATe*r

10699 v,J,CA ,.,,„.„

>/" iScan 1808M'NMf.

177

(64

06' ' '100' ' 126 ' 'lie '168 ' 166 ' 200' ' 22C

>•

<e

•70

46

«0

i*•30

•29

•16

Data Fill i >E2219nU3Nann SOPPM CTDMilCi SOPPM 6TD B/N/A FRACTION,5/23/84,OE BTLI34

Cenpound No, 42Conpound Nanei DiethvX phthalateBean Nunbiri 1008Retention Tine, 20.3B nin.Ariai 270706Concentrationi 52.16 UC/ML

021052

1583

t

Fill >£2219 BBPPH STD 60PPR its ,.„Bpk Rb 6032 1X.

411*

4406400*

3606

326*,

266ft

246ft

266*

1600;

1266

88ft

46*

67

'

71

* • i • . • i1 66

I

B'N Scan 307031,93 Mri,

167^

267

X

•90

•66

•TO

40

•60

Me

>o

•10

'ee' ' 'lie' ' 'lie' ' 'lie' ' 'lie' ' 'ise' ' '200'

Data File i >E2219nU3Nanei SOPPM STDHiftci 50HPM 8TD 6/N/A FRACTION,S/23/64,*E BTL«34

Conpound Not 6VConpound Nann bit(2-Sthylhe«yl)phthalateBean Nunben ,5070Retention Tinen Si ,93 nin,Ariai 21960Concentration! 46.64 UC/ML

021053

O • ;jtf1584 v-'

Total Ion ChromatogramFile >C2m 40.0-4(0.0 MU

Data File, >E2191,,U3Nanei SOPPM STDMiBC, SOPPM STD HTLI11

Id Filei IFBENTitle, IFB P.E.QUANT ID FILE.,,,UWC.,631114Last Calibration, 840522 1S,4B

Operator ID, WU9928Qaunt Tine, 840522 12,55

021054

1585

aFile >E!!191Bpk flb 13

1306*

1200*

1100*

10000-

9008"

640*

7006-

6000.

6000-

400*

3000.

2006-1

100*0.

264EClPPM STU S6PPM STD teiC4>n 713

79y

51/

6365

' i'e 7'o '

90jf

09

139 9

fT

F1"8 'J9Q

40

•70

40

40

M6

•?•«'

i'8

•10

lL"j"" '" 'ie'ii' " '""

Data File, >E219t, ,113Nane, SOPPM STDMi»c, SOPPM STD 6TL«U

Conpound No, 12Conpound Nanei 2-MethylphenolScan Nunben 713Retention Tine> 10.3B nin,Areai 50349Concentration, 52,74 UU/ML

021055

1586

O

File >E2IBpk Rb 19

10000'•

1600*

1400*

1200*

10000-

600*

600*

400*

•200*

0-4

91 60PPM STD G0PPM STD Si200 e.;

66

61 65 6340 47 \ \ \

0 ' 4V ' 4V 62 6'6 ' 6B 64

74 1

6I6''712''>16''8'0'I'0V'9P8'1V2

an 6393 min.100

'.

40

•70

40

40

MO

•30

iee••10

*Q

O Data File, >E2l9inU3w Nanei SOPPM STD

Misc, SOPPM STD BTLI11

Conpound No, 9Conpound Nanii PhenolScan Nunber > 539Retention Tinn 8,79 nin,Areai 79664Concentration, 51,02 UG/ML

021056>' - ' • r/':u'» iO, • \j J

r1587

File >E21Bpk Rb IS

1S000-1400*13000-

1200*

1100*10000

900*

7000-

600*

4000-300*

20ee-1000-

0-

91261

43 «/

4'4 ' 4*8

60PPM STD

t

fi

' BY ' 8i- ' W '

3t

64

01,??

' V0' ' '?'&' ' W ' 80' ' OV ' '0'0' ' 92

n S6»Air,.;100

•90

•OC

70

40

40

MO

•30

•eo

•10

'•0

Data File. >E2i91,iU3Nane, SOPPM STDMi«c, SOPPM STD BTLH1

Conpound No, 4Conpound Nane, bit(S-Chloroethyl) etherScan Nunber, 559Retention Tine, 8,97 nin.Area, 60833Concentration, 51.86 UG/ML

021057

1588

n

FU« >E21Bpk Rb 20

80000

10800

1(000;

1400*

1200ft

1000*

8006;•

600*

406*

2000-

0-

91266

WppH sT» Mpph'STB $10:

;

6143

Ur

163X

'"'6'0'

70

'7

1,,..,. ..,.1. .

^

79

90

{,.,,( , t , -,.

