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Assessment Manager: KW Page 1 of 23 Schedule of Accreditation issued by United Kingdom Accreditation Service 2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK 4409 Accredited to ISO/IEC 17025:2005 ALS Environmental Ltd Wakefield Issue No: 090 Issue date: 11 December 2019 Unit 11, Silkwood Park Janes Hill Off Albert Drive Wakefield WF5 9TG Contact: Mr J Mace Tel: +44 (0)1924 818108 Fax: +44 (0)1924 818101 E-Mail: [email protected] Website: www.alsenvironmental.co.uk Testing performed at the above address only DETAIL OF ACCREDITATION Materials/Products tested Type of test/Properties measured/Range of measurement Standard specifications/ Equipment/Techniques used WATERS: Potable and Raw waters Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable Chemical Testing Potable and Raw waters Phenols: 2,3-Dichlorophenol 2,3-Xylenol WPC34 using Pentafluorobenzoylation and Gas Chromatography/Mass Spectrometry 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Xylenol 2,5-Xylenol 2,6-Dichlorophenol 2,6-Xylenol 2-Chloro-4-Methylphenol 2-Chlorophenol 3,4-Xylenol 3,5-Xylenol 3-Chloro-4-Methylphenol 3-Chlorophenol 4-Chloro-2-Methylphenol 2-Chloro-5-Methylphenol 4-Chlorophenol 2-Methylphenol 3-Methylphenol 4-Methylphenol Phenol
Transcript
Page 1: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

Assessment Manager: KW Page 1 of 23

Schedule of Accreditation issued by

United Kingdom Accreditation Service

2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK

4409

Accredited to ISO/IEC 17025:2005

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Unit 11, Silkwood Park

Janes Hill

Off Albert Drive

Wakefield

WF5 9TG

Contact: Mr J Mace

Tel: +44 (0)1924 818108

Fax: +44 (0)1924 818101

E-Mail: [email protected]

Website: www.alsenvironmental.co.uk

Testing performed at the above address only

DETAIL OF ACCREDITATION

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable and Raw waters

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS)

Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable

Chemical Testing Potable and Raw waters Phenols:

2,3-Dichlorophenol 2,3-Xylenol

WPC34 using Pentafluorobenzoylation and Gas Chromatography/Mass Spectrometry

2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Xylenol 2,5-Xylenol 2,6-Dichlorophenol 2,6-Xylenol 2-Chloro-4-Methylphenol 2-Chlorophenol 3,4-Xylenol 3,5-Xylenol 3-Chloro-4-Methylphenol 3-Chlorophenol 4-Chloro-2-Methylphenol 2-Chloro-5-Methylphenol 4-Chlorophenol 2-Methylphenol 3-Methylphenol 4-Methylphenol Phenol

Page 2: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 2 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable and Raw waters (cont’d)

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d)

Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable (cont’d)

Chemical Testing (cont’d) Potable and Raw waters THMs and other VOCs:

1,1,1-Trichloroethane WPC28 using Headspace Gas Chromatography with MS Detection

1,1- Dichloroethane 1,2-Dichloroethane Benzene Bromodichloromethane Bromoform Carbon Tetrachloride Chlorodibromomethane Chloroform Dichloromethane Ethylbenzene m&p-Xylene MTBE o-Xylene Tetrachloroethene Trichloroethene Potable and Raw waters PAHs: WPC27 using HPLC Benzo (b) fluoranthene Benzo(k)fluoranthene Benzo(ghi)perylene Benzo(a)pyrene Fluoranthene Indeno(1,2,3-cd)pyrene

Page 3: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 3 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable and Raw waters (cont’d)

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d)

Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable (cont’d)

Chemical Testing (cont’d) Potable and Raw waters Polar herbicides: WPC45 using LCMSMS 2,3,6-Trichlorobenzoic acid 2,4,5-T 2,4,5-TP (Fenoprop) 2,4-D 2,4-DB 2,4-DP (Dichloroprop) Asulam Benazolin Bentazone Bromoxynil Clopyralid Dicamba Fluroxypyr Imazapyr Ioxynil MCPA MCPB MCPP (Mecoprop) Pentachlorophenol Picloram Propamocarb Triclopyr Potable and Raw waters Acrylamide WPC53 using HPLCMSMS

