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Feed Stream Component Flow rate kg /hr Temperature
1 2000 kg/hr 70
2 5000 L/hr 70
3 22000 L/hr 70
??? acetylal!cyl!c ac!d ????
" #ater 22000 25
5 $utlet tream %rom the reactor ??? 25
??? &!'er outlet Stream
Crytall!ne al!cyl!c ac!d
L!(u!d acet!c anhydr!de )pure*
L!(u!d concentrated )+5,*phophor!c ac!d
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&olar &a )&-#* &elt!ng .o!nt o!l!ng .o!nt en!ty
13-10 15+ 211 1-""
102-10 73 13+ 1-0
+-00 21 15 1-
10-20 135 1"0 1-35
1-00 0 100 1-00
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Stream!ng heat Capac!ty
"-1" 4/g C
1-7 4/g C
3-"1 4/g C
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eat alace
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Flows: (kg/hr) Processor Feed
2000
5000
phophor!c ac!d 2100
acetylal!cyl!c ac!d 0
6cet!c 6c!d 0#ater
Total
Temp 70
.reure )k.a*
Crytall!ne al!cyl!c ac!d
acet!c anhydr!de )pure*
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Reactor Outlet Mixer Outlet Pump Outlet Cooler Outlet Seperator
70
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1251
5000
2705
+5
For hot fuid
side o a heat
exchanger let,
mH : mass
fow rate o
the hot fuid
in kg/hrCpH : mass
heat capacity
o the hot
fuid in Joules/kgC!iH and !oH :
"especti#ely
inlet and
outlet
temperatures
on exchangerhot side in C
mC : mass
fow rate o
the cold fuid
in kg/hr
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m 8 Cp 8 )T! To* 9 mC 8 CpC 8 )ToC T!C* : )3*
CpC : mass
heat capacity
o the cold
fuid in
Joules/kgC!iC and !oC :
"especti#ely
inlet and
outlet
temperatures
on exchanger
cold side
in C
Heat lost $y
the hot fuid %
&' % mH (
CpH ( )!oH &
!iH* + )*
Heat gained
$y the cold
side % ' %
mC ( CpC (
)!oC & !iC* +
)-*
Comparinge.uations )*
and )-*,
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Gas Codesate P!" #al$sis %ork&ook%ritte &$ Ro&ert Mott' #ugust *
Th! workheet analye reult %rom C; and CC< tet on a ga condenate %lu!d
ata hould only =e entered on yellow cell
F!rt enter C; data )=elow the dew po!nt* on the heet >C; ata>
Then enter CC< relat!e olume )a=oe the dew po!nt* on the heet >CC< ata>
@ecoery %actor %or !nd!!dual component and %or tock tank o!l and ga are hown on the heet >@ecoery %actor>
The heet >C; analy!> conta!n mater!al =alance calculat!on wh!ch can =e ued a a con!tency check o% C; data
Thee check are decr!=ed !n >.hae eha!or>A S.< &onograph 20A =y #h!ton and rule
The mater!al =alance check calculate l!(u!d phae den!t!e and compo!t!on-
en!t!e and Balue %rom the mater!al =alance calculat!on are d!played a chart-
onmonoton!c =eha!our %or the Balue or l!(u!d den!ty cure w!ll cat ome dou=t on the al!d!ty o% the C; meauremen
D% the l!(u!d compo!t!on ! meaured at the end o% the C;A two other mater!al =alance check can =e ued-
The &ater!al alance check are hown on the heet >&ater!al alance>-
