semspub.epa.gov · NEL LABORATORIES Corporate Headquarters Las Vegas Laboratory 6490 S McCarran...

SDMSDocID 2027893

NEL LABORATORIESCorporate Headquarters Las Vegas Laboratory6490 S McCarran Blvd. # 0-30 4208 Arcata Way, Suite AReno, NV 89509Phone- 775.348.2522Fax 775 348 2546

Las Vegas, NV 89030Phone 702657.1010Fax: 702.657 1577

RSSN

RSSN7900 Vegas Valley DriveLas Vegas, NV 89142

TEL: 702-431-3020

2027893

REProject:DPW-9B

Dear RSSN:

Order No.: L0212203

NEL Laboratories, Las Vegas received 8 samples on 12/12/02 for the analyses presented in thefollowing report.

There were no problems with the analyses and all data for associated QC met EPA or laboratoryspecifications unless noted in the Case Narrative

If you have any questions regarding these tests results, please feel free to call.

Rod T. MillerLaboratory Director

Date

Certifications:ArizonaCaliforniaIdahoMontanaNevadaNew Mexico

AZ05182002Certified

CertifiedNV052Certified

Albuquerque866.360.5726

Boise800.200.2952

Las Vegas888.368.3282

Phoenix888.238.2514

Reno800 368.5221

Sacramento800.368.5221

NEL LABORATORIES

NEL Laboratories, Las Vegas Date: ll-Feb-03

CLIENT: RSSN

Project: DPW-9B CASE NARRATIVELab Order: L0212203

Attached are the analytical results for samples in support of the above referenced project.

The samples submitted for this project were not sampled by NEL. Should you have any questions orcomments, please feel free to contact our Client Services Department.

Analytical Comments:

EPA 8260: Samples were evaluated for the presence of Acrylonitrile and trans-l,4-Dichloro-2-butene.Neither of these two compounds were present in the samples submitted in this work-order at or above5ppb.

L2 The associated blank spike recovery was below laboratory acceptance limits. Results may be biasedlow.

Page 1 of 1

NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: DPW-9B

PROJECT #: DPW-9B

MATRIX: AQUEOUS

Parameter 3Acetone

Benzene

Bromobenzene

Bromochloromethane

Bromodichl oromethan e

Bromoform

Bromomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide

Carbon tetrachlonde

CWorobenzene

Chloroethane

2-CWoroethyl Vinyl ether

Chloroform

Chloromethane

2-Chlorotoluene

4-Chlorotoluene

Dibromochloromethane

1 ,2-Dibromo-3-cbloropropane

1 ,2-Dibromoethane

Dibromomethane

1 ,2-Dichlorobenzene



Dichlorodifluoromethane

1 , 1 -Dichloroethane

1 ,2-Dichloroethane

1 , 1 -Dichloroethene

cis-1 ,2-Dichloroethene

trans- 1 ,2-Dichloroethene

1 ,2-Dichloropropane


2,2-Dichloropropane

1 , 1 -Dichloropropene

cis-l,3-Dichloropropene

trans-1 ,3 -DicWSropropene

Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

Isopropylbenzene

ND - Not Detected at the Reporting Limit

DF - Dilution Factor

Date: 10-Feb-03

CLIENT ED: DPW-9B

DATE SAMPLED: 12/12/02

NEL SAMPLE ID: L0212203-001A

Result Units

ND ng/L

ND ng/L

ND ng/L

ND ng/L

ND ng/L

ND ug/L

ND ng/L

ND ng/L

ND ng/L

ND ng/L

ND ng/L

ND ng/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND (ig/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ng/L

ND ng/L

ReportingLimit

25

5.0

5.05.05.0 '

5.05.0255.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.0 " '

5.05.0255.05.0

B - Analyte detected

DF Method Prep Date

1 SW8260B

J SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B ' • - - - - - ~

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

in the associated Method Blank,

Analyzed

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

. DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

S - Spike Recovery outside accepted recovery limits

B - Value above quantitation range Pagel of 9

NEL LABORATORIES

CLDZNT: RSSN

PROJECT ID: DPW-9B

PROJECT #: DPW-9B

MATRIX: AQUEOUS

CLIENT ID: DPW-9B



ReportingParameterp-Isopropyltoluene

Methylene chloride

4-Methyl-2-pentanone

Methyl t-butyl ether (MTBE)

Naphthalene

n-Propylbenzene

Styiene

1,1,1 ,2-Tetrachloroethane

1 , 1 ,2,2-Tetrachloroethane

Tetrachloroethene

Toluene

1 ,2,3-Tnchlorobenzene


1,1,1-Trichloroethane

1,1,2-TnchIoroethane

Tnchloroethene

Tnchlorofluoromethane

1 ,2,3-Tnchloropropane

1 ,2,4-Tnmethylbenzene


Vinyl acetate

Vinyl chloride

o-Xylene

m,p-Xylene

Surr: Dibromofluoromethane

Sun-: Toluene-d8

Surr: 4-BromofIuorobenzene

Result

NDNDNDNDNDNDNDNDND11

NDNDNDNDNDNDNDNDNDNDNDNDNDND90.4

98.0

95.7

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Ug/L

ug/L

ug/L

Hg/L

ug/L

ug/L

ug/L L2

ug/L-

ug/L

Ug/L

ug/L

ug/L

Hg/L

ug/L

ug/L

Ug/L

ug/L

ug/L

%REC

%REC

%REC

Limit

5.0

50255.010505.05.05.05.05.05.0505.05.05.05.05.05.0505.05.05.010

80.2-106

75.5-105

71 7-120

DF

ll1ll1lllllllllllllll1ll1ll

Method

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

Prep Date Analyzed

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03 '

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV



Date: 10-Feb-03

B - Analyte detected in the associated Method Blank


E - Value above quantitation range Page 2 of 9

NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: DPW-9B

PROJECT #: DPW-9B

MATRIX: AQUEOUS

ParameterAluminumBarium

.Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

AntimonyArsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc

Mercury

Result

0.380.044

5808.7200

22

240

ND

NDNDNDND

0.059

0.013

0.099

0.00911.1

0.14

NDNDND0.20

ND

Units

mg/L B

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L B

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.050

0.0050

0.20

0.10

0.20

2.00.50

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.00500.0050

0.0050

0.0050

0.0050

0.0020

0.0050

0.00020

CLIENT ID:

DATE SAMPLED:

NEL SAMPLE ID:

Mlllll1ll55555555555

5551

Method

SW6010B-TOSW6010B-To

SW6010B-TO

SW6010B-To

SW6010B-TO

SW6010B-To

SW 6010B-TO

SW6010B-To

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-TotaSW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 7470-Tota

DPW-9B-M

12/12/02

L0212203-002A

Prep Date

12/13/02

12/13/02

12/13/02

12/13/02

12/13/02

12/13/02

12/13/02

12/13/02

12/12/02

12/12/02

12/12/02

12/12/02

12/12/02

12/12/02

12/12/02

12/12/02

12/12/02

12/12/02

12/12/02

12/12/02

12/12/02

12/12/02

12/16/02

Analyzed

12/16/02

12/16/02

12/16/02

12/16/02

12/16/02

12/16/02

12/16/02

12/16/02

12/17/02

12/17/02

12/17/02

12/17/02

12/17/02

12/17/02

12/17/02

12/17/02

12/17/02

12/17/02

12/17/02

12/17/02

12/17/02

12/17/02

12/16/02

Analyst

WG-LV

WG-LV

WG-LV

WG-LV

WG-LV

WG-LV

WG-LV

WG-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LVRMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

FAS-LV



Date: 10-Feb-03



E - Value above quantitation range Page 3 of9

NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: DPW-9B

PROJECT #: DPW-9B

MATRIX: AQUEOUS0

ParameterAluminum

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc

Mercury

Result

0.610.043

4700.20

16028190

0.026

ND0.0060

NDNDND

0.0058

0.0094

ND0.46

0.091

0.0058

NDND0.50

ND

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L B

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.050

00050

0.20

0100.20

2.00.50

00050

00050

00050

0.0050

0.0050

0.0050

0.0050

0.0050

00050

0.0050

00050

0.0050

0.0050

00020

0.0050

0.00020

CLIENT ID: DPW-9B-FFM



DF

lllllll15

5

5

55

55

55

555551

Method Prep Date

SW6010B-DJ

SW 6010B-DJ

SW6010B-D1

SW 6010B-Di

SW6010B-Di

SW 6010B-DJ

SW 6010B-DJ

SW 6010B-Di

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW7470-Diss 12/16/02

Analyzed

12/20/02

12/20/02

12/20/02

12/20/02

12/20/02

12/20/02

12/20/02

12/20/02

12/18/02

12/18/02

12/18/02

12/18/02

12/18/02

12/18/02

12/18/02

12/18/02

12/18/02

12/18/02

12/18/02

12/18/02

12/18/02

12/18/02

12/16/02

WG-LV

WG-LV

WG-LV

WG-LV

WG-LV

WG-LV

WG-LV

WG-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

RMD-LV

FAS-LV

ND - Not Detected at the Reporting Lirmr


Date: 10-Feb-03




NEL LABORATORIES

CLIENT:

PROJECT ID:PROJECT #:

MATRIX:

Parameter

Chemical Oxygen

Ammonia, as N

RSSN

DPW-9BDPW-9B

AQUEOUS

Result UnitsDemand 34 mg/L

ND mg/L

CLIENT ID:

DATE SAMPLED:

NEL SAMPLE ID:

ReportingLimit DF Method

10 1 SM5520 D0 30 1 SM4500-NH3

DPW-9B12/12/02

L0212203-004A

Prep Date Analyzed12/18/02

12/17/02

RDA-LV

BTM-LV



Date: 10-Feb-03

-B - Analyte detected in the associated Method Blank


E - Value above quantitahon range Page 5 of 9

NEL LABORATORIES

CLIENT:

PROJECT ID:

PROJECT #:

MATRLX:

RSSN

DPW-9B

DPW-9B

AQUEOUS

CLIENT ID: DPW-9B



ParameterSulfide

Result Units

ND mg/L

ReportingLimit

0030

DF Method

1 SM4500-S D

Prep Date Analyzed

12/13/02

ND - Not Detected at the Reporting-Limit


Date: 10-Feb-03




NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: DPW-9B

PROJECT #: DPW-9B

MATRIX: AQUEOUS

ParameterChloride

Nitrate, as N

Nitrite, as N

Sulfate

Alkalinity, Bicarbonate (As CaCO3)

Alkalinity, Carbonate (As CaC03)

Hydroxide (As CaCO3)

Alkalinity, Total (As CaCOS)

pHTotal Dissolved Solids

CLIENT ID: DPW-9B



Result

320

NDND1900

240NDND2407.11

3690

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

pH unitsmg/L

ReportingLimit

10001001010050505025

100600

DF

100011

1000111114

Method

EPA 300 0

EPA 300 0

EPA 300 0

EPA 300 0

SM2320 B

SM2320 B

SM2320 B

SM2320 BEPA 150 1

SM2540 C

Prep Date Analyzed

12/19/02

12/13/02

12/13/02

12/19/02

12/13/02

12/13/02

12/13/02

12/13/02

12/12/02

12/13/02

AnalystRDA-LV

PJJ-LV

PJJ-LV

RDA-LV

CRA-LV

CRA-LV

CRA-LV

CRA-LV

CRA-LV

CRA-LV



Date: 10-Feb-03




NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: DPW-9B

PROJECT #: DPW-9B

MATRIX: AQUEOUS

Parameter

Acetone

Benzene

Bromobenzene

Bromochloromethane

Bromodichloromethane

Bromoform

Bromomethane

2-Butanone

n-Butylbenzene

' sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide

Carbon tetrachloride

Chlorobenzene

Chloroethane

2-Chloroethyl vinyl ether

Chloroform

Chloromethane

2-Chlorotoluene

4-Chlorotoluene

Dibromochlorornethane

1 ,2-Dibromo-3-chloropropane

1 ,2-Dibromoethane

Dibromomethane





1,1-Dichloroethane

1 ,2-Dichloroethane


cis-l,2-Dichloroethene

trans-1 ,2-Dichloroethene



2,2-Dichloropropane


cis-1 ,3-DicWoropropene

trans- 1 ,3-Dichloropropene

Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

Isopropylbenzene

Result Units

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

. ND - Not Detected at the Reporting Limit -•- —


Date: 10-Feb-03

ReportingLimit

255.05.05.05.05.05.0255.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05-05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.0255.05.0

CLIENT ID: RPW-9B (Rinseate)

DATE SAMPLED : 12/12/02


DF Method Prep Date

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

Analyzed

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

B -Analyte detected in the associated Method Blank


E - Value above quantftation range Page 8 of 9

NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: DPW-9B

PROJECT #: DPW-9B

MATRIX: AQUEOUS

Parameterp-Isopropyltoluene

Methylene chloride

4-Methy]-2-pentanone


Naphthalene

n-PropylbenzeneStyrene


1,1 ,2,2-Tetrachloroe thane

Tetrachloroethene

Toluene

1 ,2,3-Trichlorobenzene


1,1,1 -Tnchloroethane

1 , 1 ,2-Trichloroethane

Trichloroethene

Trichlorofluoromethane

1 ,2,3 -Trichloropropane

1 ,2,4-Trimethylbenzene


Vinyl acetate

Vinyl chloride

o-Xylene

m,p-Xylene


Surr: Toluene-d8Surr: 4-Bromofluorobenzene

Result

ND

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND"NDNDNDNDND93.7

96.095.0

Units

ug/Lug/L

ug/L

ug/L

ug/Lug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/Lug/LUg/L

ug/L

ug^L

ug/L

ug/L

ug/L

"g/L%REC

%REC%REC

ReportingLimit

5.05.0255.0105.05.05.05.05.05.05.0

L2 5.0

5.05.05.05.05.05.05.05.05.05.010

80.2-10675.5-10571.7-120

CLIENT ID: RPW-9B (Rinseate)


NEL SAMPLE DD: L0212203-008A

D_F Method

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260'B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 ' SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B1 SW8260B

Prep Date Analyzed

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/0312/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/03

12/25/0312/25/03

DRM-LV

DRM-LV

DRM-LV

DRM-LVDRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV 'DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LVDRM-LV



Date: 10-Feb-03

B - Analyte detected in the associated Method Blank.

S - Spike .Recovery outside accepted recovery limits

E - Value above quantitation range Page 9 of9

A N A L Y T I C A LLABORATORIES

Vanessa Padilla-NEL Laboratories Las Vegas4208 Arcata Way, Ste A .Las Vegas, NV 89030 ^

BSK Submission #: 2002121067BSK Sample ID #: 276198Project ID:

Submission Comments:

ProjectDesc:

Certificate of AnalysisELAP Certificate #1180

• Report Issue Date: 12/24/2002

Sample Type:Sample Description:Sample Conrrnents:

InorganicsAnalyte

LiquidDPW-9B .

"

-W&S . Date Sampled: 12/12/2002: • • - ' ' - •' '_ ' ' "• - . . ' Time Sampled: 0919

- . - Date Received: 12/17/2002

• ' • • . . . Prep Analysis^Method Result. Units PQL Dilution BLR Date Date

Total Organic Carbon (TOC) SM.5310-C 1.1 mg/L 0.2 0.2 12/18/200212/18/2002

' ' "•••^^•^••-v'"^^ s^ 'iiV-' jvto^srîî^t^viiiS'isSijj;

mg/L: Milligrams/Liter (ppm) PQL: Practical Quantitation Limit ' H: Analyzed outside of hold time • . .1'%ig/Kgr'Milli ains l0§^ P: Preliminary result

ug/L: Miciograms/Liter (ppb) " * : f tjL'xTJirurSiB*""'' *-^-^'-w«v M*^ gtispect jesdfeft'S^^yei'I.^^^.CGgjfnerite; .. M

ug/Kg: Micrograms/Kilogram (ppb) ND: None Detected at DLR E: Analysis performed by External laboratory. -%Rec: Percent Recovered (surrogates) ' See External Laboratory Report attachments.

Report Authentication Code: llilll[iil!IIUlIll!lilllllIilll!llliIilllllilllllllIlill_ . . - • . Page 1 of 1 -

—^ T?«cr,n rA 93706-1623 ; Phone 559-497-2888, In CA 800-877-8310 - Fax 559-485-6935

CHAIN OF CUSTODY NEL Work OrderNEL LABORATORIES

Public Water System (PWS)800-368-5221888 368 3282888 238 2514800 200-2952800-368 5221866 360 5726888-900-7477

Las/Vegas Laboratory ,4208 Arcata Way, Ste AN Us Vegas, NV 89030

RenoLas VegasPhoenixBoiseSacramentoAlbuquerqueDenver

Project Number

urchase Order NumberPhono 702-657-1010F

Fax- 702-657-1577

Crty,StaHz,pCoUe

l\lote#1.Enter the number ofcontainers submitted for theindicated Analysis followedby the preservation (see Box#2 below)Eg LlA)= 3 containers with

HCI preservation

Expected Due Date

Requested Turnaround v 5-day? 2-day 1 - d a y O t h e r

Customer Sample IdentificationSampled J

Time Date

Custody Seal intact? Y A HCIB HNO3C HSOD

Box#1 DW Drinking Water SD SolidWW Waste Water AQ AqueousOL Oil/Organic Liquid A AirCondil ion when received

Relinquished by (Print) Received by (Print)

ORIGINAL

NEL LABORATORIESjff1 i

"i ^ w illfplBr» $* j?"SP»f<!gg~m

TO ll^^Kiiltf lilisik, >~M ^

SrBnnBiMHDk! " " ' "

CLJfiENT: RSSN ;Work Order: L02 12203'Project: DPW-9B "

Sample ID; MB-R9366

Analyte

Chloride

Nitrate, as N

Nitrite, as N

Sulfate

Sample ID: MB-R949S

Analyte

Chloride

Nitrate, as N

Nitrite, as N

Sulfate

Sample ID: LCS-R9366

Analyte

Chloride

Nitrate, as N

Nitrite, as N

Sulfate

1 SampType: MBLK

Batch ID: R9366

; Result

ND"| ND

$ ND

ND

SampType: MBLK

ij Batch ID: R949S

I Result

]' ND;' ND

; ND; ND

SampType: LCS

Batch ID: R9366

4 Result

li 1.829

0.9480.957

2.373

TestCode: 300_W

TestNo: E300

PQL SPK value

0.10

0.10

0.10

0.10

TestCode: 300_W

TestNo: E300

PQL SPK value

0.10 0

0.10 0

0.10 0

0.10 0

TestCode: 300_W

TestNo: E300

PQL SPK value

0.10 2

0.10 1

0.10 1

0.10 2.5

300JW

Units: mg/L

SPKRefVal

Units: mg/L

SPKRefVal

00

0

0

Units: mg/L

SPKRefVal

0000

ANALYTICAL QC SUMMARY REPORT

Test Method:

Prep Date:

Analysis Date: 12/13/02

%REC LowLimit HighLimit RPDRefVal

Prep Date:



0 0 0 0

0 0 0 0

0 0 0 0

0 0 0 0

Prep Date:



91.4 80 120 0

94.8 80 120 0

95.7 80 120 0

94.9 80 120 0

EPA 300.0

Run ID: LJC-1_021213A

SeqNo: 83382

%RPD RPDLimit Qual

Run ID: L_IC-1_021219A

SeqNo: 84959

%RPD RPDLimit Qual

000

0

Run ID: LJC-1_021213A

SeqNo: 83381

%RPD RPDLimit Qual

0000

Qualifiers: ND - Not Delected at the Reporting Limit C - Unspiked sample >5 times the amount spiked

Jl - MS or MSD outside accepance limits. LCS acceptable. R - RPD outside accepted recovery limits

J - This concentration is considered an estimate due to LCS failure.


Page 1 of 31

Date: W-Feb-03

CLIENT: RSSN >Work Order: L0212203.-

Project: DPW-9B -.