Sn 759filn.•100

•98

|00

•70

•60

40

;40

•30

I*8

••18

Data File, >E2191,,U3Nane, SOPPM STDMi«ci SOPPH STD *TL«11

Conpound No, 13Conpound Nanei 4-MethylphenolScan Nunber, 759Retention Tine, 10.60 nin,Areai B0156Concentrationi 53,35 UG/ML

021058

1589

o

o

N >

.................... .T. .. .. ,..... ..ss

\ : 021059r::i»

N N N « » n •*

1590

I ' 1591 1

48,00

48,00

44,00

42.00

40,00

41,00

48,00

44,00

142,00 K S g

*• G U*m MA *^ O•16,00 c b.H £•14,00

o•18.00 g |

•«.oo o

4,000 a |

•4,000

4.000

•0.00002J.OBO

5f M f* fc 4

A/D Count! VJ

48.00

1.00

[44.00

40.00

48,00

44.00

42,00

40.00

•11,00

•11.00

•14.00

•12,00

•10.00

4.000

I021061, f' i •

Oounu

48.00

48.00

44,00

42,00

40,00 >•"S-a

*" 5148,00 e|

44,00

42,00

•18,00 fj U.^ no

'18,00 "c t

14.00

•12,00

•10,00

4,000

4,000

•4.000

4,000

fl.OCO

1021062

1593A/DCounto

48.00

00

44,00

42,00OL0< ____"M "•—— - ————————••

40,00

0MB-

O

1594A/D Count*

-S8.00 g

44,00

42,00

40,00

-18,00 £ i,JL8-u.oo r|M £

-14.00 ing'12.00 g g

10,00 » ..

-8.000 g£

4.000 U S

-4,000

•8,000 021063000 r

r.V

S

48,00

48.00

44.00

42.00

40,00 >'

48.00 g,

48.00 g

•84.00 f i

42,00

h20,00

18,00 ^s no

-18.00

-14.00in

12.00 P

10,00

4,000

4,000

•4.000

*00° 0210610.000

1595A/D Counts

17.44 •BUT'

48,00

48,00

44,00

40,00

48,00

48,00

-24,00

142,0081.74

1,000

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g

-18.00 i * U.oo

•18,00 ?£M £

•14,00 m* ?9

•12,00

10,00

4.000

4.000 o' £5000 OH

A4,000

1596 •

-81,00

,00

I • IW I

•14.00

•12.00

-10.00

4,000

•4,000

4,000

•0,000

s021066

A/DOBunt6

A/D counti

48.90

48,00

44,00

42,00

40,00 >~

'•" Si48,00 N|

44,00

42,00

40,00

•"•"" g•18,00 i•14,00

•18,00 |

10,00 I

4.000 |

4.000

•4,000

4,000

4.000

II ' 1598

—jXEflagggl v "l— ™ """" ^ «l.81BJB B BB

•*" — ~m* 4**" """"" """" BSP-S8WO ——

'

,

•88.00

•88.00

44.00

42.00

40,00

48,00

48.00

•24.00

42.00 8s

40.00

•18.00

•16,00

•14,00

•12.00

•10.00

4,000

4,000

1-4.000

4.000

1 • 1599 1A/D Counti

Lg|i"ii»' i&si ;*ia* oB n0) Jufll U•n 0

0• Tl

Sgwe0 ..vl UonVl Tl

o an CCI

021Q68

':3<',V

tt.0CM-

^•wSS— 3B.n •• •••" "••mo •••••••M

•144 MM

.

iK

?

r • • • • 1 • • • ' i

48.00

•88.00

44,00

42,00

40.00

• tt AA

•88.00

•24.00^

42.00 |5

40.00 |

B18«00 s(5•18.00

•14,00

•12.00

10.00

4.000

4.000

,.000

4.000

•0,000

, 1 • 1600 SA/D Count!

,

i<rn&wg5W*$oi£mn zVIJUCD§f n"8

44•J ..•Q n£C0JD 0

SiO• Oin op n

10 aAl * *Is• a|tt

021069f\ '"* i

1601A/D counts

•88.00

•88.00

44.00

*" II(40.00 >H

X ti

(-88.00 g» X

1-24.00 V gM

•82.00

•20.00

•18.00 *

•18.00

14.00

12.00

10.00

(4,000 iu |n ff

°°° I•8.000

000

Bffr'NEt

1602A/D Count!

I

48.00

48.00

44,00

42.00

40.00

41.00

•28.00

44,00

42.00 | i g

40.00 J " f>^ -a nft <PfiiB,oo a

•14,00

•18,00

•10,00

4.000

4.000

,000

[4.000

4.000

1,00

44.00

41.00

M WM —jge gpljBS. <*'°°1.00

1,00

-j*

I . 1 6 0 3A/D count.

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Date post:	29-Jul-2018
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