6 >Forward &ater!al alance> calculate the %!nal l!(u!d compo!t!on %rom the or!g!nal compo!t!onA l!(u!d aturat!onA E%actorAamount o% ga remoedA and the ga compo!t!on at each tep-
6 >ackward &ater!al alance> calculate the or!g!nal compo!t!on %rom the %!nal l!(u!d compo!t!onA %!nal l!(u!d aturat!onA %!nalE%actorA the amount o% ga remoedA and the ga compo!t!on at each tep- Th! ! a =etter check %or lean condenate-
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46CB BDF< 1
!trogen 0 2
Car=on !o'!de 0 C$2
ðane 0-002 2S
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0-000
0-000
0-000
0-002
0-000-15"
0-1
0-0
0-3+
1-0++
3-23"
+3-7
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C!+ +ataThe %!rt preure mut =e the dew po!nt preure
The num=er o% preure entr!e mut =e et to d!play the chart correctly
um=er o% preure entr!e
.lu %ract!on
.reure )p!g* 5535 "500 3500
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o o% preure !n C; .lu %ract!o
Gpre 3 Gplu
.luFrac
1
2
3
"
5
en!ty 7
&wre% )l=/%t3*
2-013 +
""-01 103"-07
1-0"
30-07
""-0+
5-12 35-01
5-12 3-"5
72-15 3+-13
72-15 3+-3
-17 "1-1+
ular we!ght !c gra!ty
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n
2
7
C7
C
C7
C
C+
C10
C11
C12
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Geeral ,-ormatio
S1 %lu!d
@eero!r temperature )deg F* 23
Dn!t!al preure )p!g* 10""0
C5
CC. +ataonly enter data at or a=oe dew po!nt preure
enter preure !n decend!ng order
.reure @elat!e
p!g olume10""0 0-3715
5535 1
C"
C5
C
C7
$!l %rac 5
Calculated o!l ga rat!o aume ur%ace o!l 9 C5
Ttd 520 deg @
.td 1"-7 p!a
e%!n!t!on o% o!l %or ur%ace o!l andga recoer!e
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Forward material &alace ackward material &alace
Calculate re!dual l!(u!d compo!t!on Calculate !n!t!al ga compo!t!on
Calculated den!ty o% re!dual l!(u!d "1-3
en!ty to ue !n calculat!on 51-2
Measured Calculated Measured Calculate
2 0-00 0-20 2 0-3+ 0-
C$2 0-00 1-33 C$2 1-7 2-++
2S 0-00 0-00 2S 0-00 0-00
C1 0-00 37-2 C1 -25 117-"
C2 0-01 5-+ C2 7-02 11-5
C3 0-15 7-2 C3 -3 10-+3
!C" 0-1+ 1-+ !C" 1-"2 2-30
nC" 0-1 3-37 nC" 2-32 3-75
!C5 0-" 1-32 !C5 0- 1-"0
nC5 1-10 1-2 nC5 0-" 1-"0C 3-23 1-+7 C 0-+7 1-5
C7 +3-7 3-12 C7 +-53 17-"7
100-00 100-00 100-00 171-
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02000"0000000001000012000
0-0,
10-0,
20-0,
30-0,
"0-0,
50-0,
0-0,
70-0,
0-0,
+0-0,
100-0,
Reco0er$ -actors -rom depletio' o water i-lux
C1 C2
C3 C">
C5> C
C7F Ha
$!l
a&adomet pressure (psig)
R e c o
0 e r $ - a c t o r s
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3000 3500 "000 "500 5000 5500 000
0-00
50-00
100-00
150-00
200-00
250-00
Calculated oil gas ratio 1 assumes sur-ace oil 2 C34
pressure (psia)
O G R
( & & l /
M M s c - )
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3000 3500 "000 "500 5000 5500 000
0-0100
0-1000
1-0000
10-0000
510alues calculated -rom material &alace aal$sis o- C!+ data
