"tar744 Heartland TrailP.O. I3ox8923Madison, Wl 53708-8923Phono: (608)831-4444FAX: (608)831-3334

Wisconsin Department of Natural Resources

112J' N. Military Avenue

P.O. Box 10448

Green Bay, Wl 54307-0448

LETTER OF TRANSMITTAL

DATE: 25 June 2004 JOB NO.: 3453.11

ATTENTION: Ms. Linda Vogen

RE: Lemberger Landfill Superfund Site

Whitelaw, Wisconsin

WE <\RE SENDING YOU m Attached D Under separate cover via. the following items:

D Contract Documents D Purchase Ordern C ertificates of Insurance D Copy of letter

D Waiver of LienD Plans

D Laboratory Analysis ReportD

COPIES

2

DATE

6-25-04

NO.

-

DESCRIPTION

May 2004 Discharge Monitoring Report

THESE ARE TRANSMITTED as checked below:

D FOR APPROVAL

D APPROVED AS NOTED

D APPROVED AS SUBMITTED

D SIGN AND RETURN H FOR YOUR USE

D FOR REVIEW AND COMMENT D AS REQUESTED

D RETURNED FOR CORRECTIONS D

REMARKS:

Please contact me at 608-662-5228 if you have questions regarding the enclosed DMR.

COPY TO Mr. Doug Clark - Foley & Lardner

Mr. Darn/I Owens - USEPA

Mr. Mark Brooks - RMT/Site Operator SIGNED

Eric Gredell, P.E.Project Manager

Wastewater Discharge Monitoring Long Report For DNR Use Only

Facility Mame: LEMBERGER LANDFILL SUPERFUND SITEContact Address: 744 Heartland Trail

Madison, WI 53717-8923Facility Contact: Eric: Gredell, Senior Consulting EngineerPhone Number: (603)662-5228P.eporting Period: 05/01/2004 - 05/3 1/2004Form Due Date: 06/15/2004Permit Number: 0049573

Sample Point 701 701Description Influent Influent I

I

Parameter 561 117Description 1,1,1-Trichloro- Chloroethane

ethane Dich

Units i ug/L ug/LSample Type Grab Grab

Frequency Monthly Monthly NFootnotes: 2 2

Sample Results Day 1234 30 ^0.975

Date Received:DOC: 123143FIN: 11188FID: 436016790Region: NortheastPermit Drafter: David HantzReviewer: David GerdmLinOffice: Mishicot

701 701 001nfluent Influent Prior to Branch

Cr556 570 2111,1- 1,2-Dichloroethan Flow Rate

loroethaneug/L ug/L MGDGrab Grab Continuouslonthly Monthly Daily

2 2 1,2

0.30219O.3O79(e>O. J0796

7,^ +O.3(0 O - Z ^ f f Bc.iqsio

6 <9.3/S</37 0,303078 ; 0. 3067V9 0. 30^,1 f101112

13 |14

0. 3067V0,33/8<?0. 331100.3//090.31781

00 1Prior to Branch

Cr1 377

r H Field

suGrabDaily

Z-i^T

$.2i?>2V$,2fl$.24

Q -) //0 * ui f

8. if :8.2t ;8,38 ,$.38

i^ O'33fa8l0* 32 k§ I

1718192021

222324

0. 33681 8. 320,3/011 2. i oo.nk-nO,3 OSS 3.O. 33O^>^0.303^0O.30MO0.30340

8. 2,?8.28

8. 2(o25 '• O»'3^Sdy %,2iff2627 , l

2829

0.33480Q.lilaS0.3fOf^0.3(8f3

8-2fc?,2Vcf. 2 f

30 o,3/$</331

Total £0 ^O.<n "/

0<3/8<J3',</ +0,^ 1,72.353

8> 2 y j

Wasteu'iiUr Discharge Monitoring FormFacili ty Name: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC: 123143 Paae 1 of29

SummaryValuer

L.imit(s) InEffect

QA7QCInforms tion

Sample PointDescription

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

Week 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

Monthly Avg

Daily Max

Daily Min

WeeklyAverage

LOD

LOQ

QCExceedence

LabCertification

No.

701Influent

5611,1,1-Trichloro-

ethane

ug/LXXXXXXX

aoxxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

0.30

3,1

^3 'C

701Influent

117Chloroethane

ug/LXXXXXXX

*0.97xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

0.97

3.1

y«y*>7so

701Influent

556

1,1-Dichloroethane

ug/LXXXXXXX

7,Vxxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

0.1$

•?.y

yo^3«so

701Influent

5701,2-Dichloroetha

ug/LXXXXXXX

*0.36xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

0.3(*

IJ

^WSD

001Prior to Branch

Cr211

i Flow Rate

MOD

0,3/660

0.340^50.21412xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

001Prior to Branch

Cr" 377pH Field

' suXXXXXXX -

t.3%$.24

xxxxxxx ~

xxxxxxx

xxxxxxx

xxxxxxx:

9 1° 16 o'4~ i

xxxxxxx

xxxxxxx

Vi'astewatcr Discharge Monitoring FormFacility Nime: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC: 123143 Page 2 of 29

Sample PointT5escriptioh

ParameterDescription

Units1Sample Type

FrequencyFootnotes

Sample Results Day 1234

567

8910

H

001 001Prior to Branch

Cr457

Suspended Solids,Total

mg/LGrab

Weekly

±3.0

Prior to BranchCr66

BODS, Total

mg/LGrab

Monthly

^L.2,0

001Prior to Branch

Cr487

Temperature

degFGrab

Monthly

¥8.2.

,

<2.0

12131415

001 j 001 [ 001Prior to Branch

Cr388

Phosphorus,Totalmg/LGrab

Monthly

*o.osy

' SO.O\

16

1718

19 4 P.O $0.0202122 i23242526 ^3.0 5o.o272829 )3031

Total ^2.£? ^2.0 /38,2 *0.0$L/

Prior to BranchCr789

Nitrogen, Ammonia(NH3-N) Total

mg/LGrab

Monthly

*o. H

Prior to BranchCr

" 231Hardness, Total as

CaCOS

mgO.,GraB

Monthly

3~7O

\

\

\

AO. n 310 }

V/asieuati:i Discharge Monitoring FormFacili ty Nune: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC: 123143 Page 3 of29

.SummaryValuer

Sample Point) 001Description

ParameterDescription

Units

Monthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

Week 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

Limit(s) In Monthly AvgEiffect

QA/QCInformation

Daily Max

Daily Min

~~ Weekly""Average

LOD

LOQ

QCExceedence

LabCertification

No.

