DATE : June 22, 1995 · TO: Cynthia Caporale ESAT Regional Project Officer THROUGH: Dale S. Boshart...

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

"!--.vr REGION HI% i CENTRAL REGIONAL LABORATORYI 201 DE fflGHWAY ^ ^

ANNAPOLIS. MARYLAND 214O1

DATE : June 22, 1995

SUBJECT: Region III Data QA Review

FROM : Cynthia C. CaporaleRegion III ESAT RPO (3ES30)

TO : Lisa MarinoRegional Project Manager (3HW42)

Attached is the organic data validation report for the Koppers Co.Fac. Plant Site (Case 23482) completed by the Region IIIEnvironmental Services Assistance Team (ESAT) contractor under thedirection of Region III ESD.

If you have any guestions regarding this review, please call me at(410) 573-6832.

Attachment

cc: Chris Burns, TetraTech

TID File: 03950610

,-. - Printed on Recycled Paperi 3b

Environmental Sen/ices Assistance Teams Phone: (410) 268-7705Region 3 Fax: (410) 263-84721419 Forest Drive. Suite 104Annapolis, Maryland 21403

DATE: June 16, 1995

SUBJECT: Level Ml Organic Data Validation for Case 23482(SDG CNF40)Site: Koppers Co. Factory Plant.

FROM: Byron L. Munro r» Mahboobeh MecanicOrganic Data Reviewer Senior Oversight Chemist

TO: Cynthia CaporaleESAT Regional Project Officer

THROUGH: Dale S. BoshartESAT Team Manager

OVERVIEW

Case 23482 consisted of twelve (12) aqueous samples, submitted toCompuChem Environmental Corp. (COMPU) for volatile, semivolatileand pesticide/PCB analyses. The sample set included three (3)trip blanks which were analyzed for volatile only and one (1)field blank. Only samples CMW44 and CNA91 were analyzed forpesticide/PCBs. No field blank was analyzed for pesticide/PCBs.The samples were analyzed as a Contract Laboratory Program (CLP)Routine Analytical Service (RAS) according to Statement of Work(SOW) OLM03.1.

SUMMARY

All samples were successfully analyzed for all target compounds.All instrument and method sensitivities were according to the CLPRAS protocol.

The validation was performed according to the level Ml procedure.Quality control measures evaluated were limited to the Ten (10)Day Health Advisory Limits, sample paperwork, retention time,mass spectra, chromatograms , and laboratory and field blanks.

A R 3 U 8 I 3 6

page 2 of 3

Minor Problem

o The pesticide/PCB re-extraction of samples CMW44 exceeded thetechnical holding time of seven (7) days by twenty-two (22)days. The initial results were not reported by the laboratorydue to surrogate recovery outliers with the associated methodblank. The positive result was qualified "JM and thequantitation limits were qualified "UJ" on the Form I.

o In the semivolatile analysis of sample CNA93, the laboratoryused the "X11 qualifier to indicate indistinguishable coelutingisomers between the benzo(b)fluoranthene and benzo(k)fluor-anthene. Both compounds were qualified "N" by the datareviewer.

o The "P" qualifier used on the pesticide/PCB Form Is denotes apercent difference (%D) greater than 25 percent (>25%) betweenthe reported results on the two (2) columns used for theanalyses. These results were qualified "J" on the Form Is.

NOTES

o Methylene chloride and toluene were detected in the laboratorymethod and field blanks at a maximum concentration of 4 J ug/Land 1 J ug/L, respectively. Samples with concentration ofmethylene chloride (common laboratory contaminant) less thanten times (<10X) the blank concentration and with concent-ration of toluene less than five times (<5X) the blank concen-tration have been qualified "B" on the Form Is.

o In the 5X diluted analysis of sample CNA93, toluene exceededthe instrument's analytical range. The sample was reanalyzedusing a 7.7X dilution to bring the on-column amount intorange. Results reported from the diluted analysis was markedwith an asterisk "*" on the original Form I.

o In the semivolatile analysis of samples CNA91, CNA93 andCNA94, several compounds exceeded the linear calibration rangein their initial 15X dilution and were qualified "E" by thelaboratory. These samples were reanalyzed at 30X, 600X and250X dilution, respectively, to bring these compounds withinrange. Results for these compounds were reported from thediluted analysis and marked with an asterisk {*) on the FormIs. -

AR308I36K

page 3 of 3

All data for Case 23482 were reviewed in accordance with theLevel MI Innovative Approach for Validation of Organic Data inconjunction with the National Functional Guidelines forEvaluating Organic Analyses with modification for use withinRegion III.

ATTACHMENTS

1) Appendix A - Glossary of Data Qualifiers2) Appendix B - Results as Reported by the Laboratory and

Qualified by the Data Reviewer for All TargetCompounds

3) Appendix C - Support Documentation

DCN:BM506A3.KFP

AR308I37

Appendix AGlossary of Data Qualifiers

A R 3 U 8 J 3 8

GLOSSARY OF DATA QUALIFIER CODES (ORGANIC)

CODES RELATED £O_ IDENTIFICATION(confidence concerning presence or absence of compounds)

U = Not detected. The associated number indicatesapproximate sample concentration necessary to bedetected.

NO CODE « Confirmed identification.

B = Not detected substantially above the level reported inlaboratory or field blanks.

R = Unusable result. Analyte may or may not bepresent in the sample. Supporting data necessary toconfirm result.

N = Tentative identification. Consider present.Special methods may be needed to confirm its presenceor absence in future sampling efforts.

CODES RELATED TO OUANTITATION(can be used for both positive results and samplequantitation limits):

J = Analyte present. Reported value may not beaccurate or precise.

K - Analyte present. Reported value may be biasedhigh. Actual value is expected to be lower.

L = Analyte present. Reported value may be biased low.Actual value is expected to be higher.

UJ = Not detected, quantitation limit may be inaccurate orimprecise.

UL » Not detected, quantitation limit is probably higher.

CODES

NJ - Qualitative identification questionable due to poorresolution. Presumptively present at approximatequantity.

Q = No analytical result.

AR3G8139

Appendix BResults Reported by the Laboratory and Qualified by the Reviewer

Based on Level Ml Validation

AR308UO

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

CMW42Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004

Lab Code: COMPU Case No.: 23482 SAS No.: SDG No.: CNF40

Matrix: (soil/water) WATER Lab Sample ID: 706760 //L?

Sample wt/vol: 5.0 (g/mL) mL Lab File ID: CN006760C52

Level: (low/med) LOW Date Received: 04/25/95

% Moisture: not dec. ______ Date Analyzed: 04/28/95

GC Column:DB624 ID: 0.53 (mm) Dilution Factor: 1.0 .

Soil Extract Volume:______(uL) Soil Aliquot Volume: ______(uL)

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) ug/L Q

74 -87-3-------- - Chlorome thane74-83-9--------- Bromome thane75-01-4---------Vinyl Chloride75-00-3-------- -Chloroe thane75-09-2-------- -Methylene Chloride

75-15-0---------Carbon Disulfide75 -35 -4 ---------1,1 -Dichloroethene75-34-3---------1, 1 -Dichloroethane540-59-0- -------1,2-Dichloroethene (total) _67- 66 - 3 -------- -Chloroform107-06-2--------l,2 -Dichloroethane78-93-3------- - -2 -Butanone71-55-6---------l,l,l-Trichloroethane56-23-5------- - -Carbon Tetrachloride75-27-4-------- -Bromodichlorome thane78-87-5---------1, 2 -Dichloropropane10061-01-5----- -cis -1,3 -Dichloropropene ____79 - 01 - 6 -------- -Trichloroethene124-48-1------- -Dibromochl or ome thane79-00-5---------1,!, 2 -Trichloroethane

10061-02-6---- --trans- 1,3 -Dichloropropene7 5 - 2 5 - 2 - - - - - - - - - Bromof orm108-10-1--- -----4-Methyl-2-Pentanone5 9 1 - 7 8 - 6 - - - - - - - - 2 - Hexanone127-18-4------ - -Tetrachloroethene

108-88-3--------Toluene108-90-7- -------Chlorobenzene100-41-4--------Ethylbenzene100-42-5--- -----Styrene1330-20-7 ————— Xylene (Total)

10101010

10101010101010101010101010101010101010101010101010101010

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TRIP BLANK

A R 3 C 8 I I + I25452 CNF49 SflWPLE DPTP PPCKPGE 39


CMW43Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004

Lab Code: COMPU Case No.: 23482 SAS No. : SDG No. : CNF40 ^

Matrix: (soil/water) WATER Lab Sample ID: 706764




GC Column:DB624 ID: 0.53 (mm) Dilution Factor: 1.0


CONCENTRATION. UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) ug/L

74-87-3---------Chloromethane__74-83-9---------Bromomethane75-01-4---------Vinyl Chloride"75-00-3---------Chloroethane75-09-2---------Methylene Chloride]67-64-1---------Acetone75-15-0---------Carbon Disulfide________75-35-4---------1,1-Dichloroethene_____75-34-3---------1,1-Dichloroethane540-59-0--------1,2-Dichloroethene (total!67-66-3---------Chloroform __107-06-2--------1,2-Dichloroethane7S-93-3---------2-Butanone71-55-6---------l,l,l-Trichloroethane_56-23-5---------Carbon Tetrachloride_|75-27-4---------Bromodichloromethane_78-87-5---------l,2-Dichloropropane10061-01-5------cis-l,3-Dichloropropene79-01-6---------Trichloroethene124-48-1--------Dibromochloromethane_7 9 - 0 0 - 5 - - - - - - - - -1,1,2 - Tr ichl oroe t hane_71-43-2---------Benzene10061-02-6------t rans-1,3-Dichloropropene75-25-2---------Bromoform108-10-1--------4-Methyl-2-Pentanone_591-78-6--------2-Hexanone127-18-4--------Tetrachloroethene

108-88-3--------Toluene_____108-90-7--------Chlorobenzene100-41-4--------Ethylbenzene_J100-42-5--------Styrene1330-20-7—————Xylene (Total)

10101010CZ10101010101010101010101010101010101010101010101010101010

8

Review: Ml Level DVQ = Data ValidatorQualifier

Location: KOP-MW-27A FORM I VOA OLM03.0

23482 CNF4& SPM^LF PPTP PPCKPGF 46

LA EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004CMW44



Sample wt/vol: 5.0 (g/mL) mL Lab File ID: CN006768B52






—————————————————————————— -

74-87-3-------- -Chloromethane74-83-9-------- -Bromomethane75-01-4---------Vinyl Chloride75-00-3 ---------Chloroethane75 -09-2-------- -Methylene Chloride67-64-1-------- -Acetone75-15-0----- ----Carbon Disulfide75-35-4---------l,l-Dichloroethene75-34-3- --------1,1-Dichloroethane540-59-0--- -----1,2-Dichloroethene (total) _67-66-3--- ------Chloroform107-06-2----- ---1,2-Dichloroethane78-93-3------- - -2 -Butanone71-55-6---------l,l,l-Trichloroethane56-23-5--------- Carbon Tetrachloride75-27-4--------- Bromodichlorome thane78-87-5---------l,2 -Dichloropropane10061-01-5--- ---cis -1,3 -Dichloropropene/ y u J. o — — — — — — — — j_j_ xiîixuiycunciic124 -48 - i------- -Dibromochloromethane79-00-5---------l,l,2 -Trichloroe thanef ± I H jl*X14dl~XlL«

10061-02 -6- -----trans-1, 3 -Dichloropropene75-25-2---- - - - - -Bromof onti108-10-l--------4-Methyl-2-Pentanone591-78-6----- ---2-Hexanone127-18-4------- -Tetrachloroethene79_34_5____--__-l/l/2,2 -Tetrachloroe thane108-88-3------- -Toluene108-90-7-------- Chlorobenzene100-41-4--------Ethylbenzene100-42-5--------Styrene1330-20-7-------Xylene (Total)

10101010OL10101010101010101010101010101010101010101010101010101010

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Location: KOP-MW-37A FORM I VGA —.03.0

AR308U323482 CNF4Q SPMPLE DPTP PPCKPGE 53


Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004CNA89

Lab Code: COMPU Case No.: 23482 SAS No.: SDG No.: CNF40 /








74-87-3-------- -Chloromethane74 -83-9-------- -Bromomethane75-01-4---------Vinyl Chloride75-00-3--------- Chloroe thane75-09-2 -- -------Methylene Chloride67-64-1--- ------Acetone75-15 -0-- -------Carbon Disulfide75-35-4---------1, 1 -Dichloroethene75-34-3---------1, l -Dichloroethane540-59-0--- -----1,2-Dichloroethene (total)67-66-3-------- -Chloroform107-06-2--------1, 2 -Dichloroethane78-93-3-- -------2-Butanone71-55-6---------1, 1, 1-Trichloroethane56-23-5-------- -Carbon Tetrachloride75-27-4-------- -Bromodichloromethane78-87-5---------l,2 -Dichloropropane10061-01-5------cis-l/3-Dichloropropene79-01-6-------- -Trichloroethene124 -48-1---- - -- -Dibromochlorome thane79-00-5---------l,l,2-Trichloroethane

10061-02 -6- ---- -trans-1 , 3 -Dichloropropene75 -25 - 2 -------- -Bromoform108-10-l--------4-Methyl-2-Pentanone591-78 -6- ----- --2-Hexanone

79-34-5---------l,l,2,2-Tetrachloroethane

100-41-4--------Ethylbenzene100-42-5--------Styrene1330-20-7-------Xylene (Total)

10101010

10101010101010101010101010101010101010101010101010101010


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Review: Ml Level DVQ - Data ValidatorQualifier —>

Location: KOP-TB-03 FORM I VOA -—————————————""OLM03.0

TRIP BLANK A R 3 0 8 I M»

* CNF4Q SPMPLE DPTP PPCKPGE 62




Location: KOP-MW-8S FORM I VOA

AR308U523482 CNP49 SPMPLE DPTP PPCKPGE









74 - 87-3 -------- -Chloromethane74-83-9-------- -Bromomethane75-01-4---------Vinyl Chloride75-00-3-------- -Chloroe thane75-09-2--------- Methyl ene Chloride

75-15-0-------- -Carbon ' Disulf ide75-35-4---------1, 1 -Dichloroethene75-34-3---------1, 1 -Dichloroethane540-59-0------- -1,2-Dichloroethene (total) _67- 66 -3 ---------Chloroform107-06-2--------1, 2 -Dichloroethane

71-55-6---------l,l,l-Trichloroethane56-23-5-------- -Carbon Tetrachloride75-27-4-------- -Bromodichloromethane78-87-5---------1, 2 -Dichloropropane10061-01-5------cis-l,3-Dichloropropene79-01-6--------- Tr ichloroe thene124 -48 - 1------- -Dibromochloromethane79-00-5---------l,l,2-Trichloroethane

l0061-02-6------trans-l,3-Dichloropropene7 5 - 2 5 - 2 - - - - - - - - - Bromo f orm

79-34-5---------l,l,2, 2 -Tetrachloroethane

100-41-4--- -----Ethylbenzene100-42 -5-- ------Styrene!330-20-7-------Xylene (Total)

10101010C210101010101010101010101010101010101010101010101010101010

———— — "n


fin i

3-' «


CNA91Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004









74-87-3------74-83-9------75-01-4------75-00-3------75-09-2------* W -/ £*

67-64-1------75-15-0------75-35-4- ————75-34-3-- ———540-59-0-----

T f\ *"! f\ /* O107-06-2-----

71-55-6 —————56-23-5--- ——*7C O*7 A - - -

10061-01-5---

1 74.-4S-1- ----79-no-5------7T ,4-3-2------10061-02-6 ——75-95-2--- ---108-10-1-- ——

1 77-1 8-4-----79-34-5------1 -J X *J

100-41-4-----100-42-5 ————

- - - Chloromethane- - -Bromomethane---Vinyl Chloride- - -Chloroethane

---Carbon Disulfide- - - 1 , 1 -Dichloroethene- - -1 , 1 -Dichloroethane- - - 1 , 2 -Dichloroethene ( total ) _- - -Chloroform---1,2 -Dichloroethane---2-Butanone---1,1, 1-Trichloroethane---Carbon Tetrachloride- - -Bromodichloromethane- - - 1 , 2 -Dichloropropane

- - -Dibromochloromethane- - - 1 , 1 , 2 -Trichloroethane

- - - trans -1,3 -Dichloropropene---Bromoform

- - -Tetrachloroethene---1,1,2, 2 -Tetrachloroethane- - -Toluene- - -Chlorobenzene- - -Ethylbenzene---Styrene---Xylene (Total)

10101010O:10101010101010101010101010101010101010101010

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1A . EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET


Lab Code: COMPU Case No.: 23482 SAS No.: SDG No.: CNF40 + O*








W

74-87-3--------- Chlorome thane74-83-9-------- -Bromome thane75-01-4---------Vinyl Chloride7 5 - 0 0 - 3 --------- Chloroe thane75-09-2-------- -Methylene Chloride

75-15-0- --------Carbon Disulfide75-35-4---------1, 1 -Dichloroethene75-34-3---------1, 1 -Dichloroethane540-59-0- -------1,2-Dichloroethene (total) _67- 66 -3 ---------Chloroform107-06-2--------1, 2 -Dichloroethane78-93-3---------2-Butanone71-55-6---------l,l,l-Trichloroethane56-23-5-------- -Carbon Tetrachloride75-27-4-------- -Bromodichloromethane78-87-5-- -------1,2-Dichloropropane10061-01-5- -----cis-1, 3 -Dichloropropene ____79-01-6--------- Tr ichloroe thene124 -48-1------- -Dibromochlorome thane79-00-5- ------- -1 , 1 , 2 -Trichloroethane

10061-02 -6- - - - - -trans-1 , 3 -Dichloropropene __75-25-2--- ------Bromoform108-10-1- -------4-Methyl-2-Pentanone5 9 1 - 7 8 - 6 - - - - - - - - 2 - Hexanone127-18-4------- -Tetrachloroethene79-34-5---------1, 1,2, 2-TetrachlorbetEahe108-88-3--------Toluene

100-41-4------- -Ethylbenzene100-42-5--------Styrene1330-20-7- ———— Xylene (Total)

10101010C£10101010101010101010101010101010101010101010101010101010

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23482 CNF49 SPMPLE DPTP PPCKPGE 1Q1



Lab Code: COMPU Case No.: 23482 SAS No.: SDG No.: CNF40~—*





GC Column:DB624 ID: 0.53 (ram) Dilution Factor: 5.0

Soil Extract Volume:______(uL) Soil Aliquot Volume: (uL)