Sample ID: LCS-R9495 ,,

1Analyte

Chloride ;

Nitrate, as N jNitrite, as N JSulfate i'

Sample ID: LCSD-R9366

Analyte ',

ChlorideNitrate, as N ;Nitrite, as N fSulfate *

r"

Sample ID; LCSD-R9495:

Analyte

ChlorideNitrate, as N 'Nitrite, as.NSulfate

Sample ID: L0212197-001DMSi

Analyte

ChlorideSulfate

SampType: LCS

Batch ID: R9495

Result

1.9640.9450.9132.561

SampType: LCSD

Batch ID: R9366

Result

1.8350.9370.9012.433

SampType: LCSD

Batch ID: R9495

Result

1.9940.9440.9272.579

SampType: MS

Batch ID: R9495

Result

174.565.67

TestCode:

TestNo:

PQL

0.100.10 _rf-0.10 '|j:

0.10 V

TestCode:

TestNo:

PQL

0.100.100.100.10

TestCode:

TestNo:

PQL

0.100.100.100.10

TestCode-

TestNo

PQL

5.05.0

300_W

E300

SPK value

211

2.5

300_W

E300

SPK value

211

2.5

300_W

E300

SPK value

211

2.5

300_W

E300

SPK value

5050

300_W

Units: mg/L

SPKRefVal

0000

Units: mg/L

SPKRefVal

0000

Units: mg/L

SPKRefVal

0000

Units; mg/L

SPKRefVal

120.522.78


Test Method: EPA 300.0

%REC

98.294.591.3102

%REC

91.893.790.197.3

%REC

99.794.492.7103

%REC

10885.8

Prep Date.


LowLimit HighLimit

80808080

Prep Date:

Analysis Date:

120120120120

12/13/02

LowLimit HighLimit

80808080

Prep Date:

Analysis Date:

120120120120

12/19/02

LowLimit HighLimit

80808080

Prep Date:

Analysis Date:

120120120120

12/19/02

LowLimit HighLimit

8080

120120

RPDRefVal

0000

RPDRefVal

0000

RPDRefVal

1.9640.9450.9132.561

RPD Ref Val

00


SeqNo: 84958

%RPD RPDLimit

0000


SeqNo: 83383

%RPD RPDLimit

0000


SeqNo: 84960

%RPD RPDLimit

1.52 250.106 25

1.52 ' 250.700 25

Run ID. L_IC-1_021219A

SeqNo: 84966

%RPD RPDLimit

00

Qual

Qual

Qual

Qual

Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked




Page 2 of 31

Date: 10-Feb-03

CLIENT: RSSN jWork Order: L0212203;Project: DPW-9B l 300 W


Test Method: EPA 300.0 *

Sample ID: L0212202-004CMS .

Analyte 1,

Chloride

Sulfate v

Sample ID: L0212259-001AMS

Analyte

Chloride

Sulfate

Sample ID: L0212221-007CMS

Analyte j|

SampType: MS

Batch ID: R9495

Result

1317

2880

SampType: MS

Batch ID: R9495

Result

56.565.4

SampType: MS

Batch ID: R9366

Result

TestCode:

TestNo:

PQL

100100

TestCode

TestNo

PQL

5.05.0

TestCode

TestNo

PQL'

300_W

E300

SPK value

1000

1000

300_W

E300

SPK value

5050

300JW

E300

SPK value

Units: mg/L

SPK Ref Val

317.2

2025

Units: mg/L

SPK Ref Val

9.035

20

Units: mg/L

SPKRefVal

%REC

10085.6

%REC

94.990.8

%REC

Prep Date:


LowLimit HighLimit RPD Ref Val

8080

Prep Date:

Analysis Date:

120 0120 0

12/19/02

LowLimit HighLimit RPDRefVal

8080

Prep Date:

Analysis Date:

120 0

120 0

12/13/02


Run ID:

SeqNo:

L_IC-1_021219A

85010

%RPD RPDLimit

Run ID:

SeqNo:

00

L_IC-1_021219A

85386

%RPD RPDLimit

Run ID:

SeqNo:

00

L_IC-1_021213A

86037

%RPD RPDLimit

Qual

Qual

Qual

Nitrate, as N 9710 1000 10000 97.1 80 120

Sample ID: L021 2202-004 CMSD SampType: MSD

Analyte

Chloride ;

Sulfate

Batch ID: R9495

Result

1252

: 2928

TestCode: 300_W Units: mg/L Prep Date:

TestNo: E300

PQL

100100

SPK value

1000

1000

SPKRefVal

317.2

2025

%REC

93.5

. 90.4


LowLimit

7070

HighLimit

130130

RPDRefVal

1317

2880


SeqNo: 85011

%RPD

5.08

1.66

RPDLimit

2525

Qual





Page 3 of 31

Date: 10-Feb-03

CLIENT: RSSNWork Order: L0212203

Project: DPW-9B

Sample ID: MB-R9503

Analyte

Aluminum

Barium (

Calcium

Iron

MagnesiumPotassium

SodiumVanadium

Sample ID: LCS-9503 -,

Analyte

Aluminum

Barium

Calcium

Iron

Magnesium '

Potassium

Sodium ;Vanadium

Sample ID. L021 2202-003 AMS

Analyte

Aluminum

Barium

Calcium

Iron


SampType: MBLK

Batch ID: R9503

Result

NDNDNDNDNDND

1.34

ND

SampType: LCS

Batch ID: R9503

Result

0.915

0.9072

17.70.8712

18.28

19.09

18.6

0.2142

SampType: MS

Batch ID: R9503

Result

1.08

0.8893

508.51.073

TestCode:

TestNo:

PQL

0:0500.0050

0.50

0.10

0.502.0

0.500.0050

TestCode:

TestNo

PQL

0.050

0.0050

0.50

0.100.502.0

0.50

0.0050

TestCode

TestNo

PQL

0.050

0.0050

0.50

0.10

6010W_D

SW6010B

SPK value

6010W_D

SW6010B

SPK value

11

201

202020

0.25

6010W_D

SW6010B

SPK value

11

201

6010W_D

Units. mg/L

SPKRefVal

Units: mg/L

SPKRefVal

000000

1.34

0

Units: mg/L

SPKRefVal

0.083

0.03213

522.30.2244

Test Method: SW 6010B-Diss

%REC

%REC

91.5

90.7

88.587.1

91.495.4

86.3

85.7

%REC

99.7

85.7

-6984.8

Prep Date:



Prep Date:



8585858585858585

Prep Date;

Analysis Date:

115 0115 0

115 0

115 0115 0115 0

115 0

115 0

12/20/02


75757575

125 0

125 0

125 0125 0

Run ID: R_ICP-1_021 220 A

SeqNo: 85119

%RPD RPDLimit Qual

Run ID: R_ICP-1_021220A

SeqNo: 85120

%RPD RPDLimit Qual

00000000


SeqNo: 85123

%RPD RPDLimit

0000

B

Qual

C





Page 4 of 31

Date: JO-Feb-03

CLIENT: RSSN SWork Order: L02 12203*Project: DPW-9B

Sample ID: L021 2202-003 AMS .

j

Analyte

Magnesium

Potassium

Sodium *Vanadium

Sample ID: L021 2202-003 AMSD

Analyte ',

Aluminum

Barium

Calcium

Iron :

Magnesium

Potassium,Sodium

Vanadium

Sample ID: L0212202-003ADUP

'"

Analyte

Aluminum

Barium

Calcium " "

Iron '•'

Magnesium

Potassium ,

SodiumVanadium


SampType: MS

Batch ID: R9503

Result

185.8

36.1

2240.1949

SampType: MSD

Batch ID: R9503

Result

1.15

0.9238

524.21.125

189.5

39.37222

0.2141

SampType: DUP

Batch ID: R9503

Result

RSD over 20%.

0.03482

524.5

0.2328180.4

24.23224ND

TestCode:

TestNo:

PQL

0.50

2.00.50

0.0050

TestCode:

TestNo:

PQL

0.050

0.0050

0.50

0.100.50

2.00.50

0.0050

TestCode

TestNo

PQL

0.050

0.0050

0.50

0.10

0.50

2.00.50

0.0050

6010W_D

SW6010B

SPK value

202020

0.25

6010W_D

SW6010B

SPK value

11

201

202020

0.25

6010W_D

SW6010B

SPK value

00000000

6010WJD

Units: mg/L

SPKRefVal

180.1

26225

0

Units: mg/L

SPKRefVal •

0.063

0.03213

522.30.2244

180.1

23.39225

0

Units: mg/L

SPKRefVal

00000000


%REC

28.5

50.5

-578

%REC

10989.2

9.59047

79.9-15

85.6

%REC

00000000

Prep Date:


LowLimit HighLimit

75757575

Prep Date:

Analysis Date:

125125125125

12/20/02

LowLimit HighLimit

Prep Date:


LowLimit HighLimit

00000000

00000000

Run ID: R_ICP-1_021220A '

SeqNo: 85123

RPD Ref Val

0000

%RPD

0000

Run ID. R_

RPDLimit Qual

CCC

ICP-1_021220A

SeqNo: 85124

RPDRefVal

0.973

0.8893

508.5

1.073185.8

36.1224

0.1949

%RPD

16.7

3.813.04

4.71

1.978.67

0.8979.40

Run ID: R_

RPDLimit Qual

20202020202020 B20

_ICP-1_021220A

SeqNo: 85122

RPDRefVal

0.063

0.03213

522.30.2244

180.123.39

2250

%RPD

1178.04

0.420

3.67

0.166

3.53

0.4450

RPDLimit Qual

20 R

202020202020 B20





Page 5 of 31

Date: 10-Feb-03

CLIENT: RSSN ,-Work Order: L0212203;,'Project: DPW-9B

Sample ID: MB-1897j

Analyte

Aluminum

BariumCalcium

IronMagnesium i

Potassium iSodium »;

Vanadium

Sample ID: LCS-1897

Analyte

Aluminum

Barium

CalciumIronMagnesiumPotassium

SodiumVanadium

Sample ID: L0212146-001AMs'

Analyte

Aluminum

BariumCalciumIron


SampType: MBLK

Batch ID: 1897

Result

0.086

NDNDNDNDND

2.15

ND

SampType: LCS

Batch ID: 1897

Result

10.9753

19.58

1.00720.6518.85

24.1

0.2443

SampType: MS

Batch ID: 1897

Result

1.26

1.26421.57

1.127

TestCode:

TestNo:

PQL

0.050

0.00500.50

0.10

0.50

2.00.50

0.0050

TestCode:

TestNo:

PQL

0.050

0.00500.50

0.10

0.50

2.00.50

0.0050

TestCode

TestNo

PQL

0.050

0.00500.50

0.10

6010WJT

SW6010B

SPK value

6010WJT

SW6010B

SPK value

1

1

201

20

2020

0.25

6010WJT

SW6010B

SPK value

11

201

6010WJT

Units: mg/L

SPKRefVal

Units: mg/L

SPKRefVal

0.08600000

2.15

0

Units: mg/L

SPKRefVal

0.154

0.28081.666

0.2564

Test Method : SW 601 OB-Total

%REC

%REC

91.4

97.5

97.9

101103

94.2

11097.7

%RBC

11198.399.5

87

Prep Date:

Analysis Date:

12/13/02

12/16/02


Piep Date:

Analysis Date:

12/13/02

12/16/02


8585858585858585

Prep Date:

Analysis Date:

115 0

115 0

115 0115 0

115 0

115 0

115 0

115 0

12/13/02

12/16/02


75757575

125 0

125 0

125 0

125 0


SeqNo: 83816

%RPD RPDLimit Qual

Run ID. R_ICP-1_021216A

SeqNo: 83817

%RPD RPDLimit

00000000

Qual

B

B


SeqNo: 83825

%RPD RPDLimit

0000

Qual

B




B - Analyte detected'in the associated Method Blank

Page 6 of 31

Date: JO-Feb-03

CLIENT: RSSN ;.Work Order: L0212203§Project: DPW-9B ' 6010W T


Test Method: SW 6010B-Total


,

Analyte

Magnesium

Potassium

Sodium

Vanadium

Sample ID: L0212146-001AMSD

Analyte

Aluminum fj

Barium •

Calcium

Iron

Magnesium

Potassium •

SodiumVanadium

Sample ID: L0212146-001 ADUP

Analyte

Aluminum

Barium A

Calcium "

Iron

Magnesium

Potassium

SodiumVanadium

j-

SampType: MS

Batch ID: 1897

Result

20.54

21.61

1040

0.2528

SampType: MSD

Batch ID: 1897

Result

1.061.041

21.48

1.10820.94

21.27

10500.2562

SampType: DUP

Batch ID: 1897

Result

0.102

0.09708

1.285'

NDNDND

10800.01557

TestCode:

TestNo:

PQL

0.50

2.00.50

0.0050

TestCode:

TestNo:

PQL

0.050

0.0050

0.500.10

0.50

2.00.50

0.0050

TestCode:

TestNo

PQL

0.050

0.0050

0.50

0.100.50

2.00.50

0.0050

6010WJT

SW6010B

SPK value

202020

0.25

6010WJT

SW6010B

SPK value

11

201

202020

0.25

6010WJT

SW6010B

SPK value

00000000

Units: mg/L

SPKRefVal

00

1060

0

Units: mg/L

SPKRefVal

0.154

0.2808

1.6660.2564

00

1060

0

Units: mg/L

SPKRefVal

00000000

%REC

103108

-100

101

%REC

90.676

99.1

85.1105106-50102

%REC

00000000

Prep Date:

Analysis Date:

12/13/02

12/16/02

LowLimit HighLimit

75

75

75

75

Prep Date:

Analysis Date:

125

125125

125

12/13/02

12/16/02

LowLimit HighLimit

Prep Date:

Analysis Date:

12/13/02

12/16/02

LowLimit HighLimit

00000000

00000000

RPD Ref Val

0000

RPDRefVal

1.261.264

21.57

1.12720.54

21.61

10400.2528

RPDRefVal

0.154

0.2808

1.666

0.2564

00

1060

0

Run ID: RJCP-1

SeqNo: 83825

J21216A

%RPD RPDLimit Qual

0000

Run ID: RJCP-1

SeqNo: 83826

JL

JJ21216A

%RPD RPDLimit Qual

17.219.4

0.4181.72

1.93

1.590.957

1.34

Run ID: RJCP-1

SeqNo: 83820

20 B20

20

2020

2020 JL

20

JJ21216A

%RPD RPDLimit Qual

40.6

97.2

25.8

000

1.87200

0 B

000000 B

0

Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked1 Jl - MS or MSD outside accepance limits. LCS acceptable. R - RPD outside accepted recovery limits



Page 7 of 31

Date: 10-Feb-03

CLIENT: RSSN 'Work Order: L0212203 ,Project: DPW-9B ..

Sample ID:' MB-R9433

Analyte

Antimony

Arsenic

Beryllium

Cadmium -

Chromium '

CobaltCopper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc


Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

LeadManganese

Nickel

Selenium


SampType: MBLK •

Batch ID: R9433

Result

NDNDNDNDNDNDNDNDNDNDND .

NDNDND

SampType: LCS

Batch ID: R9433

Result

0.04015

0.0948

0.0678

0.0503

0.03105

0.0376

0.04140.0434

0.03755

0.039450.1104

TestCode: 6020WJ)

TestNo: SW6020

PQL SPK value

0.0050

0.0050

0.0050

0.0050

0.00500.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0020

0.0050

TestCode: 6020WJ)

TestNo: SW6020

PQL SPK value

0.0050 0.05

0.0050 0.1

0.0050 0.1

0.0050 0.05

0.0050 0.050.0050 0.05

0.0050 0.05

0.0050 , 0.05

0.0050 0.05

0.0050 0.05

0.0050 0.1

6020W_D

Units: mg/L

SPKRefVal

Units: mg/L

SPKRefVal

00000000000

Test Method: SW 6020-Diss

Prep Date:

Analysis Date:

Run ID: RJCP-2MSJ121218B

12/18/02

%REC LowLimit Htghliimit

Prep Date

Analysis Date

SeqNo: 84644

RPD Ref Val %RPD RPDLimit Qual


12/18/02

%REC LowLimit HighLimit

80.3 8594.8 85

67.8 85

101 85

62.1 85

75.2 8582.8 85

86.8 85

75.1 85

78.9 85

110 85

115115115115115115115115115115115

SeqNo: 84645

RPD Ref Val %RPD RPDLimit

0 . 0

0 0

0 0

0 0

0 00 00 ' 0

0 0

0 0

0 00 - 0

Qual

S

S

SSS

SS





Page 8 of 31

Date: JO-Feb-03

CLIENT: RSSNWork Order: L0212203''Project: DPW-9B ' 6020W D




«.

Analyte

Silver

Thallium

Zinc

Sample ID: L021 2202-003 AMS

•3

Analyte

Antimony

Arsenic

BerylliumCadmium -

ChromiumCobalt

Copper '

Lead

ManganeseNickel '

SeleniumSilver

Thallium

Zinc


Analyte

Antimony

Arsenic

Beryllium

SampType: LCS

Batch ID: R9433

Result

0.1007

0.0487

0.01335

SampType: MS

Batch ID: R9433

Result

0.0557

0.12880.09445

0.0619

0.0475

0.0555^

0.05665

0.050750.4716

0.1350.1534

0.1086

0.05685

0.5018

SampType: MSD

Batch ID: R9433

Result

0.06115 •

0.1314

0.0943

TestCode:

TestNo:

PQL

0.0050

0.00200.0050

TestCode:

TestNo:

PQL

0.0050

0.0050

0.00500.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.00200.0050

TestCode

TestNo

PQL

0.0050

0.00500.0050

6020WJ)

SW6020

SPK value

0.1

0.05

0.05

6020WJ)

SW6020

SPK value

0.05

0.1

0.10.05

0.05

0.05

0.050.05

0.05

0.05

0.1

0.1

0.05

0.05

6020WJ)

SW6020

SPK value

0.05

0.10.1

Units: mg/L

SPKRefVal

0

0

0

Units: mg/L

SPKRefVal

0

0.00595

0

0

00

0.00915

0.00505

0.4106

0.079850.00585

0

0.00205

0.4136

Units: mg/L

SPKRefVal

0

0.00595

0

%REC

101

97.4

26.7

%REC

111

12394.4124

95

11195

91.4

122

110

148

109

110

176

%REC

122

125

94.3

Prep Date:


LowLimit HighLimit

85

85

85

Prep Date:

Analysis Date:

115

115

115

12/18/02

LowLimit HighLimit

7575

7575

75

75

7575

7575

75

75

75

75

Prep Date:

Analysis Date:

125

125

125125

125125

125

125125

125

125125

125

125

12/18/02

LowLimit HighLimit

RPDRefVal

0

0

0

RPDRefVal

00

00

0

0

00

0

0

00

0

0

RPDRefVal

0.0557

s 0.12880.09445

Run ID: RJCP-2MSJ)21218B

SeqNo: 84645

%RPD RPDLimit Qual

0

0

0 S

Run ID: RJCP-2MS_021218B

SeqNo: 84648

%RPD RPDLimit Qual

0

000

0 •

0

00

00

0 Jl

00

0 C

Run ID: RJCP-2MSJI21218B

SeqNo: 84649

%RPD RPDLimit Qual

9.33 20

1.92 200.159 20





Page 9 of '31

Date: 10-Feb-03

CLIENT: RSSNWork Order: L0212203Project: DPW-9B "


Analyte

Cadmium

Chromium

Cobalt

Copper

LeadManganese

Nickel

Selenium

Silver

ThalliumZinc

Sample ID' L0212202-003ADUP

Analyte

AntimonyArsenic

BerylliumCadmium

Chromium

Cobalt

Copper

Lead

Manganese -

NickelSelenium

SilverThallium

Zinc f

SampType: MSD

Batch ID: R9433

Result

0.0625 "

0.0483

0.0564

0.0577

0.05295

0.4760.1375

0.1576

0.1097

0.05810.5082

SampType: DUP

Batch ID: R9433

Result

ND0.0055

NDNDND

0.00510.0095

0.0051

0.4174

0.08165

0.00505

ND0.00205

0.4234

TestCode:

TestNo:

PQL

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.00500.0050

0.0050

0.0020

0.0050

TestCode

TestNo

PQL

0.00500.00500.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0020

0.0050

6020WJD

SW6020

SPK value

0.05

0.05

0.05

0.05

0.05

0.050.050.10.1

0.05

0.05

6020WJ)

SW6020

SPK value

00000000000000

6020W_D

Units: mg/L



Prep Date:


SPKRefVal

000

0.009150.00505

0.41060.07985

0.00585

00.00205

0.4136

Units: mg/L

%REC

12596.6

11397.1

95.8

131115152110112189

LowLimit

•

HighLimit RPD Ref Val

0.0619

0.0475

0.0555

0.05665

0.05075

0.47160.135

0.1534

0.1086

0.05685

0.5018

Prep Date:


SPKRefVal

00000000000000

%REC

00000000000000

LowLimit

00000000000000

HighLimit

00000000000000

RPD Ref Val

00.00595

0000

0.009150.00505

0.4106

0.079850.00585

00.00205

0.4136

Run ID: R_ICP-2MSJ)21218B

SeqNo: 84649

%RPD

0.965

1.67

1.611.84

4.24

0.9391.87

2.731.05

2.17

1.26

Run ID: R_

RPDLimit

2020202020202020202020

Qual

Jl

C

ICP-2MSJ)21218B

SeqNo: 84647

%RPD

07.86

000

2003.75

• 0.985

1.64

2.23

14.7

00

2.34

RPDLimit

2020202020202020202020202020

Qual

R





Page 10 of 31

Date: 10-Feb-03

CLIENT: RSSN i|Work Order: L0212203iProject: DPW-9B J

Sample ID: MB-1893

Analyte

Antimony

Arsenic

Beryllium

Cadmium

ChromiumCobalt

CopperLead

ManganeseNickel

Selenium

Silver

Thallium

Zinc

Sample ID: LCS-1893

Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt •

Copper

Lead

ManganeseNickel

Selenium

SampType: MBLK

Batch ID: 1893

Resulti

NDNDND

f, ND

NDNDNDNDNDNDNDNDNDND

SampType: LCS

Batch ID; 1893

Result

0.0575

0.1017

0.0963

0.0497

0.0512

0.0509

0.05065

0.0483

0.05205

0.05045

0.0995

6020WJT

TestCode. 6020WJT Units: mg/L

TestNo: SW6020

PQL SPK value SPKRefVal

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.00500.0050

0.0050

0.00500.0050

0.0050

0.0020

0.0050

TestCode: 6020WJT Units: mg/L

TestNo: SW6020


0.0050 0.05 0

0.0050 0.1 0

0.0050 0.1 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 • 0.05 0

0.0050 0.05 0

0.0050 0.1 0


Test Method: SW 6020-TotaI

Prep Date:

Analysis Date:

12/12/02

12/17/02


Prep Date:

Analysis Date:

12/12/02

12/17/02


115 85

102 85

96.3 85

99.4 85

102 85

102 85

101 85

96.6 851 104 85

101 8599.5 85

115 0

115 0115 0

115 0

115 0

115 0

115 0

115 0

115 0

115 0115 0

Run ID: RJCP-2MSJJ21217D

SeqNo: 84628

%RPD RPDLimit Qual

Run ID: RJCP-2MSJJ21217D

SeqNo: 84629

%RPD RPDLimit

000000-00000

Qual


Jl - MS or M$D outside accepance limits. LCS acceptable. R - RPD outside accepted recovery limits



Page 11 of 31

Date: 10-Feb-03

CLIENT: RSSN *>Work Order: L02 12203;Project: DPW-9B

Sample ID: LCS-1893

Analyte

Silver

Thallium

Zinc


Analyte

AntimonyArsenic

Beryllium

Cadmium

ChromiumCobalt

Copper

Lead

ManganeseNickel

SeleniumSilver i.

