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Hard and Fast- The Cement Challenge_MiddleEast Reservoir Review, 2001

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    Achieving full isolation between producing

    zones has always been a major challengefor cement technologists. In some areas of

    the Middle East this is particularly difficult

    to achieve in tophole sections. In every

    well, the optimization of cement slurry to

    take account of the difficulties presented

    by formations, borehole conditions and

    wellbore fluids, and to produce a set

    cement with the necessary mechanical

    properties is a complex business.

    Here, Jo Schultz and Andrew James

    outline the problems that face cementing

    engineers in the field and explain how

    attention to particle size and distribution

    has resulted in a range of high-

    performance cements.

    Hard and fast the cement challenge

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    M i d d l e E a s t R e s e r v o i r R e v i e w

    Figure 6.2:USI*

    Ultra Sonic Imager

    images showing

    early casing

    corrosion

    The successful isolation of drilled-

    through formations is extremely

    important in preventing the migration of

    gas and fluid and limiting their

    environmental impact. It has been

    estimated that around 70% of all gas

    wells have some kind of zonal-isolation

    problem. A good, primary cement job

    could have prevented most of these

    situations and the subsequent remedial

    work. There has always been a conflict

    for conventional oilfield cements

    between optimizing slurry properties for

    mixing and placement and the resulting

    mechanical properties of set cement

    necessary for long-term zonal isolation.

    In the Middle East, zonal isolation has

    been difficult to achieve in tophole

    sections. This is due to a low fracture

    (rock failure) pressure gradient and the

    existence of highly expansive and

    fractured, vugular or cavernous dolomite

    formations such as the Wassila, Simsima,

    Shuiaba or Umm El Radhuma sequences.

    On many occasions, standard, lightweight

    cement systems have failed to provide

    the necessary zonal isolation because of

    the complex demands placed on the

    slurry. Even with the sealants and special

    casing tools that have been developed for

    complex situations such as these, the

    entire casingformation annulus is

    seldom fully isolated.

    In another Middle Eastern scenario, a

    promising oil source in South Oman is

    providing challenges to successful, high-

    density cementing operations in deep

    wells with high bottomhole pressures

    and a very narrow margin between

    formation, pore and fracture pressures.

    New technology, which focuses on the

    size and distribution of particles in the

    cement, has produced a lightweight

    slurry system with reduced water

    content that gives the set cement an

    inherent high compressive strength,

    along with low porosity and permeability.

    This increases the systems durability by,

    for example, reducing the ability of fluids

    to penetrate through the casing, which,

    in turn, arrests the onset of corrosion.

    The same principles have been applied in

    producing a range of high-density, high-

    performance slurries (HDHPS).

    Traditional cementing

    Well cementing was introduced by

    Portland Cement in 1901. This was seen

    as the most readily available, economical

    and simple means of filling the annulus

    between pipe and formation. Fluid

    density was adjusted to suit the

    hydrostatic pressure involved by

    changing the amount of water added

    during mixing.

    Cement was pumped down to the

    lowest point in the well, then back up the

    casingformation annulus. A common

    problem was contamination of the cement

    by the drilling fluid that it was displacing.

    Chemicals in the drilling fluid affected

    both the setting rate and the mechanical

    properties of cement. To overcome this,

    another fluid compatible with both the

    drilling fluid and the cement was pumped

    ahead of the cement. This fluid also

    helped to clean the casing and the

    formation prior to cementing.

    Optimizing these and all the other

    operational variables, such as correct

    pressure maintenance, was a major

    challenge. Software such as CemCADE*

    cementing design and evaluation

    software (Figure 6.1) was developed for

    this purpose and is constantly being

    updated to keep pace with new

    cementing challenges and changing

    slurry technologies. The main

    considerations are:

    Proper pressure control in the well at

    all times. The total pressure exerted

    by moving fluid on the formation is

    maintained between the pore pressure

    and the fracture pressure of the

    drilled-through formations. If this

    pressure becomes too low, fluid can

    flow between zones and could cause a

    blowout. If it becomes too high, fluid

    will be lost to the formation

    Figure 6.1:

    CemCADE dynamic

    pressure simulation

    software for the

    design and

    evaluation of

    cement jobs

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    M i d d l e E a s t R e s e r v o i r R e v i e w

    MD, ftGR(0-100 GAP)

    FMI images FMS100

    porosity(pu)

    Hist.0

    0.50.5

    00

    Log eff.por.FMI por.

