GROUNDWATER MONITORING REPORT
EASTERN SURPLUS COMPANY SITE
887 MAIN STREET (ROUTE 191)
MEDDYBEMPS, MAINE
Prepared by: Campbell Environmental Group, Inc.
173 Gray Road Falmouth, ME 04105
February 2016
Prepared for:
Mr. Christopher Swain Maine Department of environmental Protection
State House Station 17 Augusta, Maine 04333
February 24, 2016
Mr. Christopher Swain Maine Department of Environmental Protection State House Station 17 Augusta, Maine 04333 Re: Groundwater Monitoring Eastern Surplus Company Site 887 Main Street (Route 191) Meddybemps, Maine 04657
Dear Mr. Swain,
Campbell Environmental Group, Inc. (CEG) prepared this report to document groundwater
monitoring activities conducted to fulfill the requirements of the Maine Department of
Environmental protection (MEDEP) Request for Bids, RFB # 8, Water Monitoring at Eastern
Surplus Site.
If you have any questions or comments, please do not hesitate to contact us. CEG appreciates
working with you on this project.
Sincerely,
Aaron Brignull Rich Campbell Environmental Scientist Maine Certified Geologist
President
Enclosure
Mr. Christopher Swain, Maine Department of Environmental Protection Page ii Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016
Table of Contents
1.0 INTRODUCTION ................................................................................................................ 1
2.0 QUALITY ASSURANCE PROJECT PLAN ....................................................................... 1
3.0 SITE SPECIFIC HEALTH AND SAFETY PLAN ............................................................... 24.0 GROUNDWATER MONITORING ACTIVITIES ................................................................. 2
4.1 Decontamination and Investigation Derived Wastes ............................................... 2
4.2 Monitoring Well Inspection & Groundwater Elevation Data Collection .................. 2
4.3 Groundwater Sampling and Chemical Analyses ...................................................... 3
4.3.1 Chemical Testing Plan ............................................................................................. 3
4.3.2 Groundwater Sampling ............................................................................................ 3
5.0 EVALUATION AND PRESENTATION OF RESULTS ...................................................... 4
5.1 Data Quality Assessment Summary .......................................................................... 4
5.1.1 Evaluation of Sampling Procedures ........................................................................ 4
5.1.2 Quality Assurance Quality Control Samples............................................................ 4
5.2 Analytical Results ........................................................................................................ 5
6.0 CONCLUSIONS AND RECOMMENDATIONS ................................................................. 8
APPENDICES
Appendix A – Figures & Tables Figure 1 - Locus Map Figure 2 - Sampling Locations
Table 1-1 – Analytical Results Table 2-1 – Historical Trends of PCE Concentrations
Appendix B – Field Data Low Flow Data Forms Well Gauging Forms Appendix C – MEDEP Data Validation Checklist Intra-well Trend Narrative Appendix D – Laboratory Reports
Mr. Christopher Swain, Maine Department of Environmental Protection Page 1 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016
1.0 INTRODUCTION
This groundwater monitoring report documents conditions at the Eastern Surplus Company Site,
located at 887 Main Street, in Meddybemps, Maine (Figure 1, Appendix A). The report and
associated field work were conducted by Campbell Environmental Group, Inc. (CEG) per Request
for Bid #8 by the Maine Department of Environmental protection (MEDEP).
To comply with RFB #8, CEG completed the following tasks:
TASK 1- Review/Update Quality Assurance Project Plan;
TASK 2 – Prepare a Site Specific Health and Safety Plan (HASP)/Coordinate Field Work
Activities;
TASK 3 – Perform Field Work;
TASK 4- Conduct Data Validation;
TASK 5- Prepare this report.
On October 19 and 20, 2015, CEG completed contracted groundwater monitoring activities at the
Site, including the collection of aqueous samples from 13 on-site wells. One residential water
supply well was sampled by MEDEP personnel. Sampling personnel also collected groundwater
elevation data from 42 on-site wells. To complete the groundwater monitoring event, CEG
contracted Dale Mitchell of the Passamaquoddy Environmental Department for general field
assistance. Mr. Terry Connelly from the United States Environmental Protection Agency (EPA)
also graciously volunteered to assist with field tasks. No additional services or personnel were
subcontracted by CEG.
Field instrumentation utilized during this monitoring event was contracted through Pine
Environmental, of Scarborough, Maine, and included two YSI Multimeters and two HACH
Turbidity Meters.
o HACH 2100Q Turbidity Meter (Instrument ID R149473)
o HACH 2100P Turbidity Meter (Instrument ID 11638)
o YSI 556 (Instrument ID 33217)
o YSI 556 (Instrument ID 33216)
All instrumentation was calibrated daily, prior to field activities. The calibration of turbidity meters
included an automated sequence utilizing standards of 10 NTU, 20 NTU, 100 NTU, and 800 NTU,
provided by Pine Environmental. Similarly, YSI instruments were calibrated using an automated
sequence involving Pine provided standards for pH, Conductivity, and ORP.
2.0 QUALITY ASSURANCE PROJECT PLAN
Site related activities were conducted in accordance with CEGs bid submittal form dated July 22,
2015, and MEDEP Task Order 1-5, Water Monitoring at Eastern Surplus Site, Meddybemps.
CEG also referenced standard operating procedures (SOPs) outlined in the Quality Assurance
Project Plan Addendum (QAPP) for Long-Term Monitoring at the Eastern Surplus Company Site,
Mr. Christopher Swain, Maine Department of Environmental Protection Page 2 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016
dated June 27, 2013, prepared by Nobis Engineering, Inc. of Lowell Massachusetts. The Nobis
QAPP was used for guidance during this monitoring event and specific deviations were approved
by appropriate MEDEP personnel, including;
Pre-preserved laboratory provided containers were used for sample collection eliminating
the need for sample preservation in the field using nitric acid;
Laboratory SOPs and minimum detection limits were not updated for this sampling event.
Laboratory services for this projected were contracted directly between the MEDEP and
Katahdin Analytical Services, of Scarborough, ME;
Groundwater sampling included the collection of one blind-duplicate sample which was
labeled using a fictitious sample point ID (ESLT-GW-MWRP-1015);
No surface water samples were collected as part of this monitoring event;
Data validation was conducted as specified in the RFB using the MEDEP Checklist; and
Data presentation does not include the graphical presentation of trends.
3.0 SITE SPECIFIC HEALTH AND SAFETY PLAN
The purpose of a site-specific HASP is to provide guidance, standards, and critical information
necessary to address health and safety issues at the Site. CEG prepared a site-specific HASP to
comply with Occupational Safety and Health Administration (OSHA) 29 CFR 1910.120
regulations. The HASP included, but was limited to, a description of personal protective
equipment requirements, site hazards and controls, emergency telephone numbers, a
contingency plan that conforms with 29 CFR 1910.120(1)(1) and (1)(2) for Site emergencies, and
Material Safety Data Sheets (MSDS) for potential constituents of concern. Prior to field work, the
HASP was reviewed and signed by on-site sampling personnel.
4.0 GROUNDWATER MONITORING ACTIVITIES
The following subsections outline groundwater monitoring activities outlined in MEDEP Task
Order 1-5, Water Monitoring at Eastern Surplus Site, Meddybemps.
4.1 Decontamination and Investigation Derived Wastes
Decontamination of non-dedicated equipment was conducted using an Aconox wash followed by
a distilled water rinse in accordance with the QAPP. Decontamination fluids and sample purge
water were discarded directly into the onsite carbon filtration unit.
4.2 Monitoring Well Inspection & Groundwater Elevation Data Collection
CEG personnel collected one round of groundwater elevation data from MEDEP stipulated
monitoring wells. Additionally, CEG observed wells for any evidence of damage including surface
water infiltration or artesian leakage. Locks were not present on any gauged or sampled wells,
Mr. Christopher Swain, Maine Department of Environmental Protection Page 3 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016
however, no additional damage or significant deficiencies were noted. Groundwater elevation
measurements are included in the Well Gauging Form included in Appendix B of this Report.
4.3 Groundwater Sampling and Chemical Analyses
The following section presents a detailed description of the field investigation methods as well as
the sampling and chemical analyses completed for the investigation. A brief narrative describing
changes in intra-well analyte concentrations between 2014 and 2015 monitoring events is also
included in Appendix C.
4.3.1 Chemical Testing Plan
Groundwater samples were submitted to Katahdin Analytical Services for laboratory analysis of
project analytes using one or more of the following methods:
VOCs in water using United States Environmental Protection Agency (USEPA) Method
8260;
Dissolved Gas (Methane, Ethane, Ethene) using RSK SOP 175; and
TAL Metals using USEPA Method 6020 and 7470.
4.3.2 Groundwater Sampling
CEG collected groundwater samples from 13 sampling points and assigned unique identifiers
including;
- ESLT-GW-IN1B1-1015
- ESLT-GW-IN1B2-1015
- ESLT-GW-IN7B-1015
- ESLT-GW-MW23B-1015
- ESLT-GW-MW36B1-1015
- ESLT-GW-MW3B-1015
- ESLT-GW-MW51B-1015
- ESLT-GW-MW54B-1015
- ESLT-GW-MW55B-1015
- ESLT-GW-MW57B1-1015
- ESLT-GW-MW57B2-1015
- ESLT-GW-MW58B1-1015
- ESLT-GW-MW58B2-1015
With the exception of sample ESLT-GWLORD-1015, all groundwater samples were collected
using peristaltic pumps and dedicated tubing according to MEDEP Standard Operating Procedure
DR#003, Groundwater Sampling Using Low Flow Purging and Sampling For Long Term
Monitoring. Physical parameters measured prior to the collection of groundwater samples
included depth to groundwater, pH, oxidation-reduction potential, conductivity, turbidity,
temperature, and dissolved oxygen. Sample ESLT-GWLORD-1015 was collected from an
outside tap of the residential water supply well of Mr. Mathew Lord by MEDEP staff. No field
parameters were collected, however, the well was purged for approximately 15 minutes prior to
sample collection from an outside spigot located at the north side of the residence. According to
Mr. Lord, the sample collection point is located before any water treatment systems.
Mr. Christopher Swain, Maine Department of Environmental Protection Page 4 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016
5.0 EVALUATION AND PRESENTATION OF RESULTS
The following subsections summarize the analytical results and detail site conditions.
5.1 Data Quality Assessment Summary
This subsection provides a summary of results from the Quality Assurance Quality Control
(QA/QC) program. The primary purpose of the QA/QC program is to meet the data quality
objectives for the monitoring program as outlined in the QAPP.
5.1.1 Evaluation of Sampling Procedures
CEG evaluated sampling procedures and field data in conjunction with the review of project
analytical data. CEG reviewed;
Documentation of field equipment calibration activities;
Field data for technical credibility versus the sample site setting;
Field sample data and chain-of-custody records; and
Sample handling and preservation procedures.
Field sampling activities were conducted in accordance with the Site Specific QAPP Addendum.
Field screening equipment was calibrated according to the respective manufacturers SOPs and
field data was reviewed by CEG personnel. A summary of field sampling equipment and
corresponding calibration procedures is included in Appendix B of this report. Katahdin Analytical
Services documented acceptable sample receipt condition including the presence of trip blanks,
and signed chain of custodies. Additionally, Katahdin indicated that samples were received in
acceptable condition, at less than 4 degrees Celsius, on ice, and in accordance with sample
handling, preservation, and integrity guidelines. Chain of custody seals were not used for
analytical samples submitted during this project because all sample coolers were transferred
directly from CEG sampling personnel to laboratory personnel. A complete set of the laboratory
analytical data, including the chain of custodies is presented in Appendix D.
5.1.2 Quality Assurance Quality Control Samples
QA/QC samples collected in the field included a trip blank, field duplicate sample, and a matrix
spike duplicate. Additionally, laboratory method blanks, laboratory control samples, laboratory
control sample duplicates, and matrix spike duplicates were analyzed by Katahdin. All QA/QC
results are included in the attached laboratory report (Appendix D). Quality control samples
collected in the filed include;
- ESLT-TB-1015 (Trip Blank)
- ESLT-GW-MWRP-1015 (Blind Duplicate of ESLT-GW-IN1B1-1015)
- ESLT-GW-IN7BMS-1015 (Matrix Spike Duplicate Sample)
Mr. Christopher Swain, Maine Department of Environmental Protection Page 5 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016
Data validation was conducted as required by the MEDEP validation checklist included in
Appendix C of this report. As contracted by the MEDEP, Katahdin Analytical Services reported
analytical results down to respective method detection limits. Accordingly, analytical detections
below practical quantitation limits have been qualified with a “J” and should be considered
estimated. Additional data quality issues included;
The PQL and MDL for Manganese, 1,2‐Dibromo‐3‐Chloropropane, 1,2‐Dibromoethane, and Vinyl Chloride, exceeded applicable regulatory guidelines.
Re‐analysis (a dilution) of sample ESLT‐GW‐MWRP‐1015 was required but conducted 11 days outside of the prescribed hold time. As a result, the single detected compound has been qualified (J) and should be considered estimated.
Methylene Chloride was detected below the reporting limit in Method Blanks WG172846‐2 and WG172905‐2. As a result, detections of methylene chloride in associated project samples have been qualified (JB) and should be considered estimated.
Acetone, m,p‐xylene, ethylbenzene, methylene chloride, and o‐xylene, were detected in VOC Trip Blank ESLT‐TB‐1015. Corresponding detections in project samples have been appropriately qualified.
Aluminum, chromium, copper, nickel, selenium, and vandium, were outside of the acceptable RPD of 30% in field duplicate sample ESLT‐GW‐IN1B1‐1015. Arsenic and cadmium were also outside the 30% RPD. Corresponding detections in project duplicate samples have been appropriately qualified.
Based on CEG’s review, analytical data generated during the October 2015 monitoring event is complete and should be usable for the purposes of this project. 5.2 Analytical Results
Analytical results for project samples have been evaluated based on a comparison to applicable
regulatory standards, including Maine Center for Disease Controls Maximum Exposure
Guidelines (MEGs) for drinking water, dated October 19, 2012, and the Maine Remedial Action
Guidelines for Sites Contaminated with Hazardous Substances, Revised on May 8, 1013. All
detected project analytes are summarized in Table 1-1 of this report. At the request of the
MEDEP, Katahdin Analytical Services reported all analytical results down to the laboratory’s
respective method detection limits.
Volatile Organic Compounds
A total of 16 VOC compounds were detected at concentrations exceeding the laboratories
respective minimum detection limits (MDLs). Two additional compounds (1,2-dibromo-3-
chloropropane and 1-2-dibromoethane) were not detected at concentrations exceeding the
Mr. Christopher Swain, Maine Department of Environmental Protection Page 6 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016
laboratories MDLs, however, the MDLs exceeded corresponding regulatory guidelines and
project action limits. Of the 16 compounds detected, only five analytes were reported at
concentrations exceeding applicable regulatory guidelines, including cis-1,2-dichloroethene,
methylene chloride, tetrachloroethene, trichloroethene, and vinyl chloride. Methylene chloride
concentrations are most likely associated with laboratory contamination and elevated
concentrations were only observed in during subsequent sample analyses performed at a
dilution.
Cis-1,2-dichloroethene was detected in project samples ESLT-GW-MW51B-1015 and ESLT-GW-
MW54B-1015 at concentrations of 190 micrograms per litre (ug/l) and 130 ug/l, respectively. The
MEDEP Residential RAG for Cis-1,2-dichloroethene is 10 ug/l and the Project Action Limit is 70
ug/l.
Tetrachloroethene was detected in samples ESLT-GS-IN1B1-1015 (600 ug/l), ESLT-GW-MWRP-
1015 (500 ug/l), ESLT-GW-IN7B-1015 (190 ug/l), ESLT-GW-IN23B-1015 (140 ug/l), ESLT-GW-
IN36B-1015 (77 ug/l), ESLT-MW51B-1015 (100 ug/l), ESLT-MW54B-1015 (3,900 ug/l), and
ESLT-MW57B1-1015 (220 ug/l) at concentrations exceeding the MEDEP Residential RAG of 40
ug/l and a reported Project Action Limit of 3 ug/l.
CEG evaluated the Historical Trends of PCE Contamination Table from the Spring 2014
Technical Memorandum prepared by Nobis, dated January 2015. Based on the table provided in
the report, only one of the four comparable wells displayed a notable increase in PCE
concentrations. This was well IN-1B1. All other wells appeared to have generally stable
concentrations.
Trichloroethene was detected in samples ESLT-GS-IN1B1-1015 (5.6 ug/l), ESLT-GW-MWRP-
1015 (5.6 ug/l), ESLT-GW-IN1B2-1015 (12 ug/l), ESLT-GW-IN23B-1015 (5.5 ug/l), ESLT-
MW51B-1015 (12 ug/l), ESLT-MW54B-1015 (47 ug/l), and ESLT-MW57B-1015 (4.8 ug/l). The
MEDEP Residential RAG for Trichloroethene is 4 ug/l and the reported Project Action Limit is 5
ug/l. Detections of Trichloroethene in samples ESLT-GW-IN1B2-1015, ESLT-MW51B-1015, and
ESLT-MW54B-1015, also exceeded the corresponding MEDEP Construction Worker RAG of 5.8
ug/l.
Vinyl chloride was detected in samples ESLT-GS-IN1B1-1015 (0.27 ug/l), ESLT-GW-MWRP-
1015 (0.25 ug/l), ESLT-GS-IN1B2-1015 (2.2 ug/l), ESLT-MW51B-1015 (12 ug/l), ESLT-MW54B-
1015 (1.4 ug/l), and ESLT-GW-MW55B-1015 (20 ug/l), at concentrations exceeding the
corresponding MEDEP Residential RAG and reported Project Action Limit of 0.2 ug/l,
respectively. Vinyl chloride was not detected in any additional samples, however, the laboratory’s
reported minimum detected limit for this analyte exceeds applicable regulatory guidelines.
Mr. Christopher Swain, Maine Department of Environmental Protection Page 7 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016
Dissolved Gases
Groundwater samples were also analyzed for methane, ethane, and ethene. According to the
laboratory report, all three dissolved gases were detected in samples ESLT-GW-MW51B-1015
and ESLT-GW-MW55B-1015. Additionally, methane and ethene were also detected in samples
ESLT-GW-IN1B2-1015 and ESLT-GW-MW57B2-1015.
Metals
Antimony and Arsenic were detected in one project sample (ESLT-GW-MW36B1-1015) at
concentrations of 25.2 ug/l and 26 ug/l respectively, exceeding corresponding MEDEP
Residential RAGs and reported Project Action Limits. The Residential RAG and project Action
Limit for Antimony is 3 ug/l. The MEDEP Residential RAG and Project Action limit for arsenic is
10 ug/l.
Total chromium was detected in sample ESLT-GW-MW57B2-1015 at a concentration of 25.3 ug/l.
The Project Action limit for chromium is 20 ug/l. The MEDEP Residential RAG for chromium 6 is
also 20 ug/l.
Cobalt was detected in sample ESLT-GW-MW57B2-1015 at a concentration of 11.6 ug/l. The
Project Action limit for chromium is 20 ug/l. The MEDEP Residential RAG and Project Action limit
for cobalt is 10 ug/l.