Thallium ;;Zinc


-

Analyte

AntimonyArsenic

Beryllium


SampType: LCS

Batch ID: 1893

Result

0.1093

0.0508

0.03705

SampType: MS

Batch ID: 1893

Result

0.0571

0.10280.09465

0.049850.05225

0.05145

0.05220.04845

0.05315

0.05130.09965

0.1113

0.05065

0.0395

SampType: MSD

Batch ID: 1893

Result

0.057050.104

0.0966

'

TestCode:

TestNo:

PQL

0,0050

0.0020

0.0050

TestCode

TestNo

PQL

0.0050

0.00500.0050

0.0050

0.0050

0.00500.0050

0.0050

0.00500.0050

0.0050

0.0050

0.0020

0.0050

TestCode

TestNo

PQL

0.0050

0.0050

0.0050

6020WJ?

SW6020

SPK value

0.10.05

0.05

6020WJT

SW6020

SPK value

0.05

0.10.1

0.05

0.05

0.050.05

0.05

0.050.05

0.10.1

0.05

0.05

6020\VJT

: SW6020

SPK value

0.05

0.10.1

6020WJT

Units: mg/L

SPKRefVal

000

Units: mg/L

SPKRefVal

00000000000000

Units: mg/L

SPKRefVal

000

Test Method: SW 6020-Total

%REC

109102

74.1

%REC

114103

94.7

99.7104103104

96.9106103

99.7

11110179

%REC

114104

96.6

Prep Date:

Analysis Date:

12/12/02

12/17/02

LowLimit HighLimit

858585

Prep Date:

Analysis Date:

115115

115

12/12/02

12/17/02

LowLimit HighLimit

75

75

7575

75

7575

75

757575

75

75

75

Prep Date:

Analysis Date:

125125

125

125

125

125125

125

125125

125

125

125

125

12/12/02

12/17/02

LowLimit HighLimit

Run ID- RJCP-2MS_021217D

RPD Ref Val

000

SeqNo: 84629

%RPD RPDLimit

000

Qual

S

Run ID. RJCP-2MSJI21217D

RPDRefVal

00000000000000

SeqNo: 84632

%RPD RPDLimit

00000000000000

Qual

Run ID: RJCP-2MS_021217D

RPDRefVal

0.0571

0.1028

0.09465

SeqNo: 84633

%RPD RPDLimit

0.0876 201.16 20

2.04 20

Qual





Page 12 of 31

Date: 10-Feb-03

CLIENT: RSSNWork Order: L0212203''Project: DPW-9B •


Analyte

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver (]

Thallium

Zinc :


Analyte

Antimony

Arsenic

Beryllium

Cadmium '<

Chromium

Cobalt

Copper

Lead

Manganese -

Nickel

Selenium

Silver

Thallium

Zinc '


SampType: MSD

Batch ID: 1893

Result

0.0511

0.05255

0.05245

0.075

0.05205

0.05385

0.0523

0.101

0.1131

0.0524

0.03845

SampType: DUP

Batch ID: 1893

Result

NDNDNDNDNDNDNDNDNDNDNDNDNDND

TestCode:

TestNo:

PQL

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0020

0.0050

TestCode:

TestNo:

PQL

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0020

0.0050

6020WJT

SW6020

SPK value

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.10.1

0.05

0.05

6020WJT

SW6020

SPK value

00000000000000

6020WJT

Units- mg/L

SPK Ref Va!

00000000000

Units: mg/L

SPKRefVal

00000000000000


%REC

102105105150104108105101113105

76.9

%REC

00000000000000

Prep Date:

Analysis Date:

12/12/02

12/17/02

LowLimit HighLimit

Prep Date:

Analysis Date:

12/12/02

12/17/02

LowLimit HighLimit

00000000000000

00000000000000

RPDRefVal

0.04985

0.05225

0.05145

0.0522

0.04845

0.05315

0.0513

0.09965

0.1113

0.05065

0.0395

RPD Ref Val

00000000000000

Run ID: RJCP-2MS.

SeqNo: 84633

.021217D

%RPD RPDLimit

2.48

0.573

1.92

35.87.16

1.311.93

1.40

1.60

3.40

2.69

Run ID: RJCP-2MS

SeqNo: 84631

2020202020202020202020

Qual

R

_021217D

%RPD RPDLimit

00000000000000

2020202020202020202020202020

Qual





Page 13 of 31

Date: 10-Feb-03

CLIENT: RSSNWork Order: L0212203'Project: DPW-9B 8260 W


Test Method: SW8260B

Sample ID: BLANK 021221 A

Analyte

SampType: MBLK

Batch ID: R9734

Result

TestCode: 8260_W Units: ug/L

TestNo: SW8260B


Prep Date:



Run ID: L_VOAMS-2J)21224A

SeqNo: 87511

%RPD RPDLimit Qual

Acetone

Benzene

BromobenzeneBromochloromethane


Bromoform

Bromomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide


Chlorobenzene

Chloroethane


Chloroform

Chloromethane

2-Ch!oro toluene

4-Chlorotoluene

Dibi omochloromethane


1 ,2-Dibromoethane

Dibromomethane


1 ,3-DichloTobenzene' i f .1 ,4-Dichlorobenzene


1,1-Dichloroethane

1,2-Dichloroethane ';

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

25

5.05.05.05.05.05.0255.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.0



J - This concentration is considered an estimate due to LCS failure,


Page 14 of 31

, Date: 10-Feb-03

CLIENT: RSSNWork Order: L0212203 ''Project: DPW-9B

Sample ID: BLANK 021221A

Analyte






2,2-Dichloropropane


cis-1, 3-Dichloropropene

trans-1 ,3-Dichloropropene

Elhylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

Isopropylbenzene '>

p-Isopropyltoluene

Methylene chloride



Naphthalene

n-Propylbenzene

Styrene

1 ,1 ,1 ,2-Tetrachloroethane

1,1 ,2,2-Tetrachloroethane

Tetrachloroethene'

Toluene



1,1,1 -Trichloroethane

1 ,1,2-Trichloroethane

Trichloroethene

-

SampType: MBLK

Batch ID: R9734

Result

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND.


8260_W Test Method: SW8260B

TestCode: 8260_W Units: ug/L Prep Date: Run ID: L_VOAMS-2_021224A

TestNo: SW8260B Analysis Date: 12/24/03 SeqNo: 87511

PQL SPK value SPKRefVal %REC LowLimit HighLimit RPDRefVal %RPD RPDLimit Qual

5.05.05.05.05.05.05.05.05.05.05.0255.05.05.05.0255.010

5.05.05.05.05.05.05.05.05.05.05.0

Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times' the amount spiked




Page 15 of 31

Date: 10-Feb-03

CLDSNT: RSSNWork Order: L02 12203 'Project: DPW-9B

Sample ID: BLANK 021 221 A

Analyte


1 ,2,3-Trichloropropane


1 ,3,5-TrimethylbenzeneVinyl acetate

Vinyl chlorideo-Xylene

m,p-Xylene

SUIT: Dibromofluoromethane

Surr: Tohiene-d8

Surr: 4-Bromofluorobenzene

Sample ID: VstdOSO 021223A

Analyte

Acetone

BenzeneBromobenzene

Bromochioromethane


Bromoform

Bromomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide


Chlorobenzene

SampType; MBLK

Batch ID: R9734

Result

ND

': ND

ND

ND

ND

ND

NDND

46.22

48.5849.43

SampType: LCS

Batch ID: R9734

Result

42.44

64.57

67.76

62.36

57.04

47.88

65.8346.04

: 65.62

68.44

67.1959.18

63.51

63.91

— 1 '.

TestCode:

TestNo:

PQL

5.05.0

5.0

5.0

5.0

5.0

5.010

0.50

0.50

0.50

TestCode

TestNo

PQL

25

5.05.0

5.0

5.0

5.0

5.025

5.0

5.0

5.0

5.05.0

5.0

8260_W

SW8260B

SPK value

50

50

50

8260JW

SW8260B

SPK value

50

50

50

50

50

50

50

50

50

50

50

5050

50

8260_W

Units: ug/L

SPKRefVal

00

0

Units: ug/L

SPKRefVal

00

0

0

0

0

0

0

0

0

0

0

0

0



%REC

, 92.4

97.2

98.9

%REC

84.9129

136

125

114

95.8

132

92.1

. 131

137134

118

127

128

Prep Date:

Analysis Date:


12/24/03

LowLimit HighLimit

80.2

75.5

71.7

Prep Date:

Analysis Date:

106

105

120

RPDRefVal

0

0

0

SeqNo: 87511

%RPD RPDLimit

0

0

0

Qua]


12/24/03

LowLimit HighLimit

7070

70

70

70

70

70

70

70 '

70

7070

7080

130

130

130

130

130

130

130

130

130

130

130

130

130

120

RPD Ref Val

00

0

0

0

0

0

0

0

0

0

0

0

0

SeqNo: 87514

%RPD RPDLimit

0

0

0

0

0

0

0

0

00

0

0

0

0

Qual

LI

LI

LI

LI

LI

LI





Page 16 of 31

Date: 10-Feb-03

CLIENT: RSSN !(

Work Order: L0212203,!Project: DPW-9B

Sample ID: VstdOSO 021 223 A

;Analyte •

Chloroethane


Chloroform

Chloromethane

2-Chlorotoluene

4-Chlorotoluene



1 ,2-Dibromoethane

Dibromorriethane





1,1-Dichloroethane

1 ,2-Dichloroethane




1,2-Dichloropropane '


2,2-Dichloropropane

1,1-Dichloropropene

cis-1 ,3-Dichloropropene

trans-1, 3-Dichloropropene -

Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

Isopropylbenzene -


SampType: LCS

Batch ID: R9734

Result

63.28

98.16

60.97

52,43

63.71

64.2

55.53

35.11

52.15

52.69

52.61

59.97

58.62

54.78

58.72

4967.26

67.07

67.98

59.1

• 49.47

63.53

64.3

57.9

51.3

60.19

35.43

41.93

72.93

67.7

TestCode:

TestNo:

PQL

^ 5.0

5.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.0255.05.0

8260_W

SW8260B

SPK value

505050505050505050505050505050505050505050505050505050505050

8260_W

Units: ug/L

SPKRefVal

000000000000000000000000000000


%REC

127196122105127128111

70.2

10410510512011711011798

135134136118

98.9

127129116103120

70.9

83.9

146135

Prep Date.

Analysis Date:

Run ID: L_VOAMS-2_021224A

12/24/03

LowLimit HighLimit

707080707070707070707070707070707070707070707070707070707070

130130120130130130130130130130130130130130130130130130

' 130

130130130130130130130130130130130

RPD Ref Val

000000000000000000000000000000

SeqNo: 87514

%RPD RPDLimit

0000000000000000 ,

00000000000000

Qual

LILI

LILILI

LILI





Page 17 of 31

Date: 10-Feb-03

CLIENT: RSSNWork Order: L0212203,Project: DPW-9B 8260_W

Sample ID: VstdOSO 021 223 A SampType: LCS

Batch ID: R9734

Analyte

p-Isopropyltoluene

Methylene chloride

4-Methy1-2-pentanone


Naphthalene

n-Propylbenzene

Styrene't

1 , 1 , 1 ,2-Tetrachloroethane

1 , 1 ,2 ,2-Tetrachloroethane

Tetrachloroethene

Toluene


1,2,4-Tricnlorobenzene *

1,1,1 -Trich'loroethane

1 ,1 ,2-Tricnloroethane

Trichloroethene




1 ,3 ,5-Trimethylbenzene

Vinyl acetate

Vinyl chloride

o-Xy!ene

m,p-Xylene

Surr: Dibromofluoromethane ;

Surr: Toluene-d8


Result

66.71

" 62.04

36.06

44.48

43.64

64.52

59.53

61.35

47.32 "

64.5

65.76

47.9

22.37

62.22

52,14

66.76

62.02

48.45

62.02

64.34

80.59

55.64

59.22

122.4

45.86

48.55

47.77

TestCode: 8260_W Units: (ig/L

TestNo: SW8260B


5.05.0255.010

5.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05,05.05.010

0.50

0.50

0.50

50505050'50505050505050505050505050505050505050

100505050

000000000000000000000000000



Prep Date:


Run ID: L_VOAMS-2J>21224A

SeqNo: 87514


133124

72.1

8987.3

129119123

94.6

129132

95.8

44.7

124104134124

96.9

124129161111118

. 122

91.7

97.1

95.5

70707070 ,

7070707070707070707070707070707070707070

80.2

75.5

71.7

130130130130130130130130130130130130130130130130130130130130130130130130106105120

0

00000000000000000000000000

%RPD RPDLimit Qual

000000000000000000000000000

LI

LI

L2

LI

LI





Page 18 of 31

< Date: 10-Feb-03

CLIENT: RSSNWork Order: L0212203;Project: DPW-9B

Sample ID: L021 2348-001 A M

Analyte

Acetone ,

BenzeneBromobenzene

Bromochloromethane


BromoformBromomethane

2-Butanone

n-Butylbenzenesec-Butylbenzene

tert-Bu tylbenzen eCarbon disulfide


ChlorobenzeneChloroethane


Chloroform

Chloromethane

2-ChIorotoluene

4-Chloro toluene

Dibromochloromethane1 ,2-Dibrorho-3-chloropropane

1,2-Dibrornoethane

Dibromomethane

1 ,2-Dichlorobenzene *

1,3-Dichlorobenzene



1,1-Dichloroethane

1 ,2-Dichloroethane


SampType: MS

Batch ID: R9734

Result

ND62.06

53.94

51.68

50.65

29.9363.21

ND

36.0355.17

58.3358.64 -

64.06

54.67

60.54

62.11

57.6853.68

58.6854.74

41.59

ND

37.92

41.7

19.834.24

31.02

57.91

56.81

41.01

TestCode

TestNo

PQL

25

5.0

5.0

5.05.0

5.05.0

25

5.05.0

5.0

5.05.0

5.0

5.0

5.0

5.0

5.0

5.05.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.05.0

8260_W

SW8260B

SPK value

5050

50

5050

5050

50

5050

5050

50

50

5050

50

5050

50

50

50

50

50

50

50

50

50

5050

8260_W

Units: ug/L

SPKRefVal

0

0

0

0

0

00

0

00

00

0

00

0

00

0

0

0

0

0

0

0

0

0

0

00


%REC

0124

108

103

101

59.9126

0

72.1

110117

117128

109

121124

115107

117

109

83.2

0

75.883.4

39.6

68.5

62

116114

82

Prep Date:


LowLimit HighLimit

70

70

70

70

7070

7070

70

7070

70'70

70

70

70

70

7070

70

70

7070

70

70

70

7070

70

70

130130

130

130

130130

130130

130130

130130

130

130

130

130

130

130130

130

130

130

130

' 130

130

130

130130

130

130

Run ID: L_VOAMS-2_021224A

SeqNo: 87512

RPDRefVal

00

0

00

0

00

00

00

0

0

0

0

00

0

0

0

0

0

00

0

0

0

00

%RPD

0

0

0

0

0

00

0

00

00

0

0

0

0

00

0

0

0

0

0

0

0

0

00

0

0

RPDLimit Qual

M2

M2

M2

M2

M2

M2

M2





Page 19 of 31

Date: 10-Feb-03

CLIENT: RSSN ';Work Order: L0212203 "Project: DPW-9B 8260 W



Sample ID: L0212348-001A M SampType: MS

Batch ID: R9734

Analyte Result






2,2-Dichloropropane

1,1-Dichloropropene

cis-1 , 3-Dichloropropene


Bthylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane '>

Isopropylbenzene

p-Isopropyltoluene

Methylene chloride



Naphthalene

n-Propylbenzene

Styrene



Tetrachloroethene

Toluene



1 , 1 ,1 -Trichloroethane


Trichloroethene

64.6

60.89

64.82

53.5

38.32

56.3

63.81

47.53

38.99

54.91

NDND

66.97

67.32

46,81

55.45

25.55

35.21

ND62.22

47.12

50.91

28.93

60.08

61.15

NDND

62.44

39.66

63.54

TestCode: 8260_W Units: (ig/L

TestNo: SW8260B


5.05.05.05.05.05.05.05.05.05.05.0255.05.05.05.0255.010

5.05.05.05.05.05.05.05.05.05.05.0

505050505050505050505050505050505050505050505050505050505050

000000000000000000000000000000

Prep Date: Run ID: L_VOAMS-2J»21224A

Analysis Date: 12/25/03 SeqNo: 87512

%REC LowLimit HighLimit RPDRefVal %RPD RPDLimit Qual

129

122130107

76.6

113128

95.1

78110

00

134135

* 93.6

11151.1

70.4

0124

• 94.2

10257.9

120122

00

12579.3

127

707070707070707070707070707070707070707070

707070707070707070

130130130130130130130130130130130130130130130130130130130130130130130130130130130130130130

000000000000000000000000000000

000000000000000000000000 *000000

M2

M2MlMl

M2

M2

M2

M2M2





Page 20 of 31

Date: 10-Feb-03

CLIENT:' RSSN ";Work Order: L02 12203 «•'Project: DPW-9B

Sample ID: L021 2348-001 AM

Analyte

TncWorofl uoromethane

1 ,2,3-Trichloropropane1 ,2,4-Trime'thylbenzene1 ,3,5-TrimethylbenzeneVinyl acetate


m,p-XyleneSUIT: Dibromofluoromethane

SUIT: Toluene-d8Surr: 4-Bromofluorobenzene

Sample ID: L0212348-001A M

Analyte

Acetone

BenzeneBromobenzeneBromochloromethane

BromodichloromethaneBromoformBromomethane

2-Butanonen-Butylbenzene

sec-Butylbenzenetert-Butylbenzene

Carbon disulfideCarbon tetrachlorideChlorobepzene *(

SampType: MS

Batch ID: R9734

Result

65.8

31.15

45.5753.53

52.4257.64

51.1

108.845.2748.73

47.27

SampType: MSD

Batch ID: R9734

Result

ND59.7863.8852.15

49.06

38.33

60.23

26.5452.54

68.48

67.3

56.4661.33

55.47

j

TestCode:

TestNo:

PQL

5.05.05.05.05.05.05.010

0.50

0.50

0.50

TestCode-

TestNo-

PQL

255.05.05.05.05.05.0255.05.05.05.05.05.0

8260_W

SW8260B

SPK value

50505050505050

100505050

8260_W

SW8260B

SPK value

5050505050505050505050505050

8260_W

Units: ug/L



Prep Date:


SPKRefVal

00000000000

Units: u,g/L

%REC

13262.3

91.1

107105115102109

90.5

97.594.5

LowLimit

7070707070707070

80.2

75.5

71.7

HighLimit

130130130130130130130130106105120

RPDRefVal

00000000000

Prep Date:


SPKRefVal

00000000000000

%REC

0120128104

98.1

76.7

12053.1

105137135113123111

LowLimit

7070707070707070707070707070

HighLimit

130130130130130130130130130130130130130130

RPD Ref Val

062.0653.94

51.68

50.65

29.93

63.21

036.0355.17

58.3358.64

64.0654.67

Run ID: L_VOAMS-2J121224A

SeqNo: 87512

%RPD

00000000000

Run ID: L_

RPDLimit Qual

MlM2

VOAMS-2J)21224A

SeqNo: 87513

%RPD

03.74

16.9

0.905

3.19

24.6

4.83

20037.3

21.5

14.3

3.79

4.35

1.45

RPDLimit

252525

2525252525252525252525

Qual

R2

R2

RlRl

Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times Jhe amount spiked




Page 21 of 31

Date: 10-Feb-03

CLIENT: RSSN rWork Order: L02 12203,Project: DPW-9B 8260_W

Sample ID: L0212348-001A M SampType: MSD

Batch ID: R9734

Analyte

Chloroethane


Chloroform

Chloromethane2-Chlorotoluene

4-ChlorotolueneDibromochloromethane

1 ,2-Dibromo-3-chloropropane1 ,2-Dibromoethane

Dibromomethan e



1 ,4-DichlorobenzeneDichlorodifluoromethane1 , 1 -Dichloroethane

1 ,2-Dichloroethane1 , 1 -Dichloroethene




1 ,3 -Dichloropropane

2,2-Dichloropropane

1 ,1 -Dichloropropene

cis-1 , 3-Dichloropropene


EthylbenzeneHexachlorobutadiene

2-Hexanone

lodomethane

Isopropylbenzene

Result

58.13

3154.3647.44

63.5960.85

44.1219.01

41.55

42.45

39.4649.15

48.2755.7754.74

40.04

62.51

59.6763.21

51.72

40.38

53.21

60.74

46.85

39.5

53.96

11.73

25.58

65.47

71.11

TestCode. 8260_W Units: ug/L

TestNo: SW8260B


5.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05:0255.05.0

505050505050505050505050505050505050505050505050505050505050

000000000000000000000000000000



Prep Date:



SeqNo: 87513


11662

10994.9

127" 122

88.2

3883.1

84.9

78.9

98.396.5

112109

80.1125119126103

80.8

106121

93.7

79108

23.5

51.2

131142

707070707070707070707070707070707070707070707070707070707070

130130130130130130130130130130130130130130130130130130130130130130130130130130130130

) 130

130

60.54

62.11

57.68

53.68

58.6854.74

41.590

37.9241.7

19.834.24

31.02

57.9156.81

41.01

64.660.89

64.82

53.5

38.32

56.3

63.81

47.53

38.99

54.9100

66.97

67.32

%RPD RPDLimit

4.06

66.8

5.93

12.3

8.0310.65.90

2009.14

1.7866.4

35.8

43.53.76

3.712.39

3.292.02

2.52

3.385.24

5.64

4.93

1.44

1.30

1.75

200200

2.27

5.48

2525

25252525

2525

25

252525252525

25

2525

252525252525252525252525

Qual

R2

R2

R2

R2

Rl

Rl





Page 22 of 31

Date: 10-Feb-03

CLIENT: RSSNWork Order: L0212203 :Project: DPW-9B • 8260_W

Sample ID: L021 2348-001 AM SampType: MSD

Batch ID: R9734

Analyte

p-Isopropyltoluene

Methylene chloride


Methyl t-butyl ether (MTBE)Naphthalene

n-Propylbenzene ,

Styrene


1 ,1 ,2,2-Tetrachloroethane

Tetrachloroethene

Toluene1 ,2,3-TricMorobenzene


1,1,1 -Trichloroetbane


Trichloroethene

Trichlorofluoromethane1 ,2,3-Trichloropropane



Vinyl acetate

Vinyl chloride

o-Xylenem,p-Xylene


Surr: Toluene-d8


Result

60.87

53.73

27,59

36.13ND

67.77

50.49

52.09

43.87

59.5

59.33

ND6.2

59.64

41.11

60.77

63.29

44.21

55.2662.08

51.49

54.33

52.27

108.6

44.65

48.44

45.39

TestCode. 8260JV Units: ug/L

TestNo: SW8260B


5.05.0255.010

5.05.05.05.0

5.05.05.05.05.05.05.05.05.05.05.05.05.05.010

0.50

0.50

0.50

50505050505050505050505050

50

50

5050505050505050

100505050

000000000000000000000000000



Prep Date:


Run ID: LJVOAMS-2J)21224A

SeqNo: 87513


122107

55.2

72.3

0136101104

87.7

119119

012.4

11982.2

122

12788.4

111

124

103109105109

89.3

96.990.8

707070707070707070

7070

'70707070707070707070707070

80.2

75.5

71.7

130130130130130130130130130130130130130130130130130130130130130130130130106105120

46.81

55.4525.55

35.21

062.22

47.12

50.9128.93

60.08

61.15

00

62.44

39.66

63.54

65.831.15

45.57

53.53

52.42

57.64

51.1

108.8

000

%RPD RPDLimit Qual

26.1

3.15

7.68

2.58

08.54

6.912.29

41.0

0.970

3.02

02004.59

3.59

4.46

3.8934.7

19.2

14.8

1.79

5.91

2.26

0.129000

252525 R2

2525 R2

25 Rl

252525252525 R225 R2

252525252525252525 '

2525

000





Page 23 of 31

Date: JO-Feb-03

CLIENT: RSSNWork Order: L0212203 >;

Project: ' DPW-9B ''

Sample ID: MB-R9396

Analyte


Alkalinity,! Carbonate (As CaCOS)

Hydroxide (As CaC03)Alkalinity, Total (As CaC03)


Analyte

Alkalinity, Total (As CaC03)


Analyte

Alkalinity, Total (As CaCO3)

Sample ID: L0212202-004CDUP

Analyte


Alkalinity, Carbonate (As CaCO3>


Alkalinity^ Total (As CaCO3)

J

SampType: MBLK

Batch ID: R9396

Result

ND

ND

NDND

SampType: LCS

Batch ID: R9396

Result

123

SampType: LCSD

Batch ID: R9396

Result

123

SampType: DUP

Batch ID: R9396

Result

238

ND

ND

238 -

ALK_W

TestCode: ALK_W Units: mg/L

TestNo: M2320 B


5.0

5.0

5.025


TestNo: M2320 B


25 125 0


TestNo. M2320 B


25 125 0

TestCode: ALKJW Units: mg/L

TestNo: M2320 B


5.0 0 0

5.0 0 0

5.0 0 0

25 0 0


Test Method: SM2320 B

Prep Date:



Prep Date:



98.4 80 120 0

Prep Date:



98.4 80 120 0

Prep Date:



0 0 0 2 5 4

0 0 0 0

0 0 0 0

0 0 0 2 5 4

Run ID: L_ATITR-1 J)21213B

SeqNo: 83850

%RPD RPDLimit Qual


SeqNo: 83849

%RPD RPDLimit Qual

0


SeqNo: 83852

%RPD RPDLimit Qual

0


SeqNo: 83851

%RPD RPDLimit Qual

6.50 100 10

0 10

6.50 10



J -This concentration is considered an estimate due to LCS failure.


Page 24 of 31

Date: 10-Feb-03

CLIENT: RSSN *Work Order: L0212203>;

Project: DPW-9B COD

ANALYTICAL QC SUMMARY REPORTTest Method: SM5520 D

Sample ID- MB-R9434

Analyte

SampType:

- Batch ID:

MBLK

R9434

Result

TestCode:

TestNo

PQL

COD

M5220 C

SPK value

Units: mg/L

SPKRefVal

Prep Date:



Run ID:

SeqNo:

L_SPEC-1_021218A

84239

%RPD RPDLimit Qual

Chemical Oxygen Demand ND 10

Sample ID LCS-R9434

Analyte

SampType:

Batch ID:

LCS

R9434

Result

TestCode

TestNo

PQL

COD

M5220 C

SPK value

Units: mg/L

SPKRefVal

Prep Date:



Run ID:

SeqNo:

LJSPEC-1J)21218A

84238

%RPD RPDLimit Qual

Chemical Oxygen Demand 515 10 500 103 80 120


Analyte

SampType: LCSD

." Batch ID: R9434

1 Result

TestCode: COD

TestNo: M5220 C

PQL SPK value

Units: mg/L

SPKRefVal

Prep Date:



Run ID: L_SPEC-1 JJ21218A

SeqNo: 84240

%RPD RPDLimit Qual

Chemical Oxygen Demand 510 10 500 102 80 120 515 0.976 15

Sample ID- L0212148-004AMS

Analyte

SampType: MS

Batch ID: R9434

Result

TestCode: COD Units: mg/L

TestNo: M5220 C


Prep Date:



Run ID: L_SPEC-1J)21218A

SeqNo: 84241

%RPD RPDLimit Qual

Chemical Oxygen Demand 531 10 478 44 102 70 130

Sample ID: L0212148-004AMSR SampType: MSD

i

Analyte

Batch ID: R9434

Result


TestNo: M5220 C


Prep Date:




SeqNo: 84242

%RPD RPDLimit Qual

Chemical Oxygen Demand 523 10 478 44 100 70 130 531 1.52 25





Page 25 of 31

Date: 10-Feb-03

CLIENT: RSSN ,-}•Work Order: L0212203,,Project: DPW-9B hg_7470_d



Sample ID- MB-1911

Analyte

SampType: MBLK

i Batch ID: 1911A

Result

TestCode: hg_7470_d Units: mg/L

TestNo: SW7470


Prep Date: 12/16/02



Run ID: RJHG-1J)21216A

SeqNo: 83709

%RPD RPDLimit Qual

Mercury > ND 0.00020

Sample ID': LCS-1911

Analyte

SampType: LCS

Batch ID: 1911

Result


TestNo: SW7470


Prep Date: 12/16/02



Run ID: RJIG-1J>21216A

SeqNo: 83708

%RPD RPDLimit Qual

Mercury 0,00507 0.00020 0.005 101 85 115

Sample ID: L0212202-003AMS '

Analyte ..

SampType: MS

Batch ID: 1911

Result

TestCode: HG_7470J> Units: mg/L

TestNo: SW7470


Prep Date: 12/16/02



Run ID:' RJHG-1 JJ21216A

SeqNo: 83691

%RPD RPDLimit Qual

Mercury 0.00484 0.00020 0.005 96.8 85 115


-

Analyte

SampType: MSD

Batch ID: 1911

Result

TestCode: HG_7470J> Units: mg/L

TestNo: SW7470


Prep Date: 12/16/02



Run ID: RJHG-1 JJ21216A

SeqNo: 83692

%RPD RPDLimit Qual

Mercury 0.00495 0.00020 0.005 99 0.00484 2.25 20





Page 26 of 31

Date: 10-Feb-03

CLIENT: RSSN *Work Order: L0212203cProject: DPW-9B ; HG 7470 T

ANALYTICAL QC SUMMARY REPORTTest Method: SW 7470-Total

Sample ID: MB-1913

Analyte

j, SampType: MBLK

; Batch ID: 1913

Result

TestCode: hg_7470J Units: mg/L

TestNo: SW7470


Prep Date: 12/16/02



Run ID: RJHG-1 JJ21216C

SeqNo: 83750

%RPD RPDLimit Qual

Mercury ND 0.00020

Sample ID: LCS-1913

Analyte

" SampType: LCS

Batch ID: 1913

Result

TestCode: hg_7470_t Units: mg/L

TestNo: SW7470


Prep Date: 12/16/02



Run ID: RJHG-1 J>21 21 6C

SeqNo: 83749

%RPD RPDLimit Qual

Mercury 0.00484 0.00020 0.005 96.8 85 115


•

Analyte

SampType: MS

Batch ID: 1913

Result

TestCode: HG_7470_T Units: mg/L

TestNo: SW7470


Prep Date: 12/16/02



Run ID: RJHG-1 J121216C

SeqNo: 83731

%RPD RPDLimit Qual

Mercury 0.00375 0.00020 0.005 75 85 115

Sample ID:

Analyte

L0212202-002AMSD

';

SampType:

Batch ID:

MSD

1913

Result

TestCode

TestNo

PQL

HG_7470JT

SW7470

SPK value

Units: mg/L

SPKRefVal

Prep Date:

Analysis Date:

12/16/02

12/16/02


Run ID: RJHG-1 JI21216C

SeqNo: 83732

%RPD RPDLimit Qual

Mercury 0.00391 0.00020 0.005 78.2 0.00375 4.18 20

Qualifiers: ND - Not Delected at the Reporting Limit C - Unspiked sample >5 times the amount spikedt




Page 27 of 31

Date: 10-Feb-03

CLIENT:Work Order:Project:

RSSN iL0212203-!DPW-9B 7 NH3-N W


Test Method: SM4500-NH3 C

Sample ID: MB-R9421

Analyte

SampType: MBLK

Batch ID: R9421

Result

TestCode: NH3-NJW Units: mg/L

TestNo: M4500-NH3 C


Prep Date:



Run ID: L_WC_021217D

SeqNo: 84095

%RPD RPDLimit Qual

Ammonia, as N ND 0.30

Sample ID; LCS-R9421

Analyte

, SampType: LCS

!) Batch ID: R9421

Result

TestCode: NH3-NJW Units: mg/L

TestNo: M4500-NH3 C


Prep Date:



Run ID: LJWC_021217D

SeqNo: 84094

%RPD RPDLimit Qual

Ammonia, as N 0.9 0.30 90 83.9 117

Sample ID: LCSD-R9421 SampType. LCSD

Analyte

Batch ID: R9421

Result

TestCode:

TestNo

PQL

NH3-NJW

M4500-NH3

SPK value

Units: mg/L

C

SPKRefVal

Prep Date:


%REC LowLimit HighLimit RPD Ref Val

Run ID:

SeqNo:

L_WC_021217D

84096

%RPD RPDLimit Qual

Ammonia, as N 1.01 0.30 101 83.9 117 0.9 11.5 25


Analyte

SampType: MS

Batch ID: R9421

Result

TestCode: NH3-N_W Units: mg/L

TestNo: M4500-NH3 C


Prep Date:



Run ID: LJWCJ)21217D

SeqNo: 84097

%RPD RPDLimit Qual

Ammonia, as N 1.01 0.30 101 76.4 124

Qualifiers: ND - Not Defected at the Reporting Limiti

Jl - MS or MSD outside accepance limits. LCS acceptable.

C - Unspiked sample >5 times the amount spiked

R - RPD outside accepted recovery limits



Page 28 of 31

Date: 10-Feb-03

CLIENT: RSSN

Work Order: L0212203;

Project: DPW-9B . PH W




Analyte

SampType: LCS

Batch ID: R9371

Result

TestCode: PH_W

TestNo: E150.1

PQL SPK value

Units: pH units

SPKRefVal %REC

Prep Date:



Run ID: L_ATITR-1 J»21212A

SeqNo: 83443

%RPD RPDLimit Qual

pH 6.98 1.00 99.7 99.3 100.7


Analyte

1 SampType: LCSD

Batch ID: R9371

Result

TestCode: PHJW

TestNo: E150.1

PQL SPK value

Units: pH units

SPKRefVal %REC

Prep Date:

.Analysis Date: 12/12/02


Run ID: L_ATITR-1_021212A

SeqNo: 83444

%RPD RPDLimit Qual

pH 6.98 1.00 99.7 99.3 100.7


Analyte

SampType:

Batch ID:

DUP

R9371

Result

TestCode

TestNo

PQL

PHJW

E150.1

SPK value

Units: pH units

SPKRefVal %REC

Prep Date:



Run ID:

SeqNo:

L_ATITR-1J121212A

83616

%RPD RPDLimit Qual

pH 1.00 7.71 1.16





Page 29 of 31

Date: 10-Feb-03


RSSN g

L0212203^

DPW-9B '-• SULF W


Test Method: SM4500-S D

Sample ID: MB-R9393

Analyte

=• SampType: MBLK

, Batch ID: R9393

Result

TestCode: SULFJW Units: mg/L

TestNo: M4500-S D


Prep Date:



Run ID: L_SPEC-2_021213D

SeqNo: 83760

%RPD RPDLimit Qual

Sulflde ND 0.030


Analyte

SampType: LCS

Batch ID: R9393

Result


TestNo: M4500-S D


Prep Date:

' Analysis Date: 12/13/02



SeqNo: 83759

%RPD RPDLimit Qual

Sulfide 0.108 0.030 0.107 10! 80 120


Analyte

'• SampType: LCSD

Batch ID: R9393

Result


TestNo: M4500-S D


Prep Date:


_%REC LowLimit HighLimit RPDRefVal

Run ID: LJSPEC-2J021213D

SeqNo: 83761

%RPD RPDLimil Qual

Sulfide 0.113 0.030 0.107 106 80 120 0.108 4.52 25

Sample ID. L0212203-006AMS

Analyte

SampType: MS

Batch ID: R9393

Result


TestNo: M4500-S D


Prep Date:



Run ID: LJ3PEC-2J021213D

SeqNo: 83762

%RPD RPDLimit Qual

Sulfide 0.107 0.030 0.107 100 70 130


i

Analyte

SampType: MSD

Batch ID: R9393

Result


TestNo: M4500-S D


Prep Date:



Run ID: LJSPEC-2J021213D

SeqNo: 83763

%RPD RPDLimit Qual

Sulfide 0.106 0.030 0.107 99.1 70 130 0.107 0.939 25





Page 30 of 31

Date: 10-Feb-03


RSSN *•L0212203cDPW-9B '' TDS W


Test Method: SM2540 C

Sample ID: MB-R9369

Analyte

:- SampType: MBLK

* Batch ID: R9369

Result

TestCode: TDSJW Units: mg/L

TestNo: E160.1


Prep Date:



Run ID: LJWCJ021213A

SeqNo: 83424

%RPD RPDLimit Qual

Total Dissolved Solids ND 15.0

Sample ID;. LCS-R9369

Analyte

SampType: LCS

Batch ID: R9369

Result

TestCode: TDSJW Units' mg/L

TestNo: E160.1


Prep Date:



Run ID: LJWCJ)21213A

SeqNo: 83423

%RPD RPDLimit Qual

Total Dissolved Solids 950 150 1000 95 80 120

Sample ID:

Analyte

L0212032-001DDUPi

1SampType:

Batch ID:

DUP

R9369

Result

TestCode

TestNo

PQL

TDSJW

E160.1

SPK value

Units: mg/L

SPKRefVal

Prep Date:


%REC LowLimit HighLimit "RPDRefVal

Run ID: LJWC_021213A

SeqNo: 83425

%RPD RPDLimit Qual

Total Dissolved Solids 329 15.0 272 19.0 25





Page 31 0/37

Date: 10-Feb-03

NEL LABORATORIESCorporate Headquarters Las Vegas Laboratory6490 S. McCarran Blvd. # 0-30 4208 Arcata Way, Suite AReno, NV 89509 Las Vegas, NV 89030Phone- 775.348.2522 Phone: 702.657.1010Fax: 775.348.2546 Fax: 702.657.1577

RSSN

RSSN

7900 Vegas Valley DriveLas Vegas, NV 89142

TEL: 702-431-3020

RE Project: PW-9B

Dear RSSN: "

Order No.: L0212202

NEL Laboratories, Las Vegas received 7 samples on 12/12/02 for the analyses presented in thefollowing report.

There were no problems with the analyses and all data for associated QC met EPA or laboratoryspecifications unless noted in the Case Narrative.

If you have any questions regarding these tests results, please feel free to call.

