['"ft:) TETRA TECH
April 20, 2016
Mr. Todd Campbell On-Scene Coordinator U.S. Environmental Protection Agency 11201 Renner Boulevard Lenexa, Kansas 66219
Subject: Removal Assessment Report Osage and Walnut Site, Coffeyville, Kansas U.S. EPA Region 7 START 4, Contract No. EP-S7-13-06, Task Order No. 0086 Task Monitor: Todd Campbell, On-Scene Coordinator
Dear Mr. Campbell:
Tetra Tech, Inc. is submitting the attached Removal Assessment Report regarding activities conducted at the Osage and Walnut site in Coffeyville, Kansas. If you have any questions or comments, please contact the Project Manager at (816) 412-1777.
Sincerely,
nny O' Connor ST ART Project Manager
/-;:z?/ Ted Faile, PG, CHMM ST ART Program Manager
Enclosures
cc Debra Dorsey, START Project Officer (cover letter only)
X9025.15.0086.000 415 Oak Street, Kansas City, MO 64106 Tel 816.412.1741 Fax 816.410.1748 www.tetratech.com
REMOVAL ASSESSMENT REPORT
OSAGE AND WALNUT SITE
COFFEYVILLE, MONTGOMERY COUNTY, KANSAS
Superfund Technical Assessment and Response Team (START) 4
Contract No. EP-S7-13-06, Task Order No. 0086
Prepared For:
U.S. Environmental Protection Agency
Region 7
11201 Renner Boulevard
Lenexa, Kansas 66219
April 20, 2016
Prepared By:
Tetra Tech, Inc.
415 Oak Street
Kansas City, Missouri 64106
(816) 412-1741
X9025.15.0086.000 i
CONTENTS
Section Page
1.0 INTRODUCTION ........................................................................................................................... 1
2.0 BACKGROUND INFORMATION ................................................................................................. 3
2.1 THE OSAGE AND WALNUT SITE .................................................................................. 3
2.2 THE COFFEYVILLE RE-CON SITE ................................................................................ 3
2.3 PREVIOUS INVESTIGATIONS ....................................................................................... 4
2.3.1 UST Trust Fund Activities ..................................................................................... 4
2.3.2 Site Reconnaissance and Evaluation ...................................................................... 4
2.3.3 KDHE RCRA Inspection ....................................................................................... 5
2.3.4 Consent Order ........................................................................................................ 5
2.3.5 Comprehensive Investigation ................................................................................. 6
2.3.6 Comprehensive Investigation Addendum .............................................................. 6
2.3.7 Integrated Assessment ............................................................................................ 7
3.0 REMOVAL ASSESSMENT ACTIVITIES ..................................................................................... 8
3.1 CONTAINER INVENTORYING, SAMPLING, AND FIELD SCREENING ................... 8
3.2 DIRECT-PUSH TECHNOLOGY SOIL SAMPLING ........................................................ 9
3.3 SURFACE SOIL SAMPLING .......................................................................................... 13
3.4 RADIOLOGICAL SURVEY ............................................................................................ 14
3.5 QUALITY CONTROL SAMPLING ................................................................................ 15
4.0 ANALYTICAL DATA SUMMARY ............................................................................................ 16
4.1 CONTAINER SAMPLE RESULTS ................................................................................. 16
4.2 DIRECT-PUSH TECHNOLOGY SAMPLE RESULTS .................................................. 16
4.2.1 Borings within the Suspected TCE Source Area .................................................. 17
4.2.2 Borings within the Suspected Petroleum Source Area ......................................... 17
4.2.3 Boring within Suspected Source Area East of Main Re-Con Building ................ 17
4.2.4 Boring within Suspected Source Area Northwest of Main Re-Con Building ...... 17
4.2.5 Boring within Suspected Source Area along West Property Boundary ................ 18
4.3 SURFACE SOIL SAMPLE RESULTS ............................................................................ 18
4.4 QUALITY CONTROL SAMPLE RESULTS ................................................................... 18
5.0 SUMMARY ................................................................................................................................... 20
5.1 REMOVAL CONSIDERATIONS .................................................................................... 20
5.2 PRE-REMEDIAL CONSIDERATIONS .......................................................................... 20
6.0 REFERENCES .............................................................................................................................. 22
X9025.15.0086.000 ii
CONTENTS (Continued)
APPENDICES
Appendix
A FIGURES
B LOG BOOK
C PHOTOGRAPHIC DOCUMENTATION
D CONTAINER SUMMARY TABLE
E BORING LOGS
F CHAIN-OF-CUSTODY FORMS, FIELD SHEETS, AND ANALYTICAL DATA
G ANALYTICAL DATA TABLES
TABLES
Table Page
1 SUMMARY OF DPT SOIL SAMPLES ........................................................................................ 11
2 SUMMARY OF SURFACE SOIL SAMPLES ............................................................................. 13
3 SUMMARY OF RADIOLOGICAL BACKGROUND SURVEY ................................................ 14
4 SUMMARY OF SURFACE SOIL FIELD DUPLICATE DATA
COMPARISON ............................................................................................................................. 19
X9025.15.0086.000 1
1.0 INTRODUCTION
The Tetra Tech, Inc. (Tetra Tech) Superfund Technical Assessment and Response Team (START) was
tasked by the U.S. Environmental Protection Agency (EPA) Region 7 Superfund Division to conduct a
removal assessment at the Osage and Walnut site in Pittsburg, Kansas. The Osage and Walnut site was
identified during quarterly groundwater monitoring of the Miller Brothers Oil Company property (later
referred to as the Osage and Walnut site) supported by the Kansas Petroleum Storage Tank Release Trust
Fund in 2000. During groundwater sample analysis, trichloroethene (TCE) was discovered to be
interfering with analytical detection limits. Subsequent investigations concluded that a release of TCE and
other chlorinated solvents had occurred upgradient of the Miller Brothers Oil Company property, likely
originating from the Coffeyville Re-Con, Inc. facility (Kansas Department of Health and Environment
[KDHE] 2007a). Subsequent investigations identified soil and groundwater contamination on and
downgradient of the Coffeyville Re-Con property (Coffeyville Re-Con site). In addition, numerous
containers of unknown contents were documented on the Coffeyville Re-Con site.
The primary purpose of the removal assessment was to investigate previously documented containers
staged at the Coffeyville Re-Con site to determine hazardous characteristics of their contents. In addition,
the removal assessment was to further investigate two potential source areas of contamination at the
Coffeyville Re-Con site. Removal assessment tasks included, but were not limited to:
Inventorying containers (drums, totes, and other containers) staged at the Coffeyville Re-Con site
to document any label information, estimate quantity of contents, and container condition
Collecting samples from inventoried containers for field screening purposes to document
hazardous characteristics
Collecting subsurface soil samples within suspected source areas by use of a Geoprobe® direct-
push technology (DPT) rig equipped with a Macro-Core sampler
Collecting composite surface soil (0 to 6 inches below ground surface [bgs]) samples at various
locations of suspected contamination at the Osage and Walnut site
Conducting an initial radiation assessment of remaining oil well equipment and surrounding soils
to determine if past operations at the Osage and Walnut site had radiologically impacted site
surfaces.
X9025.15.0086.000 2
The removal assessment proceeded under authority of the Comprehensive Environmental Response,
Compensation, and Liability Act of 1980 (CERCLA) and the Superfund Amendments and Reauthorization
Act of 1986 (SARA).
Danny O’Connor was the START Project Manager for the removal assessment. The EPA On-Scene
Coordinator (OSC) for the project was Todd Campbell.
X9025.15.0086.000 3
2.0 BACKGROUND INFORMATION
Multiple site investigations have determined that the Coffeyville Re-Con facility is the source of
chlorinated solvent contamination first observed in groundwater at the Osage and Walnut site. The
following sections summarize previous activities at both the Osage and Walnut site and Coffeyville
Re-Con site. Removal assessment activities described in this report focused on the Coffeyville Re-Con
site. This section presents information regarding locations and descriptions, operational histories, and
relevant investigation histories of the two sites.
2.1 THE OSAGE AND WALNUT SITE
The Osage and Walnut site is at the intersection of Osage Street and Walnut Street in Coffeyville, Kansas.
Geographic coordinates of the Osage and Walnut site are 37.013167 degrees north and 95.616110 degrees
west. Residential homes border the Osage and Walnut site north and west, and commercial businesses
border the Osage and Walnut site east and south, with the Coffeyville wastewater treatment plant beyond.
The Osage and Walnut site previously hosted Miller Brothers Oil Company, with presence of several on-
site underground storage tanks (UST) and aboveground storage tanks (AST). USTs were discovered
leaking in 1999. As of 2007, on-site structures included an old building, USTs, concrete pads, and a fuel
pump island. Eight monitoring wells were installed at the Osage and Walnut site (five on site and three on
adjacent properties) during site investigative work supported by the Kansas Petroleum Storage Tank
Release Trust Fund.
2.2 THE COFFEYVILLE RE-CON SITE
The Coffeyville Re-Con site is at 2410 Brown Avenue in Coffeyville, Kansas (see Appendix A, Figure 1).
Geographic coordinates of the site are 37.016317 degrees north and 95.618357 degrees west. The
Coffeyville Re-Con site is bounded north and south by open fields, east by residential properties, and west
by an active rail line. Three buildings are on site: the north former Coffeyville Re-Con building, the
central PrimeTime Industrial Painting, LLC (PrimeTime) building, and an eastern office building (KDHE
2013). The Coffeyville Re-Con site is approximately 0.25 mile northwest of the Osage and Walnut site.
The Kansas Oil Refining Company operated at the Coffeyville Re-Con site from the early 1900s until the
1930s. During 1943, ordnance material and rocket motors were manufactured on site by Multiscope
Company, Inc. In addition, the Coffeyville Re-Con site was used as a scrap yard, trucking facility, and for
other manufacturing and storage purposes. Drum refurbishing activities began in the 1950s, and the
Coffeyville Re-Con building was constructed in 1958. Coffeyville Re-Con began drum refurbishing
X9025.15.0086.000 4
operations at the Coffeyville Re-Con site during 1977. Operations ceased in December 2007 with closure
of the facility. PrimeTime operated at the Coffeyville Re-Con site from 2005 to 2007 (KDHE 2013).
2.3 PREVIOUS INVESTIGATIONS
This section summarizes relevant investigations at the Osage and Walnut site and the Coffeyville Re-Con
site.
2.3.1 UST Trust Fund Activities
In March 1999, USTs at the Miller Brothers Oil Company property (Osage and Walnut site) were
discovered leaking. In October 2000, JB Environmental Drilling was contracted to conduct a Limited Site
Assessment (LSA) supported by the Kansas Petroleum Storage Tank Release Trust Fund. The LSA report
recommended regular groundwater monitoring for benzene, toluene, ethylbenzene, and xylenes (BTEX);
1,2-dichloroethane (DCA); naphthalene; methyl tertiary butyl ether (MTBE); and tertiary butyl alcohol
(TBA) (KDHE 2007a). Eight monitoring wells were installed within the general site vicinity to monitor
groundwater contaminants. During groundwater sampling, TCE was discovered interfering with analytical
detections; therefore, subsequent groundwater sampling included TCE and cis-1,2-dichloroethene (DCE)
as analytes. Groundwater sample analytical data indicated TCE and cis-1,2-DCE at concentrations
exceeding their respective EPA Maximum Contaminant Levels (MCL) in multiple monitoring wells.
2.3.2 Site Reconnaissance and Evaluation
During January and April 2007, KDHE conducted a Pre-Comprehensive Environmental Response,
Compensation and Liability Information System (Pre-CERCLIS) Site Reconnaissance and Evaluation
(SRE) at the Osage and Walnut site to determine if a release of TCE had occurred. The SRE was
conducted in two phases—January and April 2007.
During the January sampling event, KDHE collected groundwater samples from eight site monitoring
wells at the Osage and Walnut site. Analytical data indicated that concentrations of TCE; cis-1,2-DCE;
1,1,2-trichloroethane; and 1,2-DCA exceeded their respective EPA MCLs in groundwater samples
collected from multiple site monitoring wells. TCE, the primary contaminant of concern, was detected in
three site monitoring wells at concentrations ranging from 13.1 to 2,400 micrograms per liter (µg/L).
KDHE returned to the site in April 2007 to continue groundwater assessment by focusing on areas
surrounding the Coffeyville Re-Con property, the suspected source. Groundwater samples were collected
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from six Geoprobe® DPT temporary monitoring wells—five installed downgradient and one upgradient of
the Coffeyville Re-Con property. Groundwater samples were collected for analysis via the KDHE Mobile
Laboratory Shimadzu Gas Chromatograph (Mobile Laboratory) and by the Kansas Division of Health and
Environmental Laboratories (DHEL). Mobile laboratory data indicated TCE in three of five samples
collected from downgradient wells at concentrations exceeding the MCL. No detectable TCE was reported
in the sample collected from the upgradient well. DHEL reported similar results, confirming elevated TCE
concentrations downgradient of the Coffeyville Re-Con site.
The SRE identified elevated TCE and cis-1,2-DCE concentrations in groundwater downgradient of the
Coffeyville Re-Con facility. No detectable VOCs were reported in groundwater samples collected
upgradient of the Coffeyville Re-Con facility. KDHE concluded that a release of TCE and other
chlorinated solvents to groundwater had occurred upgradient of the Osage and Walnut site, likely
originating from the Coffeyville Re-Con facility (KDHE 2007a).
2.3.3 KDHE RCRA Inspection
On August 7 and 8, 2007, the KDHE Bureau of Environmental Field Services conducted a Resource
Conservation and Recovery Act (RCRA) Compliance Evaluation Inspection of the Coffeyville Re-Con
facility. The purpose of the inspection was to identify types of wastes generated, points of waste
generation, methods of waste management, and review of relevant documents. The inspection documented
14 violations, and a Notice of Non-Compliance was issued to Coffeyville Re-Con (KDHE 2007b).
2.3.4 Consent Order
In 2008, KDHE and Coffeyville Re-Con entered into a Consent Order (CO) (Case No. 08-E-020). The
CO documented Coffeyville Re-Con’s agreement to prepare and implement a Comprehensive
Investigation/Corrective Action Study (CI/CAS) at its facility. The CO also outlined a work schedule and
required documents.
On October 9, 2008, WSP Environment & Energy (WSP) submitted a CI/CAS work plan on behalf of
Coffeyville Re-Con. The stated purpose of the CI/CAS was to evaluate possible source areas of
KDHE-identified contaminants of concern (COC) at the facility, and potential migration onto the property
from upgradient sources (WSP 2008).
WSP conducted sampling activities at the Coffeyville Re-Con site during January and February 2009.
TCE, cis-1,2-DCE, trans-1,2-DCE, vinyl chloride, total petroleum hydrocarbons (TPH)-gasoline range
X9025.15.0086.000 6
organics (GRO), TPH-diesel range organics (DRO), arsenic, cadmium, chromium, and lead were detected
during the investigation. WSP concluded that the source of contamination was on the Coffeyville Re-Con
site, but likely associated with historical operations prior to Coffeyville Re-Con’s presence on the site
(WSP 2008).
KDHE disagreed with the conclusion and asked Coffeyville Re-Con to conduct further investigation.
Coffeyville Re-Con refused additional assessment and instead reached a settlement with KDHE in
March 2012 (KDHE 2013).
2.3.5 Comprehensive Investigation
Following termination of the CO and subsequent settlement with Coffeyville Re-Con, KDHE conducted a
Comprehensive Investigation (CI) in 2012 at the Coffeyville Re-Con site. CI sampling activities occurred
between October 30 and December 20, 2012. Soil and groundwater samples were collected at and
downgradient of the site to better characterize contaminant distribution.
Analytical data from the 2012 CI indicated presence of TCE and its degradation products at concentrations
exceeding their respective EPA MCLs in groundwater immediately east-southeast of the Coffeyville
Re-Con building. Analytical results indicated migration of chlorinated VOC-contaminated groundwater
through a residential neighborhood downgradient of Coffeyville Re-Con. In addition, TPH results
indicated migration of petroleum-impacted groundwater off site. Elevated lead and arsenic concentrations
in soil were identified near the Coffeyville Re-Con paint booth. KDHE concluded that the Coffeyville Re-
Con facility was the source of VOC, metal, and TPH contamination (KDHE 2013).
2.3.6 Comprehensive Investigation Addendum
Several data gaps were identified in the 2012 CI; therefore, KDHE conducted a Comprehensive
Investigation Addendum (2013 CI) to address data gaps through further sampling at the site. The purposes
of the 2013 CI were to (1) identify and characterize on-site source areas, (2) install groundwater
monitoring wells, and (3) gain additional data to assist in evaluating remedial alternatives (KDHE 2014a).
CI sampling activities from February 28 to November 7, 2013, included collection of soil, groundwater,
and air samples on and downgradient of the Coffeyville Re-Con site. In addition, three groundwater
monitoring wells were installed to monitor contaminant concentrations and plume migration.
Results of the 2013 CI enabled KDHE to conclusively identify the Coffeyville Re-Con site as the source of
VOC contamination. Approximately 5,000 cubic yards of impacted soil was identified near the east
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central portion of the Coffeyville Re-Con site. TCE soil contamination corresponded to nearby elevated
TCE concentrations in groundwater, indicating a TCE source. KDHE recommended long-term
groundwater monitoring to continue assessment of contaminant distribution and degradation.
2.3.7 Integrated Assessment
During September 2014, KDHE conducted an Integrated Assessment (IA) of the Coffeyville Re-Con site
to assess potential releases of hazardous substances. The IA included review of historical information, a
summary of previous analytical data, an evaluation of the site according to Hazard Ranking System (HRS)
guidance, and a compilation of a comprehensive target survey.