Iron was detected in two samples (ESLT-GW-MW51B-1015 and ELST-GW-MW57B1-1015) at
concentrations of 8,500 ug/l and 11,000 ug/l, respectively. The MEDEP Residential RAG and
project Action Limit for Iron is 5,000 ug/l.
Manganese was detected in two samples and one duplicate sample (ESLT-GW-IN1B2-1015,
ESLT-GW-IN1B1 and ESLT-GW-MWRP-1015) at concentration of 2,600 ug/l and 1,990 ug/l,
respectively. The MEDEP Residential RAG for manganese is 500 ug/l. The reported Project
Action Limit for manganese is 200 ug/l.
Sodium was detected in samples ESLT-GW-MW23B-1015 (25,700 ug/l), ESLT-GW-MW36B1-
1015 (45,900 ug/l), ESLT-GW-MW51B-1015 (41,500), ESLT-GW-IN1B2 (23,800 ug/l), ESLT-
GW-MW57B2-1015 (347,000 ug/l) and ESLT-GW-MW55B-1015 (29,100 ug/l), at concentrations
exceeding the corresponding MEDEP Residential RAG of 20,000 ug/l. The reported project
Action Limit for sodium is also 20,000 ug/l.
Mr. Christopher Swain, Maine Department of Environmental Protection Page 8 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016
6.0 CONCLUSIONS AND RECOMMENDATIONS
Based on data generated during the 2015 monitoring event, groundwater at the site continues to
be impacted with volatile organic compounds, dissolved gases, and various metals. Primary
metals of concern appear to be iron, manganese, and sodium. Volatile organic compounds
detected in groundwater consist primarily of tetrachloroethene (PCE) and daughter compounds
trichloroethene (TCE), cis-1,2-dichloroethene (cis-DCE), and vinyl chloride. While concentrations
of project analytes appear to have remained generally consistent over the most recent sampling
periods, concentration have generally decreased since initial monitoring activities at the Site.
CEG recommends continued groundwater monitoring at the Site.
APPENDIX A
Figures & Tables
FIGURE 1 Eastern Surplus Site
887 Main Street, Meddybemps, Main
SITE
FIGURE 2 October 2015 Sampling Locations
Eastern Surplus Site, Meddybemps, Maine
MW‐54B
MW‐58B1 MW‐58B2
MW‐36B1 MW‐57B1 MW‐57B2
MW‐51B MW‐55B MW‐23B
IN‐1B1 IN‐1B2
IN‐7B
MW‐3B
Residential (ug/l)
Construction Worker (ug/l)
Metals (Analytical Methods 6010/7000)ALUMINUM 7429-90-5 7,000 7,000 7,000 9,200,000 J 24 J 10 J 51.5 J 20 J 27 J 128
ANTIMONY 7440-36-0 3 3 3 3,700 J 0.52 J 0.57 1 J 0.92 1.57 25.2
ARSENIC 7440-38-2 10 10 10 1,400 J 4 UJ 2.2 7.5 U 2.2 U 2.2 26
BARIUM 7440-39-3 1,000 1,000 1,000 1,800,000 J 1.30 J 1.4 8.4 J 1.5 2.1 7.8
CADMIUM 7440-43-9 1 1 1 650 J 0.065 J 0.04 J 0.04 J 0.04 J 0.04 J 0.055
CALCIUM 7440-70-2 NR NR NR NR 20,600 20,800 14,200 15,700 35,800 8,100
CHROMIUM 7440-47-3 20 20 * 20 * 78000 * J 1.80 J 1.2 J 1.6 J 1.7 J 1.8 J 2.1
COBALT 7440-48-4 10 10 10 29000 J 0.43 J 0.45 J 0.42 J 0.075 J 0.41 J 0.14
COPPER 7440-50-8 500 500 500 130000 J 3.50 J 0.95 J 2.3 J 2 3 4
IRON 7439-89-6 5,000 5,000 5,000 6,500,000 100 J 80 870 1,670 110 110
LEAD 7439-92-1 10 10 10 1,600,000 J 0.09 U 0.073 J 0.12 U 0.073 U 0.073 J 0.29
MAGNESIUM 7439-95-4 NR NR NR NR 4,270 4,550 3,320 3,030 9,350 2,330
MANGANESE 7439-96-5 200 500 500 220,000 1,990 1,990 2,600 25.1 3 8.9
MERCURY 7439-97-6 2 2 2 28,000 U 0.013 U 0.013 U 0.013 U 0.013 U 0.013 U 0.013
NICKEL 7440-02-0 20 20 20 28,000 J 1.50 J 1.1 J 1.6 J 1.2 2.9 J 1.4
POTASSIUM 7440-09-7 NR NR NR NR 2,690 2,740 2,310 1,770 2,570 2,230
SELENIUM 7782-49-2 40 40 40 46,000 U 0.18 J 1 U 0.18 U 0.18 U 0.18 U 0.18
SODIUM 7440-23-5 20,000 20,000 20,000 NR 7,550 7,700 23,800 6,700 25,700 45,900
VANADIUM 7440-62-2 200 200 200 65,000 J 4 J 2 U 0.51 U 0.51 J 3 J 3
ZINC 7440-66-6 2,000 2,000 2,000 2,800,000 U 3.90 U 3.9 U 3.9 U 3.9 U 3.9 J 5.5
Volatile Organic Compounds - VOCs (Analytical Method 8260)1,2-DIBROMO-3-CHLOROPROPANE 96-12-8 0.2 0.4 0.4 1.2 U 0.50 U 5.0 U 0.50 U 10. U 0.50 U 0.50 U 0.50 U 0.50
1,2-DIBROMOETHANE 106-93-4 0.05 0.2 0.2 8.70 U 0.22 U 2.2 U 0.22 U 4.4 U 0.22 U 0.22 U 0.22 U 0.22
2-BUTANONE 78-93-3 4,000 4,000 4,000 22,000 U 1.3 U 13. U 1.3 U 26. U 1.3 U 1.3 U 1.3 U 1.3
4-METHYL-2-PENTANONE 108-10-1 500 500 500 11,000 U 1.3 U 13. U 1.3 U 26. U 1.3 U 1.3 U 1.3 U 1.3
ACETONE 67-64-1 6,000 6,000 6,000 160,000 JB 3.1 JB 33 JB 2.8 U 44. U 2.2 JB 2.6 U 2.2 JB 2.4
CHLOROETHANE 75-00-3 7 7 7 20,000 U 0.55 U 5.5 U 0.55 U 11. 4.7 U 0.55 U 0.55 U 0.55
CHLOROMETHANE 74-87-3 3 20 20 NR J 1.2 U 3.6 U 0.36 U 7.2 U 0.36 J 1.6 2.3 J 1.3
CIS-1,2-DICHLOROETHENE 156-59-2 70 10 10 2,000 3.1 U 2.1 2.8 U 4.2 8.1 6.3 14 3.3
ETHYLBENZENE 100-41-4 30 30 30 1,500 U 0.021 U 2.1 U 2.1 U 4.2 U 0.021 U 0.021 U 0.021 U 0.021
M-,P-XYLENE DEP2068 600 1000 ** 1000 ** 790 ** U 0.59 U 5.9 U 0.59 U 12. U 0.59 U 0.59 U 0.59 U 0.59
METHYL ACETATE 79-20-9 NR NR NR NR U 0.53 U 5.3 U 0.53 U 11. U 0.53 U 0.53 U 0.53 U 0.53
METHYLENE CHLORIDE 75-09-2 5 40 40 2,600 JB 1.3 JB 19 U 1.1 U 23. JB 1.5 JB 1.4 JB 1.3 JB 1.3
O-XYLENE 95-47-6 600 1000 ** 1000 ** 790 ** U 0.25 U 2.5 U 0.25 U 5.0 U 0.25 U 0.25 U 0.25 U 0.25
TETRACHLOROETHENE 127-18-4 3 40 40 880 E 650 600 E 710 J 500 31 190 140 77
TOLUENE 108-88-3 600 600 600 12,000 U 0.27 U 2.7 U 0.27 U 5.4 U 0.27 U 0.27 U 0.27 U 0.27
TRANS-1,2-DICHLOROETHENE 156-60-5 100 100 100 2,000 U 0.25 U 2.5 U 0.25 U 5.0 J 0.41 U 0.25 U 0.25 U 0.25
TRICHLOROETHENE 79-01-6 5 4 4 5.8 5.6 U 2.8 5.6 U 5.6 12 3.3 5.5 3.5
VINYL CHLORIDE 75-01-4 0.2 0.2 0.2 160 J 0.27 U 2.5 U 0.25 U 5.0 2.2 U 0.25 U 0.25 U 0.25
Dissolved GasMETHANE 74-82-8 NR NR NR NR
ETHANE 74-84-0 NR NR NR NR
ETHENE 74-85-1 NR NR NR NR
METHANE (Dilution) 74-82-8 NR NR NR NR
ETHANE (Dilution) 74-84-0 NR NR NR NR
ETHENE (Dilution) 74-85-1 NR NR NR NR
Notes: ug/L = micrograms per liter, NR = not regulated, NA = not analyzed, MEDEP = Maine Department of Environmental Protection, 2013 MEDEP RAGs = Maine Remedial Action Guidelines for Sites Contaminated with Hazardous Substances, Revised May 8, 2013
Bold Font = Analytical Detection, U = less than (non detect), J = Estimated, * = Guideline for Chromium VI, ** = Guideline for Xylenes, 2012 MEGs = Maine Center for Disease Control Maximum Exposure Guidelines for Drinking Water, dated October 19, 2012
Detected concentration or reporting limit exceeds MEG or Residential RAG.
Detected concentration or reporting limit exceeds Construction Worker RAG.
Detected concentration or Reporting Limit exceeds Project Action Limits
U 10
U 10
24
N/A
N/A U 10
U 10
U 10
U 10
U 10
N/A
ESLT-GW-IN1B1-1015 (Dilution)
ESLT-GW-MWRP-1015 (Lab Dilution)
U 10
U 10
U 10
U 10
U 10
U 10
N/A
N/A
ESLT-GW-IN7B-1015 ESLT-GW-MW36B1-1015ESLT-GW-IN1B1-1015 ESLT-GW-IN1B2-1015
N/A
Analyte ESLT-GW-MWRP-1015 (ESLT-GW-IN1B1-1015 DUP)
N/A
Maine CDC 2012 Maximum
Exposure Guidelines
(ug/L)
2013 Maine Remedial Action Guidelines for Groundwater
by Exposure Pathway
N/A
Project Action Limits (ug/L)
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/AN/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A N/A
N/A
N/A
N/AN/A N/A
N/A N/A
U 1044
U 10N/A
N/A
N/A
N/A
N/A
U 10
TABLE 1-1
Sample ID
N/A
N/A
N/A
CAS No.ESLT-GW-MW23B-1015
Page 1 of 3
Residential (ug/l)
Construction Worker (ug/l)
Metals (Analytical Methods 6010/7000)ALUMINUM 7429-90-5 7,000 7,000 7,000 9,200,000 J 24 J 22 J 24 J 44 J 138
ANTIMONY 7440-36-0 3 3 3 3,700 1.03 J 0.2 J 0.3 J 0.095 2.65
ARSENIC 7440-38-2 10 10 10 1,400 U 2.2 U 2.2 U 2.2 U 2.2 6.5
BARIUM 7440-39-3 1,000 1,000 1,000 1,800,000 J 1 2.6 J 1.2 J 1 3
CADMIUM 7440-43-9 1 1 1 650 J 0.06 J 0.055 J 0.04 J 0.08 J 0.08
CALCIUM 7440-70-2 NR NR NR NR 9,450 68,000 62,000 20,400 41,200
CHROMIUM 7440-47-3 20 20 * 20 * 78000 * J 1.7 J 1.9 J 1.7 J 1.6 J 3.3
COBALT 7440-48-4 10 10 10 29000 J 0.11 J 0.5 J 0.46 J 0.3 J 0.17
COPPER 7440-50-8 500 500 500 130000 J 2 J 1.9 3.3 J 1.8 J 2.7
IRON 7439-89-6 5,000 5,000 5,000 6,500,000 150 8,500 1,230 11,000 160
LEAD 7439-92-1 10 10 10 1,600,000 J 0.085 J 0.09 U 0.073 J 0.075 J 0.29
MAGNESIUM 7439-95-4 NR NR NR NR 2,200 2,650 7,100 3,500 7,250
MANGANESE 7439-96-5 200 500 500 220,000 14.9 139 252 217 12
MERCURY 7439-97-6 2 2 2 28,000 U 0.013 U 0.013 U 0.013 U 0.013 U 0.013
NICKEL 7440-02-0 20 20 20 28,000 J 1.5 J 1.4 J 1.5 J 1.2 J 1
POTASSIUM 7440-09-7 NR NR NR NR J 895 122,000 1,600 32,600 2,070
SELENIUM 7782-49-2 40 40 40 46,000 U 0.18 U 0.18 U 0.18 U 0.18 U 0.18
SODIUM 7440-23-5 20,000 20,000 20,000 NR 4,410 41,500 8,300 29,100 11,300
VANADIUM 7440-62-2 200 200 200 65,000 J 1 U 0.51 U 0.51 U 0.51 J 3
ZINC 7440-66-6 2,000 2,000 2,000 2,800,000 U 3.9 19 94.5 23 J 7
Volatile Organic Compounds - VOCs (Analytical Method 8260)1,2-DIBROMO-3-CHLOROPROPANE 96-12-8 0.2 0.4 0.4 1.2 U 0.50 U 0.50 U 0.50 U 50. U 0.50 U 0.50 U 2.5
1,2-DIBROMOETHANE 106-93-4 0.05 0.2 0.2 8.70 U 0.22 U 0.22 U 0.22 U 22. U 0.22 U 0.22 U 1.1
2-BUTANONE 78-93-3 4,000 4,000 4,000 22,000 U 1.3 58 U 1.3 U 130 U 1.3 U 1.3 U 6.6
4-METHYL-2-PENTANONE 108-10-1 500 500 500 11,000 U 1.3 25 U 1.3 U 130 U 1.3 U 1.3 U 6.6
ACETONE 67-64-1 6,000 6,000 6,000 160,000 U 2.2 B 31 JB 2.4 U 220 B 10 U 2.2 JB 14
CHLOROETHANE 75-00-3 7 7 7 20,000 U 0.55 U 0.55 U 0.55 U 55. U 0.55 U 0.55 U 2.8
CHLOROMETHANE 74-87-3 3 20 20 NR J 1.4 U 0.36 2.6 U 36. U 0.36 J 1.4 U 1.8
CIS-1,2-DICHLOROETHENE 156-59-2 70 10 10 2,000 U 0.21 190 130 110 2.7 5.0 J 3.4
ETHYLBENZENE 100-41-4 30 30 30 1,500 U 0.021 U 0.021 U 0.021 U 21 U 0.021 U 0.021 U 1.0
M-,P-XYLENE DEP2068 600 1000 ** 1000 ** 790 ** U 0.59 U 0.59 U 0.59 U 59. JB 0.74 U 0.59 U 3.0
METHYL ACETATE 79-20-9 NR NR NR NR U 0.53 4.8 U 0.53 U 53. U 0.53 U 0.53 U 2.6
METHYLENE CHLORIDE 75-09-2 5 40 40 2,600 JB 1.3 JB 1.6 JB 1.2 JB 170 U 1.1 JB 1.4 JB 8.7
O-XYLENE 95-47-6 600 1000 ** 1000 ** 790 ** U 0.25 U 0.25 U 0.25 U 25. B 2.4 U 0.25 U 1.2
TETRACHLOROETHENE 127-18-4 3 40 40 880 U 0.40 100 E 3,900 3,900 10 E 240 220
TOLUENE 108-88-3 600 600 600 12,000 U 0.27 U 0.27 U 0.27 U 27. U 0.27 U 0.27 U 1.4
TRANS-1,2-DICHLOROETHENE 156-60-5 100 100 100 2,000 U 0.25 U 0.25 U 0.25 U 25. J 0.77 U 0.25 U 1.2
TRICHLOROETHENE 79-01-6 5 4 4 5.8 U 0.28 12 47 U 28. 2.8 4.8 J 4.4
VINYL CHLORIDE 75-01-4 0.2 0.2 0.2 160 U 0.25 12 J 1.4 U 25. 20 U 0.25 U 1.2
Dissolved GasMETHANE 74-82-8 NR NR NR NR E 6,000
ETHANE 74-84-0 NR NR NR NR U 10
ETHENE 74-85-1 NR NR NR NR 1,000
METHANE (Dilution) 74-82-8 NR NR NR NR 4,800
ETHANE (Dilution) 74-84-0 NR NR NR NR U 100
ETHENE (Dilution) 74-85-1 NR NR NR NR 870Notes: ug/L = micrograms per liter, NR = not regulated, NA = not analyzed, MEDEP = Maine Department of Environmental Protection, 2013 MEDEP RAGs = Maine Remedial Action Guidelines for Sites Contaminated with Hazardous Substances, Revised May 8, 2013
Bold Font = Analytical Detection, U = less than (non detect), J = Estimated, * = Guideline for Chromium VI, ** = Guideline for Xy
Detected concentration or reporting limit exceeds MEG or Residential RAG.
Detected concentration or reporting limit exceeds Construction Worker RAG.