C$2
C1C2
C3
!C"
nC"
!C5
nC5
C
@ow
12
@ow
127
@ow
12@ow
12+
pressure (psia)
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3000 3500 "000 "500 5000 5500 000
0-00
100-00
200-00
300-00
"00-00
500-00
00-00
700-00
Oil ad Gas +esities calculated -rom material &alace aal$sis o- C!+ data
l!(u!d den!ty)kg/m3*
ga den!ty )kg/m3*
pressure (psia)
d e s i t $ ( 5 g
/ m * )
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Calculated modi-ied &lack oil properties
.reure )p!a* 5535 "500 3500
.reure )p!a* . 55"+-7 "51"-7 351"-7
Moles o- Gas Car=onGno
up to C3 "-0 7-2 +0-3
C" 3-737 3-53 3-"25 "
C5 0 0 0 5
C 0 0 0
***6**7 *896 *396;;<
Moles o- oil
!C" 0 0 0 "
nC" 0 0 0 "
!C5 0-57 0- 0-7 5
nC5 0-"2 0-77 0-757 5
C 0-+ 0-57 0-771
C7 0 0 0 7
C 0 0 0
C+ 0 0 0 +
C10 0 0 0 10
C11 0 0 0 11
C7 +-52+ -2 3-+ 7
!olume o- Oil
!C" 0-0000 0-0000 0-0000 5-12
nC" 0-0000 0-0000 0-0000 5-12
!C5 0-015 0-01" 0-01"1 72-15
nC5 0-0155 0-01"" 0-013+ 72-15
C 0-0203 0-017+ 0-011 -17
C7 0-0000 0-0000 0-0000 100-2
C 0-0000 0-0000 0-0000 11"-2
C+ 0-0000 0-0000 0-0000 12-3
C10 0-0000 0-0000 0-0000 1"2-3
C11 0-0000 0-0000 0-0000 15-3
C7 0-3171 0-15 0-100
6*9< 6* 6;3
Oil1gas ratio (&&l/MMsc-) ;7967 ;;763*
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en!ty )l=/%t3*
35-01
3-"5
3+-13
3+-30
"1-1+
"2-5
""-1+
"5-35
"5-
"-00
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Calculated reco0er$ -actors
Calculated reco0er$ -actors -or each compoet
6=andonment preure )p!a* 10""0 5535 "500 3500 2500 1700
Component
C1 0-0, I;6LJ
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C 0-000 0-0 0-10 0-12 0-105
C7 0-000 0-"+5 0-5" 0-" 0-32
!olume o- oil produced (-t*/mol o- e=uil gas)
!C" 0-000 0-000 0-000 0-000 0-000
nC" 0-000 0-000 0-000 0-000 0-000
!C5 0-000 0-001 0-002 0-002 0-002nC5 0-000 0-001 0-002 0-002 0-002
C 0-000 0-001 0-002 0-003 0-002
C7 0-000 0-015 0-015 0-012 0-00
"otal 6 6;7 6; 6 6;8
Cumulati0e total 6 6;7 68 637 6
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+00 2 2 2 2
I;6LJ
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0-12" 0-252 0-000 0-000 0-000 0-+
0-35" 2-7"5 0-000 0-000 0-000 7 +-52+
0-000 0-000 0-000 0-000 0-000 0-000
0-000 0-000 0-000 0-000 0-000 0-000
0-003 0-00" 0-000 0-000 0-000 0-010-002 0-00" 0-000 0-000 0-000 0-015
0-003 0-005 0-000 0-000 0-000 0-020
0-00+ 0-07" 0-000 0-000 0-000 0-317
6;9 6 6 6 6 6*97
67 6;
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I;6LJ
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en!ty )l=/%t3*
5-12 35-01
5-12 3-"5
72-15 3+-1372-15 3+-3
-17 "1-1+
Dn!t!al o!l
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temperature )deg @* Tre 722-7 deg @
preure )p!a* . 55"+-7 "51"-7 351"-7
welltream produced )cum %ract!on* p 0 0-07+7 0-21+
l!(u!d olume )%ract!on* SL 0 0-17 0-22"2
e( ga E%actor E 1-023 0-+202 0-515
Produced gas phase compositio
ga phae compo!t!on 2 0-3+3 0-"05 0-"33
C$2 1-77 1-2+ 1-3
