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GROUNDWATER MONITORING REPORT EASTERN SURPLUS COMPANY SITE 887 MAIN STREET (ROUTE 191) MEDDYBEMPS, MAINE Prepared by: Campbell Environmental Group, Inc. 173 Gray Road Falmouth, ME 04105 February 2016 Prepared for: Mr. Christopher Swain Maine Department of environmental Protection State House Station 17 Augusta, Maine 04333
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Page 1: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

GROUNDWATER MONITORING REPORT

EASTERN SURPLUS COMPANY SITE

887 MAIN STREET (ROUTE 191)

MEDDYBEMPS, MAINE

Prepared by: Campbell Environmental Group, Inc.

173 Gray Road Falmouth, ME 04105

February 2016

Prepared for:

Mr. Christopher Swain Maine Department of environmental Protection

State House Station 17 Augusta, Maine 04333

Page 2: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

February 24, 2016

Mr. Christopher Swain Maine Department of Environmental Protection State House Station 17 Augusta, Maine 04333 Re: Groundwater Monitoring Eastern Surplus Company Site 887 Main Street (Route 191) Meddybemps, Maine 04657

Dear Mr. Swain,

Campbell Environmental Group, Inc. (CEG) prepared this report to document groundwater

monitoring activities conducted to fulfill the requirements of the Maine Department of

Environmental protection (MEDEP) Request for Bids, RFB # 8, Water Monitoring at Eastern

Surplus Site.

If you have any questions or comments, please do not hesitate to contact us. CEG appreciates

working with you on this project.

Sincerely,

Aaron Brignull Rich Campbell Environmental Scientist Maine Certified Geologist

President

Enclosure

Page 3: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Mr. Christopher Swain, Maine Department of Environmental Protection Page ii Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016

Table of Contents

1.0 INTRODUCTION ................................................................................................................ 1

2.0 QUALITY ASSURANCE PROJECT PLAN ....................................................................... 1

3.0 SITE SPECIFIC HEALTH AND SAFETY PLAN ............................................................... 24.0 GROUNDWATER MONITORING ACTIVITIES ................................................................. 2

4.1 Decontamination and Investigation Derived Wastes ............................................... 2

4.2 Monitoring Well Inspection & Groundwater Elevation Data Collection .................. 2

4.3 Groundwater Sampling and Chemical Analyses ...................................................... 3

4.3.1 Chemical Testing Plan ............................................................................................. 3

4.3.2 Groundwater Sampling ............................................................................................ 3

5.0 EVALUATION AND PRESENTATION OF RESULTS ...................................................... 4

5.1 Data Quality Assessment Summary .......................................................................... 4

5.1.1 Evaluation of Sampling Procedures ........................................................................ 4

5.1.2 Quality Assurance Quality Control Samples............................................................ 4

5.2 Analytical Results ........................................................................................................ 5

6.0 CONCLUSIONS AND RECOMMENDATIONS ................................................................. 8

APPENDICES

Appendix A – Figures & Tables Figure 1 - Locus Map Figure 2 - Sampling Locations

Table 1-1 – Analytical Results Table 2-1 – Historical Trends of PCE Concentrations

Appendix B – Field Data Low Flow Data Forms Well Gauging Forms Appendix C – MEDEP Data Validation Checklist Intra-well Trend Narrative Appendix D – Laboratory Reports

Page 4: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Mr. Christopher Swain, Maine Department of Environmental Protection Page 1 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016

1.0 INTRODUCTION

This groundwater monitoring report documents conditions at the Eastern Surplus Company Site,

located at 887 Main Street, in Meddybemps, Maine (Figure 1, Appendix A). The report and

associated field work were conducted by Campbell Environmental Group, Inc. (CEG) per Request

for Bid #8 by the Maine Department of Environmental protection (MEDEP).

To comply with RFB #8, CEG completed the following tasks:

TASK 1- Review/Update Quality Assurance Project Plan;

TASK 2 – Prepare a Site Specific Health and Safety Plan (HASP)/Coordinate Field Work

Activities;

TASK 3 – Perform Field Work;

TASK 4- Conduct Data Validation;

TASK 5- Prepare this report.

On October 19 and 20, 2015, CEG completed contracted groundwater monitoring activities at the

Site, including the collection of aqueous samples from 13 on-site wells. One residential water

supply well was sampled by MEDEP personnel. Sampling personnel also collected groundwater

elevation data from 42 on-site wells. To complete the groundwater monitoring event, CEG

contracted Dale Mitchell of the Passamaquoddy Environmental Department for general field

assistance. Mr. Terry Connelly from the United States Environmental Protection Agency (EPA)

also graciously volunteered to assist with field tasks. No additional services or personnel were

subcontracted by CEG.

Field instrumentation utilized during this monitoring event was contracted through Pine

Environmental, of Scarborough, Maine, and included two YSI Multimeters and two HACH

Turbidity Meters.

o HACH 2100Q Turbidity Meter (Instrument ID R149473)

o HACH 2100P Turbidity Meter (Instrument ID 11638)

o YSI 556 (Instrument ID 33217)

o YSI 556 (Instrument ID 33216)

All instrumentation was calibrated daily, prior to field activities. The calibration of turbidity meters

included an automated sequence utilizing standards of 10 NTU, 20 NTU, 100 NTU, and 800 NTU,

provided by Pine Environmental. Similarly, YSI instruments were calibrated using an automated

sequence involving Pine provided standards for pH, Conductivity, and ORP.

2.0 QUALITY ASSURANCE PROJECT PLAN

Site related activities were conducted in accordance with CEGs bid submittal form dated July 22,

2015, and MEDEP Task Order 1-5, Water Monitoring at Eastern Surplus Site, Meddybemps.

CEG also referenced standard operating procedures (SOPs) outlined in the Quality Assurance

Project Plan Addendum (QAPP) for Long-Term Monitoring at the Eastern Surplus Company Site,

rob.n.peale
Sticky Note
The EDD was missing all the depth to water and groundwater elevation data except for the 13 wells from which lab samples were collected. This needs to be provided in an additional EDD with the missing water level and groundwater elevation data.
Page 5: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Mr. Christopher Swain, Maine Department of Environmental Protection Page 2 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016

dated June 27, 2013, prepared by Nobis Engineering, Inc. of Lowell Massachusetts. The Nobis

QAPP was used for guidance during this monitoring event and specific deviations were approved

by appropriate MEDEP personnel, including;

Pre-preserved laboratory provided containers were used for sample collection eliminating

the need for sample preservation in the field using nitric acid;

Laboratory SOPs and minimum detection limits were not updated for this sampling event.

Laboratory services for this projected were contracted directly between the MEDEP and

Katahdin Analytical Services, of Scarborough, ME;

Groundwater sampling included the collection of one blind-duplicate sample which was

labeled using a fictitious sample point ID (ESLT-GW-MWRP-1015);

No surface water samples were collected as part of this monitoring event;

Data validation was conducted as specified in the RFB using the MEDEP Checklist; and

Data presentation does not include the graphical presentation of trends.

3.0 SITE SPECIFIC HEALTH AND SAFETY PLAN

The purpose of a site-specific HASP is to provide guidance, standards, and critical information

necessary to address health and safety issues at the Site. CEG prepared a site-specific HASP to

comply with Occupational Safety and Health Administration (OSHA) 29 CFR 1910.120

regulations. The HASP included, but was limited to, a description of personal protective

equipment requirements, site hazards and controls, emergency telephone numbers, a

contingency plan that conforms with 29 CFR 1910.120(1)(1) and (1)(2) for Site emergencies, and

Material Safety Data Sheets (MSDS) for potential constituents of concern. Prior to field work, the

HASP was reviewed and signed by on-site sampling personnel.

4.0 GROUNDWATER MONITORING ACTIVITIES

The following subsections outline groundwater monitoring activities outlined in MEDEP Task

Order 1-5, Water Monitoring at Eastern Surplus Site, Meddybemps.

4.1 Decontamination and Investigation Derived Wastes

Decontamination of non-dedicated equipment was conducted using an Aconox wash followed by

a distilled water rinse in accordance with the QAPP. Decontamination fluids and sample purge

water were discarded directly into the onsite carbon filtration unit.

4.2 Monitoring Well Inspection & Groundwater Elevation Data Collection

CEG personnel collected one round of groundwater elevation data from MEDEP stipulated

monitoring wells. Additionally, CEG observed wells for any evidence of damage including surface

water infiltration or artesian leakage. Locks were not present on any gauged or sampled wells,

rob.n.peale
Sticky Note
sp: Alconox?
rob.n.peale
Sticky Note
The HASP needs to be provided to the Department.
rob.n.peale
Sticky Note
The RFB specifically states in Task 5: “Data presentation should include graphical presentation of trends.” Where trends are discussed in the report, graphs for the major solvent contaminants would be much more illustrative than the text discussion. Graphs are less useful for metals at this point due to changes in sampling and analytical methods.
rob.n.peale
Sticky Note
project?
rob.n.peale
Sticky Note
There is no real documentation of well inspections. The bid document and task order required specific measurements which are not provided in the report.
Page 6: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Mr. Christopher Swain, Maine Department of Environmental Protection Page 3 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016

however, no additional damage or significant deficiencies were noted. Groundwater elevation

measurements are included in the Well Gauging Form included in Appendix B of this Report.

4.3 Groundwater Sampling and Chemical Analyses

The following section presents a detailed description of the field investigation methods as well as

the sampling and chemical analyses completed for the investigation. A brief narrative describing

changes in intra-well analyte concentrations between 2014 and 2015 monitoring events is also

included in Appendix C.

4.3.1 Chemical Testing Plan

Groundwater samples were submitted to Katahdin Analytical Services for laboratory analysis of

project analytes using one or more of the following methods:

VOCs in water using United States Environmental Protection Agency (USEPA) Method

8260;

Dissolved Gas (Methane, Ethane, Ethene) using RSK SOP 175; and

TAL Metals using USEPA Method 6020 and 7470.

4.3.2 Groundwater Sampling

CEG collected groundwater samples from 13 sampling points and assigned unique identifiers

including;

- ESLT-GW-IN1B1-1015

- ESLT-GW-IN1B2-1015

- ESLT-GW-IN7B-1015

- ESLT-GW-MW23B-1015

- ESLT-GW-MW36B1-1015

- ESLT-GW-MW3B-1015

- ESLT-GW-MW51B-1015

- ESLT-GW-MW54B-1015

- ESLT-GW-MW55B-1015

- ESLT-GW-MW57B1-1015

- ESLT-GW-MW57B2-1015

- ESLT-GW-MW58B1-1015

- ESLT-GW-MW58B2-1015

With the exception of sample ESLT-GWLORD-1015, all groundwater samples were collected

using peristaltic pumps and dedicated tubing according to MEDEP Standard Operating Procedure

DR#003, Groundwater Sampling Using Low Flow Purging and Sampling For Long Term

Monitoring. Physical parameters measured prior to the collection of groundwater samples

included depth to groundwater, pH, oxidation-reduction potential, conductivity, turbidity,

temperature, and dissolved oxygen. Sample ESLT-GWLORD-1015 was collected from an

outside tap of the residential water supply well of Mr. Mathew Lord by MEDEP staff. No field

parameters were collected, however, the well was purged for approximately 15 minutes prior to

sample collection from an outside spigot located at the north side of the residence. According to

Mr. Lord, the sample collection point is located before any water treatment systems.

rob.n.peale
Sticky Note
It is not clear what the reason for the extra identifiers is since both the lab and EGAD will create their own unique identifiers. In any case the extra symbols beyond the actual location name need to be removed from the Sample Point ID field in EDDs.
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Mr. Christopher Swain, Maine Department of Environmental Protection Page 4 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016

5.0 EVALUATION AND PRESENTATION OF RESULTS

The following subsections summarize the analytical results and detail site conditions.

5.1 Data Quality Assessment Summary

This subsection provides a summary of results from the Quality Assurance Quality Control

(QA/QC) program. The primary purpose of the QA/QC program is to meet the data quality

objectives for the monitoring program as outlined in the QAPP.

5.1.1 Evaluation of Sampling Procedures

CEG evaluated sampling procedures and field data in conjunction with the review of project

analytical data. CEG reviewed;

Documentation of field equipment calibration activities;

Field data for technical credibility versus the sample site setting;

Field sample data and chain-of-custody records; and

Sample handling and preservation procedures.

Field sampling activities were conducted in accordance with the Site Specific QAPP Addendum.

Field screening equipment was calibrated according to the respective manufacturers SOPs and

field data was reviewed by CEG personnel. A summary of field sampling equipment and

corresponding calibration procedures is included in Appendix B of this report. Katahdin Analytical

Services documented acceptable sample receipt condition including the presence of trip blanks,

and signed chain of custodies. Additionally, Katahdin indicated that samples were received in

acceptable condition, at less than 4 degrees Celsius, on ice, and in accordance with sample

handling, preservation, and integrity guidelines. Chain of custody seals were not used for

analytical samples submitted during this project because all sample coolers were transferred

directly from CEG sampling personnel to laboratory personnel. A complete set of the laboratory

analytical data, including the chain of custodies is presented in Appendix D.

5.1.2 Quality Assurance Quality Control Samples

QA/QC samples collected in the field included a trip blank, field duplicate sample, and a matrix

spike duplicate. Additionally, laboratory method blanks, laboratory control samples, laboratory

control sample duplicates, and matrix spike duplicates were analyzed by Katahdin. All QA/QC

results are included in the attached laboratory report (Appendix D). Quality control samples

collected in the filed include;

- ESLT-TB-1015 (Trip Blank)

- ESLT-GW-MWRP-1015 (Blind Duplicate of ESLT-GW-IN1B1-1015)

- ESLT-GW-IN7BMS-1015 (Matrix Spike Duplicate Sample)

rob.n.peale
Sticky Note
I do not see any calibration or equipment details in Appendix B.
rob.n.peale
Sticky Note
sp: field
Page 8: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Mr. Christopher Swain, Maine Department of Environmental Protection Page 5 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016

Data validation was conducted as required by the MEDEP validation checklist included in

Appendix C of this report. As contracted by the MEDEP, Katahdin Analytical Services reported

analytical results down to respective method detection limits. Accordingly, analytical detections

below practical quantitation limits have been qualified with a “J” and should be considered

estimated. Additional data quality issues included;

The PQL and MDL for Manganese, 1,2‐Dibromo‐3‐Chloropropane, 1,2‐Dibromoethane, and Vinyl Chloride, exceeded applicable regulatory guidelines.   

Re‐analysis (a dilution) of sample ESLT‐GW‐MWRP‐1015 was required but conducted 11 days outside of the prescribed hold time.  As a result, the single detected compound has been qualified (J) and should be considered estimated.         

Methylene Chloride was detected below the reporting limit in Method Blanks WG172846‐2 and WG172905‐2.  As a result, detections of methylene chloride in associated project samples have been qualified (JB) and should be considered estimated.   

 

Acetone, m,p‐xylene, ethylbenzene, methylene chloride, and o‐xylene, were detected in VOC Trip Blank ESLT‐TB‐1015.  Corresponding detections in project samples have been appropriately qualified.   

 

Aluminum, chromium, copper, nickel, selenium, and vandium, were outside of the acceptable RPD of 30% in field duplicate sample ESLT‐GW‐IN1B1‐1015.  Arsenic and cadmium were also outside the 30% RPD.  Corresponding detections in project duplicate samples have been appropriately qualified.   

 Based on CEG’s review, analytical data generated during the October 2015 monitoring event is complete and should be usable for the purposes of this project.     5.2 Analytical Results

Analytical results for project samples have been evaluated based on a comparison to applicable

regulatory standards, including Maine Center for Disease Controls Maximum Exposure

Guidelines (MEGs) for drinking water, dated October 19, 2012, and the Maine Remedial Action

Guidelines for Sites Contaminated with Hazardous Substances, Revised on May 8, 1013. All

detected project analytes are summarized in Table 1-1 of this report. At the request of the

MEDEP, Katahdin Analytical Services reported all analytical results down to the laboratory’s

respective method detection limits.

Volatile Organic Compounds

A total of 16 VOC compounds were detected at concentrations exceeding the laboratories

respective minimum detection limits (MDLs). Two additional compounds (1,2-dibromo-3-

chloropropane and 1-2-dibromoethane) were not detected at concentrations exceeding the

rob.n.peale
Sticky Note
The calculated RPDs should be shown in a table or appendix at least for those exceeding the guideline.
rob.n.peale
Sticky Note
sp: laboratory's
Page 9: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Mr. Christopher Swain, Maine Department of Environmental Protection Page 6 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016

laboratories MDLs, however, the MDLs exceeded corresponding regulatory guidelines and

project action limits. Of the 16 compounds detected, only five analytes were reported at

concentrations exceeding applicable regulatory guidelines, including cis-1,2-dichloroethene,

methylene chloride, tetrachloroethene, trichloroethene, and vinyl chloride. Methylene chloride

concentrations are most likely associated with laboratory contamination and elevated

concentrations were only observed in during subsequent sample analyses performed at a

dilution.

Cis-1,2-dichloroethene was detected in project samples ESLT-GW-MW51B-1015 and ESLT-GW-

MW54B-1015 at concentrations of 190 micrograms per litre (ug/l) and 130 ug/l, respectively. The

MEDEP Residential RAG for Cis-1,2-dichloroethene is 10 ug/l and the Project Action Limit is 70

ug/l.

Tetrachloroethene was detected in samples ESLT-GS-IN1B1-1015 (600 ug/l), ESLT-GW-MWRP-

1015 (500 ug/l), ESLT-GW-IN7B-1015 (190 ug/l), ESLT-GW-IN23B-1015 (140 ug/l), ESLT-GW-

IN36B-1015 (77 ug/l), ESLT-MW51B-1015 (100 ug/l), ESLT-MW54B-1015 (3,900 ug/l), and

ESLT-MW57B1-1015 (220 ug/l) at concentrations exceeding the MEDEP Residential RAG of 40

ug/l and a reported Project Action Limit of 3 ug/l.

CEG evaluated the Historical Trends of PCE Contamination Table from the Spring 2014

Technical Memorandum prepared by Nobis, dated January 2015. Based on the table provided in

the report, only one of the four comparable wells displayed a notable increase in PCE

concentrations. This was well IN-1B1. All other wells appeared to have generally stable

concentrations.

Trichloroethene was detected in samples ESLT-GS-IN1B1-1015 (5.6 ug/l), ESLT-GW-MWRP-

1015 (5.6 ug/l), ESLT-GW-IN1B2-1015 (12 ug/l), ESLT-GW-IN23B-1015 (5.5 ug/l), ESLT-

MW51B-1015 (12 ug/l), ESLT-MW54B-1015 (47 ug/l), and ESLT-MW57B-1015 (4.8 ug/l). The

MEDEP Residential RAG for Trichloroethene is 4 ug/l and the reported Project Action Limit is 5

ug/l. Detections of Trichloroethene in samples ESLT-GW-IN1B2-1015, ESLT-MW51B-1015, and

ESLT-MW54B-1015, also exceeded the corresponding MEDEP Construction Worker RAG of 5.8

ug/l.

Vinyl chloride was detected in samples ESLT-GS-IN1B1-1015 (0.27 ug/l), ESLT-GW-MWRP-

1015 (0.25 ug/l), ESLT-GS-IN1B2-1015 (2.2 ug/l), ESLT-MW51B-1015 (12 ug/l), ESLT-MW54B-

1015 (1.4 ug/l), and ESLT-GW-MW55B-1015 (20 ug/l), at concentrations exceeding the

corresponding MEDEP Residential RAG and reported Project Action Limit of 0.2 ug/l,

respectively. Vinyl chloride was not detected in any additional samples, however, the laboratory’s

reported minimum detected limit for this analyte exceeds applicable regulatory guidelines.

rob.n.peale
Sticky Note
The reasons for the dilutions should be stated somewhere in the report text.
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Mr. Christopher Swain, Maine Department of Environmental Protection Page 7 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016

Dissolved Gases

Groundwater samples were also analyzed for methane, ethane, and ethene. According to the

laboratory report, all three dissolved gases were detected in samples ESLT-GW-MW51B-1015

and ESLT-GW-MW55B-1015. Additionally, methane and ethene were also detected in samples

ESLT-GW-IN1B2-1015 and ESLT-GW-MW57B2-1015.