Detected concentration or Reporting Limit exceeds Project Action Limits
N/A
U 10
Sample ID
TABLE 1-1
U 10
U 10
U 10
N/A
U 10
U 10
ESLT-GW-MW3B-1015
U 10E 5,300
ESLT-GW-MW54B-1015ESLT-GW-MW57B1-1015
(Lab Dilution)ESLT-GW-MW57B1-1015
Project Action Limits (ug/L)
Analyte ESLT-GW-MW54B-1015 (Lab Dilution)
Maine CDC 2012 Maximum
Exposure Guidelines
(ug/L)
2013 Maine Remedial Action Guidelines for Groundwater
by Exposure Pathway
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/AN/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
U 10N/A
N/AN/A
16
23 U 10
N/A
N/AN/A
N/A N/A
N/A
N/A
6,800
U100N/A
N/AN/A
N/A
N/A
N/A
N/A
N/A
N/A
U100
CAS No.ESLT-GW-MW55B-1015 ESLT-GW-MW51B-1015
Page 2 of 3
Residential (ug/l)
Construction Worker (ug/l)
Metals (Analytical Methods 6010/7000)ALUMINUM 7429-90-5 7,000 7,000 7,000 9,200,000 1,060 J 239 620
ANTIMONY 7440-36-0 3 3 3 3,700 1.3 J 0.45 J 0.43
ARSENIC 7440-38-2 10 10 10 1,400 U 2.2 J 4 J 4
BARIUM 7440-39-3 1,000 1,000 1,000 1,800,000 860 13.4 14.1
CADMIUM 7440-43-9 1 1 1 650 J 0.085 J 0.08 J 0.065
CALCIUM 7440-70-2 NR NR NR NR 625,000 56,000 55,000
CHROMIUM 7440-47-3 20 20 * 20 * 78000 * 25.3 J 2.3 J 2.2
COBALT 7440-48-4 10 10 10 29000 11.6 J 0.12 J 0.18
COPPER 7440-50-8 500 500 500 130000 16.3 J 2.5 J 1.3
IRON 7439-89-6 5,000 5,000 5,000 6,500,000 2,090 160 160
LEAD 7439-92-1 10 10 10 1,600,000 1.43 U 0.073 J 0.13
MAGNESIUM 7439-95-4 NR NR NR NR 140 2,600 2,420
MANGANESE 7439-96-5 200 500 500 220,000 7.15 J 1.2 4.8
MERCURY 7439-97-6 2 2 2 28,000 J 0.02 U 0.013 U 0.013
NICKEL 7440-02-0 20 20 20 28,000 6 J 1.4 J 1.3
POTASSIUM 7440-09-7 NR NR NR NR 191,000 8,250 9,000
SELENIUM 7782-49-2 40 40 40 46,000 U 0.18 U 0.18 U 0.18
SODIUM 7440-23-5 20,000 20,000 20,000 NR 347,000 12,500 12,800
VANADIUM 7440-62-2 200 200 200 65,000 J 1 J 3 J 3
ZINC 7440-66-6 2,000 2,000 2,000 2,800,000 10 J 8 U 3.9
Volatile Organic Compounds - VOCs (Analytical Method 8260)1,2-DIBROMO-3-CHLOROPROPANE 96-12-8 0.2 0.4 0.4 1.2 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50
1,2-DIBROMOETHANE 106-93-4 0.05 0.2 0.2 8.70 U 0.22 U 0.22 U 0.22 U 0.22 U 0.22
2-BUTANONE 78-93-3 4,000 4,000 4,000 22,000 U 1.3 U 1.3 U 1.3 U 1.3 U 1.3
4-METHYL-2-PENTANONE 108-10-1 500 500 500 11,000 U 1.3 U 1.3 U 1.3 U 1.3 U 1.3
ACETONE 67-64-1 6,000 6,000 6,000 160,000 B 93 JB 2.5 U 2.2 6.3 JB 3.5
CHLOROETHANE 75-00-3 7 7 7 20,000 U 0.55 U 0.55 U 0.55 U 0.55 U 0.55
CHLOROMETHANE 74-87-3 3 20 20 NR J 1.9 2.3 J 0.86 U 0.36 U 0.36
CIS-1,2-DICHLOROETHENE 156-59-2 70 10 10 2,000 U 0.21 J 0.32 U 0.21 U 0.21 U 0.21
ETHYLBENZENE 100-41-4 30 30 30 1,500 U 0.021 U 0.021 U 0.021 J 0.26 U 0.021
M-,P-XYLENE DEP2068 600 1000 ** 1000 ** 790 ** U 0.59 U 0.59 U 0.59 J 0.77 U 0.59
METHYL ACETATE 79-20-9 NR NR NR NR U 0.53 U 0.53 U 0.53 U 0.53 U 0.53
METHYLENE CHLORIDE 75-09-2 5 40 40 2,600 JB 1.3 JB 1.2 JB 1.4 JB 1.4 JB 1.3
O-XYLENE 95-47-6 600 1000 ** 1000 ** 790 ** U 0.25 U 0.25 U 0.25 2.4 U 0.25
TETRACHLOROETHENE 127-18-4 3 40 40 880 9.7 18 U 0.40 U 0.40 U 0.40
TOLUENE 108-88-3 600 600 600 12,000 1.8 U 0.27 U 0.27 U 0.27 U 0.27
TRANS-1,2-DICHLOROETHENE 156-60-5 100 100 100 2,000 U 0.25 U 0.25 U 0.25 U 0.25 U 0.25
TRICHLOROETHENE 79-01-6 5 4 4 5.8 J 0.49 J 0.69 U 0.28 U 0.28 U 0.28
VINYL CHLORIDE 75-01-4 0.2 0.2 0.2 160 U 0.25 U 0.25 U 0.25 U 0.25 U 0.25
Dissolved GasMETHANE 74-82-8 NR NR NR NR
ETHANE 74-84-0 NR NR NR NR
ETHENE 74-85-1 NR NR NR NR
METHANE (Dilution) 74-82-8 NR NR NR NR
ETHANE (Dilution) 74-84-0 NR NR NR NR
ETHENE (Dilution) 74-85-1 NR NR NR NR
Notes: ug/L = micrograms per liter, NR = not regulated, NA = not analyzed, MEDEP = Maine Department of Environmental Protection, 2013 MEDEP RAGs = Maine Remedial Action Guidelines for Sites Contaminated with Hazardous Substances, Revised May 8, 2013
Bold Font = Analytical Detection, U = less than (non detect), J = Estimated, * = Guideline for Chromium VI, ** = Guideline for Xy
Detected concentration or reporting limit exceeds MEG or Residential RAG.
Detected concentration or reporting limit exceeds Construction Worker RAG.
Detected concentration or Reporting Limit exceeds Project Action Limits
TABLE 1-1
CAS No.
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A N/AN/A N/A N/A
N/A
N/AN/A
N/A N/A
N/A N/A
U 10
25
N/A
U 10
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
Maine CDC 2012 Maximum
Exposure Guidelines
(ug/L)
2013 Maine Remedial Action Guidelines for Groundwater
by Exposure Pathway
ESLT-GW-MW57B2-1015
Sample ID
U 10
U 10
U 10
U 10
ESLT-GW-MW58B2-1015ESLT-GW-MW58B1-1015
26
U 10
U 10
Project Action Limits (ug/L)
Analyte ESLT-TB-1015 (Trip Blank)
ESLT-GWLORD-1015
U 10
U 10
Page 3 of 3
IN-1B1 IN-1B2 MW-3B MW-34B1 MW-34B2 MW-35B MW-36B1 MW-36B2 MW-43B1 MW-43B2 MW-42S MW-43S MW-45S IS-1B IS-2B MW-50S IS-1S IS-2S
NB NB NB NB NB NB NB NB NB NB NO NO NO SB SB SO SO SO
November-01 1,400 300 6,600 24 9,100 230 12 150 180 dry dry dry 2 19 42 8 11
April-02 1,800 310 1,100 14 3,200 380 25 220 180 13 51 dry 9 16 42 14 40
April-03 5,700 23 6,100 75 1,200 300 9 110 5 29 11 4 1U 14 5U 6
October-03 480 61 10,000 13 850 310 30 40 210 7 19 25 18 13
April-04 180 81 1,100 11 2,000 350 34 41 48 4 27 4 9 17 16 12 11
April-05 275 20 2,900 2 590 190 27 37 140 1 7 2 5 8 9 5 7
October-05 35 55 610 7 1,700 260 32 44 180 105 4 3 7 10 7 9
April-06 2,100 24 890 12 230 29.5 47 190 2 63 3 4 5 8 9 8
August-06
September-07
August-07 110 150 840 16 120 30 80.5 42 220 950 1.5 1.9 1 7.8 9.5 7.7
October-07 3,600 210 3,000 64 1,650 1 230 20 47 17 110 380 2.5
April-08 97 130 1,850 760 1.6 120 6.8 19 5.2 1.7 12 5.7 1.9 0.91 3.9 1.6 2.9
October-08 110 190 1,700 540 2.4 845 180 18 32 11 1.5 9.6
May-09 170 200 1,650 36 1.2 535 140 34 28 8.8 6.55 3.3 6.8 7 4
October-09 16 160 490 90 5U 61 10 8.4 1.2 2.7
May-10 15 97 5U 30 5U 22 23 20 2.9 dry 1.5 1.2 0.92 0.5U 4.9 3.9 2.9
October-10 35 195 3.7 510 8.1 220 48 21 28 5.5 1.1 6.5 dry
November-10
May-11 42 120 1.2 24 1.3 590 90 23 31 2.8 dry 5U 1.9 2.8 4.5 4.7 3.3 4.2
November-11 6 92 51.0 13 2.3 650 52 6.9 28 1.5 dry 22 dry
December-11
May-12 370 85 4.0 800 3.1 26 60 25 33 4.1 0.47 10 0.57 1.5 0.52 4.2 3.5 3.9
October-12
Nov-16 100 170 11 620 2 98 93 26 42 5 18 1
April-13
June-13 280 13 4 110 2U 4 62 24 41 3 8 2U
October-13 265 22 2 99 2U 950 85 20 10 2U 380 2U
May-14 330 25 2 U 660 2 U 25.5 68 13 11 2 U 17 2U 2U 2U 3 2U 3
Oct-15 600 31 0.4 U NS NS NS 77 NS NS NS NS NS NS NS NS NS NS NS
Notes:
1. Sample collected in September 2007 4. U = below contract required quantitation limit.2. Blank = not sampled or a gap in historical data reviewed. 5. italic text indicates the value listed is the average of the field sample and field dublicate results3. All concentrations listed in micrograms per liter (μg/L). 6. NO = northern overburden aquifer, NB = northern bedrock aquifer, SO = southern overburden aquifer, SB = southern bedrock aquifer
7. NS = Not Sampled
Table 2-1Hitorical PCE Concentrations
Historical PCE Concentrations Eastern Surplus Company Site Meddybemps, Maine
Treatment system and northern plume extraction wells offline.
First bioremediation injection in northern plume area.
Second bioremediation injection in northern plume area.
Sample LocationAquifer
Date
Treatment system and extraction wells offline.
Restarted treatment system and extraction wells.
Southern plume extraction well offline.
APPENDIX B
Field Data
F ______ _____ ______ ______
MI ___ ___
~~1 _____ ____ ____ _____
/~V
fl/i _________ ________ ________ _________
0’) _____ ____ ____ _____
‘.1 ___ ____ ____
A)
,ndard Operating Procedures Field FormskSampl~ng\Sanpling_AtI
______________ fovc
____________ Pvc
4a ~ (~~LJ) ri~L~
A ~ p~f ~5~ft#t~f V q~’’ ~
n —~n — I GROUNDWATER LEVEL SO~No hYD~D3 I Page j of
s.’i~sas#~W I Date b/IS/id RevMEASUREMENT LOG
Prepareo by
I tr.cwoe~g Ir,c ~~cnares~ OLin Approveo ti~SHEET
Sue Narie 4 5k ‘&i S p 1 ..i S Terroerature Range 3 2 5~~)Projeci NumberItasl. rrecipIrauon 5 %J Pc. I C oçj p 5Personnel. c. I~ C-nij~ ~ f / r e ta~, (~,r4c’ I (ywrnd Soeeo Uireci art
Mtc,4 R.—~ / ctLIt~ .l4~EQUIPMENT INFORMATION
.~‘
Tyrte or Mdci Icrelet wa1~rLev~I I Interlace Probe lype of Mar toiin~3 [quiDnien: side 01D FID / Other
---Serial No. Serial No
NobisNo 5K W,w/ O,PPt4 NobisF’o
/ NLatest .atibration Dale
FIELD DATA
eVelt or Reference F.tevalion of PlO or FIDWater Level Adjosled GrouridwaletP’ezonielei me ‘oin: (SP Reference Readiro Ooseivalioi.sReading bill Depth (1:1 Elevation Itt
No. ~5 PVCI Pain: ppnit
393-I ~‘ooo ~i.ii p39.e3-a ,nc ~
~ n ,..z — —
WRdR,~a,1 Pa3 hl~82~s,?.-I,t2tg //).p9 ~)r~q 4,2/pgnv-id- /618 g.~ ng ~Ww-/8’~ “~fl .sa.Jc ~/~;3 c4~c9v23-.B ,~s’a 637 .br,3 /4”.R9’
~ .t~2 DT,3 j-2.3~j,y~4 ,~4t~9 en’ -~ja ~ ~
,≥c-ii/ /~;~ 7 ~);i’, .23. 7~’J~7J3 70; 8.&.i )03 AS.oy)qa~s y~/9 ,‘,,7./Q /)~? .2O.~Q’4fr /Z’&/ 7.3.?? 1’ZD L/3,SO~93&~ ,2J.5 /1.34 .bra /4.fl7,34~%2~s /7%? id.9O ‘~ ~ogg3-/ /7yS //.Q) .i’7~8 .?.S.3/
~fczS~ ‘S.Es ~ //Pi.bO≥nf:3;:~~ ,,sp ZZ-3 ~o. 9,1o’./.a /5ç59 ~~713 ‘1/76‘ii vvss z at%≤~ (LII flrI4 /Lfl.qQ
Neil?? pqk
C.a’e3-~~5 ,Ov’c
NOTES S~. Startdoipi. t~. Road 8cc. PVC. Riser
~‘.3≤ FVC w~, N ~S2-ía
top~- ii.~i~
DT~ ‘15.35Sigriatu e
O~ap .~4.tI(J
4-i ___ __ ___ ___ ___ __
4i~z __ __ __ __ __ __
NOTES S~ Standp DC F~B Road Box PVC
3’
I GROUNDWATER LEVEL SOP No HYD-003 Page: 2. of 2sa’!sJe.sft.~ I Date it/ugiiS I Rev.:
I MEASUREMENT LOG Prepared by
SHEETNob~ Eng~ereg Inc. n~i~n&ne~.~ Approved by
S~e Name: E a j /tI7AJ ≤..iQ6? LU( Temperature Range 12 —f0Project Number/Task Precipitation 5 ‘-‘t.J Pa_fl Ci oc.’edjPersonnel: R’ tA cc..np~da /re~it~i ~ot.f /%. Wind Speed/Diection
/3flCo-~J gi, j~ LuEQUIPMENT INFORMATION
ype of Meter (circle) Water Level / Interface Probe Type of Montloring Equipment (circle): PID / FID / Other
Serial No. ~ fk’.— He -z~ Serial No.
Nobis No Nobis No.
Latest Calibration Date ft fi4( i S
FE14)fA~Welt or Reference Elevation of PID or FID
Piezometer Time Point (SP Reference Water Level Ad)u~Ied Groundwater Reading ObseNationsReading (It) flepd’ (It) Elevation (It)
Af1h~ RB. PVC) Point (ppm)
~~I3 4. ~s- Tot 4 /0.7 4741c3?4 4.’~e~ j~t.4 ~.oL (Oz.4O
3c41& 4; zz- ‘IX Mt J i~ 4/,. 29Mzv1~ 4:t~~ PVC- ft.w Z34o
.?rM7~ 143/ -rccMbJ q.s/ sz.~ieJ-2.’t ~&, 9’t •7.A~.2z,s4.
‘j3~l ~ Q~lc !~.6p 111,17—tM44~ 4,’s3 ??ILfS fszS
≤1s3 4S~, I~OtktLuLS~ 9 3~ zzflcu/s 4~,Ct fcc Mdd,Li 9.&.8 4e,~sr4B?1o3 fCLM~M~Ql4 940 r~.i&nc SIozl Pv~ 4Q73,? !flIc Pvc 9•gO ?3,/4-.~
.161 .≤;fll Pb’~. 4.€~B 171/9 V ,4/ b,Ilvrsmffli- 4.fl Pi€Z I Jc~cyI lv~-i32~;3r evc IL3~ /Cf.41-4 i 5jQJ n~’c- ~ ~ ~
3U~Is;4,_4- Pvc Scg1’ ~St tç49’ Pvc,
Signature
indard Operating Prooedures~Field Forms~Sampling~Sampl.ng_All
~ØROII%
C)Drinking Water Sampling Data Sheet
Site Name: /~45/~ftt~7 6o,p/u-.sLocation ID: Co
Owner/Occupant Name: fi?a/4eu’ Lo’4
Owner/Occupant Address:
Sampler(s): 1R5h Pea/c ,)Clvji Jj/t////4
Sample Collection Date:
Sample Collection Time: / ~; /c’ ~
Purge duration: f5 tn~i1jfrs~
Sample location (kitchen sink, outdoor faucet, etc.):
O~t5/h *99) north i’~i€’(&
Comments/Notes (treatment, water quality, QAIQC samples, Change innumber/age of users, etc):
3~p o~/k /4c ~≤ k&~re~ *~/mrn/
WeIl# /Y/W-.)IOAs • ~‘ .0
1~4~I~,’l~”
I’! ir -- ~ ..‘
~ -—-------~.— ~
— Sample Device ~ - IORP Turb. I
01
Laborato&y Sample NumbersAnalysis / Depth Number
Date ,scs/zo/;S
Time Water LevelBegin Time of Purge Screen Interval
Static Water Level Total Depth 3 2~ 75 Well Diameter
Monitoring Well Purge and Sample Data SheetSite Name ~ S~’rpL~’c
Flow DO Temp. Cond. p11
WrIte Meter Number of Instrument Used I ii
— Formation
Mir~. j Feet below NIP mlJMin mgIL Celcius - II -k~H+] mV NTIJ
Comments.~:io q35 -____
3:55 ~ 77 /L.5 -‘~33 -7-es 230 2Se1j9’q3 ieo ~36 /M’1 ~W1 7≠~J ~j8 ~ 2~,z3’Ly5 ci.g i’io 4iq 7.8 221
.Y.50 ,p,p’~ //.q~ ~c33’ .~ 74! 2082 2-6.)~ 5c /0./ti iz 773 /~f311:00 A]’ wlti O-ee;~eas -cQ 4~i~I 4 tkkk 8u~- ~ ‘n’-”1’-- ~,q,1/./k1,’~/.C5 7t2•)l ~7L iiB //2-// ~ 7,tL1 if~ Z/.OQ~, /o.c7 i~Z ~ //.41 435 ~ zzS 7 jq.ggi~ ~i // ~ 3~~y Z5f ‘/93 -/7,5 - -
4’~zô ,&h& /Zg ,o7’ f.Z1 . t33 7,~ 126 ,59g-zc i2~f , 1,.92i- ~ ~ /g.c~q:3o 0o5 ,q.g5 4~L 7~fl.. /7~ /c,~ C,~ni’JoIJ3[c~t.eroY.J
‘Y;iT /o.≤o /12 ~‘7 1/~~@ P3/ 7,7’? /‘I& /2J’ O/’CI oX ~iot~/ ,. ,‘
‘twp /O,~& //~. .oe-( /~,93 •~1Z~1 774’ /34(≤ /4/~3‘f4g~5~ /Q.&o il~ .o3 //~% PyZC 7~ —izCL1.-~O iz,c~l 3q13 7.~g /7Z6 [‘2iI’SS /O.bD //(~ O,00 //.~L) ‘~LL 7~ /3.5’S . ~‘A)nipk cd <;~v
Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 mtJMinWater Level +- 0.01DO +- 10%Turb +-10%
mLIFt infonnatlon3/4 In well = 87 mL/Ft2 in well = 6l7mUFt -
4inwell247OmLIFtCond. + 3%pH +- 0.1eH +- 10 myTemn. +- 0.1
Eli Correction for A9IA9CI probe:Add 190 mV to ORP value
Samplers:
Record all instrument calibrations InInstrument Calibration Log Book or Field Book j. ________
Date Revfld 1/28/2002
‘(2a’-.weU# 41W5’
Date 10 20 ZDI~Z
Static Water LevelBeqin Time of Purge
EquIlibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 mLJMinWater Level +- 001DO 4-10%Turb ~-10%Eh Correction for AgIAgCI probe:Add 199 mV to ORP value
Write Meter Number of Instrument Used
Time Water Level Flow DO Temp. Cond. pHMm Feet below MP I mtJMin mg/L Celcius -Ioq(H+] I mV NTU
Monitoring Well Purge and Sample Data SheetSite Name a Jf-caiv ~~ a L
Total Depth ‘5’. Wel Diameter .—
Screen Interval — Formation ..— Sample Device ó4nøs.y /vc.r ~ ‘t .*~
ORP Turb. t4t~ ~
Comments
~Q n~Ig/l:i5 /1.30 Zfl//kU.a 22 ¶9 a3~’8 ~:z i273 ó~’T113.3 11:7-9 rzMi~a 7,2 9~LJ .313 Y.SL 1327 3.7≤‘L’is jr~ fOtJ/~ 11.9 (0.33 .3cL ~ ec~ 2.15
ThuD /1.29 132MIrn~ ~,( 350 ~.r7 13143 2./g/j,tj5 Il~2’1 ~t~m,rq ~‘fl -319 w1i) ,ti~ 3od
ii ‘112. ~ 9 ‘~ )3.~45 .3118 s~.y~3 iVi 7 2~o3irS3 ~I ~&/h1E~~J /2.0 ic qg ..3qg L,cfg 1q10 14ss/2:oo i),2’t ~fS/n~1y1 n.j Ifl.’-17 t3Y3 7.’~7 IHZA (‘IT
mLJFL InformationSf4 in well = 87 mlJFt2 in well = 6l7mtJFt4 in well = 2470 niL/Fl
Cond. +- 3%pH +- 0.1OH +- 10 myTemp. +- 0.1
Samplers:12/ 41
Record all instrument calibrations ininstrument Calibration Log Book or Field Book
Laboratoty Sample NumbersAnalysis? Depth Number
Date Revised 1/28/2002
Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 rniJMinWater Level +- 0.01DO.- 10%Turb +- 10%Eli Correction for A91A9CI probe:Add 199 mV to ORP value
mL’Ft Information3/4 in well = 87 mL/Ft2 in well = 617mL/Ft4 in well = 2470 n,LJFI
Laboratory Sample NumbersAnalysis / Depth
weii# 2-iU -113Date /0 20 /5Static Water LevelBegin Time of Purge
Write Meter Number of Instrument Used
Time Water Level Flow DO Temp. Cond. pH
Monitoring Well Purge and Sample Data SheetSIte Name ≤.eiV ~≤Lp€ ‘LuSTotal Depth 5 1 - S wei Diameter ~
Screen Interval Formation — Sample DeviceORP Turb.