Prior to BranchCr457

Suspended Solids,Total

mg/L

0

*3.0

<?.oXXXXXXX

xxxxxxx

xxxxxxx

xxxxxxx

40 o

xxxxxxx

xxxxxxx

^,3VD30

001Prior to Branch

Cr66

BODS, Total

mg/L

XXXXXXX

u,oxxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

4 OS/ 3 275-Q

001TfioFto Branch

Cr487

Temperature

degF

XXXXXXX

50xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

001Prior to BralicTT

Cr388

Phosphorus,Totalmg/L

XXXXXXX

< o.o5 yxxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

11

001 j O'OlPrior to Branch Prior to Branch

Cr Cr789

Nitrogen, Ammon(NH3-N) Total

mg/L

XXXXXXX

*0./lxxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

o.n0.35

ww*

231a Hardness, Total as

CaCO3

mg/L

XXXXXXX

"^ 37Oxxxxxxx

j XXXXXX[

X>DCXXXX

xxxxxxx

XXXXXXX

xxxxxxx

xxxxxxx

Wjr/3 </<:>,?0

Wastewat ;r Discharge Monitoring FormFacili ty Name: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573F.eportiig Period 05/01/2004-05/31/2004 DOC: 123143 Page 4 of29

Sample PointDescription

ParameterDescription

UnitsSample Type

FrequencyFootnotes

Sample Results Day 1i 2

3456

' 7r s

910

i 11

121314151617

18 "119202122232425262728293031

Total

001Prior to Branch

Cr40

Benzene

mg/LGrab

Monthly2

£0.oooyi

£.0.000^1

001Prior to Branch

Cr40

Benzene

Ibs/dayCalculatedMonthly

t.o.oo/co<j

^D.OOIOQ^

001Prior to Branch

Cr80

Bromoform

mg/LGrab

Monthly

+o.oooq<s

tiO.OOOW

001Prior to Branch

Cr80

Bromoform

Ibs/dayCalculatedMonthly

+ O.O033O3

* 0, 003t3 03

001Prior to Branch

Cr93

Carbontetrachloride

mg/LGrab

Monthly

tC'OOO^ci

^0.000^9

001Prior to Branch

Cr93

Carbontetrachloride

liEsTdayCalculatedMonthly

<0'OO/30O

tD-OOi^OD

Wastewatrr Discharge Monitoring FormFacility Mime: LEMRERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004 - 05/31/2004 DOC: 123143 Page 5 of29

r~"

Summai-yValues

Limit(s) InEffect

QA/QCInformation

Sample PointDescription

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

Week 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

Monthly Avg

Daily Max

Daily Min

WeeklyAverage

LOD

LOQ

QC ~|Exceedence

LabCertification

No.

001Prior to Branch

Cr40

Benzene

mg/LXXXXXXX

<aoooV/XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

10'60°.

0.000^1

O.OO/3

</0SV3.P75~0

001Prior to Branch

Cr40

Benzene

Ibs/day

0

<D.OOi004XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

0.393 0

XXXXXXX

XXXXXXX

t/OS'/JJ75"0

001Prior to Branch

Cr80

Bromoform

mg/LXXXXXXX

<o.oooi¥XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

58.6 o

0.00094D.OO3O

VOSM07SO

001Prior to Branch

Cr80

Bromoform

Ibs/day

O

<zO.OO3t3o3XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

0.141 0

]

1

XXXXXXX

XXXXXXX

y 05 1 337 SO

001Prior to Branch

Cr93

Carbontetrachloride

mg/LXXXXXXX

<o.oooWXXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

70.4 0

0,000 «/?O.ooKo

vefl33Ko

r - ooiPrior to Branch

Cr93

Carbontetrachloride

Ibs/day

0 j

40.00/300XXXXXXX

XXXXXXX

xxxxxxx

XXXXXXX

XXXXXXX

0.165T0

1

r H

j

XXXXXXX "•

^XXXXXXX

Waste\v:ikr Discharge Monitoring FormFacility Niime: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC: 123143 Page 6 of 29

Sample Results

Sample PointDescription

ParameterDescription

Units

Sample TypeFreq uency

Footnotes

Day 12

34

56

001Prior to~Branch~

Cr118

Chloroform

mg/L

Grab

001Prior to Branch

Cr118

Chloroform

Ibs/dayCalculated

Monthly i Monthly

<:O.OO037

789 ;1011121314

001Prior to Branch

Cr174

Dichlorobromo-meth(bromo-dichlorometl

ug/L

001 [ 001Prior to Branch

Cr174

Prior to BranchCr570

Bichlorobromo-meth|,2-Dichloroetha(bromo-dichlorometh

Ibs/day mg/LGrab Calculated j Grab

Monthly

+ 0.00090(0 £Q.S(o

Monthly Monthly

^0.00131^. <O .0003(o

15 ,1617

001Prior to Branch

Cr570

1,2-Dichloroetha

Ibs/day

CalculatedMonthly

<L 0.000 882.

Total <O.OOO37 <O.OOO3Q>

Waitewatt r Discharge Monitoring FormFaci l i ty Name: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC: 123143 Pane''of 29

SummaryValues;

Limit(s) InEffect

Information

!

n

on

Sample Point

Description

Parameter

Description

Units

Monthly Avg

Daily Max

Daily Mir

Week 1 Avg(1-7)

Week 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

Monthly Avg

Daily Max

Daily Min

WeeklyAverage

001Prior to Branch

Cr118

Chloroform

mg/L

XXXXXXX

<£>.<%>O3 7

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

57.80

001Prior to Branch

Cr118

Chloroform

Ibs/day

O

+G.000<) \96

XXXXXXX

XXXXXXX

XXXXXXX

001Prior to Branch

Cr174

Dichlorobromo-metli(bromo-dichlorometl

ug/L

XXXXXXX

*O.S6>XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX XXXXXXX

XXXXXXX j XXXXXXX1

0.1150

LOD .,_ XXXXXXX „0. 00037 0. 56

LOQ

QCExceedence

CertificationNo.

o.oo /a xxxxxxx ;.S

001Prior to Branch

Cr174

Dichlorobromo-metli[bromo-dichlorometl

Ibs/day

O

<O.OOI313LXXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

0.141 o

XXXXXXX

XXXXXXX

yo«3,,«>-Wr/337ro VDr/3.75D www

001 | 001Prior to Branch

Cr570

Prior to BraCr

| 570 ~4,2-Dichloroetha

mg/L

XXXXXXX

<0.0003(oXXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

236 o

1,2-Dichloro

Ibs/day

O*0.000%±

nch

etha

_j

XXXXXXX

Xy*i~X.XX .X

,/v iVY.A. A .A.

X \' V "V V V^iJ\VVj\ f\.