Metals

Antimony and Arsenic were detected in one project sample (ESLT-GW-MW36B1-1015) at

concentrations of 25.2 ug/l and 26 ug/l respectively, exceeding corresponding MEDEP

Residential RAGs and reported Project Action Limits. The Residential RAG and project Action

Limit for Antimony is 3 ug/l. The MEDEP Residential RAG and Project Action limit for arsenic is

10 ug/l.

Total chromium was detected in sample ESLT-GW-MW57B2-1015 at a concentration of 25.3 ug/l.

The Project Action limit for chromium is 20 ug/l. The MEDEP Residential RAG for chromium 6 is

also 20 ug/l.

Cobalt was detected in sample ESLT-GW-MW57B2-1015 at a concentration of 11.6 ug/l. The

Project Action limit for chromium is 20 ug/l. The MEDEP Residential RAG and Project Action limit

for cobalt is 10 ug/l.

Iron was detected in two samples (ESLT-GW-MW51B-1015 and ELST-GW-MW57B1-1015) at

concentrations of 8,500 ug/l and 11,000 ug/l, respectively. The MEDEP Residential RAG and

project Action Limit for Iron is 5,000 ug/l.

Manganese was detected in two samples and one duplicate sample (ESLT-GW-IN1B2-1015,

ESLT-GW-IN1B1 and ESLT-GW-MWRP-1015) at concentration of 2,600 ug/l and 1,990 ug/l,

respectively. The MEDEP Residential RAG for manganese is 500 ug/l. The reported Project

Action Limit for manganese is 200 ug/l.

Sodium was detected in samples ESLT-GW-MW23B-1015 (25,700 ug/l), ESLT-GW-MW36B1-

1015 (45,900 ug/l), ESLT-GW-MW51B-1015 (41,500), ESLT-GW-IN1B2 (23,800 ug/l), ESLT-

GW-MW57B2-1015 (347,000 ug/l) and ESLT-GW-MW55B-1015 (29,100 ug/l), at concentrations

exceeding the corresponding MEDEP Residential RAG of 20,000 ug/l. The reported project

Action Limit for sodium is also 20,000 ug/l.

rob.n.peale
Sticky Note
need PAL for Cobalt.
rob.n.peale
Sticky Note
The iron exceedance in MW-57B1 is actually at MW-55B according to EGAD and the report table. They need to re-check for correspondence between the report tables, reported laboratory data, and text in this section of the report.
rob.n.peale
Sticky Note
Metals also need to be compared to surface water guidelines and project action limits since the purpose of the low reporting limits is to identify metals that could cause exceedance of surface water standards. This does not seem to be included in text or tables so perhaps there should be a separate table for this.
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Mr. Christopher Swain, Maine Department of Environmental Protection Page 8 Groundwater Monitoring, Eastern Surplus Company Site, Meddybemps, Maine February 24, 2016

6.0 CONCLUSIONS AND RECOMMENDATIONS

Based on data generated during the 2015 monitoring event, groundwater at the site continues to

be impacted with volatile organic compounds, dissolved gases, and various metals. Primary

metals of concern appear to be iron, manganese, and sodium. Volatile organic compounds

detected in groundwater consist primarily of tetrachloroethene (PCE) and daughter compounds

trichloroethene (TCE), cis-1,2-dichloroethene (cis-DCE), and vinyl chloride. While concentrations

of project analytes appear to have remained generally consistent over the most recent sampling

periods, concentration have generally decreased since initial monitoring activities at the Site.

CEG recommends continued groundwater monitoring at the Site.

Page 12: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

APPENDIX A

Figures & Tables

Page 13: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

FIGURE 1 Eastern Surplus Site

887 Main Street, Meddybemps, Main

 

SITE

Page 14: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

FIGURE 2 October 2015 Sampling Locations

Eastern Surplus Site, Meddybemps, Maine  

MW‐54B 

MW‐58B1  MW‐58B2 

MW‐36B1 MW‐57B1  MW‐57B2 

MW‐51B  MW‐55B  MW‐23B 

IN‐1B1 IN‐1B2 

IN‐7B 

MW‐3B 

rob.n.peale
Sticky Note
The scale could be increased so that the area of interest (the sampled wells) is shown in more detail.
Page 15: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Residential (ug/l)

Construction Worker (ug/l)

Metals (Analytical Methods 6010/7000)ALUMINUM 7429-90-5 7,000 7,000 7,000 9,200,000 J 24 J 10 J 51.5 J 20 J 27 J 128

ANTIMONY 7440-36-0 3 3 3 3,700 J 0.52 J 0.57 1 J 0.92 1.57 25.2

ARSENIC 7440-38-2 10 10 10 1,400 J 4 UJ 2.2 7.5 U 2.2 U 2.2 26

BARIUM 7440-39-3 1,000 1,000 1,000 1,800,000 J 1.30 J 1.4 8.4 J 1.5 2.1 7.8

CADMIUM 7440-43-9 1 1 1 650 J 0.065 J 0.04 J 0.04 J 0.04 J 0.04 J 0.055

CALCIUM 7440-70-2 NR NR NR NR 20,600 20,800 14,200 15,700 35,800 8,100

CHROMIUM 7440-47-3 20 20 * 20 * 78000 * J 1.80 J 1.2 J 1.6 J 1.7 J 1.8 J 2.1

COBALT 7440-48-4 10 10 10 29000 J 0.43 J 0.45 J 0.42 J 0.075 J 0.41 J 0.14

COPPER 7440-50-8 500 500 500 130000 J 3.50 J 0.95 J 2.3 J 2 3 4

IRON 7439-89-6 5,000 5,000 5,000 6,500,000 100 J 80 870 1,670 110 110

LEAD 7439-92-1 10 10 10 1,600,000 J 0.09 U 0.073 J 0.12 U 0.073 U 0.073 J 0.29

MAGNESIUM 7439-95-4 NR NR NR NR 4,270 4,550 3,320 3,030 9,350 2,330

MANGANESE 7439-96-5 200 500 500 220,000 1,990 1,990 2,600 25.1 3 8.9

MERCURY 7439-97-6 2 2 2 28,000 U 0.013 U 0.013 U 0.013 U 0.013 U 0.013 U 0.013

NICKEL 7440-02-0 20 20 20 28,000 J 1.50 J 1.1 J 1.6 J 1.2 2.9 J 1.4

POTASSIUM 7440-09-7 NR NR NR NR 2,690 2,740 2,310 1,770 2,570 2,230

SELENIUM 7782-49-2 40 40 40 46,000 U 0.18 J 1 U 0.18 U 0.18 U 0.18 U 0.18

SODIUM 7440-23-5 20,000 20,000 20,000 NR 7,550 7,700 23,800 6,700 25,700 45,900

VANADIUM 7440-62-2 200 200 200 65,000 J 4 J 2 U 0.51 U 0.51 J 3 J 3

ZINC 7440-66-6 2,000 2,000 2,000 2,800,000 U 3.90 U 3.9 U 3.9 U 3.9 U 3.9 J 5.5

Volatile Organic Compounds - VOCs (Analytical Method 8260)1,2-DIBROMO-3-CHLOROPROPANE 96-12-8 0.2 0.4 0.4 1.2 U 0.50 U 5.0 U 0.50 U 10. U 0.50 U 0.50 U 0.50 U 0.50

1,2-DIBROMOETHANE 106-93-4 0.05 0.2 0.2 8.70 U 0.22 U 2.2 U 0.22 U 4.4 U 0.22 U 0.22 U 0.22 U 0.22

2-BUTANONE 78-93-3 4,000 4,000 4,000 22,000 U 1.3 U 13. U 1.3 U 26. U 1.3 U 1.3 U 1.3 U 1.3

4-METHYL-2-PENTANONE 108-10-1 500 500 500 11,000 U 1.3 U 13. U 1.3 U 26. U 1.3 U 1.3 U 1.3 U 1.3

ACETONE 67-64-1 6,000 6,000 6,000 160,000 JB 3.1 JB 33 JB 2.8 U 44. U 2.2 JB 2.6 U 2.2 JB 2.4

CHLOROETHANE 75-00-3 7 7 7 20,000 U 0.55 U 5.5 U 0.55 U 11. 4.7 U 0.55 U 0.55 U 0.55

CHLOROMETHANE 74-87-3 3 20 20 NR J 1.2 U 3.6 U 0.36 U 7.2 U 0.36 J 1.6 2.3 J 1.3

CIS-1,2-DICHLOROETHENE 156-59-2 70 10 10 2,000 3.1 U 2.1 2.8 U 4.2 8.1 6.3 14 3.3

ETHYLBENZENE 100-41-4 30 30 30 1,500 U 0.021 U 2.1 U 2.1 U 4.2 U 0.021 U 0.021 U 0.021 U 0.021

M-,P-XYLENE DEP2068 600 1000 ** 1000 ** 790 ** U 0.59 U 5.9 U 0.59 U 12. U 0.59 U 0.59 U 0.59 U 0.59

METHYL ACETATE 79-20-9 NR NR NR NR U 0.53 U 5.3 U 0.53 U 11. U 0.53 U 0.53 U 0.53 U 0.53

METHYLENE CHLORIDE 75-09-2 5 40 40 2,600 JB 1.3 JB 19 U 1.1 U 23. JB 1.5 JB 1.4 JB 1.3 JB 1.3

O-XYLENE 95-47-6 600 1000 ** 1000 ** 790 ** U 0.25 U 2.5 U 0.25 U 5.0 U 0.25 U 0.25 U 0.25 U 0.25

TETRACHLOROETHENE 127-18-4 3 40 40 880 E 650 600 E 710 J 500 31 190 140 77

TOLUENE 108-88-3 600 600 600 12,000 U 0.27 U 2.7 U 0.27 U 5.4 U 0.27 U 0.27 U 0.27 U 0.27

TRANS-1,2-DICHLOROETHENE 156-60-5 100 100 100 2,000 U 0.25 U 2.5 U 0.25 U 5.0 J 0.41 U 0.25 U 0.25 U 0.25

TRICHLOROETHENE 79-01-6 5 4 4 5.8 5.6 U 2.8 5.6 U 5.6 12 3.3 5.5 3.5

VINYL CHLORIDE 75-01-4 0.2 0.2 0.2 160 J 0.27 U 2.5 U 0.25 U 5.0 2.2 U 0.25 U 0.25 U 0.25

Dissolved GasMETHANE 74-82-8 NR NR NR NR

ETHANE 74-84-0 NR NR NR NR

ETHENE 74-85-1 NR NR NR NR

METHANE (Dilution) 74-82-8 NR NR NR NR

ETHANE (Dilution) 74-84-0 NR NR NR NR

ETHENE (Dilution) 74-85-1 NR NR NR NR

Notes: ug/L = micrograms per liter, NR = not regulated, NA = not analyzed, MEDEP = Maine Department of Environmental Protection, 2013 MEDEP RAGs = Maine Remedial Action Guidelines for Sites Contaminated with Hazardous Substances, Revised May 8, 2013

Bold Font = Analytical Detection, U = less than (non detect), J = Estimated, * = Guideline for Chromium VI, ** = Guideline for Xylenes, 2012 MEGs = Maine Center for Disease Control Maximum Exposure Guidelines for Drinking Water, dated October 19, 2012

Detected concentration or reporting limit exceeds MEG or Residential RAG.

Detected concentration or reporting limit exceeds Construction Worker RAG.

Detected concentration or Reporting Limit exceeds Project Action Limits

U 10

U 10

24

N/A

N/A U 10

U 10

U 10

U 10

U 10

N/A

ESLT-GW-IN1B1-1015 (Dilution)

ESLT-GW-MWRP-1015 (Lab Dilution)

U 10

U 10

U 10

U 10

U 10

U 10

N/A

N/A

ESLT-GW-IN7B-1015 ESLT-GW-MW36B1-1015ESLT-GW-IN1B1-1015 ESLT-GW-IN1B2-1015

N/A

Analyte ESLT-GW-MWRP-1015 (ESLT-GW-IN1B1-1015 DUP)

N/A

Maine CDC 2012 Maximum

Exposure Guidelines

(ug/L)

2013 Maine Remedial Action Guidelines for Groundwater

by Exposure Pathway

N/A

Project Action Limits (ug/L)

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/AN/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A N/A

N/A

N/A

N/AN/A N/A

N/A N/A

U 1044

U 10N/A

N/A

N/A

N/A

N/A

U 10

TABLE 1-1

Sample ID

N/A

N/A

N/A

CAS No.ESLT-GW-MW23B-1015

Page 1 of 3

Page 16: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Residential (ug/l)

Construction Worker (ug/l)

Metals (Analytical Methods 6010/7000)ALUMINUM 7429-90-5 7,000 7,000 7,000 9,200,000 J 24 J 22 J 24 J 44 J 138

ANTIMONY 7440-36-0 3 3 3 3,700 1.03 J 0.2 J 0.3 J 0.095 2.65

ARSENIC 7440-38-2 10 10 10 1,400 U 2.2 U 2.2 U 2.2 U 2.2 6.5

BARIUM 7440-39-3 1,000 1,000 1,000 1,800,000 J 1 2.6 J 1.2 J 1 3

CADMIUM 7440-43-9 1 1 1 650 J 0.06 J 0.055 J 0.04 J 0.08 J 0.08

CALCIUM 7440-70-2 NR NR NR NR 9,450 68,000 62,000 20,400 41,200

CHROMIUM 7440-47-3 20 20 * 20 * 78000 * J 1.7 J 1.9 J 1.7 J 1.6 J 3.3

COBALT 7440-48-4 10 10 10 29000 J 0.11 J 0.5 J 0.46 J 0.3 J 0.17

COPPER 7440-50-8 500 500 500 130000 J 2 J 1.9 3.3 J 1.8 J 2.7

IRON 7439-89-6 5,000 5,000 5,000 6,500,000 150 8,500 1,230 11,000 160

LEAD 7439-92-1 10 10 10 1,600,000 J 0.085 J 0.09 U 0.073 J 0.075 J 0.29

MAGNESIUM 7439-95-4 NR NR NR NR 2,200 2,650 7,100 3,500 7,250

MANGANESE 7439-96-5 200 500 500 220,000 14.9 139 252 217 12

MERCURY 7439-97-6 2 2 2 28,000 U 0.013 U 0.013 U 0.013 U 0.013 U 0.013

NICKEL 7440-02-0 20 20 20 28,000 J 1.5 J 1.4 J 1.5 J 1.2 J 1

POTASSIUM 7440-09-7 NR NR NR NR J 895 122,000 1,600 32,600 2,070

SELENIUM 7782-49-2 40 40 40 46,000 U 0.18 U 0.18 U 0.18 U 0.18 U 0.18

SODIUM 7440-23-5 20,000 20,000 20,000 NR 4,410 41,500 8,300 29,100 11,300

VANADIUM 7440-62-2 200 200 200 65,000 J 1 U 0.51 U 0.51 U 0.51 J 3

ZINC 7440-66-6 2,000 2,000 2,000 2,800,000 U 3.9 19 94.5 23 J 7

Volatile Organic Compounds - VOCs (Analytical Method 8260)1,2-DIBROMO-3-CHLOROPROPANE 96-12-8 0.2 0.4 0.4 1.2 U 0.50 U 0.50 U 0.50 U 50. U 0.50 U 0.50 U 2.5

1,2-DIBROMOETHANE 106-93-4 0.05 0.2 0.2 8.70 U 0.22 U 0.22 U 0.22 U 22. U 0.22 U 0.22 U 1.1

2-BUTANONE 78-93-3 4,000 4,000 4,000 22,000 U 1.3 58 U 1.3 U 130 U 1.3 U 1.3 U 6.6

4-METHYL-2-PENTANONE 108-10-1 500 500 500 11,000 U 1.3 25 U 1.3 U 130 U 1.3 U 1.3 U 6.6

ACETONE 67-64-1 6,000 6,000 6,000 160,000 U 2.2 B 31 JB 2.4 U 220 B 10 U 2.2 JB 14

CHLOROETHANE 75-00-3 7 7 7 20,000 U 0.55 U 0.55 U 0.55 U 55. U 0.55 U 0.55 U 2.8

CHLOROMETHANE 74-87-3 3 20 20 NR J 1.4 U 0.36 2.6 U 36. U 0.36 J 1.4 U 1.8

CIS-1,2-DICHLOROETHENE 156-59-2 70 10 10 2,000 U 0.21 190 130 110 2.7 5.0 J 3.4

ETHYLBENZENE 100-41-4 30 30 30 1,500 U 0.021 U 0.021 U 0.021 U 21 U 0.021 U 0.021 U 1.0

M-,P-XYLENE DEP2068 600 1000 ** 1000 ** 790 ** U 0.59 U 0.59 U 0.59 U 59. JB 0.74 U 0.59 U 3.0

METHYL ACETATE 79-20-9 NR NR NR NR U 0.53 4.8 U 0.53 U 53. U 0.53 U 0.53 U 2.6

METHYLENE CHLORIDE 75-09-2 5 40 40 2,600 JB 1.3 JB 1.6 JB 1.2 JB 170 U 1.1 JB 1.4 JB 8.7

O-XYLENE 95-47-6 600 1000 ** 1000 ** 790 ** U 0.25 U 0.25 U 0.25 U 25. B 2.4 U 0.25 U 1.2

TETRACHLOROETHENE 127-18-4 3 40 40 880 U 0.40 100 E 3,900 3,900 10 E 240 220

TOLUENE 108-88-3 600 600 600 12,000 U 0.27 U 0.27 U 0.27 U 27. U 0.27 U 0.27 U 1.4

TRANS-1,2-DICHLOROETHENE 156-60-5 100 100 100 2,000 U 0.25 U 0.25 U 0.25 U 25. J 0.77 U 0.25 U 1.2

TRICHLOROETHENE 79-01-6 5 4 4 5.8 U 0.28 12 47 U 28. 2.8 4.8 J 4.4

VINYL CHLORIDE 75-01-4 0.2 0.2 0.2 160 U 0.25 12 J 1.4 U 25. 20 U 0.25 U 1.2

Dissolved GasMETHANE 74-82-8 NR NR NR NR E 6,000

ETHANE 74-84-0 NR NR NR NR U 10

ETHENE 74-85-1 NR NR NR NR 1,000

METHANE (Dilution) 74-82-8 NR NR NR NR 4,800

ETHANE (Dilution) 74-84-0 NR NR NR NR U 100

ETHENE (Dilution) 74-85-1 NR NR NR NR 870Notes: ug/L = micrograms per liter, NR = not regulated, NA = not analyzed, MEDEP = Maine Department of Environmental Protection, 2013 MEDEP RAGs = Maine Remedial Action Guidelines for Sites Contaminated with Hazardous Substances, Revised May 8, 2013

Bold Font = Analytical Detection, U = less than (non detect), J = Estimated, * = Guideline for Chromium VI, ** = Guideline for Xy

Detected concentration or reporting limit exceeds MEG or Residential RAG.

Detected concentration or reporting limit exceeds Construction Worker RAG.

