Page 1 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341001WSLH Sample:
ZANA SJIANWISCONSIN DNR
WT093
ZANA SJIANWISCONSIN DNR
Collection End: 5/23/2018 12:55:00 PM
Point or Outfall:
Project No:
Date Received:Date Reported: Sample Depth:
5/24/20186/8/2018
Customer ID:
Report To: Invoice To:
Field #: TREMP@ARCADIA
Collection Start: Collected By:
County:
Sample Type:
Sample Reason:
Sample Location:Sample Description:
CAMILLE BRUHNSU-SURFACE WATER
TREMPEALEAU RIVER X-619206 Y-4901212
ID#:
Waterbody:
Program Code:Region Code:
0.5F
Sample Comments
For the dissolved metals tests, the sample was filtered and preserved at the lab.
Analyzed past the 15 minutes holding time: Method SM4500-H+B analyzed on 05/24/18 1330
NITRIC ACID USED IN FIELD WAS EXPIRED.
Analyte Result Units LOD LOQ
Inorganic Chemistry
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
52.3TOTAL SUSPENDED SOLIDS mg/L 3.3 3.3SM2540D
05/24/18 05/24/18Prep Date Analysis Date
18.8Chloride mg/L 1.00 3.20SM4500-CL-E
05/24/18 05/24/18Prep Date Analysis Date
Comments:Analyzed past the 15 minutes holding time.
7.83pH SU 1.00 1.00SM4500-H+B
05/25/18 05/25/18Prep Date Analysis Date
33.9Turbidity NTU 0.100 0.100SM2130B
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 2 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341001WSLH Sample:
Analyte Result Units LOD LOQ
Inorganic Chemistry
Analysis Method
05/29/18 05/30/18Prep Date Analysis Date
0.413Phosphorus mg/L 0.00500 0.0160EPA 365.1
Analyte Result Units LOD LOQ
Inorganic Chemistry, Dissolved
Analysis Method
05/24/18 05/25/18Prep Date Analysis Date
0.0412FAmmonia mg/L 0.0150 0.0480EPA 350.1
Analyte Result Units LOD LOQ
Metals, Total Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
670Aluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
1.03FChromium ug/L 1.00 3.00EPA 200.7
NDCopper ug/L 5.00 15.0EPA 200.7
3.15Iron mg/L 0.100 0.300EPA 200.7
NDLead ug/L 3.00 10.0EPA 200.7
4.45FNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
5.94FZinc ug/L 5.00 15.0EPA 200.7
30.1Calcium mg/L 0.100 0.300EPA 200.7
12.3Magnesium mg/L 0.100 0.300EPA 200.7
126Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 3 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341001WSLH Sample:
Analyte Result Units LOD LOQ
Metals, Total
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
Analyte Result Units LOD LOQ
Metals, Total, Low Level
Analysis Method
05/24/18 05/24/18Prep Date Analysis Date
0.453Total Chromium ug/L 0.00150 0.0232Hi Res ICPMS
0.0914Chromium (VI) ug/L 0.0122 0.0232Hi Res ICPMS
20.2% Chromium (VI) %Hi Res ICPMS
Analyte Result Units LOD LOQ
Metals, Dissolved Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
14.8FAluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
NDChromium ug/L 1.00 3.00EPA 200.7
NDCopper ug/L 5.00 15.0EPA 200.7
NDIron mg/L 0.100 0.300EPA 200.7
NDLead ug/L 3.00 10.0EPA 200.7
3.40FNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
NDZinc ug/L 5.00 15.0EPA 200.7
29.3Calcium mg/L 0.100 0.300EPA 200.7
12.4Magnesium mg/L 0.100 0.300EPA 200.7
124Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 4 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341001WSLH Sample:
Analyte Result Units LOD LOQ
Metals, Dissolved
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
Analyte Result Units
Field Data
Analysis Method
15.72Sample Temp-field (C) CentigradeField Data
9.29DO field (mg/L) mg/LField Data
95.3% Saturation %Field Data
7.61pH (SU) field SUField Data
100Cloud Cover % %Field Data
281Cond-fld(uS/CM@25C) UMHOS/CMField Data
28Transparency Tube (cm) CMField Data
LOD = Level of detection LOQ = Level of quantification ND = None detected. Results are less than the LOD F next to result = Result is between LOD and LOQ Z next to result = Result is between 0 (zero) and LOD if LOD=LOQ, Limits were not statistically derived
Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes see http://www.slh.wisc.edu/about/compliance/nelac-laboratory-accreditationResults, LOD and LOQ values have been adjusted for analytical dilutions and percent moisture where applicable.Results relate only to the items tested.This Laboratory Report shall not be reproduced except in full, without written approval of the laboratory.The water microbiology unit analyzes samples as received and not all samples are tested for preservation before analysis is performed.
List of Abbreviations:
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 5 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341001WSLH Sample:
Responsible PartyMicrobiology: Sharon Kluender, Lab Manager, 608-224-6262Inorganic Chemistry: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Metals: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Organic Chemistry: Al Spallato, Lab Manager, 608-224-6269Emergency Chemical Response: Noel Stanton, Lab Manager, 608-224-6251Environmental Toxicology: Tracy Hanke, Lab Manager, 608-224-6270
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 6 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341002WSLH Sample:
ZANA SJIANWISCONSIN DNR
WT093
ZANA SJIANWISCONSIN DNR
Collection End: 5/23/2018 12:26:00 PM
Point or Outfall:
Project No:
Date Received:Date Reported: Sample Depth:
5/24/20186/8/2018
Customer ID:
Report To: Invoice To:
Field #: TREMP@DODGE
Collection Start: Collected By:
County:
Sample Type:
Sample Reason:
Sample Location:Sample Description:
CAMILLE BRUHNSU-SURFACE WATER
X-651729 Y-4887538
ID#:
Waterbody:
Program Code:Region Code:
0.5F
Sample Comments
NITRIC ACID USED IN FIELD WAS EXPIRED.
For the dissolved metals tests, the sample was filtered and preserved at the lab.