KDHE recommended a removal action to remove drums and contaminated soil that had released or may
pose a threat of release of hazardous substances, pollutants, and contaminants to soil, air, surface water,
and adjacent residences. Following completion of a removal action, KDHE recommended completion of a
Site Inspection to fully evaluate potential pathways (KDHE 2014b).
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3.0 REMOVAL ASSESSMENT ACTIVITIES
START Members (SM) Joann Jeplawy, Adam Watkins, Cosmo Canacari, and Tommy Rebecchi
conducted removal assessment field activities January 25 to 27, 2016. Activities included (1) a
determination of hazardous characteristics of contents of on-site containers (drums, totes, and other
containers), (2) an assessment of subsurface soil to determine presence of contaminant source areas, (3) an
assessment of metal concentrations in surface soil and surface wastes at the site, (4) and a radiological
survey of former oil-well equipment and surrounding soils. Removal assessment activities accorded with
the approved Quality Assurance Project Plan (QAPP) dated January 20, 2016. Field activities were
documented in a logbook (see Appendix B). Site conditions were documented in a photographic log
included as Appendix C. A site layout map is provided as Figure 2 in Appendix A. The following
sections detail field activities.
3.1 CONTAINER INVENTORYING, SAMPLING, AND FIELD SCREENING
On January 12, 2016, EPA and Tetra Tech START conducted an initial site reconnaissance to determine
locations and quantities of containers (drums, totes, and other containers) at the Re-Con site. Containers
were documented at the following locations: the main Re-Con building, near the west property boundary,
north of the main Re-Con building, and near the PrimeTime building and office.
Crews returned on January 25, 2016, to complete a container inventory and collect field screening samples.
During the inventory, each container received a unique identification number, and the container location
was documented (see Appendix A, Figure 3). The following container information was documented
during container inventorying: size, composition, color, estimated volume of contents, and any label
information (see Appendix D). A total of 150 containers were inventoried during the removal assessment.
After completion of inventorying, START personnel opened each container and documented measurable
volatile organics in container headspace by use of a hand-held photoionization detector (PID). Field
personnel then attempted to collect a representative sample (field screening sample) from containers using
disposable thieving rods (liquids/sludges), disposable coliwasas (liquids/sludges), or hand trowels (solids).
Thieving rods and coliwasas were disposed of after sampling each container to avoid cross-contamination.
Hand trowels were decontaminated after investigation of each container via brush and washing with non-
phosphate detergent solution, followed by a rinsing with deionized water. Field screening samples were
collected directly into 40-milliliter (mL) vials (liquids) or 8-ounce glass jars (solids and sludges). When
multiple containers with similar contents were encountered, a subset of the similar containers was sampled
to represent the entire group’s contents. The majority of similar containers observed during the removal
X9025.15.0086.000 9
assessment were filled with “overspray material,” an assumed byproduct of drum refurbishing practices. A
total of 86 field screening samples were collected from the 150 inventoried containers.
Field screening samples were tested following HazCat® Chemical Identification System procedures to
determine if container contents were explosive, water reactive, water soluble, corrosive, an oxidizer, a
sulfide, flammable, a halide, or a cyanide. Results from testing field screening samples were as follows:
24 samples identified as flammable, 18 samples identified as combustible, and 1 sample identified as
corrosive. The remaining 43 samples did not exhibit any hazardous characteristics. Results are
summarized in Appendix D.
Because a significant number of identified containers were filled with “overspray material,” a composite
sample was collected from remnants of field screening samples and submitted to the EPA Region 7
laboratory under Analytical Service Request (ASR) #7077 for analyses for total Resource Conservation
and Recovery Act (RCRA) metals via Standard Operating Procedure (SOP) 3122.03, and for toxicity
characteristic leaching procedure (TCLP) RCRA metals via SOP 3171.01. The samples were delivered on
February 17, 2016. Section 4.1 discusses results of these analyses.
3.2 DIRECT-PUSH TECHNOLOGY SOIL SAMPLING
To further evaluate multiple potential contaminant source areas at the Coffeyville Re-Con site, subsurface
soil samples were collected by use of a Geoprobe® DPT rig. Subsurface soil sampling focused on two
primary potential source areas—a suspected TCE source area north of the site office building and a
suspected petroleum source area near the formerly operating oil well. Additional borings were advanced in
areas of surface staining near the main Re-Con building (see Appendix A, Figure 4).
At the first boring location (GP-1), a continuous boring was advanced to 24 feet bgs to characterize soils
all the way into the saturated zone. All remaining borings were advanced to 8 feet bgs, approximately the
top of the water table. Continuous borings were advanced by use of a Geoprobe® DPT rig equipped with a
Macro-Core sampler. Upon retrieving borings, Tetra Tech screened soils for measurable VOCs by use of a
hand-held PID. Tetra Tech documented PID readings, any observed staining, and soil lithology in boring
logs (see Appendix E). The two 1-foot boring intervals with the highest observed PID readings or most
noticeable visual anomalies were selected for sampling. If no visual anomalies or elevated PID readings
were observed, field team members sampled at default depths: one sample collected within the 7- to 8-foot
bgs interval, and an additional sample collected within the uppermost 4 feet of the boring.
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Within each sampling interval, soil samples for analysis for VOCs were collected first according to EPA
Method 5035 guidelines. The remaining soil (see Table 1 for list of analyses) was then transferred to
appropriate sample containers. Pertinent information, including analysis to be performed and exact sample
locations, was recorded on field sheets for each sample (see Appendix F). All soil samples were stored in
coolers maintained at or below 4 degrees Celsius (C) pending submittal to the EPA Region 7 laboratory in
Kansas City, Kansas under ASR #7041. DPT soil sample analysis varied depending on the location of the
boring. Table 1 summarizes DPT soil samples and corresponding laboratory analyses.
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TABLE 1
SUMMARY OF DPT SOIL SAMPLES
OSAGE AND WALNUT SITE, COFFEYVILLE, KANSAS
Sample Name Sample
Description
Latitude
(°N)
Longitude
(°W)
Collection
Date
Collection
Time
Laboratory
Sample ID
Laboratory Analysis
VOCs via
SOP 3230.16
Cyanide via
SOP 3135.02
TPH-GRO via
SOP 3230.19
TPH-DRO/ORO
via SOP 3270.01
GP-1 (1-2)
Within
suspected
TCE source
area
37.01626 95.61806 1/25/2016 1505 7041-101 X X
GP-1 (3-4) 1/25/2016 1505 7041-102 X X
GP-2 (1-2) 37.01625 95.61800
1/25/2016 1615 7041-103 X X
GP-2 (7-8) 1/25/2016 1625 7041-104 X X
GP-3 (1-2) 37.01623 95.61790
1/26/2016 0815 7041-105 X X
GP-3 (7-8) 1/26/2016 0820 7041-106 X X
GP-4 (1-2) 37.01614 95.61806
1/26/2016 0851 7041-107 X X
GP-4 (7-8) 1/26/2016 0900 7041-108 X X
GP-5 (1-2)
37.01613 95.61798
1/26/2016 0937 7041-109 X X
GP-5 (7-8) 1/26/2016 0950 7041-110 X X
GP-5 (7-8) FD 1/26/2016 0950 7041-110 FD X X
GP-6 (2-3) 37.01616 95.61788
1/26/2016 1028 7041-111 X X
GP-6 (7-8) 1/26/2016 1037 7041-112 X X
GP-7 (3-4) 37.01607 95.61806
1/26/2016 1102 7041-113 X X
GP-7 (7-8) 1/26/2016 1110 7041-114 X X
GP-8 (3-4) 37.01606 95.61794
1/26/2016 1130 7041-115 X X
GP-8 (7-8) 1/26/2016 1138 7041-116 X X
GP-9 (3-4) 37.01607 95.61784
1/26/2016 1159 7041-117 X X
GP-9 (7-8) 1/26/2016 1207 7041-118 X X
GP-10 (3-4) Within
suspected
TPH source
area
37.01468 95.61868 1/26/2016 1340 7041-119 X X
GP-10 (3-4) 1/26/2016 1340 7041-201 X X
GP-11 (3-4) 37.01469 95.61848
1/26/2016 1420 7041-120 X X
GP-11 (3-4) 1/26/2016 1420 7041-202 X X
GP-12 (3-4) East of
main
Re-Con
building
37.01707 95.61816
1/26/2016 1454 7041-121 X X
GP-12 (3-4) 1/26/2016 1454 7041-203 X X
GP-12 (7-8) 1/26/2016 1458 7041-122 X X
TABLE 1 (Continued)
SUMMARY OF DPT SOIL SAMPLES
OSAGE AND WALNUT SITE, COFFEYVILLE, KANSAS
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Sample Name Sample
Description
Latitude
(°N)
Longitude
(°W)
Collection
Date
Collection
Time
Laboratory
Sample ID
Laboratory Analysis
VOCs via
SOP 3230.16
Cyanide via
SOP 3135.02
TPH-GRO via
SOP 3230.19
TPH-DRO/ORO
via SOP 3270.01
GP-13 (2-3) Northwest
of main
Re-Con
building
37.01715 95.61892
1/26/2016 1540 7041-123 X X
GP-13 (7-8) 1/26/2016 1547 7041-124 X X
GP-14 (3-4) Along west
property
boundary
37.01758 95.61891 1/26/2016 1600 7041-125 X X
GP-14 (7-8) 1/26/2016 1605 7041-126 X X
Notes:
°N Degrees North
°W Degrees West
DRO/ORO Diesel-range organics/oil-range organics
FD Field duplicate
GRO Gasoline-range organics
ID Identification
SOP Standard Operating Procedure
TCE Trichloroethene
TPH Total petroleum hydrocarbons
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3.3 SURFACE SOIL SAMPLING
Composite surface soil samples were collected at various locations at the Re-Con site to determine impact
from historical site operations. Sampling locations are depicted on Figure 4 (see Appendix A) and
summarized in Table 2. Composite sampling proceeded first by defining a sampling area, known as a
decision unit (DU). Then within each DU, nine aliquots of approximate equal volume were collected by
use of a hand trowel. Field team members identified locations within each DU for collection of aliquots
according to a simple random sampling pattern. The composite samples were collected into labeled 8-
ounce glass jars for analysis of RCRA metals. The hand trowel was decontaminated after sampling within
each DU. Pertinent information, including analyses to be performed and sample locations, were recorded
on field sheets for each sample (see Appendix F). All soil samples were stored in coolers maintained at or
below 4 C pending submittal to the EPA Region 7 laboratory in Kansas City, Kansas, under ASR #7041
for analysis for RCRA metals via SOP 3122.03.
TABLE 2
SUMMARY OF SURFACE SOIL SAMPLES
OSAGE AND WALNUT SITE, COFFEYVILLE, KANSAS
Sample
Name Sample Description
Sample Location* Laboratory
Sample ID Latitude °N Longitude °W
DU-1 Soil staining east of main Re-Con building 37.016884 95.618081 7041-1
DU-2 North exterior of main Re-Con building, near
paint booth 37.017336 95.618499
7041-2
7041-2FD
DU-3 West of main Re-Con building 37.017049 95.018820 7041-3
DU-4 Waste material covering floor of main Re-Con
building 37.017006 95.618749 7041-4
DU-5 West of PrimeTime shop 37.016048 95.618863 7041-5
DU-6 South of PrimeTime shop 37.015749 95.618417 7041-6
DU-7 Near oil well 37.014789 95.618481 7041-7
Notes:
* Represents a central point within each decision unit
°N Degrees North
°W Degrees West
FD Field Duplicate
ID Identification
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3.4 RADIOLOGICAL SURVEY
On January 26, 2016, Tetra Tech START conducted an initial radiation assessment at the Coffeyville Re-
Con site to determine if past site operations had radiologically impacted site surfaces. The initial
assessment included a survey of remaining oil-well equipment and surrounding soils by use of a Ludlum
Model 2221 ratemeter with a Ludlum Model 44-20 sodium iodide (NaI) scintillation detector (detector).
To ensure proper functioning of the ratemeter and detector, a source check occurred prior to the survey by
use of a cesium-137 check source. The source check confirmed that the instruments were functioning
properly. To establish background radiation levels in the site area for comparative purposes, SMs selected
three areas (background location) with no suspected previous radiological impact. At each background
location, the ratemeter was set to scaler mode, and a 1-minute count time was initiated. The resulting
reading was in units of counts per minute (cpm). Background survey results are summarized in Table 3.
TABLE 3
SUMMARY OF RADIOLOGICAL BACKGROUND SURVEY
OSAGE AND WALNUT SITE, COFFEYVILLE, KANSAS
Location Description Latitude
(°N)
Longitude
(°W)
Reading
(cpm)
Grace Park 37.01969 95.61742 26,000
Alley east of the site 37.01720 95.61759 24,000
Near Osage Street 37.01309 95.61871 24,000
Notes:
°N Degrees North
°W Degrees West
cpm Counts per minute
The survey at the Coffeyville Re-Con site focused on remaining oil-well equipment and surrounding soils.
During the initial soil survey, the surveyor walked in a forward direction at 1 to 2 feet per second while
swinging the detector back and forth approximately 6 inches above the ground—generally covering a
serpentine pattern over the ground surface. Surfaces of remaining oil-well equipment were scanned by
moving the detector in a serpentine pattern 1 to 2 inches above each surface. Survey readings from soil
and oil-well equipment ranged from 18,000 to 31,000 cpm, comparable to readings at the three
background locations. No abnormal readings, such as concentrated areas of elevated readings, were
documented during the radiological survey.
X9025.15.0086.000 15
3.5 QUALITY CONTROL SAMPLING
Quality control (QC) samples for the removal assessment included two field duplicates—one collected
during DPT soil sampling and the other collected during surface soil sampling. Field duplicates were
collected to assess precision of analytical and sampling methods.
X9025.15.0086.000 16
4.0 ANALYTICAL DATA SUMMARY
This section summarizes analytical data from the removal assessment in January 2016. Soil samples were
delivered in two batches to the EPA Region 7—the first on January 27 (ASR #7041) and the second on
February 17, 2016 (ASR #7077). Sample field sheets, chain-of-custody records, and laboratory data are in
Appendix F. Analytical data are summarized in tabular form in Appendix G.
4.1 CONTAINER SAMPLE RESULTS
One composite sample from containers of “overspray material” was submitted to the EPA Region 7
laboratory under ASR #7077 for analyses for total RCRA metals via SOP 3122.03 and TCLP RCRA
metals via SOP 3171.01. Analytical data from RCRA metals analysis were compared to EPA Regional
Screening Levels (RSL) for industrial soil and to KDHE Tier 2 risk-based soil pathway benchmarks for
non-residential scenarios. Analytical data from TCLP analysis were compared to regulatory levels
specified in 40 Code of Federal Regulations Section 261.24. Review of analytical data indicated the
following:
The RCRA metals mercury, barium, cadmium, chromium, lead, selenium, and silver were detected
in the sample. No analyte concentration exceeded a comparative benchmark. Arsenic was not
detected in the sample; however, the reported detection limit of 5.10 milligrams per kilogram
(mg/kg) exceeded the EPA RSL for industrial soil of 3.00 mg/kg.
TCLP results indicated detections of the metals barium and selenium. Reported concentrations of
these analytes did not exceed their regulatory limits. TCLP results indicated that the overspray
material did not exhibit characteristics of toxicity specified in 40 CFR Section 261.24.
Analytical data from the overspray material are summarized in Appendix G, Table G-1.
4.2 DIRECT-PUSH TECHNOLOGY SAMPLE RESULTS
A total of 30 subsurface soil samples (including one field duplicate) were collected from 14 DPT borings
within five areas of suspected contamination during the removal assessment (see Appendix A, Figure 4).
Subsurface soil analytical data were compared to EPA RSLs for industrial soil and to KDHE Tier 2 risk-
based soil pathway benchmarks for non-residential scenarios. Subsurface soil sample analytical data are
summarized in Appendix G, Table G-2. The following subsections summarize analytical data from each
of the five suspected source areas.
X9025.15.0086.000 17
4.2.1 Borings within the Suspected TCE Source Area
Nineteen soil samples (including one field duplicate) were collected from nine borings (samples GP-1
through GP-9) advanced near the suspected TCE source at the Coffeyville Re-Con site. Samples were
analyzed for VOCs via SOP 3230.16 and cyanide via SOP 3135.02. Analytical data indicated presence in
one or more samples at concentrations above the reporting limit of the VOCs 1,1-DCA, acetone, benzene,
cis-1,2-DCE, cyclohexane, ethylbenzene, isopropylbenzene, xylene (m- and/or p-), MTBE,
methylcyclohexane, o-xylene, toluene, and vinyl chloride. No reported analyte concentration exceeded a
comparative benchmark. TCE and cyanide were not detected in any of the samples.
4.2.2 Borings within the Suspected Petroleum Source Area
Four soil samples were collected from two borings (GP-10 and GP-11) advanced near the suspected
petroleum source at the Coffeyville Re-Con site. Sample analyses included VOCs via SOP 3230.16,
cyanide via SOP 3135.02, TPH-GRO via SOP 3230.19, and TPH-DRO/ORO via SOP 3270.01. No
analytes were detected in the four samples.
4.2.3 Boring within Suspected Source Area East of Main Re-Con Building
Three soil samples were collected from one boring (GP-12) advanced within an area of soil staining east of
the main Re-Con building. Sample analyses included VOCs via SOP 3230.16, cyanide via SOP 3135.02,
TPH-GRO via SOP 3230.19, and TPH-DRO/ORO via SOP 3270.01. Analytical data indicated presence
above detection limits of the VOCs 1,1-DCA, acetone, chloroethane, and cis-1,2-DCE. TPH-DRO and
TPH-ORO also were reported above detection limits. No reported analyte concentration exceeded a
benchmark value. Cyanide was not detected in any of the samples.