Page 4: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 4 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable and Raw waters (cont’d)

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d)

Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable (cont’d)

Chemical Testing (cont’d) Potable and Raw waters Polar pesticides:

Atrazine Azoxystrobin Bixafen Boscalid Bromacil

WPC43 using direct aqueous injection with on-line solid phase extraction analysed by Triple Quadrupole LC/MS/MS

Carbetamide Chlorbufam Chloridazon Chlorpropham Chlorpyriphos-Ethyl Chlorpyriphos-Methyl Chlortoluron Clomazone Cyanazine Cyproconazole Difenoconazole Diuron EPTC Epoxiconazole Flufenacet Flurtamone Flusilazole Flutrifol Isoproturon Linuron

Metconazole Metoxuron Myclobutanil Tebuconazol

Simazine Trietazine Monuron Propham Prosulfocarb Trinexapac-ethyl Fenpropimorph Fluxapyroxad Spiroxamine

Page 5: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 5 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable and Raw waters (cont’d)

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d)

Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable (cont’d)

Chemical Testing (cont’d) Potable and Raw waters (cont’d) Polar pesticides: (cont’d)

Quinmerac Oxadixyl Metazachlor Pendimethalin Propachlor Propiconazole Propyzamide Prochloraz Propthioconazole-desthio

WPC43 using direct aqueous injection with on-line solid phase extraction analysed by Triple Quadrupole LC/MS/MS (cont’d)

Potable and Raw waters Organochlorine pesticides,

polychlorinated biphenyls and selected non-polar organic compounds:

WPC50 using solvent extraction and GCMSMS

Dichlobenil alpha-HCH Hexachlorobenzene gamma-HCH Chlorothalonil Heptachlor Aldrin cis-Heptachlor Epoxide trans-Heptachlor Epoxide o,p’-DDE p,p’-DDE Dieldrin o,p’-TDE Endrin p,p’-TDE o,p’-DDT p,p’-DDT Methoxychlor Parathion-Ethyl

Page 6: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 6 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable and Raw waters (cont’d)

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d)

Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable (cont’d)

Chemical Testing (cont’d) Potable and Raw waters (cont’d) Organochlorine pesticides,

polychlorinated biphenyls and selected non-polar organic compounds (cont’d)

WPC50 using solvent extraction and GCMSMS (cont’d)

Tecnazene Trifluralin cis-Permethrin trans-Permethrin Cyfluthrin Cypermethrin Fenvalerate Deltamethrin Chlorthal-dimethyl Parathion-ethyl Pentachlorobenzene Diazinon Diflufenican Kresoxim-methyl Lambda-Cyhalothrin Triallate Potable and Raw waters Chlormequat WPC69 by LCMSMS Mepiquat

Page 7: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 7 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable and Raw waters (cont’d)

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d)

Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable (cont’d)

Chemical Testing (cont’d) Potable And Raw waters Pesticides: WPC46 using LCMSMS Ametryn Azinphos-methyl Carbendazim Chlorfenvinphos Dichlorvos Dimethoate Ethofumesate Fenpropidin Fenpropimorph Malathion Methabenzthiazuron Methiocarb Mevinphos Pirimicarb Pirimiphos-methyl Prometryn Propazine Propetamphos Terbutryn Triazophos Atrazine-desethyl Atrazine-desisopropyl Ethoprophos Fluxapyroxad Lenacil Metribuzin Metsulfuron- methyl Spiroxamine Terbuthylazine Potable and Raw waters Glyphosate WPC68 using LVI & online SPE Aminomethylphosphonic acid

(AMPA) by LCMSMS

Page 8: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 8 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable and Raw waters (cont’d)

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d)

Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable (cont’d)

Chemical Testing (cont’d)