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) ug/L

74-87-3---------Chloromethane_74-83-9---------Bromomethane__75_Oi-4---------Vinyl Chloride,75-00-3---------Chloroethane75-09-2---------Methylene Chloride,67-64-1---------Acetone75-15-0---------Carbon Disulfide75-35-4---------1,1-Dichloroethene______75-34-3---------1,1-Dichloroethane540-59-0--------l,2-Dichloroethene (total)67-66-3---------Chloroform107-06-2--------l,2-Dichloroethane7S-93-3---------2-Butanone71-55-6---------1,!,1-Trichloroethane56-23-5---------Carbon Tetrachloride_]75-27-4---------Bromodichloromethane_78-87-5---------1,2-Dichloropropane10061-01-5------cis-1,3-Dichloropropene,79-01-6---------Trichloroethene124-48-1--------Dibromochloromethane_79-00-5---------1,!,2-Trichloroethane_71-43-2---------Benzene10061-02-6------trans-1,3-Dichloropropene,75-25-2---------Bromoform108-10-l--------4-Methyl-2-Pentanone_591-78-6--------2-Hexanone127-18-4--------Tetrachloroethene79-34-5---------1,1,2,2-Tetrachloroethane_108-88-3--------Toluene108,90-7--------Chlorobenzene,100-41-4--------Ethylbenzene^100-42-5--------Styrene1330-20-7-------Xylene (Total)

50


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74 - 8 7 - 3 - - - - - - - - - Chl orome t hane74-83-9-------- -Bromomethane75-01-4---------Vinyl Chloride75-00-3--------- Chloroethane75-09-2-------- -Methylene Chloride

75-15-0---------Carbon Disulfide75-35-4--- ------1,1 -Dichloroethene75-34-3---------1, 1-Dichloroethane540-59-0--- -----1,2-Dichloroethene (total) _67-66-3---- -----Chloroform107-06-2--------l,2 -Dichloroethane7S-93-3---------2- But anone71-55-6---------1,!, 1 -Trichloroethane56-23-5-------- -Carbon Tetrachloride75-27-4------- - -Bromodichloromethane78-87-5---------l,2 -Dichloropropane10061-01-5--- ---cis-1, 3 -Dichloropropene79-01-6-------- -Trichloroethene124 -48 - i------- -Dibromochloromethane79-00-5---------l,l,2-Trichloroethane

10061-02-6------trans-l,3-Dichloropropene75-25-2--------- Bromof orm108-10-1--------4 -Methyl - 2 - Pent anone5 9 1 - 7 8 - 6 - - - - - - - - 2 - Hexanone127-18-4------- -Tetrachloroethene79-34-5---------l,l,2,2-Tetrachloroethane108-88-3--------Toluene108-90-7------- - Chlorobenzene100-41-4--------Ethylbenzene

1330-20-7 ————— Xylene (Total)

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Lab Code: COMPU Case No. : 23482 SAS No. : SDG No. : CNF40

Matrix: (soil/water) WATER Lab Sample ID: 706132 /\y






CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) ug/L Q j>*y

"•\i74-87-3-------- -Chloromethane74-83-9-------- -Bromomethane75-01-4---------Vinyl Chloride75-00-3-------- -Chloroethane75-09-2-------- -Methylene Chloride

75-15-0---- -----Carbon Disulfide75-35-4---------1, 1 -Dichloroethene75-34-3---------1,! -Dichloroethane540-59-0--------l,2-Dichloroethene (total)67-66-3--------- Chloroform107-06-2--------1, 2 -Dichloroethane78 -93-3-- ------ -2 -Butanone71-55-6---------1, 1, 1-Trichloroethane56-23-5-------- -Carbon Tetrachloride75-27-4-------- -Bromodichloromethane78-87-5---------l,2 -Dichloropropane10061-01-5------cis-l,3 -Dichloropropene79-01-6-------- -Trichloroethene124 -4 8 -i------ - -Dibromochloromethane79-00-5---------1,!, 2 -Trichloroethane

10061-02-6----- - t rans -1,3- Dichloropropene __7 5 - 2 5 - 2 - - - - - - - - - Bromo f orm108-10-l--------4-Methyl-2-Pentanone591-78-6-T------2-Hexanone127- 18 -4 - ------ -Tetrachloroethene79-34-5---------l,l,2,2- Te t rachloroe thane

108^90-7------- - Chlorobenzene100-41-4------- -Ethylbenzene100-42-5- -------Styrene1330-20-7-------Xylene (Total)

10101010

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23482 CNF40 SPMPLE DPTP PPCKPGE


CNF41Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004



Sample wt/vol: 5.0 (g/mL) mL Lab File ID: CR006136C52






74-87-3-------- -Chloromethane74-83-9-------- -Bromomethane75-01-4---------Vinyl Chloride75-00-3--------- Chloroe thane75-09-2-------- -Methylene Chloride

75-15-0- --------Carbon Disulfide75-35-4---------1, 1 -Dichloroethene75-34-3---------1, 1 -Dichloroethane540-59-0--------l,2-Dichloroethene (total)67-66-3- --------Chloroform107-06-2----- ---1,2-Dichloroethane7S-93-3---------2- But anone71-55-6---------l,l,l-Trichloroethane56-23-5------- - -Carbon Tetrachloride75-27-4-------- -Bromodichloromethane78-87-5---------l,2- Dichloropropane10061-01-5------cis-l, 3 -Dichloropropene79-01-6-------- -Trichloroethene124 -48 - i------- -Dibromochloromethane79-00-5--- ------1,1,2-Trichloroethane

10061-02-6------trans-l, 3 -Dichloropropene7 5 - 2 5 - 2 - - - - - - - - - Bromo f orm108-10 -l--------4-Methyl-2-Pentanone

127-18-4------- -Tetrachloroethene79-34 -5---------1, 1,2,2-Tetrachloroethane108- 88 -3 --------Toluene

100-41-4------- -Ethylbenzene100-42-5--- -----Styrene1330-20-7-------Xylene (Total)

10101010

10101010101010101010101010101010101010101010101010101010


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Location: KOP-MW-7B FORM I VOA w**-.WJ.0

AR308I5I23482 CNF40 SPMPLE DPTP PPCKPGE . 20J


CNF43Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004

Lab Code: COMPU Case No.: 23482 SAS No.: SDG No.: CNF40 ^_








74-87-3-- ———74-83-9------75-01-4------75-00-3 —————TC flQ O_-._

67-64-1------75-15-0------75-35-4------75-34-3 ——— --540-59-0 —— --67-66-3------

71-55-6- ————56-23-5 ——— --

10061-01-5 ——TO A1 _£_.._ _ _

1 94-48 -1 -_--<6*± "TO J.

79-00-5 —————71-43-2------t -k A — ' **

10061-02-6---TC DC O — _ —

108-10-1-----CQ1 F7Q_£_— __1 97-1 O_4___ _JLZ / — J-O *± —79-34-5 —————

100-41-4 ————100-42-5 ————1330-20-7 ———

- - -Chloromethane- - -Bromomethane---Vinyl Chloride- - -Chloroethane---Methylene Chloride

L \X*l»ll_ VAA\^

---Carbon Disulfide---1, 1 -Dichloroethene---1, 1-Dichloroethane- - - 1 , 2 -Dichloroethene ( total ) _---Chloroform---1,2 -Dichloroethane- - - 2 - But anone---1, 1, 1-Trichloroethane---Carbon Tetrachloride- - -Bromodichloromethane---1,2 -Dichloropropane- - -cis - 1 , 3 -Dichloropropene ____

- - -Dibromochloromethane---1,1,2 -Trichloroethane

T-) —— __________ucii i mm---trans-1, 3 -Dichloropropene---Bromoform- - - 4 -Methyl - 2 - Pentanone

- - -Tetrachloroethene---1,1,2,2 -Tetrachloroe thane- - -Toluene

—— Xylene (Total)

10101010d101010101010101010101010101010101010101010101010101010-10


Review: Ml Level DVQ = Data ValidatorQualifier -

Location: KOP-MW-7A FORM I VOA OLMOj.O

HR308I52COMP; r noro portsafzc ? 1

06/15/95 13:49 7T919 406 2491 COMPUCHEM ENV BI002/002

IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

CNF41Lab Name: CompuChem Env. Corp. Contract: 68D5Q004


Matrix: (soil/water) WATER Lab sample ID: 706136

Sample wt/vol: 1000 (g/mL) mL Lab File ID: OI006136A21


% Moisture: ____ decanted: fY/N)__ Date Extracted:04/27/95

Concentrated Extract Volume; 1000(uL) Date Analyzed: 04/28/95

Injection Volume: 2 0(uL) Dilution Factor: 1.0

GPC Cleanup: (V/N) N pH: ___


~7>V/D&*1

108-95-2 —————— Phenol111-44-4 ——— — — bis (2-CnTorbethyl) ether95-57-8 ——————— 2-Chlorophenol541-73-1 —————— 1, 3-Dichlorobenzena106-46-7— — • —— 1,4-Dichlorobenzene95-50-1 — - ———— 1, 2-Dichlorobenzene95-4 8-7 ——————— 2-Methylphenol108-60-1 ————— 2 , 2 ' -oxybis ( i-Chloropropane)106-44-5 ————— 4-Methylphenol621-64-7 ————— N-Nitroso-di-n-propy lamine _67-72-1 —— * ——— Hexachloroethane98-9 5-3 ————— -•— Nitr obenz ene78-59-1 —————— Isophorone8 8 -75-5 —————— 2-Nitrophenb 1105-67-9 ————— 2 , 4-Dimethylphenol111-91-1 ————— bis(2-ChloroftthoxyJineQiahe _120-83-2 —————— 2 , 4-Dichlorophenol120-82-1— ———— 1,2,4-Trichlorobenzerie91-20-3™ ——— -Naphthalene106-47-8 —————— 4-Chloroaniline87-68-3 —— — —— Hexachlorobutadiene59-50-7 ————— — 4-Chloro-3-methylphenol ____91-57-6 —— • — - — — 2-Methylnaphthalene

88-06-2 —————— 2 , 4 , 6-Trichlorophenol95-95-4 — - ———— 2,4,5-Trichlorophenol91-58-7 ——————— 2-Oiloronaphthalene88-74-4 —————— 2-Nitroaniline. 131-11-3 —————— Dimethvlphthalate208-96-8 ————— Acenaphthylene606-20-2 ————— 2 , 6-Dinitrotolu*ne99-09-2 —————— 3-Nitroaniline83—32—9 ——————— Acenaphthene

101010101010101010101010101010101010101010101010102510251010102510

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Review: Ml Level FORM I SV-l OIM03.0

Location: KOP-MW-7B

23482 CNF40 SflA/i

1C EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

CNF41Lab Name: CompuChem Env. Corp. Contract: 68D50004



Sample wt/vol: 1000 (g/mL) mL Lab File ID: GH006136A21

Level: (low/med) DOW Date Received: 04/24/95

% Moisture: ____ decanted: (Y/N)__ Date Extracted:04/27/95

Concentrated Extract Volume: 1000(uL) Date Analyzed: 04/28/95

Injection Volume: 2.0(uL) Dilution Factor: 1.0

GPC Cleanup: (Y/N) N pH: ___

CONCENTRATION UNITS:GAS NO. COMPOUND (ug/L or ug/Kg) ug/L Q

51-28-5——————2,4-Dinitrophenol_100-02-7——————4-Nitrophenol____132-64-9——————Dibenzofuran121-14-2——————2,4-Dinitrotoluene84-66-2——————Diethylphthalate7005-72-3—————4-Chlorophenyl-phenylether86-73-7——————Fluorene100-01-6——————4-Nitroaniline534-52-1——————4,6-Dinitro-2-methylphenol86-30-6——————N-nitrosodiphenylamine_(l)_101-55-3——————4-Bromophenyl-phenylether__118-74-1——————Hexachlorobenzene________87-86-5—•—————Pentachlorophenol________85-01-8——————Phenanthrene____________120-12-7——————Anthracene______________86-74-8——————Carbazole84-74-2——————Di-n-butylphthalate206-44-0——————Fluoranthene_____~_129-00-0——————Pyrene85-68-7——————Butylbenzylphthalate91-94-1——————3,3'-Dichlorobenzidine56-55-3——————Benzo(a) anthracene218-01-9—————Chrysene117-81-7—————bis(2-Ethylhexyl)phthalate__117-84-0——————Di-n-octylphthalate____'205-99-2——————Benzo(b) f luoranthene______207-08-9——————Benzo (k) f luoranthene______50-32-8——————Benzo(a)pyrene___________193-39-5——————Indeno (1,2,3-cd)pyrene_53-70-3——————Dibenzo(a,h)anthracene"191-24-2—————Benzo (g,h,i)perylene

25251010101010252510101025101010101010101010101010101010101010

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(1) - Cannot be separated from Diphenylamine

FORM I SV-2 AR308I 51* OLM03. 0

2J4S2 CNF40 SPMPLE DPTP PPCKPGE 671

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SAMPLE NO.




Sample wt/vol: 1000 (g/mL) mL Lab File ID: GH006764B60


% Moisture: _____ decanted: (Y/N)__ Date Extracted:04/30/95





108-95-2--------Phenol111-44-4 ------- -bis (2 -Chloroethyl ) ether95-57-8---------2-Chlorophenol541-73-l--------l,3 - Dichlorobenzene106-46-7- ------ -1,4-Dichlorobenzene95-50-l---------l,2 -Dichlorobenzene95-48-7---------2-Methylphenol108-£0~l--------2,2'- oxyb i s ( 1 - Chlor opropane )106-44-5- -------4-Methylphenol621-64 -7- -------N-Nitroso-di-n-propylamine67-72 - 1 -------- -Hexachloroethane

78-59-1---------I sophorone88-75-5---------2-Nitrophenol105-67-9- -------2, 4-Dimethylphenol111-91-1------- -bis ( 2 - Chloroethoxy ) methane120-83-2--------2/4-Dichlorophenol120-82-l--------l,2,4-Trichlorobenzene91-20-3 ------- --Naphthalene106-47-8--- -----4-Chloroanilme87-68-3-------- -Hexachlorobutadiene59-50-7---------4-Chloro-3-methylphenol91-57-6- --------2-Methylnaphthalene77-47-4 - ------ --Hexachlorbcyclopentadiene88-06-2 —— ------2,4,6-Trichlorophenol95-95-4-- —— ----2,4,5-Trichlorophenol91-58-7------- - -2 -Chloronaphthalene88- 74 -4------- - -2 -Nitroaniline131-11-3------ - -Dimethylphthalate208-96-8 —— -----Acenaphthylene606-20-2----- —— 2,6-Dinitrotoluene99-09-2 ------- --3 -Nitroaniline

1010101010101010101010101010101010101010101010101025102510io102510

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Review: Ml Level FORM I SV-1 OLM03.0DVQ = Data Validator

Location: KOP-MW-27A AR308 I 55 Qualifier

23482 CNF40 SPMPLE DPTP PPCKPGE 35S






Level: (low/tried) LOW Date Received: 04/25/95






100-02-7 ———132-64-9----•t 1 1 A 1121-14-2----84-66-2 -----7005-72-3 ——Of *7"3 *"7So- /J- f -----100-01-6----

86-30-6 -----101-55-3----118-74-1 ———

85-01-8- ———1 1 fl 1*5 T12U-12- /----86-74-8-----R4.-74.-2-----o** / •* ^206-44-0- ——129-00-0----85-68-7-----91-94-1 ————56-55-3 ————218-01-9 ———1 1 *T O T T117-81-7----117-84-0 ———

50-32-8 ————193-39-5 ———53-70-3 ————1 91-24-2----±y ± £* & A

Drtb----2,4 -Dinitrophenol- - - -4 -Nitrophenol- - - -Dibenzof uran- - - - 2 , 4 -Dinitro toluene- - - -Diethylphthalate- - - -4 -Chlorophenyl-phenylether _

- - - -4 -Nitroaniline----4, 6-Dinitro-2-methylphenol _- - - -N-nitrosodiphenylamine { 1 ) _- - - - 4 -Bromophenyl -phenyletEer __

- - - - Pentachlorophenol- - - - Phenanthrene

----Carbazole- - - -Di-n-butylphthalate- - - -Fluoranthene

*, j ÂAX^- - - -Butylbenzylphthalate----3,3'- Dichlorobenz idine

- - - -bis ( 2 -Ethylhexyl ) phthalate- - - -Di -n-octylphthalate- - - -Benzo (b) f luoranthene- - - -Benzo (Jc) f luoranthene- - - -Benzo (a) pyrene- - - - Indeno (1,2, 3 -cd) pyrene

--- -Benzo (q,h, ijperylene

25251010101010252510101025101010101010101010101010101010101010

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'(1) - Cannot be separated from Diphenylamine ^_ „ , . j *.-_OVQ = Data v&liciauorQualifier

FORM I SV-2 ——————————————01M03.0

HR30815623482 CNF40 SPMPLE DPTP PPCKPGE 359











CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) ug/L -wa*i f\ n f\ C *"v T*IIA A.*** *-k i

111 -44 -4 - ------ -bis (2 -Chloroethyl } ether95-57-8-- -------2-Chlorophenol

106-46-7--------l,4-Dichlorobenzene95-50-l---------l,2-Dichlorobenzene95-48-7----- —— -2-Methylphenol108-60-l--------2,2' -oxybis (1-Chloropropane)106-44 -5-- ------4-Methylphenol621-64-7------- -N-Nitroso-di-n-propylamine67-72-1-------- -Hexachloroethane

78-59-l---------Isophorone88-75-5- ------ --2 -Nitrophenol105-67-9--------2,4-Dimethylphenollll-91-l--------bis(2-Chloroethoxy) methane _120-83-2--------2,4 -Dichlorophenol

9 1 - 2 0 - 3 - - - - - - - - - Napht hal ene106-47-8------ - -4 -Chloroaniline87-68-3-------- -Hexachlorobut adiene59-50-7- --------4-Chloro-3-methylphenol91-57-6---------2-Methylnaphthalene

88-06-2---- —— --2,4,6-Trichlorophenol95-95-4--- —— ---2,4,5-Trichlorophenol91-58-7- - —— - —— 2 -Chloronaphthalene8S-74-4---------2 -Ni troani 1 ine13 1-11 -3------- -Dimethylphthalate208-96-8------- -Acenaphthylene606-20-2 ------ --2, 6-Dinitrotoluene99-09-2- --------3-Nitroaniline83-32-9-------- -Acenaphthene

101010101010101010101010101010101010101010101010102510251010102510

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Review: Ml Level FORM I SV-1 OIM03.0DVQ = Data Validator