X

x-

X

XXXXXXX

0.29

. _ __ I0

1

,, ^ _,, XXXXXXXO.OOO3(o

o.ooil

4 OS J 33750

XXXXXXX

'/DS/33-75'0 :

Wastewattr Discharge Monitoring FormFacility Niitne: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004- 05/31/2004 DOC: 123143 Page 8 of 29

Sample Point 001 | 001Description

ParameterDescription

UnitsSample Type

FrequencyFootnotes

Sample Results Day 12

345

78g

1011

Prior to BranchCr570

1,2-Dichloroetha

% RemovalCalculatedMonthly

too

121314

Prior to BranchCr558

1,1-Dichloroethy

mg/LGrab

Monthly

<O. 00051

15161718

001Prior to Branch

Cr558

1,1-Dichloroethy

Ibs/dayCalculatedMonthly

^O.OOI^b

001Prior to Branch

Cr576

1,2-transDichloroethylcne

mg/LGrab

Monthly

* 0.000 8<j

\

\

!

192021

222324252627

i 282930 '

31

i Total /00 <LO-OO05~) <O.OO/3<3£> <O.CCO$7

001Prior to Branch

Cr576

1,2-transDichloroethylene

Ibs/dayCalculatedMonthly

^ O.QO 3/8O

+C.OO3ISO

001Prior to Branch

Cr567

r~ l^cisDichloroethene

mg/LGraB

Monthly

^0.00083

<o,ooo83

V/astewatcr Discharge Monitoring FormFacility N ime: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC: 123143 Page 9 of 29

Summarylvalues

Limit<X InEffect

SJA/QCInformation

Sample PointDescription

ParameterDescription

Units

Monthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

Week 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

Monthly Avg

001Prior to Branch

Cr570

1,2-Dichloroetha

% RemovalXXXXXXX

/DO

XXXXXXX

XXXXXXX

XXXXXXX

001Prior to Branch

Cr558

1,1-Dichloroethy

mg/L

XXXXXXX

<o.ooos-iXXXXXXX

XXXXXXX

XXXXXXX

001 001Prior to Branch

Cr558

1,1-Dichloroethy

Ibs/day

O

^.<?0/3%

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX XXXXXXX XXXXXXX

XXXXXXX XXXXXXX XXXXXXX

Daily Max

Daily Miri

WeeklyAverage

60.544

Prior to BranchCr576

1,2-transDichloroethylene

mg/L

XXXXXXX

< 0.00087XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

0.165 |^

1

o 270 o

[

1LOD XXXXXXX _ _ ^ , _ XXXXXXX

O.OOOblLOQ XXXXXXX ,

QCExceedence

o.oooSlj XXXXXXX

8

LabCertification </O$'/337S'O yPS~/;?D7SZ> <-/0^/3^5O VOS/3^750

No.

001Prior to Branch

Cr576

1,2-transDichloroethylene

Ibs/day

0

< O* OOJ/80XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

21.1 o

XXXXXXX

XXXXXXX

yks 13 i so

001Prior to Bra

Cr567

nctt

1,2-cisDichloroetticni.'

mg/L

~"xxxxxx

<LO. OOO&

XXXXXX

XXXXXX

XXXXXX

XXXXXX

X

>3-J

x~"

x~~

x~"

x~~

XXXXXXX

270" o

0. 00083

0.002(0

H '05/33'? SO

V/asieuat:r Discharge Monitoring FormFacili ty Name: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC: 123143 Page 10 of 29

Sample Point! 001Description

ParameterDescription

UnitsSample Type

FrequencyFootnotes

Sample Results Day 1234567o

9

Prior to BranchCr567

1,2-cisDichloroethene

Ibs/dayCalculatedMonthly

£0.003033

101112

: 13

001Prior to Branch

Cr200

Ethylbenzene

mg/LGrab

Monthly

*-O.OO06<J

14

001Prior to Branch

Cr200

Ethylbenzene

Ibs/dayCalculatedMonthly

*0, OO/323

1516 i17 ; ;18 |1920 ;21 122 :23 ;

24

25

001Prior to Branch

Cr285

Methylenechloride

mg/LGrab

Monthly

±0.000^3

001Prior to Branch

Cr285

MethylenechlorideIbs/day

CalculatedMonthly

<0.00/0£2>

" " 001 - iPrior to Branch

Cr490

TrtrachUiro-ethylene

mg/LGraB

Monthly

i

tO.OOGVS

27 , ;

28293031 :

Total <O.OO303Z\ *O.OOO5V v0.dO/333 ^O.OOO^3 \<O,OOI053

1

1I

^D.OOD^S

V/astewatcit Discharge Monitoring FormFacility N ame: LEMHERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC: 123143 Page 11 of 29

SummaryValues

Limit(s) InElffect

C>A/QCInformation

Sample PointDescription

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

"WeeTcTAvg"(I -7)

Week 2 Avg(8-14)

00 1 i 001Prior to Branch

Cr567

U-cisDichloroethene

Ibs/day

O

Prior to BranchCr200

Ethylbenzene

mg/L1 xxxxxxx\

001Prior to Branch

Cr200

Ethylbenzene

Ibs/day

0

<D, 00/32 3XXXXXXX XXXXXXX ! XXXXXXX

I

XXXXXXX XXXXXXX XXXXXXX

001Prior to Branch

Cr285

Methylenechloride

mg/LXXXXXXX

^ 0.000^3xxxxxxx

001

Prior to BranchCr285

MethylenechlorideIbs/day

c40.0OIOS3

xxxxxxx

xxxxxxx xxxxxxx

XXXXXXX XXXXXXX XXXXXXX XXXXXXX XXXXXXX

Week 3 Avg XXXXXXX XXXXXXX(15-21)

Week 4 Avg XXXXXXX(22-28) !