Detected concentration or Reporting Limit exceeds Project Action Limits

N/A

U 10

Sample ID

TABLE 1-1

U 10

U 10

U 10

N/A

U 10

U 10

ESLT-GW-MW3B-1015

U 10E 5,300

ESLT-GW-MW54B-1015ESLT-GW-MW57B1-1015

(Lab Dilution)ESLT-GW-MW57B1-1015

Project Action Limits (ug/L)

Analyte ESLT-GW-MW54B-1015 (Lab Dilution)

Maine CDC 2012 Maximum

Exposure Guidelines

(ug/L)

2013 Maine Remedial Action Guidelines for Groundwater

by Exposure Pathway

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/AN/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

U 10N/A

N/AN/A

16

23 U 10

N/A

N/AN/A

N/A N/A

N/A

N/A

6,800

U100N/A

N/AN/A

N/A

N/A

N/A

N/A

N/A

N/A

U100

CAS No.ESLT-GW-MW55B-1015 ESLT-GW-MW51B-1015

Page 2 of 3

Page 17: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Residential (ug/l)

Construction Worker (ug/l)

Metals (Analytical Methods 6010/7000)ALUMINUM 7429-90-5 7,000 7,000 7,000 9,200,000 1,060 J 239 620

ANTIMONY 7440-36-0 3 3 3 3,700 1.3 J 0.45 J 0.43

ARSENIC 7440-38-2 10 10 10 1,400 U 2.2 J 4 J 4

BARIUM 7440-39-3 1,000 1,000 1,000 1,800,000 860 13.4 14.1

CADMIUM 7440-43-9 1 1 1 650 J 0.085 J 0.08 J 0.065

CALCIUM 7440-70-2 NR NR NR NR 625,000 56,000 55,000

CHROMIUM 7440-47-3 20 20 * 20 * 78000 * 25.3 J 2.3 J 2.2

COBALT 7440-48-4 10 10 10 29000 11.6 J 0.12 J 0.18

COPPER 7440-50-8 500 500 500 130000 16.3 J 2.5 J 1.3

IRON 7439-89-6 5,000 5,000 5,000 6,500,000 2,090 160 160

LEAD 7439-92-1 10 10 10 1,600,000 1.43 U 0.073 J 0.13

MAGNESIUM 7439-95-4 NR NR NR NR 140 2,600 2,420

MANGANESE 7439-96-5 200 500 500 220,000 7.15 J 1.2 4.8

MERCURY 7439-97-6 2 2 2 28,000 J 0.02 U 0.013 U 0.013

NICKEL 7440-02-0 20 20 20 28,000 6 J 1.4 J 1.3

POTASSIUM 7440-09-7 NR NR NR NR 191,000 8,250 9,000

SELENIUM 7782-49-2 40 40 40 46,000 U 0.18 U 0.18 U 0.18

SODIUM 7440-23-5 20,000 20,000 20,000 NR 347,000 12,500 12,800

VANADIUM 7440-62-2 200 200 200 65,000 J 1 J 3 J 3

ZINC 7440-66-6 2,000 2,000 2,000 2,800,000 10 J 8 U 3.9

Volatile Organic Compounds - VOCs (Analytical Method 8260)1,2-DIBROMO-3-CHLOROPROPANE 96-12-8 0.2 0.4 0.4 1.2 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50

1,2-DIBROMOETHANE 106-93-4 0.05 0.2 0.2 8.70 U 0.22 U 0.22 U 0.22 U 0.22 U 0.22

2-BUTANONE 78-93-3 4,000 4,000 4,000 22,000 U 1.3 U 1.3 U 1.3 U 1.3 U 1.3

4-METHYL-2-PENTANONE 108-10-1 500 500 500 11,000 U 1.3 U 1.3 U 1.3 U 1.3 U 1.3

ACETONE 67-64-1 6,000 6,000 6,000 160,000 B 93 JB 2.5 U 2.2 6.3 JB 3.5

CHLOROETHANE 75-00-3 7 7 7 20,000 U 0.55 U 0.55 U 0.55 U 0.55 U 0.55

CHLOROMETHANE 74-87-3 3 20 20 NR J 1.9 2.3 J 0.86 U 0.36 U 0.36

CIS-1,2-DICHLOROETHENE 156-59-2 70 10 10 2,000 U 0.21 J 0.32 U 0.21 U 0.21 U 0.21

ETHYLBENZENE 100-41-4 30 30 30 1,500 U 0.021 U 0.021 U 0.021 J 0.26 U 0.021

M-,P-XYLENE DEP2068 600 1000 ** 1000 ** 790 ** U 0.59 U 0.59 U 0.59 J 0.77 U 0.59

METHYL ACETATE 79-20-9 NR NR NR NR U 0.53 U 0.53 U 0.53 U 0.53 U 0.53

METHYLENE CHLORIDE 75-09-2 5 40 40 2,600 JB 1.3 JB 1.2 JB 1.4 JB 1.4 JB 1.3

O-XYLENE 95-47-6 600 1000 ** 1000 ** 790 ** U 0.25 U 0.25 U 0.25 2.4 U 0.25

TETRACHLOROETHENE 127-18-4 3 40 40 880 9.7 18 U 0.40 U 0.40 U 0.40

TOLUENE 108-88-3 600 600 600 12,000 1.8 U 0.27 U 0.27 U 0.27 U 0.27

TRANS-1,2-DICHLOROETHENE 156-60-5 100 100 100 2,000 U 0.25 U 0.25 U 0.25 U 0.25 U 0.25

TRICHLOROETHENE 79-01-6 5 4 4 5.8 J 0.49 J 0.69 U 0.28 U 0.28 U 0.28

VINYL CHLORIDE 75-01-4 0.2 0.2 0.2 160 U 0.25 U 0.25 U 0.25 U 0.25 U 0.25

Dissolved GasMETHANE 74-82-8 NR NR NR NR

ETHANE 74-84-0 NR NR NR NR

ETHENE 74-85-1 NR NR NR NR

METHANE (Dilution) 74-82-8 NR NR NR NR

ETHANE (Dilution) 74-84-0 NR NR NR NR

ETHENE (Dilution) 74-85-1 NR NR NR NR

Notes: ug/L = micrograms per liter, NR = not regulated, NA = not analyzed, MEDEP = Maine Department of Environmental Protection, 2013 MEDEP RAGs = Maine Remedial Action Guidelines for Sites Contaminated with Hazardous Substances, Revised May 8, 2013

Bold Font = Analytical Detection, U = less than (non detect), J = Estimated, * = Guideline for Chromium VI, ** = Guideline for Xy

Detected concentration or reporting limit exceeds MEG or Residential RAG.

Detected concentration or reporting limit exceeds Construction Worker RAG.

Detected concentration or Reporting Limit exceeds Project Action Limits

TABLE 1-1

CAS No.

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A N/AN/A N/A N/A

N/A

N/AN/A

N/A N/A

N/A N/A

U 10

25

N/A

U 10

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

Maine CDC 2012 Maximum

Exposure Guidelines

(ug/L)

2013 Maine Remedial Action Guidelines for Groundwater

by Exposure Pathway

ESLT-GW-MW57B2-1015

Sample ID

U 10

U 10

U 10

U 10

ESLT-GW-MW58B2-1015ESLT-GW-MW58B1-1015

26

U 10

U 10

Project Action Limits (ug/L)

Analyte ESLT-TB-1015 (Trip Blank)

ESLT-GWLORD-1015

U 10

U 10

Page 3 of 3

Page 18: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

IN-1B1 IN-1B2 MW-3B MW-34B1 MW-34B2 MW-35B MW-36B1 MW-36B2 MW-43B1 MW-43B2 MW-42S MW-43S MW-45S IS-1B IS-2B MW-50S IS-1S IS-2S

NB NB NB NB NB NB NB NB NB NB NO NO NO SB SB SO SO SO

November-01 1,400 300 6,600 24 9,100 230 12 150 180 dry dry dry 2 19 42 8 11

April-02 1,800 310 1,100 14 3,200 380 25 220 180 13 51 dry 9 16 42 14 40

April-03 5,700 23 6,100 75 1,200 300 9 110 5 29 11 4 1U 14 5U 6

October-03 480 61 10,000 13 850 310 30 40 210 7 19 25 18 13

April-04 180 81 1,100 11 2,000 350 34 41 48 4 27 4 9 17 16 12 11

April-05 275 20 2,900 2 590 190 27 37 140 1 7 2 5 8 9 5 7

October-05 35 55 610 7 1,700 260 32 44 180 105 4 3 7 10 7 9

April-06 2,100 24 890 12 230 29.5 47 190 2 63 3 4 5 8 9 8

August-06

September-07

August-07 110 150 840 16 120 30 80.5 42 220 950 1.5 1.9 1 7.8 9.5 7.7

October-07 3,600 210 3,000 64 1,650 1 230 20 47 17 110 380 2.5

April-08 97 130 1,850 760 1.6 120 6.8 19 5.2 1.7 12 5.7 1.9 0.91 3.9 1.6 2.9

October-08 110 190 1,700 540 2.4 845 180 18 32 11 1.5 9.6

May-09 170 200 1,650 36 1.2 535 140 34 28 8.8 6.55 3.3 6.8 7 4

October-09 16 160 490 90 5U 61 10 8.4 1.2 2.7

May-10 15 97 5U 30 5U 22 23 20 2.9 dry 1.5 1.2 0.92 0.5U 4.9 3.9 2.9

October-10 35 195 3.7 510 8.1 220 48 21 28 5.5 1.1 6.5 dry

November-10

May-11 42 120 1.2 24 1.3 590 90 23 31 2.8 dry 5U 1.9 2.8 4.5 4.7 3.3 4.2

November-11 6 92 51.0 13 2.3 650 52 6.9 28 1.5 dry 22 dry

December-11

May-12 370 85 4.0 800 3.1 26 60 25 33 4.1 0.47 10 0.57 1.5 0.52 4.2 3.5 3.9

October-12

Nov-16 100 170 11 620 2 98 93 26 42 5 18 1

April-13

June-13 280 13 4 110 2U 4 62 24 41 3 8 2U

October-13 265 22 2 99 2U 950 85 20 10 2U 380 2U

May-14 330 25 2 U 660 2 U 25.5 68 13 11 2 U 17 2U 2U 2U 3 2U 3

Oct-15 600 31 0.4 U NS NS NS 77 NS NS NS NS NS NS NS NS NS NS NS

Notes:

1. Sample collected in September 2007 4. U = below contract required quantitation limit.2. Blank = not sampled or a gap in historical data reviewed. 5. italic text indicates the value listed is the average of the field sample and field dublicate results3. All concentrations listed in micrograms per liter (μg/L). 6. NO = northern overburden aquifer, NB = northern bedrock aquifer, SO = southern overburden aquifer, SB = southern bedrock aquifer

7. NS = Not Sampled

Table 2-1Hitorical PCE Concentrations

Historical PCE Concentrations Eastern Surplus Company Site Meddybemps, Maine

Treatment system and northern plume extraction wells offline.

First bioremediation injection in northern plume area.

Second bioremediation injection in northern plume area.

Sample LocationAquifer

Date

Treatment system and extraction wells offline.

Restarted treatment system and extraction wells.

Southern plume extraction well offline.

rob.n.peale
Sticky Note
This table is incomplete in that it does not include all the wells sampled in 2015. It would be more useful to have a table that includes all these wells or perhaps just the wells sampled in 2015. Even better this information could be presented graphically in some way.
Page 19: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

APPENDIX B

Field Data

Page 20: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

F ______ _____ ______ ______

MI ___ ___

~~1 _____ ____ ____ _____

/~V

fl/i _________ ________ ________ _________

0’) _____ ____ ____ _____

‘.1 ___ ____ ____

A)

,ndard Operating Procedures Field FormskSampl~ng\Sanpling_AtI

______________ fovc

____________ Pvc

4a ~ (~~LJ) ri~L~

A ~ p~f ~5~ft#t~f V q~’’ ~

n —~n — I GROUNDWATER LEVEL SO~No hYD~D3 I Page j of

s.’i~sas#~W I Date b/IS/id RevMEASUREMENT LOG

Prepareo by

I tr.cwoe~g Ir,c ~~cnares~ OLin Approveo ti~SHEET

Sue Narie 4 5k ‘&i S p 1 ..i S Terroerature Range 3 2 5~~)Projeci NumberItasl. rrecipIrauon 5 %J Pc. I C oçj p 5Personnel. c. I~ C-nij~ ~ f / r e ta~, (~,r4c’ I (ywrnd Soeeo Uireci art

Mtc,4 R.—~ / ctLIt~ .l4~EQUIPMENT INFORMATION

.~‘

Tyrte or Mdci Icrelet wa1~rLev~I I Interlace Probe lype of Mar toiin~3 [quiDnien: side 01D FID / Other

---Serial No. Serial No

NobisNo 5K W,w/ O,PPt4 NobisF’o

/ NLatest .atibration Dale

FIELD DATA

eVelt or Reference F.tevalion of PlO or FIDWater Level Adjosled GrouridwaletP’ezonielei me ‘oin: (SP Reference Readiro Ooseivalioi.sReading bill Depth (1:1 Elevation Itt

No. ~5 PVCI Pain: ppnit

393-I ~‘ooo ~i.ii p39.e3-a ,nc ~

~ n ,..z — —

WRdR,~a,1 Pa3 hl~82~s,?.-I,t2tg //).p9 ~)r~q 4,2/pgnv-id- /618 g.~ ng ~Ww-/8’~ “~fl .sa.Jc ~/~;3 c4~c9v23-.B ,~s’a 637 .br,3 /4”.R9’

~ .t~2 DT,3 j-2.3~j,y~4 ,~4t~9 en’ -~ja ~ ~

,≥c-ii/ /~;~ 7 ~);i’, .23. 7~’J~7J3 70; 8.&.i )03 AS.oy)qa~s y~/9 ,‘,,7./Q /)~? .2O.~Q’4fr /Z’&/ 7.3.?? 1’ZD L/3,SO~93&~ ,2J.5 /1.34 .bra /4.fl7,34~%2~s /7%? id.9O ‘~ ~ogg3-/ /7yS //.Q) .i’7~8 .?.S.3/

~fczS~ ‘S.Es ~ //Pi.bO≥nf:3;:~~ ,,sp ZZ-3 ~o. 9,1o’./.a /5ç59 ~~713 ‘1/76‘ii vvss z at%≤~ (LII flrI4 /Lfl.qQ

Neil?? pqk

C.a’e3-~~5 ,Ov’c

NOTES S~. Startdoipi. t~. Road 8cc. PVC. Riser

~‘.3≤ FVC w~, N ~S2-ía

top~- ii.~i~

DT~ ‘15.35Sigriatu e

O~ap .~4.tI(J

Page 21: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

4-i ___ __ ___ ___ ___ __

4i~z __ __ __ __ __ __

NOTES S~ Standp DC F~B Road Box PVC

3’

I GROUNDWATER LEVEL SOP No HYD-003 Page: 2. of 2sa’!sJe.sft.~ I Date it/ugiiS I Rev.:

I MEASUREMENT LOG Prepared by

SHEETNob~ Eng~ereg Inc. n~i~n&ne~.~ Approved by

S~e Name: E a j /tI7AJ ≤..iQ6? LU( Temperature Range 12 —f0Project Number/Task Precipitation 5 ‘-‘t.J Pa_fl Ci oc.’edjPersonnel: R’ tA cc..np~da /re~it~i ~ot.f /%. Wind Speed/Diection

/3flCo-~J gi, j~ LuEQUIPMENT INFORMATION

ype of Meter (circle) Water Level / Interface Probe Type of Montloring Equipment (circle): PID / FID / Other

Serial No. ~ fk’.— He -z~ Serial No.

Nobis No Nobis No.

Latest Calibration Date ft fi4( i S

FE14)fA~Welt or Reference Elevation of PID or FID

Piezometer Time Point (SP Reference Water Level Ad)u~Ied Groundwater Reading ObseNationsReading (It) flepd’ (It) Elevation (It)

Af1h~ RB. PVC) Point (ppm)

~~I3 4. ~s- Tot 4 /0.7 4741c3?4 4.’~e~ j~t.4 ~.oL (Oz.4O

3c41& 4; zz- ‘IX Mt J i~ 4/,. 29Mzv1~ 4:t~~ PVC- ft.w Z34o

.?rM7~ 143/ -rccMbJ q.s/ sz.~ieJ-2.’t ~&, 9’t •7.A~.2z,s4.

‘j3~l ~ Q~lc !~.6p 111,17—tM44~ 4,’s3 ??ILfS fszS

≤1s3 4S~, I~OtktLuLS~ 9 3~ zzflcu/s 4~,Ct fcc Mdd,Li 9.&.8 4e,~sr4B?1o3 fCLM~M~Ql4 940 r~.i&nc SIozl Pv~ 4Q73,? !flIc Pvc 9•gO ?3,/4-.~

.161 .≤;fll Pb’~. 4.€~B 171/9 V ,4/ b,Ilvrsmffli- 4.fl Pi€Z I Jc~cyI lv~-i32~;3r evc IL3~ /Cf.41-4 i 5jQJ n~’c- ~ ~ ~

3U~Is;4,_4- Pvc Scg1’ ~St tç49’ Pvc,

Signature

indard Operating Prooedures~Field Forms~Sampling~Sampl.ng_All

Page 22: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

~ØROII%

C)Drinking Water Sampling Data Sheet

Site Name: /~45/~ftt~7 6o,p/u-.sLocation ID: Co

Owner/Occupant Name: fi?a/4eu’ Lo’4

Owner/Occupant Address:

Sampler(s): 1R5h Pea/c ,)Clvji Jj/t////4

Sample Collection Date:

Sample Collection Time: / ~; /c’ ~

Purge duration: f5 tn~i1jfrs~

Sample location (kitchen sink, outdoor faucet, etc.):

O~t5/h *99) north i’~i€’(&

Comments/Notes (treatment, water quality, QAIQC samples, Change innumber/age of users, etc):

3~p o~/k /4c ~≤ k&~re~ *~/mrn/

Page 23: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

WeIl# /Y/W-.)IOAs • ~‘ .0

1~4~I~,’l~”

I’! ir -- ~ ..‘

~ -—-------~.— ~

— Sample Device ~ - IORP Turb. I

01

Laborato&y Sample NumbersAnalysis / Depth Number

Date ,scs/zo/;S

Time Water LevelBegin Time of Purge Screen Interval

Static Water Level Total Depth 3 2~ 75 Well Diameter

Monitoring Well Purge and Sample Data SheetSite Name ~ S~’rpL~’c

Flow DO Temp. Cond. p11

WrIte Meter Number of Instrument Used I ii

— Formation

Mir~. j Feet below NIP mlJMin mgIL Celcius - II -k~H+] mV NTIJ

Comments.~:io q35 -____

3:55 ~ 77 /L.5 -‘~33 -7-es 230 2Se1j9’q3 ieo ~36 /M’1 ~W1 7≠~J ~j8 ~ 2~,z3’Ly5 ci.g i’io 4iq 7.8 221

.Y.50 ,p,p’~ //.q~ ~c33’ .~ 74! 2082 2-6.)~ 5c /0./ti iz 773 /~f311:00 A]’ wlti O-ee;~eas -cQ 4~i~I 4 tkkk 8u~- ~ ‘n’-”1’-- ~,q,1/./k1,’~/.C5 7t2•)l ~7L iiB //2-// ~ 7,tL1 if~ Z/.OQ~, /o.c7 i~Z ~ //.41 435 ~ zzS 7 jq.ggi~ ~i // ~ 3~~y Z5f ‘/93 -/7,5 - -

4’~zô ,&h& /Zg ,o7’ f.Z1 . t33 7,~ 126 ,59g-zc i2~f , 1,.92i- ~ ~ /g.c~q:3o 0o5 ,q.g5 4~L 7~fl.. /7~ /c,~ C,~ni’JoIJ3[c~t.eroY.J

‘Y;iT /o.≤o /12 ~‘7 1/~~@ P3/ 7,7’? /‘I& /2J’ O/’CI oX ~iot~/ ,. ,‘

‘twp /O,~& //~. .oe-( /~,93 •~1Z~1 774’ /34(≤ /4/~3‘f4g~5~ /Q.&o il~ .o3 //~% PyZC 7~ —izCL1.-~O iz,c~l 3q13 7.~g /7Z6 [‘2iI’SS /O.bD //(~ O,00 //.~L) ‘~LL 7~ /3.5’S . ~‘A)nipk cd <;~v

Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 mtJMinWater Level +- 0.01DO +- 10%Turb +-10%

mLIFt infonnatlon3/4 In well = 87 mL/Ft2 in well = 6l7mUFt -

4inwell247OmLIFtCond. + 3%pH +- 0.1eH +- 10 myTemn. +- 0.1

Eli Correction for A9IA9CI probe:Add 190 mV to ORP value

Samplers:

Record all instrument calibrations InInstrument Calibration Log Book or Field Book j. ________

Date Revfld 1/28/2002

Page 24: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

‘(2a’-.weU# 41W5’

Date 10 20 ZDI~Z

Static Water LevelBeqin Time of Purge

EquIlibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 mLJMinWater Level +- 001DO 4-10%Turb ~-10%Eh Correction for AgIAgCI probe:Add 199 mV to ORP value