    0 90Dips

    Cavityin connectionwith fractures

    Cylindrical view(dynamic images)

    Horizontal well

    100% mud losses are

    encountered below 6770 ft.In this interval, openfractures, cavities, andsolution-enhancedfeatures are observed

    Open fractures

    Secondary porositydue to vugs and fractures

    6782

    6784

    6786

    6788

    6792

    6794

    6796

    Dips of openfractures

    Large, open cavity causes veryhigh porosity computation

    Open fractures

    Secondaryporosity

    Secondary

    porosity

    Secondary porositydue to large cavities

    and open fractures

    The use of additives to control the

    frictional pressures caused by fluid.

    These pressures will also increase

    along with viscosity, elapsed time,

    temperature, loss of fluid to the

    formation, or combinations of these

    factors. As a result they can cause

    bridging in the annulus (due to

    premature cement setting) with

    disastrous results

    Simulation of spacer and cement

    placement at well conditions to ensure

    optimum displacement of the mud

    The design of preflushes to reduce

    risks of channeling (channels of

    unremoved drilling mud), which can

    lead to the production of formation

    fluids, gas migration to surface,

    decreasing production rates, early

    casing corrosion (Figure 6.2), and

    microannulus (hence loss of zonal

    isolation). Loss of zonal isolation results

    in loss of control between one zone and

    another (also known as underground

    blowout). Risks are minimized by

    optimizing flow regime selection,

    annular flow rate, preflush contact times

    and volumes and fluid designs.

    Figure 6.3: FMI images

    from the horizontal well

    show variations in rock

    appearance along the

    well. Porosity analysis

    from the images

    computes very high

    porosity across the

    vugs, large, open,

    solution-enlargedcavities, and fractures.

    Huge mud losses were

    encountered over this

    interval

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    M i d d l e E a s t R e s e r v o i r R e v i e w

    Cementing in low-pressure reservoirs

    In low-pressure reservoirs, the challenge

    is always to find an acceptable balance

    between the liquid slurry properties

    necessary to place the slurry

    successfully and the set cement

    properties once the slurry is in place.

    Often in low-pressure reservoircementing, problems with well balance

    between pore and fracture pressures

    arise even before the cementing

    operations begin. Extreme levels of water

    loss from the drilling fluid, or even the

    complete loss of the drilling fluid to

    the formation can occur. Current

    technologies cannot predict and manage

    these situations during drilling. Proper

    recognition and treatment of pressure

    changes can dramatically minimize their

    impact on primary cementing operations

    and can save operators between $100,000

    and $1,000,000 on the cost of a well.

    FMI* Fullbore Formation MicroImager

    data can help field managers to

    understand the extent of the vugs and

    fractures (Figures 6.3 and 6.4) and the

    mechanism of losses, and possibly help

    them to combat these losses with

    efficient solutions. Drilling fluid losses

    cause operational delays. Drillpipe must

    be removed to allow changes to pipe

    geometry for expensive and time-

    consuming circulation loss treatment.

    InstanSEAL* is a newly developed

    loss circulation treatment that can be

    pumped through the drill bit without

    interruption to the normal drilling

    operation. It has recently helped several

    companies to reduce the severity of

    drilling fluid losses (Figure 6.5) to a

    manageable level, and allowed the

    continuation of the drilling operation.

    The injection of a single fluid pumped

    through the bottomhole assembly

    (BHA) directly in front of the loss zone

    and sheared at the bit nozzles, rapidly

    generates a high-viscosity gel. This

    gelling mechanism ensures accurate

    placement of the treatment at the loss

    zones, and has a higher success ratio

    than treatments that require downhole

    temperature or fluid interaction.