4.2.4 Boring within Suspected Source Area Northwest of Main Re-Con Building
Two soil samples were collected from one boring (GP-13) advanced within an area of soil staining
northwest of the main Re-Con building. Soil samples were analyzed for VOCs via SOP 3230.16 and
cyanide via SOP 3135.02. Analytical data indicated presence of the VOC acetone above detection limits
but below comparative benchmarks.
X9025.15.0086.000 18
4.2.5 Boring within Suspected Source Area along West Property Boundary
Two soil samples were collected from one boring (GP-14) advanced within an area of soil staining near the
west property boundary. Soil samples were analyzed for VOCs via SOP 3230.16 and cyanide via SOP
3135.02. No analytes were detected in the two samples.
4.3 SURFACE SOIL SAMPLE RESULTS
A total of eight surface soil samples (including one field duplicate) were collected at various areas across
the Re-Con site. Surface soil samples were analyzed for total RCRA metals via SOP 3122.3. Surface soil
analytical data were compared to EPA RSLs for industrial soil and KDHE Tier 2 risk-based soil pathway
benchmarks for non-residential scenarios. In addition, detections were compared to U.S. Geological
Survey (USGS)-reported background concentrations in Montgomery County (USGS 2016). Surface soil
sample data are summarized in Appendix G, Table G-3.
Review of analytical data indicated detections of the metals mercury, arsenic, barium, cadmium,
chromium, and lead in one or more surface soil samples. Detected concentrations of mercury, barium,
cadmium, and lead did not exceed comparative benchmarks. Arsenic and chromium exceeded
comparative benchmarks as described below:
Arsenic was detected in all eight samples at concentrations ranging from 1.5 to 256 mg/kg,
exceeding the EPA RSL for industrial soil (3.0 mg/kg) in four samples and the KDHE Tier 2
benchmark (63.2 mg/kg) in one sample. Seven of the eight reported arsenic detections were
similar to the USGS reported average background concentration in Montgomery County of
7.94 mg/kg. The composite sample collected at DU-4, waste covering the floor of the main Re-
Con building, contained arsenic at 256 mg/kg, exceeding the EPA RSL for industrial soil and the
KDHE Tier 2 benchmark for non-residential scenarios.
Total chromium was detected in all eight samples at concentrations ranging from 7.1 to 197
mg/kg. The composite sample collected at DU-4, waste covering the floor of the main Re-Con
building, contained total chromium at 197 mg/kg, exceeding the KDHE Tier 2 benchmark for
non-residential scenarios. Further examination of KDHE’s Tier 2 Risk-Based Standards for
Kansas (RSK) values for chromium revealed that Tier 2 RSK values listed in the KDHE RSK
Manual for total chromium are based on toxicity data relevant to hexavalent chromium (the more
toxic form of chromium) (KDHE 2010). Further analysis of this DU may be warranted to assess
presence and quantity of hexavalent chromium.
4.4 QUALITY CONTROL SAMPLE RESULTS
QC sampling for this removal assessment included collection of two field duplicates. One field duplicate
was collected within the 7- to 8-foot bgs interval at DPT boring GP-5. The sample was analyzed for VOCs
X9025.15.0086.000 19
and cyanide. Analytical data indicated no analyte detections in either the field duplicate sample or the
original sample. The second field duplicate was collected at DU-2 and analyzed for RCRA metals. The
metals arsenic, barium, cadmium, chromium, and lead were detected in both the field duplicate sample and
the original sample. Table 4 summarizes surface soil field duplicate data.
TABLE 4
SUMMARY OF SURFACE SOIL FIELD DUPLICATE DATA COMPARISON
OSAGE AND WALNUT, COFFEYVILLE, KANSAS
Sample
Name
Laboratory
Sample ID
Analyte and Result
Arsenic Barium Cadmium Chromium Lead
DU-2 7041-2 1.50 30.3 0.690 14.2 141
7041-2FD 2.60 63.0 0.95 12.0 77.1
Average 2.05 46.7 0.82 13.1 109
RPD 53.7% 70.1% 31.7% 16.8% 58.6%
Notes:
All results reported as milligrams per kilogram
% Percent
DU Decision unit
FD Field duplicate
ID Identification
RPD Relative percent difference
Large variations reported in sample results for arsenic, barium, and lead likely indicate high heterogeneity
in DU-2. Reported concentrations do not exceed applicable benchmarks; therefore, reported contaminant
concentration variance does not impact project decision making.
X9025.15.0086.000 20
5.0 SUMMARY
Tetra Tech START was tasked by EPA Region 7 to conduct a removal assessment at the Osage and
Walnut site in Coffeyville, Kansas. The site previously hosted Miller Brothers Oil Company, with
presence of several on-site USTs and ASTs. Site groundwater was found contaminated with TCE during
tank closure sampling activities. Subsequent investigations determined the source of groundwater
contamination was the Coffeyville Re-Con site located northwest of the Osage and Walnut site.
Investigations documented presence of containers of unknown contents and several areas of suspected soil
contamination.
The primary purposes of this removal assessment were to (1) investigate containers staged at the site to
determine hazardous characteristics of their contents, (2) further investigate potential contaminant source
areas, and (3) investigate oil well equipment and surrounding soils to determine if they had been
radiologically impacted from historical site operations. Removal assessment activities focused on the
Coffeyville Re-Con site. The following sections discuss removal and pre-remedial considerations.
5.1 REMOVAL CONSIDERATIONS
Based on information obtained during the removal assessment, a removal action may be warranted to
address (1) containers identified as holding hazardous contents, and (2) waste covering the main Re-Con
building floor found to contain elevated concentrations of arsenic and total chromium.
Of the 150 containers inventoried during the removal assessment, 24 were identified as having flammable
contents, 18 were identified as having combustible contents, and 1 was identified as having corrosive
contents. Analytical data from DU-4, representing waste covering the floor of the main Re-Con building,
indicated presence of arsenic at 256 mg/kg and chromium at 197 mg/kg. These concentrations exceeded
comparative benchmarks.
5.2 PRE-REMEDIAL CONSIDERATIONS
Previous investigations by KDHE had identified groundwater contamination in the form of chlorinated
solvents at the site. The plume begins near the PrimeTime office building and continues southeast
(downgradient) through a residential neighborhood. The distal end of the plume is southeast of the Osage
and Walnut site near agricultural land. Previous vapor intrusion investigations in the residential
neighborhood had found no impact on indoor air quality. Drinking water for the area surrounding the
Osage and Walnut site is provided by the City of Coffeyville. Coffeyville obtains drinking water from the
X9025.15.0086.000 21
Verdigris River near Pfister Park, more than 3 miles upstream from the Osage and Walnut site. Based on
this information, no further pre-remedial considerations appear warranted at this time.
X9025.15.0086.000 22
6.0 REFERENCES
Kansas Department of Health and Environment (KDHE).
2007a. Site Reconnaissance and Evaluation. Osage and Walnut Site. May.
2007b. RCRA Compliance Evaluation Inspection Summary. August.
2010. Risk-Based Standards for Kansas, RSK Manual – 5th Version. October.
2013. Comprehensive Investigation. Coffeyville Re-Con Site. February 25.
2014a. Comprehensive Investigation Addendum. Coffeyville Re-Con Site. March 3.
2014b. Integrated Assessment. Coffeyville Re-Con Site. September 16.
WSP Environment & Energy (WSP). 2008. Comprehensive Investigation/Corrective Action Study
(CI/CAS) Work Plan. Coffeyville Re-Con, Inc. October 9.
U.S. Geological Survey (USGS). 2016. Average Concentrations of Elements in Montgomery County,
Kansas.
APPENDIX A
FIGURES
_̂
Source: USGS Coffeyville East, KS 7.5 Minute Topo Quads, 2016 USGS Coffeyville West, KS 7.5 Minute Topo Quad, 2016 USGS Elliot, OK 7.5 Minute Topo Quad, 2013 USGS South Coffeyville, OK 7.5 Minute Topo Quad, 2013X:\
G\90
25\00
86\Pr
ojects
\mxd
\Figu
re1.m
xd
Osage & Walnut SiteCoffeyville, Kansas
Date: 1/19/2016 Drawn By: Gustavo Orozco Project No: X9025.15.0086.000
Figure 1Site Location Map
Approximate Site Location
±0 2,000 4,000
Feet
Montgomery County
PrimeTime Office
Walnu
t St
Coffeyville Re-Con Site Boundaries
Main Re-Con Building
Osage and Walnut Site Boundaries
PrimeTime Shop
£¤169Wi
llow
St
Brow
n St
Osage St
Polk St
W John St
Madison St
W Adams St
W Jackson St
W Jefferson St E Jefferson St
E John St
W Jefferson St
Source: ESRI ArcGIS Online Maps, World Imagery, 2014X:\G\
9025
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ects\
mxd\F
igure2
_040
716.m
xd
Osage & Walnut SiteCoffeyville, Kansas
Date: 4/11/2016 Drawn By: Clayton Hayes Project No: X9025.15.0086.000
Figure 2Site Layout Map±0 150 300
Feet
Legend!O Former oil well
Approximate site boundarySuspected petroleum source areaSuspected TCE source area
TCE Trichloroethene
Containers #131-134Container #135
Container #148Container #149
Container #150
Container #147
Container #143
W John St
Walnu
t St
PrimeTime Office
Containers #1-27Containers #33-42
Containers #43-128Containers #136-140
Containers #29-32
Containers #144-146
Container #28
Containers #141 and 142Containers #129 and 130
£¤169
Willo
w St Br
own S
t
Osage St
Polk St
Madison St
W Adams St
W Jackson St
W Jefferson St
Coffeyville Re-Con Site Boundaries
Main Re-Con Building
PrimeTime Shop
Source: ESRI ArcGIS Online Maps, World Imagery, 2014X:\G\
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ects\
mxd\F
igure3
.mxd
Osage & Walnut SiteCoffeyville, Kansas
Date: 4/11/2016 Drawn By: Clayton Hayes Project No: X9025.15.0086.000
Figure 3Container Inventory Summary Map±0 125 250
Feet
LegendApproximate site boundaryContainer location
W Jefferson St
Walnu
t St
Location #3
Location #2
Location #1
DU-4
DU-6
DU-1
DU-2
DU-7
DU-5
DU-3
Coffeyville Re-Con Site Boundaries
Main Re-Con Building
PrimeTime Shop
GP-14
GP-13GP-12
GP-11GP-10
£¤169
Brow
n St
Osage St
Willo
w St
Polk St
W John St
Grace Blvd
Madison St
E Jefferson St
W Adams St
W Jackson St
E John St
Source: ESRI ArcGIS Online Maps, World Imagery, 2014X:\G\
9025
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ects\
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igure4
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Osage & Walnut SiteCoffeyville, Kansas
Date: 4/11/2016 Drawn By: Clayton Hayes Project No: X9025.15.0086.000
Figure 4Sample Summary Map±0 150 300
Feet
Legend"J" Background radiation survey location!( DPT soil boring location
Approximate site boundaryComposite surface soil sample location
DPTDU
Direct-push technologyDecision unit
!( !(!(
!( !(!(
!( !( !(
Brow
n St
Polk St
GP-9
GP-8
GP-7
GP-6GP-5GP-4
GP-3GP-2GP-1
PrimeTime Office
InsetScale: 1" = 80'
APPENDIX B
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APPENDIX C
PHOTOGRAPHIC DOCUMENTATION
Osage and Walnut Site
Coffeyville, Kansas
1
TETRA TECH
PROJECT NO.
103X9025150086
DESCRIPTION
This photograph shows the main Re-Con building at the
Coffeyville Re-Con, Inc. facility (Coffeyville Re-Con site).
The building, not currently in use, was previously utilized for
drum refurbishing.
1
CLIENT U.S. Environmental Protection Agency Region 7 Date
Direction: South PHOTOGRAPHER Joann Jeplawy 1/12/2016
TETRA TECH
PROJECT NO.
103X9025150086
DESCRIPTIONThis photograph shows the interior of the main Re-Con
building. 2
CLIENT U.S. Environmental Protection Agency Region 7 Date
Direction: East PHOTOGRAPHER Joann Jeplawy 1/12/2016
Osage and Walnut Site
Coffeyville, Kansas
2
TETRA TECH
PROJECT NO.
103X9025150086
DESCRIPTIONThis photograph shows the PrimeTime Industrial Painting,
LLC (PrimeTime) shop located centrally on the property. 3
CLIENT U.S. Environmental Protection Agency Region 7 Date
Direction: Northwest PHOTOGRAPHER Joann Jeplawy 1/12/2016
TETRA TECH
PROJECT NO.
103X9025150086
DESCRIPTION This photograph shows the PrimeTime office building. 4
CLIENT U.S. Environmental Protection Agency Region 7 Date
Direction: East PHOTOGRAPHER Joann Jeplawy 1/12/2016
Osage and Walnut Site
Coffeyville, Kansas
3
TETRA TECH
PROJECT NO.
103X9025150086
DESCRIPTIONThis photograph shows the former oil well and related
equipment at the Coffeyville Re-Con site. 5
CLIENT U.S. Environmental Protection Agency Region 7 Date
Direction: North PHOTOGRAPHER Joann Jeplawy 1/12/2016
TETRA TECH
PROJECT NO.
103X9025150086
DESCRIPTIONThis photograph shows the qualitative radiological survey of
soils surrounding the former oil well and related equipment.6
CLIENT U.S. Environmental Protection Agency Region 7 Date
Direction: West PHOTOGRAPHER Cosmo Canacari 1/26/2016
Osage and Walnut Site
Coffeyville, Kansas
4
TETRA TECH
PROJECT NO.
103X9025150086
DESCRIPTION
This photograph shows stained soil near the west property
boundary. Subsurface soil sampling was conducted in this
area to determine presence of contaminants.
7
CLIENT U.S. Environmental Protection Agency Region 7 Date
Direction: NA PHOTOGRAPHER Joann Jeplawy 1/12/2016
TETRA TECH
PROJECT NO.
103X9025150086
DESCRIPTION
This photograph shows a truck-mounted direct-push
technology (DPT) rig conducting subsurface soil sampling in
the vicinity of the main Re-Con building.
8
CLIENT U.S. Environmental Protection Agency Region 7 Date
Direction: North PHOTOGRAPHER Joann Jeplawy 1/26/2016
Osage and Walnut Site
Coffeyville, Kansas
5
TETRA TECH
PROJECT NO.
103X9025150086
DESCRIPTION
This photograph shows three oil-water separators northeast of
the main Re-Con building. Samples were collected from each
of the containers and field tested to determine hazardous
characteristics.
9
CLIENT U.S. Environmental Protection Agency Region 7 Date
Direction: North PHOTOGRAPHER Tommy Rebecchi 1/25/2016
TETRA TECH
PROJECT NO.
103X9025150086
DESCRIPTION
This photograph shows drums staged west of the main Re-
Con building. During the removal assessment, containers
were inventoried and subsequently sampled to determine if
contents were hazardous.
10
CLIENT U.S. Environmental Protection Agency Region 7 Date
Direction: West PHOTOGRAPHER Joann Jeplawy 1/12/2016
APPENDIX D
CONTAINER SUMMARY TABLE
CONTAINER SUMMARY TABLE
Container
ID #
Size
(gallons)Container Type Color
Estimated
Content
Amount
Material
State
PID Reading
(ppm)
Sample
Collected
(Y/N)
Explosive
(Y/N)
Water
Reactive
(Y/N)
Water
Soluble
(Dissolves,
Floats, Sinks)
pHOxidizer
(Y/N)
Sulfide
(Y/N)
Flammable
(Y/N)
Halide
(Y/N)
Cyanide
(Y/N)Comments
1 5 Paint Can/Bucket White 25% Sludge 880 Yes No No Dissolves NT NT NT Yes NT NT Industrial Finishes, satin black paint
2 5 Paint Can/Bucket Gray 100% Sludge 0 Yes No No Floats 5 No No Yes NT No Sherwin Williams Industrial Enamel
3 5 Paint Can/Bucket Rust 100% Sludge 49 Yes No No Floats 5 No No Yes NT No
4 5 Paint Can/Bucket Black 100% Sludge 849 Yes No No Floats 5 No No Yes NT No Industrial Finishes, 1346 Buff Primer
5 5 Paint Can/Bucket Black 100% Sludge 111 Yes No No Floats 5 No No Yes NT No
6 5 Paint Can/Bucket Rust 100% Sludge 36 Yes No No Floats 5 No No Yes NT No
7 5 Paint Can/Bucket White 100% Sludge 192 Yes No No Dissolves 5 No No Yes NT No Primer
8 5 Paint Can/Bucket White 100% Sludge 298 Yes No No Dissolves 5 No No Yes NT No Valspar, Black Urethane Primer
9 5 Paint Can/Bucket Gray 25% Sludge 182 Yes No No Floats 5 No No Yes NT No
10 5 Paint Can/Bucket Gray 75% Sludge 243 Yes No No Floats NT NT NT Yes NT NT
11 5 Paint Can/Bucket White 75% Sludge 656 Yes No No Floats NT NT NT Yes NT NT Industrial Finishes, DTM Enamel
12 5 Paint Can/Bucket Rust 75% Solid 225 No - - - - - - - - -Sherwin Williams Lacquer Thinner. Product was hardened and no sample was
collected
13 55 Drum Black 25% Solid 46.6 No - - - - - - - - - Crown Paint, Red Oxide Primer. Unable to collect sample
14 55 Drum Rust 50% Solid 25.5 Yes No No Dissolves 5 No No No NT No Overspray Material
15 5 Bucket Grey 25% Sludge 0 Yes No No Floats 3 No No Yes NT No
16 55 Drum Red 50% Solid 28.4 Yes No No Dissolves 5 No No No NT No Overspray Material
17 55 Drum Black 25% Sludge 171 Yes No No Dissolves 4 No No Yes NT No Primer
18 5 Bucket Black 100% Sludge 1460 Yes No No Floats NT NT NT Yes NT NT Carbit, White Booth Coating
19 5 Bucket Grey 100% Liquid 97 Yes No No Floats 5 No No Yes NT No Rich Paint Manufacturing, Ford Light Gray
20 5 Bucket Grey 25% Sludge 21 Yes No No Dissolves 8 No No No NT No Sherwin Williams, A-100 Exterior Satin Latex
21 5 Bucket Black 100% Liquid 0 Yes No No Floats 6 No No Combustible NT No Conoco, Hydraulic AW 46
22 1 Paint Can Grey 100% Liquid 43.9 Yes No No Floats 5 No No Yes NT No Unmarked paint can
23 1 Paint Can Grey 100% Liquid 254 Yes No No Floats 5 No No Yes NT No Unmarked paint can
24 1 Paint Can Rust 75% Liquid 5.5 Yes No No Floats 5 No No Yes NT No Unmarked paint can
25 5 Bucket Rust 25% Solid 275 Yes No No Floats 5 No No Yes NT No COOP, Masonry Paint
26 5 Bucket Rust 75% Sludge 448 Yes No No Sinks 5 No No Yes No No COOP, Masonry Paint
27 5 Bucket Rust 50% Sludge 15 Yes No No Sinks 5 No No No NT No COOP, Latex Masonry Paint
28 55 Drum Rust 25% Liquid 0 Yes No No Dissolves 9 No No No NT No Unmarked drum
29 5 Bucket Black 25% Liquid 0 Yes No No Floats 5 No No Combustible NT No Industrial Oil 70
30 1 Paint Can Rust 100% Liquid 146 Yes No No Floats 5 No No Yes NT No Unmarked paint can
31 5 Bucket Grey 100% Liquid 212 Yes No No Floats 5 No No Yes NT No PMI, non-lift Red Oxide Primer
32 5 Bucket Grey 100% Sludge 94.9 Yes No No Sinks 5 No No Yes No No PMI, 1329 Light Grey
33 55 Drum Black 75% Solid 7.4 Yes No No Floats 5 No No No NT No Overspray Material
34 55 Drum Black 75% Solid 0 Yes No No Floats 5 No No No NT No Overspray Material
35 55 Drum Black 75% Liquid 6 Yes No No Dissolves 5 No No No NT No Rainwater/Overspray Material
36 55 Drum Grey - - 3.4 - - - - - - - - - - Overspray Material. Same as container 33.