Monthly Avg

Daily Max

Daily Min

21. 1

WeeklyAverage

o

LOD XXXXXXX

LOQ XXXXXXX

QCExceedence

XXXXXXX

90.63

0-OOO5

xxxxxxx xxxxxxx xxxxxxx

xxxxxxx xxxxxxx xxxxxxx

110

[

0

o448

3.68

O

• ~ 001TrioFtbTJra

Crncli

490Tetrachloro-

cthylene

mg/L

XXXXXXX

+0.000&

XXXXXXX

X>DCXXXX

xxxxxx

xxxxx?c

X

x~

x>:xxxxx

o25.8

i

1r

0

</ xxxxxxx 0.PQOV3 xxxxxxx D.OOO^SYYYYYY

D.OO/7 AA^AAA-V YYYYYYYA. . / J\J\.V\.J\ YJ\J\ —, _^_ . /o.oolr 0,001 4

Lab ;Certification UQ^J 3^7 fo <JoS/337£~O ^0^/33150 yo^J3DT

No. ;

1

ft) </OS-/327SO Vf 573.2 750

Wastew:iur Discharge Monitoring FormF.icility N;ime: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC: 123143 Page 12 of 29

{Sample Result:

Sample PointDescription"

Parameter

Description

Units

Sample Type

FrequencyFootnotes

Day 1

^— 2 '34

5

[Z 7 "^ 9

^ 101112

001"Prior to Branch"

Cr490

Tetrachloro-ethyleneIbs/day

Calculated

Monthly

001Prior to Branch

Cr500

Toluene

mg/L

GrabMonthly

£0*001101 £0.000(07

001Prior to Branch

Cr500

Toluene

Ibs/dayCalculated

Monthly

tLOoOOHe'tl

001Pno~rT(TBrancii

Cr561

1,1,1-Trichloro-ethanemg/L

GrabMonthly

tLO.OQOlO

i j I14 :

1516

17

18192021222324252627282930

001 i 001Prior to Branch

Cr561

1,1,1-Trichloro-cthanc

% Removal

CalculatedMonthly

Prior to BranchCr561

1,1,1-Trichlorc-ethant

Ibs/clay

CalculatecTMonthly

/OO <L0.002~J06

r

1

i

Total OO

V/astewali:r Discharge Monitoring FormFacii ity N ime: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC: 123143 Page 13 of 29

SummaryValues

Sample PointDescription

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

Week 2 Avg(8-14)

Week 3 Avg(15-21)

001Prior to Bra

Crnch

490Tetrachloro-

ethyleneIbs/day

O

to. oo it 01XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

001Prior to Branch

Cr500

Toluene

mg/LXXXXXXX

<LO'OOO(t>7XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

001Prior to Branch

Cr500

Toluene

Ibs/day

O

+ O.OQIWIXXXXXXX

XXXXXXX

XXXXXXX

001Prior to Branch

Cr561

1,1,1-Trichloro-ethanemg/L

XXXXXXX

eLO.OOO130XXXXXXX

XXXXXXX

XXXXXXX

001Prior to Branch

Cr561

1,1,1-Trichloro-ethane

% RemovalXXXXXXX

loo

001Prior to Branch

Cr561

1,171-Trichloro-ethanc

Ibs/day

O

to.ooncsXXXXXXX XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX XXXXXXX XXXXXXX

Week 4 Avg XXXXXXX XXXXXXX XXXXXXX XXXXXXX XXXXXXX(22-28)

Limit(s)In Monthly Avg 0.361Effect

Daily Max

Daily Min

WeeklyAverage

034.918

596

O

0139.4

QA/QC LOD XXXXXXX ~ __ ._ . _, XXXXXXX^formation O.OOObl O.OOOl

oi

iXXXXXXX'o

X>LXXXXX

xxxxxpa

XXXXXXX

XXXXXXX

L ^~o

\

\\

\\

x>:xxxkxQA/QCInformat ion

LOD XXXXXXX f. __ .. . _, XXXXXXX „O.OOObl D.OOO^O

LOQ XXXXXXXO.OO3

\

\

Exceedence

Certification s/o^"/3^7<No.

XXXXXXX ^ -./ 0.0021

^0 <-/o$J33750 y^S"/3^75O t-/C>£J33->SO

XXXXXXX

XXXXXXX

^5/307-5 0

xxxxxpc1

Wastewitt r Discharge Monitoring FormFacility Niime: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004- 05/31/2004 DOC: 123143 Page 14 of29

'Sample PointDescription

Parameterprescription

Units!Sarh"pTe~Ty"|DeTrequency"Footnoted

Sample Results

001Prior to Branch

Cr508

Trichloroethylilenl

mg/L"GraTr

Monthly

T6

Total

001'rior to Branch

Cr508

frichloroethylen517

FVinyl chloride

Ibs/dayCalculatedMonthly

001 001 ~OOT"Prior to Branch Prior to Branch

Cr

GrabMonthly

Cr517

Vinyl chloride

Ibs/dayCalculated

Prior to BranchCr229

Halomethanes,Total

GrabMonthly Monthly

001

Prior to BranchCr229

Halomethanes,TotalIbsTclay

CalculatedMonthly

j I

<0.ooo</8 +0,001 nb 8 +o,oooy<Ji \<o.oo3i>c3

Vk'astewat.-r Discliarge Monitoring FormFacili ty Name: LEMHERGER LANDFILL SUPERFUND SITE Permit: 0049573P.eporti ng Period 05/01 / 2004 - 05/31 /2004 DOC: 123143 Page 15 of29

SummaryValues

/imit(X InEffect

QA/QCInforrnntion

Sample Point 001Description

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

Prior to BranchCr508

Trichloroethylen

mg/L~~xxxxxxx ~

<O'Oooy&XXXXXXX

XXXXXXX

Week 2 Avg i XXXXXXX(8-14) i

Week 3 Avg XXXXXXX(15-21)

001 001Prior to Branch

Cr508

rrichloroethylen

Ibs/day

O

<o.ooin(eXXXXXXX

Prior to BrancCr517

e Vinyl chloridi

ug/LXXXXXXX

001 1 001 ; 001h Prior to Branch Prior to Branch

Cr \ Cr517

; Vinyl chloride

Ibs/day

: Oi

+ G./8 Vo.OOQWlXXXXXXX

XXXXXXX XXXXXXXi

XXXXXXX XXXXXXX

XXXXXXX

Week 4 Avg XXXXXXX XXXXXXX(22-28)

Monthly Avg ; 0.392

Daily Max 8 1 .4O

Daily Min

WeeklyAverage

XXXXXXX

XXXXXXX

o

XXXXXXX[

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

0.0117 0

\

\1

1LOD . .... XXXXXXX ... 0O.ooo¥8 O./8L°Q n ^,f XXXXXXX ^ __,D.OOI& £>, 57QC

ExceedenceLab

Certification ^573375-0 ^OS/3j~7.No.