Write Meter Number of Instrument Used

Time Water Level Flow DO Temp. Cond. pHMm Feet below MP I mtJMin mg/L Celcius -Ioq(H+] I mV NTU

Monitoring Well Purge and Sample Data SheetSite Name a Jf-caiv ~~ a L

Total Depth ‘5’. Wel Diameter .—

Screen Interval — Formation ..— Sample Device ó4nøs.y /vc.r ~ ‘t .*~

ORP Turb. t4t~ ~

Comments

~Q n~Ig/l:i5 /1.30 Zfl//kU.a 22 ¶9 a3~’8 ~:z i273 ó~’T113.3 11:7-9 rzMi~a 7,2 9~LJ .313 Y.SL 1327 3.7≤‘L’is jr~ fOtJ/~ 11.9 (0.33 .3cL ~ ec~ 2.15

ThuD /1.29 132MIrn~ ~,( 350 ~.r7 13143 2./g/j,tj5 Il~2’1 ~t~m,rq ~‘fl -319 w1i) ,ti~ 3od

ii ‘112. ~ 9 ‘~ )3.~45 .3118 s~.y~3 iVi 7 2~o3irS3 ~I ~&/h1E~~J /2.0 ic qg ..3qg L,cfg 1q10 14ss/2:oo i),2’t ~fS/n~1y1 n.j Ifl.’-17 t3Y3 7.’~7 IHZA (‘IT

mLJFL InformationSf4 in well = 87 mlJFt2 in well = 6l7mtJFt4 in well = 2470 niL/Fl

Cond. +- 3%pH +- 0.1OH +- 10 myTemp. +- 0.1

Samplers:12/ 41

Record all instrument calibrations ininstrument Calibration Log Book or Field Book

Laboratoty Sample NumbersAnalysis? Depth Number

Date Revised 1/28/2002

Page 25: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 rniJMinWater Level +- 0.01DO.- 10%Turb +- 10%Eli Correction for A91A9CI probe:Add 199 mV to ORP value

mL’Ft Information3/4 in well = 87 mL/Ft2 in well = 617mL/Ft4 in well = 2470 n,LJFI

Laboratory Sample NumbersAnalysis / Depth

weii# 2-iU -113Date /0 20 /5Static Water LevelBegin Time of Purge

Write Meter Number of Instrument Used

Time Water Level Flow DO Temp. Cond. pH

Monitoring Well Purge and Sample Data SheetSIte Name ≤.eiV ~≤Lp€ ‘LuSTotal Depth 5 1 - S wei Diameter ~

Screen Interval Formation — Sample DeviceORP Turb.

lvlin. [ Feet below MP mLiMin mgIL Celcius -log[H+1 I mV [ NTU

•1

54ij~& ii.

g4>4rEOF *t

Comments

iz’2~S q-’5L!z~;O c7360 léo/~,,-,j 37~ /2.05 ~ 66! /13ii 35 q~ /067M,J ~~7/O~ 12,2-q 0~q ( a.c2 (57 ~tZ:’-iD ‘7..t67 /os~op’.J 1.77 12,25 a/U &ze ~~zz 233,2~16 q~eg /og/kn,% i,o~j jz,i5 •,58 &.Lq /~g,7 ~

Iklg-rI<hc_~pifr-e5a-vr~pkd_c~iz~c&

5Prn’iplC_a.*_,a;55

Cond. +- 3%pH +-0.1eN +- 10 myTemp. +- 0.1

SamplQrs:IL~L

Record all Instrument calibrations inInstrument Calibration Log Book or Field Book

Number

Date Revised 1/28/2002

Page 26: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Flow 1-2 mlJMinWater Level +- 0.01DO.- 10%Turb +-10%

Laboratoty Sample NumbersAnalysis / Depth

w.iw mflw—558Date

Static Water LevelBegIn Time of Purge

Time Water Level

Monitoring Well Purge and Sample Data SheetSite Name EaSk4er~i ≤u~PLc,~S

Flow

Write Meter Number of Instrument Used

Total Depth 9~ . 35 Well Diameter

Screen IntervalDO Temp.

Mm. Feet below MP mi/Win rn~IL Celcius II -k~(H+j I iN NTU

— FormationCond. pH ORP

Sample Device £COfL4~7y2r~Turb.

gslU4 ON4fe*

~ ~1~U(’””•~ S

401

Comments

i:3≤/‘ qo g,43 aagJn~ J?3 /231 4q~~ 751 ‘~7S 5 37pLq5 r≤z. ~/7 /2Y7 ,q~0 /q4,~, 33~J.~O /O./j ~ ~iL~1 12.5g OL1≤~ 7.6/ %7Z 3I4’~

j~,5 9#/MnJ .!& /Z~’U .44’l 772- zo~~≤ ‘L3SZoO -i~°k~ o--hwt ,i~ c,’/Thq/ ~jvi5 r~ /tL≤ /otq~2. 2G /h.l/7 50

7:1-7

Z.zg ,12.ttS

210 /057 s2/n~erj .52- ia.q~ ~iig 7,47 z/~. ç~. 35 .o4( 4~7/~,v 03.) ,‘/ZZ- 761 2o~ ) L/,f7~ /nh( ~ijø~ .5/ ~z4f 2/7 3,6’13~.Lj5 /0.44 *SqwI ,~z... i2~s ~ 7&e jô3 3.78

O41~’j

EquIlIb.lum Goals3 consecutive readings 3-5 mm. apart

mLJFt Information3/4 in well 87 mi/Ft2 in well = 61 7mL/Ft4 in well 2470 niL/Ft

Cond. + 3%pH +-ftleH +- 10 myTemp. +- 0.1

Eh Correction for A9IA9CI probe:Add 199 mV to ORP value

Samplerslit ~—C(.

Record all Instrument calibrations InInstrument Calibration Log Book or Field Book

Number

Date Revised 1/28/2002

Page 27: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Well# 4Q~/—5q’ Monitoring Well Purge and Sample Data SheetDate /0/ zo/ccStatic Water LevelBegin Time of Purge

Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 mL/MinWater Level +- 0.0100.- 10%Turb +- 10%Eh Correction for AgIAgCI probe:Add 199 mV to ORP value

Laboratory Sample NumbersAnalysis / Depth

Time Water Level Flow

Write Meter Number at Instrument Used

Site Name jC~ss~ 5~vic ‘Lc’STotal Depth ____________

Screen Interval ~ FormationDO Temp. Cond.

Mm, [ Feet below MP I mLMin rnq/L Celcius IL -log[H+1 I mV NTU

pH

Well Diameter

- Sample Device lc~o~k7/ycsTurb.ORP

—~ -~

ii. I

OF

Comments

.tai,1 CA / ~-,,,tt,

i~

5~Z5 ~ .A~ ii 07 O3BZ 235 -6Y4 it~~ 73R —thi.~i /8-

≤~ ;≤ ‘, 1o4 ~39o -Z57 ~ zojy≤!4) 113 /O6 . ~i ii ‘-i7 31’r’ 7.57 —gc.& /5~5~~~‘*≤ OIJL/ ~/,Ijej 7~3€ -7≤~’ 9~S3“~~;o 9-83 •H3 /jg7 1g7 ‘?.3~ 80.4 téLtcC q~g log ~iO 4L4-3 ~qç, 7sT 663 7.76~ -7S3 /10 -‘it 3g9 73g ≤‘1 7<08

I

Cond. +- 3%~H +-0.1eH +- 10 mVTemp. +-0.1

mlJFt Intonnatlon Samplep:3/4mnwell=B7mUFt (?c2 in well = 617mL/Fl ________

4 in well =2470 nt/Ft ________

Record all Instrument calibrations InInstrument CalibratIon Log Book or FIeld Book

Number

Date Revised 1/28/2002

Page 28: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Well#Date /O/2o/ ao,3Static Water LevelBeqin Time of Purge

Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 rnL/MinWater Level +- 0.01DO +-10%Turb +- 10%Eli Correction for AgIAgCl probe:Add 199 mV to ORP value

mLJFt informatIon Samplers:314 in well — 87 mL/Ft _________

2 n well 617mL/Ft ________

4 in well 2470 mlJFt ________

mw-5o13L

Time Water Level Flow

Monitoring Well Purge and Sample Data SheetSite Name ,r44 k2,K \ cv1-z a lvçTotal Depth 11/

WrIte Meter Number of Instrument Used

Well Diameter

Screen Interval t~- FormationDO Temp. Cond. pH

Mm. FeetbelowMP mL/Mmn rng/L Celcius -loq[H+j [ mV Nfl.)

ORP

1~

fl!.f’~~. .;~ht~t ~

Sample Device 7yci~’Tuyb. ‘4r~ OF

Comments

c34 iVJ/~~.~ /“-/?% 9 7’~ •3d9 9OL z~y[≤CLl5 /2~f~O /~‘1’~/,b~ !2.≤ it)-1’-I ~3~fi S~76 je? 6799.3<’ H.1~ L7.S5 (“‘~J o)Yf ‘? 91~ I ~ 7.7~’9f~3 1s •~

Cond. +- 3%pH +~0.1eH +- 10 myTemp. +.0.1

Record all instrument calibrations InInstrument Calibration Log Book or FIeld Book

Laboratory Sample NumbersAnalysis I Depth

nwt4Lrj

Number- 5~ L

Date Revised 1/28/2002

Page 29: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

WelI#

Date

Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 mLIMinWater Level +- 0.01DO +- 10%Turb.+- 10%Eh Correction for Ag1AgCI probe:Add 199 my to ORP value

niL/Ft information Samplers:3/4iriwell=B7mL/Ft 4632 in well = 6l7mLfFt4 in well = 2470 niiFt

Sample Device ~Lo, JrV

Turb.

Laboratory Sample NumbersAnalysis / Depth

Ps o’s,t~n4L

Monitoring Well Purge and Sample Data SheetSite Name £SCT / O€P cMtOI2fIS&4-t?S

Static Water Level (~(.c C Total Depth Y3, r~ Well Diameter —

Begin Time of Purge ~ Screen Interval .— Formalion —

Time Water Level Flow DO Temp. Cond. pH ORP

WrIte Meter Number of instrument Used

Miii. j Feet belowMP I mLiMin nng!L C&cius II -log[H+] I mV I NTU

Comments

1C17- I~D

i~ r3.’( n.’ c~at2~ ~ ~“i.c’ 71,1- - /

V~U3 (~oS 39 v~ I1.3ç~ o.~9i ~j•oi- ~ji.c~ (°2

njc trrj 7~a~ ,0.sr ~ ~ ‘isfl- g~i- 4t

Cond. +. 3%pH +- 0.1eH +- 10 mVTemp. +-O.1

Record all instrument calibrations inInstrument Calibration Log Book or Field Book

Number& (This’

Date Revised 1/28/2002

Page 30: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

WeU#Date

Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 mLJMinWater Level 4— 0.01DO +- 10%Turb +- 10%Eh Correction for Ag!A9CI probe:Add 199 mV to ORP value

Laboratory Sample NumbersAnalysis / Depth

y~c. 6n~,V41a~-L-’

Static Water Level 0j~ ~(Begin Time of Purge (~ ~. e

Time Water Level Flow

Monitoring Well Purge and Sample Data SheetSite Name (5 CT ~/ i~6O~y~4,t-ifj

Write Meter Number of Instrument Used

Total Depth ~ Well Diameter

Screen Interval -

PC Temp. Cond.Mm. Feet below MP I m[JMin rng/L Celcius ~I -loc[H~] I mV I NTU

I ‘1A -‘~c

~1

FormationpH

-r

ORPSample Device

Turb.

Comments

_____ ~

I39~ 9if3 3Cr (L?yz o..3~ 1J? I -~ tf(,~~ ~‘~°

(3S) ci ~Q ~ 11,fl o, 7.3f — iiz~ j4o3i35~ Cj 9$& too ~ ~10 IL.c5 O,iz~ 7.31 11W7 I.CtIj 9°i ~.ac fl..q o.3~ 7,~9 - 1oa3Ho 6 T. ~‘ . ~ Ltfl- L.N48

ri Il 9, ~~t3 Lj, ~ u.c.~.. o.)~’1y T,c~9i rt.-~ i~n19r( ~fCfL( 5.kj ‘I.G5 ‘~.41 o..)33 (O.$9 .- 3I.~N~ C19ç Ilc,~y o,22e ~.e’i —22-r ~~qa’ c1 •-~- ((.33 ii,.~i 0.~ C..~l -. i’-j.O

P-~aj ti.çr 1°c. ll.6S °.~L’5 (~,.~t1$ — 1.31

~ cj ç~ c.u fl.5~t O.QI° Li-) ti,9~tpi ctsy o’.> 3.38 jt.’17- O.Qo2 C.t0(- ~5’.r ~•fl(<(35’ 9,5€ ~r’t~ ô.~°1 C.c”~ .17.3 o.3I~-q~7 cUss (oo -ç. gcz ‘1.39 a. l7~ 0.53

i ~i’1° °t jc~ (00 II 39 ~.i’j3 -3çr O.~SIL.(t() 9.y8 3.SS IL-3d 0 19 C.t~ ?‘t.5 OJL

uhL ~i. r~ i L.I-~O o. I ~‘J C, Go ~ ‘(L? 0.1-1iLrfl ~. ss Lf.Jjç ft. ~a o. en L.r~- t. fl

Lqca ~..çg Co~ ‘1.3’ it.~3 o.rs-c C.s~ ~fl./

mL/Ft information3/4 in well = 87 mlJFt2 in well = 617mL/Ft4 in well = 2470 niL/Ft

Cond. +- 3%pH +-0.1eH +- 10 myTemD. +- 0.1

Record all instrument calibrations inInstrument Calibration Log Book or Field Book

Number6 ILfS7

Date Revised 1/28/2002

Page 31: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

WeII#Date

Static Water LevelBegin Time of Purge *‘:J r

Equilibrium Goals3 consecutive readin~is 3-5 mm. apartFlow 1-2 mLJMinWater Level +- 0.01DO +- 10%Turb +- 10%Eli Correction forAgIAgCl probe:Add 199 mVtoORP value

Monitoring Well i-urge ana ~arnpie isata oneetSiteName Ott’ /~~1coDy~mPj

mLIFt Information3/4 in well = 87 mIJFI2 in well = 6l7mLIFt4 in well = 2470 mL/Ft

Sample Device (r..€4 (UTurb.

Laboratoty Sample NumbeisAnalysis I Depth

Vo~ r

o:s &~4<.

Time Water Level Flow

Write Meter Number of Instrument Used

DO

Total Depth

Screen intervalTernp.

3o. ~( Well DiameterForrilalion

Cond.Mm. I Feet below MP I mLJMin mg/L Celcius II -loq[H-’-] I mV I NTU

pH ORP

~1’ Comments

_________ I

SW 7.87 SO.C~I 94o Cjq~ ?3~ ~ ~.s~c’ c~t.’~,no cj~t

03fl 15Th ≥‘-t~3 t.°~ ~ 7.3 18t8 *~cy~~sc 7. v~ a). ‘~ q ~OGz CJ.~’N :j3~ I ~ C.rf≠O’100 7.S2 Rt.sm tt.~Y7 o.219 ;~~a ity.~oqo5 ~I.57 9.11 0)93 ?.3. I ~

Cond. +- 3%pH +- 0.1eH +- 10 mVTerm,. +- 0.1

Samplers:

Record all Instrument calibrations InInstrument Calibration Lon Book or Field Book

NumberS~~(.Ae o~oS

Date Revised 1/28/2002

Page 32: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

WeIl#Date

Static Water LevelBegin Time of Purge j) ~

WrIte Meter Number of Instrument Used

Equilibrium Goals3 consecutive readinqs 3-5 mm. apartFlow 1-2 mLIMinWater Level +- 0.0100+- 10%Turb÷- 10%Lb Correction for A9IA9C1 probe:Add 199 mV to ORP value

niL/Ft Information Samplers:3/4 in well = 87 mLfFt _________

2 in well = 6l7mLIFt _________

4 in well = 2470 mIJFt

Laboratory Sample NumbersAnalysis / Depth

A/s ~g<r~ rn.

Time Water Level

Site Name (SLYMonitoring Well Purge and Sample Data Sheet

Flow DO

Total Depth ~‘3~ V~( Well Diameter

Screen IntervalTernp.

- fll

Mm. j Feet below MP mLiMin mg/L Celcius .11 -loq[H+] I mV I NTIJ

— Formation — Sample Device &-c3 1e,ji%

Cond. pH ORP Turb.

Comments

1135 /OI~~ q-o ~c45f /“tl ~44~ B.°~ 1314 ,.{lIfl ‘°~sC 7s 5-3.51 .. f~.qg O.3tc 3’.oq f3tY c.’( ,.q~ fjt~...._tiir p. g3 3o 5°.13 (~).Y9 o.3gç &. 1° (39.2 L’Ii~~y fl.s.2 4fl~J

a13__0Li_- c

Cond. +. 3%pH +- 0.1eH +- 10 myTemp. +- 0.1

Record all Instrument calIbrations inInstrument CalIbration Lou Book or Field Book

Number&.//q7.

Date Revised 1/28/2002

Page 33: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Monitoring Well Purge and Sample Data SheetSlteName ESCt /D~P 1t1,~UDY&EtttfS

Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 mLJMinWater Level +- 0.0100+- 10%Turb- 10%Eli Correction for AgIAgCI probe:Add 199 my to ORP value

mLIFt Information Samplers:314 in well = 87 mIJFI ________

2 in well = 6l7mLJFt ________

4 in well = 2470 mI/Ft

Laboratoiy Sample NumbersAnalysis I Depth

I.JDL,D~. i~i/W ,&14 k(

NumQ~rS

WeIi#Date 7a ~

Static Water Level

Begin Time of Purge ~aD ‘~

Time Water Levei Flow

12. )~j~j Total Depth ~%. o1 Well Diameter

Write Meter Number of Instrument Used

Screen IntervalDO Temp. Conci.

Mm. Feet belowMP I mL/Mmn n’~gIL Ceicius II -log[H+] I mV I NTU

Formation — Sample Device_________pH ORP Turb.

Comments

/~-fl (3.jcs 7O ~,i h.c<~ c’~~ct Z~2 5.j’~I)~~ i3.fl to5~ (471- ~ o.253 2.r, —8i.~~

‘~9I r3.tU I1.C-t r..i9’( o.22-° ~. 17 °Ti.°1~1’tj 9.L2 ‘c9.Th1 0.271 7~e~ ~ ~~i- I3.t~ q3 (,.~ i~1-c ~a13 7~i’~ -~-ç a:g3ilZD r3.’43 rj r.,~1 i°3i Ofl~( ~ —89.’ i:?-’r(253 (3L{3 ~‘9 3o’~ IoJ~rL( ctfl 3.\3 — frkL9 ~n~&t3.JC ~3”(M 59 S-~~g lo.c~3 ~ ~.ar -&&c t,~-it2~57 i~, C .t~ (o.L’~ o.~1 Th~19 —73c i.’~(3o~ (3 i4~.( C. 5? 1~.cc~ o.3~ 7J3t~ — ~oz~ j (,~j

13tC (3Lj~L( (~.,3( (c.7-3 ~ ~ ~‘.° L.5%

~ ~ SoL (c’}3 o~2s3 ~ .-72.’( ~, cjty

(311 (LW 5.IS jo.~( o.?fo 7.32.. 17-a LS~5tDi’i 13.9f ~ S.U- (oJ7-o O.2~fl 1.33 -17.3 l.s~i

Cond. +- 3%pH +- 0.1eH +- 10 myTerrn. +- 0.1

4c0

Record all instrument calibrations Ininstrument Calibration Log Book or Field Book

Date Revised 1/28/2002

Page 34: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Time Water Level Flow

WrIte Meter Number of Instrument Used

EquilibrIum Goals3 consecutive readinqs 3-5 mm. apartFlow 1-2 rnL/MinWater Level ÷- 0.0100+- 10%Turb +- 10%Eli Correction for A91AgCI probe:Add 199 mVto ORP value

mlJFt Information3/4 in well = 87 mLiFt2 in well = Gl7mL/Ft4 in well = 2470 niL/FtRecord all instrument calibrations In -

Instrument Calibration Loq Book or Field aooic

Laboratory Sample NumbersAnalysis / Depth

p< &4jPISI 4 ‘4

NumberM’ /ut~.~ c2

Static Water Level IBegin Time of Purge I ~t

>~Well# fV\ ‘J — ~7-~ t3 ~ Monitoring Well Purge and Sample Data SheetDate Site Name ec~--~ / Os M~QOY~6A4Pj

Total Depth lo ~‘.4w Well Diameter

Screen Interval —~ FormationDO Temp. Cond. pH

Mm. j Feet below MP muMin rng/L Colcius II -k~[H+1 I mV I NTU

__________Sample Device d’c~ ~

ORP Turb.

