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Graphical abstract

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2.2 FmocCl, pyridine, 7 days HBr, ace7c acid, 4 hrs. pyridine, 3 hrs. 2.2 FmocCl 2.2 FmocCl, pyridine, DMAP 3 hrs. EtOH, Zn dust, 1 hr. Ac 2 O, ZnCl 2 100 O C, 4 hrs. Et 3 N, pyridine, 1 hr. HBr, ace7c acid, 24 hrs. HBr, ace7c acid, 24 hrs. ace7c acid, Zn dust 2 hrs. 4 hrs. HBr, ace7c acid, 4 hrs. 20% 9.8% <1% 35% 24% 67% exo endo 9.6% 23% exo endo 89% 5.4% >5% 82% methyl acrylate NaHSO 3 , KBrO 3 , 15 min. ~43%

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Page 1: Graphical abstract

2.2FmocCl,pyridine,7days

HBr,ace7cacid,4hrs.

pyridine,3hrs.

2.2FmocCl

2.2FmocCl,pyridine,DMAP3hrs.

EtOH,Zndust,1hr.

Ac2O,ZnCl2

100OC,4hrs.

Et3N,pyridine,1hr.

HBr,ace7cacid,24hrs.

HBr,ace7cacid,24hrs.

ace7cacid,Zndust

2hrs.4hrs.

HBr,ace7cacid,4hrs.

20% 9.8%<1%

35%24%

67%

exo

endo

9.6%

23%

exo

endo

89%

5.4% >5%82%

methylacrylateNaHSO3,KBrO3,15min.

~43%

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