lvlin. [ Feet below MP mLiMin mgIL Celcius -log[H+1 I mV [ NTU
•1
54ij~& ii.
g4>4rEOF *t
Comments
iz’2~S q-’5L!z~;O c7360 léo/~,,-,j 37~ /2.05 ~ 66! /13ii 35 q~ /067M,J ~~7/O~ 12,2-q 0~q ( a.c2 (57 ~tZ:’-iD ‘7..t67 /os~op’.J 1.77 12,25 a/U &ze ~~zz 233,2~16 q~eg /og/kn,% i,o~j jz,i5 •,58 &.Lq /~g,7 ~
Iklg-rI<hc_~pifr-e5a-vr~pkd_c~iz~c&
5Prn’iplC_a.*_,a;55
Cond. +- 3%pH +-0.1eN +- 10 myTemp. +- 0.1
SamplQrs:IL~L
Record all Instrument calibrations inInstrument Calibration Log Book or Field Book
Number
Date Revised 1/28/2002
Flow 1-2 mlJMinWater Level +- 0.01DO.- 10%Turb +-10%
Laboratoty Sample NumbersAnalysis / Depth
w.iw mflw—558Date
Static Water LevelBegIn Time of Purge
Time Water Level
Monitoring Well Purge and Sample Data SheetSite Name EaSk4er~i ≤u~PLc,~S
Flow
Write Meter Number of Instrument Used
Total Depth 9~ . 35 Well Diameter
Screen IntervalDO Temp.
Mm. Feet below MP mi/Win rn~IL Celcius II -k~(H+j I iN NTU
— FormationCond. pH ORP
Sample Device £COfL4~7y2r~Turb.
gslU4 ON4fe*
~ ~1~U(’””•~ S
401
Comments
i:3≤/‘ qo g,43 aagJn~ J?3 /231 4q~~ 751 ‘~7S 5 37pLq5 r≤z. ~/7 /2Y7 ,q~0 /q4,~, 33~J.~O /O./j ~ ~iL~1 12.5g OL1≤~ 7.6/ %7Z 3I4’~
j~,5 9#/MnJ .!& /Z~’U .44’l 772- zo~~≤ ‘L3SZoO -i~°k~ o--hwt ,i~ c,’/Thq/ ~jvi5 r~ /tL≤ /otq~2. 2G /h.l/7 50
7:1-7
Z.zg ,12.ttS
210 /057 s2/n~erj .52- ia.q~ ~iig 7,47 z/~. ç~. 35 .o4( 4~7/~,v 03.) ,‘/ZZ- 761 2o~ ) L/,f7~ /nh( ~ijø~ .5/ ~z4f 2/7 3,6’13~.Lj5 /0.44 *SqwI ,~z... i2~s ~ 7&e jô3 3.78
O41~’j
EquIlIb.lum Goals3 consecutive readings 3-5 mm. apart
mLJFt Information3/4 in well 87 mi/Ft2 in well = 61 7mL/Ft4 in well 2470 niL/Ft
Cond. + 3%pH +-ftleH +- 10 myTemp. +- 0.1
Eh Correction for A9IA9CI probe:Add 199 mV to ORP value
Samplerslit ~—C(.
Record all Instrument calibrations InInstrument Calibration Log Book or Field Book
Number
Date Revised 1/28/2002
Well# 4Q~/—5q’ Monitoring Well Purge and Sample Data SheetDate /0/ zo/ccStatic Water LevelBegin Time of Purge
Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 mL/MinWater Level +- 0.0100.- 10%Turb +- 10%Eh Correction for AgIAgCI probe:Add 199 mV to ORP value
Laboratory Sample NumbersAnalysis / Depth
Time Water Level Flow
Write Meter Number at Instrument Used
Site Name jC~ss~ 5~vic ‘Lc’STotal Depth ____________
Screen Interval ~ FormationDO Temp. Cond.
Mm, [ Feet below MP I mLMin rnq/L Celcius IL -log[H+1 I mV NTU
pH
Well Diameter
- Sample Device lc~o~k7/ycsTurb.ORP
—~ -~
ii. I
OF
Comments
.tai,1 CA / ~-,,,tt,
i~
5~Z5 ~ .A~ ii 07 O3BZ 235 -6Y4 it~~ 73R —thi.~i /8-
≤~ ;≤ ‘, 1o4 ~39o -Z57 ~ zojy≤!4) 113 /O6 . ~i ii ‘-i7 31’r’ 7.57 —gc.& /5~5~~~‘*≤ OIJL/ ~/,Ijej 7~3€ -7≤~’ 9~S3“~~;o 9-83 •H3 /jg7 1g7 ‘?.3~ 80.4 téLtcC q~g log ~iO 4L4-3 ~qç, 7sT 663 7.76~ -7S3 /10 -‘it 3g9 73g ≤‘1 7<08
I
Cond. +- 3%~H +-0.1eH +- 10 mVTemp. +-0.1
mlJFt Intonnatlon Samplep:3/4mnwell=B7mUFt (?c2 in well = 617mL/Fl ________
4 in well =2470 nt/Ft ________
Record all Instrument calibrations InInstrument CalibratIon Log Book or FIeld Book
Number
Date Revised 1/28/2002
Well#Date /O/2o/ ao,3Static Water LevelBeqin Time of Purge
Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 rnL/MinWater Level +- 0.01DO +-10%Turb +- 10%Eli Correction for AgIAgCl probe:Add 199 mV to ORP value
mLJFt informatIon Samplers:314 in well — 87 mL/Ft _________
2 n well 617mL/Ft ________
4 in well 2470 mlJFt ________
mw-5o13L
Time Water Level Flow
Monitoring Well Purge and Sample Data SheetSite Name ,r44 k2,K \ cv1-z a lvçTotal Depth 11/
WrIte Meter Number of Instrument Used
Well Diameter
Screen Interval t~- FormationDO Temp. Cond. pH
Mm. FeetbelowMP mL/Mmn rng/L Celcius -loq[H+j [ mV Nfl.)
ORP
1~
fl!.f’~~. .;~ht~t ~
Sample Device 7yci~’Tuyb. ‘4r~ OF
Comments
c34 iVJ/~~.~ /“-/?% 9 7’~ •3d9 9OL z~y[≤CLl5 /2~f~O /~‘1’~/,b~ !2.≤ it)-1’-I ~3~fi S~76 je? 6799.3<’ H.1~ L7.S5 (“‘~J o)Yf ‘? 91~ I ~ 7.7~’9f~3 1s •~
Cond. +- 3%pH +~0.1eH +- 10 myTemp. +.0.1
Record all instrument calibrations InInstrument Calibration Log Book or FIeld Book
Laboratory Sample NumbersAnalysis I Depth
nwt4Lrj
Number- 5~ L
Date Revised 1/28/2002
WelI#
Date
Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 mLIMinWater Level +- 0.01DO +- 10%Turb.+- 10%Eh Correction for Ag1AgCI probe:Add 199 my to ORP value
niL/Ft information Samplers:3/4iriwell=B7mL/Ft 4632 in well = 6l7mLfFt4 in well = 2470 niiFt
Sample Device ~Lo, JrV
Turb.
Laboratory Sample NumbersAnalysis / Depth
Ps o’s,t~n4L
Monitoring Well Purge and Sample Data SheetSite Name £SCT / O€P cMtOI2fIS&4-t?S
Static Water Level (~(.c C Total Depth Y3, r~ Well Diameter —
Begin Time of Purge ~ Screen Interval .— Formalion —
Time Water Level Flow DO Temp. Cond. pH ORP
WrIte Meter Number of instrument Used
Miii. j Feet belowMP I mLiMin nng!L C&cius II -log[H+] I mV I NTU
Comments
1C17- I~D
i~ r3.’( n.’ c~at2~ ~ ~“i.c’ 71,1- - /
V~U3 (~oS 39 v~ I1.3ç~ o.~9i ~j•oi- ~ji.c~ (°2
njc trrj 7~a~ ,0.sr ~ ~ ‘isfl- g~i- 4t
Cond. +. 3%pH +- 0.1eH +- 10 mVTemp. +-O.1
Record all instrument calibrations inInstrument Calibration Log Book or Field Book
Number& (This’
Date Revised 1/28/2002
WeU#Date
Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 mLJMinWater Level 4— 0.01DO +- 10%Turb +- 10%Eh Correction for Ag!A9CI probe:Add 199 mV to ORP value
Laboratory Sample NumbersAnalysis / Depth
y~c. 6n~,V41a~-L-’
Static Water Level 0j~ ~(Begin Time of Purge (~ ~. e
Time Water Level Flow
Monitoring Well Purge and Sample Data SheetSite Name (5 CT ~/ i~6O~y~4,t-ifj
Write Meter Number of Instrument Used
Total Depth ~ Well Diameter
Screen Interval -
PC Temp. Cond.Mm. Feet below MP I m[JMin rng/L Celcius ~I -loc[H~] I mV I NTU
I ‘1A -‘~c
~1
FormationpH
-r
ORPSample Device
Turb.
Comments
_____ ~
I39~ 9if3 3Cr (L?yz o..3~ 1J? I -~ tf(,~~ ~‘~°
(3S) ci ~Q ~ 11,fl o, 7.3f — iiz~ j4o3i35~ Cj 9$& too ~ ~10 IL.c5 O,iz~ 7.31 11W7 I.CtIj 9°i ~.ac fl..q o.3~ 7,~9 - 1oa3Ho 6 T. ~‘ . ~ Ltfl- L.N48
ri Il 9, ~~t3 Lj, ~ u.c.~.. o.)~’1y T,c~9i rt.-~ i~n19r( ~fCfL( 5.kj ‘I.G5 ‘~.41 o..)33 (O.$9 .- 3I.~N~ C19ç Ilc,~y o,22e ~.e’i —22-r ~~qa’ c1 •-~- ((.33 ii,.~i 0.~ C..~l -. i’-j.O
P-~aj ti.çr 1°c. ll.6S °.~L’5 (~,.~t1$ — 1.31
~ cj ç~ c.u fl.5~t O.QI° Li-) ti,9~tpi ctsy o’.> 3.38 jt.’17- O.Qo2 C.t0(- ~5’.r ~•fl(<(35’ 9,5€ ~r’t~ ô.~°1 C.c”~ .17.3 o.3I~-q~7 cUss (oo -ç. gcz ‘1.39 a. l7~ 0.53
i ~i’1° °t jc~ (00 II 39 ~.i’j3 -3çr O.~SIL.(t() 9.y8 3.SS IL-3d 0 19 C.t~ ?‘t.5 OJL
uhL ~i. r~ i L.I-~O o. I ~‘J C, Go ~ ‘(L? 0.1-1iLrfl ~. ss Lf.Jjç ft. ~a o. en L.r~- t. fl
Lqca ~..çg Co~ ‘1.3’ it.~3 o.rs-c C.s~ ~fl./
mL/Ft information3/4 in well = 87 mlJFt2 in well = 617mL/Ft4 in well = 2470 niL/Ft
Cond. +- 3%pH +-0.1eH +- 10 myTemD. +- 0.1
Record all instrument calibrations inInstrument Calibration Log Book or Field Book
Number6 ILfS7
Date Revised 1/28/2002
—
WeII#Date
Static Water LevelBegin Time of Purge *‘:J r
Equilibrium Goals3 consecutive readin~is 3-5 mm. apartFlow 1-2 mLJMinWater Level +- 0.01DO +- 10%Turb +- 10%Eli Correction forAgIAgCl probe:Add 199 mVtoORP value
Monitoring Well i-urge ana ~arnpie isata oneetSiteName Ott’ /~~1coDy~mPj
mLIFt Information3/4 in well = 87 mIJFI2 in well = 6l7mLIFt4 in well = 2470 mL/Ft
Sample Device (r..€4 (UTurb.
Laboratoty Sample NumbeisAnalysis I Depth
Vo~ r
o:s &~4<.
Time Water Level Flow
Write Meter Number of Instrument Used
DO
Total Depth
Screen intervalTernp.
3o. ~( Well DiameterForrilalion
Cond.Mm. I Feet below MP I mLJMin mg/L Celcius II -loq[H-’-] I mV I NTU
pH ORP
~1’ Comments
_________ I
SW 7.87 SO.C~I 94o Cjq~ ?3~ ~ ~.s~c’ c~t.’~,no cj~t
03fl 15Th ≥‘-t~3 t.°~ ~ 7.3 18t8 *~cy~~sc 7. v~ a). ‘~ q ~OGz CJ.~’N :j3~ I ~ C.rf≠O’100 7.S2 Rt.sm tt.~Y7 o.219 ;~~a ity.~oqo5 ~I.57 9.11 0)93 ?.3. I ~
Cond. +- 3%pH +- 0.1eH +- 10 mVTerm,. +- 0.1
Samplers:
Record all Instrument calibrations InInstrument Calibration Lon Book or Field Book
NumberS~~(.Ae o~oS
Date Revised 1/28/2002
WeIl#Date
Static Water LevelBegin Time of Purge j) ~
WrIte Meter Number of Instrument Used
Equilibrium Goals3 consecutive readinqs 3-5 mm. apartFlow 1-2 mLIMinWater Level +- 0.0100+- 10%Turb÷- 10%Lb Correction for A9IA9C1 probe:Add 199 mV to ORP value
niL/Ft Information Samplers:3/4 in well = 87 mLfFt _________
2 in well = 6l7mLIFt _________
4 in well = 2470 mIJFt
Laboratory Sample NumbersAnalysis / Depth
A/s ~g<r~ rn.
Time Water Level
Site Name (SLYMonitoring Well Purge and Sample Data Sheet
Flow DO
Total Depth ~‘3~ V~( Well Diameter
Screen IntervalTernp.
- fll
Mm. j Feet below MP mLiMin mg/L Celcius .11 -loq[H+] I mV I NTIJ
— Formation — Sample Device &-c3 1e,ji%
Cond. pH ORP Turb.
Comments
1135 /OI~~ q-o ~c45f /“tl ~44~ B.°~ 1314 ,.{lIfl ‘°~sC 7s 5-3.51 .. f~.qg O.3tc 3’.oq f3tY c.’( ,.q~ fjt~...._tiir p. g3 3o 5°.13 (~).Y9 o.3gç &. 1° (39.2 L’Ii~~y fl.s.2 4fl~J
a13__0Li_- c
Cond. +. 3%pH +- 0.1eH +- 10 myTemp. +- 0.1
Record all Instrument calIbrations inInstrument CalIbration Lou Book or Field Book
Number&.//q7.
Date Revised 1/28/2002
Monitoring Well Purge and Sample Data SheetSlteName ESCt /D~P 1t1,~UDY&EtttfS
Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 mLJMinWater Level +- 0.0100+- 10%Turb- 10%Eli Correction for AgIAgCI probe:Add 199 my to ORP value
mLIFt Information Samplers:314 in well = 87 mIJFI ________
2 in well = 6l7mLJFt ________
4 in well = 2470 mI/Ft
Laboratoiy Sample NumbersAnalysis I Depth
I.JDL,D~. i~i/W ,&14 k(
NumQ~rS
WeIi#Date 7a ~
Static Water Level
Begin Time of Purge ~aD ‘~
Time Water Levei Flow
12. )~j~j Total Depth ~%. o1 Well Diameter
Write Meter Number of Instrument Used
Screen IntervalDO Temp. Conci.
Mm. Feet belowMP I mL/Mmn n’~gIL Ceicius II -log[H+] I mV I NTU
Formation — Sample Device_________pH ORP Turb.
Comments
/~-fl (3.jcs 7O ~,i h.c<~ c’~~ct Z~2 5.j’~I)~~ i3.fl to5~ (471- ~ o.253 2.r, —8i.~~
‘~9I r3.tU I1.C-t r..i9’( o.22-° ~. 17 °Ti.°1~1’tj 9.L2 ‘c9.Th1 0.271 7~e~ ~ ~~i- I3.t~ q3 (,.~ i~1-c ~a13 7~i’~ -~-ç a:g3ilZD r3.’43 rj r.,~1 i°3i Ofl~( ~ —89.’ i:?-’r(253 (3L{3 ~‘9 3o’~ IoJ~rL( ctfl 3.\3 — frkL9 ~n~&t3.JC ~3”(M 59 S-~~g lo.c~3 ~ ~.ar -&&c t,~-it2~57 i~, C .t~ (o.L’~ o.~1 Th~19 —73c i.’~(3o~ (3 i4~.( C. 5? 1~.cc~ o.3~ 7J3t~ — ~oz~ j (,~j
13tC (3Lj~L( (~.,3( (c.7-3 ~ ~ ~‘.° L.5%
~ ~ SoL (c’}3 o~2s3 ~ .-72.’( ~, cjty
(311 (LW 5.IS jo.~( o.?fo 7.32.. 17-a LS~5tDi’i 13.9f ~ S.U- (oJ7-o O.2~fl 1.33 -17.3 l.s~i
Cond. +- 3%pH +- 0.1eH +- 10 myTerrn. +- 0.1
4c0
Record all instrument calibrations Ininstrument Calibration Log Book or Field Book
Date Revised 1/28/2002
Time Water Level Flow
WrIte Meter Number of Instrument Used
EquilibrIum Goals3 consecutive readinqs 3-5 mm. apartFlow 1-2 rnL/MinWater Level ÷- 0.0100+- 10%Turb +- 10%Eli Correction for A91AgCI probe:Add 199 mVto ORP value
mlJFt Information3/4 in well = 87 mLiFt2 in well = Gl7mL/Ft4 in well = 2470 niL/FtRecord all instrument calibrations In -
Instrument Calibration Loq Book or Field aooic
Laboratory Sample NumbersAnalysis / Depth
p< &4jPISI 4 ‘4
NumberM’ /ut~.~ c2
Static Water Level IBegin Time of Purge I ~t
>~Well# fV\ ‘J — ~7-~ t3 ~ Monitoring Well Purge and Sample Data SheetDate Site Name ec~--~ / Os M~QOY~6A4Pj
Total Depth lo ~‘.4w Well Diameter
Screen Interval —~ FormationDO Temp. Cond. pH
Mm. j Feet below MP muMin rng/L Colcius II -k~[H+1 I mV I NTU
__________Sample Device d’c~ ~
ORP Turb.