Location: KOP-MW-37A Qualifier ft ft 3 0 8 t 57

23482 CNF40 SPMPLE DPTP PPCKT 371





Sample wt/vol: ~~"1000 (g/mL) mL Lab File ID: GH006768B60


% Moisture: ____ decanted: (Y/N)__ -Date Extracted:04/30/95





(1) - Cannot be separated from Diphenylamane

51-28-5---------2,4 -Dini trophenol100-02-7- -------4-Nitrophenol

121-14-2 ------- -2, 4-Dinitrotoluene84-66-2---------Diethylphthalatef V V t^ ' Ad *s ~x •4+ » ^ * kr**x_** 4p £*44 *i \~ k****tf

100-01-6--- -----4-Nitroan£line534 - 52 - 1 ----- ---4,6 -Dinitro- 2 -methylphenol _86-30-6-------- -N-nitrosodiphenylamine ( 1 ) _101-55-3--------4 -Bromcphenyl -phenyletEer __

87-86-5--------- Pentachlorophenol85-01-8-------- -Phenanthrene120-12-7------- -Anthracene86-74-8-------- -Carbazole84 - 74 -2 - --=- - - - - -Di-n-butylphthalate206 -44 - o------- -Fluoranthene129-00-0--------Pyrene85-68-7------- - -Butylbenzylphthalate3± y B± x w , *j ^ wi ^ -t- wj j.xx o t*Li\~56-55-3-------- -Benzo (a) anthracene218-01-9----- —— Chrysene117-81-7- ------ -bis (2-Ethylhexyl)phthalate117-84-0------- -Di -n-octylphthalate205-99-2------- -Benzo (b ) f luoranthene207-08-9------- -Benzo Ik) f luoranthene50-32-8---------Benzo (a) pyrene193-39-5- ------- Indeno (1,2, 3 -cd) pyrene53-70-3------- - -Dibenzo ( a , h) anthracene

1C£*J

2510^C21010

- 25ft^251010102510101010101010101010

^ ~"10101010101010

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FORM I SV-2 OIW03.0

AR308I58

IB EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

CNA90Lab Name: COMPUCHEM ENV. CORP. . Contract: 68D50004







Injection Volume: 2.0{uL) Dilution Factor: 1.0



ill-44-4--------bis(2-Chloroethyl)ether_95-57-8---------2-Chlorophenol541-73-l--------l,3-Dichlorobenzene_106-46-7--------1,4-Dichlorobenzene^95-50-l---------l,2-Dichlorobenzene"95-48-7---------2-Me thylphenol108-60-1--------2,2'-oxybis(1-Chloropropane)106-44-5--------4-Methylphenol621-64-7--------N-Nitroso-di-n-propylamine_67-72-1-------- -Hexachloroethane_______"98-95-3---------Nitrobenzene___________78-59-1---------Isophorone88-75-5---------2-NitrophenoT"105-67-9--------2,4-Dimethylphenol111-91-1--------bis(2-Chloroethoxy)methane120-83-2--------2,4-Dichlorophenol120-82-1--------1,2,4-Trichlorobenzene91-20-3---------Naphthalene106-47-8--------4-Chloroaniline87-68-3---------Hexachlorobutadiene """59-50-7------——4-Chloro-3-methylphenol91-57-6-----——-2-Methylnaphthalene77-47-4 ————— -88-06-2------——2,4,6-Trichlorophenol95-95-4--——----2,4,5-Trichlorophenol"91-58-7- —— —— - -2 -Chloronaphthalene88-74-4--- —— ---2-Nitroaniline131-11-3--------Dimethylphthalate_208-96-8--------Acenaphthylene606-20-2--------2,6-Dinitrotoluene99-09-2----——--3-Nitroaniline83-32-9---------Acenaphthene_____

101010101010101010101010101010101010101010101010102510251010102510


Review: Ml Level FORM I SV-IDVQ = vUdator °m03.0

Location: KOP-MW-8S Qualifier

23482 CNF4Q SPMPLE DPTP PPCKPGE 4QQ













51-28-5-----100-02-7 ———112-64-9----J^mJ £t W A -*

1 91-1 4-2----X^X -L*± ft

84-66-2 ————

100-01-6----

86-30-6 ————101-55-3 ———.118-74-1 ———O / — O D D85-01-8 ————i **! A n i ^7lÛ-12- /----86-74-8 ————84-74 O ___-O IA /A A

206-44-0 ———129-00-0----85-68-7 ————91-94-1-----56-55-3 ————

117-81-7 ———

50-32-8 ————193-39-5----*L VW J -* ^

53-70-3 ———

TV)- - - - 2 f 4 -Dinitrophenol- - - -4 -Nitrophenol- - - -Dibenzof uran----2,4 -Dinitrotoluene- - - -Diethylphthalate_ _ _ -4 -Chlorophenyl -phenylether- - - -Fluorene- - - -4 -Nitroaniline----4,6 -Dinitro-2 -methylphenol _- - - -N-nitrosodiphenylamine_ ( 1 ) _- - - -4 -Bromophenyl -phenylether __

- - - - Pentachlorophenol- - - - Phenanthrene- - - -Anthracene

- - - -Di-n-butylphthalate- - - - Fluor anthene

- - - -Butylbenzylphthalate----3,3' -Dichlorobenzidine----Benzo (a) anthracene

----bis (2-Ethylhexyl)phthalate- - - -Di-n-octylphthalate- - - -Benzo (b) f luoranthene- - - -Benzo (k) f luoranthene_-_ -Benzo (a) pyrene----Indeno (1, 2, 3 -cd) pyrene

-- --Benzo (g,h, i)perylene

25251010101010252510101025101010101010101010&10101010101010

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FORM I SV-2 OIM03.0

flR308!60rwC*<lC» COMPf IT HOTO





Sample wt/vol: 1000 (g/mL) mL Lab File ID: GD008425C07







1X?

lll-44-4--------bis(2-Chloroethyl) ether9 5 - 5 7 - 8 - - - - - - - - - 2 - Chl orophenol541-73-l--------l,3 -Dichlorobenzene106-46-7- -------1,4-Dichlorobenzene95-50-l---------l,2 -Dichlorobenzene95-48-7---------2-Methylphenol108-60-l--------2,2' -oxybis (1-Chloropropane)106-44-5- ------ -4-Methylphenol621-64 -7------- -N-Nitroso-di-n-propylamine67-72-1-------- -Hexachloroethane

78-59-1--------- Isophorone88-75-5--- ------2-Nitrophenol105-67-9--------2,4-Dimethylphenol111-91-1- ------ -bis (2-Chloroethoxy) methane120-83-2--------2,4-Dichlorophenol120-82-l--------l,2,4-Trichlorobenzene91-20-3------ —— Naphthalene106-47-8---- —— -4-Chloroaniline87-68-3-------- - Hexachl orobut adi ene59-50-7- --------4-Cnloro-3-methylphenol91-57-6--- ------2-Methylnaphthalene77-47-4-------- -Hexachlorocyclopentadiene88-06-2---------2,4,6-Trichlorophenol95-95-4 —— - ——— 2,4,5-Trichlorophenol91-58-7---------2- Chloronaphthalene8 8 -.74 -4 - --------2 -Nitroaniline131-ll-3--------Dimethylphthalate

606-20-2 ------- -2, 6-Dinitrotoluene99-09-2------ —— 3 -Nitroaniline

150150150150150150150150150150150150150150150150150

^ _ 150

150

150*150380150380150r 25)150380Q20]

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Review: Ml Level FORM I SV-1 OIW03 . 0DVQ = Data ValidatorLocation: KOP-MW-8A

23482 CNF40 SPMPLE DPTP PPCKPGE 412

1C , EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET




Sample wt/vol: 1000 (g/mL) mL Lab File ID: GD008425C07







51-28-5---------2,4-Dinitrophenol100-02-7- -------4- Ni t r ophenol132-64-9------- -Dibenzof uran121-14-2---- —— -2,4-Dinitrotoluene84-66-2------ —— Diethylphthalate7005 -72 -3 - - - - - - -4 -Chlorophenyl-phenylether _86-73 -7---------Fluorene100-01-6--------4-Nitroaniline534-52-l--------4,6 -Dinitro- 2 -methylphenol _86-30-6-------- -N-nitrosodiphenylamine_ ( 1 ) _101 - 55 - 3 -------- 4 -Bromophenyl -phenylether __

87-86-5 -------- -Pentachlorophenol

86-74-8------- - -Carbazole84-74-2-------- -Di -n-butylphthalate

85-68-7------- - -Butylbenzylphthalate

117-81-7----- —— bis(2-Ethylhexyl)phthalate _117-84-0 --------Di-n-octylphthalate205-99-2--------Benzo(b)f luoranthene207-08-9------- -Benzo (k) f luoranthene50-"32-8-- ------ -Benzo (a) pyrene193-39-5- -------Indeno (1,2, 3 -cd) pyrene53 -70-3 -- —— —— Dibenzot a, h) anthracene191 -24-2- -------Benzo (g/h, i)perylene

380

150150JSO.r24Q.380380150150150_3SQQ&£

150

150150150150150150150150150150150150

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(1) - Cannot be separated from Diphenylamxne

FORM I SV-2 OIM03.0

AR308I6223482 CNF40 SPMPLE DPTP PPCKPGE 413





Sample wt/vol: 1000 (g/tnL) mL Lab File ID: GD008434A02







51-28-5---------2,4-Dinitrophenol100-02-7------ - -4 -Nitrophenol132-64-9------ - -Dibenzof uran121-14-2--------2,4 -Dinitrotoluene84-66-2-------- -Diethylphthalate70 05 - 72 -3------- 4 -Chlorophenyl -phenylether

100-01-6--------4-Nitroaniline534-52-1- - ------4, 6-Dinitro-2-methylphenol _86-30-6-------- -N-nitrosodiphenylamine_ ( 1 ) _101-55-3---- - -- -4 -Bromophenyl -phenylether

87-86-5--------- Pentachlorophenol

120-12-7------- -Anthracene

84-74-2---------Di-n-butylphthalate206-44-0-------- Fluoranthene1 y U U U iryi cUC85-68-7-------- - Buty Ibenzy Ipht hala t e

56-55-3---------Benzo (a) anthracene^.LOUJL.? — "wILL y ocllc117-81-7------ --bis (2-Ethylhexyl)phthalate117-84-0---- —— Di-n-octylphthalate

50-32-8- ------- -Benzo (a) pyrene193-39-5-------- Indeno (1,2,3- cdTpyrene53_70-3---------Dibenzo (a, h) anthracene191-24-2--------Benzo(g,h,i)perylene

380380

150150150

380380150150>C3£C22Q)(-""i fTW4-(26$150

r oi:^ 4*1'150150150150150150150150150150150150

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FORM I SV-2 m ^ OIW03.0AR308I63

254S2 CNF4Q SPMPLE DPTP PPCKPGE 5S3





Sample wt/vol: 1000 (g/mL) mL Lab File ID: GD008434A02







i ofl-QC-2-----L WO J J &>

111-44-4----QC CT Q ___yb-b /_o-----541-73-1 ———106-46-7 ———95-50-1 ————95-48-7 ————108-60-1 ———106-44-5----

78-59-1-----

tnc c*7 Q — _ — _111-91-1 ———

190 ft? 191-20-3-----•/ ** W vf

106-47-8 ———orr £Q T _ _ _ —C Q C A T — — —by-bu- /- ---QT C*7 C — — — — —yj.-b /-&-----/ / — ** / — 1±~ —

3 J. DO / — —88-'74-4-----131-11-3 ———

00-09-2-----J y w J ^

----Phenol----bis (2 -Chloroethyl) ether- - - - 2 - Chlorophenol

----1,2 -Dichlorobenzene- - - - 2 -Methylphenol----2,2' -oxybis (1-Chloropropane)- - - -4 -Methylphenol- - - -N-Nitroso-di-n-propylamine

- - - - Isophorone- - - - 2 -Nitrophenol----2,4 -Dimethylphenol----bis (2-Chloroethoxy) methane----2,4 -Dichlorophenol----1,2,4 -Trichlorobenzene- - - -Naphthalene- - - -4 -ChloroaniTTne- - - -Hexachlorobutadiene----4-Chloro-3-methylphen6I- - - - 2 -Methylnaphthalene- - - -Hexachlorocyclopentadiene----2,4,6 -Trichlorophenol----2,4,5 -Trichlorophenol- - - -2 -Chloronaphthalene----2-Nitroaniline_ _ _ -Dimethylphthalate

----2,6 -Dinitrotoluene•5 »J 4>~>_K'a«<j "1 -i T1OJ 11 il» J.UAim. .XliB

f3 >Ainne-150150150150150

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150380

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Location: KOP-MW-2S Qualifier

_ .„ .... . J SPMP .1 DPTP PQCKPGE





Sample wt/vol: 1000 Cg/mL) mL Lab File ID: GD008433A02







51-28-5---------2,4-Dinitrophenol100- 02 -7------- -4 -Nitrophenol132-64-9------- -Dibenzof uran121- 14 -2 - -------2,4 -Dinitrotoluene84-66-2-------- -Diethylphthalate7005-72-3------ -4 -Chlorophenyl-phenylether86-73-7---------Fluorene100-01-6--- -----4 -Nitroaniline534-52-l--------4,6-Dinitro-2-methylphenol _86-30-6-------- -N-nitrosodiphenylamine_ ( 1 ) _101 - 55 -3 - ----- - -4 -Bromophenyl -phenylether

87-86-5--------- Pentachlorophenol85-01-8--------- Phenant hrene120-12-7------- -Anthracene86-74-8-- -------Carbazole84-74-2- —— -----Di-n-butylphthalate206-44-0--------Fluoranthene129-00-0- -------Pyrene85-68-7---------Butylbenzylphthalate

218-01-9--------Chrysene117-81-7-----* --bis (2-Ethylhexyl)phthalate117-84 -o------- -Di-n-octylphthalate205-99-2------- -Benzo (b ) f luoranthene207-08-9------- -Benzo (k) f luoranthene5 0 -"3 2 - 8 - - - - - - - - - Benz o ( a ) pyr ene193-39-5-------- Indeno ( 1 , 2 , 3 - cd J pyrene53-70-3-------- -Dibenzo (a , h) anthracene191-24 -2------- -Benzo (g,h,i)perylene

380. ___ ^ 380*ff3«rri>-3rS£e-

150150

*~fT 15°Tyfe-ct^) 18QQ380380150150150

*-xrr--N 38°JQTS* f ft-r- . \^££gJ4300

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(l") "Cannot be separated from Diphenylamine

FORM I SV-2 OIM03.0

AR308I65234S2 CHF4Q SPMPLE DPTP PPCKPGE 4S?





Sample wt/vol: 1000 (g/mL) mL Lab File ID: GD008433A02







__________ M

108-95-2--------Phenol ____^____lll-44-4--------bis(2-Chloroethyl)ether_95-57-8---------2-Chlorophenol_541-73-l--------l,3-Dichlorobenzene_10 6 - 4 6 - 7 - - - - - - - -1,4 - Di chlorobenz ene]95-50-1---------1,2-Dichlorobenzene"95-48-7---------2-Methylphenol108-60-l--------2,2'-oxybis(1-Chloropropane)106-44-5--------4-Methylphenol,621-64-7--------N-Nitroso-di-n-propylamine_67-72-1-------- -Hexachloroethane_______~98-95-3---------Nitrobenzene___________78-59-1---------Isophorone_88-75-5---------2-NitrophenoT________105-67-9--------2,4-Dimethylphenol111-91-1--------bis(2-Chloroethoxy)methane120-83-2--————2,4-Dichlorophenol120-82-1--------1,2,4-Trichlorobenzene91-20-3 —— -———Naphthalene^106-47-8--------4-Chloroaniline87-68-3---------Hexachlorobutadiene59-5Q-7---------4-Chloro-3-methylphenol ""91-57-6-——-----2-Methylnaphthalene77-47-4---------Hexachlorocyclopentadiene_88-06-2---------2,4,6-Trichlorophenol___\95-95-4--————-2,4,5-Trichlorophenol___91-58-7-- ————2-ChJ.oronaphthalene_____88-74-4--- ————2-Nitroaniline ____131-11-3-----——Dimethylphthalate208-96-8-----——Acenaphthylene_606-20-2-----——2,6-Dinitrotoluene_99-09-2---------3-Nitroaniline83-32-9------——Acenaphthene_____

150150150150150

150

150150150

150150

150150

iso150380150380150

u

tflfir

Review: Ml Level FORM I SV-1 OIW03.0

Location: KOP-MW-2A DVQ = Data ValidatorQualifier A R 0 U 0 I D D

rJ SPr*LE ^PTP PPCKPGE ~&0





Sample wt/vol: 1000 (g/mL) mL Lab File ID: GJ008428C07







C

51-28-5---------2,4-Dinitrophenol100-02-7--------4 -Nitrophenol132-64-9--------Dibenzofuran121-14-2--------2, 4 -Dinitrotoluene84-66-2-------- -Diethylphthalate7005-72-3-------4- Chlorophenyl -phenylether _86-73-7-------- -Fluorene100-01-6- -------4-Nitroaniline534-52-l--------4,6-Dinitro-2-methylphenol _86-30-6-------- -N-nitrosodiphenylamine ( 1 )101-55-3--------4 -Bromophenyl - phenyle tEer

87-86-5--------- Pentachlorophenol85-01-8--- ------Phenanthrene120-12-7------- -Anthracene86- 74 -8-------- -Carbazole84-74-2-------- -Di -n-butylphthalate206-44-0-------- Fluoranthene^ b ^ w w w fe 7 *•»« AW

85-68-7-------- -Butylbenzylphthalate

56-55-3--------- Benzo ( a ) anthracene218-01-9 —— -----Chrysene117 - 81- 7- - ----- -bis ( 2 -Ethylhexyl ) phthalate117-84-0- ------ -Di-n-octylphthalate205 - 99-2------- -Benzo (b) f luoranthene207-08-9 —— —— Benzo (k) f luoranthene50-32-8-------- -Benzo ( a ) pyrene193-39-5--------Indeno(l, 2, 3-cd) pyrene53-70-3------- - -Dibenzo (a , h) anthracene191 -24 -2- ------ -Benzo (g,h, ijperylene

25251010101010252510101025101010101010101010101010101010101010


) - Cannot be separated from Diphenylamine

/

FORM I SV-2 OLM03.0

AR308I67



Lab Code: COMPU Case No.: 23482 SAS No.: SDG No.: CNF40 rfMatrix: (soil/water) WATER Lab Sample ID: 708428


Level; (low/med) LOW Date Received: 04/27/95






•Phenol111-44-4--------bis(2-Chloroethyl)ether_95-57-S---------2-Chlorophenol541-73-l--------l,3-Dichlorobenzene_106-46-7--------1,4-Dichlorobenzene]95-50-l---------l,2-Dichlorobenzene"95-48-7----——--2-Methylphenol108-60-l--------2,2'-oxybis(1-Chloropropane)106-44-5-------4-ffethylphenol621-64-7-----r--N-Nitroso-di-n-propylamine67-72-1---------Hexachloroethane98-95-3---------Nitrobenzene____________78-59-1---------Isophorone__^____________8S-75-5---------2-Nitrophenol105-67-9--------2,4-Dimethylphenol111-9i-i--------bis(2-Chloroethoxy)methane120-83-2 —— —— --2,4-Dichlorophenol_______120-82-1 ——————1,2,4

•Naphthalene-4-Chloroaniline

87-68-3--------- Hexachlorobut adiene• 4-Chloro-3-methylphenoT- 2-Methylnaphthalene_

77-47-4---------Hexachlorocyclopentadiene88-06-2------——2,4,6-Trichlorophenol95-95-4---------2,4,5-Trichlorophenol_____91-58-7---------2-Chloronaphthalene_______

•2-Nitroaniline131-11-3--------Dimethylphthalate_208-96-8--------Acenaphthylene606-20-2--------2,6-Dinitrotoluene_99-09-2---------3-Nitroaniline

•Acenaphthene

101010101010101010101010101010101010101010101010102510251010102510


f.