Analyzed past the 15 minutes holding time: Method SM4500-H+B analyzed on 05/24/18 1330
Analyte Result Units LOD LOQ
Inorganic Chemistry
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
86.0TOTAL SUSPENDED SOLIDS mg/L 5.0 5.0SM2540D
05/24/18 05/24/18Prep Date Analysis Date
20.5Chloride mg/L 1.00 3.20SM4500-CL-E
05/24/18 05/24/18Prep Date Analysis Date
Comments:Analyzed past the 15 minutes holding time.
7.96pH SU 1.00 1.00SM4500-H+B
05/25/18 05/25/18Prep Date Analysis Date
64.1Turbidity NTU 0.100 0.100SM2130B
05/29/18 05/30/18Prep Date Analysis Date
0.547Phosphorus mg/L 0.00500 0.0160EPA 365.1
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 7 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341002WSLH Sample:
Analyte Result Units LOD LOQ
Inorganic Chemistry, Dissolved
Analysis Method
05/24/18 05/25/18Prep Date Analysis Date
0.0213FAmmonia mg/L 0.0150 0.0480EPA 350.1
Analyte Result Units LOD LOQ
Metals, Total Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
1380Aluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
2.02FChromium ug/L 1.00 3.00EPA 200.7
7.48FCopper ug/L 5.00 15.0EPA 200.7
5.57Iron mg/L 0.100 0.300EPA 200.7
4.63FLead ug/L 3.00 10.0EPA 200.7
5.79FNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
7.63FZinc ug/L 5.00 15.0EPA 200.7
36.9Calcium mg/L 0.100 0.300EPA 200.7
15.9Magnesium mg/L 0.100 0.300EPA 200.7
157Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
Analyte Result Units LOD LOQ
Metals, Total
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 8 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341002WSLH Sample:
Analyte Result Units LOD LOQ
Metals, Total, Low Level
Analysis Method
05/24/18 05/24/18Prep Date Analysis Date
1.44Total Chromium ug/L 0.00150 0.0232Hi Res ICPMS
0.0939Chromium (VI) ug/L 0.0122 0.0232Hi Res ICPMS
6.52% Chromium (VI) %Hi Res ICPMS
Analyte Result Units LOD LOQ
Metals, Dissolved Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
12.4FAluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
NDChromium ug/L 1.00 3.00EPA 200.7
NDCopper ug/L 5.00 15.0EPA 200.7
NDIron mg/L 0.100 0.300EPA 200.7
NDLead ug/L 3.00 10.0EPA 200.7
2.29FNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
NDZinc ug/L 5.00 15.0EPA 200.7
37.6Calcium mg/L 0.100 0.300EPA 200.7
16.1Magnesium mg/L 0.100 0.300EPA 200.7
160Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
Analyte Result Units LOD LOQ
Metals, Dissolved
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 9 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341002WSLH Sample:
Analyte Result Units
Field Data
Analysis Method
15.84Sample Temp-field (C) CentigradeField Data
9.21DO field (mg/L) mg/LField Data
94.8% Saturation %Field Data
7.70pH (SU) field SUField Data
90Cloud Cover % %Field Data
327Cond-fld(uS/CM@25C) UMHOS/CMField Data
16.0Transparency Tube (cm) CMField Data
LOD = Level of detection LOQ = Level of quantification ND = None detected. Results are less than the LOD F next to result = Result is between LOD and LOQ Z next to result = Result is between 0 (zero) and LOD if LOD=LOQ, Limits were not statistically derived
Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes see http://www.slh.wisc.edu/about/compliance/nelac-laboratory-accreditationResults, LOD and LOQ values have been adjusted for analytical dilutions and percent moisture where applicable.Results relate only to the items tested.This Laboratory Report shall not be reproduced except in full, without written approval of the laboratory.The water microbiology unit analyzes samples as received and not all samples are tested for preservation before analysis is performed.
List of Abbreviations:
Responsible PartyMicrobiology: Sharon Kluender, Lab Manager, 608-224-6262Inorganic Chemistry: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Metals: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Organic Chemistry: Al Spallato, Lab Manager, 608-224-6269Emergency Chemical Response: Noel Stanton, Lab Manager, 608-224-6251Environmental Toxicology: Tracy Hanke, Lab Manager, 608-224-6270
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 10 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341003WSLH Sample:
ZANA SJIANWISCONSIN DNR
WT093
ZANA SJIANWISCONSIN DNR
Collection End: 5/23/2018 11:21:00 AM
Point or Outfall:
Project No:
Date Received:Date Reported: Sample Depth:
5/24/20186/8/2018
Customer ID:
Report To: Invoice To:
Field #: LD6
Collection Start: Collected By:
County:
Sample Type:
Sample Reason:
Sample Location:Sample Description:
CAMILLE BRUHNSU-SURFACE WATER
X-625241 Y-4873056
ID#:
Waterbody:
Program Code:Region Code:
Sample Comments
NITRIC ACID USED IN FIELD WAS EXPIRED.
For the dissolved metals tests, the sample was filtered and preserved at the lab.
Analyzed past the 15 minutes holding time: Method SM4500-H+B analyzed on 05/24/18 1330
Analyte Result Units LOD LOQ
Inorganic Chemistry
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
26.0TOTAL SUSPENDED SOLIDS mg/L 5.0 5.0SM2540D
05/24/18 05/24/18Prep Date Analysis Date
19.0Chloride mg/L 1.00 3.20SM4500-CL-E
05/24/18 05/24/18Prep Date Analysis Date
Comments:Analyzed past the 15 minutes holding time.