Comments

9:2~ ,3ss ~ ~3.u ~ I3.~2 ffl3 (o~ — ~

M:23 j’f.25 cl.t, 3:;.3l ~o. t.~S U.i-3 j13o3 — ‘~S-f.9 C(i,.

92~ I1.~’1 ‘3S~’•Z~\- lo.n. ~iii ~ -Ifl~ç W5L4 ,1~c t~.J

‘-L3’~ t5.°°’ ?z.in (O.°S li.12. l3.~~3 -(SLJtcbic ~ .

Cond. +- 3%pH +- 0.1eH +- 10 mVTemp. +- 0.1

Samplers:

Date Revised 1/28(2002

Page 35: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

f•r

___________Sample Device C≤ta( -3’.12

Turb.

-~ - Comments

Equilibrium Goals3 consecutive readings 3-5 mm. apartFlow 1-2 rnL/MinWater Level +- 0.01DO.- 10%Turb~- 10%Eh Correction for A91A9CI probe:Add 199 mV to QRP value

mi/Ft informatIon3/4 in well = 87 mi/Ft2 in weD = 6l7miJFt4 in well = 2470 rnlJFt

S am P lo rs A Laboratory Sample NumbersAnalysis / Depth

‘2<. &a~

Number c:~ (5? 1.{3

WelI#DateStatic Water Level ~, 3 *Begin Time of Purge ti-3 (~

/ Monitoring Well Purge and Sample Data Sheet

/ SiteName £scT / P~.P ,~i~pOYt~C&i.t’JTotal Depth ‘1-~’i Well Diameter ___________

WrIte Meter Number of Instrument Used

Time Water Level Flow DO Temp. Cond. pHScreen Interval Formation

Mm. j Feet belowMp mi/Mm rng/L Celcius JI -lon[H+1 ITN NTU

ORP

rtt,~. z.~i .r~. iy I~.i-~ o~’jiq I-i,~~-9 - —~ ~ V2.17-5( ~o3 lao ~ lt-€~ o.~Q l[.€~~ ~-i3-l &.~.!

flsi~ S’.&3 23~9 1L4-° oz~r i~,’i° -2LSLfrnj 7. ‘~3 c$si?i~ 2.0. ii cUc~ ~.iPi 9.R-S —t.2.D &JCTtP°p ~ ()Ô Il.dli ø.(Q~- O~j~ ~

{SDC ~J’.(~g [IA-I b.i59 g~fl ~c~~a6 ~ w.ace ((9~ ô.jqs gij

1913 3. Cj (L~a o.c3) ?-.‘I’ ?~ i.i~rst~ ~ n.~ O.jar ~ H2.7- z.~g{3l’~ ~ i’ia Oai2~Z 7-.o3 qL’.y

(“P.R F..C.3 [2~ ç,c’G. ~ eLi IC’ (dAd Q.’1i-‘82w laz Ok f~2 ‘.3~ .s~(~3 g.(~~ts( 12-U .c~? IL_fl o If° G. C~’i ~&. ~

tt3c~ ci ~‘.°k ri-St2 .~(°Q ~ ~2 ~.5’jL34~ ~ ~3 s.di— ~t, o~ioG ‘-58 C~f I

~-3+ c~ - 5.21- I L55 ~ G~.S’k c.’~ç (.51-t’(° tG3 Ia.s S’15 p.~ “~ ~ ~c-C.$:;t.t3 ~ c. i2_ U4t.{ ~ cc.7

Cond. +- 3%pH +~0.1eH 4— 10 mVTemp. +- 0_i

Record all instrument calibrations InInstrument Calibration Log Book or Field Book

Date Revised 1/28/2002

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APPENDIX C

MEDEP Data Validation Checklist

Narrative - 2014-2015 Intra-well trends

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Maine DEP Basic Data Review Checklist

Revision No.:00

Effective Date: 3/7/14

Page 1 of 5

Site Eastern Surplus, Meddybemps

Project

Date(s) Sampled or Sampling Event 10/20/2015

Reviewed by Campbell Environmental Group

Date Reviewed 12/11/2015

A.  Data Completeness

Item for Review Reviewer Comments

Did report include original lab reports? X X *

Was report paginated? X *

Were all report pages received? X *

Did report contain results for all samples and analyses 

requested on the chain of custody form?X *

Were required QA/QC results included with lab report? X *

Was EGAD EDD received? X *

Were required QA/QC results included on EGAD EDD? X *

Did reported analyte lists meet project specifications? X *

Did reporting limits meet project specifications?PQL and MDL for Manganese, 1,2‐Dibromo‐3‐Chloropropane, 1,2‐

Dibromoethane, and Vinyl Chloride, exceed applicable regulatory guidelines* X

Was the laboratory Maine certified for all 

methods/analytes/matrices performed at the time of 

sample analysis(if required)?

X *

*For all items checked N‐ contact chemist, lab or consultant for resolution

B.  Preservation and Technical Holding Times

Item for Review Reviewer Comments Yes

If No, put X in box 

then click button

Sample cooler within required temperature range at time 

of receipt at laboratory(if No, enter receipt date and 

cooler temp in reviewer comments)?

X 1

Samples properly preserved at time of receipt at 

laboratory?X 1

Was sample extraction/digestion performed within 

holding time?X 2

Was sample analysis performed within analytical holding 

time?

Re‐analysis (dilution) of sample ESLT‐GW‐MWRP‐1015 was required but 

conducted 11 days out of hold time.  2 X

(1) Review SAP/QAPP requirements, if unavailable use professional judgment to flag data as estimated “J” or as unusable “R”

(2) Review SAP/QAPP requirements, if unavailable,

     If method HT<sample extraction/digestion/analysis time<2X method HT, then estimate data and flag with “J”

     If sample extraction/digestion/analysis time>2X method HT, flag detections with a “J”, flag non‐detects as “UJ” or reject data and flag with “R”

Yes No

No

No

No

No

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Maine DEP Basic Data Review Checklist

Revision No.:00

Effective Date: 3/7/14

Page 2 of 5

C.  Blanks

Item for Review Reviewer Comments Yes No

Were blanks run at the frequency specified by the 

method or SAP/QAPP?X *

Were target analytes detected in laboratory method 

blanks?

Methylene Chloride was detected below the reporting limit in Method Blanks 

WG172846‐2 and WG172905‐2X

Were target analytes detected in trip blanks(if 

applicable)?  

Acetone (> 2X rl), ethylbenzene, mp‐xylene, methylene chloride (<2x rl), and o‐

xylene, were detected in the VOC Trip Blank at concentrations exceeding 

corresponding reporting limits.

X

Were target analytes detected in equipment blanks (if 

applicable)?No equipment blanks were collected X

Were target analytes detected in any other types of 

blanks included in the laboratory data report?X

Was data appropriately qualified for blank 

contamination?X 3

*Contact chemist, lab or consultant for resolution

(3)Review SAP/QAPP requirements‐ if unavailable see Attachment A

D.  Surrogates

Did the laboratory report results for surrogates (if 

required by the analytical method)?*

If surrogates required were recoveries within acceptance 

ranges?

If surrogate recoveries were outside acceptance ranges, 

did the lab re‐analyze to confirm matrix interference?*

Was data appropriately qualified for unacceptable 

surrogate recovery(if required)?4

*Contact chemist, lab or consultant for resolution

(4)Review SAP/QAPP requirements, if unavailable:

    If recovery > higher acceptance range, flag associated detects with “J”

    If lower acceptance range > recovery > 10% (20% for volatiles), flag associated detects with “J” and associated non‐detects with “UJ”

    If recovery <10% (20% for volatiles), reject associated data and flag with “R”

Item for Review Reviewer CommentsYes If No, put X in box then 

click button

If Yes, put X in box then click 

button

X

X

No

X

X

Yes

Yes

Yes

Yes

No

No

No

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Maine DEP Basic Data Review Checklist

Revision No.:00

Effective Date: 3/7/14

Page 3 of 5

E.  Laboratory Control Samples (LCS/LCSD)

Item for Review Reviewer Comments

Did the LCS include all spiked compounds as required by 

SAP/QAPP or method?X *

Were recoveries within acceptance ranges? X 5

Was data appropriately qualified for unacceptable LCS 

recovery?X 5

Were RPD between LCS and LCSD within acceptance 

ranges?No LCSD samples were analyzed.   X 6

*Contact chemist, lab or consultant for resolution

(5)Review SAP/QAPP requirements, if unavailable:

Organics and wet chem: If recovery > higher acceptance range, flag associated detects with “J”

 If recovery significantly <lower acceptance range, reject data and flag with “R”. 

VOCs and SVOCs marginal sporadic exceedences (ME) allowed.  The number of allowable marginal exceedances is as follows:

1) >90 analytes in LCS, 5 analytes allowed in ME of the LCS control limit;

2) 71–90 analytes in LCS, 4 analytes allowed in ME of the LCS control limit;

3) 51–70 analytes in LCS, 3 analytes allowed in ME of the LCS control limit;

4) 31–50 analytes in LCS, 2 analytes allowed in ME of the LCS control limit;

5) 11–30 analytes in LCS, 1 analytes allowed in ME of the LCS control limit;

6) <11 analytes in LCS, no analytes allowed in ME of the LCS control limit;

Marginal exceedances must be random and in no cases can the %R be <10%. If the same analyte exceeds the LCS control limit repeatedly, it is an indication of a systemic problem. 

The source of the error must be located and corrective action taken.

Qualify results that are ≥ MDL as estimated low “J”,

Qualify non‐detects as estimated “UJ” 

Upper acceptance limit<Aqueous/Water and 

Soil/Sediment %R < 150% Qualify results that are ≥ MDL as estimated high “J” 

%Recovery < 40%  Qualify all results as unusable “R”

%Recovery > 150%  Qualify all results as unusable “R” 

(6) Review SAP/QAPP requirements, if unavailable use professional judgment to flag data as estimated “J” or as unusable “R”

F.  Matrix Spike Samples (MS/MSD)

Item for Review Reviewer Comments

Did the MS (if performed) include all spiked compounds 

as required by SAP/QAPP or method? WG172846‐5, MS ‐ WG173026‐4, WG173026RA X *

Were recoveries within acceptance ranges (if MS 

performed)?X 7

Was data appropriately qualified for unacceptable MS 

recovery (if MS performed)?X 7

Were RPD between MS and MSD (if performed) within 

acceptance ranges?MS/MSD ‐ WG172846‐5 & 6 X 7

*Contact chemist, lab or consultant for resolution

(7) Review SAP/QAPP requirements, if unavailable use professional judgment to flag data as estimated “J” or as unusable “R”

Metals: 40%<Aqueous/Water and Soil/Sediment %R 

<lower acceptance limit 

If No, put X in box then 

click button

YesIf No, put X in box then 

click button

Yes

No

No

No

No

No

No

No

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Revision No.:00

Effective Date: 3/7/14

Page 4 of 5

Item for Review Reviewer Comments

Yes

Were lab duplicate or field duplicate analyses performed 

(if yes list type in reviewer comments)?ESLT‐GW‐IN1B1‐1015 and ESLT‐GW‐MWRP‐1015 are Duplicate samples X

Were RPDs (if applicable) within acceptance ranges?

Aluminum, chromium, copper, nickel, selenium, and vandium, were outside of 

the acceptable RPD of 30%.  Arsenic and cadmium were outside the RPD but 

less than 2X the QL

X 8

(8) Review SAP/QAPP requirements, if unavailable:

Qualification of Organic Analytes in Lab or Field Duplicates Situation 1: Positive Detects in Both Lab or Field Duplicates

Aqueous ≤ 30%RPD Non-aqueous ≤ 50%

Sample Results Both Duplicates ≥ 2xSQL

Detects No Flag

Non-detects No Flag

Situation 2: Positive Detect in Only One Lab or Field Duplicate Sample 9

Sample Results One Sample conc. = ND (or value reported as less than the SQL) SQL < Other Sample Conc. < 2 x SQL

Detects Professional Judgment

Non-detects Professional Judgment

(9) RPDs should not be determined for duplicate pairs in this situation.

Qualification of Inorganic Analytes Based on Lab or Field Duplicates – Aqueous Matrices

Sample Results

RPD ≤ 30%Detects No Flag

Non-detects No Flag

(10) No action is taken when both field duplicate results are positive detects < SQL or are non-detects.

 G.  Duplicates (Note this also applies for analytes reported by more than one method)

Non-Aqueous Lab or Field Duplicate Sample Results

Both Duplicates

Both Duplicates ≥ 2 x SQL

UJ

J

Aqueous > 30%Non-aqueous > 50%

If No, put X in box then 

click button

Professional Judgment

NA NA

Aqueous Lab or Field Duplicate Sample Results

Both Duplicates ≥ 5 x SQL

J

UJ

RPD > 30% Abs. Diff. ≤ 2 x SQLNo Flag

UJ

One Sample conc. = ND (or value reported as less than the SQL) Other Sample Conc. >2x SQL

J

NA

Abs. Diff. > 2 x SQL

One or Both Duplicates < 5 x SQL10

One sample conc. > 2 x SQL SQL < Other sample

conc. < 2 x. SQL

No Flag

Professional Judgment

SQL < Both Duplicate samples concs. < 2 x SQL

J

No

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Revision No.:00

Effective Date: 3/7/14

Page 5 of 5

Qualification of Inorganic Analytes Based on Lab or Field Duplicates - Non-Aqueous Matrices

Sample Results

RPD ≤ 50%Detects No flag

Non-detects No flag

(11) No action is taken when both field duplicate results are positive detects < SQL or are non-detects.

H.  Data Usability

Item for Review Reviewer Comments

If Yes, put X in box 

then click button

Is there any reason to suspect carryover? * X

Is there any reason to suspect matrix interference? * X

Do chromatograms (if provided) look reasonable? Not Provided  * X

Is there a compound detected below quantitation limits 

that should be noted?

Per MEDEP request, compounds detected  below the SQL but obove the MDL 

have been reported and approrpirately qualified.  X

Is there any other reason that the data should be 

qualified?See above.  X

Was all (or most) data qualified for a particular method 

or analyte?

Numerous analytes were consistantly J flagged becaused they were reported 

below the SQL.   * X

Was any data rejected during the above review?  * X

Is data quality sufficient for the intended 

use of the data?X *

*Contact chemist, lab or consultant for resolution

Both Duplicates ≥ 5 x SQL

Non-Aqueous Lab or Field Duplicate Sample Results

Abs. Diff. > 4 x SQLJ

UJ

Abs. Diff. ≤ 4 x SQLNo Flag

No Flag UJ

RPD > 50%J

If No, put X in box then click 

button

One or Both Duplicates < 5 x SQL11

Yes

Yes

No

Yes

Yes

Page 42: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

APPENDIX D

Laboratory Report

Page 43: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Appendix C Intra-well Trend Narrative Page 1

Intra-well trends 2014-2015

It should be noted that the October 2015 sampling data was reported down to the laboratory’s respective

minimum detection limits. As a result, a greater number of volatile organic compounds (VOCs) were

detected, however, it is difficult to evaluate these detections in relation to previous data and

concentrations that were below the laboratory’s practical quantitation limit. Therefore, much of the data

should be considered estimates.

VOCs

IN7B - Concentrations appeared consistent with May 2014 sampling results. Similar to the 2015 results,

tetrachloroethene was the only analyte detected at concentrations above applicable regulatory guidelines.

While the concentration of tetrachloroethene in well IN7B increased between May 2015 and October

2015, concentrations of several additional compounds detected below regulatory guidelines decreased

during the same time period. No additional compounds were detected at concentrations exceeding

applicable regulatory guidelines.

IN1B - Concentrations appeared generally consistent with May 2014 sample results. In May 2015, four

compounds were detected at concentrations exceeding applicable regulatory guidelines (Cis-1,2-

dichloroethene, tetrachloroethene, trichloroethene, and vinyl chloride). In October 2015, only

tetrachloroethene, trichloroethene, and vinyl chloride were detected above corresponding regulatory

guidelines. The detected concentration of tetrachloroethene increased from 330 micrograms per liter

(ug/l) to 600 ug/l between the two sampling periods, while concentrations of additional compounds

decreased. No additional compounds were detected at concentrations exceeding applicable regulatory

guidelines.

IN-1B2 - Concentrations appeared consistent with May 2014 sample results. In May 2013, three

compounds (cis-1,2-dichloroethene, tetrachloroethene, and vinyl chloride) were detected at

concentrations exceeding regulatory guidelines. Concentrations of tetrachloroethene and vinyl chloride

were also detected above corresponding guidelines during the October 2015 monitoring event, however,

trichloroethene was also detected above corresponding regulatory guidelines in 2015, while cis-1,2-

dichloroethene was not. No additional compounds were detected at concentrations exceeding applicable

regulatory guidelines.

MW-3B - No VOC concentrations were detected at concentrations exceeding corresponding regulatory

guidelines during the October 2015 monitoring event. In May 2014, tetrachloroethene was detected at 14

ug/l, exceeding applicable guidelines.

MW-23B - In May 2014, cis-1,2-dichloroethene, tetrachloroethene, and trichloroethene were detected at

concentrations exceeding regulatory guidelines. VOC concentrations decreased at this location during

the October 2015 monitoring event, however, concentrations of tetrachloroethene and trichloroethene

continued to exceed corresponding regulatory guidelines. No additional compounds were detected at

concentrations exceeding applicable regulatory guidelines.

rob.n.peale
Sticky Note
The intrawell trend narrative needs to be moved to Appendix C.
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Appendix C Intra-well Trend Narrative Page 2

MS51B - In May 2014, cis-1,2-dichloroethene, tetrachloroethene, trichloroethene, and vinyl chloride were

detected at concentrations exceeding corresponding regulatory guidelines. The same four compounds

were detected at similar concentrations during the October 2015 monitoring event. No additional

compounds were detected at concentrations exceeding applicable regulatory guidelines.

MW54B - In May 2014, cis-1,2-dichloroethene, tetrachloroethene, trichloroethene, and vinyl chloride were

detected at concentrations exceeding corresponding regulatory guidelines. The same four compounds

were detected at similar concentrations during the October monitoring event. No additional compounds

were detected at concentrations exceeding applicable regulatory guidelines.

MW55B - In May 2014, cis-1,2-dichloroethene and vinyl chloride were detected at concentrations

exceeding corresponding regulatory guidelines. During the October monitoring event, only vinyl chloride

was detected at a concentration exceeding corresponding guidelines. No additional compounds were

detected at concentrations exceeding applicable regulatory guidelines.

MW36B - In May 2014, tetrachloroethene was detected at a concentrations of 36 ug/l, exceeding the

corresponding regulatory guideline. In October 2015, tetrachloroethene was detected at a concentration

of 77 ug/l. No additional compounds were detected at concentrations exceeding applicable regulatory

guidelines.

MW57B1- In May 2014, tetrachloroethene was detected at a concentrations of 55 ug/l, exceeding

corresponding regulatory guidelines. In October 2015, tetrachloroethene was detected at a concentration

of 220 ug/l. Additionally, trichloroethene was also detected in 2015 at a concentration of 4.8 ug/l,

exceeding corresponding regulatory guidelines. No additional compounds were detected at

concentrations exceeding applicable regulatory guidelines.

MW57B2 - No compounds were detected in May 2014 or October 2015 at concentrations exceeding

corresponding regulatory guidelines.

MW58B1 - No compounds were detected in May 2014 or October 2015 at concentrations exceeding

corresponding regulatory guidelines.

MW58B2 - No compounds were detected in May 2014 or October 2015 at concentrations exceeding

corresponding regulatory guidelines.

Metals

IN7B - No metals were detected at concentrations exceeding applicable regulatory guidelines as a result

of the May 2014 or October 2015 monitoring event.