Review: Ml Level FORM I SV l OU403.0

Location: KOPFB-01 DVQ = Data ValidatorQualifier RR 308 I DO

FIELD BLANK^ —— ^ ^ SPMPLE DPTP PPCKPGE 4^0












108-95-2—————Phenol_____,__^__111-44-4——————bis (2-Chloroethyl) ether95-57-8——————2-Chlorophenol541-73-1——————l,3-Dichlorobenzene_106-46-7——————1,4-Dichlorobenzene"95-50-1——————1,2-Dichlorobenzene"95-48-7——————2-Methylphenol108-60-1——————2,2' -oxybis (1 -Chloropr opane)106-44-5——————4-Methylphenol621-64 -7 ——————N-Nitroso-di-n-propy lamine67-72-1——————Hexachloroethane_________98-95-3——————Nitrobenzene____________78 -59-1——————Isophorone88-75-5——————2-Nitrophenol105-67-9——————2,4-Dimethylphenol111-91-1——————bis (2-Chloroethoxy) methane120-83-2——————2,4-Dichlorophenol120-82-1——————1,2,4-Trichlorobenzene91-2 0-3 ———————Naphthalene106-47-8——————4-Chloroaniline87-68-3——————Hexachlorobutadiene59-50-7——————4 -Chloro-3 -methylphenol91-57-6———————2-Methylnaphthalene77-47-4——————Hexach lor ocycl open taaieneT88-06-2——————2,4,6-Trichlorophenol95-95-4———————2,4,5-Trichlorophenol91-58-7——————2-Chloronaphthalene____88J-74-4——————2-Nitroaniline131-11-3——————Dimethylphthalate208-96-8——————Acenaphthylene606-20-2——————2,6-Dinitrotoluene_99-09-2——————3 -Ni tr oani 1 ine83-32-9——————Acenaphthene_____

101010101010101010101010101010101010101010101010102510251010102510

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Review: Ml Level TOPM T ^ OIM03.0

Location: KOP-MW-7A DVQ - Data Validatorn o n Q | ggQualifier "if

_ _ . _ _ .,.. .J SPMPLE DPTP PPCKPGE 681

1C EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET











51-28-5———————2,4-Dinitrophenol100-02-7——————4-Nitrophenol___'_132-64-9——————Dibenzofuran121-14-2——————2,4-Dinitrotoluene84-66-2——————Diethylphthalate7005-72-3—————4-Chlorophenyl-phenylether86-73-7——————Fluorene100-01-6——————4-Nitroaniline534-52-1——————4,6-Dinitro-2-methylphenol ~86-30-6——————N-nitrosodiphenylamine (1) _101-55-3——————4-Bromophenyl-phenyletHer__118-74-1——————Hexachloro benzene________87-86-5——————Pentachlorophenol________85-01-8——————Phenanthrene____________12 0-12 -7 ——————Anthracene______________86-74-8——————Carbazole84-74*2——————Di-n-butylphthalate206-44-0—————Fluoranthene_____~129-00-0——————Pyrene85-68*7——————Butylbenzylphthalate91-94*1——————3,3'-Dichlorobenzidine56-55-3——————Benzo (a) anthracene218-01-9——————Chrysene117-81-7——————bis (2-Ethylhexyl) phthalate__117-84-0——————Di-n-octylphthalate_______205-99-2———-——Benzo (b) f luoranthene______207-08-9——————Benzo (k) f luoranthene______50-32-8——————Benzo (a) pyrene193-39-5——————Indeno(1,2,3-cd) pyrene_53-70-3——————Dibenzo(a,h) anthracene"191-24-2——————Benzo(g,h,i)perylene

25251010101010252510101025101010101010101010101010101010101010

UUuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

(;.) - Cannot be separated from Diphenylamine

• ——•

FORM I SV-2 OIM03.0


1D EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET ____

Name:COMPUCHEM ENV. CORP. Contract:68D50004CMW44


Matrix: (soil/water)WA1ER Lab Sample ID: 706768 Rl

Sample wt/vol: 1000(a/ml)ML Lab File ID:

% Moisture: decanted: (Y/N) Date Received: 04/25/95

Extraction: (SepF/Cont/Sonc) SEPF Date Extracted:05/23/95

Concentrated Extract Volume: 10000 fuL) Date Analyzed: 05/25/95

Injection Volume: 2 . 0 fuL) Dilution Factor: 1.

GPC Cleanup: (Y/N)N pH: Sulfur Cleanup: (Y/N) N

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kcr) UG/L Q

319-84-6--------alpha-BHC_________319-85-7--------beta-BHC_________319-86-8--------delta-BHC_________58-89-9---------gamma-BHC (Lindane)76-44-8---------Heptachlor________309-00-2--------Aldrin___________1024-57-3-------Heptachlor epoxide959-98-8--------Endosulfan I_____60-57-1---------Dieldrin________72-55-9---------4,4'-DDE__________72-20-8---------Endrin___________33213-65-9------Endosulfan II____72-54-8---------4,4'-DDD__________1031-07-8-------Endosulfan sulfate_50-29-3---------4,4'-DOT__________72-43-5-------- -Methoxychlor_____;53494-70-5------Endrin ketone____7421-93-4-------Endrin aldehyde__5103-71-9-------alpha-Chlordane__5103-74-2-------gamma-Chlordane__8001-35-2-------Toxaphene_______12674-1-1-2------Aroclor-1016_____11104-28-2------Aroclor-1221_____11141-16-5------Aroclor-1232_____53469-21-9------Aroclor-1242_____12672-29-6------Aroclor-1248_____11097-69-1------Aroclor-1254_____11096-82-5------Aroclor-1260_____

0.0500.0500.0500.0500.0500.0500.0500.0500.100.100.100.10n i n

C 0.00870.100.50

0.100.0500.0505.0

2.01.0

1.01.01.0

U

UUUUUUUUUUU

uuu_uuuuuuuu.

Review: Ml Level ————- —————————————DVQ «= Data ValidatorLocation: KOP-MW-37A FORM I PEfl-fl 3 Q Q | J | Qualifier

40 SPMPLE DPTP PPCKPGE 985

ID ' EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET

CNA91Lab Name:COMPUCHEM ENV. CORP. Contract:68D50004

Lab Code: 'COMPU Case No. : 23.482 SAS No. : SDG No. : CNF40

Matrix: (soil/water)WATER Lab Sample ID: 708425


% Moisture: decanted: (Y/N) Date Received: 04/27/95



Injection Volume: 2 . Q (uL) Dilution Factor: 1.


CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg)UG/L

319-84-6-----319-85-7-----319-86-8-----58-89-9------76-44-8------309-00-2-----1024-57-3----959-98-8-----60-57-1------72-55-9------72-20-8------33213-65-9---72-54-8------1031-07-8----50-29-3------72-43-5------53494-70-5---7421-93-4----5103-71-9----5103-74-2----8001-35-2----12674-11-2---11104-28-2---11141-16-5---53469-21-9---12672-29-6---11097-69-1---11096-82-5---

---alpha-BHC---beta-BHC---delta-BHC- - - gamma - BHC ( Lindane )---Heptachlor---Aldrin---Heptachlor epoxide---Endosulf an I---Dieldrin---4,4' -DDE---Endrin---Endosulf an II---4.4' -DDD---Endosulf an sulfate---4.4' -DDT- - -Methoxychlor---Endrin ketone---Endrin aldehyde---alpha-Chlordane---gamma-Chlordane---Toxaphene---Aroclor-1016---Aroclor-1221---Aroclor-1232---Aroclor-1242---Aroclor-1248---Aroclor-1254---Aroclor-1260

-

0.0500.0500.0500.0500.0500.0500.0500.0500.100.100.100.10

C 0.012J0.100.100.50

ro.ooss;0.100.0500.0505.01.02.01.01.01.01.01.0

uU 'uuuuuuuuuuJuuuJuuuuuuuuuuu

7)l/fi»f

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—Review: Ml Level DVQ = Data Validator

FORM I PEST Qualified R 308.1^/6Location: KOP-MW-8A -— '

'F40 SPMPLE DPTP PPCKPGE 9S>

SDG HCLH41

(UNFILTERED SAMPLES)

AR308I73

U.S. EPA - CLP

EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET

MCLM41Lab Name: CHEMTECH CONSULTING GROUP Contract: 68D30038

Lab Code: CHEM Case No.: 23482 SAS No.: JoG No.: MCLM41

Matrix (soil/water): WATER Lab Sample ID: 41523S

Level (low/med): LOW Date Received: 04/25/95

% Solids: 0.0 Lot^Vav, ; |< o

Concentration Units (ug/L or mg/Kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration_ _

(j.800./3.08.0

f 6 2 . 5Axli.oj_2_.Q

'20100 """

C

UuBBU

7.8 IB6.5 B37.1

11100 120.1

\12700 J\282^— CT2010.0

2 4 40)——— 5 . 0___ 3.0(¥4~Top

8.0rii ,-cTv\4 5 . 9 J

UuBUuuB

Q M

PPPPPPPPPPPPPPcvPPPPPPPPNR

5>V^

s?

e,&

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Color Before: BROWN Clarity Before: CLOUDY Texture:

Color After: YELLOW Clarity After: CLEAR Artifacts:

Comments:€1

FORM I - IN . ILM03.0

BRJ08I7U

U.S. EPA - CLP

EPA SAMPLE NOINORGANIC ANALYSIS DATA SHEET

MCNB89Lab Name: CHEMTECH CONSULTING GROUP Contract: 68D30038

C U c> U*- <v fLab Code: CHEM Case No.: 23482 SAS No.: SDG NoT: NTCLM41



% Solids : 0.0 \_ o c Jt -. K of-/vi u


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadium .ZincCyanide

Concentration

CJ.2J333.08.0

Vl3T>1.02.0

Upooo)5.0

)10.0

£2285)"~~ . 0

3.0(T290J3)

8.02.0

CslF?

cBUUBUU

UBB

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uu

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PPPPPPPPPPPPPPCVPPPPPPPPNR

ft OS,

&

<2>Q

G>•er-f t



Comments: fc\t Q -A I Dv g , i .< 3k_-vrjv3v> i

FORM I - IN ILM03.0

AR308I75

U.S. EPA - CLP H>A V1 * —


MCND39Lab Name: CHEMTECH CONSULTING GROUP Contract: 68D30038

Lab Code: CHEM Case No.: 23482 SAS No.: SDG No.: MCLM41



% Solids: 0.0 l_ o CL-aJo «v^ -,


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte


Concentration

C429J3.0-8-sJL

C237S>1.02.0rfsJcP\

--xjj.g)2.0

/ 23.6 V/746/ 11.3Usio\13.2/rrso-1£<0

(8975 . 0

__ 3.0foTo)

8.02.0

'M4/D)

C

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BUUBUU

UU

Q M


35VJGS,

6

6&&

S

BwMUtvyCbtT)



Comments:

FORM I - IN ILM03.0

ftR308l?6

U.S. EPA - CLP_ — . -*



aLab Code: CHEM Case No . : 23482 SAS No. : SDG No. : MCLM41

Matrix (soil/water) : WATER Lab Sample ID: 41522S

Level (low/med) : LOW Date Received: 04/25/95

% Solids: °'° LConcentration Units (ug/L or mg/Kg dry weight) : UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte


Concentration

<"3800 X

TTO64 . 6")1.02.0

4415.6\6.7

28.88920

33.712000 I\105£/

0.2010.0

\2240 >5?03.0

(1450 )8.0(yj)

C

BUBUU

B

UUBUU

uB

Q M


bx^

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(2,

WcUColor Before: BROWN Clarity Before: CLOUDY Texture:


Comments,

FORM I - IN ILM03.0

AR308I77

U.S. EPA - CLP


MCPY61Lab Name: CHEMTECH CONSULTING GROUP Contract: 68D30038

Lab Code: CHEM Case No.: 23482 SAS No.: SDC7No.: MCLM41



% Solids: 0.0 V_oc^W^%


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte


Concentration.— i i" —

3.08.0

2!oT16500 \\ 11.1

11.428.1

806017.1

W1200 I\666/—— ET20

(l36 /— 5.Q

____ 3.0f4630~3) •^ —— "8.0

U9.4J

C

UuBBU

B

UBBUU

UB

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Dv



Comments:

FORM I - IN ILM03.0

AR308I78

U.S. EPA - CLP1 '



<« (Lab Code: CHEM Case No. : 23482 SAS No. : SDG No. : MCLM41


Level (low/med) : LOW- Date Received: 04/27/95

% Solids: 0.0 Lo Un'sv, ; Kof- <v\W-

Concentration Units (ug/L or mg/Kg dry weight) : UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte


Concentration_

/3120V —— l.o

8.0QT7J?1.02.0

r2450Q ">11.13.825.7

267009.7

27500V. 965 X

0 . 2 '1Q.O

(2740 )— "~ lT.o___ 3.0

3

— nr . o

C

UuBUU

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UB

Q M


Dwta

&

6»

gm,Color Before: BROWN Clarity Before: CLOUDY Texture:


Comments:DVQ ^

FORM I - IN flR3n8|7g 11*03.0

U.S. EPA - CLP1


MCPY65f+c*HLab Name: CHEMTECH CONSULTING GROUP Contract: 68D30038&—4p.




% Solids: 0.0 Lo c_^tv<sv> ; Kof-Fi3-o\


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte


Concentration

(13 1/3.08.0

rTT?\\1_-_OJ.. j. 0

n/rf)5.02.0

/2T78"\(3311 12.4I 65.4\ 4o10.0200

5.03.0.

(207}8.02.0

\28.~5\

C

BUUBBUBUUB

BBUUauuBUU

Q M



Color After: YELLOW Clarity After: CLEAR Artifacts

Comments:fr V -

AR308I80

U.S. EPA - CLP1


MCPY70Lalp Name: CHEMTECH CONSULTING GROUP Contract: 68D30038

-Lab Code: CHEM Case No.: 23482 SAS No.: SDG No MCLM41



% Solids: 0.0 t-o W


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte

AluminumAnt imonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

CJ82Q33.08.0

22}1.02.0

59700 A12. 3\11.428.0

6010014.8

43100 J\4520^/^ T720X 13 .~3}(3640 XV— "iTo_ __ 3.0[6880)- —— 8.0rji . e\\4S.6J

c

uuBUu

B

UBBUU

UB

Q M

P~PPPPPPPPPPPPPCVPPPPPPPPNR

$0^

&

&

g,

NOP<4 •( Kov)


Color After: YELLOE Clarity After: CLEAR Artifacts:

Comments:

FORM I - IN ILM03 .0

flR3G8l8!

8D6 HCLM43

(FILTERED SAMPLES)

f\.

&R308I82

U.S. EPA -


MCLM43Lab Name: CHEMTECH CONSULTING GROUP Contract: 68D30038

Lab Code: CHEM Case No.: 23482 SAS No.: SDG^No?



% Solids: 0.0 l_oi-^l-it-oC t,


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte


Concentration

C£T_.J;3.08 . Q

f25 . 3\V^J__2/I2.0

£!94pJ3/'5.02.03.0

30.0___ 3.0Cll900 NV 21 .4J

0.2010.0

(Joso)5.0

___ 3.0( 7295?

8.02.0

C 20_.j)

C

BUUBBU

UUuuu

uuBUU

UU

Q M


D,«

B

£,

&

Color Before: COLORLESS Clarity Before: CLEAR Texture:

Color After: COLORLESS Clarity After: CLEAR Artifacts:DVQ = Data Validation

Comments: Qualifier

FORM I - IN ILM03.0

AR308I83

U.S. EPA - CLP1


MCNB90Lab Name: CHEMTECH CONSULTING GROUP Contract: 68D30038




% Solids: 0.0 Lc c Jct&n ; ko


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte


Concentration

C54J?TTo8.0

<fT2 >N

\U 2)2.0

(Tl6Q>——— 5.0

7.63.0

[-51200}3.0

r4T7 \\29lj

0.2010.0

[1940)5.03.0

\1130d>8.02.0

\25TT)

C

BUUBBU

UBU

UB

UUBUU

uu

Q M


b/<?G>

a

B



Comments: Qualifier

FORM I - IN ILM03.0AR308I8U

U.S. EPA - CLP



. Jk *v^wDi°oLab Code: CHEM Case No.: 23482 SAS No.: SDG No.:>ICLM43



%. Solids: 0.0 Lo< 0v .. K*/


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte


Concentration

\ 7 5 . 2\XuJ8.0rioTTA

\ 1.4J2 . 0

VsiioJ5.02.03.0

30.03.0

f734lT-\qp>TT72010.0

[84j£)5.03.0

{8420)8.02.0

^20. g)

C

BBUBBU

UUuuuBUuBUuuu

Q M


r>/6?

6

£

B

9


Color After: COLORLESS Clarity After: CLEAR Artifacts:

Comments: DVQ = Data ValidationQualifier

FORMI'IN AR308I85

U.S. EPA -



DLab Code: CHEM Case No.: 23482 SAS No.: SDG No.: MCLM43



% Solids: 0.0 \ -,„ L. ,, n — .U.o< sUr> -. \CoP_ûi-n AConcentration Units (ug/L or mg/Kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48*47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte


Concentration

C 60.413.08.0

r"29 . 8\VJ..l)2.0

(llSOO)—— 5.0

c33D3.0

. (f2~7T/__ 3 . 0riTJo1,

\ J739 *0.20

10.0130J)

5.0__ 3 . 0/TTscfop——— 8.0

2.0(""'18 .1?.