Potable and Raw waters Metaldehyde WPC31 using SPE GC/MS Potable and Raw waters Metaldehyde WPC62 using LC-qTOF MS Potable, River and Groundwaters Microcystin - LR WPC59 using LCMSMS Potable and Raw waters Haloacetic acids: WPC60 using GCMS MonoChloroAcetic Acid (MCAA) MonoChloroAcetic Acid (MCAA) MonoBromoAcetic Acid (MBAA) DiChloroAcetic Acid (DCAA) 2,2-DiChloroPropanoic Acid (Dalapon) TriChloroAcetic Acid (TCAA) BromoChloroAcetic Acid (BCAA) DiBromoAcetic Acid (DBAA) BromoDiChloroAcetic Acid (BDCAA) DiBromoChloroAcetic Acid (DBCAA) TriBromoAcetic Acid (TBAA) Potable and Raw waters Taste & Odour Compounds: WPC66 using GCMSMS 2- Bromophenol 2-6-Dibromophenol 2-4-Dibromophenol 2,4,6 -Tribromophenol 2-Isopropyl-3-methoxypyrazine 3-Chloroanisole 4-Chloroanisole 2-Chloroanisole 2-Isobutyl-3-methoxypyrazine 2-methylisoborneal 2,4,6-Trichloroanisole Geosmin 2,3,4-Trichloroanisole 2,4,6-Tribromoanisole

Page 9: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 9 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable and Raw waters (cont’d)

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d) Chemical Testing (cont’d)

Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable (cont’d)

Potable and Raw waters Ametryn WPC71 - using direct aqueous Atrazine injection with on-line solid phase Atrazine-desethyl extraction analysed by Triple Atrazine - desisopropyl Quadrupole LC/MS/MS

Azinphos-methyl Azoxystrobin Bixafen Boscalid Bromacil Carbendazim Carbetamide Chlorbufam Chlorfenvinphos Chloridazon Chlorpropham Chlorpyriphos-Ethyl Chlorpyriphos-Methyl Chlortoluron Clomazone Cyanazine Cyproconazole Dichlorvos Difenoconazole Dimethoate Diuron Epoxiconazole EPTC Ethofumesate Ethoprophos Fenpropidin Fenpropimorph Flufenacet Flurtamone Flusilazole Flutrifol Fluxapyroxad Isoproturon

Lenacil

Page 10: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 10 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable and Raw waters (cont’d)

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d)

Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable (cont’d)

Chemical Testing (cont’d) Potable and Raw waters Linuron WPC71 - using direct aqueous Malathion injection with on-line solid phase Metazachlor extraction analysed by Triple Metconazole Quadrupole LC/MS/MS Methabenzthiazuron Methiocarb Metoxuron Metribuzin Metsulfuron-methyl Mevinphos Monuron Myclobutanil Oxadixyl Pendimethalin Pirimicarb Pirimiphos-methyl Prochloraz Prometryn Propachlor Propazine Propetamphos Propham Propiconazole Propyzamide Prosulphocarb Propthioconazole-desthio Quinmerac Simazine Spiroxamine Tebuconazole Terbuthylazine Terbutryn Triazophos trietaxzine Trinexapac-ethyl

Page 11: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 11 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable and Raw waters (cont’d)

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d)

Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable (cont’d)

Potable and Raw waters Chemical Testing (cont’d) WPC70 by GCMS Phenol 2-Methylphenol 3-Methylphenol 4-Methylphenol 2-Chlorophenol 3-Chlorophenol 4-Chlorophenol 2,3-Dimethylphenol 2,4-Dimethylphenol 2,5-Dimethylphenol 2,6-Dimethylphenol 3,4-Dimethylphenol 3,5-Dimethylphenol 2-Chloro-4-methylphenol 2-Chloro-5-methylphenol + 4-

Chloro-2-methylphenol

3-Chloro-4-methylphenol 2,3-Dichlorophenol 2,4-Dichlorophenol 2,6-Dichlorophenol 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol

Page 12: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 12 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable and Raw waters (cont’d)

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d)

Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable (cont’d)

Chemical Testing (cont’d) Potable and Raw waters pH WPC 8 using manual meter Potable and Raw waters Conductivity WPC 7 using manual meter Potable and Raw waters Turbidity WPC 6 using manual meter Potable and Raw waters Colour WPC13 using UV-Vis spectrometer Potable and Raw waters Fluoride WPC20 using Ion Selective

Electrode Potable and Raw waters Suspended Solids (105 C) WPC22 by gravimetry

Potable and Raw waters Total Dissolved Solids (180 C) WPC25 by gravimetry

Potable and Raw waters Chlorite, Chlorate, and Bromide WPC18 Potable and Raw waters Chlorite, Chlorate, and Bromide WPC61 using ion chromatography Potable and Raw (Surface & Bromate WPC42 using IC (Dionex) Ground) waters Potable and Raw waters Bottled waters

Free Cyanide Total Cyanide

WPC65 using continuous flow autoanalyser

Potable and Raw waters Metals (total and dissolved):

Iron Aluminium Manganese Phosphorus Sulphur as Sulphate (SO4) Silicon as Silica (SiO2)

WPC12 using Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES)

Potable and Raw waters Metals (total):

Calcium Magnesium Hardness as CaCO3 Potassium Sodium

WPC12 using Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES)

Page 13: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 13 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable and Raw waters (cont’d)

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d)

Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable (cont’d)

Chemical Testing (cont’d) Potable and Raw waters Metals (total):

Boron WPC12 using Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES)

Potable and Raw waters Permanganante Index WPC47 using manual titration Potable and Raw waters Total & Dissolved Metals:

Lead Copper Zinc Nickel Cadmium Chromium Silver

WPC15 using Inductively Coupled Plasma Mass Spectrometry (ICP-MS) – Nexion & Agilent

Antimony Selenium Arsenic

Strontium Barium Cobalt Molybdenum Uranium Vanadium

Tin Titanium

Beryllium Lithium Thallium

Page 14: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 14 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable, Raw and Surface waters

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d)

Documented In-House Methods based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable (cont’d)

Chemical Testing (cont’d) Potable and Raw waters Mercury WPC21 using ICP-MS Potable and Raw (Surface & Ground) waters

TOC/DOC WPC67 using Shimadzu TOC-L CPH analyser

Potable, Bottled and Raw waters Bromate WPC54 using IC (Methrom) Potable, Raw, Surface and Groundwaters

Dissolved and total metals: Iron Manganese Aluminium Sodium Potassium Calcium Magnesium Sulphur (as sulphate) Silicon (as Silica) Phosphorus Boron

WPC 49 using Inductively Coupled Plasma optical emission spectrometry (ICP-OES)

Drinking water, Groundwater and Surface Water

Ammonium Total Oxidised Nitrogen Nitrite Nitrate (by calculation) Chloride Orthophosphate Silica Alkalinity

WPC64 by discrete analysis (Aquakem

Page 15: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 15 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable, Raw and Surface waters (cont’d)

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d)

Documented In-House Methods based on procedures in the Standing Committee of Analysts Publication “The Microbiology of Water 2002” unless stated otherwise

Microbiological Testing Isolation and enumeration of: Potable, Raw and Surface waters Total Aerobic Colony Count at 22C

and at 37C

WPM1 based on “The Microbiology of Drinking Water” Part 7 (2007) (by Pour Plate)

Potable, Raw and Surface waters Coliforms, presumptive and

confirmed WPM4 & W10 based on “The Microbiology of Drinking Water” Part 4 (2009) using membrane filtration using MLGA followed by traditional or protein profiling confirmation (Maldi-ToF)

Potable, Raw and Surface waters Escherichia coli, presumptive and

confirmed WPM4 & W10 based on “The Microbiology of Drinking Water” Part 4 (2009) using membrane filtration using MLGA followed by traditional or protein profiling confirmation (Maldi-ToF)