8.32pH SU 1.00 1.00SM4500-H+B
05/25/18 05/25/18Prep Date Analysis Date
21.5Turbidity NTU 0.100 0.100SM2130B
05/29/18 05/30/18Prep Date Analysis Date
0.141Phosphorus mg/L 0.00500 0.0160EPA 365.1
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 11 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341003WSLH Sample:
Analyte Result Units LOD LOQ
Inorganic Chemistry, Dissolved
Analysis Method
05/24/18 05/25/18Prep Date Analysis Date
0.0163FAmmonia mg/L 0.0150 0.0480EPA 350.1
Analyte Result Units LOD LOQ
Metals, Total Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
339Aluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
NDChromium ug/L 1.00 3.00EPA 200.7
NDCopper ug/L 5.00 15.0EPA 200.7
1.20Iron mg/L 0.100 0.300EPA 200.7
NDLead ug/L 3.00 10.0EPA 200.7
3.01FNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
NDZinc ug/L 5.00 15.0EPA 200.7
55.9Calcium mg/L 0.100 0.300EPA 200.7
22.1Magnesium mg/L 0.100 0.300EPA 200.7
230Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
Analyte Result Units LOD LOQ
Metals, Total
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 12 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341003WSLH Sample:
Analyte Result Units LOD LOQ
Metals, Total, Low Level
Analysis Method
05/24/18 05/24/18Prep Date Analysis Date
0.537Total Chromium ug/L 0.00150 0.0232Hi Res ICPMS
0.0796Chromium (VI) ug/L 0.0122 0.0232Hi Res ICPMS
14.8% Chromium (VI) %Hi Res ICPMS
Analyte Result Units LOD LOQ
Metals, Dissolved Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
12.7FAluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
NDChromium ug/L 1.00 3.00EPA 200.7
NDCopper ug/L 5.00 15.0EPA 200.7
NDIron mg/L 0.100 0.300EPA 200.7
NDLead ug/L 3.00 10.0EPA 200.7
2.36FNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
NDZinc ug/L 5.00 15.0EPA 200.7
57.6Calcium mg/L 0.100 0.300EPA 200.7
22.7Magnesium mg/L 0.100 0.300EPA 200.7
237Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
Analyte Result Units LOD LOQ
Metals, Dissolved
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 13 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341003WSLH Sample:
Analyte Result Units
Field Data
Analysis Method
17.95Sample Temp-field (C) CentigradeField Data
9.19DO field (mg/L) mg/LField Data
98.8% Saturation %Field Data
8.21pH (SU) field SUField Data
50Cloud Cover % %Field Data
469Cond-fld(uS/CM@25C) UMHOS/CMField Data
29.0Transparency Tube (cm) CMField Data
LOD = Level of detection LOQ = Level of quantification ND = None detected. Results are less than the LOD F next to result = Result is between LOD and LOQ Z next to result = Result is between 0 (zero) and LOD if LOD=LOQ, Limits were not statistically derived
Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes see http://www.slh.wisc.edu/about/compliance/nelac-laboratory-accreditationResults, LOD and LOQ values have been adjusted for analytical dilutions and percent moisture where applicable.Results relate only to the items tested.This Laboratory Report shall not be reproduced except in full, without written approval of the laboratory.The water microbiology unit analyzes samples as received and not all samples are tested for preservation before analysis is performed.
List of Abbreviations:
Responsible PartyMicrobiology: Sharon Kluender, Lab Manager, 608-224-6262Inorganic Chemistry: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Metals: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Organic Chemistry: Al Spallato, Lab Manager, 608-224-6269Emergency Chemical Response: Noel Stanton, Lab Manager, 608-224-6251Environmental Toxicology: Tracy Hanke, Lab Manager, 608-224-6270
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 14 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341004WSLH Sample:
ZANA SJIANWISCONSIN DNR
WT093
ZANA SJIANWISCONSIN DNR
Collection End: 5/23/2018 10:49:00 AM
Point or Outfall:
Project No:
Date Received:Date Reported: Sample Depth:
5/24/20186/8/2018
Customer ID:
Report To: Invoice To:
Field #: PERROT
Collection Start: Collected By:
County:
Sample Type:
Sample Reason:
Sample Location:Sample Description:
CAMILLE BRUHNSU-SURFACE WATER
TREMPEALEAU RIVER X-622126 Y-4875013
ID#:
Waterbody:
Program Code:Region Code:
0.5F
Sample Comments
NITRIC ACID USED IN FIELD WAS EXPIRED.
For the dissolved metals tests, the sample was filtered and preserved at the lab.
Analyzed past the 15 minutes holding time: Method SM4500-H+B analyzed on 05/24/18 1330
Analyte Result Units LOD LOQ
Inorganic Chemistry
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
133TOTAL SUSPENDED SOLIDS mg/L 5.0 5.0SM2540D
05/24/18 05/24/18Prep Date Analysis Date
25.0Chloride mg/L 1.00 3.20SM4500-CL-E
05/24/18 05/24/18Prep Date Analysis Date
Comments:Analyzed past the 15 minutes holding time.