C

BUuBBU

UBU

U

UUBUU

uuB

Q M


Dv*

B

B

B

Color Before: COLORLESS Clarity Before: CLEAR Texture:-


Comments: Qualifier

FORM I - IN ILM03.0

AR308I86



>-J. *L -f CLP \\Lab.Code: CHEM Case No.: 23482 SAS No.: SDG. No.: MCLM43



% Solids: 0.0 LOC-A^JTVI -, \<of—


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte


Concentration

G¥\73.2)—- —— ;, —— .

8.0r327e\V1.4J2.0

CTssjDjp5..0

cloTi]^ __ 3.0CS£>___ 3.0

(3780CT)V. 744/—— 0.20X13.27(_3_19

5.03.0

(£8400>8.02.0

< 387T)

C

BBUBBU

UBU

U

UBBUU

uu

Q M


2>*PS

B

S



Comments: Qualifier

FORM I - IN ILM03.0

AR308I87

U.S. EPA - CLP1






% Solids: 0.0 , CooaJo^-. Kop-


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte


Concentration

(69.9^1V^_pJ8.0

(~£TTT]VJL_3j

2.0(g40jKp

5.02.03.0

C2230C[>__ 3.0

(2570CT\L_874 J

0.201C 1.0

1650}5.0

__ 3.0cf9ooj£8.02.0

Q3.3}

C

BBUBBU

UUuu

uuBUU

uu

Q M


?>Y<9B>

£

6



Comments: Qualifier

FORM I - IN ILM03.0

«R308I88

U.S. EPA - CLPjLrv\i

EPA SAMPLE NO'INORGANIC ANALYSIS DATA SHEET


Lab Code: CHEM Case No.: 23482 SAS No.: SJDG *NoT: MCLM4V



% Solids: 0.0 L.oc-0 . K


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte


Concentration

CJ56 .QjT708.0(i 72]Li.iJ2.0

/TsToj— 5To2.03.0

(233103.0

/23 .2]i_ i .4;

0.2010.02005.03.0

cjTTT)8.02.0

27.2 A

C

BUUBBUBUUUBUBBUUUuuBUU

Q M


wG

£>

B


Color After: COLORLESS Clarity After: CLEAR Artifacts:DVQ - Data Validation

Comments: Qualifier

FORM I - IN ILM03.0

AR308I89

U.S. EPA -1



ALab Code: CHEM Case No.: 23482 SAS No.: SDG No.: MCLM43

Matrix (soil/water)': WATER Lab Sample ID: 41760S


% Solids: 0.0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-67440-66-6

Analyte


Concentration

Q7j33^ 3To8.0

fesTT]\1.3j2.0

£Hl227SjJLJZ

__ __ 3.0£354(32?^ IM»I '

____ 3.0f4480CM444j7

0.2010.0dH5.03.0

<2H$78.02.0

CHil

C

BUUBBU

UBU

U

uuBUU

UU

Q M


&/<£

G>

&

S

Color Before: YELLOW Clarity Before: CLEAR Texture:

Color After: YELLOW Clarity After: CLEAR Artifacts:DVQ - Data Validation

Comments: Qualifier

FORM I - IN ILM03.0

AR308I90

APPENDIX C

SUPPORT DOCUMENTATION

AR308I9

AR308I9I4

AR308I95

U.S. EPA - CLP

10INSTRUMENT DETECTION LIMITS (QUARTERLY)

Name: CHEMTECH CONSULTING GROUP Contract: 68D3003S


ICP ID Number: Date: 04/15/95

Flame AA ID Number: CV

Furnace AA ID Number:

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

Wave-length

(nm)

253.70

Back-ground

CRDL(ug/L)

2006010

20055

50001050251003

5000150.240

5000510

5000105020

IDL(ug/L}

0.2

M

NRNRNRNRNRNRNRNRNRNRNRNRNRNRCVNRNRNRNRNRNRNRNR

Comments:CV: SPECTRO-PRODUCTS MERCURY ANALYZER

FORM X - IN ILM03.0

AR308I96

U.S. EPA - CLP

10INSTRUMENT DETECTION LIMITS (QUARTERLY)

Lab Name: CHEMTECH CONSULTING GROUP Contract: 68D30038


ICP ID Number: PO Date: 04/15/95

Flame AA ID Number:

Furnace AA ID Number:

Analyte

AluminumAnt imonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

Wave-length(nm)

308.20206.80189.00493.40313.00226.50317.90267.70228.60324.70271.40220.40279.00257.60

231.60766.50196.00328.00588.90190.90292.40213.80

Back-ground

CRDL(ug/L)

200601020055

5000105025100

35000150.240

50005

105000105020

IDL(ug/L)

25.03.08.01.01.02.0

10.05.02.03.0

30.03.0

15.01.0

10.0200.05.03.0

10.08.02.04.0

M

PPPPPPPPPPPPPPNRPPPPPPPP

Comments:PO: ICP 61E TRACE ANALYZER

FORM X - IN ILM03.0

flR3Q8I97

8DQ HCLM41

AR308I98

U.S. EPA - CLP

3

BLANKS



Preparation Blank Matrix (soil/water): WATER

Preparation Blank Concentration Units (ug/L or mg/kg): UG/L

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalcium^hromiumbait

. xPPsrIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

InitialCalib.Blank(ug/L) C

25.03.08.01.01.02.0

10.05.02.03.0

30.03.0

15.01.00.2

10.0200.0

5.03.017.38.02.04.0

UUUUUUUUUUUUUUUUUuuBUUU

Continuing CalibrationBlank (ug/L)

1 C 2 C 3 C

52.63.08.01.01.02.0

40.65.02.03.0

30.03.0

44.11.00.2

10.0200.0

5.03.0

10.08.02.04.0

BUUUUUBUUUUUBUUUUUUUUUU

25.63.08.01.01.02.0

23.75.02.03.0

30.03.0

15.01.00.2

10.0200.05.03.0

10.08.02.04.0

BUUUUUBUUUUUUUUUUUUUUUu

35.33.08.01.01.02.0

10.05.02.03.0

30.03.0

15.01.00.2

10.0200.05.03.0

10.08.02.04.0

BUUUUUUUUUUUUUUUUUUUuuu

Prepa-rationBlank C

62.3203.0008.0001JLOOCiTesjP2.00010.0005.0002.0003.00030.0003.00015.0001.0000.20010.000200.0005.0003.00010.0808.0002.0004.000

BUUUBUUUUUUUUUUUUUUBUUU

M

PPPPPPPPPPPPPPCVppppppppNR

FORM III - IN ILM03.0

AR308I99

U.S. EPA - CLP

3

BLANKS



Preparation Blank Matrix (soil/water):

Preparation Blank Concentration Units (ug/L or mg/kg):

Analyte




-3r ^ _ C * C -3- C<S> © (S>43.73.08.01.01.02.0

10.05.02.03.0

30.03.0

15.01.00.2

10.0200.05.03.0

10.08.02.04.0

BUUUUUuuuuuuuuuuuuuuuuu

47.93.08.01.01.02.0

20.75.02.03.030.03.015.01.0

10.0200.05.03.010.08.02.04.0

BUUUUUBUUUUUUU

UUUUUUUu

57.63.08.01.01.02.010.05.02.03.0

30.03.015.01.0

10.0200.05.03.'010.08.02.04.0

BUUUUUUUUUUUUU

UUUUUUUU

Prepa-rationBlank C M

P~PPPPPPPPPPPPPCVPPPPPPPPNR


AR3082QO

U.S. EPA - CLP

3

BLANKS





Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumpv»romium

>alt- pperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide



i- c --a- c -3- cQ2_ -3.08.01.01.22.0

10.05.02.03.0

30.03.0

cjTTJ1.0

10.0200.05.03.0

10.08.02.04.0

t

BUUUBUUUUUUUBU

UUUUUUUU

64.63.08.01.01.42.0

-15.85.02.03.0

30.03.0

15.01.0

10.0200.05.03.010.08.02.04.0

1

BUUUBUBU"UUUUUU

UUUUUUUU

67.23.08.01.01.52.0

10.05.02.03.0

30.03.0

16.61.0

10.0200.05.03.0

10.08.02.04.0

BUUUBUUUUUUUBU

UUUUUUUU

j, J-


PPPPPPPPPPPPPPNRPPPPPPPPNR

FORM III - IN ILM03.0AR30S20I

U.S. EPA - CLP

14ANALYSIS RUN LOG



Instrument ID Number: PO Method: P

Start date: 05/20/95 End date: 05/20/95

EPASampleNo.

SOSSSSICVICVICVICVICBCRIICSAICSABCCVCCB— iZZ2ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB-x-ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZ

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001*001.00

Time

08510854085608580859090009040907091109140917092309290932093509380941094509490953095710161019102210251028103110341037104210451049

% R AL

X

X

X

X

XXXX

XX

sB

XX

X

XXXXXX

XX

AsXX

X

XXXXXX

XX

BA

XX

X

X

XXXX

XX

BE

XX

X

XXXXXX

XX

cD

XX

X

XXXXXX

XX

cA

X

X

X

X

XXXX

XX

cR

XX

X

XXXXXX

XX

coXX

X

XXXXXX

XX

pcuXX

X

XXXXXX

XX

ina

FE

X

X

X

X

XXXX

XX

lypB

XX

X

XXXXXX

XX

rte

MG

X

X

X

X

XXXX

XX

s

MN

XX

X

XXXXXX

XX

HGNIXX

X

XXXXXX

XX

K

X

X

X

X

XXXX

XX

sE

X

X

X

XXXXXX

XX

AG

X

XX

XXXXXX

XX

NA

X

X

X

X

XXXX

XX

TL

X

X

XXXXXXX

XX

V

XX

X

XXXXXX

XX

zN

XX

X

X

XXX

XX

cN

s

FORM XIV - IN ILM03.C

AR308202

U.S. EPA - CLP

14ANALYSIS RUN LOG

_.D Name: CHEMTECH CONSULTING GROUP Contract: 68D30038




EPASampleNo.

ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB— !»ZZZZZZZZZZZZZZZZZZzzzz*zzzz

~tzzzzzZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB->-fZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB S"ZZZZZZ

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00;.oo1.00

Time

10521055105811011104110711101113111611191122112511291132113511381141114411471150115311561159120212051208121112141218122112241236

% R

Analytes

L

XX

XX

XX

sB

XX

XX

XX

AS

XX

XX

XX

BA

XX

XX

XX

BE

XX

XX

XX

cD

XX

XX

XX

cA

XX

XX

XX

cR

XX

XX

XX

co

XX

XX

XX

cu

XX

XX

XX

FE

XX

XX

XX

pB

XX

XX

XX

MG

XX

XX

XX

MN

XX

XX

XX

HGNI

XX

XX

XX

K

XX

XX

XX

sE

XX

XX

XX

AG

XX

XX

XX

NA

XX

XX

XX

TL

XX

XX

XX

V

XX

XX

XX

zN

XX

XX

XX

QN

FORM XIV - IN ILM03.0

AR308203

U.S. EPA - CLP

14ANALYSIS RUN LOG





EPASampleNo.

ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB-^MCND43MCND39MCND39DMCND39SMCND39LMCLM4 1MCNB89MCPY70MCPY63MCPY65CCVCCB-"fMCPY61ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZ

D/F

1.001.005.001.001.001.005.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00x.oo1.00

Time

12391242124512481253125612591303130913121315131913221325132813311334133713401344134813511354135714001403140614091412141514181421

% R AL

XXXXXXXXXXXXXXX

sB

XXXXXXXXXXXXXXX

As

XXXXXXXXXXXXXXX

BA

XXXXXXXXXXXXXXX

BE

XXXXXXXXXXXXXXX

cD

XXXXXXXXXXXXXXX

cA

XXXXX

XXXXXXXXX

cR

XXXXXXXXXXXXXXX

c0

XXXXXXXXXXXXXXX

p.cu

XXXXXXXXXXXXXXX

jia

FE

XXXXXXXXXXXXXXX

lypB

XXXXXXXXXXXXXXX

te

MG

XXXXX

XXXXXXXXX

s

MN

XXXXXXXXXXXXXXX

H(•1\JNI

XXXXXXXXXXXXXXX

K

XXXXX

XXXXXXXXX

sE

XXXXXXXXXXXXXXX

Ar*\3

XXXXXXXXXXXXXXX

NA

XXXXX

XXXXXXXXX

TL

XXXXXXXXXXXXXXX

V

XXXXXXXXXXXXXXX

zN

X

-rXXXXXXXXXXX

cN

/—

FORM XIV - IN ILM03.'

AR308201*

U.S. EPA - CLP

14ANALYSIS RUN LOG

Name: CHEMTECH CONSULTING GROUP . Contract: 68D30038




••" ^ ^""•"-

EPASampleNo.

ZZZZZZCCVCCB-*ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZ"IZZZZ

\zzz_.zzzzZZZZZZCCVCCB— 1ZZZZZZZZZZZZZZZZZZZZZZZZPBWZZZZZZLCSWZZZZZZCCVCCB-tc?ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZ

D/F

1.001.001.001.001.001.005.001.001.001.005.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001*001.00

Time

14241427143014331436143914421445144814511454145715001503150615091512151515181522152515301535153815411545154815511555155816011604

% R AL

XX

XX

X

X

XX

sB

XX

XX

X

X

XX

AS

XX

XX

X

X

XX

BA

XX

XX

X

X

XX

BE

XX

XX

X

X

XX

cD

XX

XX

X

X

XX

cA

XX

XX

X

X

XX

cR

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AR308205

fculQ U.S. EPA - CLP

COVER PAGE - INORGANIC ANALYSES DATA PACKAGE



SOW No.: ILM03.0

EPA SAMPLE NO. Lab Sample ID.MCLM41 41523S —^MCNB89 41524SMCND39 41519S ^MCND39D 41520S2MCND39S 41521DSMCND43 41522SMCPY61 41767SMCPY63 41765SMCPY65 41766SMCPY70 41764S

MM 301995

Were ICP interelement corrections applied? Yes/No YESWere ICP background corrections applied? Yes/No YES

If yes-were raw data generated beforeapplication of background corrections? Yes/No NO

Comments:

I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or theManager's designee, as verified by the following signature.

V^ ____Signature: f / 4£\ /JML. ^ Name: PARVEEN HASAN

AiDate: _______O£/&*>/9 _____ Title: QA/QC OFFICER

COVER PAGE - IN ILM03.0

AR308206

SDG MCLM43

AR308207

U.S. EPA - CLP

3

BLANKS


Lab Code: CHEM Case No.: 23482 SAS No.: . SDG No.: MCLM43

Preparation Blank Matrix (soil/water): WATER

Preparation Blank Concentration Units (ug/L or mg/kg): UG/L

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumbait

j PPerIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide


25.03.08.01.01.02.010.05.02.03.030.03.015.01.00.210.0

200.05.03.017.38.02.04.0

UUuuuuuuuuuuuuuuuuuBuuu


1 C 2 C 3 C

52.63.08.01.01.02.040.65.02.03.030.03.044.11.00.210.0200.05.03.010.08.02.04.0

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25.63.08.01.01.02.023.75.02.03.030.03.015.01.00.210.0

200.05.03.010.08.02.04.0

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35.33.08.01.01.02.010.05.02.03.030.03.015.01.00.210.0200.0

5.03.010.08.02.04.0

BUUUUUUUUUUUUUUUUUUUuuu

Prepa-rationBlank C

62.5103.0008.0001.000

£L 66$,2.000

-14.1705.0002.0003.00030.0003.00015.0001.0000.20010.000200.0005.0003.00010.0008.0002.0004.000

BUUuBUBUUUUUUUUUUUUUUUU

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FORM III -IN HOOflQOnO ILM03.0AR308208

U.S. EPA - CLP

3

BLANKS





Analyte




-1- ^^C -a- _C 3- C© <S> ©

43.73.08.01.01.02.010.05.02.03.030.03.015.01.00.2

10.0200.05.03.010.08.02.04.0

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47.93.08.01.01.02.020.75.02.03.030.03.0

15.01.0

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57,63.08.01.01.02.010.05.02.03.030.03.015.01.0

10.0200.05.03.010.08.02.04.0

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AR308209 ILM03'°

U.S. EPA - CLP

3

BLANKS





Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumbait..pperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide



-i- C -fi- C - -.C

<C?2 . O3.08.01.01.22.0

10.05.02.03.0

30.03.0

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64.63.08.01.01.42.0

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67.23.08.01.01.52.0

10.05.02.03.030.03.016.61.0

10.0200.0

5.03.010.08.02.04.0

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PPPPPPPPPPPPPPNRPPPPPPPPNR


AR3082IO

U.S. EPA - CLP

14ANALYSIS RUN LOG





EPASampleNo.

SOSSSSICVICVICVICVICBCRIICSAICSABCCVCCB— \ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB— -2-zzzzzzZZZZZZZZZZZZZZZZZZZZZZZZ

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00l-.OO1.00

Time

08510854085608580859090009040907091109140917092309290932093509380941094509490953095710161019102210251028103110341037104210451049

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AR3082

U.S. EPA - CLP

14ANALYSIS RUN LOG

^_o Name: CHEMTECH CONSULTING GROUP Contract: 68D30038




EPASampleNo.

ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB--3ZZZZZZZZZZZZv.ZZZZZzzzz*zzzzZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB-HZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB-STZZZZZZ

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

10521055105811011104110711101113111611191122112511291132113511381141114411471150115311561159120212051208121112141218122112241236

% R AL

XX

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AR3082I2

U.S. EPA - CLP

14ANALYSIS RUN LOG





EPASampleNo.

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1.001.005.001.001.001.005.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001,001.00

Time

12391242124512481253125612591303130913121315131913221325132813311334133713401344134813511354135714001403140614091412141514181421

% R

Analytes

AL

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AR3082I3

U.S. EPA - CLP

14ANALYSIS RUN LOG

_ ,b Name: CHEMTECH CONSULTING GROUP Contract: 68D30038




EPASampleNo.

ZZZZZZCCVCCB— rMCND95MCND95DMCND95SMCND95LZZZZZZZZZZZZZZZZZZzzzzzLZZZZ

[ZZZZZZCCVCCB— ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZPBWZZZZZZLCSWCCVCCB— 10ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZ

D/F

1.001.001.001.001.001.005.00.1.001.001.005.001.001.001.001.001..001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.00

Time

14241427143014331436143914421445144814511454145715001503150615091512151515181522152515301535153815411545154815511555155816011604

% R AL

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AR3082IU

1 U.S. EPA - CLP

COVER PAGE - INORGANIC ANALYSES DATA PACKAGE


Lab Code: CHEM Case No.: 23482 SAS No.: 'SDG No.: MCLM43

SOW No.: ILM03.0

EPA SAMPLE NO. Lab Sample ID.MCLM43 41530SMCNB90 41531SMCND95 41526SMCND95D 41527S2MCND95S 41528DSMCND97 41529SMCPY62 41763SMCPY64 41761SMCPY66 41762SMCPY69 41760S

Were ICP interelement corrections applied? Yes/No YESWere ICP background corrections applied? Yes/No YES

If yes-were raw data generated beforeapplication of background corrections? Yes/No NO

Comments:

I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or theManager's designee.£S__verified by the following signature.