Potable, Raw and Surface waters Enterococci, presumptive and

confirmed WPM2 & W7 based on “The Microbiology of Drinking Water” Part 5 (2010) using membrane filtration followed by traditional or protein profiling confirmation (Maldi-ToF)

Potable, Raw and Surface waters Clostridium perfringens

presumptive and confirmed WPM3 & W8 based on “The Microbiology of Drinking Water” Part 6 (2010) using membrane filtration followed by traditional or protein profiling confirmation (Maldi-ToF)

Potable, Raw and Surface waters Cryptosporidium Oocysts WCRY1, WCRY2, & WCRY3 based

on “The Microbiology of Drinking Water” Part 14 (2009)

Page 16: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 16 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: Potable, Raw and Surface waters (cont’d)

Testing for the purpose of enforcement of the Water Supply (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) (cont’d)

Documented In-House Methods based on procedures in the Standing Committee of Analysts Publication “The Microbiology of Water 2002” unless stated otherwise

Microbiological Testing (cont’d) Potable waters only Quantitative Taste WPM 10 using assessed Panel Potable and Raw waters Quantitative Odour WPM 10 using assessed Panel Isolation and enumeration of: Potable, Groundwater, Surface, Process and Recreational waters (natural and man-made)

Pseudomonas aeruginosa WPM11 & W11 based on “The Microbiology of Drinking Water” Part 8 (2010) using membrane filtration followed by traditional or protein profiling confirmation (Maldi-ToF)

Potable, Groundwater, Surface, Process and Recreational waters (natural and man-made)

Pseudomonas spp WPM12 in house method based on “The Microbiology of Water”1994 Part 1 using membrane filtration

Radiochemisty Testing: Documented In-House Methods

based on Standing Committee of Analysts Methods for the Examination of Waters and Associated Materials, HMSO Publication, Year and ISBN No given where applicable

Potable, Raw and Surface waters Radioactivity -

Gross Alpha (relative to Am-241) Gross Beta (relative to K-40)

WPC23

Page 17: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 17 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS Microbiological Testing Documented In-House Methods Recreational & Process waters Total Aerobic Colony Count at 22C

and at 37C (37C for 48 4 hours,

22C for 72 4 hours)

WPM1 using Yeast Extract Agar based on “The Microbiology of Drinking Water” Part 7 (2007) (by Pour Plate)

Process waters Total Aerobic Colony Count at 30oC WPM1 based on “The Microbiology for 2 days Of Drinking Water” Part 7 (2012) (by Pour Plate) Recreational water Total Aerobic Colony Count at 37oC WPM1 based on “The Microbiology for 1 day Of Drinking Water” Part 7 (2012) (by Pour Plate) Recreational & Process waters Enterococci, presumptive and

confirmed WPM2 based on “The Microbiology of Drinking Water” Part 5 (2010) using membrane filtration

Clostridium perfringens,

presumptive and confirmed WPM3 based on “The Microbiology of Drinking Water” Part 6 (2010) using membrane filtration

Coliforms and Escherichia coli,

presumptive & confirmed WPM4 based on “The Microbiology of Drinking Water” (2016) Part 4

Pure waters Pseudomonas aeruginosa WPM11 based on “The

Microbiology of Drinking Water” (2015) Part 8 & HTM 04-01 (2013)

Waters for the preparation of Ultrapure Dialysis Fluid and Dialysis water

Total Aerobic Colony Count at 22oC for 7 days

WPM13 using a) Pour plate, or b) Membrane filtration

Using R2A based on BS EN ISO 11663:2015

Endoscope Washer Disinfector Rinse water

Total Aerobic Colony Count at 30oC for 5 days

WPM13 by membrane filtration using R2A based on HTM 01-06 Part E 2016

Potable, Raw & Surfacewater Legionella – Confirmation only

Legionella spp Legionella pneumophila

W5 – Confirmation by protein profiling (Maldi-ToF) ONLY

Page 18: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 18 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WASTE WATERS:

Chemical Testing Documented In-House Method to meet the requirements of the Environment Agency MCERTS Performance Standard - sampling and chemical testing of untreated sewage, sewage effluent and trade effluent

Untreated sewage, treated sewage effluent, trade effluent to sewer, trade effluent to controlled water

Alkalinity (to pH 4.5)

WWC9 using manual titration

Untreated sewage, treated sewage effluent, trade effluent to sewer, trade effluent to controlled water

pH WWC14 using manual probe system

Untreated sewage, treated sewage effluent, trade effluent to sewer, trade effluent to controlled water

Suspended Solids (105 °C) Ashed suspended solids (450 °C)

WWC21 by gravimetry

Untreated sewage, treated sewage effluent, trade effluent to sewer, trade effluent to controlled water

Aluminium, , Boron Cadmium, Calcium, Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Nickel, Phosphorus, Potassium, , Sodium, Thallium, Vanadium, Zinc and Sulphur (as SO4)

WWC8 by ICP-OES

Untreated sewage, treated sewage effluent, trade effluent to sewer, trade effluent to controlled water

Mercury WWC17 by ICP-MS

Untreated sewage, treated sewage effluent, trade effluent to sewer, trade effluent to controlled water

BOD WWC11 using dissolved oxygen meter

Untreated sewage, treated sewage effluent, trade effluent to sewer, trade effluent to controlled water

COD WWC13 using DR3800 Spectrophotometer

Page 19: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 19 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WASTE WATERS: (cont’d) Chemical Testing (cont’d) Documented In-House Method to

meet the requirements of the Environment Agency MCERTS Performance Standard - sampling and chemical testing of untreated sewage, sewage effluent and trade effluent

Untreated sewage, treated sewage effluent, trade effluent to sewer, trade effluent to controlled water

Total Organic Carbon WWC24 using GE Analytical Instruments Sievers InnovOx TOC analyser

Untreated sewage, treated sewage effluent, trade effluent to sewer, trade effluent to controlled water

Ammonia Nitrite Total Oxidised Nitrogen Nitrate (by calculation) Chloride Soluble reactive phosphorus

WWC47 by discrete analysis (Aquakem)

Untreated sewage, treated sewage effluent, trade effluent to sewer, trade effluent to controlled water

Metals (total and dissolved) Aluminium Vanadium Chromium Iron Manganese Cobalt Nickel Copper Zinc Arsenic Molybdenum Cadmium Thallium Lead

WWC46 using ICP-MS

Treated sewage effluent and trade effluent to sewer, trade effluent controlled waters

Elements (total and dissolved) Selenium Phosphorus

WWC46 using ICP-MS

Untreated sewage, treated sewage effluent, trade effluent to sewer, trade effluent to controlled water

Petroleum ether extractable matter WWC48

Untreated sewage, treated sewage effluent, trade effluent to sewer, trade effluent to controlled water

pH and Conductivity (20 C) WWC14 using manual probe system

Page 20: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 20 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WASTE WATERS: (cont’d) Chemical Testing (cont’d) Documented In-House Method to

meet the requirements of the Environment Agency MCERTS Performance Standard - sampling and chemical testing of untreated sewage, sewage effluent and trade effluent (cont’d)

Untreated sewage, treated sewage effluent, trade effluent to sewer, trade effluent to controlled water

Ammonia Nitrite Total Oxidised Nitrogen Nitrate (by calculation) Chloride Soluble reactive phosphorus

WWC50 by Gallery Plus Discrete Analyser

Page 21: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 21 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS Chemical Testing (cont’d) Documented In-House Methods Process (High Purity & DI Waters) Turbidity WPC 6 using manual meter & Bottled waters Conductivity WPC 7 using manual meter Colour WPC13 using UV-Vis spectrometer Fluoride WPC20 using Ion Selective Electrode Total Dissolved Solids (180 C) WPC25 by gravimetry

Conductivity, Turbidity and Colour WPC 40 using the Peerless Automated Robotic System Process (High Purity & DI Waters) Total & Free Cyanide WPC65 using continuous flow waters autoanalyser Process (High Purity & DI Waters) & Bottled waters