8.04pH SU 1.00 1.00SM4500-H+B
05/25/18 05/25/18Prep Date Analysis Date
147Turbidity NTU 0.100 0.100SM2130B
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 15 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341004WSLH Sample:
Analyte Result Units LOD LOQ
Inorganic Chemistry
Analysis Method
05/29/18 05/30/18Prep Date Analysis Date
0.873Phosphorus mg/L 0.00500 0.0160EPA 365.1
Analyte Result Units LOD LOQ
Inorganic Chemistry, Dissolved
Analysis Method
05/24/18 05/25/18Prep Date Analysis Date
0.0396FAmmonia mg/L 0.0150 0.0480EPA 350.1
Analyte Result Units LOD LOQ
Metals, Total Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
2420Aluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
4.13Chromium ug/L 1.00 3.00EPA 200.7
14.0FCopper ug/L 5.00 15.0EPA 200.7
10.4Iron mg/L 0.100 0.300EPA 200.7
7.98FLead ug/L 3.00 10.0EPA 200.7
7.39Nickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
7.48FZinc ug/L 5.00 15.0EPA 200.7
42.1Calcium mg/L 0.100 0.300EPA 200.7
17.9Magnesium mg/L 0.100 0.300EPA 200.7
179Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 16 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341004WSLH Sample:
Analyte Result Units LOD LOQ
Metals, Total
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
Analyte Result Units LOD LOQ
Metals, Total, Low Level
Analysis Method
05/24/18 05/24/18Prep Date Analysis Date
4.67Total Chromium ug/L 0.00150 0.0232Hi Res ICPMS
0.122Chromium (VI) ug/L 0.0122 0.0232Hi Res ICPMS
2.61% Chromium (VI) %Hi Res ICPMS
Analyte Result Units LOD LOQ
Metals, Dissolved Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
NDAluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
NDChromium ug/L 1.00 3.00EPA 200.7
NDCopper ug/L 5.00 15.0EPA 200.7
NDIron mg/L 0.100 0.300EPA 200.7
NDLead ug/L 3.00 10.0EPA 200.7
2.63FNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
NDZinc ug/L 5.00 15.0EPA 200.7
41.0Calcium mg/L 0.100 0.300EPA 200.7
17.8Magnesium mg/L 0.100 0.300EPA 200.7
175Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 17 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341004WSLH Sample:
Analyte Result Units LOD LOQ
Metals, Dissolved
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
Analyte Result Units
Field Data
Analysis Method
15.74Sample Temp-field (C) CentigradeField Data
8.92DO field (mg/L) mg/LField Data
91.4% Saturation %Field Data
7.82pH (SU) field SUField Data
40Cloud Cover % %Field Data
356Cond-fld(uS/CM@25C) UMHOS/CMField Data
5.0Transparency Tube (cm) CMField Data
LOD = Level of detection LOQ = Level of quantification ND = None detected. Results are less than the LOD F next to result = Result is between LOD and LOQ Z next to result = Result is between 0 (zero) and LOD if LOD=LOQ, Limits were not statistically derived
Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes see http://www.slh.wisc.edu/about/compliance/nelac-laboratory-accreditationResults, LOD and LOQ values have been adjusted for analytical dilutions and percent moisture where applicable.Results relate only to the items tested.This Laboratory Report shall not be reproduced except in full, without written approval of the laboratory.The water microbiology unit analyzes samples as received and not all samples are tested for preservation before analysis is performed.
List of Abbreviations:
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 18 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341004WSLH Sample:
Responsible PartyMicrobiology: Sharon Kluender, Lab Manager, 608-224-6262Inorganic Chemistry: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Metals: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Organic Chemistry: Al Spallato, Lab Manager, 608-224-6269Emergency Chemical Response: Noel Stanton, Lab Manager, 608-224-6251Environmental Toxicology: Tracy Hanke, Lab Manager, 608-224-6270
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 19 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341005WSLH Sample:
ZANA SJIANWISCONSIN DNR
WT093
ZANA SJIANWISCONSIN DNR
Collection End: 5/23/2018 11:55:00 AM
Point or Outfall:
Project No:
Date Received:Date Reported: Sample Depth:
5/24/20186/8/2018
Customer ID:
Report To: Invoice To:
Field #: T35
Collection Start: Collected By:
County:
Sample Type:
Sample Reason:
Sample Location:
Sample Description:
CAMILLE BRUHNSU-SURFACE WATER
TEMPEALEAU RIVER NEARCENTERVILLEX-616720 Y-4880708
ID#: 623002
Waterbody:
Program Code:Region Code:
0.5F
Sample Comments
NITRIC ACID USED IN FIELD WAS EXPIRED.
For the dissolved metals tests, the sample was filtered and preserved at the lab.
Analyzed past the 15 minutes holding time: Method SM4500-H+B analyzed on 05/24/18 1330
Analyte Result Units LOD LOQ
Inorganic Chemistry
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
86.0TOTAL SUSPENDED SOLIDS mg/L 10.0 10.0SM2540D
05/24/18 05/24/18Prep Date Analysis Date
21.0Chloride mg/L 1.00 3.20SM4500-CL-E
05/24/18 05/24/18Prep Date Analysis Date
Comments:Analyzed past the 15 minutes holding time.
8.09pH SU 1.00 1.00SM4500-H+B
05/25/18 05/25/18Prep Date Analysis Date
87.0Turbidity NTU 0.100 0.100SM2130B
05/29/18 05/30/18Prep Date Analysis Date
0.581Phosphorus mg/L 0.00500 0.0160EPA 365.1
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 20 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341005WSLH Sample:
Analyte Result Units LOD LOQ
Inorganic Chemistry, Dissolved
Analysis Method
05/24/18 05/25/18Prep Date Analysis Date
0.0264FAmmonia mg/L 0.0150 0.0480EPA 350.1
Analyte Result Units LOD LOQ
Metals, Total Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
1670Aluminum ug/L 10.0 30.0EPA 200.7
SPIKE QC EXCEEDED. SPIKE RECOVERY: 196%
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
2.54FChromium ug/L 1.00 3.00EPA 200.7
8.49FCopper ug/L 5.00 15.0EPA 200.7
6.65Iron mg/L 0.100 0.300EPA 200.7
4.63FLead ug/L 3.00 10.0EPA 200.7
6.00Nickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
7.48FZinc ug/L 5.00 15.0EPA 200.7
40.3Calcium mg/L 0.100 0.300EPA 200.7
17.8Magnesium mg/L 0.100 0.300EPA 200.7
174Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
Analyte Result Units LOD LOQ
Metals, Total
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 21 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341005WSLH Sample:
Analyte Result Units LOD LOQ
Metals, Total, Low Level
Analysis Method
05/24/18 05/24/18Prep Date Analysis Date
1.84Total Chromium ug/L 0.00150 0.0232Hi Res ICPMS
0.0935Chromium (VI) ug/L 0.0122 0.0232Hi Res ICPMS
5.08% Chromium (VI) %Hi Res ICPMS
Analyte Result Units LOD LOQ
Metals, Dissolved Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
19.5FAluminum ug/L 10.0 30.0EPA 200.7
SPIKE QC EXCEEDED. SPIKE RECOVERY: 196%
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
NDChromium ug/L 1.00 3.00EPA 200.7
NDCopper ug/L 5.00 15.0EPA 200.7
NDIron mg/L 0.100 0.300EPA 200.7
NDLead ug/L 3.00 10.0EPA 200.7
2.25FNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
NDZinc ug/L 5.00 15.0EPA 200.7
39.6Calcium mg/L 0.100 0.300EPA 200.7
17.6Magnesium mg/L 0.100 0.300EPA 200.7
171Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
Analyte Result Units LOD LOQ
Metals, Dissolved
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 22 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341005WSLH Sample:
Analyte Result Units
Field Data
Analysis Method
16.62Sample Temp-field (C) CentigradeField Data
9.73DO field (mg/L) mg/LField Data
101.8% Saturation %Field Data
7.89pH (SU) field SUField Data
80Cloud Cover % %Field Data
342Cond-fld(uS/CM@25C) UMHOS/CMField Data
14.0Transparency Tube (cm) CMField Data
LOD = Level of detection LOQ = Level of quantification ND = None detected. Results are less than the LOD F next to result = Result is between LOD and LOQ Z next to result = Result is between 0 (zero) and LOD if LOD=LOQ, Limits were not statistically derived
Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes see http://www.slh.wisc.edu/about/compliance/nelac-laboratory-accreditationResults, LOD and LOQ values have been adjusted for analytical dilutions and percent moisture where applicable.Results relate only to the items tested.This Laboratory Report shall not be reproduced except in full, without written approval of the laboratory.The water microbiology unit analyzes samples as received and not all samples are tested for preservation before analysis is performed.