XXXXXXX

XXXXXXX

229Halomethanes,

Totalug/L

XXXXXXX

<o.wXXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

1

0.9V

3.0

fO y^5/JP75"O '/O5/33.75O </£>Sy3-175D

Prior to BranchCr

" 229Halometh

TotalIbVda

ar

rn:s,

O

<0,0033XXXXX

xxxxx

xxxxxx;cxxx^

x^cxxx1

0.141

_

xxxxx

"locxxx

0X

X

X

X

X

~

x"

1 1-1 ix tX 1

X

X

x~~

o

X

xx ji

7

iJT

5~0

Wastewatrr Discharge Monitoring FormFacility N urns: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC: 123143 Page 16 of29

Sample Results

Sample PointDescription

Parameter

Description

Units

Sample Type

Frequency

Footnotes

Day 1

234

5

6789101112131415161718 "

192021 '22 "

232425262728293031 "

Total

001Prior to Branch

Cr117

Chloroethane

ug/L

Grab

Monthly

<o.<T)

<LO.i-l

001Prior to Branch

Cr117

Chloroethane

% Removal

Calculated

Monthly

SOO

IOO

001Prior to Branch

Cr556

1,1-Dichloroethane

ug/LGrab

Monthly

<ao.~)S

<0.~1S

001Prior to Branch

Cr556

1,1-Dichloroethane

% Removal

Calculated

Monthly

/OO

/DO

001 001 1iPrior to Branch Prior to Branch

Cr Cr35 35

Arsenic, Total Arsenic, TotalRecoverable Recoverable

ug/L Ibs/clay

Grab Calculated

Monthly Monthly1

<3.y \40.oot & &?\

i

•1i

<3.V <0,OO833<?\

Wastewatrr Discharge Monitoring FormFacility N line: LEMBERGER LANDFILL SUPERFUNO SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC: 123143 Page 17 of 29

Summa-yValues

Limit(s) InEffect

QA/QCInformation

Sample Point! 001Description

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avgd-7)

Week 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

I 001Prior to Branch

Cr117

Chloroethane

ug/LXXXXXXX

< £ , V 7xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

Monthly Avg:

Daily Max ;

Daily Min

WeeklyAverage

LOD ^ a

LOQ 3.1QC

ExceedenceLab :

Certification </o$'/337No.

Prior to BranchL Cr

117Chloroethane

% RemovalXXXXXXX

IOO

001Prior to Branch

Cr556

1,1-Dichloroethane

ug/LXXXXXXX

! <o. isxxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx xxxxxxx

xxxxxxx xxxxxxx

xxxxxxx xxxxxxx

xxxxxxxC/, /o

xxxxxxx

001Prior to Branch

Cr5561,1-

Dichloroethane% RemovalXXXXXXX

tooXXXXXXX

XXXXXXX

xxxxxxx

xxxxxxx

xxxxxxx

1 001Prior to Branch

Cr35

Arsenic, TotalRecoverable

ug/LXXXXXXX

*3.yxxxxxxx

0

727.6 Q

51 0

xxxxxxx ? .>3. 7

xxxxxxx .

S"0 </O5~/3J750 y&5'/3J75~O *SoS/3J~?5~O 1-}1J5I3'*/03O

" 001Prior to Branch

Cr35

Arsenic, TotalRecoverable

Ibs/day

O'

xxxxxxx

X)CXXX]XX

xxxxxxx

xxxxxxx

x;cxxxxx

3'88tt°1

r\

xxxxxpfx

xxxxxxx

J

V'astewaUr Discharge Monitoring FormFacil i ty N.ime: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period. 05/01/2004-05/31/2004 DOC: 123143 Page 18 of 29

Sample

Sample PoinlDescription

ParameterDescription

UnitsSample Type

FrequencyFootnotes.

Results Day 1

L 2 _34

56

: 1891011121314151617 ~"

1819202122232425262728 '293031

Total

001 001Prior to Branch Prior to Branch

Cr Cr50 50

Beryllium, Total Beryllium, TotalRecoverable Recoverable

ug/L Ibs/dayGrab Calculated

Monthly Monthly

0,3*/ 0. 000833

0,3<{ 0.000$3'&

001Prior to Branch

Cr87

Cadmium, TotalRecoverable

ug/LGrab

Monthly

£0.1%

*o,/8

001Prior to Branch

Cr87

Cadmium, TotalRecoverable

Ibs/dayCalculatedMonthly

<L 0.000441

to.oooWl

001Prior to Branch

Cr126

Chromium +3

mg/LGrab

Monthly

0,00079

o.oootl

001Prior to Branch

Cr" " 126Chromium +3

Ibs/day "J

CalculatedMonthly

,_

\o.oo^yzs^

\

\\

11

o>- 003^35

Wastewati r Discharge Monitoring FormFaci l i ty Niune: I.EMBERGER LANDFILL SUPIERFUND SITE Permit: 0049573Reporting Period. 05/01/2004-05/31/2004 DOC: 123143 Page 19 of29

SummaryiValues

'imit(s) Iniffect

A/QCInforms tion

Sam pie PointDescription

ParameterDescription

UnitsMonthly Avg

00 1Prior to Bra

Cr50

nch

Beryllium, TotalRecoverable

ug/LXXXXXXX

pa-ly Ma*^ ^y

Daily Min

Week 1 Avg(1-7) j

Week 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

Monthly Avg

Daily Max ; 4660

Daily MTn

WeeklyAverage

LOD" o.H

0

001Prior to Branch

Cr50

Beryllium, TotalRecoverable

Ibs/day

0,000833

0,000833xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

0.00258

\\[

0

001 | 001Prior to Branch

Cr87

Cadmium, TotalRecoverable

ug/LXXXXXXX

+ 0.18xxxxxxx

0

Prior to BranchCr87

Cadmium, TotalRecoverable

Ibs/day

O

^o.oooi11xxxxxxx

xxxxxxx

xxxxxxx

! XXXXXXX

27.08

0.573

001Prior to Branch

Cr126

Chromium +3

mg/LXXXXXXX

0.00013xxxxxxx

o,ooo<?<l

xxxxxxx!

i 0.775

O \

1

o

o «0.046

xxxxxxx O f i g xxxxxxx Of000?

LOQ ^ ^ XXXXXXX _ _ 0 XXXXXXX

o

- DOTPrior to Branch

Cr126

Chromiif

Ibs/da

n

v"

+3"

o.coji/ysO.C03H3I5^xxxxxxx

x>;xxxXXXXX

x>:xxx

XXXXX

X

X

X

k"1097C

oXXXXX

of

XXXXX

—

x

X

X

X

X

X

0

X

X

- - Q C ;Exceedence

LabCertification

No.

Waste\\at:r Discharge Monitoring FormFacility Name: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reportiig Period.1)5/01/2004-05,31/2004 DOC: 123143 Page 20 of 29

I

Sample Results]"

Sample PointDescription

ParameterDescription

UnitsSample Type

FrequencyFootnotes;

Day 1234567

8910

1213 "14

L 1516171819202122 "'"I232425262728293031

Total

001Prior to Branch

Cr147"

Copper, TotalRecoverable

ug/L

GrabMonthly

£ 1,2

+ 1.2

001Prior to Branch

Cr155

Cyanide, Total

ug/LGrab

Monthly

£/,6

*/.b

001Prior to Branch

Cr155

Cyanide, Total

Ibs/dayCalculatedMonthly

t-O'OO'3 9 /*?