37 55 Drum Black - - 0 - - - - - - - - - - Overspray Material. Same as container 33.
38 5 Bucket Black 50% Liquid 0 Yes No No Floats 5 No No No NT No Conoco, Hydraulic AW 46
39 5 Bucket Black 25% Solid 0 Yes No No Floats NT NT NT Combustible NT NT Unmarked
40 55 Drum Black - - 24.3 - - - - - - - - - - Overspray Material. Same as container 33.
41 55 Drum Black 75% Solid 4.1 Yes No No Floats 5 No No No NT No Overspray Material
42 55 Drum Black - - 3.3 - - - - - - - - - - Overspray Material. Same as container 33.
43 5 Bucket Yellow 50% Liquid 0 Yes No No Floats 5 No No No NT No Orscheln, Premium 303 Tractor Hydraulic and Transmission Fluid
44 55 Drum Rust - - 0 - - - - - - - - - - Overspray Material. Same as container 33.
45 55 Drum Rust - - 18 - - - - - - - - - - Overspray Material. Same as container 33.
46 55 Drum Rust - - 0.4 - - - - - - - - - - Overspray Material. Same as container 33.
47 55 Drum Rust - - - - - - - - - - - - Overspray Material. Same as container 33.
48 55 Drum Rust - - 24 - - - - - - - - - - Overspray Material. Same as container 33.
49 55 Drum Rust - - - - - - - - - - - - Overspray Material. Same as container 33.
50 55 Drum Rust 75% Solid 11.1 Yes No No Floats 5 No No No NT No Overspray Material
51 55 Drum Rust - - 8.1 - - - - - - - - - - Overspray Material. Same as container 33.
52 55 Drum Rust - - 61.1 - - - - - - - - - - Overspray Material. Same as container 33.
53 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
54 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
55 55 Drum Rust - - 11 - - - - - - - - - - Overspray Material. Same as container 33.
56 55 Drum Rust - - 3 - - - - - - - - - - Overspray Material. Same as container 33.
57 55 Drum Rust - - 77 - - - - - - - - - - Overspray Material. Same as container 33.
58 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
Page 1 of 3
CONTAINER SUMMARY TABLE
Container
ID #
Size
(gallons)Container Type Color
Estimated
Content
Amount
Material
State
PID Reading
(ppm)
Sample
Collected
(Y/N)
Explosive
(Y/N)
Water
Reactive
(Y/N)
Water
Soluble
(Dissolves,
Floats, Sinks)
pHOxidizer
(Y/N)
Sulfide
(Y/N)
Flammable
(Y/N)
Halide
(Y/N)
Cyanide
(Y/N)Comments
59 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
60 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
61 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
62 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
63 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
64 55 Drum Rust 100% Solid 0 Yes No No Floats 6 No No No NT No Overspray Material and Rain Water
65 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
66 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
67 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
68 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
69 55 Drum Rust - - 13 - - - - - - - - - - Overspray Material. Same as container 33.
70 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
71 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
72 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
73 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
74 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
75 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
76 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
77 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
78 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
79 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
80 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
81 55 Drum Rust 75% Solid 0 Yes No No Floats 5 No No No NT No Overspray Material
82 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
83 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
84 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
85 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
86 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
87 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
88 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
89 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
90 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
91 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
92 55 Drum Rust - - 0 - - - - - - - - - - Overspray Material. Same as container 33.
93 55 Drum Rust - - - - - - - - - - - - Overspray Material. Same as container 33.
94 55 Drum Rust - - - - - - - - - - - - Overspray Material. Same as container 33.
95 55 Drum Rust - - - - - - - - - - - - Overspray Material. Same as container 33.
96 55 Drum Rust - - - - - - - - - - - - Overspray Material. Same as container 33.
97 55 Drum Rust - - - - - - - - - - - - Overspray Material. Same as container 33.
98 55 Drum Rust - - 128 - - - - - - - - - - Overspray Material. Same as container 33.
99 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
100 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
101 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
102 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
103 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
104 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
105 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
106 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
107 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
108 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
109 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
110 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
111 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
112 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
113 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
Page 2 of 3
CONTAINER SUMMARY TABLE
Container
ID #
Size
(gallons)Container Type Color
Estimated
Content
Amount
Material
State
PID Reading
(ppm)
Sample
Collected
(Y/N)
Explosive
(Y/N)
Water
Reactive
(Y/N)
Water
Soluble
(Dissolves,
Floats, Sinks)
pHOxidizer
(Y/N)
Sulfide
(Y/N)
Flammable
(Y/N)
Halide
(Y/N)
Cyanide
(Y/N)Comments
114 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
115 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
116 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
117 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
118 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
119 55 Drum Rust 100% Solid - Yes No No Floats 5 No No No NT No Overspray Material
120 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
121 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
122 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
123 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
124 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.
125 55 Drum Rust 50% Solid 0 Yes No No Floats 5 No No No NT No Overspray Material
126 5 Bucket Black 75% Liquid 0 Yes No No Dissolves 5 No No No NT No Industrial Oil
127 5 Bucket Black 50% Liquid 0 Yes No No Floats 5 No No Combustible NT No Industrial Oil 70
128 5 Bucket Black 100% Liquid 0 Yes No No Dissolves 5 No No No NT No Industrial Oil
129 55 Drum Black 25% Solid 0 Yes No No Sinks 5 No No No NT No Overspray Material
130 55 Drum Black - - 0 - - - - - - - - - - Overspray Material. Same as container 33.
131 5 Bucket Grey 75% Sludge 401 Yes No No Floats NT NT NT Yes NT NT Partial flammable sticker on outside of container
132 40 Drum Blue 75% Sludge 0 Yes No No Floats 6 No No Combustible NT No Unisol Liquid Green 2B
133 40 Drum Blue 50% Sludge 73.9 Yes No No Floats 6 No No Combustible NT No Unisol Liquid Blue A
134 55 Drum Rust 75% Liquid - Yes No No Sinks 5 No No No No No Unisol Liquid Blue A
135 5 Bucket Rust 50% Sludge - Yes No No Sinks 6 No No No NT No No markings on outside of drum
136 5 Bucket Rust 50% Liquid - Yes No No Floats 5 No No Combustible NT No No markings on outside of drum
137 55 Drum Rust 25% Liquid - Yes No No Floats 5 No No Combustible NT No No markings on outside of drum
138 55 Drum Rust 50% Liquid - Yes No No Floats 5 No No Combustible NT No No markings on outside of drum
139 1 Sprayer Rust 75% Liquid - Yes No No Floats 5 No No Combustible NT No No markings on outside of drum
140 5 Bucket Rust 50% Solid - Yes No No Floats NT NT NT Combustible NT No Plastic Roof Cement
141 5 Bucket Rust 100% Liquid - Yes No No Sinks 5 No No Combustible No No WT-2010 Polymer Blend
142 5 Bucket Rust 25% Liquid - Yes No No Dissolves 10 No No Combustible No No Brainerd, Cyclohexylamine
143 5 Bucket Rust 50% Liquid - Yes No No Dissolves 14 No No No NT No Betco, Stripper
144 5 Bucket Rust 25% Sludge - Yes No No Sinks 6 No No Combustible No No No markings on outside of drum
145 55 Drum Rust 50% Sludge - Yes No No Floats NT NT NT Combustible NT NT No markings on outside of drum
146 55 Drum Rust 50% Sludge - Yes No No Floats NT NT NT Combustible NT NT No markings on outside of drum
147 55 Drum Rust 50% Solid - Yes No No Floats 5 No No Combustible NT No No markings on outside of drum
148 ~2,000 Oil/Water Separator Black 10% Liquid - Yes No No Dissolves 5 No No No NT No
149 ~2,000 Oil/Water Separator Black 10% Liquid - Yes No No Floats 5 No No No NT No
150 ~2,000 Oil/Water Separator Black 10% Liquid - Yes No No Floats 5 No No Combustible NT No
Notes:
% Percent
# Number
NT Not tested
PID Photoionization detector
ppm Parts per million
Page 3 of 3
APPENDIX E
BORING LOGS
Boring Loa Form
Site Name: OsaQe and Walnut Boring Number: 1:;;-f( - \ Date Drilled (Start/Finish): \I~ cf11- IL.I C.u - l f,, f) .;-
Drilling Method: DPT Drilling Company: Sea au II Elevation: Total Depth: 1-D' Coordinates: 1 J. C \'D'J..io Iv ti:i !~f'OCf.2 IN Depth to Water: Geologist:
Project Number: 103X9025150086.000 Weather: ~"F '"-... "' •,,, r .. .e:-l- . -~r.rl_~ I
' C» \J
> c: ., - iii :s - " - "' " .c:~ ,.. :C: en c. > > .,
"' E - 1i) Color C» E ~ ~ a: ., c. c. ., 0 c. 0 Description and Remarks .,
a: c. Ql LL 0 f! ..J "' - - (Munsell (/) .E .E ·s c~ c~
<.!l .c: (/) c:: or Rock) -:i
1,.. "}, - ')Vf}."t\
\')'~ - c\1'1 0. "\ -
-- c_\lJ ~cltl 5
0 'i)
t~"/~W,\~l v/b -(). \ -
\)'{;NV\ 0u'J - ....
~.\j I-
10 ~,\,
\). t \ If\ 'x VJ\j\JJJV\ -I- ''\ - cJ<P) Q.C I-
\'\..,\\ -{ <;\1/\1,\\k.\ Wl...\ ! 15
t,.t ~
' ' I I --/ \) . (..· - \
' ·'1 1.) - \~h"0'fti J \ \9 -
n.O - lvJe..-t) 20
- ,\1)\) ·.':/ - ·1? ... ~Jc - '°""""<? 2.tl l -...,. --~··- - '.?"°If'
25
----
30
Boring Log Form
Site Name: Osaqe and Walnut Boring Number: G-P - 2 Date Drilled (Start/Finish): l I 2.4 lt;i \\ii \O-\i,,'7 .<; Drilling Method: DPT Drilling Company: Seaaull Elevation: Total Depth: q, \ Coordinates: Depth to Water: Geologist: Project Number: 103X9025150086.000 Weather: i..-jf)',::;. 'f\Vl\,-t.v.i- 1. lV\d\.J
' C) J
Ill - > c: () - "' iii () :s - .c: ~ "' :.c C') c. > > Ill
"' E - di Color C)
E lii ~ cc Ill c. c. Ill 0 c. 0 Description and Remarks Ill cc c. Ill Ll. 0 f! .J "' - - '(5 c- (Munsell en .E .E c- .c: (!j en a: or Rock) -::i \, D - lvt-,vt..I
(1 \ \ v\'1.'.«k~ iet I -~-4 U· \J ~ - cu{, 11vi;.uV\ Git/ --
\ ~.t
5 ' l -
\.\A \).U - \ ''l """ vv~v.M Lit! ---___!Q
-
---15 r------20 ,..____
----y
----30
Boring Log Form
Site Name: Osage and Walnut Boring Number: r..-v - z, Date Drilled (Start/Finish): ,j11,,i1to r1<! \C .- ~,tr> "7 r-..
Drilling Method: DPT Drilling Company: Seaoull Elevation: Total Depth: ~~' Coordinates: Depth to Water: Geologist:
Project Number: 103X9025150086.000 Weather: 7-.vc i::- C:.. \,)y'\V'\A A
• Cl J
Q) -,; c
.S:! - "' iii 0 :.a - .c ~ >-c. > > Q) "' E c. 1i) Color Cl .c Cl
E ~ ~ cc Q) c. 0 c. 0 Description and Remarks Q) Q) Q)
"' - - 'Ci cc c. o~ (Munsell 0 !!! -'
(/) .E .E o~ .c (.!) (/) a: or Rock) -:::;
0 () - io •' vr,1it.~
-A1<1\.t vvvWV\ tL~J
))-\ e·~ - ' •\;
- -•:\ , .. 5 ~·V -
q.'-1, - \'J\~\}J"' t\ll ,r \i<'\} ---
-10 ,____
-"""" --
15 --
---
20 ----
-25 -
-
---
30
Boring Log Form
Site Name: Osage and Walnut Boring Number: l...-i7-Li Date Drilled (Start/Finish): \I ?Ao Ii r~ h4 (.j <:'.: - G"l () i'l Drilling Method: DPT •
Drilling Company: Seaaull Elevation: Total Depth: Q ' Coordinates: Depth to Water: Geologist:
Project Number: 103X9025150086.000 Weather: .z, Cj ~ \)VWv-.A
C)
Ql - > c (.) - "' ~ (.) :s - .c ~ >- :c C> c. > Ql "' E a ru Color C)
E - - a: Ql c. 0 c. 0 Description and Remarks Ql Ql a: c. Ql Ql ~ ...J "' - - ·a c1=- (Munsell 0 (J) .5 .5 c- .c c.!l
(J) a: or Rock) -:J
\) u ,_ \f o-1(, \ y·iicvt\ ! t,ctvv{
v, - {U.\ ~ \/Vli,(l ~/
i) ~ ,_ 19vi;..v"' l, •'1 ,v
c\i;tvll \?Vii.NII GVJ -,_
\) .l:i ,___§.
~}b - \')vuJvh L(J fl c ,_ U'
\11 v """" ( lt<-j 4. ';)r-1.vx:l ---
10
---
-15
--
--
20 ----
-~
-
-
--
30
Boring log Form
Site Name: Osaqe and Walnut Boring Number: LP- CJ" Date Drilled (Start/Finish): ,;,,,,,,,,,, 1)C/ 2 .. r-, Drilling Method: DPT ' Drilling Company: Seaaull Elevation: Total Depth:
Coordinates: Depth to Water: Geologist:
Project Number: 103X9025150086.000 Weather: '2, c.. "'>""' V'-.~ •
m } :> c:
Q) - o; :s - " - "' " .c:~ ,.. :.c Cl c. > > Q) "' E - Qi Color m
E lii ~ 0: Q) c. c. Q) 0 c. 0 Description and Remarks "' - $ 0: c. Ql LL
(Munsell 0 f! ...J (/) .E .E ·a c- c- .c: (!)
(/) a: or Rock) -:::; ~.~
•Jfi14S - (tlt
0~ \..\ - \ '~1"'-" 'QV'Jv.J(\ \A•"'i \ 1Ctvv:A I.I ~ .l'l -
/JJ)..JV- "I'll \).)V\ c,~ --0 ll 5 -
c.-1, '!:> -~\fW''i\ clj
~.\l -
- i-
I-
10
i-
I-
i-
-15
----
20
-
-
--
25
----
30
Boring log Form
Site Name: Osaqe and Walnut Boring Number: l-P.-/ ,, Date Drilled (Start/Finish): \ j,., I" 111" lo ? ('.: Drilling Method: DPT Drilling Company: Seagull Elevation: Total Depth: 4. \
Coordinates: Depth to Water: Geologist:
Project Number: 1 03X9025150086. 000 Weather: :,c:, L'\.JnlAA~
' Cl ,I
Ql - :> c () - "' ~ () :s - .c: ~ > :c C> Q. > Ql "' E c. (i) Color Cl E iii - a: Ql Q. 0 Q. 0 Description and Remarks Ql Ql Ql
"' -- 'i5 a: Q. c !::. (Munsell 0 f: ...J
en .5 .5 c~ .c: Cl en c:: or Rock) -::J - y tl\.lC,
- <Jt!"-&11 'JVV-Vv\
{)-"' - JJt Vl'N"i"'- \:,,~ --5 - \fl I! l, '.\i'(\ . '" .