Rod T. MillerLaboratory Director

//ot/oz/ Date

Certifications:ArizonaCaliforniaIdahoMontanaNevadaNew Mexico

AZ05182002CertifiedCertifiedNV052Certified

Albuquerque866.360.5726

Boise800.200.2952

Las Vegas888.368.3282

Phoenix888.238.2514

Reno800.368.5221

Sacramento800.368.5221

NEL LABORATORIES

NEL Laboratories, Las Vegas Date: ll-Feb-03

CLIENT: RSSN

Project: PW-9B CASE NARRATIVELab Order: L0212202

Attached are the analytical results for samples in support of the above referenced project.

The samples submitted for this project were not sampled by NEL. Should you have any questions orcomments, please feel free to contact our Client Services Department.

Analytical Comments:

EPA 8260: Samples were evaluated for the presence of Acrylonitrile and trans-l,4-Dichloro-2-butene.Neither of these two compounds were present in the samples submitted in this work-order at or above5ppb.

Page 1 of 1

NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: PW-9B

PROJECT #: PW-9B

MATRIX: AQUEOUS

ParameterAcetone

Benzene

Brornobenzene

Bromochloromethane


Bromoform

Bromomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide


Chlorobenzene

Chloroethane


Chloroform

Chloromethane

2-Chloro toluene

4-CMorotoluene



1 ,2-Dibrotnoethane

Dibromomethane





1 ,1 -Dichloroethane

1 ,2-Dichloroethane


cis- 1 ,2-Dichloroethene


1 ,2-DichIoropropane


2,2-Dichloropropane




Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

Isopropylbenzene

Result Units

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND .ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND-- Not Detected at the Reporting Limit


Date: 10-Feb-03

CLIENT ID: PW-9B



ReportingLimit

255.05.05.05.05.05.025

5.0

5.05.05.05.05.05.05.05.05.05.05.05.05.0

5.05.05.0

5.05.0

5.05.05.05.05.05.05.05.05.05.05.05.05.05.0255.05.0


DF Method Prep Date

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B - " •

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

in the associated Method Blank •

Analyzed

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

, 12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV"DRM-LV

DRM-LV


E - Value above quantitation range Page 1 of 1 1

NEL LABORATORIES

CLIENT: RSSN

PROJECT LD: PW-9B

PROJECT #: PW-9B .

MATRIX: AQUEOUS


Methylene chlonde



Naphthalene

n-Propylbenzene

Styiene


1 , 1 ,2,2-Tetrachloroe thane

Tetrachloroethene

Toluene



1,1,1-Tnchloroethane

1 , 1 ,2-Tnchloroethane

Tnchloroethene

Tnchlorofluoromethane

1 ,2,3-Tnchloropropane



Vinyl acetate

Vinyl chlonde

o-Xylene

m,p-Xylene


Surr: Toluene-d8


Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

8.2

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND94.1

97.8

98.3

Units

ug/L

ug/L

ug/L

ug/L

Mg/L

ug/L

pg/L

ug/L

ug/L

ng/LMg/L

ug/L

U-g/L L2

Mg/L

Mg/L

ug/L

Mg/L

Mg/L

Mg/L

Mg/L

Mg/L

Mg/L

Mg/L

Mg/L

%REC

%REC

%REC

ReportingLimit

50

50

25

50

10

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

10802-106

75 5-105

71 7-120

CLIENT ID: PW-9B



DF Method Prep Date

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B _

1 SW8260B

1 SW8260B

1 " SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

Analyzed

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03 '

12/24/03

12/24/03

12/24/03

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

ND - Not Detected at the Repoitmg Limit


Date: 10-Feb-03

B -Analyte detected in the associated Method Blank



NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: PW-9B

PROJECT #: PW-9B

MATRIX: AQUEOUS

Parameter

AluminumBarium

Calcium

Iron

Magnesium

Potassium

SodiumVanadium

Antimony• Arsenic

BerylliumCadmium

Chromium

Cobalt

CopperLeadManganeseNickel

SeleniumSilver

ThalliumZinc

Mercury

Result

0.38

0.0455809.020022

240

0.013

NDNDNDND

0.0590.012

0.096

0.00901.1

0.14

ND

ND

ND0.19

ND

Units

mg/L B

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L B

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.050

0.00500.20

0.10

0.20

2.00.50

0.00500.0050

00050

• i' -P)050,0.00500.0050

0.00500.0050

0.00500.00500.0050

0.00500,0050

0.00200.0050

0.00020

CLIENT ID:

DATE SAMPLED:

NEL SAMPLE ED:

DEllll1lll5

5'

5

555555

5

55551

Method

SW 6010B-TOSW 6010B-TO

SW 6010B-TO

SW 6010B-TOSW 60108-To

SW6010B-To

SW6010B-TO

SW6010B-TOSW 6020-Tota


SW 6020-TotaSW 6020-TotaSW 6020-Tota

SW 6020-Tota





PW-9B-M

12/12/02

L0212202-002A

Prep Date

12/13/0212/13/02

12/13/02.

12/13/0212/13/02

12/13/02

12/13/0212/13/02

12/12/0212/12/02

12/12/0212/12/02

12/12/0212/12/02

12/12/02

12/12/0212/12/0212/12/02

12/12/0212/12/0212/12/02

12/12/0212/16/02

Analyzed

12/16/0212/16/02

12/16/02

12/16/02

12/16/0212/16/02

12/16/02

12/16/0212/17/02

12/17/0212/17/02

12/17/0212/17/02

12/17/02

12/17/0212/17/0212/17/02

12/17/0212/17/0212/17/02

12/17/0212/17/0212/16/02

Analyst

WG-LVWG-LV

WG-LV

WG-LVWG-LV

WG-LV

WG-LVWG-LVRMD-LVRMD-LV

RMD-LV

RMD-LVRMD-LV

RMD-LVRMD-LV

RMD-LV' RMD-LV

RMD-LVRMD-LVRMD-LVRMD-LV

RMD-LVFAS-LV

ND - Not Detected at the-Reporting Limit


Date: 10-Feb-03




NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: PW-9B

PROJECT #: PW-9B

MATRIX:

ParameterAluminumBarium

Calcium

IronMagnesium

Potassium

Sodium

Vanadium

AntimonyArsenicBeryllium

CadmiumChromium

CobaltCopper

LeadManganese

NickelSelenium

SilverThalliumZincMercury

Result

0.0830.032

5200.22

18026

220NDND

0.0060NDNDNDND

0.0092

0.0050

0.41

0.080

0.0058

ND0.0021

0.41

ND

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L B

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/Lmg/L

mg/L

mg/L

ReportingLimit

0.0500.0050

0.20

0.10

0202.00.50

0.00500.0050

0.00500.00500.00500.0050

0.0050

0.0050

0.00500.0050

0.00500.00500.00500.00200.00500.00020

CLIENT ID: PW-9B-FFM


NEL SAMPLE ID: L02 12202-003 A

DF1lllll1155555

55555555

51

Method Prep Date

SW6010B-DiSW6010B-DJSW 6010B-DJ

SW 6010B-D1

SW 6010B-DiSW 6010B-Di

SW6010B-Di

SW6010B-DJSW 6020-Diss

SW 6020-DissSW 6020-DissSW 6020-Diss

SW 6020-DissSW 6020-Diss

SW 6020-Diss

SW 6020-DissSW 6020-Diss

SW 6020-DissSW 6020-DissSW 6020-Diss

SW 6020-DissSW 6020-DissSW7470-Diss 12/16/02

Analyzed

12/20/0212/20/0212/20/02

12/20/0212/20/02

12/20/02

12/20/02

12/20/0212/18/0212/18/0212/18/0212/18/02

12/18/02 '12/18/02

12/18/02

12/18/0212/18/02

12/18/0212/18/0212/18/0212/18/0212/18/0212/16/02

Analyst

WG-LVWG-LVWG-LV

WG-LVWG-LV

WG-LV

WG-LVWG-LV

RMD-LVRMD-LVRMD-LVRMD-LVRMD-LV

RMD-LVRMD-LV

RMD-LVRMD-LV

RMD-LVRMD-LVRMD-LVRMD-LVRMD-LVFAS-LV



Date: 10-Feb-03

B - Analyte detected in the associated Method Blank,



NEL LABORATORIES

CLIENT:

PROJECT ID:

PROJECT #:

MATRIX:

RSSN

PW-9B

PW-9B

Parameter Result Units

Chemical Oxygen Demand 41 mg/L

Ammonia, as N ND mg/L

CLIENT ID:

DATE SAMPLED:

NEL SAMPLE ID:

Reporting

Limit DF Method

10 I SM5520 D

0 30 1 SM4500-NH3

PW-9B

12/12/02

L0212202-004A

Prep Date Analyzed Analyst

12/18/02 RDA-LV

12/17/02 ' BTM-LV

ND -Not Detected at the Reporting Limit- B - Analyte detected in the associated Method Blank

DF - Dilution Factor S - Spike Recovery outside accepted recovery limits

Date: 10-Feb-03 E - Value above quantitation range Page 5 of 11

NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: PW-9B

PROJECT #: PW-9B

MATRIX:

ParameterChloride

Nitrate, as N

Nitrite, as N

Sulfate


Alkalinity, Carbonate (As CaCO3)



PHTotal Dissolved Solids

CLIENT LD:

DATE SAMPLED:

Result

320NDND2000

250

NDND250

7.25

3790

Units

mg/L

mg/L

mg/L •

mg/L

mg/L

mg/L

mg/L

mg/L

pH units

mg/L

ReportingLimit

1000.10

0.10

1005.05.05.025

1.00

60.0

NEL

DF:1000

11

1000

111114

SAMPLE ID:

Method

EPA 300.0

EPA 300.0

EPA 300.0

EPA 300.0

SM2320 B

SM2320 B

SM2320 B

SM2320 B

EPA 150.1

SM2540 C

PW-9B

12/12/02

L0212202-004C

Prep Date Analyzed

12/19/02

12/13/02

12/13/02

12/19/02

12/13/02

12/13/02

12/13/02

12/13/02

12/12/02

12/13/02

Analyst

RDA-LV

PJJ-LV

PJJ-LV

RDA-LV

CRA-LV

CRA-LV

CRA-LV

CRA-LV

CRA-LV

CRA-LV

- • ND - Not Detected at the Reporting Limit -.


Date: 10-Feb-03

B - AnaJyte detected in the associated Method Blank



NEL LABORATORIES

CLIENT: RSSN CLIENT ID: PW-9B

PROJECT ID: PW-9B DATE SAMPLED: 12/12/02

PROJECT #: PW-9B NEL SAMPLE ID: L0212202-005A

MATRIX:

ReportingParameter Result Units Limit DF Method Prep Date Analyzed

Sulfide ND mg/L 0.030 1 SM4500-S D 12/13/02'

ND - Not Detected at the Reporting Limit ._. . ^. B - Analyte detected in the associated Method Blank _ ,

DF - Dilution Factor S - Spike Recovery outside accepted recovery limits

Date: 10-Feb-03 E - Value above quantitation range Page 7 of 11

NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: PW-9B

PROJECT #: PW-9B

MATRIX: AQUEOUS

Parameter ]Acetone

Benzene

Bromobenzene

Bromochloromethane


Bromoform

Bromomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide


Chlorobenzene

Chloroethane

2:Chloroethyl vinyl ether

Chloroform

Chloromethane

2-Chlorotoluene

4-Chlorotoluene

Dibromochlorome thane


1 ,2-Dibromoethane

Dibromomethane




Dichlorodifluorometliane

1,1-Dichloroethane

1 ,2-Dichloroethane

1,1-Dichloroethene





2,2-Dichloropropane

1,1-Dichloropropene


trans- 1 ,3-Dichloroprbpene

Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

Isopropylbenzene



Date: 10-Feb-03

CLIENT ID: FPW-9B (Field Blank)



Result Units

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L'

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

- -

ReportingLimit

255.05.05.05.05.05.0255.05.05.05.05.05.0

5.05.05.05.0

5.05.05.0

5.0

5.0

5.0

5.0

5.05.0

5.05.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0-

5.0

5.0255.05.0


DF Method Prep Date

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

^1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

I SW8260B

in the associated Method Blank

Analyzed

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03 '

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

. . . . . . . -.. ,

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV


E - Value above quantitation range Page 8 of 1 1

NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: PW-9B

_ PROJECTS PW-9B

MATRIX: AQUEOUS


Methylene chloride



Naphthalene

n-Propylbenzene

Styrene


1 ,1,2,2-TetrachIoroethane

Tetrachloroethene

Toluene




1 ,1 ,2-Trichloroethane

Trichloroethene




1 ,3 ,5-Tnmethylbenzene

Vinyl acetate

Vinyl chloride

o-Xylene ,. ,.'(gj./s1..

m,p-Xylene


Surr: Toluene-d8


Result

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND91.4

97.6

98.2

Units

Mg/L

Mg/LMg/L

Mg/L

Mg/L

Mg/L

Mg/L

Mg/L

Mg/LMg/LMg/LMg/LUg/L L2

Mg/L

Mg/L

Mg/L

Mg/L

Mg/L

Mg/L

Mg/L

Mg/LMg/L

Mg/L

Mg/L%REC%REC%REC

ReportingLimit

5.0

5.0

25

5.0

10

5.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.010

80.2-106

75.5-105

71.7-120

CLIENT ID : FP W-9B (Field Blank)

DATE SAMPLED : 1 2/1 2/02

NEL SAMPLE LD: L0212202-006A

DF Method

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

Prep Date Analyzed

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV



Date: 10-Feb-03

B --Analyte detected in the associated Method Blank



NEL LABORATORIES

CLIENT: RSSN

PROJECTED: PW-9B

PROJECT #: PW-9B

MATRIX: AQUEOUS

ParameterAcetone

Benzene

Bromobenzene

Bromochlorome thane


Bromoform

Bromomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide


Chlorobenzene

Chloroethane


Chloroform

Chloromethane

2-ChIoro toluene

4-Chlorotoluene



1 ,2-Dibromoethane

Dibromomethane


1,3-Dichlorobenzene



1 ,1-Dichloroethane

1 ,2-Dichloroethane

1,1-Dichloroethene





2,2-Dichloropropane



trans- 1 ,3-Dichloropropene

Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

Isopropylbenzene

Result Units

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND Mg/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND' ug/L'

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND - Not Detected, at the Reporting Limit . . . - „ . .


Date: 10-Feb-03

CLIENT ED: TPW-9B (Trip Blank)



ReportingLimit

255.0505.05.05.05.0255.05.05.05.05.05.05.05.05.05.05.05.05.0

5.0

5.05.05.0

5.05.0

5.0S.O

5.0

5.0

5.0505.0

5.05.05.05.05.05.05.0255.05.0

- B - Analyte detected

DF Method Prep Date

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW826QB

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B


Analyzed

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV.

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV r '

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV - '

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

-. -' , >•-. , - - -


E - Value above quantitation range Page 10 of l l

NEL LABORATORIES

CLIENT: RSSN

PROJECTED: PW-9B

PROJECT #: PW-9B

MATRIX: AQUEOUS

Parameter

p-Isopropyltoluene

Memylene chloride4-Methyl-2-pentanone


Naphthalene

n-Propylbenzene

Styrene

1 , 1 ,1 ,2-Tetrachloroethane


TetrachloroetheneToluene1 ,2,3-Trichlorobenzene



1 ,1 ,2-Tnchloroethane

Trichloroethene





Vinyl acetate

Vinyl chloride

o-Xylene

m,p-Xylene


Surr: Toluene-d8Surr: 4-Bromofluorobenzene

Result

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND92.0

96.995.6

Units

Mg/LMg/LMg/L

Mg/L

Mg/L

MS/L

Mg/L

Mg/L

Mg/L .

Mg/L

Mg/L

Mg/Lug/L L2

M8/L

Mg/L

Mg/L 'Mg^L

Mg/L

Mg/L

Mg/L

Mg/L

Mg/L

Mg/L

Mg/L%REC%REC%REC

ReportingLimit

5.0

5.025

5.0105.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.0

1080.2-106

75.5-10571.7-120

CLIENT LD: TPW-9B (Trip Blank)


NEL SAMPLE ED: L02 12202-007 A

DF

1lllll11llllll11lll111ll1ll

Method

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B "

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260BSW8260B

Prep Date Analyzed

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/0312/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/03

12/24/0312/24/03

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LVDRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LVDRM-LV

• ND - Not Detected at the Reporting Limit


Date: 10-Feb-03

B -Analyte detected in the associated Method BJank



12/24/2002 TUB 10:12 FAX 559 485 6935 BSK LABS @002/002

A N A L Y T I C A LLABORATORIES

Andrea Certificate of AnalysisNEL Laboratories Las Vegas ELAP Certificate #11804208 AlCata Way, Ste A Report Issue Date: 12/24/2002

Las Vegas, NV 89030

BSK Submission #: 2002121064BSK Sample ID #: 276195Project ID: L.&^ ' fi^<) •.. Project Desc:

Submission Comments:Sample Type:

Sample Description:Sample Comments:

Inorganics

Analyte

LiquidPW-9B

Total Organic Carbon (TOC)

Date Sampled: 12/12/2002Time Sampled: Q830Date Received: 12/17/2002

Prep AnalysisMethod Result Units PQL Dilution DLR Date Date

SM5310-C 1.1 mg/L 0.2 1 0.2 12/18/2002 12/18/2002

mg/L: Milligrams/Liter (pprn) PQL: Practical Quantitation Limit H: Analyzed outside of hold timerag/Kg. Milligrams/Kilogram (ppm) DLR: Detection Limit for Reporting P. Preliminary resultug/L: Micrograms/Liter (ppb) : PQL x Dilution S: Suspect result See Cover Letter for comments.ug/Kg: Micrograms/Kflogram (ppb) ND: None Detected at DLR E: Analysis performed by External laboratory.%Rec: Percent Recovered (surrogates) See External Laboratory Report attachments.

ationCcde:" lilllllilillllllililliUIIIIEIIilglOllllliyi " ' " ' Page 2 of 2 ' "

1414 Stanislaus Street Fresno, CA 93706-1623 Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935

NEL LABORATORIES CHAIN OF CUSTODY NEL Work Order:

Las Vegas Laboratory4208 Arcata Way, Ste AN Las Vegas, NV 89030Phone 702-657-1010

Fax 702-657-1577

RenoLas VegasPhoenixBoiseSacramentoAlbuquerqueDenver

800 368 5221

888 368-3282888-238 2514800 200-2952800-368 5221866-<360 5726888 900 7477

Public Water System (PWS) Number:Project Name

'urchase Order Number

NEL Quote No

Project Number

Sampled By

NEL Sales Rep / ' " f7 7"

Company Attention

Address,

Qty, State Z,p Co

Phone Number

Billing Address'

Number /" » \/ 'fe ) •-/ y - bo 7Expected Due Date

Requested Turnaround

SampledTime Date

5-day. .2-day. .1-day.

Customer Sample Identification

_Other

NELID

Analysis

Note#1. * ,Enter the numbercontainers submitted for tneindicated Analysis followedby the preservation (see Box#2 below)Eg [3A"l= 3 containers with

HCI preservation

Remarks

if. ' .-1

tf£rl /if08'Hl Afl

'"'tftnj.

'£7

Custody Seal intact? Y N

Condition when received

Temp. Box#1 DW Drinking Water SD SolidWW Waste Water AQ AqueousOL Oil/Organic Liquid A Air

Box #2 A HCIB HN03C HSOD

E Ice OnlyFOtherG Not Preserved

Relinquished by (Print) Signature Date/Time Received by (Print) Signature Date/Time

A f • «°f'\. P. V&jkj r\n/-

LAB COPY

NEL LABORATORIESill i H'l

.A spH'fiff $11 IS it M 11_ ^ 3Js !-£?£ ^tlJi-vteJirf iLri1 si

CLIENT: RSSN •Work Order: L02 12202-Pr eject: . PW-9B •

Sample ID: MB-R9366

Analyte

Chloride

Nitrate, as N

Nitrite, as NSulfate

Sample ID: MB-R9495

Analyte

Chloride

Nitrate, as N



Analyte !

Chloride _>

Nitrate, as N

Nitrite, as N '.-

Sulfate

i114: ft fife. , . .,.,.,., — ,..,.