IN1B1 - In May 2014, sampling results identified concentrations of arsenic, barium, iron, and manganese

in monitoring well IN1B1. In October 2015, sampling results reflected in a drop in all observed detections

with the exception of iron. Manganese was the only metal detected at a concentration exceeding

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Appendix C Intra-well Trend Narrative Page 3

applicable regulatory guidelines and between 2014 and 2015, manganese concentrations decreased from

3,200 ug/l to 1,990 ug/l. The corresponding MEDEP Residential RAG and reported Project Action Limit

for manganese are 500 ug/l and 200 ug/l, respectively.

IN-1B2 - In May 2014, aluminum, antimony, arsenic, barium, iron, and manganese were detected in well

IN-1B2. Concentrations of Arsenic (17 ug/L) and Manganese (1,900 ug/l) exceeded corresponding

MEDEP Residential RAGs of 10 ug/l and 500 ug/l, respectively. In October 2015, arsenic was not

detected above the MEDEP Residential RAG, however manganese was detected at a concentration of

2,600 ug/l and sodium was detected at a concentration of 23,800 ug/l. The MEDEP Residential RAG and

Project Action Limit for Sodium is 20,000 ug/l.

MW-3B - No metals were detected at concentrations exceeding applicable regulatory guidelines as a

result of the May 2014 or October 2015 monitoring event.

MW-23B - No metals were detected in May 2014 at a concentration exceeding applicable regulatory

guidelines. In October 2015, Sodium was detected at a concentration of 25,700 ug/l, exceeding the

corresponding MEDEP Residential RAG and reported Project Action Limits of 20,000 ug/l.

MS51B - In May 2014, no metals were detected at concentrations greater than corresponding regulatory

guidelines. Barium, iron, and manganese were detected at concentrations of 2.5 ug/l, 2,100 ug/l, and 90

ug/l, respectively. In October 2015, barium was detected at 2.6 ug/l, iron was detected at 8,500 ug/l, and

manganese was detected at 139 ug/l. Additionally, sodium was detected in October 2015 at a

concentration of 41,500 ug/l. These concentrations, although different, do not appear to reflect a

significant trend from the previous year. October 2015 concentrations of iron and sodium both exceeded

corresponding MEDEP Residential RAGs of 5,000 ug/l and 20,000 ug/l, respectively.

MW54B - May 2014 indicated elevated concentrations of iron, manganese and zinc. The manganese

concentration (360 ug/l) exceeded the corresponding MEDEP Residential RAG and reported Project

Action Limits of 500 ug/l and 200 ug/l, respectively. In October 2015, manganese was detected at 252

ug/l, while the concentration of iron increased and the concentration of zinc decreased from May 2014.

MW55B - In May 2014, concentrations of iron and manganese were detected below corresponding

regulatory guidelines. In October 2015, Iron (11,000 ug/l) and sodium (19,100 ug/l) were detected at

concentrations exceeding corresponding MEDEP Residential Rags of 5,000 ug/l and 20,000 ug/l

respectively. Additionally, manganese was detected in October 2015 at a concertation exceeding the

reported Project Action Limit of 200 ug/l, but less than the MEDEP Residential RAG of 500 ug/l.

MW36B1 - In May 2014, Antimony and Arsenic were detected at concentrations of 20.7 ug/l and 28 ug/l

respectively. In October 2015, antimony and arsenic were detected at concentrations of 25.2 ug/l and 26

ug/l, respectively. The MEDEP Residential Rag and reported Project Action Limit for antimony and

arsenic are 3 ug/l and 10 ug/l, respectively. In 2015, sodium (45,900 ug/l) was also detected above

corresponding guidelines.

Page 46: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Appendix C Intra-well Trend Narrative Page 4

MW57B1- Manganese was detected in 2014 at a concentration of 390, exceeding the 200 ug/l MEDEP

Residential RAG and Project Action limit. In October 2015, manganese was detected at a concentration

of 12 ug/l.

MW57B2 - In May 2014, barium, chromium, copper, iron, and lead were detected at this sampling

location. Only chromium (30 ug/l) was detected at a concentration exceeding applicable regulatory

guidelines. In October 2015, two compounds were detected at concentrations exceeding applicable

regulatory guidelines. Chromium was detected at a concentration of 25.3 ug/l, exceeding the Project

Action Limit and MEDEP Residential RAG of 20 ug/l. Cobalt was also detected at a concentration of 11.6

ug/l, exceeding the 10 ug/l Project Action Limit and MEDEP Residential RAG.

MW58B1 - Not metals were detected over corresponding regulatory guidelines in May 2014 or October

2015.

MW58B2 - In May 2014, aluminum (9,300) and arsenic (11 ug/l) concentrations were both over regulatory

guidelines, but the concentration dropped below corresponding action limits (7,000 ug/l and 10 ug/l) in

2015.

Page 47: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

November 19, 2015

Project ID: EASTERN SURPLUS

Project Manager: Ms. Diane Paul

Dear Ms. Hewett:

RE: Katahdin Lab Number: SI8365

Please find enclosed the following information:

Sample Receipt Date(s): October 21, 2015

Ms. Rebecca Hewett

Maine DEP

State House Station 17

Augusta,ME 04333

* Report of Analysis (Analytical and/or Field)

* Quality Control Data Summary

* Chain of Custody (COC)

* Login Report

A copy of the Chain of Custody is included in the paginated report. The original COC is attached as an

addendum to this report.

Should you have any questions or comments concerning this Report of Analysis, please do not hesitate to

contact the project manager listed above. The results contained in this report relate only to the submitted

samples. This cover letter is an integral part of the ROA.

We certify that the test results provided in this report meet all the requirements of the NELAC standards unless

otherwise noted in an attached technical narrative or in the Report of Analysis.

We appreciate your continued use of our laboratory and look forward to working with you in the future. The

following signature indicates technical review and acceptance of the data.

Please go to http://www.katahdinlab.com/cert.html for copies of Katahdin Analytical Services Inc. current

certificates and analyte lists.

Sincerely,

KATAHDIN ANALYTICAL SERVICES

__________________________________________ _________________

Authorized Signature Date

11/19/2015

Katahdin Analytical Services 0000001

Page 48: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

TECHNICAL NARRATIVE

Organics Analysis The samples of Work Order SI8365 were analyzed in accordance with "Test Methods for Evaluating

Solid Wastes: Physical/Chemical Methods." SW-846, 2nd edition, 1982 (revised 1984), 3rd edition, 1986,

and Updates I, II, IIA, III, IIIA, and IIIB 1996, 1998 & 2004, Office of Solid Waste and Emergency

Response, U.S. EPA, and/or for the specific methods listed below or on the Report of Analysis.

8260B Analysis

Sample SI8365-14 was analyzed within hold time and needed to be reanalyzed diluted in order to bring

the high concentration of tetrachloroethene into the calibration range. Due to laboratory error, the sample

was reanalyzed diluted 11 days out of hold time. The results for both analyses are reported.

The reported percent recovery acceptance limits for the Laboratory Control Samples (LCSs) are

statistically derived for the full list of spiked compounds. The recoveries of the spiked analytes in the

LCS, Matrix Spike (MS) and Matrix Spike Duplicate (MSD) are compared to these acceptance limits.

Katahdin standard operating procedure is to take corrective action only if the number of spiked analytes in

the LCS that are outside of the QC limits is greater than ten percent of the client compound list. If the

associated MS/MSD has greater than the allowable number of exceedances, no corrective action is taken,

as long the LCS is acceptable.

There were no other protocol deviations or observations noted by the organics laboratory staff.

Metals Analysis

On the Report of Analysis for metals for Katahdin Work Order SI8365, the column labeled as “Adjusted

PQL” contains the laboratory standard Practical Quantitation Level, or reporting level, for that parameter

by the method listed, which has been corrected for the amount of sample used, dilution required, and

percent solids (if applicable). In order to meet the client’s reporting levels, the laboratory evaluated data

down to the method detection limit (MDL). For hits that fell between the lab adjusted MDL and the lab

adjusted PQL, a “J” flag has been used to indicate that the value is estimated. For hits that fell below the

adjusted MDL, a “U” qualifier and the adjusted MDL have been entered into the result field. Hits above

the adjusted PQL have been reported without a flag.

Katahdin Analytical Services SI8365 page 0000002 of 0000115

Page 49: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

Katahdin Analytical Services SI8365 page 0000003 of 0000115

Page 50: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

DM-003 – Revision 6 – 10/15/2014

KATAHDIN ANALYTICAL SERVICES – INORGANIC DATA QUALIFIERS

The sampled date indicated on the attached Report(s) of Analysis (ROA) is the date for which a grab sample was collected or the date for which a composite sample was completed. Beginning and start times for composite samples can be found on the Chain-of-Custody. U Indicates the compound was analyzed for but not detected above the specified level. This level may be the Limit of

Quantitation (LOQ)(previously called Practical Quantitation Level (PQL)), the Limit of Detection (LOD) or Method Detection Limit (MDL) as required by the client.

Note: All results reported as “U” MDL have a 50% rate for false negatives compared to those results reported as “U” PQL/LOQ or “U” LOD, where the rate of false negatives is <1%.

E Estimated value. This flag identifies compounds whose concentrations exceed the upper level of the calibration range of the

instrument for that specific analysis. J Estimated value. The analyte was detected in the sample at a concentration less than the laboratory Limit of Quantitation

(LOQ)(previously called Practical Quantitation Limit (PQL)), but above the Method Detection Limit (MDL). I-7 The laboratory’s Practical Quantitation Level could not be achieved for this parameter due to sample composition, matrix

effects, sample volume, or quantity used for analysis. A-4 Please refer to cover letter or narrative for further information. H_ Please note that the regulatory holding time for _______ is “analyze immediately”. Ideally, this analysis must be performed in

the field at the time of sample collection. _______ for this sample was not performed at the time of sample collection. The analysis was performed as soon as possible after receipt by the laboratory.

H1 - pH H2 - DO H3 - sulfide H4 - residual chlorine T1 The client did not provide the full volume of at least one liter for analysis of TSS. Therefore, the PQL of 2.5 mg/L could not be

achieved. T2 The client provided the required volume of at least one liter for analysis of TSS, but the laboratory could not filter the full one

liter volume due to the sample matrix. Therefore, the PQL of 2.5 mg/L could not be achieved. M1 The matrix spike and/or matrix spike duplicate recovery performed on this sample was outside of the laboratory acceptance

criteria. Sample matrix is suspected. The laboratory criteria was met for the Laboratory Control Sample (LCS) analyzed concurrently with this sample.

M2 The matrix spike and/or matrix spike duplicate recovery was outside of the laboratory acceptance criteria. The native sample

concentration is greater than four times the spike added concentration so the spike added could not be distinguished from the native sample concentration.

R1 The relative percent difference (RPD) between the duplicate analyses performed on this sample was outside of the laboratory

acceptance criteria (when both values are greater than ten times the PQL). MCL Maximum Contaminant Level NL No limit NFL No Free Liquid Present FLP Free Liquid Present NOD No Odor Detected TON Threshold Odor Number D-1 As required by Method 5210B, APHA Standard Methods for the Examination of Water and Wastewater (21

st edition), the BOD

value reported for this sample is ‘qualified’ because the check standard run concurrently with the sample analysis did not meet the criteria specified in the method (198 +/- 30.5 mg/L). These results may not be reportable for compliance purposes.

D-2 The measured final dissolved oxygen concentrations of all dilutions were less than the method-specified limit of 1 mg/L. The

reported BOD result was calculated assuming a final oxygen concentration equal to 1 mg/L. D-3 The dilution water used to prepare this sample did not meet the method and/or regulatory criteria of less than 0.2 or 0.4 mg/L

dissolved oxygen (DO) uptake over the five day period of incubation. These results may not be reportable for compliance purposes.

Katahdin Analytical Services SI8365 page 0000004 of 0000115

Page 51: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-1

EASTERN SURPLUSESLT-GW-MW51B-1015

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl ChlorideBromomethane

Chloroethane

Trichlorofluoromethane

1,1-DichloroetheneCarbon Disulfide

Freon-113

Methylene Chloride

Acetonetrans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-DichloroetheneBromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-ButanoneBenzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-PentanoneTetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

J

U

U

JB

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.24

0.36

12

0.49

0.55

0.24

0.82

0.25

0.31

1.6

31

0.25

0.36

0.21

190

0.21

0.32

0.22

0.20

58

0.26

0.31

0.20

12

0.25

0.33

0.19

0.27

25

100

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4137.D

Katahdin Analytical Services SI8365 page 0000005 of 0000115

Page 52: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-1

EASTERN SURPLUSESLT-GW-MW51B-1015

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl AcetateMethylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

4.8

0.30

101.

98.9

122.

113.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4137.D

Katahdin Analytical Services SI8365 page 0000006 of 0000115

Page 53: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-2

EASTERN SURPLUSESLT-GW-MW54B-1015

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl ChlorideBromomethane

Chloroethane

Trichlorofluoromethane

1,1-DichloroetheneCarbon Disulfide

Freon-113

Methylene Chloride

Acetonetrans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-DichloroetheneBromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

J

U

U

U

J

U

U

JB

J

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

E

U

U

U

U

U

0.24

2.6

1.4

0.49

0.55

0.24

0.52

0.25

0.31

1.2

2.4

0.25

0.36

0.21

130

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

47

0.25

0.33

0.19

0.27

1.3

3900

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4138.D

Katahdin Analytical Services SI8365 page 0000007 of 0000115

Page 54: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-2

EASTERN SURPLUSESLT-GW-MW54B-1015

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

104.

104.

123.

116.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4138.D

Katahdin Analytical Services SI8365 page 0000008 of 0000115

Page 55: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-2DL

EASTERN SURPLUSESLT-GW-MW54B-1015

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene ChlorideAcetone

trans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-DichloroetheneBromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene

1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

18-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

JB

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

24

36

25

49

55

24

35

25

31

170

220

25

36

21

110

21

32

22

20

130

26

31

20

28

25

33

19

27

130

3900

20

33

30

22

170

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

200

200

200

200

200

200

100

100

100

500

500

100

100

100

100

100

100

100

100

500

100

100

100

100

100

100

100

100

500

100

100

100

100

100

500

24.

36.

25.

49.

55.

24.

35.

25.

31.

110

220

25.

36.

21.

21.

21.

32.

22.

20.

130

26.

31.

20.

28.

25.

33.

19.

27.

130

40.

20.

33.

30.

22.

170

Cert No E87604

Report of Analytical Results

Lab File ID: W4163.D

Katahdin Analytical Services SI8365 page 0000009 of 0000115

Page 56: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-2DL

EASTERN SURPLUSESLT-GW-MW54B-1015

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

18-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

22

21

59

25

23

23

23

38

26

24

15

50

37

27

53

30

104.

100.

127.

118.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

100

100

200

100

100

100

100

100

100

100

100

100

100

100

100

100

22.

21.

59.

25.

23.

23.

23.

38.

26.

24.

15.

50.

37.

27.

53.

30.

Cert No E87604

Report of Analytical Results

Lab File ID: W4163.D

Katahdin Analytical Services SI8365 page 0000010 of 0000115

Page 57: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-3RA

EASTERN SURPLUSESLT-GW-MW55B-1015

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl ChlorideBromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetonetrans-1,2-DichloroetheneMethyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-DichloroetheneBromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

J

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.24

0.36

20

0.49

0.55

0.24

0.35

0.25

0.31

1.1

10

0.77

0.36

0.21

2.7

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

2.8

0.25

0.33

0.19

0.27

1.3

10

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4164.D

Katahdin Analytical Services SI8365 page 0000011 of 0000115

Page 58: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-3RA

EASTERN SURPLUSESLT-GW-MW55B-1015

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-XyleneStyrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

J

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.74

2.4

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

110.

103.

133.

118.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4164.D

Katahdin Analytical Services SI8365 page 0000012 of 0000115

Page 59: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-4

EASTERN SURPLUSESLT-GW-MW36B1-101

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Dichlorodifluoromethane

ChloromethaneVinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetonetrans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-DichloroetheneBromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

J

U

U

U

U

U

U

U

JB

J

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.24

1.3

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.3

2.4

0.25

0.36

0.21

3.3

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

3.5

0.25

0.33

0.19

0.27

1.3

77

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4140.D

Katahdin Analytical Services SI8365 page 0000013 of 0000115

Page 60: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-4

EASTERN SURPLUSESLT-GW-MW36B1-101

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

95.7

104.

116.

114.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4140.D

Katahdin Analytical Services SI8365 page 0000014 of 0000115

Page 61: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-5

EASTERN SURPLUSESLT-GW-MW57B1-101

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Dichlorodifluoromethane

ChloromethaneVinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene ChlorideAcetone

trans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-DichloroetheneBromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

J

U

U

U

U

U

U

U

JB

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

E

U

U

U

U

U

0.24

1.4

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.4

2.2

0.25

0.36

0.21

5.0

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

4.8

0.25

0.33

0.19

0.27

1.3

240

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4141.D

Katahdin Analytical Services SI8365 page 0000015 of 0000115

Page 62: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-5

EASTERN SURPLUSESLT-GW-MW57B1-101

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

95.6

105.

121.

114.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4141.D

Katahdin Analytical Services SI8365 page 0000016 of 0000115

Page 63: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-5DL

EASTERN SURPLUSESLT-GW-MW57B1-101

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetonetrans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-DichloroetheneBromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

18-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

JB

J

U

U

U

J

U

U

U

U

U

U

U

U

J

U

U

U

U

U

U

U

U

U

U

1.2

1.8

1.2

2.4

2.8

1.2

1.8

1.2

1.6

8.7

14

1.2

1.8

1.0

3.4

1.0

1.6

1.1

1.0

6.6

1.3

1.6

1.0

4.4

1.2

1.6

0.95

1.4

6.6

220

1.0

1.6

1.5

1.1

8.5

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

10.

10.

10.

10.

10.

10.

5.0

5.0

5.0

25.

25.

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

25.

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

25.

5.0

5.0

5.0

5.0

5.0

25.

1.2

1.8

1.2

2.4

2.8

1.2

1.8

1.2

1.6

5.6

11.

1.2

1.8

1.0

1.0

1.0

1.6

1.1

1.0

6.6

1.3

1.6

1.0

1.4

1.2

1.6

0.95

1.4

6.6

2.0

1.0

1.6

1.5

1.1

8.5

Cert No E87604

Report of Analytical Results

Lab File ID: W4165.D

Katahdin Analytical Services SI8365 page 0000017 of 0000115

Page 64: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-5DL

EASTERN SURPLUSESLT-GW-MW57B1-101

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

18-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

1.1

1.0

3.0

1.2

1.2

1.2

1.2

1.9

1.3

1.2

0.75

2.5

1.8

1.4

2.6

1.5

105.

102.

126.

110.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

5.0

5.0

10.

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

1.1

1.0

3.0

1.2

1.2

1.2

1.2

1.9

1.3

1.2

0.75

2.5

1.8

1.4

2.6

1.5

Cert No E87604

Report of Analytical Results

Lab File ID: W4165.D

Katahdin Analytical Services SI8365 page 0000018 of 0000115

Page 65: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-6RA

EASTERN SURPLUSESLT-GW-MW57B2-101

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Dichlorodifluoromethane

ChloromethaneVinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetonetrans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-Dichloroethene

Bromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

J

U

U

U

U

U

U

U

JB

U

U

U

U

U

U

U

U

U

U

U

U

J

U

U

U

U

U

U

U

U

U

0.24

1.9

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.3

93

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.49

0.25

0.33

0.19

1.8

1.3

9.7

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4166.D

Katahdin Analytical Services SI8365 page 0000019 of 0000115

Page 66: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-6RA

EASTERN SURPLUSESLT-GW-MW57B2-101

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

110.

106.

129.