2S 0 0 0
C1 -25 71-+13 7"-33+
C2 7-02" 7-17 7-2""
C3 -25 -501 -501
!C" 1-"1 1-352 1-312nC" 2-31+ 2-17 2-113
!C5 0-57 0- 0-7
nC5 0-"2 0-77 0-757
C 0-+ 0-57 0-771
C7 0 0 0
C 0 0 0
C+ 0 0 0
C10 0 0 0
C11 0 0 0
C7 +-52+ -2 3-+
Gplu 1+-53 1"+-703 13-501
Gga 37-25+ 30-+5 2-+7
ol o% 1 l= mole )%t3* ; 1-5125 1-50 1-7+0
Ha den!ty )l=/%t3* ga den!ty )l=/%t3* 2"-3" 1+-"17 1"-33
Ha den!ty )Bg/m3* ga den!ty )kg/m3* 3+"-5 311-03 230-0
L= &ole ga produced gaGp 0 0-07+7 0-1"00"
;ol o% ga !n cell ;ga 1-5125 1-255" 1-170
L= mole o% ga !n cell ga 1-0000 0-7+"2 0-211L= mole o% l!(u!d l!( 0-0000 0-121 0-15+1
&a remoed &gaGp 0-000 2-"" 3-77+
&a o% ga !n cell &ga 37-2 2"-3 1-7
&a o% l!(u!d &l!( 0-00 10-"3 1"-27
o% l!(u!d 2-75 +-+
L!(u!d den!ty )l=/%t3* l!(u!d den!ty )l=/%t3* "0-5 "1-30
L!(u!d den!ty )Bg/m3* l!(u!d den!ty )kg/m3* 50-00 1-57
moles o- each compoet 2 0-3+3 0-31 0-300remaiig i cell C$2 1-77 1-30 1-3+
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(a-ter extra gas has &ee remo0ed) 2S 0 0-000 0-000
C1 -25 2-51" 52-10"
C2 7-02" -"51 5-"37
C3 -25 -10 5-1+
!C" 1-"1 1-310 1-12
nC" 2-31+ 2-1"5 1-"+
!C5 0-57 0-7+3 0-
nC5 0-"2 0-77+ 0-73
C 0-+ 0-+00 0-7+2
C7 0 0-000 0-000
C 0 0-000 0-000
C+ 0 0-000 0-000
C10 0 0-000 0-000
C11 0 0-000 0-000
C7 +-52+ +-03" -"
Total 100-001 +2-025 7-021
moles o- li=uid i cell 2 0-000 0-03+ 0-031
C$2 0-000 0-17 0-212
2S 0-000 0-000 0-000
C1 0-000 5-"0" 5-+32
C2 0-000 0-751 0-+3
C3 0-000 0-+"" 1-15
!C" 0-000 0-23 0-312
nC" 0-000 0-"1 0-537
!C5 0-000 0-15 0-210
nC5 0-000 0-15" 0-203
C 0-000 0-21+ 0-313
C7 0-000 0-000 0-000C 0-000 0-000 0-000
C+ 0-000 0-000 0-000
C10 0-000 0-000 0-000
C11 0-000 0-000 0-000
C7 0-000 "-111 -0
Total 0-000 12-10 15-+12
o% C7 %ract!on !n l!(u!d I;6LJ
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C+ 0-00 0-00
C10 0-00 0-00
C11 0-00 0-00
C7 32-0 3-12
510alues
2 1-3073 2-2137
C$2 1-2+5 1-3+75
2S ID;/0K ID;/0K
C1 1-77+ 1-++"1
C2 1-2051 1-22+1
C3 0-7 0-+30
!C" 0-7210 0-701
nC" 0-0 0-21
!C5 0-3+0 0-500
nC5 0-"3" 0-5+32
C 0-"+33 0-3+22
C7 0-1+02 0-1023
ackward material &alace calculatio
Calculate or!g!nal ga compo!t!on %rom re!dual l!(u!d and produced ga compo!t!on
"51"-7 351"-7
2 69
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JHC 10-732
;cell 1-513
Dn!t ma 37-2
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&eaured
l!(u!d
compo!t!on
1+-3
0-00
0-00
0-00
0-00
0-01
0-15
0-1+
0-1
0-"
1-10
3-23
0-000-00
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0-00
0-00
0-00
+3-7
@e!dual ga @e!dual l!(u!d &ole o% re!dual l!(u!d
0-2+21 0-0000 Ha molar ol 1-7+0
1-2570 0-0000 L!( molar ol 3-5571
0-0000 0-0000 Total mole 0-702
50-150 0-0002 L!( at 0-22"
"-75 0-000 L!( mole %rac 0-1352
"-32 0-012
0-52 0-01+ &ole re!d l!( 0-1055
1-"25 0-0"1 &oleGre!dGga 0-7"7
0-51 0-05
0-5107 0-110
0-5202 0-3"12
0-0000 0-0000
0-0000 0-0000
0-0000 0-0000
0-0000 0-0000
0-0000 0-0000
2-313 +-+03
7-"7 10-550