    Reaction time for the change of the fluid

    (from a few seconds to an hour) is

    controlled by adjusting the activator

    concentration to match the planned

    Figure 6.4: FMI images from the vertical well showing an abrupt change in

    porosity type in the interval 45754620 ft. Huge mud losses were encountered

    in this interval due to a well-connected system of vugs and solution-enhanced,

    open cavities as shown by the images. Very high porosity is computed for such

    features due to their open nature.

    MD, ftGR(0100 GAPI)

    FMI dynamic images

    50

    FMI porosity histogram

    (pu) 0

    0.50.5

    00

    Log effective porosityFMI porosity

    4570

    4580

    4590

    4600

    4610

    4620

    4630

    4594

    4596

    Verticalscale1/100

    Verticalscale1/100

    Solution-enhanced cavity

    High FMI porosity due to vugs, largecavities and solution-enhanced fractures

    Secondary porosity

    fluid pump rates. After placement, the

    gel is stable for several weeks under

    downhole conditions, and provides

    enough time to drill and complete the

    section. The BHA can be pulled through

    the set gel. However, in cases where the

    asset team are trying to avoid damage to

    a producing zone, the gel can be broken

    with a weak acid.

    Another method used to prevent

    losses during cementing uses special

    ported tools, known as stage collars, in

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    M i d d l e E a s t R e s e r v o i r R e v i e w

    CG62P70 x80 100microns

    Figure 6.6: 35% foam-quality cement (top)

    62% foam-quality cement (bottom)

    0

    Well 1 Well 2 Well 3 Well 4

    200

    400

    600

    800

    1000

    Losses,

    bbl/hr

    BeforeAfter

    Figure 6.5: These case histories show that drilling fluid losses

    decrease dramatically after an InstanSEAL pill is pumped downhole

    lightweight slurry system based on

    CemCRETE* concrete-based oilwell

    cementing technology. This new system

    gives high compressive strength along

    with very low porosity and permeability of

    the set cement for longer durability and

    reduced casing corrosion.

    Traditional cementing:low-density, low-strength

    The traditional optimum water-to-

    cement ratio is 44% (unaltered Portland

    API class G cement mixed at a density of

    15.8 lbm/gal). This has moderate

    viscosity and acceptable levels of

    separation of free water from the slurry

    when settling. The set cement has a

    permeability to gas of about 0.1 md. Its

    compressive strength is more than

    sufficient, and, under normal

    circumstances, it is used as the anchor

    or tail-in slurry for casing strings.

    The following are some of the options for

    reducing the cement density:

    Adding more water. Adding too much

    water upsets the settling properties of

    the slurry and therefore collodial clays

    or polymers are needed to maintain

    stability. In addition, the set

    properties of the cement are affected.

    Compressive strength decreases with

    increasing liquid-to-solid ratio, and

    the porosity and permeability of the

    set cement increase. Any reduced-

    density system needing less water will

    have clear operational advantages

    Lightweight additives. The cement

    content of the dry powder is partly

    replaced with a lightweight aggregatesuch as diatomaceous earth, fly ash or

    hollow aluminosilicate or glass

    spheres. With this method, the

    stability of the system decreases

    rapidly below the 11.5lbm/gal mark as

    the lightweight material becomes the

    major component of the powder blend

    Foaming with gas. Gases such as

    nitrogen or compressed air are used

    to generate foam with the normal-

    density cement slurry. The

    permeability remains relatively low

    until a ratio of gas-to-cement slurry

    greater than 35% is reached. Above

    this ratio (referred to as foam

    quality), the permeability increases

    rapidly and the compressive strength

    falls. A 62% foamed cement exhibits

    interconnected bubbles contributing

    to high porosity and early corrosion

    attack (Figure 6.6).

    the casing string that allow the

    cementing of casing to be done in

    several stages. As a result of this phased

    cementing, the lower formations are

    never exposed to the full weight of the

    cement. The ports of the stage collars

    are closed after the cement has been

    pumped. The more sophisticated stage

    collars have inflatable seals or packers

    just below the opening ports. Theseisolate the pressure of the annular fluid

    above the ports completely from the

    weak lower formations.