^.0039/9

001Prior to Branch

Cr264

Lead, TotalRecoverable

mg/LGrab

Monthly

^-O'OOO/^

<0. 00014

001 001Prior to Branch Prior to Branch

Cr Cr264 280

Lead, Total Mercury, TotalRecoverable Recoverable

Ibs/day ng/LCalculated GrabMonthly Monthly

£ O. OOO3V3 £.5(0

\

•

;

* 0 .0003*4 3- £.5 {?

Wastewar.T Discharge Monitoring FormFaci l i ty Name: LEMHERGER LANDFILL SUPERFUND SITE Permit: 0049573F.eport'ing Period-05/01/2004-O.V31/2004 DOC: 123143 Page 21 of29

• • - ••

ISumma-yValues

Sample PointDescription

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

^eek 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

Limit(s) In Monthly AvgEiffect

QA/QCInformation

Daily Max

Daily Min

WeeklyAverage

001Prior to Branch

Cr147

Copper, TotalRecoverable

ug/LXXXXXXX

£1- a.xxxxxxx

0

93.34

11.3

LOD /.aLOQ 3.8

ExceedenceLab

Certification <J(/5~/3</0No.

001Prior to Branch

Cr155

Cyanide, Total

ug/LXXXXXXX

^/.6

001Prior to Branch

Cr155

Cyanide, Total

Ibs/day

0

£0,003111xxxxxxx xxxxxxx

~ | XXXXXXX

XXXXXXX

xxxxxxx

xxxxxxx

47

o 44'8 oI

o L65 o

o

xxxxxxx

^^ — . ^VyV^\j\^\.^j\

o , 6

30 Vyiwww :*«*».

001Prior to Branch

Cr264

Lead, TotalRecoverable

mg/LXXXXXXX

t,o,ooc>i4xxxxxxx

0

1.37

0.0145

o.oooi

o

o4

o.oooIR

MSWo-lo

001 001Prior to Branch Prior to Branch

Cr Cr264 280

Lead, Total j Mercury, ToRecoverable Recovers bl

Ibs/day

0

r ng/L

O

£D.oo03<J3xxxxxxx

xxxxxxx

^Sb^XXXXXX

r xxxxxx

sr"e

x-x~~

xxxxxxx xxxxxxx

xxxxxxx xxxxxxx

xxxxxxx

3.86

xxxxxxx

o °'67

1

3.06^h

o

0

xxxxxxx ,_ ,o (oXXXXXXX Q

\

V/aslewatrr Discharge Monitoring FormFaciliW N ime: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004 -05/31/2004 DOC: 123143 Page 22 of 29

Sample PoinDescription

ParameterDescription

UnitsSample Type

FrequencyFootnotes

Sample Results; Day 12

1

45678910 "11121314

1516171819202122 ~

"" 23 "242526272829 "3031

Total

001Prior to Branch

Cr280

Mercury, TotalRecoverable

Ibs/day

CalculatedMonthly

^O.oo/os^

£0. OO/OS3

001Prior to Branch

Cr315

Nickel, TotalRecoverable

mg/L

GrabMonthly

<0f0031

<,0,OO37

001Prior to Branch

Cr315

Nickel, TotalRecoverable

Ibs/dayCalculated

Monthly

£0. 00(0(01*}

<0,00(tbi<J

001Prior to Branch

Cr423

Selenium, TotalRecoverable

ug/L

GrabMonthly

3.1 ~1

Q.I

001Prior to Branch

Cr423

Selenium, TotalRecoverable

Ibs/dayCalculatedMonthly

0.005/yy

0. 005 I'M-

001Prior to Branch

Cr430

Silver, TotalRecoverable

ug/LGraB

MontKly

*0.'3ff

1

+ 0*38

V/aslewatcr Discharge Monitoring FormFacility Name: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC: 123143 Page 23 of 29

SummaryValues

Sample PointDescription

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avgd-7)

Week 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

Limit(s] In Monthly AvgEffect

QA/QCInforrnntion

L

Daily Max

Daily Min

u WeeklyAverage

001Prior to Branch

Cr280

Mercury, TotalRecoverable

001Prior to Branch

Cr315

Nickel, TotalRecoverable

Ibs/day mg/L~ XXXXXXX

t0.00/OS3XXXXXXX

< 0.00 31XXXXXXX

XXXXXXX ^

XXXXXXX

XXXXXXX

XXXXXXX

0.0062 o

001Prior to Branch

Cr315

Nickel, TotalRecoverable

Ibs/day

0

*:O.OO(0(0li-tXXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

001Prior to Branch

Cr423

001 n 001Prior to Branch

Cr423

Prior to BranchCr

! 430Selenium, Total j Selenium, Total

Recoverable ! Recoverableug/L

XXXXXXX

Q.IXXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX XXXXXXX

5.06

0.052

LOD XXXXXXX

13.1

0

o

o116

O

0,0031 xxxxxxx /, 2LOQ XXXXXXX .,

QCExceedence

Certification ^V^/S^O'^O </</ST/3/<9No.

XXXXXXX j.

3o */*/£> /^yo*.30 tS<jZ/3</(.

Ibs/day

0.00514*1

o.oosiWXXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

^' Silver, TotalRecoverable

ug/EXXXXXXX

^0.38XXXXXXX

o

rXXXXXXX

0.785 o12'lff o

H 2'03 oXXXXXXX -* .^ f\

XXXXXXX i. 2

t/t/sjsy&SD WSMVO

V/astewatT Discharge Monitoring FormFacility Name: LEMflERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC: 123143 Page 24 of 29

Sample PointDescription

LParameter

Description

UnitsSample Type

FrequencyFootnotes

Sample Results Day 1

r 23

; 41

5

678910

1112131415~ '16" "

17181920 ^

' 22 ""'1 23

24 H

25 _J

2728

" 29 J30 ~!31 "~"

Total

001Prior to Branch

Cr430

Silver, TotalRecoverable

Ibs/dayCalculatedMonthly

±0,0003 31

^0. 000331

001Prior to Branch

Cr553

Zinc, TotalRecoverable

ug/LGrab

Monthly

/I3.tf

^3.5

001Prior to Branch

Cr553

Zinc, TotalRecoverable

Ibs/dayCalculatedMonthly

^o.ooyzol

£0.00 ?30l

001Prior to Branch

Cr251

Iron, TotalRecoverable

mg/LGrab

Monthly

«C<9,OJ3

^£.033

001Prior to Branch

Cr27

Aluminum, TotalRecoverable

mg/LGrab

Monthly

tLO-OlO

^CcOlO

001Prior to Branch

Cr1 " 1 0 5

Chloride

mg/LGraB

Monthly

^~ 14 \Ir 1L•

-\- i1 !