Metals (total and dissolved): Iron Aluminium Manganese Phosphorus Sulphur as Sulphate (SO4) Silicon as Silica (SiO2)

WPC12 using Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES)

Metals (total):

Calcium Magnesium Hardness as CaCO3 Potassium Sodium Boron

WPC12 using Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES)

Process (High Purity & DI Waters) Bromate WPC54 using IC (Methrom) waters Process (High Purity & DI Waters) & Bottled waters

Ammonium Total Oxidised Nitrogen Nitrite Nitrate (by calculation) Chloride Orthophosphate Silica Alkalinity

WPC64 by discrete analysis (Aquakem)

Page 22: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 22 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS (cont’d) Chemical Testing (cont’d) Documented In-House Methods Process (High Purity & DI Waters) & Bottled waters

Metals: Lead Copper Zinc Nickel Cadmium Chromium Silver Antimony Selenium Arsenic Strontium Barium Cobalt Molybdenum Uranium Vanadium

WPC15 using Inductively Coupled Plasma Mass Spectrometry (ICP-MS) – Nexion & Agilent instruments

Tin Titanium Beryllium Lithium Thallium

Mercury WPC21 using ICP-MS Dissolved and total metals:

Iron Manganese Aluminium Sodium Potassium Calcium Magnesium Sulphur (as sulphate) Silicon (as Silica) Phosphorus Boron

WPC 49 using Inductively Coupled Plasma optical emission spectrometry (ICP-OES)

Untreated sewage, treated sewage effluent, trade effluent to sewer, trade effluent to controlled water

Sulphides WWC20 using spectrophotometer

Page 23: issued by United Kingdom Accreditation Service · (Water Quality) Regulations 2016 (SI 614). The testing is in accordance with the Drinking Water Testing Specification (DWTS) Documented

4409

Accredited to ISO/IEC 17025:2005

Schedule of Accreditation issued by

United Kingdom Accreditation Service 2 P ine Trees , Cher t sey Lane, S ta i nes -upon-Thames , TW 18 3HR, UK

ALS Environmental Ltd Wakefield

Issue No: 090 Issue date: 11 December 2019

Testing performed at main address only

Assessment Manager: KW Page 23 of 23

Materials/Products tested

Type of test/Properties

measured/Range of measurement

Standard specifications/

Equipment/Techniques used

WATERS: (cont’d) Chemical Testing (cont’d) Documented In-House Methods Raw water (surace & groundwater) BOD WWC11 using dissolved oxygen

meter Raw water (surface & grounwater) COD WWC13

using DR3800 Spectrophotometer Potable and Raw waters Vinyl Chloride WPC63 using Headspace GC-MS

QQQ SOILS: Chemical Tests Sludge only Alkalinity WSC1 by titration Soil and sludge Kjeldahl Nitrogen WSC8 determined spectrometrically Soil and sludge pH WSC11 Ion Selective Electrode Soil and sludge Total Solids (105 °C)

Total Ash Solids (550 °C) WSC12 by gravimetry

Soil and sludge Vanadium, Cadmium, Chromium,

Cobalt, Nickel, Copper, Arsenic, Selenium, Molybdenum, Thallium, Lead, Zinc

WSC 16 by Boiling Acid Digestion Followed by ICP-MS

Soil and sludge Mercury WSC5 using ICP-MS Soil and sludge Antimony WSC7 using ICP-MS Soil and sludge Fluoride WSC18 using ion selective

electrode Soil Extractable potassium WSC13 using ICP-AES Extractable magnesium Soil Extractable phosphorus WSC14 using UV 1800

Spectrophotometer Soil and sludge Aluminium, Calcium, Chromium,

Copper, Iron, Lead, Nickel, Phosphorus, Sulphur, Tin, Zinc, Potassium, Magnesium, Manganese, Sodium, Lithium, Cadmium

WSC6 using ICPAES

END


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