List of Abbreviations:
Responsible PartyMicrobiology: Sharon Kluender, Lab Manager, 608-224-6262Inorganic Chemistry: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Metals: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Organic Chemistry: Al Spallato, Lab Manager, 608-224-6269Emergency Chemical Response: Noel Stanton, Lab Manager, 608-224-6251Environmental Toxicology: Tracy Hanke, Lab Manager, 608-224-6270
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 23 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341006WSLH Sample:
ZANA SJIANWISCONSIN DNR
WT093
ZANA SJIANWISCONSIN DNR
Collection End: 5/23/2018 2:26:00 PM
Point or Outfall:
Project No:
Date Received:Date Reported: Sample Depth:
5/24/20186/8/2018
Customer ID:
Report To: Invoice To:
Field #: POKER REFERENCE
Collection Start: Collected By:
County:
Sample Type:
Sample Reason:
Sample Location:Sample Description:
CAMILLE BRUHNSU-SURFACE WATER
POKER COULEE CREEK X 629892 Y-4910534
ID#:
Waterbody:
Program Code:Region Code:
0.5F
Sample Comments
NITRIC ACID USED IN FIELD WAS EXPIRED.
For the dissolved metals tests, the sample was filtered and preserved at the lab.
Analyzed past the 15 minutes holding time: Method SM4500-H+B analyzed on 05/24/18 1330
Analyte Result Units LOD LOQ
Inorganic Chemistry
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
16.0TOTAL SUSPENDED SOLIDS mg/L 2.5 2.5SM2540D
05/24/18 05/24/18Prep Date Analysis Date
9.04Chloride mg/L 1.00 3.20SM4500-CL-E
05/24/18 05/24/18Prep Date Analysis Date
Comments:Analyzed past the 15 minutes holding time.
8.03pH SU 1.00 1.00SM4500-H+B
05/25/18 05/25/18Prep Date Analysis Date
9.74Turbidity NTU 0.100 0.100SM2130B
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 24 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341006WSLH Sample:
Analyte Result Units LOD LOQ
Inorganic Chemistry
Analysis Method
05/29/18 05/30/18Prep Date Analysis Date
0.259Phosphorus mg/L 0.00500 0.0160EPA 365.1
Analyte Result Units LOD LOQ
Inorganic Chemistry, Dissolved
Analysis Method
05/24/18 05/25/18Prep Date Analysis Date
0.0197FAmmonia mg/L 0.0150 0.0480EPA 350.1
Analyte Result Units LOD LOQ
Metals, Total Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
215Aluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
NDChromium ug/L 1.00 3.00EPA 200.7
NDCopper ug/L 5.00 15.0EPA 200.7
0.443Iron mg/L 0.100 0.300EPA 200.7
NDLead ug/L 3.00 10.0EPA 200.7
NDNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
NDZinc ug/L 5.00 15.0EPA 200.7
27.0Calcium mg/L 0.100 0.300EPA 200.7
11.4Magnesium mg/L 0.100 0.300EPA 200.7
114Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 25 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341006WSLH Sample:
Analyte Result Units LOD LOQ
Metals, Total
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
Analyte Result Units LOD LOQ
Metals, Total, Low Level
Analysis Method
05/24/18 05/24/18Prep Date Analysis Date
0.208Total Chromium ug/L 0.00150 0.0232Hi Res ICPMS
0.147Chromium (VI) ug/L 0.0122 0.0232Hi Res ICPMS
70.7% Chromium (VI) %Hi Res ICPMS
Analyte Result Units LOD LOQ
Metals, Dissolved Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
11.8FAluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
NDChromium ug/L 1.00 3.00EPA 200.7
NDCopper ug/L 5.00 15.0EPA 200.7
NDIron mg/L 0.100 0.300EPA 200.7
NDLead ug/L 3.00 10.0EPA 200.7
NDNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
NDZinc ug/L 5.00 15.0EPA 200.7
25.5Calcium mg/L 0.100 0.300EPA 200.7
10.8Magnesium mg/L 0.100 0.300EPA 200.7
108Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 26 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341006WSLH Sample:
Analyte Result Units LOD LOQ
Metals, Dissolved
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
Analyte Result Units
Field Data
Analysis Method
15.92Sample Temp-field (C) CentigradeField Data
10.04DO field (mg/L) mg/LField Data
103.3% Saturation %Field Data
7.7pH (SU) field SUField Data
100Cloud Cover % %Field Data
216Cond-fld(uS/CM@25C) UMHOS/CMField Data
86.0Transparency Tube (cm) CMField Data
LOD = Level of detection LOQ = Level of quantification ND = None detected. Results are less than the LOD F next to result = Result is between LOD and LOQ Z next to result = Result is between 0 (zero) and LOD if LOD=LOQ, Limits were not statistically derived
Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes see http://www.slh.wisc.edu/about/compliance/nelac-laboratory-accreditationResults, LOD and LOQ values have been adjusted for analytical dilutions and percent moisture where applicable.Results relate only to the items tested.This Laboratory Report shall not be reproduced except in full, without written approval of the laboratory.The water microbiology unit analyzes samples as received and not all samples are tested for preservation before analysis is performed.