Comments
9:2~ ,3ss ~ ~3.u ~ I3.~2 ffl3 (o~ — ~
M:23 j’f.25 cl.t, 3:;.3l ~o. t.~S U.i-3 j13o3 — ‘~S-f.9 C(i,.
92~ I1.~’1 ‘3S~’•Z~\- lo.n. ~iii ~ -Ifl~ç W5L4 ,1~c t~.J
‘-L3’~ t5.°°’ ?z.in (O.°S li.12. l3.~~3 -(SLJtcbic ~ .
Cond. +- 3%pH +- 0.1eH +- 10 mVTemp. +- 0.1
Samplers:
Date Revised 1/28(2002
f•r
___________Sample Device C≤ta( -3’.12
Turb.
-~ - Comments
Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 rnL/MinWater Level +- 0.01DO.- 10%Turb~- 10%Eh Correction for A91A9CI probe:Add 199 mV to QRP value
mi/Ft informatIon3/4 in well = 87 mi/Ft2 in weD = 6l7miJFt4 in well = 2470 rnlJFt
S am P lo rs A Laboratory Sample NumbersAnalysis / Depth
‘2<. &a~
Number c:~ (5? 1.{3
WelI#DateStatic Water Level ~, 3 *Begin Time of Purge ti-3 (~
/ Monitoring Well Purge and Sample Data Sheet
/ SiteName £scT / P~.P ,~i~pOYt~C&i.t’JTotal Depth ‘1-~’i Well Diameter ___________
WrIte Meter Number of Instrument Used
Time Water Level Flow DO Temp. Cond. pHScreen Interval Formation
Mm. j Feet belowMp mi/Mm rng/L Celcius JI -lon[H+1 ITN NTU
ORP
rtt,~. z.~i .r~. iy I~.i-~ o~’jiq I-i,~~-9 - —~ ~ V2.17-5( ~o3 lao ~ lt-€~ o.~Q l[.€~~ ~-i3-l &.~.!
flsi~ S’.&3 23~9 1L4-° oz~r i~,’i° -2LSLfrnj 7. ‘~3 c$si?i~ 2.0. ii cUc~ ~.iPi 9.R-S —t.2.D &JCTtP°p ~ ()Ô Il.dli ø.(Q~- O~j~ ~
{SDC ~J’.(~g [IA-I b.i59 g~fl ~c~~a6 ~ w.ace ((9~ ô.jqs gij
1913 3. Cj (L~a o.c3) ?-.‘I’ ?~ i.i~rst~ ~ n.~ O.jar ~ H2.7- z.~g{3l’~ ~ i’ia Oai2~Z 7-.o3 qL’.y
(“P.R F..C.3 [2~ ç,c’G. ~ eLi IC’ (dAd Q.’1i-‘82w laz Ok f~2 ‘.3~ .s~(~3 g.(~~ts( 12-U .c~? IL_fl o If° G. C~’i ~&. ~
tt3c~ ci ~‘.°k ri-St2 .~(°Q ~ ~2 ~.5’jL34~ ~ ~3 s.di— ~t, o~ioG ‘-58 C~f I
~-3+ c~ - 5.21- I L55 ~ G~.S’k c.’~ç (.51-t’(° tG3 Ia.s S’15 p.~ “~ ~ ~c-C.$:;t.t3 ~ c. i2_ U4t.{ ~ cc.7
Cond. +- 3%pH +~0.1eH 4— 10 mVTemp. +- 0_i
Record all instrument calibrations InInstrument Calibration Log Book or Field Book
Date Revised 1/28/2002
APPENDIX C
MEDEP Data Validation Checklist
Narrative - 2014-2015 Intra-well trends
Maine DEP Basic Data Review Checklist
Revision No.:00
Effective Date: 3/7/14
Page 1 of 5
Site Eastern Surplus, Meddybemps
Project
Date(s) Sampled or Sampling Event 10/20/2015
Reviewed by Campbell Environmental Group
Date Reviewed 12/11/2015
A. Data Completeness
Item for Review Reviewer Comments
Did report include original lab reports? X X *
Was report paginated? X *
Were all report pages received? X *
Did report contain results for all samples and analyses
requested on the chain of custody form?X *
Were required QA/QC results included with lab report? X *
Was EGAD EDD received? X *
Were required QA/QC results included on EGAD EDD? X *
Did reported analyte lists meet project specifications? X *
Did reporting limits meet project specifications?PQL and MDL for Manganese, 1,2‐Dibromo‐3‐Chloropropane, 1,2‐
Dibromoethane, and Vinyl Chloride, exceed applicable regulatory guidelines* X
Was the laboratory Maine certified for all
methods/analytes/matrices performed at the time of
sample analysis(if required)?
X *
*For all items checked N‐ contact chemist, lab or consultant for resolution
B. Preservation and Technical Holding Times
Item for Review Reviewer Comments Yes
If No, put X in box
then click button
Sample cooler within required temperature range at time
of receipt at laboratory(if No, enter receipt date and
cooler temp in reviewer comments)?
X 1
Samples properly preserved at time of receipt at
laboratory?X 1
Was sample extraction/digestion performed within
holding time?X 2
Was sample analysis performed within analytical holding
time?
Re‐analysis (dilution) of sample ESLT‐GW‐MWRP‐1015 was required but
conducted 11 days out of hold time. 2 X
(1) Review SAP/QAPP requirements, if unavailable use professional judgment to flag data as estimated “J” or as unusable “R”
(2) Review SAP/QAPP requirements, if unavailable,
If method HT<sample extraction/digestion/analysis time<2X method HT, then estimate data and flag with “J”
If sample extraction/digestion/analysis time>2X method HT, flag detections with a “J”, flag non‐detects as “UJ” or reject data and flag with “R”
Yes No
No
No
No
No
Maine DEP Basic Data Review Checklist
Revision No.:00
Effective Date: 3/7/14
Page 2 of 5
C. Blanks
Item for Review Reviewer Comments Yes No
Were blanks run at the frequency specified by the
method or SAP/QAPP?X *
Were target analytes detected in laboratory method
blanks?
Methylene Chloride was detected below the reporting limit in Method Blanks
WG172846‐2 and WG172905‐2X
Were target analytes detected in trip blanks(if
applicable)?
Acetone (> 2X rl), ethylbenzene, mp‐xylene, methylene chloride (<2x rl), and o‐
xylene, were detected in the VOC Trip Blank at concentrations exceeding
corresponding reporting limits.
X
Were target analytes detected in equipment blanks (if
applicable)?No equipment blanks were collected X
Were target analytes detected in any other types of
blanks included in the laboratory data report?X
Was data appropriately qualified for blank
contamination?X 3
*Contact chemist, lab or consultant for resolution
(3)Review SAP/QAPP requirements‐ if unavailable see Attachment A
D. Surrogates
Did the laboratory report results for surrogates (if
required by the analytical method)?*
If surrogates required were recoveries within acceptance
ranges?
If surrogate recoveries were outside acceptance ranges,
did the lab re‐analyze to confirm matrix interference?*
Was data appropriately qualified for unacceptable
surrogate recovery(if required)?4
*Contact chemist, lab or consultant for resolution
(4)Review SAP/QAPP requirements, if unavailable:
If recovery > higher acceptance range, flag associated detects with “J”
If lower acceptance range > recovery > 10% (20% for volatiles), flag associated detects with “J” and associated non‐detects with “UJ”
If recovery <10% (20% for volatiles), reject associated data and flag with “R”
Item for Review Reviewer CommentsYes If No, put X in box then
click button
If Yes, put X in box then click
button
X
X
No
X
X
Yes
Yes
Yes
Yes
No
No
No
Maine DEP Basic Data Review Checklist
Revision No.:00
Effective Date: 3/7/14
Page 3 of 5
E. Laboratory Control Samples (LCS/LCSD)
Item for Review Reviewer Comments
Did the LCS include all spiked compounds as required by
SAP/QAPP or method?X *
Were recoveries within acceptance ranges? X 5
Was data appropriately qualified for unacceptable LCS
recovery?X 5
Were RPD between LCS and LCSD within acceptance
ranges?No LCSD samples were analyzed. X 6
*Contact chemist, lab or consultant for resolution
(5)Review SAP/QAPP requirements, if unavailable:
Organics and wet chem: If recovery > higher acceptance range, flag associated detects with “J”
If recovery significantly <lower acceptance range, reject data and flag with “R”.
VOCs and SVOCs marginal sporadic exceedences (ME) allowed. The number of allowable marginal exceedances is as follows:
1) >90 analytes in LCS, 5 analytes allowed in ME of the LCS control limit;
2) 71–90 analytes in LCS, 4 analytes allowed in ME of the LCS control limit;
3) 51–70 analytes in LCS, 3 analytes allowed in ME of the LCS control limit;
4) 31–50 analytes in LCS, 2 analytes allowed in ME of the LCS control limit;
5) 11–30 analytes in LCS, 1 analytes allowed in ME of the LCS control limit;
6) <11 analytes in LCS, no analytes allowed in ME of the LCS control limit;
Marginal exceedances must be random and in no cases can the %R be <10%. If the same analyte exceeds the LCS control limit repeatedly, it is an indication of a systemic problem.
The source of the error must be located and corrective action taken.
Qualify results that are ≥ MDL as estimated low “J”,
Qualify non‐detects as estimated “UJ”
Upper acceptance limit<Aqueous/Water and
Soil/Sediment %R < 150% Qualify results that are ≥ MDL as estimated high “J”
%Recovery < 40% Qualify all results as unusable “R”
%Recovery > 150% Qualify all results as unusable “R”
(6) Review SAP/QAPP requirements, if unavailable use professional judgment to flag data as estimated “J” or as unusable “R”
F. Matrix Spike Samples (MS/MSD)
Item for Review Reviewer Comments
Did the MS (if performed) include all spiked compounds
as required by SAP/QAPP or method? WG172846‐5, MS ‐ WG173026‐4, WG173026RA X *
Were recoveries within acceptance ranges (if MS
performed)?X 7
Was data appropriately qualified for unacceptable MS
recovery (if MS performed)?X 7
Were RPD between MS and MSD (if performed) within
acceptance ranges?MS/MSD ‐ WG172846‐5 & 6 X 7
*Contact chemist, lab or consultant for resolution
(7) Review SAP/QAPP requirements, if unavailable use professional judgment to flag data as estimated “J” or as unusable “R”
Metals: 40%<Aqueous/Water and Soil/Sediment %R
<lower acceptance limit
If No, put X in box then
click button
YesIf No, put X in box then
click button
Yes
No
No
No
No
No
No
No
Maine DEP Basic Data Review Checklist
Revision No.:00
Effective Date: 3/7/14
Page 4 of 5
Item for Review Reviewer Comments
Yes
Were lab duplicate or field duplicate analyses performed
(if yes list type in reviewer comments)?ESLT‐GW‐IN1B1‐1015 and ESLT‐GW‐MWRP‐1015 are Duplicate samples X
Were RPDs (if applicable) within acceptance ranges?
Aluminum, chromium, copper, nickel, selenium, and vandium, were outside of
the acceptable RPD of 30%. Arsenic and cadmium were outside the RPD but
less than 2X the QL
X 8
(8) Review SAP/QAPP requirements, if unavailable:
Qualification of Organic Analytes in Lab or Field Duplicates Situation 1: Positive Detects in Both Lab or Field Duplicates
Aqueous ≤ 30%RPD Non-aqueous ≤ 50%
Sample Results Both Duplicates ≥ 2xSQL
Detects No Flag
Non-detects No Flag
Situation 2: Positive Detect in Only One Lab or Field Duplicate Sample 9
Sample Results One Sample conc. = ND (or value reported as less than the SQL) SQL < Other Sample Conc. < 2 x SQL
Detects Professional Judgment
Non-detects Professional Judgment
(9) RPDs should not be determined for duplicate pairs in this situation.
Qualification of Inorganic Analytes Based on Lab or Field Duplicates – Aqueous Matrices
Sample Results
RPD ≤ 30%Detects No Flag
Non-detects No Flag
(10) No action is taken when both field duplicate results are positive detects < SQL or are non-detects.
G. Duplicates (Note this also applies for analytes reported by more than one method)
Non-Aqueous Lab or Field Duplicate Sample Results
Both Duplicates
Both Duplicates ≥ 2 x SQL
UJ
J
Aqueous > 30%Non-aqueous > 50%
If No, put X in box then
click button
Professional Judgment
NA NA
Aqueous Lab or Field Duplicate Sample Results
Both Duplicates ≥ 5 x SQL
J
UJ
RPD > 30% Abs. Diff. ≤ 2 x SQLNo Flag
UJ
One Sample conc. = ND (or value reported as less than the SQL) Other Sample Conc. >2x SQL
J
NA
Abs. Diff. > 2 x SQL
One or Both Duplicates < 5 x SQL10
One sample conc. > 2 x SQL SQL < Other sample
conc. < 2 x. SQL
No Flag
Professional Judgment
SQL < Both Duplicate samples concs. < 2 x SQL
J
No
Maine DEP Basic Data Review Checklist
Revision No.:00
Effective Date: 3/7/14
Page 5 of 5
Qualification of Inorganic Analytes Based on Lab or Field Duplicates - Non-Aqueous Matrices
Sample Results
RPD ≤ 50%Detects No flag
Non-detects No flag
(11) No action is taken when both field duplicate results are positive detects < SQL or are non-detects.
H. Data Usability
Item for Review Reviewer Comments
If Yes, put X in box
then click button
Is there any reason to suspect carryover? * X
Is there any reason to suspect matrix interference? * X
Do chromatograms (if provided) look reasonable? Not Provided * X
Is there a compound detected below quantitation limits
that should be noted?
Per MEDEP request, compounds detected below the SQL but obove the MDL
have been reported and approrpirately qualified. X
Is there any other reason that the data should be
qualified?See above. X
Was all (or most) data qualified for a particular method
or analyte?
Numerous analytes were consistantly J flagged becaused they were reported
below the SQL. * X
Was any data rejected during the above review? * X
Is data quality sufficient for the intended
use of the data?X *
*Contact chemist, lab or consultant for resolution
Both Duplicates ≥ 5 x SQL
Non-Aqueous Lab or Field Duplicate Sample Results
Abs. Diff. > 4 x SQLJ
UJ
Abs. Diff. ≤ 4 x SQLNo Flag
No Flag UJ
RPD > 50%J
If No, put X in box then click
button
One or Both Duplicates < 5 x SQL11
Yes
Yes
No
Yes
Yes
APPENDIX D
Laboratory Report
Appendix C Intra-well Trend Narrative Page 1
Intra-well trends 2014-2015
It should be noted that the October 2015 sampling data was reported down to the laboratory’s respective
minimum detection limits. As a result, a greater number of volatile organic compounds (VOCs) were
detected, however, it is difficult to evaluate these detections in relation to previous data and
concentrations that were below the laboratory’s practical quantitation limit. Therefore, much of the data
should be considered estimates.
VOCs
IN7B - Concentrations appeared consistent with May 2014 sampling results. Similar to the 2015 results,
tetrachloroethene was the only analyte detected at concentrations above applicable regulatory guidelines.
While the concentration of tetrachloroethene in well IN7B increased between May 2015 and October
2015, concentrations of several additional compounds detected below regulatory guidelines decreased
during the same time period. No additional compounds were detected at concentrations exceeding
applicable regulatory guidelines.
IN1B - Concentrations appeared generally consistent with May 2014 sample results. In May 2015, four
compounds were detected at concentrations exceeding applicable regulatory guidelines (Cis-1,2-
dichloroethene, tetrachloroethene, trichloroethene, and vinyl chloride). In October 2015, only
tetrachloroethene, trichloroethene, and vinyl chloride were detected above corresponding regulatory
guidelines. The detected concentration of tetrachloroethene increased from 330 micrograms per liter
(ug/l) to 600 ug/l between the two sampling periods, while concentrations of additional compounds
decreased. No additional compounds were detected at concentrations exceeding applicable regulatory
guidelines.
IN-1B2 - Concentrations appeared consistent with May 2014 sample results. In May 2013, three
compounds (cis-1,2-dichloroethene, tetrachloroethene, and vinyl chloride) were detected at
concentrations exceeding regulatory guidelines. Concentrations of tetrachloroethene and vinyl chloride
were also detected above corresponding guidelines during the October 2015 monitoring event, however,
trichloroethene was also detected above corresponding regulatory guidelines in 2015, while cis-1,2-
dichloroethene was not. No additional compounds were detected at concentrations exceeding applicable
regulatory guidelines.
MW-3B - No VOC concentrations were detected at concentrations exceeding corresponding regulatory
guidelines during the October 2015 monitoring event. In May 2014, tetrachloroethene was detected at 14
ug/l, exceeding applicable guidelines.
MW-23B - In May 2014, cis-1,2-dichloroethene, tetrachloroethene, and trichloroethene were detected at
concentrations exceeding regulatory guidelines. VOC concentrations decreased at this location during
the October 2015 monitoring event, however, concentrations of tetrachloroethene and trichloroethene
continued to exceed corresponding regulatory guidelines. No additional compounds were detected at
concentrations exceeding applicable regulatory guidelines.
Appendix C Intra-well Trend Narrative Page 2
MS51B - In May 2014, cis-1,2-dichloroethene, tetrachloroethene, trichloroethene, and vinyl chloride were
detected at concentrations exceeding corresponding regulatory guidelines. The same four compounds
were detected at similar concentrations during the October 2015 monitoring event. No additional
compounds were detected at concentrations exceeding applicable regulatory guidelines.
MW54B - In May 2014, cis-1,2-dichloroethene, tetrachloroethene, trichloroethene, and vinyl chloride were
detected at concentrations exceeding corresponding regulatory guidelines. The same four compounds
were detected at similar concentrations during the October monitoring event. No additional compounds
were detected at concentrations exceeding applicable regulatory guidelines.