Signature: ^ /GEQ>g^v—______ Name: PARVEEN HASAN

Date: 7«L£ AS________ Title: QA/QC OFFICER7 T

COVER PAGE - IN ILM03 .0

AR3082.I5

Appendix C

Support Documentation

AR3082I6

COMPUCHEMENVIRONMENTALCORPORATION

SDG NARRATIVECASE NUMBER: 23482SDG NUMBER; CNF40

CONTRACT NUMBER; 68D50004SAMPLE IDENTIFICATIONSt CMW42, CMW43, CMW44, CNA89, CNA90, CNA91,

CNA92, CNA93, CNA94, CN740, CNP41, CNF43The twelve (12) water samples listed above were received intact, ina sealed shipping container, on April 24, 25, and 27, 1995. Thesamples were received at 6 and 8 degrees Celsius. No U. S. EPACooler Temperature Indicator was received with these samples. Thesamples were scheduled for the requested analyses of the volatile,semivolatile, and pesticide/PCB fractions. In accordance with theorganic traffic reports (OTRs), samples CNF40, CMW42, and CNA89were scheduled for the analysis of the volatile fraction only. Ofthe twelve samples in this SDG, only samples CMW44 and CNA91 werescheduled for the analysis of the pesticide/PCB fraction. Thesesamples were analyzed following document OLM03.1 protocol.

All pertinent Quality Assurance notices are included in thenarrative section, and all pertinent Laboratory notices for CaseNumber 23482, SDG Number CNF40 are included in the sample datasections.

VOLATILES

The pH values of these samples are tabulated on the attached batchsheet. Analysis holding time requirements were met for all ofthese samples. There were no target compound list (TCL) analytesidentified above the contract required quantitation limit (CRQL) innine of these samples. The common laboratory solvent acetone wasidentified above the CRQL in sample CNA94. There were a fewaromatic TCL analytes identified above the CRQL at varyingconcentrations in the remaining samples. Tentatively identifiedcompounds (TICs) were found in five of these samples. Some of theTICs were assessed as hydrocarbons, substituted benzenes, andunknowns.

Due to the results of a screening analysis, sample CNA93 wasanalyzed using 1 milliliter (ml) of raw sample rather than themethod specified volume of 5 ml. In the initial analysis of 1 mLof sample CNA93, the on-column amount of toluene exceeded theinstrument's analytical range as defined by the highestconcentration level of the Initial Calibration. The sample wasreanalyzed using a smaller aliquot of raw sample to bring the on-column amount into range. We have reported and billed for bothanalyses of sample.

AR30B2I723482 CNF40 SPMPLE DPTP PPCKPGE


In the analysis of the Initial and the Continuing CalibrationStandards and some of the samples and the blanks, the operatorperformed manual integrations and/or manual edits of one or more ofthe TCL analytes. These manual integrations or edits are indicatedby the "M", "H", or the »MH" flag present on the quantitationreport. An extracted ion current profile (EICP) has been providedfor each analyte requiring a manual integration or a manual edit.As noted on the quantitation reports by number, these manual editsand/or manual integrations were required for the following reasons:1) TCL analytes were initially not found by the automaticintegration routine, 2) TCL analytes were incorrectly integrated bythe automatic integration routine, 3) the operator selected analternate peak within the retention time window for a particularTCL analyte than that chosen by the computer software. Theexplanations for the manual integrations and/or manual edits aresummarized in a quality assurance notice which is located in thenarrative section of the data package.

All of the system monitoring compounds met recovery criteria in theanalyses of these samples. All of the internal standards metresponse and retention time criteria in the analyses of thesesamples. The associated method blanks met all quality contro1criteria. The method blanks contained levels of the conLmo.laboratory solvent methylene chloride, which were within allowable"limits. There were no TICs found in the associated volatile methodblanks or the holding blank. Methylene chloride was detected at aconcentration below the CRQL in the volatile holding blank. CNF41was used as the original sample to prepare the duplicate matrixspikes are requested. The associated duplicate matrix spikes metall advisory accuracy and precision criteria.

SEMI-VOIATILES

Extraction and analysis holding time requirements were met for allof these samples. There were no semivolatile TCL analytesidentified above the CRQL in six of these samples. There were anumber of aromatic and phenolic compound TCL analytes identifiedabove the CRQL at varying concentrations in the remaining samples.TICs were found in nine of these samples. Some of the TICs foundin these samples could be characterized as substituted benzenes,hydrocarbons, and unknowns, and alkanes. Some of the other TICsfound in these samples were assessed as laboratory artifacts andblank contaminants, and therefore may not be sample constituents.

Due to the results of screening analyses, samples CNA91, CNA93 andCNA94 were each analyzed at a 15:1 dilution. Screen reconstructedion chromatograms (RICs) have been included with the data for thesesamples. In the 15:1 diluted analyses of these samples, ttamounts of one or more TCL analytes exceeded the instrument'-analytical range as defined by the highest concentration level of

AR3082I82 23482 CNF40

23482 CNF4Q SflWPLF n


the Initial Calibration. The samples were reanalyzed at 30:1,600:1, and 250:1 dilutions respectively in order to bring theamounts into range. At these levels of dilution, the surrogateswere present at concentration levels which preclude accuratequantitation. The surrogates met recovery criteria in the initialanalysis. We have reported and billed for both analyses of samplesCNA91, CNA93, and CNA94.

In sample CNF43, the surrogate d!4-terphenyl failed quality controlcriteria. 2,4,6-Tribromophenol failed quality control criteria insample CNA90. Six of the surrogate compounds were flagged asoutliers in the matrix spike duplicate, CNF41 MSD.

The 'X' flag is used to denote indistinguishable coeluting isomers.We have provided an EICP for each pair of isomers flagged with an'X' on the Form I.

In the analysis of the Initial and the Continuing CalibrationStandards and some of the samples and blanks, the operatorperformed manual integrations and/or manual edits of one or more ofthe TCL analytes. These manual integrations or edits are indicatedby the "M", "H", or the "MH" flag present on the quantitationreport. An EICP has been provided for each analyte requiring amanual integration or a manual edit.

All of the surrogates not previously discussed met recoverycriteria in the analyses of these samples. All of the internalstandards met response and retention time criteria in the analysesof these samples. The associated method blanks met all qualitycontrol criteria. The method blanks did not contain any TCLanalytes. TICs were found in three of the method blanks. CNF41was used as the original sample to prepare the duplicate matrixspikes as requested. The associated duplicate matrix spikes didnot meet all advisory accuracy and precision criteria. Spikingcompounds 1,2,4-trichlorobenzene, 4-chloro-3-methylphenol, and 4-nitrophenol were flagged as outliers in the matrix spike. In thematrix spike duplicate, 2-chlorophenol, 1,4-dichlorobenzene, n-nitroso-di-n-propylamine, 1,2,4-trichlorobenzene, 4-nitrophenol,2,4-dinitrotoluene, pentachlorophenol, and pyrene were flagged asoutliers. The majority of the relative percent differences (RPDs)failed quality control criteria in the comparison of the duplicatematrix spikes. In accordance with the statement of work (SOW), wehave reported the data without further analysis.

PBBTICIDES/PCBa

Holding time requirements were met for the initial extraction ofboth of the samples in this SDG which required pesticide/PCBanalyses. In the analysis of the initial extract of sample CMW44,surrogate recovery criteria were not met in the associated method

flR3082!93 23482 CNF40

234S2 CNF49 SPMPLE PPTP PPCKPGE


blank. To comply with the requirements of the SOW, the sample wasreextracted. The re-extraction of this sample was performedoutside of holding times. The analysis of the second extract metall quality control criteria. We have reported only the analysisof the second extract of sample CMW44. The data from the analysisof the initial extract may be found in the complete SDG file (CSF).

There were no pesticide/PCB TCL analytes confirmed by dual columnabove the CRQL in either of the two samples.

In the analysis of some of the Calibration Standards and some ofthe samples and blanks, the operator performed manual integrationsand/or manual edits of one or more of the TCL analytes. Thesemanual integrations or edits are indicated by the "M" flag presenton the process file. An EICP has been provided for each analyterequiring a manual integration or a manual edit.

Severe matrix interference on the DB-608 and the RTX-1701analytical columns in the analyses of samples CNA91, CNA91 MS, andCNA91 MSD precluded the accurate identification and quantitation ofthe advisory surrogate tetrachloro-m-xylene (TCX). The remainingsamples met all advisory surrogate recovery criteria for TCX anddecachlorobiphenyl (DCB). The associated method blanks met allquality control criteria. These method blanks did not contain anyconfirmed TCL analytes. CNA91 was used as the original to preparethe duplicate matrix spikes. With two exceptions, the associatedduplicate matrix spikes met all accuracy and precision criteria.The recovery values of the spiking compound gamma-BHC were flaggedas outliers in the matrix spike and the matrix spike duplicate.

I certify that this data package is in compliance with the termsand conditions of the contract, both technically and forcompleteness, for other than conditions detailed above. Release ofthe data contained in the hardcopy data package and in thecomputer-readable data submitted on diskette has been authorized bythe Laboratory Manager or his designee, as verified by thefollowing signature.

51. HI 95E. Edwards

Technical ReviewerMay 31, 1995

AR3Q82204 23482 CNF40

'34S2 CNF40 SPMPLE DPTP PPCKPGF

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CNA93DLLab Name: COMPUCHEM ENV. CORP. Contract: 68D50004



Sample wt/vol: 5.0 {g/mL) mL Lab File ID: CR008433B52






74-87-3-------- -Chloromethane74-83-9--------- Bromomethane75-01-4---------Vinyl Chloride75-00-3-------- -Chloroethane75-09-2-------- -Methylene Chloride

75-15-0-------- -Carbon Disulfide75 -35 -4 ---------1, 1-Dichloroethene75-34-3---------1, 1 -Dichloroethane540 -59-0- - ------1,2-Dichloroethene (total) _67-66-3 ---------Chloroform107-06-2- -------1,2-Dichloroethane78-93-3---------2-Butanone71-55-6---------1,!,!- Trichloroe thane56-23-5-------- -Carbon Tetrachloride75-27-4-------- -Bromodichloromethane78-87-5---------1/2 -Dichloropropane10061-01-5- - ----cis-1, 3 -Dichloropropene ____79-01-6-------- -Trichloroethene124 -48 - i ------ - -Dibromochloromethane79-00-5---------l,l,2-Trichloroethane

l0061-02-6------trans-l, 3 -Dichloropropene7 5 - 2 5 - 2 - - - - - - - - - Bromo f orm108-10-l--------4-Methyl-2-Pentanone

127-18-4------- -Tetrachloroethene79-34-5---------l,l,2,2- Tetrachloroe thane

100-41-4 ------ - -Ethylbenzene100-42-5--------Styrene1330-20-7- ------Xylene (Total)

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1

DVQ = Data ValidatorQualifier

FORM I VOA - - - - - ULM03.0

SR30822723482 CNF4Q SPMPLE &8TP PPCKPGE





Sample wt/vol: 1000 (g/mL) mL Lab File ID: G2D08425A07







inn QC *5 ___ — — __ -OVienril111-44-4-- ------bis (2-Chloroethyl) ether9 5 - 5 7 - 8 - - - - - - - - - 2 - Chloropheno 1541-73-l--------l,3 -Dichlorobenzene106-46-7- ------ -1,4-Dichlorobenzene

95-48-7---------2-Methylphenol108-60-l--------2/2' -oxybis(l-Chloropropane)106-44-5--------4-Methylphenol621-64-7------- -N-Nitroso-di-n-propylamine67-72-1------- - -Hexachloroethane98-95-3-------- -Nitrobenzene78-59-1--------- Isophorone88-75-5----- —— -2-Nitrophenol105-67-9---- ----2, 4-Dimethylphehollll-9l-l--------bis { 2 -Chloroethoxy) methane120-83-2--------2,4-Dichlorophenol

91-20-3--- ------Naphthalene106-47-8- ------ -4-Chloroaniline87-68-3-------- -Hexachlorobutadiene59-50-7------ —— 4 -Chloro-3 -methylphenol91-57-6- --------2-Methylnaphthalene77 -47 -4 - ------- - Hexachlorocyc lopent adiene88-06-2---------2,4/6 - Tr i chlorophenol95_95_4__----__-2,4/ 5 -Trichlorophenol91-58-7---------2- ChloronaphthaleneS8-74-4---------2 -Nitroaniline131-11-3 ------ --Dimethylphthalate

606-20-2---- —— -2,6-Dinitrotoluene

300300300300300300300300300300300300300300300300300300

C220_3afto300300320300300750300750300300300750380

UUuuuuuuuuuuuuuuuuDuuuDUuuuuuuuuD

' (

t

FORM I SV-1DVQ _ Data Validator

23482 CNF<*8 SfWPLE DPTP P8CKPGE 44

1C . EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET




Sample wt/vol: 1000 (g/mL) mL Lab File ID: G2D08425A07







6#51-28-5---------2,4-Dinitrophenol_ ^^n TT Y100-02-7--------4 -Nitrophenol___~132-64-9--------Dibenzofuran121-14-2--------2,4-Dinitrotoluene84-66-2---------Diethylphthalate7005-72-3-------4-Chlorophenyl-phenylether86-73-7---------Fluorene100-01-6--------4-Nitroaniline534-52-l--------4,6-Dinitro-2-methylphenol86-30-6---------N-nitrosodiphenylamine (1)101-55-3--------4-Bromophenyl-phenyletEer118-74-1--------Hexachlorobenzene87-86-5---------Pentachlorophenol85-01-8---------Phenanthrene120-12-7--------Anthracene86-74-8---------Carbazole84-74-2---------Di-n-butylphthalate_206-44-0-------- Fluoranthene_____~129-00-0--------Pyrene85-68-7- —— - - - - - Butylbenzylphthalate

-Dichlorobenzidine56-55-3------- - -Benzo (a) anthracene2 1 8 - 0 1 - 9 - - - - - - - - Chry s ene117-81-7--------bis(2-Ethylhexyl)phthalate117-84-0--------Di-n-octylphthalate_____'205-99-2--------Benzo(b)fluoranthene207-08-9--------Benzo(k)fluoranthene50-32-8---------Benzo(a)pyrene193-39-5--------Indenod, 2,3-cd) pyrene53-70-3---------Dibenzo(a, h)anthracene191-24-2--------Benzo(g,h,i)perylene

7507502303003003002107507503003003007502203003530033300300300300300300300300300300300300300

UuDJUUUDJUUuuuuDJUDJUDJUUUUUUUUUUUUu


FORM I SV-2 OLM03.0

AR30822923482 CNF40 SflWPLE DPTP PPCKPGE 449





Sample wt/vol: 1000 (g/mL) mL Lab File ID: G3D08433C07







108-95-2----111-44-4----95-57-8 ————^ A •* T "^ ^541-73-1----

95-50-1 ————95-48-7 ————108-60-1----106-44-5----

C7-79-1 --~_-O / / A J- — — —jO — jD— J -— —TQ CQ _1 _ _ _

OO /D"D — -—105-67-9 ———111-91-1 ———

91-20-3 ————

QT C7_C_ _ _yj.-D /-b----77-47-4 ————

95-95-4 ————

131-11-3 ———

606-20-2 ———

m----Phenol- - - -bis ( 2 - Chloroethyl ) ether- - - - 2 -Chlorophenol----1,3 -Dichlorobenzene

- - - - 2 -Methylphenol----2,2' -oxybis (1-Chloropropane)- - - -4 -Methylphenol- - - -N-Nitroso-di-n-propylamine _

- - - - Isophorone- - - - 2 -Nitrophenol----2,4 -Dimethylphenol----bis (2-Chloroethoxy) methane----2,4 -Dichlorophenol

, At i t 1 i. J- li-LUx, UUdl CllC- - - -Naphthalene----4-Chloroaniline- - - -Hexachlorobutadiene- - - -4 -Chloro-3 -methylphenol ____- - - - 2 -Methylnaphthalene- - - -Hexachlorocyclopentadiene----2,4,6 -Trichlorophenol----2,4,5 -Trichlorophenol- - - - 2 - Chloronaphthalene- - - - 2 -Nitroaniline- - - -Dimethylphthalate

4-M **MA rf**fe>** \ *4

----2,6-Dinitrotoluene- - - - 3 -Nitroaniline

(3M3>60006000600060006000

1 50 ore6000

60006000600060006000

60006000

_ 6000

600060006000

<225B3600060001500060001500060006000600015000/ZuW

9uuuuuDUDUUUUUDUUUDUUUDJUUUUUUUUUDJ

*

FORM I SV-1 OLM03.0

DVQ = Data Validatorfl R 3 Q 82 30Qualifier

23482 CNF4Q '-PMPLE DPTP PPCKPGE 554




Macrix: (soil/water) WATER Lab Sample ID: 708433








51-28-5---------2,4-Dinitrophenol100 -02 -7------- -4 -Nitrophenol132-64-9------- -Dibenzof uran121-14-2--- -----2, 4 -Dinitrotoluene84-66-2- --------Diethylphthalate7005-72-3 -------4-Chlorophenyl-phenylether _

100-01-6- -------4-Nitroaniline534-52-l--------4,6-Dinitro-2-methylphenol _86-30-6-------- -N-nitrosodiphenylamine_ ( 1 ) _101 -55 -3 - ------ -4 -Bromophenyl -phenylether

87-86-5--------- Pentachlorophenol

120-12-7------- -Anthracene86-74-8-------- -Carbazole84-74-2---------Di-n-butylphthalate206-44 -o------- -Fluoranthene

85-68-7--------- Butylbenzylpht halate91-94-1- ------ --3, 3' -Dichlorobenzidine

218 -01-9- -------Chrysene117-81-7--------bis(2-Ethylhexyl)phthalate117-84-0--- -----Di-n-octylphthalate205-99-2---- —— -Benzo (b) f luoranthene207-08-9------ - -Benzo (k) f luoranthene

193-39-5-------- Indeno ( 1 , 2 , 3 - cd ) pyrene53-70-3-------- -Dibenzo ( a , h) anthracene191-24-2- -------Benzo (g,h, ijperylene