    Unfortunately, even with such

    elaborate devices, successful isolation of

    the casingformation annulus is rarely, if

    ever, complete. To eliminate the stage

    collar and perform the cement job in

    a single stage would require very

    low-density slurries to reduce the

    hydrostatic pressure of the fluid column

    and prevent lost circulation or formation

    breakdown. Also, the ultralightweight

    slurry must not only perform during the

    placement stage but also after the

    cement has set. It must isolate the

    casing from formation fluids and prevent

    the movement of fluids from one

    formation type to another.

    This has been made possible by the

    introduction of a reduced-water,

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    M i d d l e E a s t R e s e r v o i r R e v i e w

    Packed particles equalperformance plus

    Recent advances in cementing technology

    have focused on the way particles fit

    together and the principle of solids

    fraction, as used in the construction

    industry. These are the key factors in

    optimizing set cement performance. The

    fraction of a volume of a blend that is

    actually occupied by solids (i.e., particles)

    is known as the packing volume fraction

    (PVF). When all the particles are identical

    spheres in a perfect, hexagonal, closest

    configuration, the PVF is 0.74. Randomly

    packed spheres, however, exhibit a PVF of

    0.64 due to the decreased efficiency of

    packing. A powder containing various

    sizes of particles will have a higher PVF

    since the smaller particles fill the voids

    between the larger ones.

    This concept has been used by

    Schlumberger in the oil field to develop

    the CemCRETE technology for

    designing new high-performance

    cement slurries. In this technology, a dry

    blend is designed that has the specific

    gravity to create a slurry of the required

    weight. At the same time optimum

    particle size distribution is used to

    maximize the PVF up to 0.87.

    The low-density application of this

    technology, the LiteCRETE* slurry

    system, has demonstrated properties

    superior to any other technology for

    lightweight cement design. The high-

    performance, low-density LiteCRETE

    mixture contains cement and a number

    of particulates with narrow ranges of

    particle diameter (Figure 6.7). To

    achieve the desired specific gravity for

    the dry blend, oilwell cement, silica flour

    (for bottomhole static temperatures

    exceeding 230F) and correctly sized,

    lightweight particles are used in

    optimum ratios.

    The high-performance, lightweight

    cements of the CemCRETE family

    display remarkable slurry and set

    properties. The development of early

    compressive strength is very fast, as

    indicated by the relatively short time

    elapsed between 50psi and 500psi of all

    CemCRETE-based slurries. As a result,

    waiting on cement time during drilling

    operations is considerably reduced. The

    24-hr compressive strengths are also

    very high compared with other

    lightweight, conventional cement

    systems. The latest developments allow

    slurries to match the densities of drilling

    fluids. A 8.0-lbm/gal slurry with a water-

    to-solid ratio of 42% will develop a 24-hr

    compressive strength of 1300psi,

    whereas a 8.9-lbm/gal slurry reaches a

    compressive strength of 2733psi

    in 24 hr.

    An additional benefit of the high-

    solids fraction of CemCRETE

    technology, is the permeability of the set

    cement when compared to a

    conventional 15.8-lbm/gal system.

    LiteCRETE, even at 11lbm/gal, displays

    permeabilities 10 times lower than

    conventional set cement and effective

    porosity is around 22%, compared to

    34% for the conventional neat system.

    Drilling 121/4-in. holeTwo-stage cementconventional slurry

    One-stage cementlightweight slurry

    Hyd. press.At zone 'A'= 0.62 psi/ftAt zone 'C'= 0.65 psi/ft

    Hyd. press.At zone 'A'= 0.56 psi/ftAt zone 'C'= 0.58 psi/ft

    Mud weight10.5ppg

    (79 pcf)

    133/8 -in. casingat 5880ft

    10.5 ppg(79 pcf)

    12.7 ppg

    15.8 ppg16.7 ppg

    15.8 ppg16.7 ppg

    Lightweight11 ppg(82 pcf)

    Hyd. press.At zone 'A'= 0.55psi/ftAt zone 'C'= 0.55psi/ft

    Figure 6.8: Previous

    and most recent

    technology for

    cementing 95/8-in.

    casing string interval

    Figure 6.7:

    LiteCRETE particles

    fill maximum pore

    space

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    Cement medium particles

    Fine particles

    Coarse particles

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    M i d d l e E a s t R e s e r v o i r R e v i e w

    Answers for Abu Dhabi

    Cementing 95/8-in. casing in land wells in

    Abu Dhabi presents unique challenges.