' t.\,q, - i -
- I- \\vjl'1..\' ~ cvv; -
10 -I-
I-
-I-
15 --I-
I-
-20
----
25
----
30
Boring Log Form
Site Name: Osaae and Walnut Boring Number: 4-17-\ Date Drilled (Start/Finish): \)li.\\Ji 1(-'.l!:;n i o'7 C,
Drilling Method: DPT Drilling Company: Seai:iull Elevation: Total Depth: {/_ ; , Coordinates: Depth to Water: Geologist: Project Number: 103X9025150086.000 Weather: 1,?) ". Vi\V\-' {,. J\\I\ ,,jAA
• Cl / ~
Q) - > c: 0 - "' o; 0 :c - J: ~ >- :c tJ) c. > > Q)
"' E Q.. (i) Color Cl E ~ ~ cc Q) c. 0 c. 0 Description and Remarks Q) Q) Q)
"' - - ·5 cc c. c !:!::. (Munsell 0 !!! ..J (/) .5 .5 c~ J: (!)
(/) a: or Rock) ."!::: -'
I- ( tl""
i))\ I- \tll tlN"j
- i,\tj YJvv.NV'< -,.... I 5 - I
\,\-Lb - '1; - \ '1)~'< \;VrpiV\ rJt'-"-j - --
10 -----
15 ----
-~ I-
-I-
I-
25 r--
I-
I-
-I-
30
Boring Log Form
Site Name: Osage and Walnut Boring Number: i-rO-' 'f.. Date Drilled (Start/Finish): \/,He 11 Iv ~ \ [ '2,c:.- I I 7,'*-.
Drilling Method: DPT Drilling Company: Sea~ull
Elevation: Total Depth: Cf..'
Coordinates: Depth to Water: Geologist:
Project Number: 103X9025150086.000 Weather: U D' i:: <;ul'll'\M Ww·l..t
Cl
"' - :> c: .S:? - "' c;; 0 :a - .s::~ ,.,
c. > > "' "' E c. (i) Color Cl .s:: Cl E ~ ~ a: "' c. 0 c. 0 Description and Remarks
"' "' Q) "' - - ·c; a: c. c !!::. (Munsell 0 E-' (/) .E .E c~ .s:: (.!) (/) c: or Rock) -:J
i).il - {u:A.4 ~\\ \\"'1,\tV-q_t
\)'\.\ f-
~(') f- \1\'0WYI Cllvf -- \ 5 C.\\ f---
} i,\-4 -~.\) - \' iWI\ c lcvj -f- \ 11,1\A I
-10
----
15
----
20
----
25
----
30
Boring log Form
Site Name: Osage and Walnut Boring Number: 1-rP ·- q Date Drilled (Start/Finish): \f'11.li(/l \1C::>-v Drilling Method: DPT I
Drilling Company: Seaqull Elevation: Total Depth: "O \ Coordinates: Depth to Water: Geologist:
Project Number: 1 03X9025150086. 000 Weather: Wu "c '>Vl'lVVVi
Cl J :> c: Q>- a; " :s- .c: ~ » " Q. ~ > <I> "' E - 'al Color Cl :c Ol E iii ~ a: <I> c. c. <I> 0 c. 0 Description and Remarks <I> a: c. <I> u. 0 ~ ...J "' - - '(5 o~ (Munsell (/) .5 .5 o~ .c: <.!l
(/) ii: or Rock) -:::; .Y\ \\ [tJr-~~~
~t .... l>J 2,,\- C '""} ~ \:JVIV.n J
vv\ ....
~ \, - ()At· \?11\)\.>JY\ cL°'1 \J•
--5 . ,___
\X ~~ \~~ vwv-J \-\A --
·- --~
10
----
15
----
20 ---
--
25 --
--
-30
Boring log Form
Site Name: Osaqe and Walnut Boring Number: /!2!Ji irP-ID Date Drilled (StarUFinish): I/ Z,l!J I I lo 1;-z,t:; - 1;'--10 Drilling Method: DPT Drilling Company: Seaaull Elevation: Total Depth: u' Coordinates: Depth to Water: Geologist:
Project Number: 103X9025150086.000 Weather: u O'' r:; c -·-·-Cl
_, <ll - > <::
.!::! - "' iii " :s - .s::~ >-c. > > <ll "' E - 1ii Color Cl .s:: Cl E lii ~ cc <ll c. c. <ll 0 c. 0 Description and Remarks <ll cc c. <ll LL 0 E-' "' - - (Munsell (/) .E .E ·c; c~
c~ .s:: (!)
(/) 0:: or Rock) :!::: ...J
\~ '{ o().l
I- ,e\\\ ~ . ).eV. -b "''~
~,'\ - VIAl\t Wt'-"\'\ c ltx; '( V: \c~ 1,,\'l1~" ~.I:> -
¥"ft"'" rJ~ - -5
-I-
--
10
----
15 ---
-I-
20 I---
----~ I-
--I-
30
Boring Log Form
Site Name: Osage and Walnut Boring Number: L~9--\\ Date Drilled (Start/Finish): d ·1 lo 111., \'-(\e;- -Drilling Method: DPT Drilling Company: SeaQull Elevation: Total Depth: L.i \ Coordinates: Depth to Water: Geologist:
Project Number: 103X9025150086.000 Weather: LtO" ~ c..' <V"\l!'V..__A
' Cl J ., - :> c
.S:? - "' Oi 0 :a - .c:~ "' c. > > ., "' E Q. Q) Color Cl .c: Cl
E ~ ~ 0: ., c. 0 c. 0 Description and Remarks ., ., ., "' - - ·c; 0: c. Q !:!:. (Munsell 0 E-' en .E .E Q~ .c: (!) en a: or Rock) -:::;
~~ - .811 \lfU-SS Y~0~v c{'~
0'\-\ >- (~~) (,\lb \:JtDWV\
~~ --- \'.)VbvJI\. ~ 5
-
-
--
10
----
15 ---
--
20 -
-
-->--
25 t---
->---- 30
Boring Log Form
Site Name: Osaae and Walnut Boring Number: (.,.\/- \ ")
Date Drilled (Start/Finish): \/'7i- \In 11..f '70 - it>bD Drilling Method: DPT I
Drilling Company: SeaQull Elevation: Total Depth: <;('I
Coordinates: Depth to Water: Geologist: Project Number: 103X9025150086.000 Weather: LID" C...\)f\V\M
~
01 \J :> c <1>-~ (.) ~- .J: ~ >-
(.) - "' :C en Cl. > <I> "' E - a; Color 01 E Oi - a: <I> Cl. Cl. <I> 0 Cl. 0 Description and Remarks <I> a: Cl. <I> LI.. 0 f: ...I "' - - (Munsell ({) .E .E "C5 Cl~
o~ C) .J:
({) 0:: or Rock) -::J - voc\L
\~ - ~ \\ ~.\0\f\C\,\
J: I-
c\cvi ~rt>)\~ fs1c>.1 'N.cl) o.y<f' e,1" !r ~eiYo\9.u , ,,~ -,_ OcUv
~" ~ ' v/tJ -
\1vvt '>tAl"Wj Clvv--/
--I-
'()ytWJ\ (;~ I-
10 r---
I-
I-
-I-
15
-I-
I-
-20
----
25
----
30
Boring log Form
Site Name: Osage and Walnut Boring Number: (.., V- \2.. Date Drilled (Start/Finish): \I 11 n II in I '7 :z, i.:.,
Drilling Method: DPT '
Drilling Company: Seaaull Elevation: Total Depth: q,' Coordinates: Depth to Water: Geologist: Project Number: 103X9025150086.000 Weather: L\l) . C.; vW\• '
Cl ) Cl> - :> " .!:? - "' <ti " =s - .c: ~ ,., c. > > Cl> "' E - -a; Color Cl .c: Cl E lii ~ a: C1> c. c. Cl> 0 c. 0 Description and Remarks Cl> a: c. Cl> u. 0 E _. "' - - ·o o~ (Munsell en .E .E o~ .c: (!) en 0:: or Rock) -:::;
\1\t\(,\t 'i V1.Ji.i.u, ';~1>"1f'ol \_I" 'Ii," ) -H(Ys(~\\
~_,'\ --
\')Vbwn C\fM..j ;l' -Ir
5 I ,• ...---~ -
"\;1, - \I;
·11c1h.\: iovc,..V\ Cl~ - .... ....
10 ,.._
----15
----
20
----
25
----
30
Boring log Form
Site Name: OsaQe and Walnut Boring Number: forF'-IY Date Drilled (Start/Finish): \l'7,L·,l\1., I c:. c:., c... - I/,; (Jc;-
Drilling Method: DPT ' . Drilling Company: Seaoull Elevation: Total Depth: ~I, I
Coordinates: Depth to Water: Geologist:
Project Number: 103X9025150086. 000 Weather:
Cl <1>- :> c
" - tll iii " =a - .c ~ >- :E en Cl. > > Cl> m E c..m Color Cl E Q; - a: Cl> Cl. 0 Cl. 0 Description and Remarks Cl> Cl> Cl> tll - - 'i5
a: Cl. c '==- (Munsell 0 e _, (fJ ..5 ..5 c~ .c G
(fJ c:: or Rock) -::; \" \11titlt ";iwko..tt '7ttilV\•l"J - \rQ[,\,_ I h\I -
V"'-\ - \1l'Olr!V1 e,livj ,f -... 1 ~ 5 -
'\''-Ii - \ ll)Y,-1- W C"'"' cl~ -~ ~
-10 -
-
---_:!2
--
--20 --------25 -------30
APPENDIX F
CHAIN-OF-CUSTODY FORMS, FIELD SHEETS, AND ANALYTICAL DATA
J
ACTIVITY LEADER(Print) --fvdd c. <?<1 pbetl
CONTENTS OF SHIPMENT
SAMPLE
CHAIN OF CUSTODY RECORD ENVIRONMENTAL PROTECTION AGENCY REGION VII
I NAME OF SURVEY OR ACTIVITY Osa'!c:. tv'cl Wo.l "Vl- ~ 1 Ir..
~
TYPE OF CONTAINERS SAMPLED MEDIA
IDATE OF COLLECTION I SHtt I ~ J....,_ ~I ltl DAY MONTH YEAR I 0
)._
RECEIVING LABORATORY ro ;e c,i..~i1 ... v~._,,1 ... \.-z. ~OA SET c olher AEMARKS10THEA INFORMATION NUMBER eUeii'AiNER" iOi'fIT BOT'TiT BOTTLE VIALS EA) ~
~ lcond11ton of samples upon rece<pl , '\)•Q"' ... g '5 ~ olher sample numbers. elc I NUMBERS OF CONTAINERS PER SAMPLE NUMBER ~ " ~ 'O
7041 - IOI I I )C.
- loz. I I
- 10~ I I - IOI./ ' ' -10s I '2..
-101.. I I
-101 I I
- 108 ' I - l DC\ I I
-110 I I
-\lo F1> t l - It\ I I
' I • - 111-
-113 I I
-114 I I
-11;" I I - II lo ' ' -111 I ' - I\ 8 I I
- 11 '\ \ I -1'2.o I l
- l'-1 I 2. -IZ't. I I I - I 'Z. 3 I ' hV
DESCRIPTION OF SHIPMENT MODE OF SHIPMENT
PIECE(S) CONSISTING OF BOX(ES) --COMMERCIAL CARRIER:
s --COURIER ICE CHEST(S): OTHER ---X--SAMPLER CONVEYED -(SHIPPING DOCUMENT NUMBER)
PERSONNEL CUSTODY RECORD
nEU~:tr ~MPLER) DATE TIME RECEI V ED B Y REASON FOR CHANGE OF CUS T ODY
1/i-1/1/tJ /2- c:, 0 TuiJ~ Ze~· J o:f::,, fl.e-6 11 SEAi:: D UNSEALED Ii:_ h SEALED UNSEALED N R ELIN Q UI SHED BY DATE TI M E RECEI V ED B Y REASON FOR CHAN GE O F CUST O D Y
nsEALED UNSEALEDr hsEALED UNSEALED r RELIN QUISHED BY DATE TIME RECEIVED B Y REASON FOR CHANGE OF CU STODY
I SEALED UNSEALEDr ! SE A LED UNSEALEDr
7-EPA-9262 (Rev1sed 5/ 85)
CHAIN OF CUSTODY RECORD ENVIRONMENTAL PROTECTION AGENCY REGION Vil
ACTIVITY LEADER(Print) I NAME OF SURVEY OR ACTIVITY lDATE OF C~LECTION <.. I SHtt1
f' odd f' owl Jo< I/ ()544~ 6¥'.J ""*"'"'"'+ Sile. ~ <V\ U>I I I 'I DAY Mt'1NTH ~ ..2 O ..:2
CONTENTS OF SHIPMENT TYPE OF CONTAINERS SAMPLED MEOIA RECEIVING LABORATORY
SAMPLE 8·..,.. l11. [ ., ~ (. 'J~ <lb.\ t.~vOA SET c other REMARKS.OTHER INFORMATION NUMBER Ctl81TAIN£1r BcffiIT BOTILE BOTILE VIALS EA)
~ e (cond1l1on ol samples upon 1ece1p1
~ ~ "' other sample numbers etc I NUMBERS OF CONTAINERS PER SAMPLE NUMBER o.o. 3' " 'O
-o~\-1?.c.f I I y.
-.'ZS l t -I lb ' I -zol I I
-2oZ.. I I
-20'3 I I lw
/ ~
/ r7
.,v \ \ v
/ \ t
~\ [/ \ \U A - /
/ \ l, / \~ /
h, \. \ / / ",) IV
/ \l "' \ -\A~' v:,\< r 0 . '/ VJ' v
r I\
/ / ~o Y1 \ / '" /"'\:~ I~
/ ~1\u Y/
v ...
/ / '
DESCRIPTION OF SHIPMENT MODE OF SHIPMENT
PIECE(S) CONSISTING OF BOX( ES) --COMMERCIAL CARRIER
3 --COURIER
ICE CHEST(S): OTHER -X....SAMPLER CONVEYED (SHIPPING DOCUMENT NUMBER)
PERSONNEL CUSTODY RECORD Ft~~JISHED,,SY (SAMPLER) OATE TIME RECEIVED BY REASON FOR CHANGE OF CUSTODY
- ~ 1/1r ''- /Z~lJ ~~~ f2ev'J af:- rbJ..b M SEALED UNSEALED rt: h SEALED UNSEALEO L RELINQUISHED BY DATE TIME RECEIVED BY REASON FOR CHANGE OF CUSTODY
llsEALED UNSEALEDr hsEALED UNSEALED r RELINQUISHED BY DATE TIME RECEIVED BY REASON FOR CHANGE OF CUSTODY
lSEALED UNSEALEDr 11 SEALED UNSEALEDr
7-EPA-9262(Rev1sed 5/85 J ·u.s. GPO: 2002-756-917140053
... CHAIN OF CUSTODY RECORD
ENVIRONMENlAL PROTECTION AGENCY REGION VII ACTIVITY LEADER(Print) I NAME OF SURVEY OR ACTIVITY 1D~TE OF COLLECTION I SHEEl
·d '/ """'DAY MONTH -vdir- I I I ofl ' , 14 t "'
CONTENTS OF SHIPMENT -TYPE OF CONT AINEAS SAMPLED MEDIA RECEIVING LABORATORY
SAMPLE .JI' l VOA SET c oiner REMARKS OTHER INFO RMATION
NUMBER CUBITAtNER 8cITTIT BOTILE BoffIT (2 VIALS EA) ~ e (cond111on ot samples upon 1ece1p1
; ~ ~ ~ othe1 sample numbe1s etc l
NUMBERS OF CONTAINERS PEA SAMPLE NUMBER " " "lol./l-1 y.
_., .. ' -2FD I
- 3 I
- t.f I -s I -(., I -7 I , ... ,,, \{I
·- ... -I- --'--- -- -- _,,,
~ _,,/
,,.,,. i..-
I/ ,,. ..,
1\ '""' / /
~
) / . ,, .
I -1' r /1 v
/ /IC. ' .J
/. ~ I
'
/""' ~f v 1/V
v I ~-
,, _,., y
- - --· - --- .__. - -- - - ,_ a-. - - -DESCRIPTION OF SHIPMENT MODE OF SHIPMENT
PIECE(S) CONSISTING OF BOX(ES) --COMMERCIAL CARRIER --COURIER
' ICE CHEST(S). OTHER ~SAMPLER CONVEYED (SHIPPING DOCUMENT NUMBER)
PERSONNEL CUSTODY RECORD FIELINQUISHEO BY (SAMPLER) DATE TIME REJ;;EIVEO BY •• REASON FOR CHANGE OF CUSTODY
:i' 'I I 1- ~, ,i; 12, ... 1~~--- t.~,_ ·)(IA .,_{)
!").SEALED UNSEALED r,- h SEALED ''-'' UNSEALED r REL INQUI SHED BY DATE TIME RECEIVED BY REASON FOR CHANGE OF CUSTODY
ll SEAL ED U NSEALEDr hsEALED UNSEALED r RELINQUISHED BY DATE TIME RECEIVED BY REASON FOR CHANGE OF CUSTODY
n SEALED UNSEALED! hsEALED UNSEALEDr
7-EPA-9262<Rev1sed 5/85) ·u.s. GPO: 2002-755-917/~0053
CHAIN OF CUSTODY RECORD ENVIRONMENlAL PROTECTION AGENCY REGION VII
f\CTIVITY LEADER(Print) I NAME OF SURVEY OR ACTIVITY IDATE OF COLLECTION I SHtt I
; "J.J l <- ·\Pb• II .,~ 't- w-u:I t.)e../ •1 vf _:z_ '· - ~I 1°11 DAY MONTH YEAR I
CONTENTS OF SHIPMENT TYPE. OF CONTAINERS SAMPLED MEDIA RECEIVING LABORATORY
SAMPLE rr '", ~"-"'< //..alt-C!J~' -- VOA SET c otner REMARKS.OTHER INFORMATION NUMBER CVlll Al NEil' '8lffitf eom E 8oTlli (2 VIALS EA) u e (cond1t1on ol samples upon receipt
i ~ ~ ~ otner sample numbers elc )
NUMBERS OF CONTAINERS PER SAMPLE NUMBER :0
"' /Oi , - I J I x - - - ~ - I-
J
,/
/ ,,
....... "" /
/ f1 I/ /
\ ~
/ l' '7
" ... / "
1/ J
'-',, ~I\
(" I
7~/ J \ \ \l·" r- \\
,.., ,,.