List of Abbreviations:
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 27 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341006WSLH Sample:
Responsible PartyMicrobiology: Sharon Kluender, Lab Manager, 608-224-6262Inorganic Chemistry: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Metals: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Organic Chemistry: Al Spallato, Lab Manager, 608-224-6269Emergency Chemical Response: Noel Stanton, Lab Manager, 608-224-6251Environmental Toxicology: Tracy Hanke, Lab Manager, 608-224-6270
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 28 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341007WSLH Sample:
ZANA SJIANWISCONSIN DNR
WT093
ZANA SJIANWISCONSIN DNR
Collection End: 5/23/2018 2:53:00 PM
Point or Outfall:
Project No:
Date Received:Date Reported: Sample Depth:
5/24/20186/8/2018
Customer ID:
Report To: Invoice To:
Field #: TREMP@Q
Collection Start: Collected By:
County:
Sample Type:
Sample Reason:
Sample Location:Sample Description:
CAMILLE BRUHNSU-SURFACE WATER
X-625991 Y-4911901
ID#:
Waterbody:
Program Code:Region Code:
0.5F
Sample Comments
For the dissolved metals tests, the sample was filtered and preserved at the lab.
Analyzed past the 15 minutes holding time: Method SM4500-H+B analyzed on 05/24/18 1330
NITRIC ACID USED IN FIELD WAS EXPIRED.
Analyte Result Units LOD LOQ
Inorganic Chemistry
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
26.7TOTAL SUSPENDED SOLIDS mg/L 4.8 4.8SM2540D
05/24/18 05/24/18Prep Date Analysis Date
16.1Chloride mg/L 1.00 3.20SM4500-CL-E
05/24/18 05/24/18Prep Date Analysis Date
Comments:Analyzed past the 15 minutes holding time.
7.72pH SU 1.00 1.00SM4500-H+B
05/25/18 05/25/18Prep Date Analysis Date
20.1Turbidity NTU 0.100 0.100SM2130B
05/29/18 05/30/18Prep Date Analysis Date
0.349Phosphorus mg/L 0.00500 0.0160EPA 365.1
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 29 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341007WSLH Sample:
Analyte Result Units LOD LOQ
Inorganic Chemistry, Dissolved
Analysis Method
05/24/18 05/25/18Prep Date Analysis Date
0.112Ammonia mg/L 0.0150 0.0480EPA 350.1
Analyte Result Units LOD LOQ
Metals, Total Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
365Aluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
NDChromium ug/L 1.00 3.00EPA 200.7
NDCopper ug/L 5.00 15.0EPA 200.7
2.24Iron mg/L 0.100 0.300EPA 200.7
NDLead ug/L 3.00 10.0EPA 200.7
5.28FNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
13.4FZinc ug/L 5.00 15.0EPA 200.7
24.3Calcium mg/L 0.100 0.300EPA 200.7
9.79Magnesium mg/L 0.100 0.300EPA 200.7
101Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
Analyte Result Units LOD LOQ
Metals, Total
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 30 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341007WSLH Sample:
Analyte Result Units LOD LOQ
Metals, Total, Low Level
Analysis Method
05/24/18 05/24/18Prep Date Analysis Date
0.420Total Chromium ug/L 0.00150 0.0232Hi Res ICPMS
0.0956Chromium (VI) ug/L 0.0122 0.0232Hi Res ICPMS
22.8% Chromium (VI) %Hi Res ICPMS
Analyte Result Units LOD LOQ
Metals, Dissolved Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
10.9FAluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
NDChromium ug/L 1.00 3.00EPA 200.7
NDCopper ug/L 5.00 15.0EPA 200.7
NDIron mg/L 0.100 0.300EPA 200.7
NDLead ug/L 3.00 10.0EPA 200.7
4.32FNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
NDZinc ug/L 5.00 15.0EPA 200.7
23.5Calcium mg/L 0.100 0.300EPA 200.7
9.31Magnesium mg/L 0.100 0.300EPA 200.7
97.0Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
Analyte Result Units LOD LOQ
Metals, Dissolved
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 31 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341007WSLH Sample:
Analyte Result Units
Field Data
Analysis Method
15.11Sample Temp-field (C) CentigradeField Data
9.12DO field (mg/L) mg/LField Data
92.4% Saturation %Field Data
7.36pH (SU) field SUField Data
80Cloud Cover % %Field Data
230Cond-fld(uS/CM@25C) UMHOS/CMField Data
50.0Transparency Tube (cm) CMField Data
LOD = Level of detection LOQ = Level of quantification ND = None detected. Results are less than the LOD F next to result = Result is between LOD and LOQ Z next to result = Result is between 0 (zero) and LOD if LOD=LOQ, Limits were not statistically derived
Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes see http://www.slh.wisc.edu/about/compliance/nelac-laboratory-accreditationResults, LOD and LOQ values have been adjusted for analytical dilutions and percent moisture where applicable.Results relate only to the items tested.This Laboratory Report shall not be reproduced except in full, without written approval of the laboratory.The water microbiology unit analyzes samples as received and not all samples are tested for preservation before analysis is performed.