9 ;

' ' '

>


SampType: MBLK TestCode: 300_W

Batch ID: R9366 TestNo: E300

Result PQL SPK value

ND 0,10

ND 0.10

ND 0.10

ND 0.10

SampType: MBLK TestCode: 300_W



ND 0.10 0

ND 0.10 0

ND 0.10 0ND 0.10 0

SampType: LCS TestCode: 300_W



1.829 0.10 2

0.948 0.10 1

0.957 0.10 12.373 0.10 2,5

300_W

Units: mg/L

SPKRefVal

Units: mg/L

SPKRefVal

0000

Units: mg/L

SPKRefVal

0000

Prep Date:

Analysis Date:

Test Method:

12/13/02


Prep Date:



0 0

0 0

0 00 0

Prep Date:

Analysis Date:

0 0

0 00 00 0

12/13/02

%REC LowLirnit HighLimit RPDRefVal

91.4 80

94.8 80

95.7 80

94.9 80

120 0120 0

120 0120 0

EPA 300.0


SeqNo: 83382

%RPD RPDLimit Qual


SeqNo: 84959

%RPD RPDLimit Qual

0000


SeqNo: 83381

%RPD RPDLimit Qual

0000





Page 1 of 31

Date: 10-Feb-03

CLIENT: RSSN :Work Order: L0212202'Project: PW-9B 300 W




j

Analyte '

Chloride I

Nitrate, as N [



Analyte

ChlorideNitrate, as N

Nitrite, as NSulfate ''.

Sample ID: LCSD-R9495 ?,

Analyte

ChlorideNitrate, as N

Nitrite, as N

Sulfate

Sample ID: L0212197-001DMS

Analyte

Chloride

Sulfate

SampType: LCS

Batch ID: R9495

Result

1.964

0.9450.913

2.561

SampType: LCSD

Batch ID: R9366

Result

1.835

0.9370.901

2.433

SampType: LCSD

Batch ID: R9495

Result

1.994

t< 0.944

$ 0.927

2.579

SampType: MS

Batch ID: R9495

Result

174.5

65.67

TestCode:

TestNo:

PQL

0.10

0.10

0.10

0.10

TestCode:

TestNo:

PQL

0.10

0.10

0.100.10

TestCode:

TestNo:

PQL

0.10

0.10

0.10

0.10

TestCode

TestNo

PQL

5.05.0

300_W

E300

SPK value

211

2.5

300_W

E300

SPK value

211

2.5

300_W

E300

SPK value

21

1

2.5

300_W

E300

SPK value

5050

Units: mg/L

SPK Ref Val

0

0

0

0

Units: mg/L

SPKRefVal

0000

Units: mg/L

SPKRefVal

0

0

00

Units: mg/L

SPKRefVal

120.5

22.78

%REC

98.2

94.5

91.3

102

%REC

91.893.7

90.1

97.3

%REC

99.7

94.4

92,7

103

%REC

10885.8

Prep Date:


LowLimit HighLimit

80808080

Prep Date:

Analysis Date:

120120120120

12/13/02

LowLimit HighLimit

8080

8080

Prep Date:

Analysis Date:

120

120

120120

12/19/02

LowLimit HighLimit

80808080

Prep Date:

Analysis Date:

120120

120

120

12/19/02

LowLimit HighLimit

8080

120120

RPDRefVal

0000

RPDRefVal

0000

RPD Ref Val

1.964

0.945

0.913

2.561

RPDRefVal

00

Run ID. LJC-1_021219A

SeqNo: 84958

%RPD RPDLimit Qual

0000


SeqNo: 83383

%RPD RPDLimit Qual

0000


SeqNo: 84960

%RPD RPDLimit Qual

1.52 25

0.106 25

1.52 25

0.700 25


SeqNo: 84966

%RPD RPDLimit Qual

00

Qualifiers: ND - Not Detected at the Reporting Limit " C - Unspiked sample >5 times the amount spiked


! J - This concentration is considered an estimate due to LCS failure.


Page 2 of 31

Date: 10-Feb-03


RSSN |L0212202^,PW-9B 300 W



Sample ID: L0212202-004CMS

Analyte

Chloride

Sulfate


Analyte -

Chlonde

Sulfate

Sample ID: L0212221-007CMS .

Analyte

SampType: MS

Batch ID: R9495

Result

1317

2880

SampType: MS

Batch ID: R9495

Result

56.565.4

SampType: MS

Batch ID: R9366

Result

TestCode:

TestNo:

PQL

100100

TestCode:

TestNo:

PQL

5.05.0

TcslCode:

TestNo:

PQL

300JW

E300

SPK value

1000

1000

300_\V

E300

SPK value

5050

300_W

E300

SPK value

Units: mg/L

SPKRefVal

317.2

2025

Units: mg/L

SPKRefVal

9.035

20

Units: mg/L

SPKRefVal

Prep Date:



100 80

85.6 80

Prep Date:

"" Analysis Date:

120 0

120 0

12/19/02


94.9 80

90.8 80

Pi ep Dale.

Analysis Date:

120 0

120 0

12/13/02


Run ID:

SeqNo:

L_IC-1_021219A

85010

%RPD

Run ID:

SeqNo:

00

L_

RPDLimit

IC-1_021219A

Qual

85386

%RPD

Run ID:

SeqNo:

00

L_

RPDLimit

IC-1_021213A

Qual

86037

%RPD RPDLimit Qual

Nitrate, as N 9710 1000 10000 97.1 80 120

Sample ID: L0212202-004CMSD SampType: MSD

Analyle

Chloride

Sulfate

Batch ID: R9495

Result

; 1252

2928

TestCode: 300_W Units: mg/L Prep Date:

TestNo: E300

PQL

100100

SPK value

1000

1000

SPKRefVal

317.2

2025

%REC

93.5

90.4


LowLimit

7070

HighLimit

130130

RPDRefVal

1317

2880

Run ID L_IC-1_021219A

SeqNo: 85011

%RPD

5.08

1.66

RPDLimit

2525

Qual





Page 3 of 31

Date: 10-Feb-03

CLIENT: RSSNWork Order: L02122021"Project: PW-9B ,

Sample ID: MB-R9503

•

Analyte

Aluminum

Barium

Calcium ,

Iron i

Magnesium f

Potassium

Sodium

Vanadium

Sample ID' LCS-9503

Analyte

Aluminum ,

Barium

Calcium

Iron 'i

Magnesium

Potassium

Sodium

Vanadium

Sample ID: L0212202-003AMS"

Analyte

Aluminum

Barium

Calcium

Iron


SampType: MBLK

Batch ID: R9503

Result

ND

ND

ND

ND

ND

ND1.34

ND

SampType: LCS

Batch ID: R9503

Result

0.915

0.9072

17.7

0.8712

18.2819.09

18.60.2142

SampType MS

Batch ID: R9503

Result

1.08

0.8893

508.5

1.073

TestCode:

TestNo:

PQL

0.050

0.0050

0.50

0.10

0.50

2.00.50

0.0050

TestCode:

TestNo:

PQL ,

0.050

0.0050

0.50

0.10

0.50

2.00.50

0.0050

TestCode

TestNo

PQL

0.050

0.0050

0.500.10

6010W_D

SW6010B

SPK value

6010W_D

SW6010B

SPK value

1

1

20

1

2020

200.25

6010W_D

SW6010B

SPK value

1

1

201

6010W_D

Units: mg/L

SPKRefVal

Units: mg/L

SPKRefVal

0

0

0

0

00

1.34

0

Units: mg/L

SPKRefVal

0.083

0.03213

522.3

0.2244

Test Method: SW 6010B-Diss ,

%REC

%REC

91.5

90.7

88.5

87.191.4

95.4

86.3

85.7

%REC

99.7

85.7

-6984.8

Prep Date:



Prep Date:

Analysis Date:

.


SeqNo: 85119

%RPD RPDLimit Qual


12/20/02


85

85

85

85

8585

85

85

Prep Date:

Analysis Dale:

115 0

115 0115 0

115 0

115 0115 0

115 0115 0

SeqNo. 85120

%RPD RPDLimit

00

0

0

00

0

0

Qual

B


12/20/02


75

75

7575

125 0

125 0

125 0125 0

SeqNo: 85123

%RPD RPDLimit

0

000

Qual

C





Page 4 of 31

Date: 10-Feb-03

CLIENT: RSSN •}Work Order: L021 22021Project: PW-9B


i

Analyte

Magnesium

Potassium

Sodium

Vanadium


Analyte

Aluminum

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium


Analyte "

Aluminum

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

'

SampType: MS

Batch ID: R9503

Result

185.8

36.1

2240.1949

SampType: MSD

Batch ID: R9503

Result

1.15"

0.9238

524.2

1.125

189.5

39.37

2220.2141

SampType: DUP

Batch ID: R9503

Result

RSD over 20%.

0.03482

524.5

0.2328

180.4

24.23

224ND

TestCode:

TestNo:

PQL

0.50

2.00.50

0.0050

TestCode:

TestNo:

PQL

0.050

0.0050

0.50

0.100.50

2.00.50

0.0050

TestCode

TestNo

PQL

0.050

0.0050

0.50

0.10

0.50

2.00.50

0.0050

6010WJD

SW6010B

SPK value

202020

0.25

6010W_D

SW6010B

SPK value

11

201

202020

0.25

6010W_D

SW6010B

SPK value

00000000

6010W_D

Units: mg/L

SPKRefVal

180.1

26225

0

Units: mg/L

SPKRefVal

0.063

0.03213

522.3

0.2244

180.1

23.39

2250

Units: mg/L

SPKRefVal

00000000

', ANALYTICAL QC SUMMARY REPORT


%REC

28.5

50.5

-578

%REC

10989.2

9.59047

79.9

-1585.6

%REC

00000000

Prep Date:


LowLimit HighLimit

75757575

Prep Date:

Analysis Date:

125125125125

12/20/02

LowLimit HighLimit

Prep Date:


LowLimit HighLimit

00000000

00000000

Run ID' R_1CP-1_021220A

SeqNo: 85123

RPD Ref Val

0000

%RPD

0000

Run ID: R_

RPDLimit Qual

CCC

ICP-1_021220A

SeqNo: 85124

RPDRefVal

0.973

0.8893

508.5

1.073

185.8

36.1224

0.1949

%RPD

16.73.81

3.04

4.71

1.97

8.67

0.897

9.40

Run ID: R.

RPDLimit

20

20

20

20

20

20

20

20

Qual

B

ICP-1_021220A

SeqNo: 85122

RPDRefVal

0.063

0.03213

522.3

0.2244

180.1

23.39

2250

%RPD

1178.04

0.420

3.67

0.166

3.53

0.445

"0

RPDLimit

20

20202020202020

Qual

R

B





Page 5 of 31

Date: 10-Feb-03

CLIENT: RSSN 'Work Order: L0212202iProject: PW-9B

Sample ID. MB-1897

Analyte

Aluminum

Barium

Calcium >

Iron

Magnesium

Potassium ;

SodiumVanadium

Sample ID: LCS-1897 ]

^

Analyte

Aluminum

Barium '

Calcium

Iron

Magnesium

Potassium

SodiumVanadium

Sample ID: L0212146-001AMS.

Analyle

Aluminum

Barium

CalciumIron


SampType: MBLK

Batch ID: 1897

Result

0.086

NDNDNDNDND

2.15

ND

SampType: LCS

Batch ID: 1897

Result

10.9753

19.581.007

20.65

18.8524.1

02443

SampType: MS

Batch ID: 1897

Result

1.26

1.264

21.571.127

TestCode:

TestNo:

PQL

0.050

0.0050

0.50

0.100.50

2.00.50

0.0050

TestCode:

TestNo:

PQL

0.050

0.0050

0.500.10

0.50

2.00.50

0.0050

TestCode

TestNo

PQL

0.050

0.00500.500.10

6010W_T

SW6010B

SPK value

6010W_T

SW6010B

SPK value

11

201

202020

0.25

6010WJT

SW6010B

SPK value

11

201

6010WJT

Units: mg/L

SPKRefVal

Units: mg/L

SPKRefVal

0.086

00000

2.150

Units: mg/L

SPKRefVal

0.154

0.2808

1.6660.2564


%REC

%REC

91.4

97.5

97.9101103

94.2

11097.7

%REC

11198.3

99.587

Prep Date:

Analysis Date:

12/13/02

12/16/02


Prep Date:

Analysis Date:

12/13/02

12/16/02


8585858585858585

Prep Date:

Analysis Date:

115 0

115 0

115 0

115 0

115 0115 0

115 0115 0

12/13/02

12/16/02


75

75

7575

125 0

125 0

125 0125 0


SeqNo: 83816

%RPD RPDLimit Qual


SeqNo: 83817

%RPD RPDLimit

00000000

Qual

B

B


SeqNo: 83825

%RPD RPDLimit

0000

Qual

B

Qualifiers: ND - Not Detected at the Reporting Limit < C - Unspiked sample >5 times the amount spiked




Page 6 of '31

Date: 10-Feb-03

CLIENT: RSSN ,.

Work Order: L02 12202.Project: PW-9B ,:


Analyte

MagnesiumPotassium-

Sodium 'Vanadium

Sample ID: L021 21 46-001 AMSD .

'

Analyte

Aluminum

Barium

CalciumIron ,_MagnesiumPotassium

SodiumVanadium


Analyte

Aluminum

BariumCalciumIron

MagnesiumPotassium ~

SodiumVanadium


SampType: MS

Batch ID: 1897

Result

20.54 .

21.61

1040

0.2528

SampType: MSD

Batch ID: 1897

Result

1.06

1.041

21.481.10820.9421.271050

0.2562

SampType: DUP

Batch ID: 1897

Result

0.1020.09708

1.285NDNDND

10800.01557

TestCode:

TestNo:

PQL

0.502.0

0.500.0050

TestCode:

TestNo

PQL

0.050

0.00500.500.100.502.0

0.500.0050

TestCode

TestNo

PQL

0.0500.0050

0.500.100.50

2.00.50

0.0050

eoiowjr

SW6010B

SPK value

202020

0.25

6010WJT

SW6010B

SPK value

11

201

202020

0.25

6010WJT

SW6010B

SPK value

00000000

6010W_T

Units: mg/L

SPKRefVal

00

10600

Units: mg/L

SPKRefVal

0.154

0.2808

1.6660.2564

00

10600

Units: mg/L

SPKRefVal

0000000

•0


%REC

103108

-100101

%RJEC

90.676

99.185.1105106-50102

%REC

00000000

Prep Date:

Analysis Date:

12/13/02

12/16/02

LowLimit HighLimit

75757575

Prep Date:

Analysis Date:

125

125

125125

12/13/02

12/16/02

LowLimit HighLimit

Prep Date:

Analysis Date:

12/13/02

12/16/02

LowLimit HighLimit

00000000

00000000

RPDRefVal

0000

RPDRefVal

1.261.26421.571.12720.5421.611040

0.2528

RPDRefVal

0.1540.2808

1.6660.2564

00

10600

Run ID: RJCP-1

SeqNo: 83825

J)21216A

%RPD RPDLimit

0000

Run ID: RJCP-1

SeqNo: 83826

Qual

JL

J121216A

%RPD RPDLimit

17.2

19,4

0.4181.72

1.931.59

0.9571.34

Run ID: RJCP-1

SeqNo: 83820

20

20

202020202020

Qual

B

JL

J)21216A

%RPD RPDLimit

40.697.2

25.8

0

00

1.87200

0

0000000

Qual

B

B





Page 7 of 31

Date: 10~Feb-03

CLIENT: RSSN

Work Order: L0212202'

Project: PW-9B

Sample ID: MB-R9433

Analyte

AntimonyArsenic

Beryllium'Cadmium

ChromiumCobalt '

Copper

Lead

ManganeseNickel

SeleniumSilver

ThalliumZinc


Analyte

Antimony

Arsenic

BerylliumCadmium

Chromium

Cobalt

CopperLead

Manganese

Nickel

Selenium

SampType: MBLK

Batch ID: R9433

Result

;; NDND

" NDNDND

7 ND

NDNDNDNDNDND

: ND

". ND

SampType: LCS

Batch ID: R9433

Result

0.04015

0.0948

0.0678

0.0503

0.03105

0.03760.0414

0.0434

0.03755

0.03945

,' 0.1104

6020W_D

TestCode: 6020WJD Units: mg/L

TestNo: SW6020


0.00500.0050

0.0050

0.00500.0050

0.00500.0050

0.0050

0.0050

0.0050

0.0050

0.00500.0020

0.0050

TestCode: 6020WJD Units: mg/L

TestNo: SW6020


0.0050 0.05 0

0.0050 0.1 0

0.0050 0.1 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.1 0



Prep Date:

Analysis Date:' 12/18/02


Prep Date:



80.3 85 115 0

94.8 85 115 0

67.8 85 115 0

101 85 115 0

62.1 85 115 0

75.2 ' 8 5 1 1 5 0

82.8 85 115 0

86.8 85 115 0

75.1 85 115 0

78.9 85 115 0

110 85 115 0


SeqNo: 84644

%RPD RPDLimit

^

Qual

Run ID: RJCP-2MSJJ21218B

SeqNo: 84645

%RPD RPDLimit

00

0

0

0

00

0

0

00

Qual

S

S

SSS

SS





Page 8 of 31

Date: 10-Feb-03

CLIENT: RSSN :Work Order: L02 1 2202 ,Project: PW-9B


Analyte

Silver

ThalliumZinc


Analyte

Antimony

Arsenic

Beryllium

CadmiumChromium

Cobalt

CopperLead

Manganese

Nickel

SeleniumSilver

ThalliumZinc


Analyte

AntimonyArsenic

Beryllium


SampType: LCS

Batch ID: R9433

Result

0.1007

0.0487

0.01335

SampType: MS

Batch ID: R9433

Result

0.0557

0.1288

0.09445

0.06190.0475

6.0555

0.056650.05075

0.4716

0.135

0.1534

0.1086

0.05685

0.5018

SampType: MSD

Batch ID: R9433

Result

0.061150.1314

0.0943

TestCode:

TestNo:

PQL

0.0050

0.0020

0.0050

TestCode:

TeslNo:

PQL

0.0050

0.0050

0.0050

0.0050

0.0050

0.00500.0050

0.00500.0050

0.0050

0.00500.0050

0.0020

0.0050

TestCode-

TestNo

PQL

0.0050

0.00500.0050

6020WJD

SW6020

SPK value

0.1

0.05

0.05

6020WJD

SW6020

SPK value

0.05

0.1

0.10.05

0.05

0.050.05

0.050.05

0.05

0.10.1

0.050.05

6020WJD

SW6020

SPK value

0.05

0.1

0.1

6020W_D

Units: mg/L

SPKRefVal

0

00

Units: mg/L

SPKRefVal

00.00595

0000

0.009150.00505

0.41060.07985

0.00585

00.00205

04136

Units: mg/L

SPKRefVal

00.00595

0

Test Method : S W 6020-Diss

%REC

10197.4

26.7

%REC

111123

94.4

12495

11195

91.4

122110148109

_ 110176

%REC

122

12594.3

Prep Date:

Analysis Date:


12/18/02

LowLimit HighLimit

858585

Prep Date:

Analysis Date:

115115115

RPDRefVal

000

SeqNo: 84645

%RPD RPDLimit

0

0

0

Qual

S


12/18/02

LowLimit HighLimit

75

75

75

75

75

7575

7575

7575757575

Prep Date:

Analysis Date:

125125

125

125

125

125

125125

125125

125125

125125

RPDRefVal

00000000000000

SeqNo: 84648

%RPD RPDLimit

00000000000000

Qual

Jl

C


12/18/02


0.0557

0.12880.09445

SeqNo: 84649

%RPD RPDLimit

9.33 201.92 20

0.159 20

Qual





Page 9 of 31

Date: 10-Feb-03

-I

CLIENT: RSSN fWork Order: L02 12202 =Project: PW-9B

Sample ID: L0212202-003AMSD '

Analyte

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium -

Zinc


Analyte

Antimony

Arsenic

Beryllium

Cadmium ,

Chromium

Cobalt ; !