MW55B - In May 2014, cis-1,2-dichloroethene and vinyl chloride were detected at concentrations
exceeding corresponding regulatory guidelines. During the October monitoring event, only vinyl chloride
was detected at a concentration exceeding corresponding guidelines. No additional compounds were
detected at concentrations exceeding applicable regulatory guidelines.
MW36B - In May 2014, tetrachloroethene was detected at a concentrations of 36 ug/l, exceeding the
corresponding regulatory guideline. In October 2015, tetrachloroethene was detected at a concentration
of 77 ug/l. No additional compounds were detected at concentrations exceeding applicable regulatory
guidelines.
MW57B1- In May 2014, tetrachloroethene was detected at a concentrations of 55 ug/l, exceeding
corresponding regulatory guidelines. In October 2015, tetrachloroethene was detected at a concentration
of 220 ug/l. Additionally, trichloroethene was also detected in 2015 at a concentration of 4.8 ug/l,
exceeding corresponding regulatory guidelines. No additional compounds were detected at
concentrations exceeding applicable regulatory guidelines.
MW57B2 - No compounds were detected in May 2014 or October 2015 at concentrations exceeding
corresponding regulatory guidelines.
MW58B1 - No compounds were detected in May 2014 or October 2015 at concentrations exceeding
corresponding regulatory guidelines.
MW58B2 - No compounds were detected in May 2014 or October 2015 at concentrations exceeding
corresponding regulatory guidelines.
Metals
IN7B - No metals were detected at concentrations exceeding applicable regulatory guidelines as a result
of the May 2014 or October 2015 monitoring event.
IN1B1 - In May 2014, sampling results identified concentrations of arsenic, barium, iron, and manganese
in monitoring well IN1B1. In October 2015, sampling results reflected in a drop in all observed detections
with the exception of iron. Manganese was the only metal detected at a concentration exceeding
Appendix C Intra-well Trend Narrative Page 3
applicable regulatory guidelines and between 2014 and 2015, manganese concentrations decreased from
3,200 ug/l to 1,990 ug/l. The corresponding MEDEP Residential RAG and reported Project Action Limit
for manganese are 500 ug/l and 200 ug/l, respectively.
IN-1B2 - In May 2014, aluminum, antimony, arsenic, barium, iron, and manganese were detected in well
IN-1B2. Concentrations of Arsenic (17 ug/L) and Manganese (1,900 ug/l) exceeded corresponding
MEDEP Residential RAGs of 10 ug/l and 500 ug/l, respectively. In October 2015, arsenic was not
detected above the MEDEP Residential RAG, however manganese was detected at a concentration of
2,600 ug/l and sodium was detected at a concentration of 23,800 ug/l. The MEDEP Residential RAG and
Project Action Limit for Sodium is 20,000 ug/l.
MW-3B - No metals were detected at concentrations exceeding applicable regulatory guidelines as a
result of the May 2014 or October 2015 monitoring event.
MW-23B - No metals were detected in May 2014 at a concentration exceeding applicable regulatory
guidelines. In October 2015, Sodium was detected at a concentration of 25,700 ug/l, exceeding the
corresponding MEDEP Residential RAG and reported Project Action Limits of 20,000 ug/l.
MS51B - In May 2014, no metals were detected at concentrations greater than corresponding regulatory
guidelines. Barium, iron, and manganese were detected at concentrations of 2.5 ug/l, 2,100 ug/l, and 90
ug/l, respectively. In October 2015, barium was detected at 2.6 ug/l, iron was detected at 8,500 ug/l, and
manganese was detected at 139 ug/l. Additionally, sodium was detected in October 2015 at a
concentration of 41,500 ug/l. These concentrations, although different, do not appear to reflect a
significant trend from the previous year. October 2015 concentrations of iron and sodium both exceeded
corresponding MEDEP Residential RAGs of 5,000 ug/l and 20,000 ug/l, respectively.
MW54B - May 2014 indicated elevated concentrations of iron, manganese and zinc. The manganese
concentration (360 ug/l) exceeded the corresponding MEDEP Residential RAG and reported Project
Action Limits of 500 ug/l and 200 ug/l, respectively. In October 2015, manganese was detected at 252
ug/l, while the concentration of iron increased and the concentration of zinc decreased from May 2014.
MW55B - In May 2014, concentrations of iron and manganese were detected below corresponding
regulatory guidelines. In October 2015, Iron (11,000 ug/l) and sodium (19,100 ug/l) were detected at
concentrations exceeding corresponding MEDEP Residential Rags of 5,000 ug/l and 20,000 ug/l
respectively. Additionally, manganese was detected in October 2015 at a concertation exceeding the
reported Project Action Limit of 200 ug/l, but less than the MEDEP Residential RAG of 500 ug/l.
MW36B1 - In May 2014, Antimony and Arsenic were detected at concentrations of 20.7 ug/l and 28 ug/l
respectively. In October 2015, antimony and arsenic were detected at concentrations of 25.2 ug/l and 26
ug/l, respectively. The MEDEP Residential Rag and reported Project Action Limit for antimony and
arsenic are 3 ug/l and 10 ug/l, respectively. In 2015, sodium (45,900 ug/l) was also detected above
corresponding guidelines.
Appendix C Intra-well Trend Narrative Page 4
MW57B1- Manganese was detected in 2014 at a concentration of 390, exceeding the 200 ug/l MEDEP
Residential RAG and Project Action limit. In October 2015, manganese was detected at a concentration
of 12 ug/l.
MW57B2 - In May 2014, barium, chromium, copper, iron, and lead were detected at this sampling
location. Only chromium (30 ug/l) was detected at a concentration exceeding applicable regulatory
guidelines. In October 2015, two compounds were detected at concentrations exceeding applicable
regulatory guidelines. Chromium was detected at a concentration of 25.3 ug/l, exceeding the Project
Action Limit and MEDEP Residential RAG of 20 ug/l. Cobalt was also detected at a concentration of 11.6
ug/l, exceeding the 10 ug/l Project Action Limit and MEDEP Residential RAG.
MW58B1 - Not metals were detected over corresponding regulatory guidelines in May 2014 or October
2015.
MW58B2 - In May 2014, aluminum (9,300) and arsenic (11 ug/l) concentrations were both over regulatory
guidelines, but the concentration dropped below corresponding action limits (7,000 ug/l and 10 ug/l) in
2015.
November 19, 2015
Project ID: EASTERN SURPLUS
Project Manager: Ms. Diane Paul
Dear Ms. Hewett:
RE: Katahdin Lab Number: SI8365
Please find enclosed the following information:
Sample Receipt Date(s): October 21, 2015
Ms. Rebecca Hewett
Maine DEP
State House Station 17
Augusta,ME 04333
* Report of Analysis (Analytical and/or Field)
* Quality Control Data Summary
* Chain of Custody (COC)
* Login Report
A copy of the Chain of Custody is included in the paginated report. The original COC is attached as an
addendum to this report.
Should you have any questions or comments concerning this Report of Analysis, please do not hesitate to
contact the project manager listed above. The results contained in this report relate only to the submitted
samples. This cover letter is an integral part of the ROA.
We certify that the test results provided in this report meet all the requirements of the NELAC standards unless
otherwise noted in an attached technical narrative or in the Report of Analysis.
We appreciate your continued use of our laboratory and look forward to working with you in the future. The
following signature indicates technical review and acceptance of the data.
Please go to http://www.katahdinlab.com/cert.html for copies of Katahdin Analytical Services Inc. current
certificates and analyte lists.
Sincerely,
KATAHDIN ANALYTICAL SERVICES
__________________________________________ _________________
Authorized Signature Date
11/19/2015
Katahdin Analytical Services 0000001
TECHNICAL NARRATIVE
Organics Analysis The samples of Work Order SI8365 were analyzed in accordance with "Test Methods for Evaluating
Solid Wastes: Physical/Chemical Methods." SW-846, 2nd edition, 1982 (revised 1984), 3rd edition, 1986,
and Updates I, II, IIA, III, IIIA, and IIIB 1996, 1998 & 2004, Office of Solid Waste and Emergency
Response, U.S. EPA, and/or for the specific methods listed below or on the Report of Analysis.
8260B Analysis
Sample SI8365-14 was analyzed within hold time and needed to be reanalyzed diluted in order to bring
the high concentration of tetrachloroethene into the calibration range. Due to laboratory error, the sample
was reanalyzed diluted 11 days out of hold time. The results for both analyses are reported.
The reported percent recovery acceptance limits for the Laboratory Control Samples (LCSs) are
statistically derived for the full list of spiked compounds. The recoveries of the spiked analytes in the
LCS, Matrix Spike (MS) and Matrix Spike Duplicate (MSD) are compared to these acceptance limits.
Katahdin standard operating procedure is to take corrective action only if the number of spiked analytes in
the LCS that are outside of the QC limits is greater than ten percent of the client compound list. If the
associated MS/MSD has greater than the allowable number of exceedances, no corrective action is taken,
as long the LCS is acceptable.
There were no other protocol deviations or observations noted by the organics laboratory staff.
Metals Analysis
On the Report of Analysis for metals for Katahdin Work Order SI8365, the column labeled as “Adjusted
PQL” contains the laboratory standard Practical Quantitation Level, or reporting level, for that parameter
by the method listed, which has been corrected for the amount of sample used, dilution required, and
percent solids (if applicable). In order to meet the client’s reporting levels, the laboratory evaluated data
down to the method detection limit (MDL). For hits that fell between the lab adjusted MDL and the lab
adjusted PQL, a “J” flag has been used to indicate that the value is estimated. For hits that fell below the
adjusted MDL, a “U” qualifier and the adjusted MDL have been entered into the result field. Hits above
the adjusted PQL have been reported without a flag.
Katahdin Analytical Services SI8365 page 0000002 of 0000115
Katahdin Analytical Services SI8365 page 0000003 of 0000115
DM-003 – Revision 6 – 10/15/2014
KATAHDIN ANALYTICAL SERVICES – INORGANIC DATA QUALIFIERS
The sampled date indicated on the attached Report(s) of Analysis (ROA) is the date for which a grab sample was collected or the date for which a composite sample was completed. Beginning and start times for composite samples can be found on the Chain-of-Custody. U Indicates the compound was analyzed for but not detected above the specified level. This level may be the Limit of
Quantitation (LOQ)(previously called Practical Quantitation Level (PQL)), the Limit of Detection (LOD) or Method Detection Limit (MDL) as required by the client.
Note: All results reported as “U” MDL have a 50% rate for false negatives compared to those results reported as “U” PQL/LOQ or “U” LOD, where the rate of false negatives is <1%.
E Estimated value. This flag identifies compounds whose concentrations exceed the upper level of the calibration range of the
instrument for that specific analysis. J Estimated value. The analyte was detected in the sample at a concentration less than the laboratory Limit of Quantitation
(LOQ)(previously called Practical Quantitation Limit (PQL)), but above the Method Detection Limit (MDL). I-7 The laboratory’s Practical Quantitation Level could not be achieved for this parameter due to sample composition, matrix
effects, sample volume, or quantity used for analysis. A-4 Please refer to cover letter or narrative for further information. H_ Please note that the regulatory holding time for _______ is “analyze immediately”. Ideally, this analysis must be performed in
the field at the time of sample collection. _______ for this sample was not performed at the time of sample collection. The analysis was performed as soon as possible after receipt by the laboratory.
H1 - pH H2 - DO H3 - sulfide H4 - residual chlorine T1 The client did not provide the full volume of at least one liter for analysis of TSS. Therefore, the PQL of 2.5 mg/L could not be
achieved. T2 The client provided the required volume of at least one liter for analysis of TSS, but the laboratory could not filter the full one
liter volume due to the sample matrix. Therefore, the PQL of 2.5 mg/L could not be achieved. M1 The matrix spike and/or matrix spike duplicate recovery performed on this sample was outside of the laboratory acceptance
criteria. Sample matrix is suspected. The laboratory criteria was met for the Laboratory Control Sample (LCS) analyzed concurrently with this sample.
M2 The matrix spike and/or matrix spike duplicate recovery was outside of the laboratory acceptance criteria. The native sample
concentration is greater than four times the spike added concentration so the spike added could not be distinguished from the native sample concentration.
R1 The relative percent difference (RPD) between the duplicate analyses performed on this sample was outside of the laboratory
acceptance criteria (when both values are greater than ten times the PQL). MCL Maximum Contaminant Level NL No limit NFL No Free Liquid Present FLP Free Liquid Present NOD No Odor Detected TON Threshold Odor Number D-1 As required by Method 5210B, APHA Standard Methods for the Examination of Water and Wastewater (21
st edition), the BOD
value reported for this sample is ‘qualified’ because the check standard run concurrently with the sample analysis did not meet the criteria specified in the method (198 +/- 30.5 mg/L). These results may not be reportable for compliance purposes.
D-2 The measured final dissolved oxygen concentrations of all dilutions were less than the method-specified limit of 1 mg/L. The
reported BOD result was calculated assuming a final oxygen concentration equal to 1 mg/L. D-3 The dilution water used to prepare this sample did not meet the method and/or regulatory criteria of less than 0.2 or 0.4 mg/L
dissolved oxygen (DO) uptake over the five day period of incubation. These results may not be reportable for compliance purposes.
Katahdin Analytical Services SI8365 page 0000004 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-1
EASTERN SURPLUSESLT-GW-MW51B-1015
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl ChlorideBromomethane
Chloroethane
Trichlorofluoromethane
1,1-DichloroetheneCarbon Disulfide
Freon-113
Methylene Chloride
Acetonetrans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-DichloroetheneBromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-ButanoneBenzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-PentanoneTetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
J
U
U
JB
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.24
0.36
12
0.49
0.55
0.24
0.82
0.25
0.31
1.6
31
0.25
0.36
0.21
190
0.21
0.32
0.22
0.20
58
0.26
0.31
0.20
12
0.25
0.33
0.19
0.27
25
100
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4137.D
Katahdin Analytical Services SI8365 page 0000005 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-1
EASTERN SURPLUSESLT-GW-MW51B-1015
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl AcetateMethylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
4.8
0.30
101.
98.9
122.
113.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4137.D
Katahdin Analytical Services SI8365 page 0000006 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-2
EASTERN SURPLUSESLT-GW-MW54B-1015
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl ChlorideBromomethane
Chloroethane
Trichlorofluoromethane
1,1-DichloroetheneCarbon Disulfide
Freon-113
Methylene Chloride
Acetonetrans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-DichloroetheneBromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
J
U
U
U
J
U
U
JB
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
E
U
U
U
U
U
0.24
2.6
1.4
0.49
0.55
0.24
0.52
0.25
0.31
1.2
2.4
0.25
0.36
0.21
130
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
47
0.25
0.33
0.19
0.27
1.3
3900
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4138.D
Katahdin Analytical Services SI8365 page 0000007 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-2
EASTERN SURPLUSESLT-GW-MW54B-1015
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
104.
104.
123.
116.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4138.D
Katahdin Analytical Services SI8365 page 0000008 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-2DL
EASTERN SURPLUSESLT-GW-MW54B-1015
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene ChlorideAcetone
trans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-DichloroetheneBromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
18-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
JB
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
24
36
25
49
55
24
35
25
31
170
220
25
36
21
110
21
32
22
20
130
26
31
20
28
25
33
19
27
130
3900
20
33
30
22
170
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
200
200
200
200
200
200
100
100
100
500
500
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
500
100
100
100
100
100
500
24.
36.
25.
49.
55.
24.
35.
25.
31.
110
220
25.
36.
21.
21.
21.
32.
22.
20.
130
26.
31.
20.
28.
25.
33.
19.
27.
130
40.
20.
33.
30.
22.
170
Cert No E87604
Report of Analytical Results
Lab File ID: W4163.D
Katahdin Analytical Services SI8365 page 0000009 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-2DL
EASTERN SURPLUSESLT-GW-MW54B-1015
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
18-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
22
21
59
25
23
23
23
38
26
24
15
50
37
27
53
30
104.
100.
127.
118.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
100
100
200
100
100
100
100
100
100
100
100
100
100
100
100
100
22.
21.
59.
25.
23.
23.
23.
38.
26.
24.
15.
50.
37.
27.
53.
30.
Cert No E87604
Report of Analytical Results
Lab File ID: W4163.D
Katahdin Analytical Services SI8365 page 0000010 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-3RA
EASTERN SURPLUSESLT-GW-MW55B-1015
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl ChlorideBromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetonetrans-1,2-DichloroetheneMethyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-DichloroetheneBromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.24
0.36
20
0.49
0.55
0.24
0.35
0.25
0.31
1.1
10
0.77
0.36
0.21
2.7
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
2.8
0.25
0.33
0.19
0.27
1.3
10
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4164.D
Katahdin Analytical Services SI8365 page 0000011 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-3RA
EASTERN SURPLUSESLT-GW-MW55B-1015
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-XyleneStyrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.74
2.4
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
110.
103.
133.
118.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4164.D
Katahdin Analytical Services SI8365 page 0000012 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-4
EASTERN SURPLUSESLT-GW-MW36B1-101
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Dichlorodifluoromethane
ChloromethaneVinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetonetrans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-DichloroetheneBromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
J
U
U
U
U
U
U
U
JB
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.24
1.3
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.3
2.4
0.25
0.36
0.21
3.3
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
3.5
0.25
0.33
0.19
0.27
1.3
77
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4140.D
Katahdin Analytical Services SI8365 page 0000013 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-4
EASTERN SURPLUSESLT-GW-MW36B1-101
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
95.7
104.
116.
114.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4140.D
Katahdin Analytical Services SI8365 page 0000014 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-5
EASTERN SURPLUSESLT-GW-MW57B1-101
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Dichlorodifluoromethane
ChloromethaneVinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene ChlorideAcetone
trans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-DichloroetheneBromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
J
U
U
U
U
U
U
U
JB
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
E
U
U
U
U
U
0.24
1.4
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.4
2.2
0.25
0.36
0.21
5.0
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
4.8
0.25
0.33
0.19
0.27
1.3
240
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4141.D
Katahdin Analytical Services SI8365 page 0000015 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-5
EASTERN SURPLUSESLT-GW-MW57B1-101
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
95.6
105.
121.
114.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4141.D
Katahdin Analytical Services SI8365 page 0000016 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-5DL
EASTERN SURPLUSESLT-GW-MW57B1-101
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetonetrans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-DichloroetheneBromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
18-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
JB
J
U
U
U
J
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
1.2
1.8
1.2
2.4
2.8
1.2
1.8
1.2
1.6
8.7
14
1.2
1.8
1.0
3.4
1.0
1.6
1.1
1.0
6.6
1.3
1.6
1.0
4.4
1.2
1.6
0.95
1.4
6.6
220
1.0
1.6
1.5
1.1
8.5
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
10.
10.
10.
10.
10.
10.
5.0
5.0
5.0
25.
25.
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
25.
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
25.
5.0
5.0
5.0
5.0
5.0
25.
1.2
1.8
1.2
2.4
2.8
1.2
1.8
1.2
1.6
5.6
11.