List of Abbreviations:
Responsible PartyMicrobiology: Sharon Kluender, Lab Manager, 608-224-6262Inorganic Chemistry: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Metals: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Organic Chemistry: Al Spallato, Lab Manager, 608-224-6269Emergency Chemical Response: Noel Stanton, Lab Manager, 608-224-6251Environmental Toxicology: Tracy Hanke, Lab Manager, 608-224-6270
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 32 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341008WSLH Sample:
ZANA SJIANWISCONSIN DNR
WT093
ZANA SJIANWISCONSIN DNR
Collection End: 5/23/2018 1:43:00 PM
Point or Outfall:
Project No:
Date Received:Date Reported: Sample Depth:
5/24/20186/8/2018
Customer ID:
Report To: Invoice To:
Field #: TREMP@121
Collection Start: Collected By:
County:
Sample Type:
Sample Reason:
Sample Location:Sample Description:
CAMILLE BRUHNSU-SURFACE WATER
TREAMPEALEAU RIVER X-629994 Y-4914148
ID#:
Waterbody:
Program Code:Region Code:
0.5F
Sample Comments
NITRIC ACID USED IN FIELD WAS EXPIRED.
For the dissolved metals tests, the sample was filtered and preserved at the lab.
Analyzed past the 15 minutes holding time: Method SM4500-H+B analyzed on 05/24/18 1330
Analyte Result Units LOD LOQ
Inorganic Chemistry
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
20.0TOTAL SUSPENDED SOLIDS mg/L 3.3 3.3SM2540D
05/24/18 05/24/18Prep Date Analysis Date
16.7Chloride mg/L 1.00 3.20SM4500-CL-E
05/24/18 05/24/18Prep Date Analysis Date
Comments:Analyzed past the 15 minutes holding time.
7.66pH SU 1.00 1.00SM4500-H+B
05/25/18 05/25/18Prep Date Analysis Date
15.6Turbidity NTU 0.100 0.100SM2130B
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 33 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341008WSLH Sample:
Analyte Result Units LOD LOQ
Inorganic Chemistry
Analysis Method
05/29/18 05/30/18Prep Date Analysis Date
0.326Phosphorus mg/L 0.00500 0.0160EPA 365.1
Analyte Result Units LOD LOQ
Inorganic Chemistry, Dissolved
Analysis Method
05/24/18 05/25/18Prep Date Analysis Date
0.112Ammonia mg/L 0.0150 0.0480EPA 350.1
Analyte Result Units LOD LOQ
Metals, Total Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
237Aluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
NDChromium ug/L 1.00 3.00EPA 200.7
NDCopper ug/L 5.00 15.0EPA 200.7
1.80Iron mg/L 0.100 0.300EPA 200.7
NDLead ug/L 3.00 10.0EPA 200.7
5.06FNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
8.83FZinc ug/L 5.00 15.0EPA 200.7
20.7Calcium mg/L 0.100 0.300EPA 200.7
7.80Magnesium mg/L 0.100 0.300EPA 200.7
83.8Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 34 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341008WSLH Sample:
Analyte Result Units LOD LOQ
Metals, Total
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
Analyte Result Units LOD LOQ
Metals, Total, Low Level
Analysis Method
05/24/18 05/24/18Prep Date Analysis Date
0.367Total Chromium ug/L 0.00150 0.0232Hi Res ICPMS
0.114Chromium (VI) ug/L 0.0122 0.0232Hi Res ICPMS
31.1% Chromium (VI) %Hi Res ICPMS
Analyte Result Units LOD LOQ
Metals, Dissolved Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
NDAluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
NDChromium ug/L 1.00 3.00EPA 200.7
NDCopper ug/L 5.00 15.0EPA 200.7
NDIron mg/L 0.100 0.300EPA 200.7
NDLead ug/L 3.00 10.0EPA 200.7
5.09FNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
NDZinc ug/L 5.00 15.0EPA 200.7
22.0Calcium mg/L 0.100 0.300EPA 200.7
8.49Magnesium mg/L 0.100 0.300EPA 200.7
89.8Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 35 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341008WSLH Sample:
Analyte Result Units LOD LOQ
Metals, Dissolved
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
Analyte Result Units
Field Data
Analysis Method
14.98Sample Temp-field (C) CentigradeField Data
8.91DO field (mg/L) mg/LField Data
90.0% Saturation %Field Data
7.25pH (SU) field SUField Data
100Cloud Cover % %Field Data
212Cond-fld(uS/CM@25C) UMHOS/CMField Data
69.0Transparency Tube (cm) CMField Data
LOD = Level of detection LOQ = Level of quantification ND = None detected. Results are less than the LOD F next to result = Result is between LOD and LOQ Z next to result = Result is between 0 (zero) and LOD if LOD=LOQ, Limits were not statistically derived
Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes see http://www.slh.wisc.edu/about/compliance/nelac-laboratory-accreditationResults, LOD and LOQ values have been adjusted for analytical dilutions and percent moisture where applicable.Results relate only to the items tested.This Laboratory Report shall not be reproduced except in full, without written approval of the laboratory.The water microbiology unit analyzes samples as received and not all samples are tested for preservation before analysis is performed.
List of Abbreviations:
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 36 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341008WSLH Sample:
Responsible PartyMicrobiology: Sharon Kluender, Lab Manager, 608-224-6262Inorganic Chemistry: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Metals: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Organic Chemistry: Al Spallato, Lab Manager, 608-224-6269Emergency Chemical Response: Noel Stanton, Lab Manager, 608-224-6251Environmental Toxicology: Tracy Hanke, Lab Manager, 608-224-6270
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 37 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341009WSLH Sample:
ZANA SJIANWISCONSIN DNR
WT093
ZANA SJIANWISCONSIN DNR
Collection End: 5/23/2018 2:12:00 PM
Point or Outfall:
Project No:
Date Received:Date Reported: Sample Depth:
5/24/20186/8/2018
Customer ID:
Report To: Invoice To:
Field #: POKER BELOW SPILL
Collection Start: Collected By:
County:
Sample Type:
Sample Reason:
Sample Location:Sample Description:
CAMILLE BRUHNSU-SURFACE WATER
POKER COULEE CREEK X 629383 Y-4911304
ID#:
Waterbody:
Program Code:Region Code:
0.5F
Sample Comments
NITRIC ACID USED IN FIELD WAS EXPIRED.