1500015000

600060006000

150001500060006000600015000

600060006000isofi)1000600060006000600060006000600060006000600060006000

UUDJUUUDJUUUUUuDJUuuDJDJUUUUUUUUUUUU

*


FORM I SV-2 OLM03.0






Sample wt/vol: 1000 (g/tnL) mL Lab File ID: G2D08434C07







108-95-2- -------Phenol ____^_^^^___111-44-4--- —— --bis (2-Chloroethyl) ether95-57-8---------2-Chlorophenol_541-73-1--------1,3-Dichlorobenzene_______106-46-7--------1,4-Dichlorobenzene_______95-50-1---------1,2-Dichlorobenzene_______95-48-7---------2-Methylphenol________108-60-l--------2,2'-oxybis(1-Chloropropane)106-44-5--——---4-Methylphenol_621-64-7--------N-Nitroso-di-n-propylamine67-72-1---------Hexachloroethane_________98-95-3---------Nitrobenzene____________78-59-l---------Isophorone88-75-5---------2-Nitrophenol105-67-9--------2,4-Dimethylphenollll-91-l--------bis(2-Chloroethoxy)methane120-83-2--------2,4-Dichlorophenol120-82-1--------1,2,4-Trichlorobenzene91-20-3 —— -----Naphthalene106-47-8--------4-Chloroaniline87-68-3--------- Hexachlorobut adiene ~~"59-50-7------——4-Chloro-3-methylphenol91-57-6- —— ----2-Methylnaphthalene77 -47-4 - ------- -Hexachlorocyclopentadiene88-06-2---——---2,4,6-Trichlorophenol_____95-95-4------——2,4,5-Trichlorophenol_____91-58-7---------2-Chloronaphthalene_______88-74-4---——--2-Nitroaniline131-11-3--------Dimethylphthalate_208-96-8------- -Acenaphthylene606-20-2--------2,6-Dinitrotoluene_99-09-2--- ——— -3-Nitroaniline83-32-9-- —— ——Acenaphthene_____

250025002500nooooj250025002500600250025006200250062002500250025006200440

DUUUUUDJUDUUUUUDJUUUDUUUDJUUUUUUUUUDJ

FORM I SV-1 OLM03.0

23482 CHF40 SPMPLE DPTP PPCKPGE 64S


CNA94DLLab Name: COMPUOffiM ENV. CORP. Contract: 68D50004










51-28-5---------2,4-Dinitrophenol_100-02-7--------4 -Ni t rophenol___~132-64-9--------Dibenzofuran121-14-2--------2,4-Dinitrotoluene84-66-2---------Diethylphthalate7005-72-3-------4-Chlorophenyl-phenylether86-73-7---------Fluorene100-01-6--------4-Nitroaniline534-52-1--------4,6-Dinitro-2-methylphenol86-30-6---------N-nitrosodiphenylamine_(1)_101-55-3------- -4 -Brotnophenyl-phenylether__118-74-1--------Hexachlorobenzene________87-86-5---------Pentachlorophenol________85-01-8---------Phenanthrene____________120-12-7--------Anthracene_____________86-74-8---------Carbazole84-74-2---------Di-n-butylphthalate_206-44-0-------- Fluorant hene_____~129-00-0--------Pyrene85-68-7-------- -Butylbenzylphthalat e

-Dichlorobenzidine56-55-3-------- -Benzo (a) anthracene218-01-9- -------Chrysene117-81-7——-----bis(2-Ethylhexyl)phthalate117-84-0--------Di-n-octylphthalate____'205-99-2---- —— -Benzo (b) f luoranthene______207-08-9--------Benzo(k)fluoranthene______50-32-8---------Benzo(a)pyrene193-39-5--------Indeno(1,2,3-cd)pyrene_53-70-3---------Dibenzo(a,h)anthracene]191-24-2--------Benzo(g,h,i)perylene

620062002902500250025002500620062002500250025006200250025002500250025002500250025002500250025002500250025002500250025002500

UUDJUUUUUUUUUUUUUUUUUUuuuuuuuuuu

(1) - Cannot be separated from Dipnenylamine

FORM I SV-2 OLM03.6

AR30823323482 CNF4Q SPMPLE DPTP PPCKPGE 649


VBLKJLLab Name: COMPUCHEM ENV. CORP. Contract: 68D50004

Lab Code: COMPU Case No.: 23482 SAS No.: SDG No.: CNF40 -^

Matrix: (soil/water) WATER Lab Sample ID: VBLKJL

Sample wt/vol: 5.0 (g/mL) mL Lab File ID: CB950427B52

Level: (low/med) LOW Date Received: ______





74-87-3---------Chloromethane_74-83-9---------Bromomethane75-01-4---------Vinyl ChloricEe"

-Chloroethane75-09-2---------Methylene Chloride67-64-1---------Acetone _________75-15-0---------Carbon Disulfide75-35-4---------1,1-Dichloroethene______75-34-3---------1,1-Dichloroethane540-59-0--------l,2-Dichloroethene (total)

•Chloroform107-06-2--------l,2-Dichloroethane_7S-93-3---------2-Butanone71-55-6---------1,1,1-TricnToroethane56-23-5---------Carbon Tetrachloride75-27-4---------Bromodichloromethane_78-87-5---------l,2-Dichloropropane10061-01-5------cis-l,3-Dichloropropene_79-01-6---------Trichloroethene124-48-1--------Dibromochloromethane_79-00-5---------1,!,2-Trichloroethane_71-43-2---------Benzene10061-02-6------trans-1,3-Dichloropropene

•Bromoform108-10-l--------4-Methyl-2-Pentanone591-78-6------ - -2 -Hexanone________~127-18-4 ———— -79-34-5---------1,1,2,2-Tetrachloroethane

•Toluene108-90-7--------Chlorobenzene_100-41-4--------Ethylbenzene_J100-42-5--------Styrene1330-20-7—————Xylene (Total)

10101010101010101010101010101010101010101010101010101010

uuuuJuuuuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I VOA OLM03.0

AR3Q8231*

IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDSVBLKJL

Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004


Matrix: (soil/water) WATER Lab Sample ID: VBLKJL

Sample wt/vol: 5.0 (g/mL) mL Lab File ID: CB950427B52





CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) ug/L

CAS NUMBER

1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

COMPOUND NAME RT EST. CONC. Q

FORM I VOA-TIC OLM03.0

AR308235

23482 CNF40 SPMPLE DPTP PPCKPGE 2S5


Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004VBLKMI


Matrix: (soil/water) WATER Lab Sample ID: VBLKMI

Sample wt/vol: 5.0 (g/mL) mL Lab File ID: CB950503A52





CONCENTRATION UNITS:CAS NO. COMPOUND {ug/L or ug/Kg) ug/L Q

74-87-3---------Chloromethane_74-83-9---------Bromomethane75-Ol-4---------Vinyl ChloriHe"75-00-3---------Chloroethane75-09-2---------Methylene Chloride____67-64-1---------Acetone _________75-15-0---------Carbon Disulfide75-35-4---------1,1-Dichloroethene______75-34-3---------1,!-Dichloroethane___540-59-0--------l,2-Dichloroethene (total)67-66-3---------Chloroform107-06-2--------l,2-Dichloroethane_7S-93-3---------2-Butanone71-55-6---------1,1,1-Trichloroethane56-23-5---------Carbon Tetrachloride__75-27-4---------Bromodichloromethane__78-87-5---------l,2-Dichloropropane___10061-01-5------cis-1,3-Dichloropropene_79-01-6---------Trichloroethene124-48-i--------Dibromochloromethane_79-00-5---------1,!,2-Trichloroethane

10061-02-6------trans-1,3-Dicnloropropene_75-25-2---------Bromoform

•4-Methyl-2-Pentanone591-78-6--------2-Hexanone127-18-4--------Tetrachloroethene79-34-5---------l,l,2,2-Tetrachloroethane

•Toluene108 -*90 -7 --------Chlorobenzene_10 0 - 41 - 4 - - - - - - - - Ethylbenzene_J100-42-5--------Styrene

,_7__-__,_Xylene (Total)

10101010101010101010101010101010101010101010101010101010


FORM I VOA OLM03.0

AR308236 '23482 CNF4Q SPMPLE DPTP PPCKPGE 291


TENTATIVELY IDENTIFIED COMPOUNDS

Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004VBLKMI


Matrix: (soil/water) WATER Lab Sample ID: VBLKMI

Sample wt/vol: 5.0 (g/mL) mL Lab File ID: CB950503A52






CAS NUMBER

1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.


FORM I VOA-TIC OLM03 . 0

AR30823723482 CNF4Q SPMPLE DPTP PPCKPGE 29.

LA EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

VBLKVHLab Name: COMPUCHEM ENV. CORP. Contract: 68D50004

Lab Code: COMPU Case No.: 23482 SAS No.: SDG No.: CNF40 •—_Matrix: (soil/water) WATER Lab Sample ID: VBLKVH

Sample wt/vol: 5.0 (g/mL) mL Lab File ID: CB950504C52





CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L, or ug/Kg) ug/L Q

74-87-3- —— --

75-01-4------75-00-3------

67-64-1------*?er ic n — _ _ —/D-J.D-U-- ---75-35-4 —————75-34-3 —————540-59-0-- ——67-66-3 ———— -

71-55-6 —————56-23-5 —————7C-27-4---- --t & / I

10061-01-5 ——

1 24-48-1-----^ j^ ' Jl ' Ju LJ J*.

79-00-5------71-43-2------10061-02-6---7S-2^-2------f *J ** *J **

108-10-1-----

79-34-5 —————

100-41-4-- ——100-42-5 ————

- - - Chlorome thane- - -Bromomethane---Vinyl Chloride- - -Chloroethane---Methylene Chloride

---Carbon Disulfide- - - 1 , 1 -Dichloroethene

---1,2 -Dichloroethene (total) _---Chloroform---1,2 -Dichloroethane- - - 2 -Butanone---1, 1, 1 -Trichloroethane---Carbon Tetrachloride- - -Bromodichloromethane---1,2 -Dichloropropane- - -cis- 1 , 3 -Dichloropropene ____

A » 1^»**rfi \ A- «••**•» Wf A4* i**W

- - -Dibromochloromethane---1, 1, 2 -Trichloroethane

- - - trans -1,3 -Dichloropropene- - -Bromof orm- - - 4 -Methyl - 2 - Pentanone

- - -Tetrachloroethene---1,1,2,2 -Tetrachloroethane- - -Toluene

- - -Ethylbenzene---Styrene—— Xylene (Total)

10101010

10101010101010101010101010101010101010101010101010101010


FORM I VGA OLM03.0

AR3082387.T4S2 CNF40 F^WPLE DPTP PPCKPGE 297

IE . EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDSVBLKVH



Matrix: (soil/water) WATER Lab Sample ID: VBLKVH

Sample wt/vol: 5.0 (g/mL) mL Lab File ID: CB950504C52






CAS NUMBER

1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.


"

FORM I VOA-TIC

23482 CNF40 SPMPLF DPTP PPCKQGE 29.9


VHBLK30Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004

Lab Code: COMPU Case No. : 23482 SAS No. : SDG No. : CNF40 •~—Matrix: (soil/water) WATER Lab Sample ID: 706141







74-87-3---------Chloromethane_74-83-9---------Bromomethane75-01-4---------Vinyl Chlori3e]75-00-3---------Chloroethane75-09-2---------Methylene Chloride67-64-1---------Acetone,-15-0---------Carbon Disulfide

75-35-4---------1,1-Dichloroethene______75-34-3---------1,1-Dichloroethane540-59-0--------l,2-Dichloroethene (total)67-66-3---------Chloroform107-06-2--------l,2-Dichloroethane_78-93-3---------2-Butanone71-55-6---------1,1,1-Trichloroethane56-23-5---------Carbon TetrachlorideJ75-27-4---------Bromodichloromethane_78-87-5---------l,2-Dichloropropane10061-01-5------cis-l,3-Dichloropropene_79-01-6---------Trichloroethene

48-1--------Dibromochloromethane_79-00-5---------l,l,2-Trichloroethane_71-43-2---------Benzene10061-02-6------trans-1,3-Dichloropropene_75-25-2---------Bromoform108-10-1--------4-Methyl-2-Pentanone_591-78-6--------2-Hexanone127-18-4--------Tetrachloroethene79-34-5---------1,1,2,2-TetrachloroetHane"108-88-3--------Toluene108-90-7--------Chlorobenzene^100-41-4--------Ethylbenzene_]100-42-5--------Styrene1330-20-7-------Xylene (Total)

10101010

10101010101010101010101010101010101010101010101010101010

uuuuJBuuuuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I VOA OLM03.0

234S2 CNF40 SPMPLE DPTP PPCKPGE


TENTATIVELY IDENTIFIED COMPOUNDSVHBLK30










CAS NUMBER

1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

COMPOUND. NAME RT EST. CONC. Q

FORM I VOA-TIC OLM03 . 0

AR3082UI23482 CNF40 SPMPLE DPTP PPCKPGE . 30

IB EPA SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SBLK28Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004





% Moisture: _____ decanted: (Y/N)__ ' Date Extracted:05/02/95





1 n Q _ OC "5 __

111-44-4 ———95-57-8 ————541-73-1 ———106-46-7 ———95-50-1 ————QC AQ 7 _ _ _ —

108-60-1 ———106-44-5----f 1 1 /" A *J621-64-7----f~t Tl 167- /2-1- ----QQ QC "3 _ _ _ _

»7Q C Q 1 _ _

QQ 7C C _ _ _

111-91-1 ———

106-47-8----

59-50-7 ————91-57-6 ————77-47-4 ————

95-95-4 ————Q1 CQ 7 ___yi-oo- /- ---oo — /•*— ** __ — —131-11-3 ———^ n /" ^ f\ *\606-20-2----99-09-2-----J J W 3 4*

----Phenol----bis (2 -Chloroethyl) ether ___- - - - 2 - Chlorophenol----1, 3 -Dichlorobenzene

_ _ _ _ 2 -Methylphenol----2,2' -oxybis { 1 - Chloropropane )- - - -4-Methylphenol- - - -N-Nitroso-di-n-propylamine _- - - -Hexachloroethane- - - -Nitrobenzene- - - - I sophorone- - - - 2 -Nitrophenol____ 2 , 4-Dimethylphenol----bis (2 -Chloroethoxy) methane----2,4- Dichlorophenol----1,2,4 -Trichlorobenzene- - - -Naphthalene_ _ _ -4-Chloroaniline- - - -Hexachlorobutadiene- —— 4 -Chloro-3 -methylphenol_ _ _ _ 2 -Methylnaphthalene- - - -Hexachlorocyclopentadiene----2,4,6 -Trichlorophenol—— 2,4,5-Trichlorophenol- - - - 2 -Chloronaphthalene

iYXUXUcUiXXXXlC

- - - -Dimethylphthalate

----2,6 -Dinitrotoluene----3-Nitroaniline- — Acenaphthene

101010101010101010101010101010101010101010101010102510251010102510

UUUUUUUUuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I SV-1 OLM03.0

AR3082U223482 CNF40 SPMPLE DPTP PPCKPGE







% Moisture: _____ decanted: (Y/N)__. Date Extracted:05/02/95





C 1 TO C51-28-5-----100-02-7----i T2 64 9-±J4 w^ y1 OT -.1 4-2 - _j.4,±, -i. ff84-66-2-----7005-72-3 ——86-73-7 ————100-01-6----c. "34-52-1----_?j*± -j£i -L86-30-6-----101-55-3 ———118-74-1 ———QT nc_ £ _ _ _ _ _85-01-8-- ——120-12-7 ———86-74-8-----P.4-74-2-----U~X f **

206-44-0----129-00-0----85-68-7-- ——91-94-1 ————56-55-3 ————71 8-01-9-----b ±Q \S.JU _/^ 1 'T O T ^117-oi- /----1 1 O A f\117-O4-U----*> f\ C QQ 120b-yy-^-----on7_no_Q____.en ^ i ob 0 -o _;-B------193-39-5-----J. J _Jr *J J -**

53-70-3 ———— -1 <31 -24-2-----X7X ^^ ft

- - - -2 , 4 -Dinitrophenol- - - -4 -Nitrophenol- - - -Dibenzof uran----2,4 -Dinitrotoluene- - - -Diethylphthalate- - - -4 -Chlorophenyl -phenylether _----Fluorene- - - -4 -Nitroaniline----4, 6-Dinitro-2-methylphenol _- - - -N-nitrosodiphenylamine (1) _- - - -4 -Bromophenyl -phenyletHer __- - - -Hexachlorobenzene- - - - Pentachlorophenol- - - - Phenanthr ene

----Carbazole- - - -Di-n-butylphthalate- - - - Fluoranthene----Pyrene- - - -Butylbenzylphthalate----3,3' -Dichlorobenzidine

X*4**i* J W_-*ll_»

- - - -bis { 2 -Ethylhexyl ) phthalate _• - - -Di -n-octylphthalate- - - -Benzo (b) f luoranthene

• - - -Benzo (a) pyrene• - - - Indeno (1,2, 3 -cd) pyrene•---Dibenzo(a,h) anthracene• - - -Benzo (g, h, i) perylene

25251010101010252510101025101010101010101010101010101010101010

UUUUuuuuuuuuuuuuuuuuuuuuuuuuuuu

(1) Cannot be separated from Diphenylamine

FORM I SV-2 OI_ 03.0

AR3082U3234S2 CNF40 SPMPLE DPTP PPCKPGE S9S

IF , EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDSSBLK28











CAS NUMBER

1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

COMPOUND NAME

UNKNOWN (BC)

RT

15.51

EST. CONC.