    High hydrostatic pressure is required to

    control the shale sections, and there is a

    high pressure contrast between different

    reservoir units. Under these conditions,

    considerable losses into depleted aquifer

    zones have been experienced. Losses

    during cementation, poor performance of

    the stage collar tool and poor mechanical

    properties of the set cement resulted in

    unsatisfactory primary cementing. These

    challenges had previously been addressed

    by cementing in two stages. A comparison

    between the previous and the most recent

    technology is shown in Figure 6.8.

    In more than 50 successful cases for

    this customer, improved casing

    protection and mechanical properties

    have been achieved with LiteCRETE

    systems. A 95/8-in. casing is set just

    above the reservoir, a few feet below

    Nahr Umr shales at 80008500ft and at

    85009000ft to cover the Shuiaba

    reservoir pay zone. In special cases,

    LiteCRETE is also used for loss

    circulation plugs during drilling. A

    typical USI tool/variable density log is

    shown in Figure 6.9.

    400 (US)

    Transit time (sliding gate)(TTSL)

    200 0 (mV)

    CBL amplitude (CBL)

    100200 (US)

    Amplitude

    1200

    Max.

    VDL variable density(VDL)

    Min.

    Min. ofamplitude(AWMN)

    Externalradius

    average(ERAV)

    (in.)5 4

    Externalradius

    average(ERAV)

    (in.)4

    0.08000.00400.0800

    0.25002.00004.0000

    0.30003.10914.0000

    5

    Min. ofthickness

    (THMN)(in.)

    0.1 0.6(DB)0 75

    0 (mV)

    CBL amplitude (sliding gate)(CBSL)

    100

    0

    Tension(TENS)

    (lbf)

    8100

    8200

    1000

    -20

    CCL(CCLU)(----)

    20

    0 (GAPI)

    Gamma ray (GR)

    70

    400 (US)

    Transit time (TT)

    200

    Internalradii

    minusave.

    (IRBK)(----)

    Rawacousticimped.(AIBK)(----)

    Bonded Cement map withimpedance

    classification(Al_MICRO_

    DEBONDING_IMAGE)

    (----)

    Figure 6.10: Coarse, medium and fine

    particle distribution in HDHPS blend matrix

    Figure 6.9: A typical USIT/VDL log

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    M i d d l e E a s t R e s e r v o i r R e v i e w

    These systems are applied at one of

    two surface densities: 10.0l b m / g a l

    (75pcf) and 10.5 l bm / ga l (79pcf).

    The downhole density increases due to

    compaction of the lightweight particles

    under the weight of wellbore fluids,

    resulting in 10.5 l b m / g a l (79 pcf) and

    11.2l b m / g a l (84 pcf) respectively.

    High-density, high-performance slurries

    High-density, high-performance

    (HDHPS) technology optimizes slurry

    placement performance and ensures a

    high-quality set cement. It allows

    slurries with densities up to 24 lbm/gal

    (2900 kg/m3) to be used to cement

    critical casing strings in wells with high

    pressure gradients.

    Using particle size distribution (PSD)

    optimization, particles of at least three

    different sizes are selected (Figure 6.10).

    Adjusting the PSD allows engineers to

    introduce more solids per unit volume

    than would be possible with a

    conventional cement slurry. The

    compressive strength of the set cement

    is increased, and the porosity and

    permeability are lowered due to the

    higher PVF that is achieved, regardless

    of the slurry density. HDHPS technology

    usually requires lower concentrations of

    most chemical additives than

    conventional technology.

    As with low-density applications, the

    smaller particles in the blend act like

    ball bearings in providing extra lubricity.

    HDHPS blends are more stable during

    transportation than conventional

    hematite blends, and less susceptible to

    segregation of the various particles.

    Testing has shown that the major

    advantages of HDHPS are:

    High-density slurry designs (up to

    24 lbm/gal) are possible with

    controllable and adjustable rheology

    More field-tolerant, less sensitive to

    possible density fluctuations and

    more stable

    Density adjustment of 0.5lbm/gal is

    possible using the same blend. This

    provides system flexibility for of last-

    minute changes in mud weight.

    More tolerant to mud contamination

    Higher early compressive strength

    development

    Uniform and faster setting over a

    range of temperatures prevents well

    instability and kicks

    Higher final compressive strength

    Lower bulk shrinkage

    Lower permeability and porosity

    South Oman case study

    In the southern Oman oil fields, operators

    are exploring the production potential of

    oil and gas from high-pressure carbonate

    stringers embedded in salt. The

    cementing operations face a range of

    challenges, including depths of

    3,5004,800m, temperatures of 95125C

    and bottomhole pressures of 13,000psi.

    The high densities required of the

    cement slurries were achieved initially

    using hematite as the weighting agent.

    This gives a low Bingham-yield-point

    slurry that is easily placed. The lower

    water content reduces sedimentation,

    the superior mechanical properties

    develop more quickly and waiting on

    cement time is significantly reduced

    (see Figure 6.11).

    HDHPS does not need specialized

    equipment or personnel and the slurries

    are more tolerant to mixing errors or

    density variations. The dry blends may be

    mixed with fresh, sea or salt water.

    Optimized suspensions can include

    conventional defoamers, accelerators,

    dispersants, retarders, fluid loss and

    control additives, and latex additives to

    control gas migration.

    20

    18

    16

    14

    12

    10

    8

    6

    4

    2

    0

    5000

    4500

    4000

    3500

    3000

    2500

    2000

    1500

    1000

    500

    0

    Transittime,

    sec/in.

    Compressivestrength,

    psi

    177

    159.3

    141.6

    123.9

    106.2

    88.5

    70.8

    53.1

    35.4

    17.7

    0

    Temperature,

    C

    0:00 1:45 3:30 5:15 7:00 8:45 10:30 12:15 14:00 15:45 17:30 19:15 21:00

    Time (HH:MM)

    UCA initial: 50 at 4:37UCA strength 1500 at 5:20

    UCA strength 4280 at 20:04Comments: HDHPS at 19.5 ppg and 90C

    Figure 6.12:Graphical comparison of conventional slurry and HDHPS in

    terms of waiting on cement time and cement contamination for plugs

    0

    50

    250

    300

    350

    400

    200

    150

    100

    HDHPS plugs,wells 47

    Conventional plugs,wells 13

    Time,h

    r

    WOC time, hr

    Actual TOC belowtheoretical TOC

    1 2 3 3 4 4

    Well

    5 6 6 7 7

    Figure 6.11:Compressive strength development for HDHPS

    slurry measured at 90C

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    Physical and chemical robustness. The

    salt-saturated mud necessarily used

    affects the cement slurry and the set-

    cement properties. In the past, this

    has resulted in a large column of

    contaminated slurry, making it

    necessary to repeat some plugs. Other

    problems arose due to microannulus

    caused by bulk shrinkage on setting

    that compromised zonal isolation.

    In addition to transportation and

    handling problems, placement and set-

    cement mechanical properties were

    below expectations. This led to a number

    of problems, including loss of

    homogeneity in the blend during

    transportation caused by the hematite

    separating from the blend. A well kicked

    14 hr after cementing, causing the loss of

    four days in controlling the well. In

    addition, engineers had to deal with a

    build-up of annulus pressure. This was

    possibly due to microannulus caused by

    bulk shrinkage after cement setting, or to

    improper mud displacement. Downhole

    contamination led to increased setting

    time and four plugs had to be repeated

    after setting lower than planned.

    Intrasalt stringers set

    challengesIn conventional, high-density cement

    slurries, chemical additives, the amounts

    and types of solid, water volume,

    temperature and pressure all affect

    performance. Although chemical

    additives are helpful up to a point,

    cement performance at high densities is

    largely a function of density.

    Density can be increased by reducing

    the water content of the blend or by

    adding weighting materials. Both options

    have their drawbacks. Water reduction

    beyond a certain level causes the slurry

    to become unpumpable or unmixable.

    Adding weighting materials such as

    barite, hematite or ilmenite begins to

    cause problems with segregation and

    separation. The cementing operations

    face a range of challenges.

    HDHPS technology was seen as the

    way forward for addressing the major

    challenges that engineers face in liner

    and plug cementing for these wells:

    Enhanced isolation requirement. 100%

    zonal isolation is essential for testing

    and for separate production from

    adjacent stringers

    Placement pressure restrictions. The

    pressure window between the

    formation pore and fracture pressures

    is small. This results in a small density

    differential between the salt-saturated

    mud system, the spacer and the

    cement slurry. The cement-slurry

    rheology must be low enough for

    successful placement and, at the same

    time, sufficient to suspend the

    weighting agents

    Properties Conventional slurry HDHPS slurry

    Density, lbm/gal 19.5 19.5

    PV, cP 126 110

    TY, lb/100ft2 20 8.5

    Gels 1min/10min 14/125 9/65

    Fluid loss API cm3/30 min 204 64

    8-hr compressive strength, psi 0 2698

    Initial set 50 psi After 18hr 29 min After 5hr 44 mins

    24-hr compressive strength, psi 1750 3700

    Stability of set cement (BP settling test) 0.30lbm/gal top to bottom 0.15lbm/gal top to bottom

    24-hr compressive strength, psi 1750 3700

    Bulk shrinkage 1.5% after 24hr 0% after 24hr

    Separation of heavy particles fromblend during transport

    High risk Very low risk

    Tolerance to density variation Low High

    Table 1: Comparison of properties of HDHPS and conventional slurry for liner applications

    Job date BHCT, C Well name

    1 Feb 98 38 Yard trial

    20 May 98 90 Well-122 May 98 90 Well-1

    25 May 98 80 Well-1

    20 Sep 98 90 Well-2

    23 Sep 98 85 Well-2

    15 Jan 99 90 Well-3

    24 Jan 99 90 Well-3

    28 Apr 99 90 Well-4

    Job type

    HDHPS

    PlugPlug

    7-in. liner

    Plug

    Plug

    7-in. liner

    4-in. liner

    7-in. liner

    Depth, m

    No

    43004100

    3850

    4713

    3533

    4520

    4674

    4418

    HDHPS density, lbm/gal

    19.5

    21.621.6

    19.5

    22.1

    22.1

    19.1

    19.1

    19.5

    Table 2: HDHPS jobs done to date in South Oman

    Wells Cement type, hr WOC time, hr

    Well-1 Conventional 45

    Well-2 Conventional 101

    Well-3 Conventional 40

    Well-3 Conventional 120

    Well-4 Conventional 79

    Well-4 Conventional

    HDHPS

    HDHPS

    HDHPS

    HDHPS

    71

    40

    37

    34

    26

    Well-5

    Well-6

    Well-6

    Well-7

    Well-7

    Conventional

    Actual top of cement vs plannedbelow tested depth, m

    54

    206

    330

    120

    344

    84

    105

    124

    135

    106

    50

    130

    Good cement

    Yes

    No

    Yes

    No

    No

    Yes

    Yes

    Yes

    Yes

    Yes

    No

    Table 3: Comparing results of HDHPS and conventional slurry in terms of waiting on cementtime and cement contamination for plugs

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    Application for Oman

    Before HDHPS was introduced in Oman,

    comprehensive tests were conducted at

    several research centers in Oman and

    overseas. The tests confirmed that

    HDHPS would surpass the critical

    performance requirements for wells in

    southern Oman. In addition to exceeding

    the performance of conventional cements

    in 8- and 24-hour compressive strength,

    stability and shrinkage tests, HDHPS

    cement offered superior optimization of

    slurry rheology and density (Table 1).

    A trial in early 1998 demonstrated that

    the HDHPS blend would not segregate

    during transport but would remain

    mixable after transport and easily meet the

    relevant design criteria for rheology,

    compressive strength and fluid loss.

    Compressive strength development for

    HDHPS and conventional slurry was

    M i d d l e E a s t R e s e r v o i r R e v i e w

    4000

    3950

    4050

    4100

    4150

    4200

    4250

    Tension

    (TENS)(lbf)

    (MW)Variable density (VDL)

    (US)

    Min. Amplitude Max.