Copper '

Lead

Manganese ;

Nickel

Selenium

Silver (

Thallium

Zinc

SampType: MSD

Batch ID: R9433

Result

0.0625

0.0483

0.0564

0.0577

0.05295

0.476

0.1375

0.1576

0.1097

0.0581

0.5082

SampType: DUP

Batch ID: R9433

Result

ND0.0055

NDNDND

0.0051

0.0095

0.0051

0.4174

0.08165

0.00505

ND0.00205

0.4234

TestCode:

TestNo:

PQL

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0020

0.0050

TestCode

TestNo

PQL

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0020

0.0050

6020WJD

SW6020

SPK value

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.10.1

0.05

0.05

6020WJD

SW6020

SPK value

00000000000000

6020W_D

Units: mg/L

SPKRefVal

000

0.00915

0.00505

0.4106

0.07985

0.00585

00.00205

0.4136

Units: mg/L

SPKRefVal

0

0

0

0

0

0

0

0

000000



%REC

12596.6

11397.1

95.8

131115152110112189

%REC

00000000000000

Prep Date:


LowLimit HighLimit

Prep Date:


LowLimit HighLimit

00000000

000000

00000000000000

Run ID: R_ICP-2MSJ121218B

SeqNo: 84649

RPDRefVal

0.0619

0.0475

0.0555

0.05665

0.05075

0.4716

0.135

0.1534

0.1086

0.05685

05018

%RPD

0.965

1.67

1.61

1.84

4.24

0.939

1.87

2.73

1.05

2.17

1.26

Run ID: R_

RPDLimit

2020202020202020

20

2020

Qual

Jl

C

ICP-2MS_021218B

SeqNo: 84647

RPD Ref Val

00.00595

0000

0.00915

0.00505

0.4106

0.07985

0.00585

00.00205

0.4136

%RPD

07.86

000

2003.75

0.985

1.64

2.23

14.7

00

2.34

RPDLimit

2020202020202020202020202020

Qual

R


Jl - MS or MSD outside accepance limits. LCS acceptable, R - RPD outside accepted recovery limits



Page I Oof 31

Date: 10-Feb-03

CLIENT: RSSN .'Work Orders L0212202 !

Project: PW-9B i

Sample ID: MB-1893

Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel >

Selenium

Silver

Thallium

Zinc

Sample ID. LCS-1893

Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

SampType: MBLK

Batch ID: 1893

, Result

ND

NDNDND

NDND

NDNDND>NDNDNDNDND

SampType: LCS

Batch ID: 1893

Result

0.0575

0.1017

0.0963

0.0497

0.0512

0.0509

0.05065

0.0483

0.05205

; 0.05045

0.0995

6020WJT

TestCode: 6020WJT Units: mg/L

TestNo: SW6020


0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0020

0.0050

TestCode: 6020W_T Units: mg/L

TestNo: SW6020


0.0050 0.05 0

0.0050 0.1 0

0.0050 0.1 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.05 0

0.0050 0.1 0



Prep Date-

Analysis Date:

12/12/02

12/17/02


Prep Date:

Analysis Date:

12/12/02

12/17/02


115 85

102 85

96.3 85

99.4 85

102 85

102 85

101 85

96.6 85104 85

101 8599.5 85

115 0

115 0

115 0

115 0

115 0

115 0

115 0

115 0

115 0115 0

115 0

Run ID: RJCP-2MSJ121217D

SeqNo: 84628

%RPD RPDLimit Qual

Run ID: RJCP~2MSJ)21217D

SeqNo: 84629

%RPD RPDLimit

0

00

0

0

0

0

0

000

Qual

Qualifiers: ND - Not Detected at the Reporting Limit , C - Unspiked sample >5 times the amount spiked

Jl - MS or MSD outside accepance limits. LCS acceptable. R - RPD oulside accepted recovery limits



Page 11 of 31

Date: 10-Feb-03

CLIENT: RSSNWork Order: L0212202Project: PW-9B

Sample ID: LCS-1893

Analyte

SilverThalliumZinc


Analyte

AntimonyArsenic .

Beryllium ,

CadmiumChromium

CobaltCopper

LeadManganeseNickel

SeleniumSilver

ThalliumZinc


-

Analyte

Antimony

ArsenicBeryllium


SampType: LCS

Batch ID: 1893

Result '

0.1093

0.05080.03705

SampType: MS

Batch ID: 1893

Result

0.05710.1028

0.094650.04985,0.05225

0.051450.0522

0.048450.05315

0.05130.09965

0.11130.05065

0.0395

SampType: MSD

Batch ID: 1893

Result

0.057050.104

0.0966

TestCode:

TestNo:

PQL

0.00500.00200.0050

TestCode:

TestNo:

PQL

0.00500.0050

0.00500.00500.0050

0.00500.0050

0.00500.00500.00500.00500.0050

0.0020

0.0050

TestCode

TestNo

PQL

0.0050

0.00500.0050

6020WJT

SW6020

SPK value

0.10.05

0.05

6020W_T

SW6020

SPK value

0.05

0.10.1

0.05

0.05

0.05

0.05

0.050.05

0.050.10.1

0.05

0.05

6020WJ1

SW6020

SPK value

0.05

0.10.1

6020W_T

Units: mg/L

SPKRefVal

000

Units: mg/L

SPKRefVal

00000000000000

Units: mg/L

SPKRefVal

000


%REC

109102

74.1

%REC

114103

94.7

99.7

104103104

96.9106103

99.7

11110179

%REC

114104

96.6

Prep Date:

Analysis Date:

12/12/02

12/17/02

LowLimit HighLimit

8585

85

Prep Date.

Analysis Date:

115115

115

12/12/02

12/17/02

LowLimit HighLimit

75

75

75

75

75

7575

75

75757575

7575

Prep Date:

Analysis Date:

125

125125

125

125

125125

125

125

125 '

125125

125

125

12/12/02

12/17/02

LowLimit HighLimit

Run ID: RJCP-2MSJ»21217D

RPDRefVal

00

0

SeqNo: 84629

%RPD RPDLimit

0

0

0

Qual

S

Run ID: RJCP-2MSJI21217D

RPD Ref Val

0

00

0

0

00

0

0

0

0000

SeqNo. 84632

%RPD RPDLimit

0

00

0

0

00

0000000

Qual

Run ID: RJCP-2MSJ121217D

RPDRefVal

0.057101028

0.09465

SeqNo: 84633

%RPD RPDLimit

0.0876 20

1.16 202.04 20

Qual

Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times'the amount spiked

Jl - MS or MSD outside accepance limits. LCS acceptable. R - RPD outside accepted recovery limils



Page 12 of 31

Date: 10-Feb-03

CLIENT: RSSNWork Order: L0212202Project: PW-9B ,


Analyte

Cadmium

ChromiumCobalt

CopperLead

ManganeseNickel

SeleniumSilver

Thallium

Zinc

Sample ID: L0212189-002ADUP"

Analyte

Antimony

Arsenic

Beryllium

CadmiumChromium

Cobalt

Copper •

Lead

Manganese

Nickel '

Selenium

Silver <

ThalliumZinc

/

SampType: MSD

Batch ID: 1893

Result

0.0511

0.05255

0.05245

0.075

0.052050.05385

0.05230.101

0.11310.0524

0.03845

SampType: DTJP

Batch ID: 1893

Result

NDNDNDNDNDNDNDNDNDNDNDNDNDND

TestCode:

TestNo:

PQL

0.0050

0.0050

0.0050

0.00500.0050

0.00500.0050

0.00500.0050

0.0020

0.0050

TestCode-

TestNo

PQL

0.0050

0.00500.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0020

0.0050

6020WJ"

SW6020

SPK value

0.05

0.05

0.05

0.05

0.050.05

0.05

0.10.1

0.05

0.05

6020WJT

SW6020

SPK value

00

00

0

0

0

0000000

6020WJT

Units: mg/L

SPKRefVal

00000000000

Units: mg/L

SPKRefVal

00000000000000



%REC

102" 105

105150104108105101113105

76.9

%REC

00000000000000

Prep Date:

Analysis Date;

12/12/02

12/17/02

LowLimit HighLimit

Prep Date:

Analysis Date:

12/12/02

12/17/02

LowLimit HighLimit

0

0

0

00000000000

00000000000000

Run ID: R_ICP-2MSJ)21217D

SeqNo: 84633

RPD Ref Val

0.04985

0.05225

0.05145

0.0522

0.04845

0.053150.0513

0.09965

0.1113

0.05065

0.0395

%RPD

2.48

0.573

1.92

35.87.16

1.311.93

1.401.60

3.40

2.69

Run ID: R_

RPDLimit

2020202020202020

20

20

20

Qual

R

ICP-2MSJ)21217D

SeqNo: 84631

RPDRefVal

0

0

000000000000

%RPD

00000000000000

RPDLimit

20

20

20

202020

20

202020

20202020

Qual





Page 13 of 31

Date: 10-Feb-03


Project: PW-9B 8260 W



Sample ID: BLANK 021221 A

Analyte ,

SampType:

Batch ID:

MBLK

R9734

Result

TestCode

TestNo

PQL

8260_W

SW8260B

SPK value

Units: u.g/L

SPKRefVal

Prep Date:



Run ID:

SeqNo:

LJVOAMS-2 J)21 224A

87511

%RPD RPDLimit Qual

AcetoneBenzeneBromobenzeneBromochloromethaneBromodichlorome thane

BromoformBromomethane

2-Butanonen-Butylbenzenesec-Butylbenzene

tert-ButylbenzeneCarbon disulfideCarbon tefracMoride ;ChlorobenzeneChloroethane t

2-Chloroethyl vinyl etherChloroformChloromethane2-Chloro toluene4-Chloro tolueneDibromochloromethane1 ,2-Dibromo-3-chloropropane

1,2-Dibromoethane

Dibromomethane

1,2-Dichlorobenzene -1 ,3-Dichlorobenzene


Dichlorodifluoromethane1 , 1 -Dichloroethane1 ,2-DicMoroethane

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND>roNDND

(NDNDNDND

NDNDNDNDNDND

255.05.05.05.05.05.0255.05.05.05.05.05.05.05.05.05.05.05.0

,5.0

5.05.05.05.05.05.05.05.05.0

Qualifiers: ND - Not Detected at the Reporting Limit ' C - Unspiked sample >5 times the amount spiked




Page 14 of 31

Date: 10-Feb-03

CLIENT: RSSN iWork Order: L0212202 rProject: PW-9B 8260 W



Sample ID: BLANK 021221A

Analyte

1 ,1 -Dichloroethenecis-1 ,2-Dichloroethene

trans-1 ,2-Dichloroethene *1 ,2-Dichloropropane

1 ,3 -Dichloropropane2,2-Dichloropropane



trans-1, 3-Dichloropropene

Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethaneIsopropylbenzene

p-Isopropyltoluene

Methylene chloride4-Methyl-2-pentanone


Naphthalenen-Propylbenzene

Styrene1 , 1 , 1 ,2-Tetrachloroethane


Tetrachloroethene

Toluene -1 ,2,3-Trichlorobenzene


1,1,1 -Trichloroethane1,1,2-Trichloroethane

Trichloroethene

SampType: MBLK

Batch ID: R9734

Result

ND

ND

ND

ND

ND

NDND '

ND

ND

ND

ND

ND

NDND

ND

NDND

ND

ND

ND

ND

ND

ND

ND

ND

NDND

ND

ND

ND

TestCode: 8260_W Units: ug/L Prep Date: Run ID' L_VOAMS-2 J)21 224 A

TestNo: SW8260B Analysis Date: 12/24/03 SeqNo: 87511

PQL SPK value SPKRefVal %REC LowLimit HighLimit RPDRefVal %RPD RPDLimit Qual

5.05.0

5.0

5.0

5.0

5.05.0

5.0

5.0

5.0

5.0

25

5.05.0

5.0

5.0

25

5.010

5.0

5.0

5.0

5.0

5.05.0

5.0

5.05.0

5.0

5.0

Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked^




Page 15 of 31

Date: 10-Feb-03

CLIENT: RSSN 'Work Order: L02 12202;Project: PW-9B

Sample ID; BLANK 021221 A

Analyte





Vinyl acetate

Vinyl chloride

o-Xy)ene

m,p-Xylene


Surr: Toluene-d8

SUIT: 4-Bromofluorobenzene

Sample ID: VstdOSO 021223A '

Analyte

Acetone :

Benzene

Bromobenzene

Bromochloromethane

Bromodichloromethane ;'

Bromoform

Bromomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide


Chlorobenzene

t "

>

SampType. MBLK

Batch ID: R9734

Result

ND

NDNDNDNDNDNDND

46.22

48.58

49.43

SampType: LCS

Batch ID: R9734

Result

42.44

64.57

' 67.76

62.36

57.04

47.88

65.83

46.04

65.62

68.44

67.19

59.18

63.51

63.91

TestCode:

TestNo:

PQL

5.0

5.0

5.05.05.05.05.010

0.50

0.50

0.50

TestCode

TestNo

PQL

25

5.05.0

5.05.0

5.0

5.0255.05.05.05.05.05.0

Qualifiers: ND - Not Detected at the Reporting Limit

8260_W

SW8260B

SPK value

5050

50

8260_W

SW8260B

SPK value

50

5050

50

50

505050505050505050

8260_W

Units: ftg/L



Prep Date: Run ID: L_VOAMS-2J)21224A


SPK Ref Val

000

Units: ug/L

%REC

92.4

97.2

98.9

LowLimit

80.2

75.5

71.7

HighLimit

106105120

RPDRefVal

000

Prep Date:


SPKRefVal

00000000000000

%REC

84.9

129136125

114

95.8

13292.1

131137134118127128

LowLimit

707070

70

70

7070

70

707070

707080

C - Unspiked sample >5 times the amount spiked

HighLimit

130

130130

130130130130130130130130130130120

B

RPD Ref Val

00

0

00000000000

- Analyte detectec

SeqNo: 87511

%RPD RPDLimit

000

Qual


SeqNo: 87514

%RPD RPDLimit

000 .

00000000000

Qual

LI

LI

LILILI

LI




Page 16 of 31

Date: 10-Feb-03

CLD2NT: RSSNWork Order: L02 12202 •Project: PW-9B -; 8260_W

Sample ID: VstdOSO 021223A SampType: LCS

Batch ID: R9734 '

Analyte

Chloroethane

2-CWoroethyl vinyl ether

Chloroform

Chloromethane

2-Chlorotoluene

4-Chlorotoluene



1 ,2-Dibromoethane <

Dibromomethane



1 ,4-Dichldrobenzene


1,1-Dichloroethane

1 ,2-DichlOTOethane

1,1-Dichloroethene

cis- 1 ,2-Dichloroethene




2,2-Dichloropropane




Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

Isopropylbenzene

Result

63.28

98.16

60.97

52.43

63.71

64.2

55.53

35.11

52.15

52.69

52.61

59.97

58.62

54.78

58.72

4967.26

67.07

67.98

59.1

49.47

63.53

64.3

57.9

51.3

60.19

35.43

41.93

72.93

67.7

TestCode:

TestNo

PQL

5.05.05.05.05.05.05.05.05.05.05.05.05.05.0

5.05.05.05.05.05.05.05.05.05.05.05.05.0255.05.0

8260_W Units: ug/L

SW8260B

SPK value SPKRefVal

505050505050505050505050505050505050

50

5050505050505050505050

000000000000000000000000000000



Prep Date:



SeqNo: 87514


127196122105127128111

70.2

10410510512011711011798

135134136118

98.9

127129116103120

70.9

83.9

146135

707080707070707070707070707070707070707070707070707070707070

130130120130130130130130130130130130130130130130130130130130130130130130130130130130130130

000000000000000000000000000000

%RPD RPDLimit

000000000000000000000000000000

Qual

LILI

LILILI

LILI





Page 17 of 31

Date: 10-Feb-03


Project: PW-9B 8260_W

Sample ID: VstdOSO 021 223 A , SampType: LCS

Batch ID: R9734

Analyte

p-Isopropyltoluene

Methylene chloride



Naphthalene

n-Propylbenzene

Styrene



Tetrachloroethene

Toluene


1 ,2,4-Trichl orobenzene



Trichloroethene





Vinyl acetate

Vinyl chloride

o-Xylene

m,p-Xylene

Surr: Dibromofluoromethane -

Surr: Toluene-d8

Surr: 4jBromofluorobenzene

Result

66.71

62.04

36.06

44.48

43.64

64.52

59.53

61.35

47.32

64.5

65.76

47.9

22.37

62.22

52.14-

66.76

62.02

48.45

62.02

64.34

80.59

55.64

59.22

122.4

45.86

48.55

47.77


TestNo: SW8260B


5.05.0255.010

5.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.010

0.50

0.50

0.50

5050505050505050505050505050505050505050505050

100505050

000000000000000000000000000



Prep Date:


Run ID: L_VOAMS-2 J)21 224A

SeqNo: 87514


133124

72.1

8987.3

129119123

94.6

129132

95.8

44.7

124104134124

96.9

124

129

161111118122

91.7

97.1

95.5

707070707070707070707070707070707070707070707070

80.2

75.5

71.7

130130130130130130130130130130130130130130130130130130130130

'130

130130130'l06

105120

00000,0000000000000000000000

%RPD RPDLimit Qual

000000000000000000000000000

LI

LI

L2

LI

LI





Page 18 of 31

Date: 10-Feb-03

CLIENT: RSSNWork Order: L0212202-Project: PW-9B 8260 W



Sample ID: L0212348-001A M SampType: MS

Batch ID: R9734

Analyte Result

Acetone > '

Benzene .Bromoben/rene

Bromochkiromethane


Bromoforrn

Bromomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide


Chlorobenzene

Chloroethane


Chloroform

Chloromethane

2-Chlorotoluene

4-Chloro toluene

Dibromochloromethane1 ,2-Dibromo-3-ehloropropane

1 ,2-Dibromoethane

Dibromomethane


1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene


1,1-Dichloroethane1,2-Dichloroethane

ND

62.06

53.94

51.6850.65

29.9363.21

ND

36.03

55.1758.33

58.64

64.0654.67

60.54

62.1157.68

53.68

58.6854.74

41.59ND

37.92

41.7

19.834.24

31.02

57.91

56.81

41.01

TestCode: 8260_W Units: u-g/L

TestNo- SW8260B


25

5.0

5.0

5.05.0

5.05.0

25

5.05.0

5.0

5.0

5.05.0

5.0

5.05.0

5.0

5.05.0

5.0

5.05.0

5.0

5.0

5.05.0

5.0

5.0

5.0

50

50

50

5050

5050

50

50

50

50

50

5050

50

5050

5050

50

50

50

50

50

50

5050

50

5050

0

0

0

000

0

00

0

0

0

0

00

0

00

0

0

0

0

0

0

0

0

0

0

0

0

Prep.Date: Run ID: L_VOAMS-2J)21224A

Analysis Date: 12/25/03 SeqNo: 87512

%REC LowLimit HighLimit RPDRefVal %RPD RPDLimit Qual

0

124

108103

10159.9

1260

72.1

110117

117

128

109121

124

115

107117

109

83.2

075.8

83.4

39.6

68.562

116114

82

70

70

70

70

7070

70

70

70

70

70

70

7070

70

7070

7070

70

70

7070

70

7070

70

7070

70

130

130

130

130130

130130

130

130

130

130

130

130130

130130

130130

130

130

130

130

130

130

130

130

130

130

130

130

0

0

0

00

00

00

0

0

0

0

00

0

00

00

0

0

0

0

0

00

0

0

0

0

00

0

00

00

0

0

0

0

00

0

00

00

0

0

00

0

0

00

00

0

M2

M2

M2

M2

M2

M2M2





Page 19 of 31

Date: 10-Feb-03

CLIENT: RSSN IWork Order: L0212202'Project: PW-9B

Sample ID: L0212348-001A M

Analyte

1 ,1 -Dichloroethene





2,2-Dichloropropane

1 ,1 -Dichloropropene



Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

Isopropylbenzene

p-Isopropyltoluene

Methylene chloride



Naphthalene

n-Propylbenzene

Styrene


1 ,1 ,2,2-Tetrachloroethane

Tetrachloroethene

Toluene





Trichloroethene


SampType: MS

Batch ID: R9734

Result

64.6

60.89

64.82

53.5

38.32

56.3

63.81

47.53

38.99

54.91

NDND

66.97

67.32

46.81

55.45

25.55

35.21

ND62.22

47.12

50.91

28.93

60.08

61.15

NDND

62.44

39.66

63.54

TestCode:

TestNo

PQL

5.05.05.05.05.05.05.05.05.05.05.0255.05.05.05.0255.010

5.05.05.05.05.05.05.05.05.05.05.0

8260 JW

SW8260B

SPK value

50505050505050505050

50505050505050505050

50

50

50

50

50

50

50505050

8260_W

Units: ug/L

SPKRefVal

000000000000000000000000000000


%REC

129122130107

76.6

113128

95.1

78110

0

0134

13593.6

11151.1

70.4

0124

94.2

102

57.9

120

122

0

0

12579.3

127

Prep Date:

Analysis Date:


12/25/03

LowLimit HighLimit

70707070707070707070707070707070707070707070

70

70707070707070

130130130130130130130130130130130130130130130130130130130130130130130130130130130130130130