115.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4166.D

Katahdin Analytical Services SI8365 page 0000020 of 0000115

Page 67: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-7

EASTERN SURPLUSESLT-GW-IN1B1-1015

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl ChlorideBromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetonetrans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-DichloroetheneBromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

J

J

U

U

U

U

U

U

JB

J

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

E

U

U

U

U

U

0.24

1.2

0.27

0.49

0.55

0.24

0.35

0.25

0.31

1.3

3.1

0.25

0.36

0.21

3.1

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

5.6

0.25

0.33

0.19

0.27

1.3

650

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4143.D

Katahdin Analytical Services SI8365 page 0000021 of 0000115

Page 68: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-7

EASTERN SURPLUSESLT-GW-IN1B1-1015

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

94.3

99.7

112.

111.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4143.D

Katahdin Analytical Services SI8365 page 0000022 of 0000115

Page 69: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-7DL

EASTERN SURPLUSESLT-GW-IN1B1-1015

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetonetrans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-Dichloroethene

Bromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene

1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

18-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

JB

J

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

2.4

3.6

2.5

4.9

5.5

2.4

3.5

2.5

3.1

19

33

2.5

3.6

2.1

2.1

2.1

3.2

2.2

2.0

13

2.6

3.1

2.0

2.8

2.5

3.3

1.9

2.7

13

600

2.0

3.3

3.0

2.2

17

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

20.

20.

20.

20.

20.

20.

10.

10.

10.

50.

50.

10.

10.

10.

10.

10.

10.

10.

10.

50.

10.

10.

10.

10.

10.

10.

10.

10.

50.

10.

10.

10.

10.

10.

50.

2.4

3.6

2.5

4.9

5.5

2.4

3.5

2.5

3.1

11.

22.

2.5

3.6

2.1

2.1

2.1

3.2

2.2

2.0

13.

2.6

3.1

2.0

2.8

2.5

3.3

1.9

2.7

13.

4.0

2.0

3.3

3.0

2.2

17.

Cert No E87604

Report of Analytical Results

Lab File ID: W4167.D

Katahdin Analytical Services SI8365 page 0000023 of 0000115

Page 70: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-7DL

EASTERN SURPLUSESLT-GW-IN1B1-1015

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

18-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

2.2

2.1

5.9

2.5

2.3

2.3

2.3

3.8

2.6

2.4

1.5

5.0

3.7

2.7

5.3

3.0

106.

101.

125.

115.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

10.

10.

20.

10.

10.

10.

10.

10.

10.

10.

10.

10.

10.

10.

10.

10.

2.2

2.1

5.9

2.5

2.3

2.3

2.3

3.8

2.6

2.4

1.5

5.0

3.7

2.7

5.3

3.0

Cert No E87604

Report of Analytical Results

Lab File ID: W4167.D

Katahdin Analytical Services SI8365 page 0000024 of 0000115

Page 71: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-8RA

EASTERN SURPLUSESLT-GW-IN1B2-1015

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl ChlorideBromomethane

ChloroethaneTrichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene ChlorideAcetone

trans-1,2-DichloroetheneMethyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-DichloroetheneBromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

JB

U

J

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.24

0.36

2.2

0.49

4.7

0.24

0.35

0.25

0.31

1.5

2.2

0.41

0.36

0.21

8.1

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

12

0.25

0.33

0.19

0.27

1.3

31

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4168.D

Katahdin Analytical Services SI8365 page 0000025 of 0000115

Page 72: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-8RA

EASTERN SURPLUSESLT-GW-IN1B2-1015

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

106.

100.

131.

116.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4168.D

Katahdin Analytical Services SI8365 page 0000026 of 0000115

Page 73: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-9

EASTERN SURPLUSESLT-GW-MW23B-1015

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Dichlorodifluoromethane

ChloromethaneVinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene ChlorideAcetone

trans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-DichloroetheneBromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

JB

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.24

2.3

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.3

2.2

0.25

0.36

0.21

14

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

5.5

0.25

0.33

0.19

0.27

1.3

140

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4145.D

Katahdin Analytical Services SI8365 page 0000027 of 0000115

Page 74: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-9

EASTERN SURPLUSESLT-GW-MW23B-1015

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

96.9

102.

120.

115.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4145.D

Katahdin Analytical Services SI8365 page 0000028 of 0000115

Page 75: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-10

EASTERN SURPLUSESLT-GW-IN7B-1015

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Dichlorodifluoromethane

ChloromethaneVinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetonetrans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-DichloroetheneBromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

J

U

U

U

U

U

U

U

JB

J

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.24

1.6

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.4

2.6

0.25

0.36

0.21

6.3

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

3.3

0.25

0.33

0.19

0.27

1.3

190

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4146.D

Katahdin Analytical Services SI8365 page 0000029 of 0000115

Page 76: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-10

EASTERN SURPLUSESLT-GW-IN7B-1015

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

96.3

102.

117.

116.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4146.D

Katahdin Analytical Services SI8365 page 0000030 of 0000115

Page 77: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-11

EASTERN SURPLUSESLT-GW-MW3B-1015

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Dichlorodifluoromethane

ChloromethaneVinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene ChlorideAcetone

trans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-Dichloroethene

Bromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene

1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

J

U

U

U

U

U

U

U

JB

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.24

1.4

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.3

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4147.D

Katahdin Analytical Services SI8365 page 0000031 of 0000115

Page 78: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-11

EASTERN SURPLUSESLT-GW-MW3B-1015

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

118.

112.

129.

118.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4147.D

Katahdin Analytical Services SI8365 page 0000032 of 0000115

Page 79: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-12

EASTERN SURPLUSESLT-GW-MW58B1-101

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Dichlorodifluoromethane

ChloromethaneVinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetonetrans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-DichloroetheneBromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

JB

J

U

U

U

J

U

U

U

U

U

U

U

U

J

U

U

U

U

U

U

U

U

U

U

0.24

2.3

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.2

2.5

0.25

0.36

0.21

0.32

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.69

0.25

0.33

0.19

0.27

1.3

18

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4148.D

Katahdin Analytical Services SI8365 page 0000033 of 0000115

Page 80: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-12

EASTERN SURPLUSESLT-GW-MW58B1-101

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

98.6

104.

120.

114.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4148.D

Katahdin Analytical Services SI8365 page 0000034 of 0000115

Page 81: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-13

EASTERN SURPLUSESLT-GW-MW58B2-101

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Dichlorodifluoromethane

ChloromethaneVinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene ChlorideAcetone

trans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-Dichloroethene

Bromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene

1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

J

U

U

U

U

U

U

U

JB

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.24

0.86

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.4

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4149.D

Katahdin Analytical Services SI8365 page 0000035 of 0000115

Page 82: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-13

EASTERN SURPLUSESLT-GW-MW58B2-101

SI8365

20-OCT-1521-OCT-15

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

99.2

104.

120.

115.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4149.D

Katahdin Analytical Services SI8365 page 0000036 of 0000115

Page 83: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-14

EASTERN SURPLUSESLT-GW-MWRP-1015

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetonetrans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-DichloroetheneBromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

J

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

E

U

U

U

U

U

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.8

0.25

0.36

0.21

2.8

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

5.6

0.25

0.33

0.19

0.27

1.3

710

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4175.D

Katahdin Analytical Services SI8365 page 0000037 of 0000115

Page 84: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-14

EASTERN SURPLUSESLT-GW-MWRP-1015

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

108.

102.

133.

117.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4175.D

Katahdin Analytical Services SI8365 page 0000038 of 0000115

Page 85: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-14DL

EASTERN SURPLUSESLT-GW-MWRP-1015

SI8365

20-OCT-1521-OCT-15

14-NOV-15AAB

SW846 8260B

14-NOV-15

WG174238

AQNA

AABSW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetone

trans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-Dichloroethene

Bromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene

1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethenetrans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

4.8

7.2

5.0

9.8

11

4.8

7.0

5.0

6.2

23

44

5.0

7.2

4.2

4.2

4.2

6.4

4.4

4.0

26

5.2

6.2

4.0

5.6

5.0

6.6

3.8

5.4

26

500

4.0

6.6

6.0

4.4

34

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

40.

40.

40.

40.

40.

40.

20.

20.

20.

100

100

20.

20.

20.

20.

20.

20.

20.

20.

100

20.

20.

20.

20.

20.

20.

20.

20.

100

20.

20.

20.

20.

20.

100

4.8

7.2

5.0

9.8

11.

4.8

7.0

5.0

6.2

23.

44.

5.0

7.2

4.2

4.2

4.2

6.4

4.4

4.0

26.

5.2

6.2

4.0

5.6

5.0

6.6

3.8

5.4

26.

8.0

4.0

6.6

6.0

4.4

34.

Cert No E87604

Report of Analytical Results

Lab File ID: T5380.D

Katahdin Analytical Services SI8365 page 0000039 of 0000115

Page 86: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-14DL

EASTERN SURPLUSESLT-GW-MWRP-1015

SI8365

20-OCT-1521-OCT-15

14-NOV-15AAB

SW846 8260B

14-NOV-15

WG174238

AQNA

AABSW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

4.4

4.2

12

5.0

4.6

4.6

4.6

7.6

5.2

4.8

3.0

10

7.4

5.4

11

6.0

103.

101.

117.

109.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

20.

20.

40.

20.

20.

20.

20.

20.

20.

20.

20.

20.

20.

20.

20.

20.

4.4

4.2

12.

5.0

4.6

4.6

4.6

7.6

5.2

4.8

3.0

10.

7.4

5.4

11.

6.0

Cert No E87604

Report of Analytical Results

Lab File ID: T5380.D

Katahdin Analytical Services SI8365 page 0000040 of 0000115

Page 87: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-16

EASTERN SURPLUSESLT-TB-1015

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetonetrans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-Dichloroethene

Bromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene

1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

JB

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.4

6.3

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4162.D

Katahdin Analytical Services SI8365 page 0000041 of 0000115

Page 88: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-16

EASTERN SURPLUSESLT-TB-1015

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-XyleneStyrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

J

J

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.26

0.77

2.4

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

107.

103.

135.

119.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4162.D

Katahdin Analytical Services SI8365 page 0000042 of 0000115

Page 89: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

Maine DEPSI8365-17

EASTERN SURPLUSESLT-GWLORD-1015

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetonetrans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-Dichloroethene

Bromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene

1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

JB

J

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.3

3.5

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

5

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

5.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

1.7

Cert No E87604

Report of Analytical Results

Lab File ID: W4176.D

Katahdin Analytical Services SI8365 page 0000043 of 0000115

Page 90: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

Maine DEPSI8365-17

EASTERN SURPLUSESLT-GWLORD-1015

SI8365

20-OCT-1521-OCT-15

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

110.

104.

135.

119.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4176.D

Katahdin Analytical Services SI8365 page 0000044 of 0000115

Page 91: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://[email protected]

Cert No E87604

Form 4 Method Blank Summary

Lab Name : Katahdin Analytical Services SDG : SI8365

Lab File ID : T5377.DLab Sample ID : WG174238-2

This Method Blank applies to the following samples, LCS, MS and MSD:

09:21Time Analyzed :14-NOV-15Date Analyzed :

Instrument ID : GCMS-THeated Purge : No

WG174238-1SI8365-14DL

Laboratory Control SESLT-GW-MWRP-1015

T5374.DT5380.D

11/14/1511/14/15

07:2311:04

Project : EASTERN SURPLUS

Client Sample ID Lab Sample ID Lab File ID Date Analyzed Time Analyzed

- VOA

Katahdin Analytical Services SI8365 page 0000045 of 0000115

Page 92: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

WG174238-2Method Blank Sample

SI8365

14-NOV-15AAB

SW846 8260B

14-NOV-15

WG174238

AQNA

AABSW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetone

trans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-Dichloroethene

Bromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene

1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

Cert No E87604

Report of Analytical Results

Lab File ID: T5377.D

Katahdin Analytical Services SI8365 page 0000046 of 0000115

Page 93: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

WG174238-2Method Blank Sample

SI8365

14-NOV-15AAB

SW846 8260B

14-NOV-15

WG174238

AQNA

AABSW846 5030

2-Hexanone

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

1.7

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

100.

100.

110.

109.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

5

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

5.0

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.7

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: T5377.D

Katahdin Analytical Services SI8365 page 0000047 of 0000115

Page 94: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

WG174238-1LCS

SI8365

14-NOV-15AAB

SW846 8260B

14-NOV-15

WG174238

AQNA

AABSW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetone

trans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-Dichloroethene

Bromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene

1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Recovery (%) Conc Added Conc Recovered Conc Units

* 27.8

* 52.2

68.8

76.8

80.4

85.6

96.8

81.2

96.0

93.6

94.4

106.

104.

105.

99.6

102.

101.

* 82.2

97.8

101.

104.

89.8

97.6

110.

101.

107.

97.6

104.

108.

96.0

103.

102.

95.2

110.

102.

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

100.

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

13.9

26.1

34.4

38.4

40.2

42.8

48.4

40.6

48.0

46.8

47.2

52.9

104.

52.4

49.8

51.1

50.3

41.1

48.9

50.5

51.9

44.9

48.8

55.1

50.4

53.7

48.8

51.9

53.9

48.0

51.4

50.9

47.6

54.8

51.0

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Cert No E87604

LCS Recovery Report

Limits

29-164

59-123

64-131

57-135

53-157

70-149

88-127

71-129

73-126

72-129

62-172

78-125

81-125

76-130

85-123

85-117

78-128

87-126

77-129

71-132

86-116

71-133

81-125

79-121

84-118

85-122

83-119

84-118

83-122

47-155

85-135

84-115

85-119

84-116

80-124

T5374.DLCS File ID:

Katahdin Analytical Services SI8365 page 0000048 of 0000115

Page 95: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

WG174238-1LCS

SI8365

14-NOV-15AAB

SW846 8260B

14-NOV-15

WG174238

AQNA

AABSW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Recovery (%) Conc Added Conc Recovered Conc Units

104.

109.

110.

108.

105.

99.8

115.

101.

103.

100.

107.

100.

108.

111.

98.0

98.4

100.

100.

98.0

100.

50.0

50.0

100.

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

52.2

54.3

110.

53.9

52.7

49.9

57.7

50.6

51.5

50.0

53.4

50.0

53.9

55.5

49.0

49.2

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Cert No E87604

LCS Recovery Report

Limits

89-113

88-113

88-116

90-116

88-117

86-117

96-136

79-121

86-110

86-111

86-112

67-124

76-126

70-122

70-132

73-125

56-133

65-128

67-135

68-128

T5374.DLCS File ID:

Katahdin Analytical Services SI8365 page 0000049 of 0000115

Page 96: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://[email protected]

Cert No E87604

Form 4 Method Blank Summary

Lab Name : Katahdin Analytical Services SDG : SI8365

Lab File ID : W4136.DLab Sample ID : WG172846-2

This Method Blank applies to the following samples, LCS, MS and MSD:

11:24Time Analyzed :23-OCT-15Date Analyzed :

Instrument ID : GCMS-WHeated Purge : No

WG172846-1SI8365-1SI8365-2SI8365-4SI8365-5SI8365-7SI8365-9SI8365-10SI8365-11SI8365-12SI8365-13WG172846-5WG172846-6

Laboratory Control SESLT-GW-MW51B-1015ESLT-GW-MW54B-1015ESLT-GW-MW36B1-1015ESLT-GW-MW57B1-1015ESLT-GW-IN1B1-1015ESLT-GW-MW23B-1015ESLT-GW-IN7B-1015ESLT-GW-MW3B-1015ESLT-GW-MW58B1-1015ESLT-GW-MW58B2-1015Matrix SpikeMatrix Spike Duplica

W4134.DW4137.DW4138.DW4140.DW4141.DW4143.DW4145.DW4146.DW4147.DW4148.DW4149.DW4150.DW4151.D

10/23/1510/23/1510/23/1510/23/1510/23/1510/23/1510/23/1510/23/1510/23/1510/23/1510/23/1510/23/1510/23/15

10:1012:1912:5113:5414:2515:2816:3117:0317:3418:0618:3719:0919:40

Project : EASTERN SURPLUS

Client Sample ID Lab Sample ID Lab File ID Date Analyzed Time Analyzed

- VOA

Katahdin Analytical Services SI8365 page 0000050 of 0000115

Page 97: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

WG172846-2Method Blank Sample

SI8365

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetone

trans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-Dichloroethene

Bromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene

1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

J

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

3.3

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

Cert No E87604

Report of Analytical Results

Lab File ID: W4136.D

Katahdin Analytical Services SI8365 page 0000051 of 0000115

Page 98: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

WG172846-2Method Blank Sample

SI8365

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

2-Hexanone

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

1.7

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

97.5

99.4

122.

115.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

5

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

5.0

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.7

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4136.D

Katahdin Analytical Services SI8365 page 0000052 of 0000115

Page 99: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

WG172846-1LCS

SI8365

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetone

trans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-Dichloroethene

Bromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene

1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Recovery (%) Conc Added Conc Recovered Conc Units

74.8

94.0

98.6

103.

108.

119.

101.

102.

106.

96.2

117.

106.

105.

103.

91.4

96.6

105.

110.

105.

117.

96.8

101.

98.8

101.

92.0

103.

107.

97.6

* 122.

95.6

101.

96.4

106.

106.

118.

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

100.

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

37.4

47.0

49.3

51.4

54.2

59.3

50.4

51.0

52.8

48.1

58.5

52.8

105.

51.4

45.7

48.3

52.7

55.1

52.7

58.4

48.4

50.7

49.4

50.4

46.0

51.7

53.5

48.8

60.8

47.8

50.4

48.2

53.2

53.1

58.8

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Cert No E87604

LCS Recovery Report

Limits

29-164

59-123

64-131

57-135

53-157

70-149

88-127

71-129

73-126

72-129

62-172

78-125

81-125

76-130

85-123

85-117

78-128

87-126

77-129

71-132

86-116

71-133

81-125

79-121

84-118

85-122

83-119

84-118

83-122

47-155

85-135

84-115

85-119

84-116

80-124

W4134.DLCS File ID:

Katahdin Analytical Services SI8365 page 0000053 of 0000115

Page 100: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

WG172846-1LCS

SI8365

23-OCT-15EME

SW846 8260B

23-OCT-15

WG172846

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Recovery (%) Conc Added Conc Recovered Conc Units

97.2

103.

102.

96.2

93.4

112.

113.

98.4

98.8

97.8

103.

107.

100.

108.

98.0

102.

102.

100.

109.

104.

50.0

50.0

100.

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

48.6

51.3

102.

48.1

46.7

55.8

56.3

49.2

49.4

48.9

51.3

53.3

50.0

54.2

49.0

51.2

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Cert No E87604

LCS Recovery Report

Limits

89-113

88-113

88-116

90-116

88-117

86-117

96-136

79-121

86-110

86-111

86-112

67-124

76-126

70-122

70-132

73-125

56-133

65-128

67-135

68-128

W4134.DLCS File ID:

Katahdin Analytical Services SI8365 page 0000054 of 0000115

Page 101: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://[email protected]

Cert No E87604

Form 4 Method Blank Summary

Lab Name : Katahdin Analytical Services SDG : SI8365

Lab File ID : W4161.DLab Sample ID : WG172905-2

This Method Blank applies to the following samples, LCS, MS and MSD:

13:49Time Analyzed :24-OCT-15Date Analyzed :

Instrument ID : GCMS-WHeated Purge : No

WG172905-1SI8365-16SI8365-2DLSI8365-3RASI8365-5DLSI8365-6RASI8365-7DLSI8365-8RASI8365-14SI8365-17

Laboratory Control SESLT-TB-1015ESLT-GW-MW54B-1015ESLT-GW-MW55B-1015ESLT-GW-MW57B1-1015ESLT-GW-MW57B2-1015ESLT-GW-IN1B1-1015ESLT-GW-IN1B2-1015ESLT-GW-MWRP-1015ESLT-GWLORD-1015

W4158.DW4162.DW4163.DW4164.DW4165.DW4166.DW4167.DW4168.DW4175.DW4176.D

10/24/1510/24/1510/24/1510/24/1510/24/1510/24/1510/24/1510/24/1510/24/1510/24/15

11:5414:2014:5215:2315:5516:2716:5817:2921:1021:42

Project : EASTERN SURPLUS

Client Sample ID Lab Sample ID Lab File ID Date Analyzed Time Analyzed

- VOA

Katahdin Analytical Services SI8365 page 0000055 of 0000115

Page 102: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

WG172905-2Method Blank Sample

SI8365

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetone

trans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-Dichloroethene

Bromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene

1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

J

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.9

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

2

2

2

2

1

1

1

5

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

1

1

1

5

1

1

1

1

1

2.0

2.0

2.0

2.0

2.0

2.0

1.0

1.0

1.0

5.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

0.24

0.36

0.25

0.49

0.55

0.24

0.35

0.25

0.31

1.1

2.2

0.25

0.36

0.21

0.21

0.21

0.32

0.22

0.20

1.3

0.26

0.31

0.20

0.28

0.25

0.33

0.19

0.27

1.3

0.40

0.20

0.33

0.30

0.22

Cert No E87604

Report of Analytical Results

Lab File ID: W4161.D

Katahdin Analytical Services SI8365 page 0000056 of 0000115

Page 103: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

WG172905-2Method Blank Sample

SI8365

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

2-Hexanone

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL ADJ MDL

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

1.7

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

103.