3

Q

J

FORM I SV-TIC OLM03.0

AR3082UI*

23482 CNF40 SPMPLE DPTP PPCKPGE . S99


SBLK29Lab Name: CompuChem Env. Corp. Contract: 68D50004


Matrix: (soil/water) WATER Lab Sample ID: 7107G4








108-95-2——————Phenol_______^__^__111-44-4——————bis(2-Chloroethyl) ether_95-57-8———————2-Chlorophenol541-73-1——————1,3-DichIorobenzene_106-46r7——————1,4 -Dichlorobenzene"95-50-1——————1,2-Dichlorobenzene"95-48-7——————2-Methylphenol108-60-1——————2,2' -oxybis (1-Ch lor opr opane)106-44-5——————4-Methylphenol621-64-7——————N-Nitroso-di-n-propy lamine67-72-1——————Hexachloroethane_________98-9 5-3 ———————Nitrobenzene_____________78-59-1———————Isophorone88-75-5——————2-Nitrophenol105-67-9——————2,4-Dimethylphenol_______111-91-1——————bis (2-Chloroethoxy) methane_120-83-2——————2,4-Dichlorophenol120-82-1—————1,2,4-Trichlorobenzene91-20-3——————Naphthalene_106-47-8——————4-Chloroaniline87-68-3——————Hexachlorobutadiene59-50-7——————4-Chloro-3-methylphenol_91-57-6——————2-Methylnaphthalene_77-47-4——————Hexachlorocyclopentadiene_88-06-2——————2,4,6-Trichlorophenol95-95-4——————2,4,5-Trichlorophenol91-58-7——————2-Chloronaphthalene_____88-74-4——————2-Nitroaniline131-11-3——————Dimethylphthalate_208-96-8——————Acenaphthylene606-20-2——————2, 6-Dinitrotoluene_99-09-2——————3 -Ni troani 1 ine83-32-9———————Acenaphthene_____

101010101010101010101010101010101010101010101010102510251010102510

UUUUUUuuuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I SV-1 OLM03.0

AR3Q82l*523482 CNF40 SPMPLE DPTP PPCKPGE 9Q9



Lab Code: COMPU Case No.: 23482 SAS No.:-- SDG No.: CNF40


Sample wt/vol: 1000 (g/mL) mL Lab File ID: GJ0107 4C07




Injection Volume: 2.0(uL) t Dilution Factor: 1.0

GPC Cleanup: (Y/N) N pK: ___


51-28-5———————2,4-Dinitrophenol100-02 -7——————4 -Nitropheno 1___~132-64 -9 ——————Dibenzof uran121-14-2—————2,4-Dinitrotoiuene84-66-2——————Diethylphthalate7005-72-3—————4-Chloropheny1-phenylether86-7 3 -7———————Fluorene100-01-6=-————4-Nitroaniline534-52-1—-———4,6-Dinitro-2-methylphenol86-30-6——————N-nitrosodiphenylamine_(l)~101-55-3——————4-Bromophenyl-phenylether_J118-74-1——————Hexachlorobenzene_______87-86-5——————Pentachlorophenol_______85-01-8——————Phenanthrene___________120-12-7—————Anthracene____________86-74-8——————Carbazole84-74-2——•-"——Di-n-butylphthalate206-44-0——————Fluoranthene_____]129-00-0——————Pyrene85-68-7——————Butylbenzylphthalate91-94-1——————3,3' -Dichlorobenzidine_56-55-3———————Benzo (a) anthracene218-01-9——————Chrysene117-81-7 -—————bis (2 -Ethylhexyl) phthalate117-84-0—-———Di-n-octylphthalate______205-99-2——————Benzo (b) f luoranthene_____207—08-9——————Benzo (k) f luoranthene_____50-32-8——————Benzo (a) pyrene_________193-39-5——————Indeno (1,2,3-53-70-3——————Dibenzo(a,h) anthracen131-24-2—————Benzo(g,h,i)perylene

25251010101010252510101025101010101010101010101010101010101010


(:.) - Cannot be separated from Diphenylaraine

FORM I SV-2 OLM03.0

AR3082U6no TO

IF EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET


Lab Name: CompuChem Env. Corp. Contract: 68D50004

Lab Code: COMPU Case NO.: 23482 SAS No.: SDG No.: CNF40









GAS NUMBER

1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.


- 9

FORM I SV-TIC .«onOOli7 OLM03.0AR3082U7

23482. CNF4Q SPMPLE DPTP PPCKPGE 911

IB EPA SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET






% Moisture: ____ decanted: (Y/N)__ Date Extracted: 04/27/95




CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or Ug/Kg) ug/L Q

108-95-2 ————111-44-4 ————95— D / o— —— — — —541—73-1 —————^*m ± / -k

106-46-7 ————

95-48-7 —————108-60-1 ————106-44-5 ————621-64-7 ————

oo— /i>— D— — — — ~105-67-9 ————111-91-1 ————

91-20-3 —————106-47-8 ————

*_T «* <rf W *

91-57-6 —————77-47-4 —————

95-9 5-4 —— - — •3 •* *f ** T

88-74-4 —————131-11-3 ————** ^ **

—— Phenol—— bis (2-Chloroethyl) ether ___—— 2 -chlorophenol—— 1, 3— Dichlorobenzene

—— 1, 2— Dichlorobenzene—— 2 -Methylphenol—— 2 , 2 ' -oxybis ( l-Chloropropane)—— 4-Methylphenol—— N-Nitroso-di-n-propylamine _—— Hexachloroethane

11 4. i W*-«*— i ***<—* H»

—— Isophorone—— 2 -Nitr opheno 1—— 2 , 4-Dimethylphenol—— bis ( 2-Chloroethoxy ) methane _—— 2 , 4-Dichlorophenol

f Ai t *t J.i i.\f\\±\Ji. (JJjBllOBllC

—— Naphthalene—— 4-Chloroaniline—— Hexachlorobutadiene—— 4-Chloro-3-methylphenol ___—— 2 — Me thy Inaphtha lene—— Hexachlorocyclopentadiene—— 2 , 4 , 6-Trichlorophenol—— 2 , 4 , 5-Trichlorophenol—— 2— Chloronaphthalene—— 2-Nitroaniline—— Dimethylphthalate

rUrftSilClf IlUliy •_«-» WS—— 2 , 6-Dinitrotoluene—— 3 -Nitroaniline

AU»die;iyiit.tW3iit!

101010101010101010101010101010101010101010101010102510251010102510

UUUUUuUUuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I SV-1 OLM03.0

AR3082U8'J4S2 CNF4Q SPMPLE DPTP PPCKPGE 92J












51-28-5——————2,4-Dinitrophenol100-02-7——————4-Nitrophenol___~132-64-9——————Dibenzofuran121-14-2——————2,4-Dinitrotoluene84-66-2——————Diethylphthalate7005-72-3—-————4-Chlorophenyl-phenylether86^73-7——————Fluorene100-01-6——————4-Nltroaniline534-52-1——————4,6-Dinitro-2-methylphenol_86-3 0-6——————N-nitrosodipheny lamine_ (1)"101-55-3——————4-Bromophenyl-phenylether_118-74-1——————Hexa Chlorobenzene_______87-86-5——————Pentachlorophenol_______85-01-8——————Phenanthrene___________12 0-12 -7 ——————Anthracene____________86-74-8———————Carbazole84-74-2——————Di-n-butylphthalate206-44-0——————Fluoranthene_____"129-00-0—————Pyrene85-68-7———————Butylbenzylphthalate91-94-1——————3,3' -Dichlorobenzidine_56-55-3——————Benzo (a) anthracene218-01-9——————Chrysene117-81-7——————bis (2-Ethy Ihexyl) phthalate117-84-0——————Di-n-octylphthalate_____~205-99-2——————Benzo (b) f luoranthene_____207-08-9——————Benzo (k) f luoranthene_____50-32-8——————Benzo (a) pyrene_________193-39-5——————Indeno (1,2,3-cd) pyrene53-70-3——————Dibenzo(a,h)anthracene"191-2 4 -2 ——————Benzo (g, h, i) pery lene

25251010101010252510101025101010101010101010101010101010101010



OIM03.0AR3082U9

23432 CNF4Q SPMPLE DPTP PPCKPGE 924

IF EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET


Lab Name: CompuChem Env. Corp. Contract: 68D50004




Level: (low/tned) LOW Date Received: ______



Inj ection Volume: 2.0 (uL) Dilution Factor: 1.0



CAS NUMBER-a-a ———— «_=S____B:

2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

COMPOUND NAME

LABORATORY ARTIFACT ———————UNKNOWN (BC)

RT

——— 15.3818.04

EST. CONC.

——————————— fr6

Q•ft- — - ——

J

•.

FORM I SV-TIC OLM03.0

AR308250'3432 CNF4Q SPMPLE DPTP PPCKPGE 925




Matrix: (soil/water) WATER Lab Sarrple ID: 708921








108-95-2--------Phenol____lll-44-4--------bis(2-Chloroethyl)ether95-57-8---------2-Chlorophenol541-73-i--------l,3-Dichlorobenzene_106-46-7--------l,4-Dichlorobenzene"95-50-1———————1,2-] _______95-48-7---------2-Methylphenol_________[108-60-l--------2,2'-oxybis(1-Chloropropane;106-44-5-----——4-Methylphenol

•N-Nitroso-di-n-propylamine_67-72-1---------Hexachloroethane98-95-3---------Nitrobenzene_78-59-1---------Isophorone88-75-5——————2-Nitrophenol

•2,4 -Dimethylphenol111-91-1--------bis(2-Chloroethoxy)methane120-83-2--------2,4-Dichlorophenol120-82-l--------l,2,4-Trichlorobenzene91-20-3-- —— -——Naphthalene106-47-8--------4-Chloroaniline

• Hexachlorobutadiene•4-Chloro-3-methylphenoT

91-57-6------——2-Methylnaphthalene_____77-47-4-------- -Hexachlorocyclopentadiene88-06-2-----——-2,4,6-Trichlorophenol95-95-4---------2,4,5-Trichlorcphenol_____91-58-7——-----2-Chloronaphthalene_______88-74-4-----——-2-Nitroaniline131-11-3——————Dimethylphthalate_208-96-8--------Acenaphthylene606-20-2--------2,6-Dinitrotoluene99-09-2----- —— -3-Nitroaniline___~83-32-9---------Acenaphthene_____

101010101010101010101010101010101010101010101010102510251010102510

UUUUUUUUUUUUuuuuuuuuuuuuuuuuuuuuu

FORM I SV-1 OLM03.0

AR30825I'3482 CNF40 SPMPLE DPTP PPCKPGE 93?

1C EPA SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET



Matrix: (soil/water) WATER Lab Sample ID: 7C8921








51-28-5-----100-02-7----1 7-fi4-9----XJ£> w^ -'191-1 4.-?----±.ft±. i ft

84-66-2 ————7005-72-3---

100-01-6----m4-c2-l-----J -J -L *J *- <J-

86-30-6 ————101-55-3----.JU W -IP - — ' »**

118-74-1 ———n <~t of c87-oo-b-----

1 on~l 9 7-- -xzu — j.z / — —86-74-8 ————fl4-74-?-----O^ it ft

206-44-0 ———129-00-0 ———O C CQ *7_-. __

91-94-1-----56-55-3 ————218-01-9----ft ±\J \J _k m*

117-81-7 ———117-84-0 ———9 n S, - Q 9 - 2 - - - -ft \i j y y fi

50-32-8 ————193-39-5----JU-7-J J -/ *-*

53-70-3 ————1 Q.l-24-2----_L _7 _b Jl -u

----2,4 -Dinitrophenol_ , _ -4 -Nitrophenol- - - -Dibenzof uran----2,4 -Dinitro toluene- - - -Diethylphthalate- - - -4 -Chlorophenyl -phenylether _----Fluorene- - - -4 -Nitroaniline----4, 6-Dinitro-2-methylphenol _- - - -N-nitrosodiphenylamine ( 1 ) _- - - -4 -Bromophenyl -phenyletHer

- - - - Pentachlorophenol- - - - Phenanthrene

- - - -Di-n-butylphthalate- - - - Fluoranthene----Pyrene- - - -Butylbenzylphthalate

, J U *IJ-LU£ULJCI1 J.U.LI1C

• fc 1 ill J h** 4* ^

- - - -bis ( 2 -Ethylhexyl ) phthalate— -Di-n-octylphthalate- - - -Benzo (b) f luoranthene- - - -Benzo (k) f luoranthene

----Indeno (1, 2, 3-cdi pyrene

- - - -Benzo (q , h, i ) perylene

25251010101010252510101025101010101010101010101010101010101010



-^—————

FORM I SV-2 OLM03.0

AR308252234S2 CNF40 SPMPLE DPTP PPCKPGE 9-3S

IF EPA SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS

Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004SBLK68










CAS NUMBER

1.2.3.4.5. 122-99-66.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

COMPOUND NAME

SUBSTITUTED ALCOHOL (BC)SUBSTITUTED ALCOHOL (BC)SUBSTITUTED ALCOHOL (BC)SUBSTITUTED ALCOHOL (BC)ETHANOL, 2-PHENOXY-UNKNOWN (BC)

RT

6.266.627.449.559.9510.51

EST. CONC.

1338242

Q

JJJJ.NJJ

FORM I SV-TIC „ OIW03.0AR308253

234S2 CNF40 SOMPLE D8TQ PQCXQGF 939

ID ; EPA SAMPLE NOPESTICIDE ORGANICS ANALYSIS DATA SHEET

PBLK59Name :CQMPUCHEM ENV. CORP. Contract: 68D50Q04

Lab Code: COMPU Case No.: 234B2 SAS No.: SDG No.: CNF40


Sample wt/vol: 1000(g/ml)ML Lab File ID:

% Moisture: decanted: (Y/N) Date Received:


Concentrated Extract Volume: 10000(uL) ' Date Analyzed: 05/25/95

Injection Volume: 2.0 fuL) Dilution Factor: 1


CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ua/Ka)UG/L (

319-84-6-----319-85-7-----319-86-8-----58-89-9------76-44-8------309-00-2-----1024-57-3----ysa-jo-o60-57-1------72-55-9------

33213-65-9---72-54-8------

72-43-5------53494-70-5-- -wf *J JL -«/ X 'v *-*

7421 -93 -4-- --/ A A *L -* -J "±

5103-71-9----C103 -74-2----+J -L V J / "X £t

8001-35-2----12674-11-2---11104-28-2---11141-16-5---

1OCT5 *5Q Cizo /_!-<sy-D---TinQT £Q 1 _ _ _

11096-82-5---

-- -alpha -BHC---beta-BHC---delta-BHC- - -gamma -BHC ( Lindane )---Heptachlor---Aldrin.---Heptachlor epoxide---Endosulf an I---Dieldrin---4, 4 '-DDE---Endrin---Endosulfan II---4.4'-DDD---Endosulfan sulfate---4.4'-DDT- - -Methoxychlor---Endrin ketone---Endrin aldehyde- - - alpha - Chlordane- - - aamma - Chlordane---Toxaphene---Aroclor-1016---Aroclor-1221---Aroclor-1232---Aroclor-1242---Aroclor-1248

fVL WlH»^W-L ^ "±

---Aroclor-1260-

0.0500.0500.0500.0500.0500.0500.0500.0500.100.100.100.100.100.100.100.500.100.100.0500.0505.01.02.01.01.01.01.01.0

uU 'uuuuuuuuuuuuuuuuuuuuuuuuuu

AR308255FORM I PEST nuv*ww-~- OLM03 . 0

23482 CNF40 SPMPLE DPTff PBCKOGF 1

ID EPA SAMPLE NOPESTICIDE ORGANICS ANALYSIS DATA SHEET

PBLK50Lab Name:COMPUCHEM ENV. CORP. Contract:68D50004

Lab Code: COMPU Case No.: 23482 SAS No.: SDG No.: CNF4Q



% Moisture: decanted: (Y/N) Date Received:


Concentrated Extract Volume: 10000(uL) ' Date Analyzed: 05/08/95

Injection Volume: 2.0(uL) Dilution Factor: 1.


CONCENTRATION UNITS:CAS NO. ' COMPOUND (ug/L or ua/Ka)UQ/L <

jiy-o*t - o -319-85-7-----

bb-cjy-y76-44-8------309-00-2-----1024 -57-3 - - - -j. \j ft «j / -j

60-57-1------/ Z OD - y - - - - - -72-20-8------33213-65-9---72-54-8------1031-07-8----sn-?9-3- - - -- -J \J ft 3 -*

72-43-5------53494-70-5---7421-93-4----i ** -fci -^ -^ *

5103-71-9----m m -74 -2 - - - -D X U J / *t ^8001-35-2----12674-1T.-2---11104-28-2---11141-16-5---53469-21-9---12672-29-6---11097-69-1---

---alpha-BHCKot-a _nWP

---delta-BHC---qamma-BHC (Lindane)---Heptachlor---Aldrin- - -Heptachlor epoxide---Endosulfan I---Dieldrin_ _ _ 4 4 ' - DDE•* f t LJ it-find

---Endrin---Endosulfan II---4.4' -DDD---Endosulfan sulfate_ _ _ 4, 4 ' _ DDT•a j •» LJLJ JL

- - -Methoxychlor---Endrin ketone---Endrin aldehyde---alpha-Chlordane- - -qamma-Chlordane---Toxaphene---Aroclor-1016---Aroclor-1221---Aroclor-1232---Aroclor-1242---Aroclor-1248---Aroclor-1254---Aroclor-1260

0.0500.0500.0500.0500.0500.0500.0500.0500.100.100.100.100.100.100.100.500.100.100.0500.0505.01.02.01.01.01.01.01.0

uU 'uuuuuuuuuu_uuuuuuuuuuuuuuuu

FORM I PES'flR30825U OLM03.0

23482 CNF40 SPMPLE DPTP PPCKPGE 12S6

10A EPA SAMPLE NO.PESTICIDE IDENTIFICATION SUMMARYFOR SINGLE COMPONENT ANALYTES

Lab Name;COMPUCHEM ENV. CORP. Contract:68D5Q004CMW44


Lab Sample ID : 706768 RI Date(s) Analyzed: 05/25^95 05/25/95

Instrument ID (1): VARIAN02 Instrument ID (2): VARIAN03

GC Column(l): DB-608 ID: 0.53(mm) GC Column(2): RTX-1701 ID: 0.53(mm)

ANALYTE

Endosulfan sulfate

—

• •

COL

1

2

1

2

1

2

1

2

1

2

1

2

1

2

1

2

RT

19.67

19.78

RT WIFROM

19.54

19.73

-

NDOWTO

19.68

19.87

page 1 of 1 » . - -

CONCENTRATION

0.0087

0.025

%D

'187.4

^ ——— '

~ i

OLM03.0

23482 CNF4& SPMPLE DPTP PQCk'PGF

10A " EPA SAMPLE NO.PESTICIDE IDENTIFICATION SUMMARY ______________FOR SINGLE COMPONENT ANALYTES

CNA91Name : COMPUCHEM ENV. CORP. Contract: 68D500Q4


Lab Sample ID : 708425 Date(s) Analyzed: 05/09/95 05/09/95

Instrument ID (1): VARIAN09 Instrument ID (2): VARIAN08

GC Column(1): RTX-1701 ID: 0.53(mm) GC Column(2): DB-608 ID: 0.53(mm]

ANALYTE

4.4'- DDD

Endrin ketone

—

r"

COL

1

2

1

2

1

2

1

2

1

2

1

2

1

2

1

2

RT

18.22

21.83

22.27

26.91

RT W]FROM

18,16

21.73

22.21

26.78

-

:NDOWTO

18.30

21.87

22.35

26.92

CONCENTRATION

0.012

0.013

0.011

0.0056

%D

8.3

96.4

• *

page 1 of 1 _FORM X PEST-1 AR308257 OLM03.0

234.82 CNF40 SPMPLE DPTP PPCKPGE 1068

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DATE : June 22, 1995 · TO: Cynthia Caporale ESAT Regional Project Officer THROUGH: Dale S. Boshart...

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