1.2
1.8
1.0
1.0
1.0
1.6
1.1
1.0
6.6
1.3
1.6
1.0
1.4
1.2
1.6
0.95
1.4
6.6
2.0
1.0
1.6
1.5
1.1
8.5
Cert No E87604
Report of Analytical Results
Lab File ID: W4165.D
Katahdin Analytical Services SI8365 page 0000017 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-5DL
EASTERN SURPLUSESLT-GW-MW57B1-101
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
18-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.1
1.0
3.0
1.2
1.2
1.2
1.2
1.9
1.3
1.2
0.75
2.5
1.8
1.4
2.6
1.5
105.
102.
126.
110.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
5.0
5.0
10.
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
1.1
1.0
3.0
1.2
1.2
1.2
1.2
1.9
1.3
1.2
0.75
2.5
1.8
1.4
2.6
1.5
Cert No E87604
Report of Analytical Results
Lab File ID: W4165.D
Katahdin Analytical Services SI8365 page 0000018 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-6RA
EASTERN SURPLUSESLT-GW-MW57B2-101
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Dichlorodifluoromethane
ChloromethaneVinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetonetrans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Bromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
J
U
U
U
U
U
U
U
JB
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
0.24
1.9
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.3
93
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.49
0.25
0.33
0.19
1.8
1.3
9.7
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4166.D
Katahdin Analytical Services SI8365 page 0000019 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-6RA
EASTERN SURPLUSESLT-GW-MW57B2-101
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
110.
106.
129.
115.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4166.D
Katahdin Analytical Services SI8365 page 0000020 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-7
EASTERN SURPLUSESLT-GW-IN1B1-1015
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl ChlorideBromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetonetrans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-DichloroetheneBromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
J
J
U
U
U
U
U
U
JB
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
E
U
U
U
U
U
0.24
1.2
0.27
0.49
0.55
0.24
0.35
0.25
0.31
1.3
3.1
0.25
0.36
0.21
3.1
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
5.6
0.25
0.33
0.19
0.27
1.3
650
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4143.D
Katahdin Analytical Services SI8365 page 0000021 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-7
EASTERN SURPLUSESLT-GW-IN1B1-1015
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
94.3
99.7
112.
111.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4143.D
Katahdin Analytical Services SI8365 page 0000022 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-7DL
EASTERN SURPLUSESLT-GW-IN1B1-1015
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetonetrans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Bromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
18-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
JB
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
2.4
3.6
2.5
4.9
5.5
2.4
3.5
2.5
3.1
19
33
2.5
3.6
2.1
2.1
2.1
3.2
2.2
2.0
13
2.6
3.1
2.0
2.8
2.5
3.3
1.9
2.7
13
600
2.0
3.3
3.0
2.2
17
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
20.
20.
20.
20.
20.
20.
10.
10.
10.
50.
50.
10.
10.
10.
10.
10.
10.
10.
10.
50.
10.
10.
10.
10.
10.
10.
10.
10.
50.
10.
10.
10.
10.
10.
50.
2.4
3.6
2.5
4.9
5.5
2.4
3.5
2.5
3.1
11.
22.
2.5
3.6
2.1
2.1
2.1
3.2
2.2
2.0
13.
2.6
3.1
2.0
2.8
2.5
3.3
1.9
2.7
13.
4.0
2.0
3.3
3.0
2.2
17.
Cert No E87604
Report of Analytical Results
Lab File ID: W4167.D
Katahdin Analytical Services SI8365 page 0000023 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-7DL
EASTERN SURPLUSESLT-GW-IN1B1-1015
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
18-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
2.2
2.1
5.9
2.5
2.3
2.3
2.3
3.8
2.6
2.4
1.5
5.0
3.7
2.7
5.3
3.0
106.
101.
125.
115.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
10.
10.
20.
10.
10.
10.
10.
10.
10.
10.
10.
10.
10.
10.
10.
10.
2.2
2.1
5.9
2.5
2.3
2.3
2.3
3.8
2.6
2.4
1.5
5.0
3.7
2.7
5.3
3.0
Cert No E87604
Report of Analytical Results
Lab File ID: W4167.D
Katahdin Analytical Services SI8365 page 0000024 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-8RA
EASTERN SURPLUSESLT-GW-IN1B2-1015
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl ChlorideBromomethane
ChloroethaneTrichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene ChlorideAcetone
trans-1,2-DichloroetheneMethyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-DichloroetheneBromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
JB
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.24
0.36
2.2
0.49
4.7
0.24
0.35
0.25
0.31
1.5
2.2
0.41
0.36
0.21
8.1
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
12
0.25
0.33
0.19
0.27
1.3
31
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4168.D
Katahdin Analytical Services SI8365 page 0000025 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-8RA
EASTERN SURPLUSESLT-GW-IN1B2-1015
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
106.
100.
131.
116.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4168.D
Katahdin Analytical Services SI8365 page 0000026 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-9
EASTERN SURPLUSESLT-GW-MW23B-1015
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Dichlorodifluoromethane
ChloromethaneVinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene ChlorideAcetone
trans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-DichloroetheneBromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
JB
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.24
2.3
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.3
2.2
0.25
0.36
0.21
14
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
5.5
0.25
0.33
0.19
0.27
1.3
140
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4145.D
Katahdin Analytical Services SI8365 page 0000027 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-9
EASTERN SURPLUSESLT-GW-MW23B-1015
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
96.9
102.
120.
115.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4145.D
Katahdin Analytical Services SI8365 page 0000028 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-10
EASTERN SURPLUSESLT-GW-IN7B-1015
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Dichlorodifluoromethane
ChloromethaneVinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetonetrans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-DichloroetheneBromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
J
U
U
U
U
U
U
U
JB
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.24
1.6
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.4
2.6
0.25
0.36
0.21
6.3
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
3.3
0.25
0.33
0.19
0.27
1.3
190
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4146.D
Katahdin Analytical Services SI8365 page 0000029 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-10
EASTERN SURPLUSESLT-GW-IN7B-1015
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
96.3
102.
117.
116.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4146.D
Katahdin Analytical Services SI8365 page 0000030 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-11
EASTERN SURPLUSESLT-GW-MW3B-1015
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Dichlorodifluoromethane
ChloromethaneVinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene ChlorideAcetone
trans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Bromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
J
U
U
U
U
U
U
U
JB
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.24
1.4
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.3
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4147.D
Katahdin Analytical Services SI8365 page 0000031 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-11
EASTERN SURPLUSESLT-GW-MW3B-1015
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
118.
112.
129.
118.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4147.D
Katahdin Analytical Services SI8365 page 0000032 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-12
EASTERN SURPLUSESLT-GW-MW58B1-101
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Dichlorodifluoromethane
ChloromethaneVinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetonetrans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-DichloroetheneBromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
JB
J
U
U
U
J
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
0.24
2.3
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.2
2.5
0.25
0.36
0.21
0.32
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.69
0.25
0.33
0.19
0.27
1.3
18
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4148.D
Katahdin Analytical Services SI8365 page 0000033 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-12
EASTERN SURPLUSESLT-GW-MW58B1-101
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
98.6
104.
120.
114.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4148.D
Katahdin Analytical Services SI8365 page 0000034 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-13
EASTERN SURPLUSESLT-GW-MW58B2-101
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Dichlorodifluoromethane
ChloromethaneVinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene ChlorideAcetone
trans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Bromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
J
U
U
U
U
U
U
U
JB
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.24
0.86
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.4
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4149.D
Katahdin Analytical Services SI8365 page 0000035 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-13
EASTERN SURPLUSESLT-GW-MW58B2-101
SI8365
20-OCT-1521-OCT-15
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
99.2
104.
120.
115.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4149.D
Katahdin Analytical Services SI8365 page 0000036 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-14
EASTERN SURPLUSESLT-GW-MWRP-1015
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetonetrans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-DichloroetheneBromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
E
U
U
U
U
U
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.8
0.25
0.36
0.21
2.8
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
5.6
0.25
0.33
0.19
0.27
1.3
710
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4175.D
Katahdin Analytical Services SI8365 page 0000037 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-14
EASTERN SURPLUSESLT-GW-MWRP-1015
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
108.
102.
133.
117.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4175.D
Katahdin Analytical Services SI8365 page 0000038 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-14DL
EASTERN SURPLUSESLT-GW-MWRP-1015
SI8365
20-OCT-1521-OCT-15
14-NOV-15AAB
SW846 8260B
14-NOV-15
WG174238
AQNA
AABSW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetone
trans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Bromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethenetrans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
4.8
7.2
5.0
9.8
11
4.8
7.0
5.0
6.2
23
44
5.0
7.2
4.2
4.2
4.2
6.4
4.4
4.0
26
5.2
6.2
4.0
5.6
5.0
6.6
3.8
5.4
26
500
4.0
6.6
6.0
4.4
34
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
40.
40.
40.
40.
40.
40.
20.
20.
20.
100
100
20.
20.
20.
20.
20.
20.
20.
20.
100
20.
20.
20.
20.
20.
20.
20.
20.
100
20.
20.
20.
20.
20.
100
4.8
7.2
5.0
9.8
11.
4.8
7.0
5.0
6.2
23.
44.
5.0
7.2
4.2
4.2
4.2
6.4
4.4
4.0
26.
5.2
6.2
4.0
5.6
5.0
6.6
3.8
5.4
26.
8.0
4.0
6.6
6.0
4.4
34.
Cert No E87604
Report of Analytical Results
Lab File ID: T5380.D
Katahdin Analytical Services SI8365 page 0000039 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-14DL
EASTERN SURPLUSESLT-GW-MWRP-1015
SI8365
20-OCT-1521-OCT-15
14-NOV-15AAB
SW846 8260B
14-NOV-15
WG174238
AQNA
AABSW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
4.4
4.2
12
5.0
4.6
4.6
4.6
7.6
5.2
4.8
3.0
10
7.4
5.4
11
6.0
103.
101.
117.
109.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
20.
20.
40.
20.
20.
20.
20.
20.
20.
20.
20.
20.
20.
20.
20.
20.
4.4
4.2
12.
5.0
4.6
4.6
4.6
7.6
5.2
4.8
3.0
10.
7.4
5.4
11.
6.0
Cert No E87604
Report of Analytical Results
Lab File ID: T5380.D
Katahdin Analytical Services SI8365 page 0000040 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-16
EASTERN SURPLUSESLT-TB-1015
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetonetrans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Bromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
JB
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.4
6.3
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4162.D
Katahdin Analytical Services SI8365 page 0000041 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-16
EASTERN SURPLUSESLT-TB-1015
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-XyleneStyrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
J
J
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.26
0.77
2.4
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
107.
103.
135.
119.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4162.D
Katahdin Analytical Services SI8365 page 0000042 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
Maine DEPSI8365-17
EASTERN SURPLUSESLT-GWLORD-1015
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetonetrans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Bromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
JB
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.3
3.5
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
5
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
1.7
Cert No E87604
Report of Analytical Results
Lab File ID: W4176.D
Katahdin Analytical Services SI8365 page 0000043 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
Maine DEPSI8365-17
EASTERN SURPLUSESLT-GWLORD-1015
SI8365
20-OCT-1521-OCT-15
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
110.
104.
135.
119.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4176.D
Katahdin Analytical Services SI8365 page 0000044 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://[email protected]
Cert No E87604
Form 4 Method Blank Summary
Lab Name : Katahdin Analytical Services SDG : SI8365
Lab File ID : T5377.DLab Sample ID : WG174238-2
This Method Blank applies to the following samples, LCS, MS and MSD:
09:21Time Analyzed :14-NOV-15Date Analyzed :
Instrument ID : GCMS-THeated Purge : No
WG174238-1SI8365-14DL
Laboratory Control SESLT-GW-MWRP-1015
T5374.DT5380.D
11/14/1511/14/15
07:2311:04
Project : EASTERN SURPLUS
Client Sample ID Lab Sample ID Lab File ID Date Analyzed Time Analyzed
- VOA
Katahdin Analytical Services SI8365 page 0000045 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
WG174238-2Method Blank Sample
SI8365
14-NOV-15AAB
SW846 8260B
14-NOV-15
WG174238
AQNA
AABSW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetone
trans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Bromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
Cert No E87604
Report of Analytical Results
Lab File ID: T5377.D
Katahdin Analytical Services SI8365 page 0000046 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
WG174238-2Method Blank Sample
SI8365
14-NOV-15AAB
SW846 8260B
14-NOV-15
WG174238
AQNA
AABSW846 5030
2-Hexanone
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.7
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
100.
100.
110.
109.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
5
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
5.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.7
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: T5377.D
Katahdin Analytical Services SI8365 page 0000047 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
WG174238-1LCS
SI8365
14-NOV-15AAB
SW846 8260B
14-NOV-15
WG174238
AQNA
AABSW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetone
trans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Bromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Recovery (%) Conc Added Conc Recovered Conc Units
* 27.8
* 52.2
68.8
76.8
80.4
85.6
96.8
81.2
96.0
93.6
94.4
106.
104.
105.
99.6
102.
101.
* 82.2
97.8
101.
104.
89.8
97.6
110.
101.
107.
97.6
104.
108.
96.0
103.
102.
95.2
110.
102.
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
100.
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
13.9
26.1
34.4
38.4
40.2
42.8
48.4
40.6
48.0
46.8
47.2
52.9
104.
52.4
49.8
51.1
50.3
41.1
48.9
50.5
51.9
44.9
48.8
55.1
50.4
53.7
48.8
51.9
53.9
48.0
51.4
50.9
47.6
54.8
51.0
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Cert No E87604
LCS Recovery Report
Limits
29-164
59-123
64-131
57-135
53-157
70-149
88-127
71-129
73-126
72-129
62-172
78-125
81-125
76-130
85-123
85-117
78-128
87-126
77-129
71-132
86-116
71-133
81-125
79-121
84-118
85-122
83-119
84-118
83-122
47-155
85-135
84-115
85-119
84-116
80-124
T5374.DLCS File ID:
Katahdin Analytical Services SI8365 page 0000048 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
WG174238-1LCS
SI8365
14-NOV-15AAB
SW846 8260B
14-NOV-15
WG174238
AQNA
AABSW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Recovery (%) Conc Added Conc Recovered Conc Units
104.
109.
110.
108.
105.
99.8
115.
101.
103.
100.
107.
100.
108.
111.
98.0
98.4
100.
100.
98.0
100.
50.0
50.0
100.
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
52.2
54.3
110.
53.9
52.7
49.9
57.7
50.6
51.5
50.0
53.4
50.0
53.9
55.5
49.0
49.2
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Cert No E87604
LCS Recovery Report
Limits
89-113
88-113
88-116
90-116
88-117
86-117
96-136
79-121
86-110
86-111
86-112
67-124
76-126
70-122
70-132
73-125
56-133
65-128
67-135
68-128
T5374.DLCS File ID:
Katahdin Analytical Services SI8365 page 0000049 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://[email protected]
Cert No E87604
Form 4 Method Blank Summary
Lab Name : Katahdin Analytical Services SDG : SI8365
Lab File ID : W4136.DLab Sample ID : WG172846-2
This Method Blank applies to the following samples, LCS, MS and MSD:
11:24Time Analyzed :23-OCT-15Date Analyzed :
Instrument ID : GCMS-WHeated Purge : No
WG172846-1SI8365-1SI8365-2SI8365-4SI8365-5SI8365-7SI8365-9SI8365-10SI8365-11SI8365-12SI8365-13WG172846-5WG172846-6
Laboratory Control SESLT-GW-MW51B-1015ESLT-GW-MW54B-1015ESLT-GW-MW36B1-1015ESLT-GW-MW57B1-1015ESLT-GW-IN1B1-1015ESLT-GW-MW23B-1015ESLT-GW-IN7B-1015ESLT-GW-MW3B-1015ESLT-GW-MW58B1-1015ESLT-GW-MW58B2-1015Matrix SpikeMatrix Spike Duplica
W4134.DW4137.DW4138.DW4140.DW4141.DW4143.DW4145.DW4146.DW4147.DW4148.DW4149.DW4150.DW4151.D
10/23/1510/23/1510/23/1510/23/1510/23/1510/23/1510/23/1510/23/1510/23/1510/23/1510/23/1510/23/1510/23/15
10:1012:1912:5113:5414:2515:2816:3117:0317:3418:0618:3719:0919:40
Project : EASTERN SURPLUS
Client Sample ID Lab Sample ID Lab File ID Date Analyzed Time Analyzed
- VOA
Katahdin Analytical Services SI8365 page 0000050 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
WG172846-2Method Blank Sample
SI8365
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetone
trans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Bromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
3.3
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
Cert No E87604
Report of Analytical Results
Lab File ID: W4136.D
Katahdin Analytical Services SI8365 page 0000051 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
WG172846-2Method Blank Sample
SI8365
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
2-Hexanone
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.7
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
97.5
99.4
122.
115.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
5
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
5.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.7
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4136.D
Katahdin Analytical Services SI8365 page 0000052 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
WG172846-1LCS
SI8365
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetone
trans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Bromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Recovery (%) Conc Added Conc Recovered Conc Units
74.8
94.0
98.6
103.
108.
119.
101.
102.
106.
96.2
117.
106.
105.
103.
91.4
96.6
105.
110.
105.
117.
96.8
101.
98.8
101.
92.0
103.
107.
97.6
* 122.
95.6
101.
96.4
106.
106.
118.
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
100.
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
37.4
47.0
49.3
51.4
54.2
59.3
50.4
51.0
52.8
48.1
58.5
52.8
105.
51.4
45.7
48.3
52.7
55.1
52.7
58.4
48.4
50.7
49.4
50.4
46.0
51.7
53.5
48.8
60.8
47.8
50.4
48.2
53.2
53.1
58.8
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Cert No E87604
LCS Recovery Report
Limits
29-164
59-123
64-131
57-135
53-157
70-149
88-127
71-129
73-126
72-129
62-172
78-125
81-125
76-130
85-123
85-117
78-128
87-126
77-129
71-132
86-116
71-133
81-125
79-121
84-118
85-122
83-119
84-118
83-122
47-155
85-135
84-115
85-119
84-116
80-124
W4134.DLCS File ID:
Katahdin Analytical Services SI8365 page 0000053 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
WG172846-1LCS
SI8365
23-OCT-15EME
SW846 8260B
23-OCT-15
WG172846
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Recovery (%) Conc Added Conc Recovered Conc Units
97.2
103.
102.
96.2
93.4
112.
113.
98.4
98.8
97.8
103.
107.
100.
108.
98.0
102.
102.
100.
109.
104.
50.0
50.0
100.
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
48.6
51.3
102.