, \ Iv \ \c \ v~v
I . \ \ .. . f' . /\f; /'
' ~
' / ~ ,
/
/ /
I I I - -
DESCRIPTION OF SHIPM ENT MODE OF SHIPMENT
--PIECE(S) CONSISTING OF BOX(ES) --COMMERCIAL CARRIER --COURIER
ICE CHEST(S). OTHER _.:__ SAMPLER CONVEYED (SHIPPING DOCUMENT NUMBER)
PERSONNEL CUSTODY RECO RD FtELINQUISHED BY (S A M PL E R) DATE TIM E REC~1f BY / •
REASO N F O R CH A N G E OF CUSTODY
- .-2 I '1/1 1 I A.J
Z<:'olcit ~ ' ...,. tfi;-r' h SEAL~O ~f-rl SEALED U N S EAL E D i7
R E LINQU ISH E D B Y DATE T IME R E CE IVED B Y REA SON F O R CHANGE OF CUSTODY
hsEALED UNSEALEDr hsEAL E D U NSEALED l RELINQUISHED BY DATE TIME REC E IVED B Y REASON F O R CH A NG E O F CUSTODY
n SEALE D UNS EALED! hsEALE D UNSEAL ED r
7-EPA-92621Rev1sed 5185) ·u.s. GPO: 200?-755-917/(0053
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 101 QC Code: _ Matrix: Solid Tag ID: 7041-101-_
Project ID: TCB794 Project Manager: Todd Campbell -Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date Time(24 hr) I .,--o-S-
@t::~ •/""')'"
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 102 QC Code: _ Matrix: Solid Tag ID: 7041-102-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date
LJ2£/11P _}_)_
Time(24 hr)
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 103 QC Code: _ Matrix: Solid Tag ID: 7041-103-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40ml VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High) Date Time(24 hr)
Sample Collection: Start:
End:
Holding Time Analysis
14 Days 1 VOC's in Soi! at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 104 QC Code: _ Matrix: Solid Tag ID: 7041-104-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 8794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C1 H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
,;.p- 2 0 -'?>) Date
J_j']f)J]Q
_/_/_
Time(24 hr)
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 105 QC Code: _ Matrix: Solid Tag ID: 7041-105-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A) \t-l';v \"' .
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date Time(24 hr)
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 106 QC Code: _ Matrix: Solid Tag ID: 7041-106-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 6794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date Time(24 hr)
L:i_::b_C
14 Days ,
1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 107 QC Code: _ Matrix: Solid Tag ID: 7041-107-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Oeg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date
L!1kllli _/_/_
Time(24 hr)
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 108 QC Code: _ Matrix: Solid Tag ID: 7041-108-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 8794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date Time(24 hr)
0°1 :CC
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 109 QC Code: _ Matrix: Solid Tag ID: 7041-109-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 6794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High) Date Time(24 hr)
Sample Collection: Start:
End:
Holding Time Analysis
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 110 QC Code: _ Matrix: Solid Tag ID: 7041-110-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 8794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High.)
Sample Collection: Start:
End:
Holding Time Analysis
Date
lJ11cl Tu> _J_j_
Time(24 hr)
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
i\0 "!\D·-1=0 ASR Number: 7041 Sample Number: .J.R QC Code: :e,? Matrix: Solid Tag ID: 7041-;t,.;q-~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~-*'~µ.~ll~
Project ID: TCB794 ,\,_,v\\ Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site -
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisu!fate (in 2 vials) 4 Deg C
Sample Collected By: TT
Site ID: B794 Site OU: 00
External Sample Number:
Low Medium High) Date Time(24 hr)
()C}_: So Sample Collection: Start:
Holding Time
14 Days
28 Days
1 of 1
End:
Analysis
1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
1 Cyanide, Total in Soil
Sample Collection Field Sheet us EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 111 QC Code:_ Matrix: Solid Tag ID: 7041-111-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date
j_jJMJ_lo _}_}_
Time(24 hr)
-·-
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 112 QC Code: _ Matrix: Solid Tag ID: 7041-112-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: DO
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40ml VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Oeg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date
lJ21&11o _/_/_
Time(24 hr)
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 113 QC Code: _ Matrix: Solid Tag ID: 7041-113-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date Time(24 hr)
\_\ :1:>'2..
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 114 QC Code: _ Matrix: Solid Tag ID: 7041-114-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 8794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date Time(24 hr)
\j_: \0
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet: US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 115 QC Code: _ Matrix: Solid Tag ID: 7041-115-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: DO
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soi! VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date Time(24 hr)
l_I :~ o
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Tota! in Soil
1 of 1
Sample Collection Field Sheet: US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 116 QC Code: _ Matrix: Solid Tag ID: 7041-116-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: Soil VOA & CN samples
External Sample Number:
Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)
Latitude: Sample Collection: Start:
Longitude: End:
Laboratory Analyses: Container Preservative Holding Time Analysis
4 - 40mL VOA vials (soil VOA 5035)
4 Deg C, H20 + sodium 14 Days bisulfate (in 2 vials)
1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
1 - 8 oz glass
Sample Comments:
(N/A)
4 Deg C 28 Days
Sample Collected By: TT
1 of 1
1 Cyanide, Total in Soil
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 117 QC Code: _ Matrix: Solid Tag ID: 7041-117-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: DO
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40ml VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date
lJfu!l_fv _/_/_
Time(24 hr)
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soll
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 118 QC Code: _ Matrix: Solid Tag ID: 7041-118-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 8794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40ml VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date
_l__j 2Jd __Llo
_)_)_
Time(24 hr)
\k_:v·:i
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 119 QC Code: _ Matrix: Solid Tag ID: 7041-119-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 8794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date
VZiolU.o _J_J_
Time(24 hr)
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 120 QC Code: _ Matrix: Solid Tag ID: 7041-120-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 8794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40ml VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date Time(24 hr)
i.':L: io
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Tota! in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 121 QC Code: _ Matrix: Solid Tag ID: 7041-121-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 8794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High) Date Time(24 hr)
Sample Collection: Start:
End:
Holding Time Analysis
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: \1-'2- QC Code:_ Matrix: Solid Tag ID: 7041-\7.2--_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 6794 Site OU: 00
Location Desc: Soil VOA & CN samples
External Sample Number:
Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate {in 2 vials) 4 Deg C
Sample Collected By: TT
Sample Colle~tion: Start: LlWllP _J_J_
l:i.:_2'b
Holding Time
14 Days
28 Days
1of1
End: -·-
Analysis
1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
1 Cyanide, Total in Soil
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: \I-3 QC Code:_ Matrix: Solid Tag ID: 7041-\7.. 3-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 6794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A}
Preservative
4 Deg C, H20 + sodium bisulfate {in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date Time(24 hr)
l.i:.:!_O
-·-
14 Days 1 VDC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1of1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: \Z- '-\ QC Code: _ Matrix: Solid Tag ID: 7041-\L.'-\-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: OD
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials} 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Colle.ction: Start:
End:
Holding Time Analysis
Date
L'.lk'lli _J_J_
<
Time(24 hr)
6-: L\\
-·-
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1of1
Sample Collection field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: \1-t5 QC Code: _ Matrix: Solid Tag ID: 7041- \V7-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 6794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Colle.ction: Start:
End:
Holding Time Analysis
Date
L!lW.llo _j_J_
Time(24 hr)
ik_:oD
-·-
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1of1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: \1..l.ll QC Code:_ Matrix: Solid Tag ID: 7041-\'Zio-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: Soil VOA & CN samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C, H20 + sodium blsulfate (in 2 vials) 4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collei:;tion: Start:
End:
Holding Time Analysis
Date Time(24 hr)
-·-
14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
28 Days 1 Cyanide, Total in Soil
1 of 1
Sample Collection Field Sheet: US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 201 QC Code: _ Matrix: Solid Tag ID: 7041-201-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 8794 Site OU: 00
Location Desc: Soil TPH VOA (GRO) & SVOA (DRO/ORO) samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
2 - 40ml VOA vial
1 ~ 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C
4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High) Date Time(24 hr)
Sample Collection: Start: \~:40
End:
Holding Time Analysis
14 Days 1 Volatile TPH in Soil by GC/MS
14 Days 1 Semi-Volatile TPH (DRO & ORO) in Soil by GC/FID
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 202 QC Code: _ Matrix: Solid Tag ID: 7041-202-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: Soil TPH VOA (GRO) & SVOA (DRO/ORO) samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
2 - 40mL VOA vial
1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C
4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High) Date
Sample Collection: Start:
End:
Holding Time Analysis
14 Days 1 Volatile TPH in Soil by GC/MS
Time(24 hr)
L1:L:Lo
14 Days 1 Semi-Volatile TPH (ORO & ORO) in Soil by GC/FID
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 203 QC Code: _ Matrix: Solid Tag ID: 7041-203-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 6794 Site OU: 00
Location Desc: Soil TPH VOA (GRO) & SVOA (DRO/ORO) samples
Expected Cone: (or Circle One:
Latitude:
Longitude:
Laboratory Analyses: Container
2 - 40ml VOA vial
1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C
4 Deg C
Sample Collected By: TT
External Sample Number:
Low Medium High)
Sample Collection: Start:
End:
Holding Time Analysis
Date
l_f&l(i?
__/__/_
14 Days 1 Volatile TPH in Soil by GC/MS
Time(24 hr)
IL\ :_2'-1
-·-
14 Days 1 Semi-Volatile TPH (DRO & ORO) in Soil by GC/FID
1 of 1
ACTIVITY LEAOER(Print) lt>c/,,., (,.-pl t'.I/
CONTENTS OF SHIPMENT
SAMPLE ' ~11"!n· ir,.·
CHAIN OF CUSTODY RECORD ENVIRONMENtAL PROTECTION AGENCY REGION VII I NAME OF SURVEY OR ACTIVITY
( r r ,;;;.•. i-J If., i-1 ..,
TYPE OF CONTAINERS SAMPLED MEDIA
IOATE OF COLLECTION I SHttl
-2...L ~ ~ .2a!L. I I I of I I DAY -ONTH YEAR
RECEIVING LABORATORY VOA SET c Olher REMARKS.OTHER IN FORMATION
NUMBER CUBITAtNER BOTILE Bomf BciffiE (2 VIALS EA) ~ e (cond1t1on of samples upon receipt
NUMBERS OF CONTAINERS PER SAMPLE NUMBER i ~ ~ ~ other sample numbers etc l 'C
I 'I I J I y. _.,
I ... -lFD I
- 3 I -~ I -s j
-1.. I
-7 I 1- / '1t' -- -- ~~
~ ~ ,,....
~,.,,
/ .....
> "'\ ./
t\vtv ~ v""
J,. ,) iv ./
_ ,., e /i v
//Jt. f / ~
/. ~~ I ) ,
/ r1 ')F ,.vt.ll( v l 1" J I/'-_, ""4"""
/ !.-l/
/ / '\ ------· - ·- --
DESCRIPTION OF SHIPMENT MODE OF SHIPMENT
PIECE(S) CONSISTING OF BOX(ES) --COMMERCIAL CARRIER --COURIER
J ICE CHEST(S). OTHER ___'L_sAMPLER CONVEYED (SHIPPING DOCUMENT NUMBER)
PERSONNEL CUSTODY RECORD .. DATE TIME Rrt-iVEO BY • •• REASON FOR CHANGE O F CUSTODY FlELINGIUISH-ED. &Y (SAMPLER) , c·') ;z. .1,; ,1, ... C'11 c; -avJ~>---· 2~4 1) ~146 t~SEALED ...__ UNSEALED [."'" ilSEALED ~ UNSEALED f" RELINQUISHED BY DATE TIME RECEIVED BY REASON FOR CHANGE OF CUSTODY
n SEALED UNSEA LEDr nsEALED UNSEALED j RELINQUISHED BY DATE TI ME RECEIVED BY REASON F OR CHANGE OF CUSTODY
l SEALED UNSEALED! l SEALED UNSEALEDr
7-EPA-9262(Re111sed 5185) 'U.S . GPO: 2002-755-917/~0053
Sample Collection field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 1 QC Code:_ Matrix: Solid Tag ID: 7041-1-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: DO
Location Desc: RCRA metals & Hg samples
External Sample Number: _u_tJ_-~i __________ _
Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)
!l_:OS Latitude: iE:,_011p&&"I'
Longitude: -M· '-•&Oii ·
Laboratory Analyses: Container
1 - 8 oz glass
1 - 8 oz glass
Sample Comments:
(N/A)
Preservative
4 Deg C
4 Deg C
Sample Collected By: TT
Sample Collection: Start: _LJ~ ~
End: _J_J_
Holding Time Analysis
28 Days 1 Mercury in Soil or Sediment
180 Days 1 Total Metals Analysis of TCLP Metals in Soil by ICP-AES
1 of 1
Sample Collection field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 2 QC Code:_ Matrix: Solid Tag ID: 7041-2-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: RCRA metals & Hg samples
External Sample Number: [)() - 2.
Expected Cone: (or Circle One: Low Medium High) Date
Latitude: J-=t-. ot=l-'!1"'.14"
Longitude: -"I§·~ ~'I\·
Laboratory Analyses: Container
1 - 8 oz glass
Preservative
4 Deg C
Sample Collection: Start: l_fl..~llo>
End: _J_J_
Holding Time Analysis
28 Days 1 Mercury in Soil or Sediment
Time(24 hr)
1 - 8 oz glass 4 Deg C 180 Days 1 Total Metals Analysis of TCLP Metals in Soil by ICP-AES
Sample Comments:
(N/A)
Sample Collected By: TT
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
z.- f."D
ASR Number: 7041 Sample Number: 8 QC Code:_ ..