'••

i

Iiii

/«/

V/aslewatci Discharge Monitoring FormFacil i t j 'Nmie: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004-05/31/2004 DOC. 123143 Page 2:5 of 29

Sample Point 001Description

ParameterDescription

UnitsSummary Monthly AvgValues

Daily MaxI!• Daily Min

Week 1 Avg(1-7)

Week 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

limit(s) In Monthly AvgEffect

Daily Max

. Daily Mir

WeeklyAverage

QA7QC LODInformation

LOQ

QCExceedence

Prior to BranchCr430

Silver, TotalRecoverable

Ibs/day

O

CO'OOO^ >3/xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

0.4580

xxxxxxxxxxxxxx

LabCertification ^</573</£>3C>

No.

001Prior to Branch

Cr553

Zinc, TotaRecoverable

ug/LXXXXXXX

^3.8xxxxxxx

O

572

43.7

o

O

3.%/3.

W$;3yo3o

001Prior to Branch

Cr553

Zinc, TotalRecoverable

Ibs/day

O

£G.OO93t•><*xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

391 o

xxxxxxx

xxxxxxx

001Prior to Branch

Cr251

Iron, TotalRecoverable

mg/LXXXXXXX

46.033xxxxxxx

o

333

001 " T " 001Prior to Branch

Cr27

Aluminum, TotalRecoverable

mg/LXXXXXXX

^O.OIOxxxxxxx

xxxxxxx

xxxxxxx

Prior to BraCr

ITch"

r ~ 105Chloride

mg/LXXXXXXX

/?"XXXXXXX

H \

xxxxxxx

xxxxxxx

2.2

o

o

XXXXXXX ^1 O.o/o

I1576h

133_ L

o

oX

xxxxxxx xxxxxxxO.033

W/3,o*>| W/3*>30 W/5Vto*> WS73^3O

VYaslewatrr Discharge Monitoring FormFacility Nime: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 05/01/2004 - 05/31/2004 DOC: 123143 Page 26 of 29

Sample PointDescription

ParameterDescription

UnitsSample Type

Frequency1 Footnotes

Sample Results1 Day 1234

567891011121314151617 "1819

" 20 ~~\2122 .2324252627282930 "31

Total

001Prior to Branch

Cr531

Additive WaterTreatment - Specify

Ibs/day

Record ofAddition

Daily

3

'

j

1

!

!

=1

I

\Vastew at^r Discharge Monitoring FormFacil i ty Name: LEMHERGER LANDFILL SUPERFUND SITE Permit: 0049573F:ePort"hg Period 05/01/2004-05/31/2004 DOC: 123143 Page 2 7 of 29

SummaryValues

Lim ills' InEffect '

QA/QCInformationn

Sample PointDescription

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avgd-7) ,

Week 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

Monthly Avg

Daily Max

Daily Miri

WeeklyAverage

LOD "

001Prior to Branch

Cr531

Additive WaterTreatment - Specify

Ibs/day

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

1

XXXXXXX

LOQ XXXXXXX

QCExceedence

LabCertification

No.

i ;

1

'

r

Waitewat.T Discharge Monitoring FormFacility Name: LEMHERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period 05/01/2004-05/31/2004 DOC: 123143 Page 28 of 29

Footnotes

1. Results of annual priority pollutant and RCRA Appendix 9 must be attached to DMR.2. Only VOCs detected in influent or effluent must be on DMR. Attach all VOC results.

I 3. Attach monthly record of water treatment additive use.

General Remarks

of a.^/on a Monday. / h e . Monday vQ-lu*- vJoi^ld be

4or 3 das, Goverina the. weekend.

Laboratory Quality Control Comments

r J

Soibmittjl of this form is recuired by section 283.55, Wis. Stats, and chapters NR 205 and 214, Wis. Adm. Code.

Personally identifiable information collected on this form may be used for purposes other than that for which it was originally collected.Under Vi/isconsin's open records laws, DNR is required to provide all non-confidential information to any person who requests it. Sujchinformation may be provided to the public in written or electronic form. Information reported may be made available to the public v a aDNR web page.

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance tvith asystem designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of theperson or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is,to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting falseinforma:ion, including the possibility of fine and imprisonment for knowing violations.

If you have any questions about this form, please call Linda Vogen at (920)492-5900.

Return Form To Authorized Representative Signature Date

LSRG-WI Department of Natural Resources

,,,„..,... -— Operator Signature Certificate Number Datel i : :5N Military p0BOX 10448 -Green Bay, Wl 54307 322.35 ZS Jfr* ZooV-

Make two copies of the completed form. Keep one copy and return the original and one copy to the DNR address provided.

Wastewat.'r Discharge Monitoring FormFacilitv Name: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period 05/01/2004 - 05/31/2004 DOC: 123143 p 29 of 29

En Chem Inc.Analytical Report Number: 846234

Client: RMT - MADISON

Project Name : LEMBERGER LANDFILL

Project Number : 3452.11

Field ID : MONTHLY EFFLUENT

1241 Bellevue StreetGreen Bay, Wl 54302920-469-2436

Matrix Type : WASTEWATER

Collection Date: 05/04/04

Report Date : 06/01/04

Lab Sample Number : 846234-001

VOLflTILES - SPECIAL LIST

Analjle Result LOD

1,1.1-Tri chloroethane

1,1--Dic:hloroethane

1,1- D chloroethene

1 ,2-D chloroethane

Ber.zone

Bro-n sdichloromethane

Bromoform

BroTiomethane

Carbc n Tetrachloride

Chloroethane

Chloroform

Chloromethane

cis- 1 ,:?-Dichloroethene

Dichlc rodifluoromethane

Ethyltenzene

Fluorc trichloromethane

Metaylene Chloride

Tetrac.hloroelhene

Toluene

tran.3- 1 ,2-Dichloroethene

Trichltiroethene

Vinyl (Chloride

< 0.90

< 0.75

< 0.57

< 0.36

< 0.41

< 0.56

< 0.94

< 0.91

< 0.49

< 0.97

< 0.37

< 0.24

< 0.83

< 0.99

< 0.54

< 0.79

<: 0.43

< 0.45

< 0.67

< 0.89

< 0.48

< 0.18

0.90

0.75

0.57

0.36

0.41

0.56

0.94

0.91

0.49

0.97

0.37

0.24

0.83

0.99

0.54

0.79

0.43

0.45

0.67

0.89

0.48

0.18

LOQ EQL Dll.