48.1
46.7
55.8
56.3
49.2
49.4
48.9
51.3
53.3
50.0
54.2
49.0
51.2
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Cert No E87604
LCS Recovery Report
Limits
89-113
88-113
88-116
90-116
88-117
86-117
96-136
79-121
86-110
86-111
86-112
67-124
76-126
70-122
70-132
73-125
56-133
65-128
67-135
68-128
W4134.DLCS File ID:
Katahdin Analytical Services SI8365 page 0000054 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://[email protected]
Cert No E87604
Form 4 Method Blank Summary
Lab Name : Katahdin Analytical Services SDG : SI8365
Lab File ID : W4161.DLab Sample ID : WG172905-2
This Method Blank applies to the following samples, LCS, MS and MSD:
13:49Time Analyzed :24-OCT-15Date Analyzed :
Instrument ID : GCMS-WHeated Purge : No
WG172905-1SI8365-16SI8365-2DLSI8365-3RASI8365-5DLSI8365-6RASI8365-7DLSI8365-8RASI8365-14SI8365-17
Laboratory Control SESLT-TB-1015ESLT-GW-MW54B-1015ESLT-GW-MW55B-1015ESLT-GW-MW57B1-1015ESLT-GW-MW57B2-1015ESLT-GW-IN1B1-1015ESLT-GW-IN1B2-1015ESLT-GW-MWRP-1015ESLT-GWLORD-1015
W4158.DW4162.DW4163.DW4164.DW4165.DW4166.DW4167.DW4168.DW4175.DW4176.D
10/24/1510/24/1510/24/1510/24/1510/24/1510/24/1510/24/1510/24/1510/24/1510/24/15
11:5414:2014:5215:2315:5516:2716:5817:2921:1021:42
Project : EASTERN SURPLUS
Client Sample ID Lab Sample ID Lab File ID Date Analyzed Time Analyzed
- VOA
Katahdin Analytical Services SI8365 page 0000055 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
WG172905-2Method Blank Sample
SI8365
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetone
trans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Bromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.9
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
1
1
1
5
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
1
1
1
5
1
1
1
1
1
2.0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
0.24
0.36
0.25
0.49
0.55
0.24
0.35
0.25
0.31
1.1
2.2
0.25
0.36
0.21
0.21
0.21
0.32
0.22
0.20
1.3
0.26
0.31
0.20
0.28
0.25
0.33
0.19
0.27
1.3
0.40
0.20
0.33
0.30
0.22
Cert No E87604
Report of Analytical Results
Lab File ID: W4161.D
Katahdin Analytical Services SI8365 page 0000056 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
WG172905-2Method Blank Sample
SI8365
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
2-Hexanone
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.7
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
103.
104.
125.
115.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
5
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
5.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.7
0.22
0.21
0.59
0.25
0.23
0.23
0.23
0.38
0.26
0.24
0.15
0.50
0.37
0.27
0.53
0.30
Cert No E87604
Report of Analytical Results
Lab File ID: W4161.D
Katahdin Analytical Services SI8365 page 0000057 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
WG172905-1LCS
SI8365
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetone
trans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Bromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
1,2-Dibromoethane
2-Hexanone
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Recovery (%) Conc Added Conc Recovered Conc Units
58.0
87.4
87.4
95.8
89.8
97.6
88.8
89.6
91.2
90.8
91.2
93.6
96.7
96.0
* 82.8
89.8
96.6
92.6
91.0
114.
92.8
88.0
93.4
93.4
92.2
98.4
103.
91.8
* 122.
93.6
92.2
94.2
98.6
94.8
116.
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
100.
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
29.0
43.7
43.7
47.9
44.9
48.8
44.4
44.8
45.6
45.4
45.6
46.8
96.7
48.0
41.4
44.9
48.3
46.3
45.5
56.8
46.4
44.0
46.7
46.7
46.1
49.2
51.3
45.9
61.1
46.8
46.1
47.1
49.3
47.4
58.2
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Cert No E87604
LCS Recovery Report
Limits
29-164
59-123
64-131
57-135
53-157
70-149
88-127
71-129
73-126
72-129
62-172
78-125
81-125
76-130
85-123
85-117
78-128
87-126
77-129
71-132
86-116
71-133
81-125
79-121
84-118
85-122
83-119
84-118
83-122
47-155
85-135
84-115
85-119
84-116
80-124
W4158.DLCS File ID:
Katahdin Analytical Services SI8365 page 0000058 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
WG172905-1LCS
SI8365
24-OCT-15EME
SW846 8260B
24-OCT-15
WG172905
AQNA
EMESW846 5030
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-Bromofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
Dibromofluoromethane
17-NOV-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Recovery (%) Conc Added Conc Recovered Conc Units
89.4
94.4
92.8
* 87.8
* 85.4
98.8
100.
93.4
89.4
89.6
94.0
96.8
93.6
108.
99.6
92.2
101.
100.
103.
101.
50.0
50.0
100.
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
44.7
47.2
92.8
43.9
42.7
49.4
50.0
46.7
44.7
44.8
47.0
48.4
46.8
54.1
49.8
46.1
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Cert No E87604
LCS Recovery Report
Limits
89-113
88-113
88-116
90-116
88-117
86-117
96-136
79-121
86-110
86-111
86-112
67-124
76-126
70-122
70-132
73-125
56-133
65-128
67-135
68-128
W4158.DLCS File ID:
Katahdin Analytical Services SI8365 page 0000059 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 2
WG172846-5
SI8365
23-OCT-15 EMESW846 8260B
23-OCT-15
WG172846AQ
NA
EMESW846 5030
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Carbon Disulfide
Freon-113
Methylene Chloride
Acetone
trans-1,2-Dichloroethene
Methyl tert-butyl Ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Bromochloromethane
Chloroform
Carbon Tetrachloride
1,1,1-Trichloroethane
2-Butanone
Benzene
Cyclohexane
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
Toluene
4-Methyl-2-Pentanone
Tetrachloroethene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Dibromochloromethane
17-NOV-15Project:
Extraction Method:Analysis Method:
Report Date:
MS ID: Received Date:
Extracted By:Analyst:
Matrix:
SDG:
Extract Date: Analysis Date:
Lab Prep Batch: % Solids:
CompoundMS Rec
(%)MS
SpikeMS
Conc
80.0
114.
114.
95.2
117.
136.
94.6
92.0
95.8
89.6
100.
95.2
102.
102.
83.4*
95.4
107.
109.
107.
140.*
117.*
96.8
109.
116.
121.*
117.
118.
114.
147.*
64.0
114.
122.*
114.
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
100.
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
40.0
58.8
57.2
47.6
58.5
68.0
47.3
46.0
47.9
46.2
52.6
47.6
102.
50.9
48.0
47.7
53.5
54.4
53.5
70.2
58.7
48.4
54.5
61.3
60.3
58.5
58.9
56.9
73.6
218.
57.1
61.2
57.0
Cert No E87604
MS/MSD Recovery Report
Limits
MSD ID:
Conc Units
MSD Rec(%)
MSDConc RPD (%)
RPD Limit
77.0
122.
119.
102.
100.
116.
103.
105.
100.
94.0
107.
105.
93.0
115.
100.
106.
107.
97.0
95.8
133.*
106.
122.
92.2
104.
107.
99.2
102.
102.
131.*
72.0
97.2
104.
98.8
38.5
62.6
59.3
51.2
50.2
58.0
51.7
52.7
50.2
48.4
56.3
52.5
93.0
57.5
56.5
52.8
53.6
48.5
47.9
66.3
52.8
60.8
46.1
55.2
53.3
49.6
51.2
51.2
65.6
222.
48.6
52.0
49.4
4
6
4
7
15
16
9
14
5
5
7
10
9
12
16
10
0
11
11
6
10
23*
17
10
12
16
14
10
11
2
16
16
14
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
29-164
59-123
64-131
57-135
53-157
70-149
88-127
71-129
73-126
72-129
62-172
78-125
81-125
76-130
85-123
85-117
78-128
87-126
77-129
71-132
86-116
71-133
81-125
79-121
84-118
85-122
83-119
84-118
83-122
47-155
85-135
84-115
85-119
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
WG172846-6
U0.24
J1.6
U0.25
U0.49
U0.55
U0.24
U0.35
U0.25
U0.31
JB1.4
J2.6
U0.25
U0.36
U0.21
6.3
U0.21
U0.32
U0.22
U0.20
U1.3
U0.26
U0.31
U0.20
3.3
U0.25
U0.33
U0.19
U0.27
U1.3
190
U0.20
U0.33
U0.30
SampConc
MSD Spike
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
100.
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
Sample ID: SI8365-10Client ID: ESLT-GW-IN7B-1015
W4150.DMS File ID: W4151.DMSD File ID:
Katahdin Analytical Services SI8365 page 0000060 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of2 2
WG172846-5
SI8365
23-OCT-15 EMESW846 8260B
23-OCT-15
WG172846AQ
NA
EMESW846 5030
1,2-Dibromoethane
2-Hexanone
Chlorobenzene
Ethylbenzene
m+p-Xylenes
o-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Methyl Acetate
Methylcyclohexane
P-BromofluorobenzeneToluene-d81,2-Dichloroethane-d4Dibromofluoromethane
17-NOV-15Project:
Extraction Method:Analysis Method:
Report Date:
MS ID: Received Date:
Extracted By:Analyst:
Matrix:
SDG:
Extract Date: Analysis Date:
Lab Prep Batch: % Solids:
CompoundMS Rec
(%)MS
SpikeMS
Conc
117.*
132.*
107.
114.*
110.
106.
102.
116.
123.
125.*
107.
107.
116.*
118.
107.
119.
83.4
121.
50.0
50.0
50.0
50.0
100.
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
58.7
65.8
53.4
57.0
110.
53.2
51.1
58.2
61.3
62.3
53.4
53.4
57.9
59.2
53.4
59.5
41.7
60.7
102.101.107.94.9
Cert No E87604
MS/MSD Recovery Report
Limits
MSD ID:
Conc Units
MSD Rec(%)
MSDConc RPD (%)
RPD Limit
100.
123.
98.0
103.
100.
95.4
91.0
97.6
111.
111.
96.8
96.2
102.
102.
97.4
107.
85.2
118.
50.2
61.7
49.0
51.3
100.
47.7
45.5
48.8
55.6
55.5
48.4
48.1
51.0
51.2
48.7
53.4
42.6
59.1
16
6
8
10
10
11
12
18
10
12
10
10
13
14
9
11
2
3
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
84-116
80-124
89-113
88-113
88-116
90-116
88-117
86-117
96-136
79-121
86-110
86-111
86-112
67-124
76-126
70-122
70-132
73-125
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
98.4104.103.101.
WG172846-6
56-13365-12867-13568-128
U0.22
U1.7
U0.22
U0.21
U0.59
U0.25
U0.23
U0.23
U0.23
U0.38
U0.26
U0.24
U0.15
U0.50
U0.37
U0.27
U0.53
U0.30
SampConc
MSD Spike
50.0
50.0
50.0
50.0
100.
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
Sample ID: SI8365-10Client ID: ESLT-GW-IN7B-1015
W4150.DMS File ID: W4151.DMSD File ID:
Katahdin Analytical Services SI8365 page 0000061 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-1
EASTERN SURPLUSESLT-GW-MW51B-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
MethaneEthane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
E 5300
16.
23.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2072.D
Katahdin Analytical Services SI8365 page 0000062 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-1DL
EASTERN SURPLUSESLT-GW-MW51B-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
MethaneEthane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
U
6800
100
100
ug/L
ug/L
ug/L
10
10
10
10
10
10
100
100
100
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2088.D
Katahdin Analytical Services SI8365 page 0000063 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-2
EASTERN SURPLUSESLT-GW-MW54B-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
Methane
Ethane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
U
U
10.
10.
10.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2073.D
Katahdin Analytical Services SI8365 page 0000064 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-3
EASTERN SURPLUSESLT-GW-MW55B-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
MethaneEthane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
E
U
6000
10.
1000
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2074.D
Katahdin Analytical Services SI8365 page 0000065 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-3DL
EASTERN SURPLUSESLT-GW-MW55B-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
MethaneEthane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
4800
100
870
ug/L
ug/L
ug/L
10
10
10
10
10
10
100
100
100
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2089.D
Katahdin Analytical Services SI8365 page 0000066 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-4
EASTERN SURPLUSESLT-GW-MW36B1-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
Methane
Ethane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
U
U
10.
10.
10.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2075.D
Katahdin Analytical Services SI8365 page 0000067 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-5
EASTERN SURPLUSESLT-GW-MW57B1-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
Methane
Ethane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
U
U
10.
10.
10.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2076.D
Katahdin Analytical Services SI8365 page 0000068 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-6
EASTERN SURPLUSESLT-GW-MW57B2-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
MethaneEthane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
26.
10.
25.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2077.D
Katahdin Analytical Services SI8365 page 0000069 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-7
EASTERN SURPLUSESLT-GW-IN1B1-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
Methane
Ethane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
U
U
10.
10.
10.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2078.D
Katahdin Analytical Services SI8365 page 0000070 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-8
EASTERN SURPLUSESLT-GW-IN1B2-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
MethaneEthane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
44.
10.
24.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2079.D
Katahdin Analytical Services SI8365 page 0000071 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-9
EASTERN SURPLUSESLT-GW-MW23B-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
Methane
Ethane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
U
U
10.
10.
10.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2080.D
Katahdin Analytical Services SI8365 page 0000072 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-10
EASTERN SURPLUSESLT-GW-IN7B-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
Methane
Ethane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
U
U
10.
10.
10.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2081.D
Katahdin Analytical Services SI8365 page 0000073 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-11
EASTERN SURPLUSESLT-GW-MW3B-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
Methane
Ethane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
U
U
10.
10.
10.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2082.D
Katahdin Analytical Services SI8365 page 0000074 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-12
EASTERN SURPLUSESLT-GW-MW58B1-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
Methane
Ethane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
U
U
10.
10.
10.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2083.D
Katahdin Analytical Services SI8365 page 0000075 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-13
EASTERN SURPLUSESLT-GW-MW58B2-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
Methane
Ethane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
U
U
10.
10.
10.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2084.D
Katahdin Analytical Services SI8365 page 0000076 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-14
EASTERN SURPLUSESLT-GW-MWRP-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
Methane
Ethane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
U
U
10.
10.
10.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2085.D
Katahdin Analytical Services SI8365 page 0000077 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
Maine DEPSI8365-16
EASTERN SURPLUSESLT-TB-1015
SI8365
20-OCT-1521-OCT-15
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
Methane
Ethane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
U
U
10.
10.
10.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2069.D
Katahdin Analytical Services SI8365 page 0000078 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://[email protected]
Cert No E87604
Form 4 Method Blank Summary
Lab Name : Katahdin Analytical Services SDG : SI8365
Lab File ID : 5IJ2067.DLab Sample ID : WG173026-1
This Method Blank applies to the following samples, LCS, MS and MSD:
11:48Time Analyzed :28-OCT-15Date Analyzed :
Instrument ID : GC05Heated Purge : No
WG173026-2SI8365-16WG173026-4SI8365-1SI8365-2SI8365-3SI8365-4SI8365-5SI8365-6SI8365-7SI8365-8SI8365-9SI8365-10SI8365-11SI8365-12SI8365-13SI8365-14WG173026-3RASI8365-1DLSI8365-3DL
Laboratory Control SESLT-TB-1015Matrix Spike DuplicaESLT-GW-MW51B-1015ESLT-GW-MW54B-1015ESLT-GW-MW55B-1015ESLT-GW-MW36B1-1015ESLT-GW-MW57B1-1015ESLT-GW-MW57B2-1015ESLT-GW-IN1B1-1015ESLT-GW-IN1B2-1015ESLT-GW-MW23B-1015ESLT-GW-IN7B-1015ESLT-GW-MW3B-1015ESLT-GW-MW58B1-1015ESLT-GW-MW58B2-1015ESLT-GW-MWRP-1015Matrix SpikeESLT-GW-MW51B-1015ESLT-GW-MW55B-1015
5IJ2068.D5IJ2069.D5IJ2071.D5IJ2072.D5IJ2073.D5IJ2074.D5IJ2075.D5IJ2076.D5IJ2077.D5IJ2078.D5IJ2079.D5IJ2080.D5IJ2081.D5IJ2082.D5IJ2083.D5IJ2084.D5IJ2085.D5IJ2086.D5IJ2088.D5IJ2089.D
10/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/15
12:0512:2212:5613:1413:3113:4814:0514:2214:4615:0315:2015:3715:5416:1116:2816:4617:0317:2017:5418:11
Project : EASTERN SURPLUS
Client Sample ID Lab Sample ID Lab File ID Date Analyzed Time Analyzed
- VOA
Katahdin Analytical Services SI8365 page 0000079 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
WG173026-1Method Blank Sample
SI8365
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
Methane
Ethane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Qualifier Result Units Dilution PQL ADJ PQL
U
U
U
10.
10.
10.
ug/L
ug/L
ug/L
1
1
1
10
10
10
10.
10.
10.
Cert No E87604
Report of Analytical Results
Lab File ID: 5IJ2067.D
Katahdin Analytical Services SI8365 page 0000080 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
WG173026-2LCS
SI8365
28-OCT-15JMS
RSK SOP 175
28-OCT-15
WG173026
AQNA
JMSRSK SOP 175
Methane
Ethane
Ethene
29-OCT-15
Client:
Project:
Sample Date:
Extraction Method:
Analysis Method:
Report Date:
Lab ID: Received Date:
Extracted By:
Analyst:
Matrix: Client ID:
SDG:
Extract Date:
Analysis Date:
Lab Prep Batch:% Solids:
Compound Recovery (%) Conc Added Conc Recovered Conc Units
115.
114.
118.
133.
249.
233.
153.
283.
274.
ug/L
ug/L
ug/L
Cert No E87604
LCS Recovery Report
Limits
70-130
70-130
70-130
5IJ2068.DLCS File ID:
Katahdin Analytical Services SI8365 page 0000081 of 0000115
600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029
http://www.katahdinlab.com
Page of1 1
WG173026-3RA
SI8365
28-OCT-15 JMSRSK SOP 175
28-OCT-15
WG173026AQ
NA
JMSRSK SOP 175
Methane
Ethane
Ethene
29-OCT-15Project:
Extraction Method:Analysis Method:
Report Date:
MS ID: Received Date:
Extracted By:Analyst:
Matrix:
SDG:
Extract Date: Analysis Date:
Lab Prep Batch: % Solids:
CompoundMS Rec
(%)MS
SpikeMS
Conc
113.
111.
116.
133.
249.
233.
150
280
270
Cert No E87604
MS/MSD Recovery Report
Limits
MSD ID:
Conc Units
MSD Rec(%)
MSDConc RPD (%)
RPD Limit
112.
111.
115.
150
280
270
1
0
0
30
30
30
70-130
70-130
70-130
ug/L
ug/L
ug/L
WG173026-4
U10.
U10.
U10.
SampConc
MSD Spike
133.
249.
233.
Sample ID: SI8365-10Client ID: ESLT-GW-IN7B-1015
5IJ2086.DMS File ID: 5IJ2071.dMSD File ID:
Katahdin Analytical Services SI8365 page 0000082 of 0000115
Katahdin Analytical Services SI8365 page 0000083 of 0000115
Katahdin Analytical Services SI8365 page 0000084 of 0000115
Katahdin Analytical Services SI8365 page 0000085 of 0000115
Katahdin Analytical Services SI8365 page 0000086 of 0000115
Katahdin Analytical Services SI8365 page 0000087 of 0000115
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Katahdin Analytical Services SI8365 page 0000099 of 0000115
Katahdin Analytical Services SI8365 page 0000100 of 0000115
Katahdin Analytical Services SI8365 page 0000101 of 0000115
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Katahdin Analytical Services SI8365 page 0000113 of 0000115
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Katahdin Analytical Services SI8365 page 0000115 of 0000115