Matrix: Solid Tag ID: 7041-;#_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: RCRA metals & Hg samples
External Sample Number:
Expected Cone: (or Circle One: Low Medium High) Date
Latitude: 3~·0\'l!:.~.'~!. •
Longitude: -"t'll'.~"l"l"l•
Laboratory Analyses: Container
1 - 8 oz glass
Preservative
4 Deg C
Sample Collection: Start: _j_/£!}!.J,_
End: __J__J_
Holding Time Analysis
28 Days 1 Mercury in Soil or Sediment
Time(24 hr)
1 - 8 oz glass 4 Deg C 180 Days 1 Total Metals Analysis of TCLP Metals in Soil by ICP-AES
Sample Comments:
(N/A)
Sample Collected By: TT
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 3 QC Code:_ Matrix: Solid Tag ID: 7041-3-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: 8794 Site OU: 00
Location Desc: RCRA metals & Hg samples
External Sample Number:
Expected Cone: (or Circle One: Low Medium High) Date
Latitude: :!>':!-. 01=!-0"t~'
Longitude: -"16'.~&20'
Laboratory Analyses: Container
1 - 8 oz glass
Preservative
4 Deg C
Sample Collection: Start: _l__P.~1111>
End: _/_/_
Holding Time Analysis
28 Days 1 Mercury in Soil or Sediment
Time(24 hr)
1 - 8 oz glass 4 Deg C 180 Days 1 Total Metals Analysis of TCLP Metals in Soil by ICP-AES
Sample Comments:
(N/A)
Sample Collected By: TT
1of1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 4 QC Code:_ Matrix: Solid Tag ID: 7041-4-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: RCRA metals & Hg samples
External Sample Number: Du- l/
Expected Cone: (or Circle One: Low Medium High) Date
Latitude: n,_o 11t-oo to·
Longitude: -~.~~ •
Laboratory Analyses: Container
1 - 8 oz glass
Preservative
Sample Collection: Start: _l_fl.~\lo
End: _)_)_
Holding Time Analysis
28 Days 1 Mercury in Soi! or Sediment
Time(24 hr)
~:"Z-"1
1 - 8 oz glass
4 Deg C
4 Deg C 180 Days 1 Total Metals Analysis of TCLP Metals in Soil by ICP-AES
Sample Comments:
(N/A)
Sample Collected By: TT
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 5 QC Code:_ Matrix: Solid Tag ID: 7041-5-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: RCRA metals & Hg samples
External Sample Number:
Expected Cone: (or Circle One: Low Medium High) Date
Latitude: 1'11-. 01 i. o"ifL_ Sample Collection: Start: J_fo__'!/llo
Longitude: •"1'!L!o1t&tU.'S' End: _)_)_
Laboratory Analyses: Container Preservative Holding Time Analysis
' /- 8 oz glass 4 Deg C 28 Days 1 Mercury in Soil or Sediment
Time(24 hr)
!l__ :'?!>I
~ )I'- 8 oz glass 4 Deg C 180 Days 1 Total Metals Analysis of TCLP Metals in Soil by ICP-AES
Sample Comments:
(N/A)
Sample Collected By: TT
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 6 QC Code:_ Matrix: Solid Tag ID: 7041-6-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: RCRA metals & Hg samples
External Sample Number:
Expected Cone: (or Circle One: Low Medium High) Date
Latitude: ~':1-.0~'ll-~'
Longitude: •':\!i .1.1$ "I l'=I-'
Laboratory Analyses: Container
1 - 8 oz glass
Preservative
4 Deg C
Sample Collection: Start: _L;2.__!; ~
End: _)_)_
Holding Time Analysis
28 Days 1 Mercury in Soil or Sediment
Time(24 hr)
l.\_:~
1 - 8 oz glass 4 Deg C 180 Days 1 Total Metals Analysis of TCLP Metals in Soil by ICP-AES
Sample Comments:
(N/A)
Sample Collected By: TT
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7041 Sample Number: 7 QC Code:_ Matrix: Solid Tag ID: 7041-7-_
Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling
City: Coffeyville State: Kansas Program: Superfund
Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00
Location Desc: RCRA metals & Hg samples
External Sample Number:
Expected Cone: (or Circle One: Low Medium High) Date
Latitude: ~'*· 0\'4 ~6'"1 •
Longitude: ~'l'J.~~·
Laboratory Analyses: Container
1 - 8 oz glass
Preservative
4 Deg C
Sample Collection: Start: _l__fo__:!!:/ Ile
End: _/_/_
Holding Time Analysis
28 Days 1 Mercury in Soil or Sediment
Time(24 hr)
1 - 8 oz glass 4 Deg C 180 Days 1 Total Metals Analysis of TCLP Metals in Soil by ICP-AES
Sample Comments:
(N/A)
Sample Collected By: TT
1 of 1
1 of 1
7077ASR Number: 1Sample Number: __QC Code: SolidMatrix:
_____________________________________________________________Location Desc:
__/__/__Start:
__/__/__End:
__________________________External Sample Number:
TTSample Collected By:
(N/A)
Sample Comments:
TCB794Project ID: Todd CampbellProject Manager:Osage and Walnut site - Removal Assessment samplingProject Desc:CoffeyvilleCity: KansasState:SuperfundProgram:
B794Site ID: 00Site OU:Osage and Walnut site - Site Name:
Sample Collection:
Tag ID: 7077-1-__
Date Time(24 hr)Expected Conc: (or Circle One: Low Medium High)
Latitude:
Longitude:
___ ___ ___
___ ___ ___
__:__
__:__
Sample Collection Field SheetUS EPA Region 7Kansas City, KS
1 - 8 oz glass
1 - 8 oz glass
1 - 8 oz glass
1 - 8 oz glass
0 -
Container
4 Deg C
4 Deg C
4 Deg C
None
4 Deg C
Preservative
28
180
180
28
0
Holding Time
Mercury in Soil or Sediment
Total Metals Analysis of TCLP Metals in Soil by ICP-AES
TCLP Metals in Soil
TCLP Mercury in Soil
Percent Solid
Analysis Laboratory Analyses:
Days
Days
Days
Days
Days
1
1
1
1
1
Page 1 of 23
02/29/2016Date:
7041
TCB794
Osage and Walnut site - Removal Assessment sampling
Todd CampbellSUPR/ERNB
Transmittal of Sample Analysis Results for ASR #:
Project ID:
Project Description:
Margaret E.W. St. Germain, ChiefLaboratory Technology & Analysis Branch, Environmental Sciences & Technology Division
To:
Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.
Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.
If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.
Enclosures
cc: Analytical Data File.
United States Environmental Protection AgencyRegion 7
300 Minnesota AvenueKansas City, KS 66101
Subject:
From:
Page 2 of 23
7041ASR Number: 02/29/2016
Todd Campbell SUPR/ERNB 913-551-7115
TCB794
Osage and Walnut site - Removal Assessment sampling
Coffeyville Kansas Superfund
Osage and Walnut site - B794Site ID: 00
Site Cleanup Support
Removal assessment sampling at the Osage and Walnut site. Field activities includesurface & subsurface soil sampling.
Project Manager: Org: Phone:
Project ID:
Project Desc:
Location: State: Program:
Site Name: Site OU:
Purpose:
__ = Field SampleFD = Field Duplicate
QC Codes identify the type of sample for quality control purpose.
Milligrams per KilogramMicrograms per Kilogram
Specific units in which results arereported.
The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.The presence or absence of the analyte can not be determined from the datadue to severe quality control problems. The data are rejected andconsidered unusable.The identification of the analyte is acceptable; the reported value is anestimate.The analyte was not detected at or above the reporting limit.
Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.
Summary of Project Information
Explanation of Codes, Units and Qualifiers used on this report
Sample QC Codes: Units:
UJ
R
J
U
=
=
=
=
Data Qualifiers:
= Values have been reviewed and found acceptable for use. (Blank)
mg/kgug/kg
==
TO BE SUBMITTEDQAPP Number:
303DC6GPRA PRC:
Page 3 of 23
1
2
2
3
4
5
6
7
101
102
103
104
105
106
107
108
109
110
110
111
112
113
114
115
116
117
118
119
120
121
122
123
124
125
126
201
202
203
SampleNo
__
__
FD
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
FD
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
QCCode
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Matrix
DU-1
DU-2
DU-2
DU-3
DU-4
DU-5
DU-6
DU-7
GP-1 (1-2)
GP-1 (3-4)
GP-2 (1-2)
GP-2 (7-8)
GP-3 (1-2)
GP-3 (7-8)
GP-4 (1-2)
GP-4 (7-8)
GP-5 (1-2)
GP-5 (7-8)
GP-5 (7-8)
GP-6 (2-3)
GP-6 (7-8)
GP-7 (3-4)
GP-7 (7-8)
GP-8 (3-4)
GP-8 (7-8)
GP-9 (3-4)
GP-9 (7-8)
GP-10 (3-4)
GP-11 (3-4)
GP-12 (3-4)
GP-12 (7-8)
GP-13 (2-3)
GP-13 (7-8)
GP-14 (3-4)
GP-14 (7-8)
GP-10 (3-4)
GP-11 (3-4)
GP-12 (3-4)
Location DescriptionExternal
Sample No
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/25/2016
01/25/2016
01/25/2016
01/25/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
01/26/2016
Start Date
11:05
11:10
11:10
11:18
11:24
11:31
11:38
11:49
15:05
15:05
16:15
16:25
08:15
08:20
08:51
09:00
09:37
09:50
09:50
10:28
10:37
11:02
11:10
11:30
11:38
11:59
12:07
13:40
14:20
14:54
14:58
15:40
15:47
16:00
16:05
13:40
14:20
14:54
Start Time
End Date
End Time
02/01/2016
02/01/2016
02/01/2016
02/01/2016
02/01/2016
02/01/2016
02/01/2016
02/01/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
01/27/2016
ReceiptDate
7041 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
ASR Number: Sample Information Summary
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Page 4 of 23
1
1
1
1
Cyanide, Total in Soil
Mercury in Soil or Sediment
Semi-Volatile TPH (DRO & ORO) in Soil by GC/FID
Total Metals Analysis of TCLP Metals in Soil by ICP-AES
Contract Lab Program (Out-Source)
Contract Lab Program (Out-Source)
RASP Contract Lab (Out-Source)
Contract Lab Program (Out-Source)
Lab:
Lab:
Lab:
Lab:
CLP Statement of Work
CLP Statement of Work
Similar to Modified version of SW846 Method 8015 (see comments)
CLP Statement of Work
Method:
Method:
Method:
Method:
(N/A)
(N/A)
Silver in samples -1 through -7 was UJ-coded. This analyte was not found in the samplesat or above the reporting limits, however, the reporting limits are an estimate (UJ-coded)due to negative recovery of this analyte in the interference check samples (ICS) which was
Comments:
Comments:
Comments:
Comments:
101-__ 102-__ 103-__ 104-__ 105-__ 106-__ 107-__108-__ 109-__ 110-__ 110-FD 111-__ 112-__ 113-__114-__ 115-__ 116-__ 117-__ 118-__ 119-__ 120-__121-__ 122-__ 123-__ 124-__ 125-__ 126-__
1-__ 2-__ 2-FD 3-__ 4-__ 5-__ 6-__7-__
201-__ 202-__ 203-__
1-__ 2-__ 2-FD 3-__ 4-__ 5-__ 6-__7-__
Samples:
Samples:
Samples:
Samples:
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Dry
Dry
Dry
Dry
Basis:
Basis:
Basis:
Basis:
Page 5 of 23
1
1
VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
Volatile TPH in Soil by GC/MS
Contract Lab Program (Out-Source)
RASP Contract Lab (Out-Source)
Lab:
Lab:
CLP Statement of WorkMethod:
not present in the ICS solution but whose absolute values were greater than the methoddetection limits (MDL), therefore, a possibility of false negatives exists. The actualreporting limits may be higher than the reported values.
1,2-dibromoethane had unacceptable response in one initial calibration curve (RRF: 0.195vs 0.20). It was therefore not possible to obtain valid results for this analyte. Results of'N/A' were reported for 1,2-dibromoethane with R-codes for samples -102 through -106, -108, and -110.
Bromoform, 1,2-dichlorobenzene, 1,3-dichlorobenzene, 1,4-dichlorobenzene, 1,2-dibromo-3-chloropropane, 1,2,4-trichlorobenzene, and 1,2,3-trichlorobenzene were UJ-coded insample -103. These analytes were not found in the sample at or above the reportinglimits, however, the reporting limits are an estimate (UJ-coded) due to low internalstandard response. The actual reporting limits for these analytes may be lower than thereported values.
Acetone, cyclohexane, and methylcyclohexane were J-coded in sample -101. Although theanalyte in question has been positively identified in the sample, the quantitation is anestimate (J-coded) due to high recoveries of surrogate analytes (2-butanone-d5: 137-161% vs 20-135% and 1,2-dichloropropane-d6: 123-136% vs 70-120%) in this sample.The actual concentrations for these analytes may be lower than the reported values.
Cis-1,2-dichloroethene was J-coded in samples -103 and -108. Although the analyte inquestion has been positively identified in the samples, the quantitations are an estimate (J-coded) due to low recoveries of a surrogate analyte (1,1-dichloroethene-d2: 36-44% vs 45-110%) in these samples. The actual concentrations for this analyte may be higher than thereported values.
Cis-1,2-dichloroethene in samples -104, -105, -106, and -110 and trans-1,2-dichloroethene and 1,1-dichloroethene in samples -103 through -106, -108, and -110 wereUJ-coded. These analytes were not found in the samples at or above the reporting limits,however, the reporting limits are an estimate (UJ-coded) due to low recoveries of thesurrogate analyte (1,1-dichloroethene-d2: 36-44% vs 45-110%). The actual reportinglimits for these analytes may be higher than the reported values.
Comments:
101-__ 102-__ 103-__ 104-__ 105-__ 106-__ 107-__108-__ 109-__ 110-__ 110-FD 111-__ 112-__ 113-__114-__ 115-__ 116-__ 117-__ 118-__ 119-__ 120-__121-__ 122-__ 123-__ 124-__ 125-__ 126-__
Samples:
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
DryBasis:
Page 6 of 23
Similar to Volatile TPH by GC/MS (see comments)Method:
(N/A)Comments:
201-__ 202-__ 203-__ Samples:
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
DryBasis:
Page 7 of 23
1
1
Mercury in Soil or Sediment
Total Metals Analysis of TCLP Metals in Soil by ICP-AES
Analysis/ Analyte
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Units 1-__ 2-__ 2-FD 3-__
0.11 U 0.11 U 0.11 U 0.12 U
1.7 1.5 2.6 8.5
52.9 30.3 63.0 103
1.2 0.69 0.95 1.4
7.1 14.2 12.0 32.9
36.6 141 77.1 140
3.1 U 3.0 U 3.0 U 3.2 U
0.89 UJ 0.86 UJ 0.84 UJ 0.90 UJ
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 8 of 23
1
1
Mercury in Soil or Sediment
Total Metals Analysis of TCLP Metals in Soil by ICP-AES
Analysis/ Analyte
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Units 4-__ 5-__ 6-__ 7-__
0.73 0.11 U 0.12 U 0.29
256 1.9 3.2 3.8
597 94.7 125 66.5
22.1 1.3 2.6 4.7
197 11.7 18.0 69.4
256 82.7 151 31.9
3.2 U 3.3 U 3.3 U 3.4 U
9.0 UJ 0.94 UJ 0.93 UJ 0.97 UJ
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 9 of 23
1
1
Cyanide, Total in Soil
VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
Analysis/ Analyte
Cyanide
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units 101-__ 102-__ 103-__ 104-__
0.60 U 0.62 U 0.62 U 0.62 U
120 J 11 27 11 U
5.3 U 5.5 U 10 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 UJ 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
11 U 11 U 10 U 11 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
15 J 5.5 U 1300 5.3 U
5.3 U 5.5 U 5.0 UJ 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U N/A R N/A R N/A R
5.3 U 5.5 U 5.0 UJ 5.3 U
5.3 U 5.5 U 5.0 UJ 5.3 U
5.3 U 5.5 U 5.0 UJ 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
21 12 16 20
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 UJ 5.3 UJ
7.9 5.5 U 5.2 J 5.3 UJ
5.3 U 5.5 U 5.0 UJ 5.3 UJ
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
8.3 5.5 U 54 5.3 U
5.3 U 11 U 10 U 11 U
5.3 U 5.5 U 9.2 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 14
6.7 J 5.5 U 23 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
11 U 11 U 10 U 11 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
16 5.5 U 130 5.3 U
5.3 U 5.5 U 5.0 UJ 5.3 U
5.3 U 5.5 U 5.0 UJ 5.3 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 10 of 23
Analysis/ Analyte
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units 101-__ 102-__ 103-__ 104-__
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 U 5.5 U 5.0 U 5.3 U
5.3 7.1 5.0 U 6.2
39 5.5 U 1300 5.3 U
27 5.5 U 850 5.3 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 11 of 23
1
1
Cyanide, Total in Soil
VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
Analysis/ Analyte
Cyanide
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units 105-__ 106-__ 107-__ 108-__
0.59 U 0.62 U 0.61 U 0.59 U
10 U 11 U 21 10 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
10 U 11 U 13 U 10 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
N/A R N/A R 6.3 U N/A R
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 6.8
5.2 U 5.6 U 6.3 U 5.0 U
5.2 UJ 5.6 UJ 6.3 U 5.0 UJ
5.2 UJ 5.6 UJ 6.3 U 24 J
5.2 UJ 5.6 UJ 6.3 U 5.0 UJ
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 23 5.0 U
10 U 11 U 13 U 10 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 33 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
10 U 11 U 13 U 10 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 12 of 23
Analysis/ Analyte
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units 105-__ 106-__ 107-__ 108-__
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
5.2 U 5.6 U 42 5.0 U
5.2 U 5.6 U 6.3 U 5.0 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 13 of 23
1
1
Cyanide, Total in Soil
VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
Analysis/ Analyte
Cyanide
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units 109-__ 110-__ 110-FD 111-__
0.60 U 0.61 U 0.61 U 0.66 U
19 10 U 9.9 U 12 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
10 U 10 U 9.9 U 12 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U N/A R 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 UJ 5.0 U 6.2 U
5.2 U 5.1 UJ 5.0 U 6.2 U
5.2 U 5.1 UJ 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
10 U 10 U 9.9 U 12 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
10 U 10 U 9.9 U 12 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 14 of 23
Analysis/ Analyte
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units 109-__ 110-__ 110-FD 111-__
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
5.2 U 5.1 U 5.0 U 6.2 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 15 of 23
1
1
Cyanide, Total in Soil
VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
Analysis/ Analyte
Cyanide
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units 112-__ 113-__ 114-__ 115-__
0.62 U 0.64 U 0.59 U 0.66 U
11 U 11 9.4 U 11 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
11 U 11 U 9.4 U 11 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
11 U 11 U 9.4 U 11 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
11 U 11 U 9.4 U 11 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 16 of 23
Analysis/ Analyte
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units 112-__ 113-__ 114-__ 115-__
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
5.4 U 5.5 U 4.7 U 5.5 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 17 of 23
1
1
Cyanide, Total in Soil
VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
Analysis/ Analyte
Cyanide
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units 116-__ 117-__ 118-__ 119-__
0.61 U 0.57 U 0.59 U 0.56 U
11 U 9.6 U 9.3 U 9.2 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
11 U 9.6 U 9.3 U 9.2 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
11 U 9.6 U 9.3 U 9.2 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
11 U 9.6 U 9.3 U 9.2 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 18 of 23
Analysis/ Analyte
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units 116-__ 117-__ 118-__ 119-__
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
5.3 U 4.8 U 4.7 U 4.6 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 19 of 23
1
1
Cyanide, Total in Soil
VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
Analysis/ Analyte
Cyanide
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units 120-__ 121-__ 122-__ 123-__
0.63 U 0.57 U 0.61 U 0.62 U
10 U 11 9.3 U 13
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
10 U 9.1 U 9.3 U 9.8 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 17 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 9.9 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 42 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
10 U 9.1 U 9.3 U 9.8 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
10 U 9.1 U 9.3 U 9.8 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 20 of 23
Analysis/ Analyte
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units 120-__ 121-__ 122-__ 123-__
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
5.2 U 4.5 U 4.6 U 4.9 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 21 of 23
1
1
1
Cyanide, Total in Soil
Semi-Volatile TPH (DRO & ORO) in Soil by GC/FID
VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap
Analysis/ Analyte
Cyanide
TPH DRO
TPH ORO
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
mg/kg
mg/kg
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units 124-__ 125-__ 126-__ 201-__
0.59 U 0.60 U 0.58 U
10.8 U
86.7 U
10 U 9.5 U 9.8 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
10 U 9.5 U 9.8 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
10 U 9.5 U 9.8 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
10 U 9.5 U 9.8 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 22 of 23
1 Volatile TPH in Soil by GC/MS
Analysis/ Analyte
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
TPH GRO
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
mg/kg
Units 124-__ 125-__ 126-__ 201-__
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
5.2 U 4.8 U 4.9 U
2.24 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 23 of 23
1
1
Semi-Volatile TPH (DRO & ORO) in Soil by GC/FID
Volatile TPH in Soil by GC/MS
Analysis/ Analyte
TPH DRO
TPH ORO
TPH GRO
mg/kg
mg/kg
mg/kg
Units 202-__ 203-__
10.3 U 21.5
82.8 U 201
2.09 U 2.21 U
7041ASR Number: 02/29/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
7041
TCB794Project ID:
Osage and Walnut site - Removal Assessment sampling
Todd CampbellSUPR/ERNB
United States Environmental Protection AgencyRegion VII
300 Minnesota AvenueKansas City, KS 66101
__/__/____
Data Disposition/Sample Disposition for ASR #
Project Description:
Subject:
Alisha ClaycampENST/LTAB/LABS
I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of theboxes for Data Disposition and Sample Disposition.