RPD Ref Val

000000000000000000000000000000

SeqNo: 87512

%RPD RPDLimit

0 "

00000000000000000000000000000

Qual

M2M2MlMl

M2

M2

M2

M2M2

Qualifiers: ND - Not De'tected at the Reporting Limit C - Unspiked sample >5 times the amount spiked

Jl - MS or MSD outside accepance limits. LCS acceptable. R - RPD outside accepted recoveiy limits



Page 20 of 31

Date: 10-Feb-03

CLIENT: RSSN :

Work Order: L0212202Project: PW-9B 8260 W



Sample ID: L0212348-001AM

Analyte


1 ,2,3-Trichloropropane1 ,2,4-Trimethylbenzene

1 ,3,5-Trirrtethylbenzene

Vinyl acetate


m,p-Xylene


Sun-: Toluene-d8Surr: 4^Bromofluorobenzene

Sample ID: L0212348-001AM

Analyte

Acetone

Benzene

Bromobenzene

Bromochloromethane 'i


Bromoform

Bromomethane

2-Butanone

n-Butylbenzene :

sec-Butylbenzenetert-Butylbenzene

Carbon disulfide


Chlorobenzene

SampType: MS

Batch ID: R9734

Result

65.8

31.15

45.57

53.5352.42

57.64

51.1

108.845.27

48.73

47.27

SampType: MSD

Batch ID: R9734

Result

ND59.78

63.88

52.15

49.06

38.33

60.23

26.54"

52.54

68.48

67.3

56.4661.33

55.47

TestCode:

TeslNo:

PQL

5.05.05.05.05.05.05.010

0.50

0.500.50

TestCode

TestNo

PQL

255,05.05.05.05.05.0255.05.05.05.05.05.0

8260_W

SW8260B

SPK value

50505050505050

100505050

8260_W

SW8260B

SPK value

5050505050505050505050

- 50

5050

Units: ug/L Prep Date:


SPKRefVal

00000000000

Units: (ig/L

%REC

13262.3

91.1107-105115102109

90.5

97.5

94.5

LowLimit

7070707070707070

80.2

75.5

71.7

HighLimit

130130130130130130130130106105

120

RPD Ref Val

00000000000

Prep Date:


SPKRefVal

00000000000000

%REC

0120128104

98.176.7

120

53.1

105137135113123111

LowLimit

70

7070

70

70707070707070707070

HighLimit

130130130130130130130130130130130130130130

RPDRefVal

062.0653.94

51.68

50.6529.93

63.21

036.03

55.17

58.3358.64

64.0654.67


SeqNo: 87512

%RPD

0

0

0

00

00

0000

Run ID: L_

RPDLimit Qual

MlM2

VOAMS-2J)21224A

SeqNo: 87513

%RPD

03.74

16.9

0.905

3.1924.6

4.83

20037.3

21.514.3

3.79

4.35

1.45

RPDLimit

252525252525252525252525

25

25

Qual

R2

R2

RlRl


i Jl - MS or MSD outside accepance limits. LCS acceptable. R - RPD outside accepted recovery limits



Page 21 of 31

Date: 10-Feb-03

CLIENT: RSSN .Work Order: L02 12202Project: PW-9B 8260_W

Sample ID: L021 2348-001 A M SampType: MSD

Batch ID: R9734

Analyte '

Chloroethane


Chloroform

Chlorome thane

2-Chloro toluene4-Chlorotoluene

Dibromochloromethane t


1 ,2-Dibromoethane

Dibromomethane1 ,2-Dichlorobenzene


1 ,4-DichlorobenzeneDichlorodifluoromethane

1 , 1 -Dichloroethane

1 ,2-Dichloroethane

1,1 -Dichloroethene

cis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene

1 ,2-Dichloropropane1,3-Dichloropropane i

2,2-Dichloropropane


cis-1 ,3-Dichloropropenetrans-1 ,3-Dichloropropene

Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethaneIsopropylbenzene

Result

58.13

31

54.3647.44

63.5960.85

44.12

19.0141.55

42.45

39.4649.15

48.2755.77

54.74

40.04

62.51

59.6763.21

51.72

40.38

53.21

60.74

46.85

39.5

53.96

11.73

25.58

65.47

71.11

TestCode: 8260_W Units' ug/L

TestNo: SW8260B


5.0

5.0

5.0

5.0

5.0

5.05.0

5.0

5.05.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.05.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

25

5.0

5,0

50

50

50

50

5050

50

5050

50

5050

5050

50

50

50

5050

5050

50

50

50

50

50

50

50

50

50

0

0

00

0

0

0

0

00

00

0

0

0

0

0

0

0

0

00

0

0

0

0

0

00

0



Prep Date.



SeqNo: 87513


116

62

109

94.9

127122

88.2

3883.1

84.9

78.998.3

96.5

112

109

80.1

125

119126

103

80.8

106121

93.7

79

* 108

23.551.2

131

142

70

70

70

70

7070

70

70

70

70

70

7070

70

70

7070

7070

70

70

70

70

7070

70

70

70

7070

130

130

130

130

130

130130

130130

130

130130

130

130

130

130

130

130130

130130

130

130130

130

130

'l30

130130

130

60.54

62.11

57.68

53.68

58.6854.74

41.590

37.9241.7

19.834.24

31.02

57.91

56.81

41.0164.6

60.8964.82

53.538.32

56.3

63.81

47.53

38.99

54.91

0

0

66.9767.32

%RPD RPDLimit

4.06

66.8

5.93

12.3

8.03

10.65.90

2009.14

1.78

66.4

35.843.5

, 3.763.71

2.39

3.29

2022.52

3.385.24

5.64

4.93

1.44

. 1.301.75

200

2002.27

5.48

25

25

25

25

2525

2525

25

25

2525

25

25

25

25

25

2525

2525

25

2525

25

25

25

2525

25

Qual

R2

R2

R2

R2

Rl

Rl




B - Analyte detected in Ihe associated Method Blank

Page 22 of 31

Date: 10-Feb-03

(-CLIENT: RSSN

Work Order: L0212202''Project: PW-9B 8260_W

Sample ID: L0212348-001A M ' SampType: MSD

Batch ID: R9734

Analyte

p-Isopropyltoluene

Methylene chloride



Naphthalene

n-Propylbenzene

Styrene '


1 ,1 ,2,2-Teirachloroethane

Tetrachloroethene

Toluene

1 ,2,3-Tricalorobenzene


1,1,1-Tricnloroelhane '


Trichloroethene





Vinyl acetate

Vinyl chloride

o-Xylene

m,p-Xylene

Surr: Dibromofluoromethane ,

Sun" Toluene-d8


Result

60.87

53.73

27.59

36.13

ND67.77

50.49

52.09

43.87

59.5

59.33

ND62

59.64

41.11*

60.77

63.29

44.21

55.26

62.08

51.49

54.33

52.27

108.6

44.65

48.44

45.39


TestNo: SW8260B


5.05.025

5.010

5.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.010

0.50

0.50

0.50

505050505050SO50505050505050505050505050505050

100505050

000000000000000000000000000

ANALYTICAL QC SUMMARY


Prep Date:


REPORT


SeqNo: 87513


122107

55.2

72.3

0136101104

87.7

119119

012.4

11982.2

122127

88.4

111124103109105109

89.3

96.9

90.8

707070707070707070

• 70

7070707070707070707070707070

80.2

75.5

71.7

130130130130130130130130130130130130130130130130130130130130130130130130106105120

46.81

55.45

25.55

35.21

062.22

47.12

50.91

28.93

60.08

61.15

00

62.44

39.66

63.54

65.8

31.15

45.57

53.53

52.42

57.64

51.1

108.8

000

%RPD RPDLimit

26.1

3.15

7.68

2.58

08.54

6.91

2.29

41.0

0.970

3.02

02004.59

3.59

4.46

3.89

34.7

19.2

14.8

1.79

5.91

2.26

0.129

000

252525252525252525252525252525252525252525252525000

Qual

R2

R2Rl

R2R2





Page 23 of 31

Date: 10-Feb-03

CLIENT: RSSN r.Work Order: L0212202CProject: PW-9B

Sample ID: MB-R9396

1

Analyte ;

Alkalinity! Bicarbonate (As CaC03)Alkalinity] Carbonate (As CaCO3)Hydroxide! (As CaCO3)Alkalinity, Total (As CaCO3)


>i

Analyte ,

Alkalinity,' Total (As CaCO3)

Sample ID; LCSD-R9396

:Analyte


Sample ID: L0212202-004CDUF

Analyte

Alkalinity, Bicarbonate (As CaC03)Alkalinity, Carbonate (As CaCO3)Hydroxide (As CaC03)Alkalinity, Total (As CaCO3)


SampType: MBLK

Batch ID: R9396

Result

NDNDNDND

SampType: LCS

Batch ID: R9396

Result

123

SampType: LCSD

Batch ID: R9396

Result

123

SampType: DUP

Batch ID: R9396

Result

238NDND238

ALK_W


TestNo: M2320 B


5.05.05.025

TestCode. ALK_W Units: mg/L

TestNo. M2320 B


25 125 0

TestCode. ALK_W Units: mg/L

TestNo: M2320 B


25 125 0


TestNo: M2320 B

PQL SPK value SPK Ref Val

5.0 0 05.0 0 05.0 0 025 0 0

Test Method: SM2320 B

Prep Date:



Prep Date:



98.4 80 120 0

Prep Date:



98.4 80 120 0

Prep Date:



0 0 0 2 5 40 0 0 00 0 0 00 0 0 2 5 4


SeqNo: 83850

%RPD RPDLimit Qual

Run ID: L_ATITR-1 JJ21213B

SeqNo: 83849

%RPD RPDLimit Qual

0

Run ID: L_ATITR-1 J121213B

SeqNo: 83852

%RPD RPDLimit Qual

0

Run ID: L_ATITR-1J)21213B

SeqNo: 83851

%RPD RPDLimit Qual

6.50 100 100 10

6.50 10


Jl - MS or M'SD outside accepance limits. LCS acceptable. R - RPD outside accepted recovery limits



Page 24 of 31

Date: 10-Feb-03


RSSN :

L0212202"'

PW-9B COD


Test Method: SM5520 D

Sample ID: MB-R9434

Analyte

SampType:' MBLK

Batch ID: R9434

Result

TestCode: COD

TestNo: M5220 C

PQL SPK value

Units: mg/L

SPKRefVal

Prep Date:



Run ID: L_SPEC-1_021218A

SeqNo: 84239

%RPD RPDLimit Qual

Chemical Oxygen Demand ND 10

Sample ID; LCS-R9434

Analyte '

SampType: LCS

Batch ID: R9434

Result


TestNo: M5220 C


Prep Date:




SeqNo: 84238

%RPD RPDLimit Qual

Chemical Oxygen Demand 515 10 500 103 80 120

Sample ID' LCSD-R9434

Analyte

SampType: LCSD

^ Batch ID: R9434

iResult


TestNo: M5220 C


Prep Date:




SeqNo: 84240

%RPD RPDLimit Qual

Chemical Oxygen Demand 510 10 500 102 80 120 515 0.976 15


Analyte

SampType: MS

BalchID: R9434

Result


TestNo: M5220 C


Prep Date:




SeqNo: 84241

%RPD RPDLimit Qual

Chemical Oxygen Demand 531 10 478 44 102 70 130

Sample ID:

i

Analyte

L0212148-004AMSB

*

SampType:

Batch ID:

MSD

R9434

Result

TestCode

TestNo

PQL

COD

M5220 C

SPK value

Units: mg/L

SPKRefVal

Prep Date:

Analysis Date:


12/18/02


SeqNo: 84242

%RPD RPDLimit Qual

Chemical Oxygen Demand 523 10 478 44 100 70 130 531 1.52 25

Qualifier's: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount'spiked

Jl - MS or MSD outside accepance limits. LCS acceptable R - RPD outside accepted recovery limits



Page 25 of 31

Date: 10-Feb-03


RSSN -L02 12202PW-9B

AN4/\l~r:

hg_7470_d



Sample ID: MB-1911

Analyte

SampType: MBLK

Batch ID: 1911

Result


TestNo: SW7470


Prep Date: 12/16/02



Run ID: R_HG-1_021216A

SeqNo: 83709

%RPD RPDLimit Qual

Meicury ND 0.00020

Sample ID. LCS-1911

Analyte

SampType: LCS

Batch ID: 1911

Result


TestNo: SW7470


Prep Date: 12/16/02




SeqNo: 83708

%RPD RPDLimit Qual

Mercury 0.00507 0.00020 0.005 101 85 115

Sample ID:

Analyte

L021 2202-003 AMSf1

-

SampType:

Batch ID:

MS

1911

Result

TestCode:

TestNo:

PQL

HG_7470_D

SW7470

SPK value

Units: mg/L

SPKRefVal

Prep Date:

Analysis Date:

12/16/02

12/16/02



SeqNo: 83691

%RPD RPDLimit Qual

Mercury 0.00484 0.00020 0.005 96.8 85 115


*Analyte

SampType: MSD

Batch ID: 1911

Result

TestCode: HG_7470_D Units: mg/L

TestNo: SW7470


Prep Date: 12/16/02




SeqNo: 83692

%RPD RPDLimit Qual

Meicury 0.00495 0.00020 0.005 99 0.00484 2.25 20



J - This concentration is considered an estimate due to LCS .failure.


Page 26 of 31

Date: 10-Feb-03


RSSN ,'L02122021

PW-9B HG 7470 T



Sample ID: MB-1913

Analyte

._ SampType: MBLK

Batch ID: 1913I

Result

TestCode: hg_7470_t Units: mg/L

TestNo: SW7470


Prep Date: 12/16/02



Run ID- R_HG-1_021216C

SeqNo: 83750

%RPD RPDLimit Qual

Mercury ND 0.00020

Sample ID: LCS-1913

Analyte

SampType: LCS

p Batch ID: 1913

Result

TestCode' hg_7470_t Units. mg/L

TestNo: SW7470


Prep Date: 12/16/02



Run ID: R_HG-1_021216C

SeqNo: 83749

%RPD RPDLimit Qual

Mercury 0.00484 0.00020 0.005 85 115


Analyte

SampType: MS

Batch ID: 1913

Result

TestCode: HG_7470_T Unite: mg/L

TestNo: SW7470


Prep Date: 12/16/02

Analysis Date. 12/16/02


Run ID: R_HG-1_02121<SC

SeqNo: 83731

%RPD RPDLimit Qual

Mercury 0.00375 0.00020 0.005 75 85 115

Sample ID:

Analyte

L0212202-002AMSD SampType:

Batch ID:

MSD

1913

Result

TestCode:

TestNo:

PQL

HG_7470_T

SW7470

SPK value

Units: mg/L

SPKRefVal

Prep Date:

Analysis Date:

12/16/02

12/16/02


Run ID: R_HG-1_021216C

SeqNo: 83732

%RPD RPDLimit Qual

Mercury 0.00391 0,00020 0.005 78.2 0.00375 4.18 20


Jl - MS or MjSD outside accepance limits. LCS acceptable. R - RPD outside accepted recovery limits



Page 27 of 31

Date: 10-Feb-03

CLIENT: RSSN jWork Order: L0212202,Project: PW-9B '-. NH3-N W


Test Method: SM4500-NH3 C

Sample ID: MB-R9421

Analyte

SampType: MBLK

Batch ID: R9421

Result

TestCode. NH3-N_W Units: mg/L

TestNo: M4500-NH3 C


Prep Date:




SeqNo: 84095

%RPD RPDLimit Qua!

Ammonia, as N ND 0.30


Analyte

: SampType: LCS1 Batch ID: R9421

Result


TestNo: M4500-NH3 C


Prep Date:




SeqNo: 84094

%RPD RPDLimit Qual

Ammonia, as N 0.9 030 90 839 117


Analyte

SampType: LCSD

Batch ID: R9421

; Result


TestNo: M4500-NH3 C


Prep Date:




SeqNo: 84096

%RPD RPDLimit Qual

Ammonia, as N 1.01 0.30 101 83.9 117 09 11.5 25

Sample ID: L0212181-002AMS '

Analyte

SampType: MS

Batch ID: R9421

Result


TestNo: M4500-NH3 C


Prep Date:


%REC LowLimit HighLimit • RPD Ref Val


SeqNo: 84097

%RPD RPDLimit Qual

Ammonia, as N 1.01 0.30 101 76.4 124

Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked\




Page 28 of 31

Date: 10-Feb-03


RSSNL0212202'PW-9B " PH W



Sample ID- LCS-R9371

Analyte

SampType:

Batch ID: f

.

LCS

R9371

Result

TestCode

TestNo

PQL

PH_W

E150.1

SPK value

Units: pH units

SPKRefVal %REC

Prep Date:



Run ID:

SeqNo:

L_AT1TR-1_021212A

83443

%RPD RPDLimit Qual

pH 6.98 1.00 99.7 99.3 100.7

Sample ID: LCS-R9371 SampType: LCSD

Analyte

Batch ID: R9371

Result

TestCode: PH_W Units: pH units Prep Date:

TestNo: E150.1




Run ID: L_ATITR-1_021212A

SeqNo: 83444

%RPD RPDLimit Qual

pH 1.00 99.7 99.3 1007

Sample ID: L0212186-001ADXJP

Ânalyte

SampType:

Batch ID:

DUP

R9371

Result

TestCode:

TestNo

PQL

PH_W

E150.1

SPK value

Units: pH units

SPKRefVal %REC

Prep Date:



Run ID:

SeqNo:

L_ATITR-1_021212A

83616

%RPD RPDLimit Qual

pH 1.00 7.71 1.16





Page 29 of 31

Date: 10-Feb-03


RSSN ;,L0212202"

PW-9B SULF W


Test Method: SM4500-S D

Sample ID: MB-R9393

Analyte

SampType: MBLK

'• Batch ID: R9393

Result

TestCode: SULF_W Units: mg/L

TestNo: M4500-S D


Prep Date:




SeqNo: 83760

%RPD RPDLimit Qual

Sulfide ND 0.030


Analyte

SampType: LCS

Batch ID: R9393

Result


TestNo: M4500-S »


Prep Date:



Run ID: I,_SPEC-2_021213D

SeqNo: 83759

%RPD RPDLimit Qual

Sulfide 0.108 0.030 0.107 101 80 120


Analyte

SampType: LCSD

Batch ID: R9393

; . Result


TestNo: M4500-S D


Prep Date:




SeqNo. 83761

%RPD RPDLimit Qual

Sulfide 0.113 0030 0.107 106 80 120 0.108 4.52 25

Sample ID: L021 2203-006 AMS •

'

Analyte

SampType: MS

Batch ID: R9393

Result


TestNo: M4500-S D


Prep Date:




SeqNo: 83762

%RPD RPDLimit Qual

Sulfide 0.107 0.030 0.107 100 70 130

Sample ID: L0212203-006AMSD SampType: MSD

i

Analyte

Batch ID: R9393

Result


TestNo: M4500-S D


Prep Date:


%REC LowLimit HighLimit RPD Ref Val


SeqNo: 83763

%RPD RPDLimit Qual

Sulfide ' 0.106 0.030 0107 99.1 70 130 0.107 0.939 25





Page 30 of 31

Date: JO-Feb-03


RSSN l

L02122021'PW-9B - TDS W


Test Method: SM2540 C

Sample ID: MB-R9369

Analyte i

:" SampType: MBLK

Batch ID: R9369

Result

TestCode: TDSJW Units: mg/L

TestNo: E160.1


Prep Date:



Run ID: L_WC_021213A

SeqNo: 83424

%RPD RPDLimit Qual

Total Dissolved Solids ND 15.0

Sample ID': LCS-R9369

Analyte

SampType: LCS

Batch ID: R9369

Result

TestCode: TDSJW

TestNo: E160.1

PQL SPK value

Units: mg/L

SPKRefVal

Prep Date:



Run ID: LJWC_021213A

SeqNo: 83423

%RPD RPDLimit Qual

Total Dissolved Solids 950 15.0 1000 95 80 120

Sample ID:

Analyte

L0212032-001DDUF,\'<!

SampType:

Batch ID:

DUP

R9369

Result

TestCode

TestNo

PQL

TDS_W

E160.1

SPK value

Units: mg/L

SPKRefVal

Prep Date:



Run ID: L_WC_021213A

SeqNo: 83425

%RPD RPDLimit Qual

Total Dissolved Solids 329 15.0 272 19.0 25

Qualifiers: ' ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked




Page 31 of 31

Date: 10-Feb-03

Date post:	24-Apr-2018
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