104.

125.

115.

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

5

1

1

2

1

1

1

1

1

1

1

1

1

1

1

1

1

5.0

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.7

0.22

0.21

0.59

0.25

0.23

0.23

0.23

0.38

0.26

0.24

0.15

0.50

0.37

0.27

0.53

0.30

Cert No E87604

Report of Analytical Results

Lab File ID: W4161.D

Katahdin Analytical Services SI8365 page 0000057 of 0000115

Page 104: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

WG172905-1LCS

SI8365

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetone

trans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-Dichloroethene

Bromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene

1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

1,2-Dibromoethane

2-Hexanone

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Recovery (%) Conc Added Conc Recovered Conc Units

58.0

87.4

87.4

95.8

89.8

97.6

88.8

89.6

91.2

90.8

91.2

93.6

96.7

96.0

* 82.8

89.8

96.6

92.6

91.0

114.

92.8

88.0

93.4

93.4

92.2

98.4

103.

91.8

* 122.

93.6

92.2

94.2

98.6

94.8

116.

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

100.

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

29.0

43.7

43.7

47.9

44.9

48.8

44.4

44.8

45.6

45.4

45.6

46.8

96.7

48.0

41.4

44.9

48.3

46.3

45.5

56.8

46.4

44.0

46.7

46.7

46.1

49.2

51.3

45.9

61.1

46.8

46.1

47.1

49.3

47.4

58.2

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Cert No E87604

LCS Recovery Report

Limits

29-164

59-123

64-131

57-135

53-157

70-149

88-127

71-129

73-126

72-129

62-172

78-125

81-125

76-130

85-123

85-117

78-128

87-126

77-129

71-132

86-116

71-133

81-125

79-121

84-118

85-122

83-119

84-118

83-122

47-155

85-135

84-115

85-119

84-116

80-124

W4158.DLCS File ID:

Katahdin Analytical Services SI8365 page 0000058 of 0000115

Page 105: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

WG172905-1LCS

SI8365

24-OCT-15EME

SW846 8260B

24-OCT-15

WG172905

AQNA

EMESW846 5030

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-Bromofluorobenzene

Toluene-d8

1,2-Dichloroethane-d4

Dibromofluoromethane

17-NOV-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Recovery (%) Conc Added Conc Recovered Conc Units

89.4

94.4

92.8

* 87.8

* 85.4

98.8

100.

93.4

89.4

89.6

94.0

96.8

93.6

108.

99.6

92.2

101.

100.

103.

101.

50.0

50.0

100.

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

44.7

47.2

92.8

43.9

42.7

49.4

50.0

46.7

44.7

44.8

47.0

48.4

46.8

54.1

49.8

46.1

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Cert No E87604

LCS Recovery Report

Limits

89-113

88-113

88-116

90-116

88-117

86-117

96-136

79-121

86-110

86-111

86-112

67-124

76-126

70-122

70-132

73-125

56-133

65-128

67-135

68-128

W4158.DLCS File ID:

Katahdin Analytical Services SI8365 page 0000059 of 0000115

Page 106: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 2

WG172846-5

SI8365

23-OCT-15 EMESW846 8260B

23-OCT-15

WG172846AQ

NA

EMESW846 5030

Dichlorodifluoromethane

Chloromethane

Vinyl Chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

1,1-Dichloroethene

Carbon Disulfide

Freon-113

Methylene Chloride

Acetone

trans-1,2-Dichloroethene

Methyl tert-butyl Ether

1,1-Dichloroethane

cis-1,2-Dichloroethene

Bromochloromethane

Chloroform

Carbon Tetrachloride

1,1,1-Trichloroethane

2-Butanone

Benzene

Cyclohexane

1,2-Dichloroethane

Trichloroethene

1,2-Dichloropropane

Bromodichloromethane

cis-1,3-Dichloropropene

Toluene

4-Methyl-2-Pentanone

Tetrachloroethene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

Dibromochloromethane

17-NOV-15Project:

Extraction Method:Analysis Method:

Report Date:

MS ID: Received Date:

Extracted By:Analyst:

Matrix:

SDG:

Extract Date: Analysis Date:

Lab Prep Batch: % Solids:

CompoundMS Rec

(%)MS

SpikeMS

Conc

80.0

114.

114.

95.2

117.

136.

94.6

92.0

95.8

89.6

100.

95.2

102.

102.

83.4*

95.4

107.

109.

107.

140.*

117.*

96.8

109.

116.

121.*

117.

118.

114.

147.*

64.0

114.

122.*

114.

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

100.

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

40.0

58.8

57.2

47.6

58.5

68.0

47.3

46.0

47.9

46.2

52.6

47.6

102.

50.9

48.0

47.7

53.5

54.4

53.5

70.2

58.7

48.4

54.5

61.3

60.3

58.5

58.9

56.9

73.6

218.

57.1

61.2

57.0

Cert No E87604

MS/MSD Recovery Report

Limits

MSD ID:

Conc Units

MSD Rec(%)

MSDConc RPD (%)

RPD Limit

77.0

122.

119.

102.

100.

116.

103.

105.

100.

94.0

107.

105.

93.0

115.

100.

106.

107.

97.0

95.8

133.*

106.

122.

92.2

104.

107.

99.2

102.

102.

131.*

72.0

97.2

104.

98.8

38.5

62.6

59.3

51.2

50.2

58.0

51.7

52.7

50.2

48.4

56.3

52.5

93.0

57.5

56.5

52.8

53.6

48.5

47.9

66.3

52.8

60.8

46.1

55.2

53.3

49.6

51.2

51.2

65.6

222.

48.6

52.0

49.4

4

6

4

7

15

16

9

14

5

5

7

10

9

12

16

10

0

11

11

6

10

23*

17

10

12

16

14

10

11

2

16

16

14

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

29-164

59-123

64-131

57-135

53-157

70-149

88-127

71-129

73-126

72-129

62-172

78-125

81-125

76-130

85-123

85-117

78-128

87-126

77-129

71-132

86-116

71-133

81-125

79-121

84-118

85-122

83-119

84-118

83-122

47-155

85-135

84-115

85-119

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

WG172846-6

U0.24

J1.6

U0.25

U0.49

U0.55

U0.24

U0.35

U0.25

U0.31

JB1.4

J2.6

U0.25

U0.36

U0.21

6.3

U0.21

U0.32

U0.22

U0.20

U1.3

U0.26

U0.31

U0.20

3.3

U0.25

U0.33

U0.19

U0.27

U1.3

190

U0.20

U0.33

U0.30

SampConc

MSD Spike

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

100.

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

Sample ID: SI8365-10Client ID: ESLT-GW-IN7B-1015

W4150.DMS File ID: W4151.DMSD File ID:

Katahdin Analytical Services SI8365 page 0000060 of 0000115

Page 107: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of2 2

WG172846-5

SI8365

23-OCT-15 EMESW846 8260B

23-OCT-15

WG172846AQ

NA

EMESW846 5030

1,2-Dibromoethane

2-Hexanone

Chlorobenzene

Ethylbenzene

m+p-Xylenes

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-Chloropropane

1,2,4-Trichlorobenzene

1,2,3-Trichlorobenzene

Methyl Acetate

Methylcyclohexane

P-BromofluorobenzeneToluene-d81,2-Dichloroethane-d4Dibromofluoromethane

17-NOV-15Project:

Extraction Method:Analysis Method:

Report Date:

MS ID: Received Date:

Extracted By:Analyst:

Matrix:

SDG:

Extract Date: Analysis Date:

Lab Prep Batch: % Solids:

CompoundMS Rec

(%)MS

SpikeMS

Conc

117.*

132.*

107.

114.*

110.

106.

102.

116.

123.

125.*

107.

107.

116.*

118.

107.

119.

83.4

121.

50.0

50.0

50.0

50.0

100.

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

58.7

65.8

53.4

57.0

110.

53.2

51.1

58.2

61.3

62.3

53.4

53.4

57.9

59.2

53.4

59.5

41.7

60.7

102.101.107.94.9

Cert No E87604

MS/MSD Recovery Report

Limits

MSD ID:

Conc Units

MSD Rec(%)

MSDConc RPD (%)

RPD Limit

100.

123.

98.0

103.

100.

95.4

91.0

97.6

111.

111.

96.8

96.2

102.

102.

97.4

107.

85.2

118.

50.2

61.7

49.0

51.3

100.

47.7

45.5

48.8

55.6

55.5

48.4

48.1

51.0

51.2

48.7

53.4

42.6

59.1

16

6

8

10

10

11

12

18

10

12

10

10

13

14

9

11

2

3

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

84-116

80-124

89-113

88-113

88-116

90-116

88-117

86-117

96-136

79-121

86-110

86-111

86-112

67-124

76-126

70-122

70-132

73-125

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

98.4104.103.101.

WG172846-6

56-13365-12867-13568-128

U0.22

U1.7

U0.22

U0.21

U0.59

U0.25

U0.23

U0.23

U0.23

U0.38

U0.26

U0.24

U0.15

U0.50

U0.37

U0.27

U0.53

U0.30

SampConc

MSD Spike

50.0

50.0

50.0

50.0

100.

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

Sample ID: SI8365-10Client ID: ESLT-GW-IN7B-1015

W4150.DMS File ID: W4151.DMSD File ID:

Katahdin Analytical Services SI8365 page 0000061 of 0000115

Page 108: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-1

EASTERN SURPLUSESLT-GW-MW51B-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

MethaneEthane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

E 5300

16.

23.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2072.D

Katahdin Analytical Services SI8365 page 0000062 of 0000115

Page 109: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-1DL

EASTERN SURPLUSESLT-GW-MW51B-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

MethaneEthane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

U

6800

100

100

ug/L

ug/L

ug/L

10

10

10

10

10

10

100

100

100

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2088.D

Katahdin Analytical Services SI8365 page 0000063 of 0000115

Page 110: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-2

EASTERN SURPLUSESLT-GW-MW54B-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

Methane

Ethane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

U

U

10.

10.

10.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2073.D

Katahdin Analytical Services SI8365 page 0000064 of 0000115

Page 111: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-3

EASTERN SURPLUSESLT-GW-MW55B-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

MethaneEthane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

E

U

6000

10.

1000

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2074.D

Katahdin Analytical Services SI8365 page 0000065 of 0000115

Page 112: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-3DL

EASTERN SURPLUSESLT-GW-MW55B-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

MethaneEthane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

4800

100

870

ug/L

ug/L

ug/L

10

10

10

10

10

10

100

100

100

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2089.D

Katahdin Analytical Services SI8365 page 0000066 of 0000115

Page 113: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-4

EASTERN SURPLUSESLT-GW-MW36B1-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

Methane

Ethane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

U

U

10.

10.

10.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2075.D

Katahdin Analytical Services SI8365 page 0000067 of 0000115

Page 114: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-5

EASTERN SURPLUSESLT-GW-MW57B1-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

Methane

Ethane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

U

U

10.

10.

10.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2076.D

Katahdin Analytical Services SI8365 page 0000068 of 0000115

Page 115: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-6

EASTERN SURPLUSESLT-GW-MW57B2-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

MethaneEthane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

26.

10.

25.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2077.D

Katahdin Analytical Services SI8365 page 0000069 of 0000115

Page 116: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-7

EASTERN SURPLUSESLT-GW-IN1B1-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

Methane

Ethane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

U

U

10.

10.

10.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2078.D

Katahdin Analytical Services SI8365 page 0000070 of 0000115

Page 117: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-8

EASTERN SURPLUSESLT-GW-IN1B2-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

MethaneEthane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

44.

10.

24.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2079.D

Katahdin Analytical Services SI8365 page 0000071 of 0000115

Page 118: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-9

EASTERN SURPLUSESLT-GW-MW23B-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

Methane

Ethane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

U

U

10.

10.

10.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2080.D

Katahdin Analytical Services SI8365 page 0000072 of 0000115

Page 119: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-10

EASTERN SURPLUSESLT-GW-IN7B-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

Methane

Ethane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

U

U

10.

10.

10.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2081.D

Katahdin Analytical Services SI8365 page 0000073 of 0000115

Page 120: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-11

EASTERN SURPLUSESLT-GW-MW3B-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

Methane

Ethane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

U

U

10.

10.

10.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2082.D

Katahdin Analytical Services SI8365 page 0000074 of 0000115

Page 121: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-12

EASTERN SURPLUSESLT-GW-MW58B1-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

Methane

Ethane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

U

U

10.

10.

10.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2083.D

Katahdin Analytical Services SI8365 page 0000075 of 0000115

Page 122: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-13

EASTERN SURPLUSESLT-GW-MW58B2-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

Methane

Ethane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

U

U

10.

10.

10.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2084.D

Katahdin Analytical Services SI8365 page 0000076 of 0000115

Page 123: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-14

EASTERN SURPLUSESLT-GW-MWRP-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

Methane

Ethane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

U

U

10.

10.

10.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2085.D

Katahdin Analytical Services SI8365 page 0000077 of 0000115

Page 124: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

Maine DEPSI8365-16

EASTERN SURPLUSESLT-TB-1015

SI8365

20-OCT-1521-OCT-15

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

Methane

Ethane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

U

U

10.

10.

10.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2069.D

Katahdin Analytical Services SI8365 page 0000078 of 0000115

Page 125: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://[email protected]

Cert No E87604

Form 4 Method Blank Summary

Lab Name : Katahdin Analytical Services SDG : SI8365

Lab File ID : 5IJ2067.DLab Sample ID : WG173026-1

This Method Blank applies to the following samples, LCS, MS and MSD:

11:48Time Analyzed :28-OCT-15Date Analyzed :

Instrument ID : GC05Heated Purge : No

WG173026-2SI8365-16WG173026-4SI8365-1SI8365-2SI8365-3SI8365-4SI8365-5SI8365-6SI8365-7SI8365-8SI8365-9SI8365-10SI8365-11SI8365-12SI8365-13SI8365-14WG173026-3RASI8365-1DLSI8365-3DL

Laboratory Control SESLT-TB-1015Matrix Spike DuplicaESLT-GW-MW51B-1015ESLT-GW-MW54B-1015ESLT-GW-MW55B-1015ESLT-GW-MW36B1-1015ESLT-GW-MW57B1-1015ESLT-GW-MW57B2-1015ESLT-GW-IN1B1-1015ESLT-GW-IN1B2-1015ESLT-GW-MW23B-1015ESLT-GW-IN7B-1015ESLT-GW-MW3B-1015ESLT-GW-MW58B1-1015ESLT-GW-MW58B2-1015ESLT-GW-MWRP-1015Matrix SpikeESLT-GW-MW51B-1015ESLT-GW-MW55B-1015

5IJ2068.D5IJ2069.D5IJ2071.D5IJ2072.D5IJ2073.D5IJ2074.D5IJ2075.D5IJ2076.D5IJ2077.D5IJ2078.D5IJ2079.D5IJ2080.D5IJ2081.D5IJ2082.D5IJ2083.D5IJ2084.D5IJ2085.D5IJ2086.D5IJ2088.D5IJ2089.D

10/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/1510/28/15

12:0512:2212:5613:1413:3113:4814:0514:2214:4615:0315:2015:3715:5416:1116:2816:4617:0317:2017:5418:11

Project : EASTERN SURPLUS

Client Sample ID Lab Sample ID Lab File ID Date Analyzed Time Analyzed

- VOA

Katahdin Analytical Services SI8365 page 0000079 of 0000115

Page 126: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

WG173026-1Method Blank Sample

SI8365

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

Methane

Ethane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Qualifier Result Units Dilution PQL ADJ PQL

U

U

U

10.

10.

10.

ug/L

ug/L

ug/L

1

1

1

10

10

10

10.

10.

10.

Cert No E87604

Report of Analytical Results

Lab File ID: 5IJ2067.D

Katahdin Analytical Services SI8365 page 0000080 of 0000115

Page 127: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

WG173026-2LCS

SI8365

28-OCT-15JMS

RSK SOP 175

28-OCT-15

WG173026

AQNA

JMSRSK SOP 175

Methane

Ethane

Ethene

29-OCT-15

Client:

Project:

Sample Date:

Extraction Method:

Analysis Method:

Report Date:

Lab ID: Received Date:

Extracted By:

Analyst:

Matrix: Client ID:

SDG:

Extract Date:

Analysis Date:

Lab Prep Batch:% Solids:

Compound Recovery (%) Conc Added Conc Recovered Conc Units

115.

114.

118.

133.

249.

233.

153.

283.

274.

ug/L

ug/L

ug/L

Cert No E87604

LCS Recovery Report

Limits

70-130

70-130

70-130

5IJ2068.DLCS File ID:

Katahdin Analytical Services SI8365 page 0000081 of 0000115

Page 128: GROUNDWATER MONITORING REPORT EASTERN SURPLUS …

600 Technology WayP.O. Box 540, Scarborough, ME 04070Tel:(207) 874-2400 Fax:(207) 775-4029

http://www.katahdinlab.com

Page of1 1

WG173026-3RA

SI8365

28-OCT-15 JMSRSK SOP 175

28-OCT-15

WG173026AQ

NA

JMSRSK SOP 175

Methane

Ethane

Ethene

29-OCT-15Project:

Extraction Method:Analysis Method:

Report Date:

MS ID: Received Date:

Extracted By:Analyst:

Matrix:

SDG:

Extract Date: Analysis Date:

Lab Prep Batch: % Solids:

CompoundMS Rec

(%)MS

SpikeMS

Conc

113.

111.

116.

133.

249.

233.

150

280

270

Cert No E87604

MS/MSD Recovery Report

Limits

MSD ID:

Conc Units

MSD Rec(%)

MSDConc RPD (%)

RPD Limit

112.

111.

115.

150

280

270

1

0

0

30

30

30

70-130

70-130

70-130

ug/L

ug/L

ug/L

WG173026-4

U10.

U10.

U10.

SampConc

MSD Spike

133.

249.

233.

Sample ID: SI8365-10Client ID: ESLT-GW-IN7B-1015

5IJ2086.DMS File ID: 5IJ2071.dMSD File ID:

Katahdin Analytical Services SI8365 page 0000082 of 0000115

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Katahdin Analytical Services SI8365 page 0000087 of 0000115

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Katahdin Analytical Services SI8365 page 0000088 of 0000115

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Katahdin Analytical Services SI8365 page 0000089 of 0000115

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Katahdin Analytical Services SI8365 page 0000090 of 0000115

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Katahdin Analytical Services SI8365 page 0000091 of 0000115

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Katahdin Analytical Services SI8365 page 0000092 of 0000115

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Katahdin Analytical Services SI8365 page 0000093 of 0000115

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Katahdin Analytical Services SI8365 page 0000098 of 0000115

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Katahdin Analytical Services SI8365 page 0000099 of 0000115

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Katahdin Analytical Services SI8365 page 0000100 of 0000115

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Katahdin Analytical Services SI8365 page 0000101 of 0000115

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Katahdin Analytical Services SI8365 page 0000102 of 0000115

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Katahdin Analytical Services SI8365 page 0000103 of 0000115

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Katahdin Analytical Services SI8365 page 0000104 of 0000115

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Katahdin Analytical Services SI8365 page 0000107 of 0000115

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Katahdin Analytical Services SI8365 page 0000111 of 0000115

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Katahdin Analytical Services SI8365 page 0000112 of 0000115

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Katahdin Analytical Services SI8365 page 0000113 of 0000115

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