3.0

2.5

1.9

1.2

1.4

1.9

3.1

3.0

1.6

3.2

1.2

0.80

2.8

3.3

1.8

2.6

1.4

1.5

2.2

3.0

1.6

0.60

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Code An I Date

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04 '

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

Prep Date: 05/06/04

Prep Method Anl Method

SW846 5030B

SW846 5030B

SWB46 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 826;

SW846 826 1

SW846 826I

SW846 826(

SW846 826(

SW846 826(

SW846 826t

SW846 826C

SW846 826C

SW846 826(

SW846 826<

SW6^6 826C

SW646 826C

SW846 826C

B

)B

)B

B

B

B

B

B

B

B

B

B

B

B

SW846 8260^

SW846 8260B

SW846 82BOp

SW846 8260^

SW846 82Sob

SW846 8260B

SW846 8260B

SW846 8260B

En Chem Inc.Analytical Report Number: 846234

Client: RMT - MADISON

Project Name : LEMBERGER LANDFILLProject Number: 3453.11

Field ID : MONTHLY INFLUENT

1241 Bellevue StreetGreen Bay, Wl 54302920-469-2436

Matrix Type: WASTEWATERCollection Date : 05/04/04

Report Date : 06/01/04Lab Sample Number : 846234-002

VOLATILES - SPECIAL

Analyte

1,1,1 -Trichloroethane1,1-Cicfiloroethane1,2-Cichloroethane

Choroethane

LIST

Result

207.4

< 0.36

< 0.97

Prep Date: 05/06/04

LOD

0.900.75

0.36

0.97

LOQ EQL

3.02.5

1.2

3.2

Dil.

11

11

Units

ug/L

ug/L

ug/L

ug/L

Code An I Date

05/06/0405/06/0405/06/04

05/06/04

Prep Method

SW846 5030BSW846 5030BSW846 5030B

SW846 5030B

Anl Method

SW846 8260BSW846 8260BSW846 826

SW846 8.26

DB

DB

En Chem Inc.

Client: RMT - MADISON

Project Name : LEMBERGER LANDFILL

Project Number : 3453.11

Field ID : TRIP BLANK

Analytical Report Number: 846234

1241 Bellevue StreetGreen Bay, Wl 54302920-469-2436

Matrix Type : WASTEWATER

Collection Date : 05/04/04

Report Date : 06/01/04Lab Sample Number: 846234-004

VOLATILES - SPECIAL LIST

Anal,rte Result LOD

1,1,1-Trichloroethane

1,1-Cichloroethane

1,1-Cichloroethene

1,2-Cichloroethane

BenzsneBrorcodichloromethane

Brcimoform

Brcimomethane

Ca'bon Tetrachloride

Chloraethane

Chloraform

Chlorsmethanecis- 1 ,2Oichloroethene

Dichlorodifluoromethane

Ethylhe.nzeneFluarotrichloromethane

Methylene Chloride

Tetra ;hloroethene

Toluenetrans- 1 ,2-Dichioroethene

Trichlaroethene

Vinyl Chloride

< 0.90

< 0.75< 0.57

< 0.36

< 0.41

< 0.56

< 0.94

< 0.91

< 0.49

< 0.97

< 0.37

< 0.24

< 0.83

< 0.99< 0.54

< 0.79

0.62

< 0.45

< 0.67

< 0.89

< 0.48

< 0.18

0.90

0.75

0.57

0.360.41

0.56

0.94

0.91

0.49

0.97

0.37

0.24

0.83

0.99

0.54

0.79

0.43

0.45

0.67

0.89

0.48

0.18

LOQ EQL Dil.

3.02.5

1.9

1.21.4

1.9

3.1

3.0

1.6

3.2

1.2

0.80

2.8

3.3

1.8

2.6

1.4

1.5

2.2

3.0

1.6

0.60

111

1

11

1

1

1

11

11

1

1

11

1

1

11

1

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Code Anl Date

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

Q 05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

Prep Date: 05/06/04

Prep Method Anl Method

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 826 DB

SW846 826(3B

SW846 826 OB

SW846 826 OB

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 826'

SW846 826I

SW846 826(

SW846 826I

)B

B

)B

)B

SW846 8260B

SW846 826(j)B

SW846 8261

SW846 826;

SWB46 826C

)B

B

B

SW846 826(JBSW846 826<j>B

SW846 826t)B

SW846 8260B

En Chem Inc.Analytical Report Number: 846234

Client : RMT - MADISON

Project Name : LEMBERGER LANDFILL

Project Number : 3453.11

Field ID : STORAGE BLANK

1241 Bellevue StreetGreen Bay, Wl 54302920-469-2436

Matrix Type: WASTEWATER

Collection Date: 05/04/04

Report Date: 06/01/04

Lab Sample Number: 846234-005

VOLATILES - SPECIAL LIST

Analj-te Result

1,1,1-Trichloroethane

1,1-Dichloroethane

1,1-Dichloroethene

1,2-D chloroethane

Benzone

Brom jdichloromethane

Brom jform

Bromorriethane

Carbc n Tetrachlorice

Chloroethane

Chloroform

Chloromethane

cis-1,:!-Dichloroethene

Dichlc rodifluoromethane

Ethyltenzene

Fluorc trichloromethane

Methylene Chloride

Tetrac hloroethene

Toluene

trans- 1 ,2-Dichloroetnene

Tricilnroethene

Vinyl Chloride

< 0.90

< 0.75

< 0.57

< 0.36

< 0.41

< 0.56

< 0.94

< 0.91

< 0.49

< 0.97

< 0.37

< 0.24

< 0.83

< 0.99

< 0.54

< 0.79

< 0.43

< 0.45

< 0.67

< 0.89

< 0.48

< 0.18

LOD

0.90

0.75

0.57

0.36

0.41

0.56

0.94

0.91

0.49

0.97

0.37

0.24

0.83

0.99

0.54

0.79

0.43

0.45

0.67

0.89

0.48

0.18

LOQ EQL Dil.

3.0

2.5

1.9

1.2

1.4

1.9

3.1

3.0

1.6

3.2

1.2

0.80

2.8

3.3

1.8

2.6

1.4

1.5

2.2

3.0

1.6

0.60

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Code An I Date

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

05/06/04

Prep Date: 05/06/04

Prep Method Anl Method

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 82.60B

SW846 826QB

SW846 826CJB

SW846 826QB

SW846 826(|B

SW846 826CJB

SW846 826QB

SW846 8260B

SW846 8260iB

SW846 826qB

SW846 826dB

SW846 8260JB

SW846 8260b

SW846 8260B

SW846 8250B

SW846 8260B