For the dissolved metals tests, the sample was filtered and preserved at the lab.
Analyzed past the 15 minutes holding time: Method SM4500-H+B analyzed on 05/24/18 1330
Analyte Result Units LOD LOQ
Inorganic Chemistry
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
204TOTAL SUSPENDED SOLIDS mg/L 10.0 10.0SM2540D
05/24/18 05/24/18Prep Date Analysis Date
18.7Chloride mg/L 1.00 3.20SM4500-CL-E
05/24/18 05/24/18Prep Date Analysis Date
Comments:Analyzed past the 15 minutes holding time.
7.74pH SU 1.00 1.00SM4500-H+B
05/25/18 05/25/18Prep Date Analysis Date
209Turbidity NTU 0.100 0.100SM2130B
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 38 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341009WSLH Sample:
Analyte Result Units LOD LOQ
Inorganic Chemistry
Analysis Method
05/29/18 05/30/18Prep Date Analysis Date
1.27Phosphorus mg/L 0.0100 0.0320EPA 365.1
Analyte Result Units LOD LOQ
Inorganic Chemistry, Dissolved
Analysis Method
05/24/18 05/25/18Prep Date Analysis Date
0.0635Ammonia mg/L 0.0150 0.0480EPA 350.1
Analyte Result Units LOD LOQ
Metals, Total Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
1.29FCadmium ug/L 1.00 3.00EPA 200.7
6.40Chromium ug/L 1.00 3.00EPA 200.7
18.5Copper ug/L 5.00 15.0EPA 200.7
13.7Iron mg/L 0.100 0.300EPA 200.7
11.1Lead ug/L 3.00 10.0EPA 200.7
10.2Nickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
9.19FZinc ug/L 5.00 15.0EPA 200.7
30.4Calcium mg/L 0.100 0.300EPA 200.7
12.9Magnesium mg/L 0.100 0.300EPA 200.7
129Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
3770Aluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 39 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341009WSLH Sample:
Analyte Result Units LOD LOQ
Metals, Total
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
Analyte Result Units LOD LOQ
Metals, Total, Low Level
Analysis Method
05/24/18 05/24/18Prep Date Analysis Date
3.90Total Chromium ug/L 0.00150 0.0232Hi Res ICPMS
0.289Chromium (VI) ug/L 0.0122 0.0232Hi Res ICPMS
7.41% Chromium (VI) %Hi Res ICPMS
Analyte Result Units LOD LOQ
Metals, Dissolved Recoverable
Analysis Method
05/25/18 05/29/18Prep Date Analysis Date
NDAluminum ug/L 10.0 30.0EPA 200.7
MATRIX SPIKE QC EXCEEDED.
NDAntimony ug/L 5.00 16.0EPA 200.7
NDBeryllium ug/L 0.500 1.60EPA 200.7
NDCadmium ug/L 1.00 3.00EPA 200.7
NDChromium ug/L 1.00 3.00EPA 200.7
NDCopper ug/L 5.00 15.0EPA 200.7
NDIron mg/L 0.100 0.300EPA 200.7
NDLead ug/L 3.00 10.0EPA 200.7
NDNickel ug/L 2.00 6.00EPA 200.7
NDSelenium ug/L 10.0 30.0EPA 200.7
NDSilver ug/L 2.00 6.00EPA 200.7
NDZinc ug/L 5.00 15.0EPA 200.7
28.6Calcium mg/L 0.100 0.300EPA 200.7
12.2Magnesium mg/L 0.100 0.300EPA 200.7
122Hardness (SM 2340B) mg/L 0.660 2.00EPA 200.7
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
Page 40 of 41
Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341009WSLH Sample:
Analyte Result Units LOD LOQ
Metals, Dissolved
Analysis Method
05/25/18 05/25/18Prep Date Analysis Date
NDMercury ug/L 0.030 0.080EPA 245.1
Analyte Result Units
Field Data
Analysis Method
15.40Sample Temp-field (C) CentigradeField Data
8.88DO field (mg/L) mg/LField Data
90.4% Saturation %Field Data
7.15pH (SU) field SUField Data
100Cloud Cover % %Field Data
242Cond-fld(uS/CM@25C) UMHOS/CMField Data
5.0Transparency Tube (cm) CMField Data
LOD = Level of detection LOQ = Level of quantification ND = None detected. Results are less than the LOD F next to result = Result is between LOD and LOQ Z next to result = Result is between 0 (zero) and LOD if LOD=LOQ, Limits were not statistically derived
Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes see http://www.slh.wisc.edu/about/compliance/nelac-laboratory-accreditationResults, LOD and LOQ values have been adjusted for analytical dilutions and percent moisture where applicable.Results relate only to the items tested.This Laboratory Report shall not be reproduced except in full, without written approval of the laboratory.The water microbiology unit analyzes samples as received and not all samples are tested for preservation before analysis is performed.
List of Abbreviations:
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev:
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Laboratory ReportWisconsin State Laboratory of Hygiene
2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996
(800)442-4618 - FAX (608)224-6213http://www.slh.wisc.edu
D.F. Kurtycz, M.D., Medical Director - Prof. James J. Schauer, Ph.D., Director
Environmental Health DivisionWDNR LAB ID: NELAP LAB ID: EPA LAB ID: WI DATCP ID:113133790 E37658 WI00007, WI00008 105-415
384341009WSLH Sample:
Responsible PartyMicrobiology: Sharon Kluender, Lab Manager, 608-224-6262Inorganic Chemistry: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Metals: DeWayne Kennedy-Parker, Lab Manager, 608-224-6282Organic Chemistry: Al Spallato, Lab Manager, 608-224-6269Emergency Chemical Response: Noel Stanton, Lab Manager, 608-224-6251Environmental Toxicology: Tracy Hanke, Lab Manager, 608-224-6270
DRAFTReport ID: 0000.25.2.WSLH.0Report Rev: