Disclosure to Promote the Right To Information Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public. इंटरनेट मानक “!ान $ एक न’ भारत का +नम-ण” Satyanarayan Gangaram Pitroda “Invent a New India Using Knowledge” “प0रा1 को छोड न’ 5 तरफ” Jawaharlal Nehru “Step Out From the Old to the New” “जान1 का अ+धकार, जी1 का अ+धकार” Mazdoor Kisan Shakti Sangathan “The Right to Information, The Right to Live” “!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता ह ै” Bhartṛhari—Nītiśatakam “Knowledge is such a treasure which cannot be stolen” IS 5409-1 (1985): Agricultural Liming Materials as Soil Amendments, Part 1: Hydrated Lime and Burnt Lime [FAD 7: Soil Quality and Gertilizers]
Transcript
Disclosure to Promote the Right To Information
Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public.
इंटरनेट मानक
“!ान $ एक न' भारत का +नम-ण”Satyanarayan Gangaram Pitroda
“Invent a New India Using Knowledge”
“प0रा1 को छोड न' 5 तरफ”Jawaharlal Nehru
“Step Out From the Old to the New”
“जान1 का अ+धकार, जी1 का अ+धकार”Mazdoor Kisan Shakti Sangathan
“The Right to Information, The Right to Live”
“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता है”Bhartṛhari—Nītiśatakam
“Knowledge is such a treasure which cannot be stolen”
“Invent a New India Using Knowledge”
है”ह”ह
IS 5409-1 (1985): Agricultural Liming Materials as SoilAmendments, Part 1: Hydrated Lime and Burnt Lime [FAD 7:Soil Quality and Gertilizers]
Gr2
IS: 5409 ( Part 1 ) ·1985
Indian StandardSPECIFICATION FOR
AGRICULTURAL LIMING MATERIALSAS SOIL AMENDMENTS
PART 1 HYDRATED LIME AND BURNT LIME
( First Revision)
UDC 631-821-1: 666'924'3
@ CopyriglU 1986
INDIAN STANDARDS INSTITUTIONMANAK BHAVAN, 9 BAHADUR SHAH ZAl'AB. MARO
NEW DELHI 110002
Fibrl/tJY)' J986
IS: 5409 ( Part 1 ) - 1985
Indian StandardSPECIFICAnON FOR
AGRICULTURAL LIMING MATERIALSAS SOIL AMENDMENTS
PART 1 HYDRATED LIME AND BURNT LIME
( First Revision)
Sod Amendments and Reclamation of Problem Soils SectionalCommittee, AFDC 45
ChairmtJrl
DR J. S. P. YADH~
Representme
Indian Council of Agrrcultural Research, New Delhr
SHRID.N.BH~llOAVA
DB K. L. JADW
SHRI]. V. K-\LOKltE
DR G. P. GUPTA ( Alternate)DB N. C. DEBNATH
DR M. G. DXSH1"ANDE
Membe,s
Du M. S. BAJWA Punjab Agricultural Unrverauv , LudhfanaDR B HAJAN SING 11 ( Alternate)
SlIRI M. S. HAL Department of Agriculture, Government of Punjab,Chandigarh
Indian Bureau of Mines, Mrmstrv of Steel & Mines,Nagpur
SHRI A S. GOPALACJIARI ( Alternate)DR P. C. BH.-\TJA Indian Council of Agricultural Research, New DelhiSHut D. C. Dxs JOint Commrssroner ( 5011 Conservanon ), Mirustrv
of Agerculture & Rural Development, New Delhi
Hidhan Chandra Kr.rsb i Vrswa Vrdyalay a, Kalya mDepartment of Agrrculture, Government of
Karnataka, Bangalore8RB.I P. G. Drvn Hmdustan Copper Ltd, Calcutta
SHHI P. CHOUIJHURJ ( Alternate)DR C. P. GHoNSIKAR Marathwada Agricultural Universuv, Perbam
DR G U. MALEWAR ( Alternate)DR R. N. G~l"TA Department of Agr tcu lture, Governme-nt of Utfar
Pradesh, LucknowDirectorate of Agrrcuhure, Government of Gujarar,
AhmadabadDn-ectorate of Agriculture Maharashtra State,
Thrs pubhcatlon IS protected under the /tuiulJI Cop>f"I!!;ht Act (XIV of LCJ57) andreproduction in whole or an pan by any means except wrth wruten oernueocn of thepublISher shalT be dpeDll!"d to bE' a.n lnfrm,Elf'lT'eot 0{ cQp"~nght under the said ACE.
Himachal Pradesh Agncultural Umveranv, SolanA P Agncultural UmVPTSlty, HyderabadDirector General, lSI ( Ex-ojJieto Memb~r)
Dn M K SINHA
Drl B P ~AHI ( AII".at. )DRS. B SINHA
DR T A. SINGH
S HRI Y. K. SHARMA
Representing
Department of Agriculture, Government of Andhr&Pradesh, Hyderabad
SHR! P V. KRISHNA RAO ( AII.,.al.)SHRI K. L LUTHRA Pvrues, Phosphates & Chemicals Ltd, New Delhi
SaRI P. K AWASTHI ( Alternate)DR K T MARAJAN Rashtnya Chemicals & Fertilizers Ltd, BombayDR MAHYN'"DRA SINGH College of Agriculture, Haryana Agrlcultural
Umve rsrt y , HrssarDR S C Mvnasw xur The Peeuheer Assoctatron of India, New DelhIDR A K. NATH A5Sam Agrrculrural Umversny, JorhatDR M. M. PATf"L Khar Land Development Board. AhmadabadDR N D. PA'JIL Mahatma Phule Agr.rcultural Umversrty, RahuriDK K P RAJARAM Kerala Agricultural University, TrichurS.HRI P. jAYANTHA RAO Mrrnsn-y of Petrcdeum & ChemicalsSHRI B B. ROH<\TGI The Ferrrbzer Corporanon of Indra., New Delhi
SHRI A K HINDU ( AII".al. )SH.RI M N. RoY Rajasthan State Mines & Mmerals Ltd, UdaipurDR M B. SEN GUPI'A Indian Agncultural Research Institure, New DelhjDR D N SHARMA Chander Shekher Azad Um versrty of Agnculture &.
Technology, KanpurRajas-than State Industr-ial Development & Invest
ment Corporarron Ltd, jalpurCollege of Agnculture, G B Pant University of
Agriculture & Technologv, PanrnagarRajendra Agrrcultura l University, Patna
Members
SHRI M. A KHA.YYAM
...Qa.B R. TRIPATHI
GBK. VENKATA RAJU
SURIT.PrrRNANANDAM,
Director ( Agn & Food)
Secretary
SHRI N. K GROVERDeputy Director ( Ag.. & Food ), lSI
Soil Amendments for Acid Soils Panel, AFDC 45 : PI
ConDmwDR B. R. TRIPATHI
Members
SKRI P K AWABTHIDR S. K SABA ( AII"."aU )
DR N. C. DEBNATH
DR P. B. DESHPANDE
Suer A. S. GoPALACHARI
DB M. M. KOSKY
Himachal Pradesh Agricultural University, SImla
Pyrites, Phosphates & Chemicals Ltd, New Delhi
Bidban Chandra Krjshr Vrswa Vrdvalaya, KalyaniUmverstty of Agricultural Sciences, Hebbal,
BangaJoreIndian Bureau of Mmes, NagpurKerala Agricultural University, Mannuthy
2
AMENDMENT NO. 2 SEPTEMBER 2012TO
IS 5409 (PART 1) : 1985 SPECIFICATION FORAGRICULTURAL LIMING MATERIALS AS SOIL
AMENDMENTS
PART 1 HYDRATED LIME AND BURNT LIME
( First Revision )
[Page 5, clause 5.2(b)] — Substitute ‘Quantity of the material in thepackage;’ for ‘Mass of the material in the package;’.
(FAD 7)
Reprography Unit, BIS, New Delhi, India
AMENDMENT NO, 1 MARCH 1996TO
IS 5409 ( Part 11 : 1985 SPECIFICATION FORAGRICULTURAL LIMING MATERIALS AS SOIL
AMENDMENTS
PART 1 HYDRATED LIME AND BURNT UME
( First Revisiofl)
(Page 3, clause 0.4 ) - Substitute '[S 1540 ( Part 2 ) :1990t' for 'IS : 1540( Part 2) -1978t',
( Page 3, foot-note marked 't' ) - Substitute '( third reviswn)' for '( second",,,,,,.on J' at the end of text.
( Page 5. Table I, column 6 ) - Substitute 'IS /514 1990·' for 'IS 15141959",
(Page 5, foot-note mnrked '.' ) -Add '(/i,..t TPv,,,on) ' at the end of text
( Page 6, clallse 6 I ) - Substitute '[S 1514 : 1990" for 'IS: 1514 1'159·' ,
( Page 6, foot-note marked ' •• ) - Add '(first rev;"on)' at the end of text
( Page 6, clause 72 )- Substttute '(see IS uno :l992t)' for '(seeIS: 1070 . 1977t)'.
( Page 6, [oa-note marked 't') - Substitute 'Reagent grade ,..Ier ( thirdrev",.,,;' for the exisnng title
(FAD27)Reprography UBi!, 6IS, New Delhi~ India
IS : 5409 ( Part I ) • 1985
Indian StandardSPECIFICATION FOR
AGRICULTURAL LIMING MATERIALSAS SOIL AMENDMENTS
PART 1 HYDRATED LIME AND BURNT LIME
( First Revision)
O. FO R E W 0 R D
0.1 This Indian Standard (First Revision ) was adopte d by the IndianStandards Insnrunon on 30 August 1985, after the draft finahzed by theSoil Amendments an d Reclamation of Problem Soils Sectional Committee had been approved by the Agncultural and Food ProductsDivision Council.
0.2 Hydrated lime and burnt lime, apart from being important rawmaterials for various chemical industries, are also used for correcungsoil acidity to create opum al plant growth conditions in acidrc soils.These amendments are among the few hrmng materrals known for theirhigh Calcium Carbonate Equivalent (CeE) percent and usually haverapid neutralizing effect on acidic soils.
0.3 This standard was first pubhshed in 1969 The liming materialssuch as limestone, dolomite, basic slag, sea shell", presvmud, by-product,calcium carbonate and by-product hydrated lime have been included.Since the neutralizing value and physical characteristics of limingmaterials vary to a great extent. It was considered desirable to prepareseparate specifications for different hming materials used as soil amendments. Hence, a series of Indian Standards covering different limingmaterials used as soil amendments is being prepared. Limestone anddolomite have been covered under Part 2. It is hoped that adoption ofthese standards would enable both consumers and producers for procuring and supplying quality materials.
0.4 The requirement. for quick lime and hydrated lime for chemicalindustries, have been covered in IS . 1540 ( Part I )-1980* and IS: 1540( Part 2 )·1978t respectively.
---_._--e Specifice.non for quick. lime and hydrated lime for chemical industr-ies; Part 1 Q .rick
lime { .seccmd TelJlSIOn r,tS pecrficanon {or qurck Itme and hydrated itme for chermca] mdusrrres: Part 2
Hydrated lime ( second reviSion).
3
IS : 540g ( Part 1 ) - Ig85
0.5 For the purpose of deciding whether a particular requirement ofthis standard is complied with, the final value, observed or calculated,expressing the I esult of a test or analysis, shall be rounded 011' inaccordance with IS : 2·1960·. The number of significant places retainedin the rounded off value should be the same as that of the specifiedvalue in this standard.
I. SCOPE
1.1 This standard ( Part I ) prescribes the requirements and methods ofsampling and test for hydrated lime and burnt lime used as soilamendments.
2. TERMINOLOGY
2.0 For the purpose of this standard, the following definitions shall apply.
2.1 Agricultural Liming Material - A product containing calciumand magnesiurn compounds capable of neutralizing soil acidity.
2.2 Calcium Carbonate Equivalent (CCE ) Percent - It is theacid neutralizing capacity or the agricultural liming material and isdefined as the number of parts by mass of pure calcium carbonate whichhas the same acid neutralizing capacity as 100 parts by mass of the
~ricultural limmg material
23 Hydrated Lhne - A powder obtained by treating quick lime withwater enough to satisfy its chemical affinity for water under the conditions of hydration.
2.4 Burnt Lime or Quick Lime - A calcmed material the majorpart of which is CaO or Ca'O III natural assocration with lesser amountof MgO, capable of slaking with water.
2.5 Active LilDe (Available) - The proportion of the limingmaterial which enters into a desired reaction under the conditions of aspecified method.
2.6 Dead, Burnt or Over-Burnt Lbne - Lime which is not madeavailable in any chemical reaction.
3. GRADES
3.1 There shall be two grades of liming materials, namely, Grade I andGrade II.
.Rules. far rounding off numerica! values ( ,.'lIased ).
4
IS : 5409 ( Part 1 ) - 1985
4. REQUIREMENTS
4.1 Fineness - When tested by the method prescribed in 15 ofIS : 1514-1959·, 90 percent of the material shall pass through 2-mm sieveand 25 percent shall pass through 0'15-mm sieve.
4.2 The material shall also comply with the requirements specified inTable I.
TABLE I REllUIREMENTS FOR HYDRATED LIME ANDBURNT LIME AS SOIL AMENDMENTS
v) Dead burnt hme ( as CaO ), 30 40 14percent by mass , Max
"Methods of samphng and test for qmck hme and hydrated lime.
5. PACKING AND MARKING
5.1 Packing - The material shall be supplied in bulk or in packages asagreed to between the purchaser and the supplier.
5.2 Marking - When supplied in packages, each package shallsecurely be closed and marked with the following information:
a) Name and grade of the material;b) Mass of the material in the package;
c) Neutralizing value and active CaO content of the material;
·Methods of sampling test for quick lime and hydrated lime.
5
IS : 5409 ( "art 1 ) • 1985
d) Supplier's name and recognized trade-mark, if any; ande) Lot number to enable the consignment to be traced back to the
record.
5.2.1 When supplied in bulk, a good sized metallic label bearing theabove information shall be conspicuously displayed on the bulk carrierand also placed inside.
5.2.2 The material may also be marked with the lSI CertificationMark.
NOTE - The use of the lSI Certificatron Mark ill governed bv the provisions of theIndIan Sr...ndards Instjtutwn (Certdication Marks) Act and the Rwles and Regulations made thereunder. The lSI Mark on products covered by an Indian Standardconveys tbe assurance that they have been produced to comply with the requirements of that standard under a well-defined syste-m of Inspection, testing and qualItycontrol which is devised and eupervrsed hy lSI and operated by the producer. lSImarked products are also contlnuouslv checked by lSI for conformity to thatstandard as a further safeguard Details of conditions under which a licence for the,use of the lSI Cerdfieanon Mark may be granted to manufacturers or processors,may be obtained from the Indian Standards Institution.
6. SAMPLING
6.1 The procedure for drawing representative samples of the materialand the criteria for finding out the conformity of the material to therequrrements of this specification .hall be as prescribed in:l of IS . 15141959·.
'7tn:STS7.1 Tests shall be carried out by the appropriate methods referred to incol 5 and 6 of Table 1.
7.2 Q.uality of Reagents - Unless specified otherwise, pure chemicalsand distilled water ( see IS : 1070-1977t ) shall be employed in tests.
NOTE - 'Pure chemicals' shaH mean chermca.ls that do nor contain impuritieswhich affect the result of analysis.
-Method! of samphng and test for quick lime and hydrated lrme.tSpeclficauon for water for general laboratory use ( slColid "l'JSlon ~.
6
IS : 5409 ( Part 1 ) • 1985
APPENDIX A( Table 1, Sl No. (i) ]
DETERMINATION OF NEUTRALIZING VALUE
A-O. PRINCIPLE - The ground sample is heated with an excess ofstandard acid and the excess acid is back-titrated.
A.1. REAGENTS
A-I.I Standard Hydrochloric Add - 0'5 N.
A-I.2 Standard Sodium Hydroxide Solution - 0'5 N.
A-I.3 Phenolphthalein Indicator Solution - Dissolve 0'1 g ofphenolphthalein in 60 ml of rectified spirit (conforming to IS: 3231959* ) and dilute with water to 100 ml,
A-'l. PROCEDURE
A-'l.1 Weigh accurately about 0'5 g of the previously groundsample to pass through 250,um IS sieve, 1U a 250-ml stopperedconical flask. Add 40 ml of standard hydrochloric acid, with swirling.Heat to gentle boiling, agitating continuously. Boil for 5 minutes andthen cool to room temperature. Titrate against standard sodiumhydroxide solution using 2 to 3 drops of phenolphthalein indicator.
A-2.1.1 Carry out a blank test usmg the same quantities of all reagents?"but without adding the sample.
A-2.2 Calculation
Neutralizing value ( as CaCGa ),percent by mass
5(B-A)NM
where
B = volume in ml of standard sodium hydroxide solutionused in the blank determination,
A = volume in ml of standard sodium hydroxide solutionused with the sample,
N = normality of standard sodium hydroxide solution, and
M = mass in g of the sample taken for the test.
·SpecJfication for rectified ,pirit ( 'llJ'Jld ).
1
IS : 5409 ( Part 1 ) - 1985
APPENDIX B[ Table 1, Sl No. (iv] J
DETERMINATION OF MOISTURE CONTENT
B-1. PROCEDURE
B-1.1 Weigh accurately 2 g of the powdered sample in a platinum orsilica dish. Place It in an Oven maintained at 105° ± 2°C, until oncooling in a desiccator and weighing, constant mass ( ± 2 rng) isobta ined. Calculate the percent moisture m the sample
B-2. CALCULATION
100 ( M1 - Mz )B-2.1 Moisture, percent by mass = M
1_ M
where
M 1 = mass III g of the moisture dish with the material beforedrying,
M z = mass in g of the moisture dish with the material afterdrying, and
M = mass in g of the empty moisture dish.
pSI1 I N D I A N S TAN 0 A R D SIN S TIT UTI 0 N
41 2442
87328
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He.dqusfttl / 8 J
Manak Shavan, 9 Bahadur Shah Zafar Marg, NEW DELHI 110002Telepnones : 3 31 01 31, 331 1376 Telegrams: ManaksanstM