    200 12000 50

    Gamma ray (GR)

    0 100 20004000

    Transit time (TT)

    (US)400 200

    Transit time (sliding gate) (TTSL)(US)400 200

    Casing collar locator (CCL)(----)-19 1

    Casing collarfrom (CCL) to T1

    Fluid-compensated CBL amplitude

    (CBLF)

    (GAPI)

    Figure 6.13: Cement

    bond log (CBL) forreservoir section

    showing excellent

    bond

    measured at various temperatures. Figure

    6.12 shows the performance at 90C.

    The first HDHPS cementing operation

    in Oman was performed in the second

    quarter of 1998. Cement plugs were set

    at 4,100 m (13,451 ft) and 4,300m

    (14,108ft) with 21.5lbm/gal slurry. A

    7-in. liner was set at 3,850m (12,631 ft)

    with 19.5-lbm/gal slurry. There was a

    fault around total depth, and mud losses

    were encountered. The operator

    decided to set cement plugs across the

    fault and then cement the liner using

    HDHPS for both operations.

    To date, eight HDHPS jobs have been

    performed for this operator, including

    four liner cementing jobs and four plug

    jobs (Table 2).

    The average waiting on cement (WOC)

    time for conventional cement before it

    could be tagged was at least 72hr. The

    average WOC for an HDHPS system was

    34 hr. HDHPS slurries were found to be

    less susceptible to contamination with

    mud. Table 3 and Figure 6.12 show the

    comparison between HDHPS and

    conventional slurries on WOC times and

    actual top of cement (TOC) tagged as

    compared to the planned TOC. The top

    of the HDHPS plugs tagged is closer to

    the theoretical top than that of

    conventional cement plugs. HDHPS

    rheology can be optimized relatively

    easily, which allows for more efficient

    displacement of drilling fluids.

    Uniformity of the blend was not

    reduced by transportation to the rig site.

    Mixing was smooth and without

    problems. Figures 6.13 and 6.14 show the

    CBL/VDL and CET log respectively for

    the cement jobs on the most recent wells.

    Excellent bonding was achieved over the

    full cemented section.

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    8

    Num

    ber

    2,20

    01

    M i d d l e E a s t R e s e r v o i r R e v i e w

    HDHPS is worth its weight

    HDHPS has eliminated a large number of

    the difficulties experienced previously in

    South Oman.

    Compressive strength is developed

    much more rapidly. This saves rig time

    by allowing drilling operations to

    resume sooner. Faster build-up of

    mechanical properties also reduces

    the risk of fluid influx from the

    formation during setting

    The reliability of the technology

    decreases the need for remedial block

    squeezes or repetition of plugs

    Lower porosity and permeability of set

    cements using this technology will

    increase the safe life of the wells by

    providing isolation of aquifers from

    hydrocarbon zones and also safer

    abandonment of well

    Low-permeability cements are more

    resistant to corrosive brines and there

    is less bulk shrinkage as the cement

    sets, resulting in superior isolation

    through time.

    According to the operators, the

    success of the HDHPS technology used

    so far in the eight jobs in South Oman

    has ensured that it will be the preferred

    system for critical cementation in all

    future high-pressure wells to be drilled

    in the region.

    4000

    3950

    4050

    4100

    4150

    4200

    4250

    Gamma ray (GR)

    (GAPI)0 100

    Relative bearing (RB)(Deg.)0 360

    Eccentering (ECCE)

    (MM)0 10

    WW (WW)

    (----)0 2

    CCLU (CCLU)

    (----)-0.95 0.05

    CSMN (CSMX)(psi)

    (psi)

    AR_CSMNfrom CSMN to

    RHT2

    5000 0

    CSMN (CSMN)

    5000 0

    ARF1

    Between REF1 and FFLG1

    ARF2

    Between REF2 and FFLG2

    ARF3Between REF3 and FFLG3

    ARF4

    Between REF4 and FFLG4

    ARF5

    Between REF5 and FFLG5

    ARF6

    Between REF6 and FFLG6

    ARF7

    Between REF7 and FFLG7

    ARF8

    Between REF8 and FFLG8

    Tension(lbf)

    20004000

    Figure 6.14:CET logfor a recent well


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