I understand all samples will be disposed of unless samples are requested to be held. If I do notreturn this form within 30 days of the transmittal all samples will have a waste determinationmade and scheduled for disposal.
"RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS"Customer" account. All Samples may be disposed of upon receipt of this form if not requested to
"Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples maybe disposed of upon receipt of this form if not requested to be held.
"Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requestedthrough the laboratory. All samples may be disposed of upon receipt of the form if not requestedto be held.
Transmittal Date:
From:
To:
No longer need samples for site characterization
Hold Samples - I have determined that the samples need to be held until ______________, afterwhich time they will be disposed of in accordance with applicable regulations. The reason for the hold is:
Samples are associated with a legal proceeding.
Question/Concern with data - possible reanalysis requested.
Other:________________________________________________________________
Data Disposition
Sample Disposition
Page 1 of 6
03/17/2016Date:
7077
TCB794
Osage and Walnut site - Removal Assessment sampling
Todd CampbellSUPR/ERNB
Transmittal of Sample Analysis Results for ASR #:
Project ID:
Project Description:
Margaret E.W. St. Germain, ChiefLaboratory Technology & Analysis Branch, Environmental Sciences & Technology Division
To:
Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.
Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.
If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.
Enclosures
cc: Analytical Data File.
United States Environmental Protection AgencyRegion 7
300 Minnesota AvenueKansas City, KS 66101
Subject:
From:
Page 2 of 6
7077ASR Number: 03/17/2016
Todd Campbell SUPR/ERNB 913-551-7115
TCB794
Osage and Walnut site - Removal Assessment sampling
Coffeyville Kansas Superfund
Osage and Walnut site - B794Site ID: 00
Site Cleanup Support
Removal Assessment.Sample collected from 55-gallon drum containing overspray material. This samplewas a sample of opportunity collected w/ASR #7041.
Project Manager: Org: Phone:
Project ID:
Project Desc:
Location: State: Program:
Site Name: Site OU:
Purpose:
__ = Field Sample
QC Codes identify the type of sample for quality control purpose.
Milligrams per KilogramPercentMilligrams per Liter
Specific units in which results arereported.
The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.The identification of the analyte is acceptable; the reported value is anestimate.The analyte was not detected at or above the reporting limit.
Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.
Summary of Project Information
Explanation of Codes, Units and Qualifiers used on this report
Sample QC Codes: Units:
UJ
J
U
=
=
=
Data Qualifiers:
= Values have been reviewed and found acceptable for use. (Blank)
mg/kg%
mg/L
===
303DC6GPRA PRC:
Page 3 of 6
1
SampleNo
__
QCCode
Solid
Matrix
Overspray material
Location DescriptionExternal
Sample No
01/27/2016
Start Date
12:00
Start Time
End Date
End Time
02/17/2016
ReceiptDate
7077 03/17/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
ASR Number: Sample Information Summary
-
Page 4 of 6
1
1
1
1
1
Mercury in Soil or Sediment
Percent Solid
TCLP Mercury in Soil
TCLP Metals in Soil
Total Metals Analysis of TCLP Metals in Soil by ICP-AES
Region 7 ESAT Contract Lab (In-House)
Region 7 ESAT Contract Lab (In-House)
Region 7 ESAT Contract Lab (In-House)
Region 7 ESAT Contract Lab (In-House)
Region 7 ESAT Contract Lab (In-House)
Lab:
Lab:
Lab:
Lab:
Lab:
EPA Region 7 RLAB Method 3121.23D
EPA Region 7 RLAB Method 3142.9G
EPA Region 7 RLAB Method 3121.23D applied to TCLP extracts
EPA Region 7 RLAB Method 3122.3F TCLP
EPA Region 7 RLAB Method 3122.3F
Method:
Method:
Method:
Method:
Method:
(N/A)
(N/A)
Sample 1 was analyzed 6 day(s) past their 28 day holding time. The results foranalytes that were not found at or above the reporting limit were UJ-coded to indicate thatthe reporting limit is an estimated value. The actual reporting limit may be higher than thereported value.
Comments:
Comments:
Comments:
Comments:
1-__
1-__
1-__
1-__
Samples:
Samples:
Samples:
Samples:
7077ASR Number: 03/17/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Dry
N/A
N/A
N/A
Basis:
Basis:
Basis:
Basis:
Page 5 of 6
Arsenic (56,44,75-115) was UJ-coded in sample 1. This analyte was not found in thesample at or above the reporting limit, however, the reporting limit is an estimate (UJ-coded) due to low recovery of this analyte in the laboratory matrix spike. The actualreporting limit for this analyte may be higher than the reported value.
Selenium (41,32,75-108) was J-coded in sample 1. Although the analyte in question hasbeen positively identified in the sample, the quantitation is an estimate (J-coded) due tolow recovery of this analyte in the laboratory matrix spike. The actual concentration forthis analyte may be higher than the reported value.
Arsenic (23,7.6) was UJ-coded in sample 1. This analyte was not found in the sample at orabove the reporting limit, however, the reporting limit is an estimate (UJ-coded) due topoor precision obtained for this analyte in the laboratory matrix spike and matrix spikeduplicate. The actual reporting limit for this analyte may be higher than the reportedvalue.
Comments:
1-__ Samples:
7077ASR Number: 03/17/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
DryBasis:
Page 6 of 6
1
1
1
1
1
Mercury in Soil or Sediment
Percent Solid
TCLP Mercury in Soil
TCLP Metals in Soil
Total Metals Analysis of TCLP Metals in Soil by ICP-AES
Analysis/ Analyte
Mercury
Solids, percent
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
mg/kg
%
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Units 1-__
0.00857
98.7
0.000250 UJ
0.050 U
0.162
0.005 U
0.015 U
0.050 U
0.542
0.025 U
5.1 UJ
36.1
1.9
20.8
8.1
96.3 J
3.6
7077ASR Number: 03/17/2016
TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:
RLAB Approved Sample Analysis Results
7077
TCB794Project ID:
Osage and Walnut site - Removal Assessment sampling
Todd CampbellSUPR/ERNB
United States Environmental Protection AgencyRegion VII
300 Minnesota AvenueKansas City, KS 66101
__/__/____
Data Disposition/Sample Disposition for ASR #
Project Description:
Subject:
Alisha ClaycampENST/LTAB/LABS
I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of theboxes for Data Disposition and Sample Disposition.
I understand all samples will be disposed of unless samples are requested to be held. If I do notreturn this form within 30 days of the transmittal all samples will have a waste determinationmade and scheduled for disposal.
"RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS"Customer" account. All Samples may be disposed of upon receipt of this form if not requested to
"Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples maybe disposed of upon receipt of this form if not requested to be held.
"Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requestedthrough the laboratory. All samples may be disposed of upon receipt of the form if not requestedto be held.
Transmittal Date:
From:
To:
No longer need samples for site characterization
Hold Samples - I have determined that the samples need to be held until ______________, afterwhich time they will be disposed of in accordance with applicable regulations. The reason for the hold is:
Samples are associated with a legal proceeding.
Question/Concern with data - possible reanalysis requested.
Other:________________________________________________________________
Data Disposition
Sample Disposition
APPENDIX G
ANALYTICAL DATA TABLES
Mercury Arsenic Barium Cadmium Chromium Lead Selenium Silver
Overspray Material 7077-1 0.00857 5.10 UJ 36.1 1.90 20.8 8.10 96.3 J 3.60
46 3.00 2.25E+05 980 NE* 800 5.80E+03 5.80E+03
20 63.2 2.77E+05 965 111** 1.00E+03 1.02E+04 1.02E+04
Overspray Material 7077-1 2.50E-04 U 0.050 U 0.162 0.005 U 0.015 U 0.050 U 0.542 0.025 U
0.200 5.00 100 1.00 5.00 5.00 1.00 5.00
Notes:
Italicized value indicates the reporting limit exceeds a benchmark.
* No benchmark exists for total chromium
** This value is for total chromium
EPA U.S. Environmental Protection Agency
ID Identification
J The identification of the analyte is acceptable. The reported value is an estimate.
KDHE Kansas Department of Health and Environment
mg/kg milligrams per kilogram
mg/L milligrams per liter
RCRA Resource Conservation and Recovery Act
RSL Regional Screening Level
TCLP Toxicity characteristic leaching procedure
U The analyte was not detected at or above the reporting limit
UJ The analyte was not detected at or above the reporting limit. The reporting limit is an estimate.
TCLP Regulatory Limits
Sample Name Laboratory Sample IDAnalyte and Result
Total RCRA Metals Results (mg/kg)
TABLE G-1
SUMMARY OF OVERSPRAY MATERIAL ANALYTICAL DATA
OSAGE AND WALNUT SITE, COFFEYVILLE, KANSAS
TCLP RCRA Metals Results (mg/L)
EPA RSL for Industrial Soil
KDHE Tier 2 Benchmark for Non-Residential Scenario
1,1
-DC
A
Aceto
ne
Ben
zen
e
Ch
loroeth
an
e
cis
-1,2
-DC
E
Cyclo
hexan
e
Eth
yl
Ben
zen
e
Isop
rop
ylb
en
zen
e
m a
nd
/or p
-Xyle
ne
Meth
yl
tert-
bu
tyl
eth
er
Meth
ylc
yclo
hexan
e
o-X
yle
ne
Tetr
ach
loroeth
en
e
Tolu
en
e
Tric
hlo
roeth
en
e
Vin
yl
Ch
lorid
e
TP
H-D
RO
TP
H-O
RO
TP
H-G
RO
GP-1 (1-2) 1/25/2016 1505 7041-101 21 120 J 5.3 U 5.3 U 7.9 15 J 8.3 5.3 U 39 5.3 U 6.7 J 27 5.3 U 16 5.3 U 5.3 - - -
GP-1 (3-4) 1/25/2016 1505 7041-102 12 11 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 7.1 - - -
GP-2 (1-2) 1/25/2016 1615 7041-103 16 27 10 5.0 U 5.2 J 1.30E+03 54 9.2 1.30E+03 5.0 U 23 850 5.0 U 130 5.0 U 5.0 U - - -
GP-2 (7-8) 1/25/2016 1625 7041-104 20 11 U 5.3 U 5.3 U 5.3 UJ 5.3 U 5.3 U 5.3 U 5.3 U 14 5.3 U 5.3 U 5.3 U 5.3 U 5.3 U 6.2 - - -
GP-3 (1-2) 1/26/2016 0815 7041-105 5.2 U 10 U 5.2 U 5.2 U 5.2 UJ 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U - - -
GP-3 (7-8) 1/26/2016 0820 7041-106 5.6 U 11 U 5.6 U 5.6 U 5.6 UJ 5.6 U 5.6 U 5.6 U 5.6 U 5.6 U 5.6 U 5.6 U 5.6 U 5.6 U 5.6 U 5.6 U - - -
GP-4 (1-2) 1/26/2016 0851 7041-107 6.3 U 21 6.3 U 6.3 U 6.3 U 6.3 U 23 6.3 U 42 6.3 U 33 6.3 U 6.3 U 6.3 U 6.3 U 6.3 U - - -
GP-4 (7-8) 1/26/2016 0900 7041-108 6.8 10 U 5.0 U 5.0 U 24 J 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U - - -
GP-5 (1-2) 1/26/2016 0937 7041-109 5.2 U 19 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U - - -
GP-5 (7-8) 1/26/2016 0950 7041-110 5.1 U 9.9 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U - - -
GP-5 (7-8) FD 1/26/2016 0950 7041-110 FD 5.0 U 10 U 5.1 U 5.1 U 5.1 UJ 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U - - -
GP-6 (2-3) 1/26/2016 1028 7041-111 6.2 U 12 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U - - -
GP-6 (7-8) 1/26/2016 1037 7041-112 5.4 U 11 U 5.4 U 5.4 U 5.4 U 5.4 U 5.4 U 5.4 U 5.4 U 5.4 U 5.4 U 5.4 U 5.4 U 5.4 U 5.4 U 5.4 U - - -
GP-7 (3-4) 1/26/2016 1102 7041-113 5.5 U 11 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U - - -
GP-7 (7-8) 1/26/2016 1110 7041-114 4.7 U 9.4 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U - - -
GP-8 (3-4) 1/26/2016 1130 7041-115 5.5 U 11 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U - - -
GP-8 (7-8) 1/26/2016 1138 7041-116 5.3 U 11 U 5.3 U 5.3 U 5.3 U 5.3 U 5.3 U 5.3 U 5.3 U 5.3 U 5.3 U 5.3 U 5.3 U 5.3 U 5.3 U 5.3 U - - -
GP-9 (3-4) 1/26/2016 1159 7041-117 4.8 U 9.6 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U - - -
GP-9 (7-8) 1/26/2016 1207 7041-118 4.7 U 9.3 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U 4.7 U - - -
GP-10 (3-4) 1/26/2016 1340 7041-119 4.6 U 9.2 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U - - -
GP-10 (3-4) 1/26/2016 1340 7041-201 - - - - - - - - - - - - - - - - 1.08E+04 U 8.67E+04 U 2.24E+03 U
GP-11 (3-4) 1/26/2016 1420 7041-120 5.2 U 10 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U - - -
GP-11 (3-4) 1/26/2016 1420 7041-202 - - - - - - - - - - - - - - - - 1.03E+04 U 8.28E+04 U 2.09E+03 U
GP-12 (3-4) 1/26/2016 1454 7041-121 4.5 U 11 4.5 U 17 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U - - -
GP-12 (3-4) 1/26/2016 1454 7041-203 - - - - - - - - - - - - - - - - 2.15E+04 2.01E+05 2.21E+03 U
GP-12 (7-8) 1/26/2016 1458 7041-122 9.9 9.3 U 4.6 U 4.6 U 42 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U - - -
GP-13 (2-3) 1/26/2016 1540 7041-123 4.9 U 13 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U - - -
GP-13 (7-8) 1/26/2016 1547 7041-124 5.2 U 10 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U - - -
GP-14 (3-4) 1/26/2016 1600 7041-125 4.8 U 9.5 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U - - -
GP-14 (7-8) 1/26/2016 1605 7041-126 4.9 U 9.8 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U 4.9 U - - -
2.00E+03 6.70E+08 5.10E+03 2.30E+07 2.30E+06 3.10E+06 2.50E+04 NE 2.50E+06 2.10E+05 NE 2.80E+06 1.20E+05 4.70E+07 6.00E+03 1.70E+03 6.00E+05 4.20E+05 3.30E+07
7.99E+04 4.06E+08 2.82E+04 2.81E+07 3.87E+04 1.33E+07 1.45E+05 NE 1.41E+06 1.05E+06 NE 1.41E+06 2.10E+05 2.98E+04 9.91E+03 9.21E+03 3.50E+05 9.50E+05 2.75E+07
Notes
°N Degrees north
°W Degrees west
µg/kg Micrograms per kilogram
1,1-DCA 1,1-Dichloroethane
cis-1,2-DCE cis-1,2-Dichloroethene
DPT Direct-push technology
DU Decision Unit
EPA U.S. Environmental Protection Agency
ID Identification
J The identification of the analyte is acceptable; the reported value is an estimate
KDHE Kansas Department of Health and Environment
NE Not established
RSL Regional Screening Level
TCE Trichloroethene
TPH-DRO Total petroleum hydrocarbons-diesel range organics
TPH-GRO Total petroleum hydrocarbons-gasoline range organics
TPH-ORO Total petroleum hydrocarbons-oil range organics
U The analyte was not detected at or above the reporting limit
USGS United States Geological Survey
KDHE Tier 2 Risk Based Benchmark for Nonresidential Scenarios
TABLE G-2
SUMMARY OF DPT SOIL SAMPLE ANALYTICAL DATA
OSAGE AND WALNUT SITE, COFFEYVILLE, KANSAS
East of main Re-Con
building
Northwest of main
Re-Con building
Along west property
boundary
Latitude
(°N)
Longitude
(°W)
EPA RSL for Industrial Soil
37.01468 95.61868
37.01707 95.61816
37.01469 95.61848
Within suspected
TCE source area
Within suspected
Petroleum source
area
95.6179037.01623
95.6180037.01625
95.6180637.01626
37.01613 95.61798
37.01614 95.61806
95.6178437.01607
37.01606 95.61794
37.01607 95.61806
37.01616 95.61788
37.01758 95.61891
37.01715 95.61892
Analyte and Result (µg/kg)
Sample Name Sample DescriptionCollection
Date
Collection
Time
Laboratory
Sample ID
Latitude °N Longitude °W Mercury Arsenic Barium Cadmium Chromium Lead Selenium Silver
DU-1 Soil staining east of main Re-Con building 37.016884 95.618081 7041-1 0.11 U 1.7 52.9 1.2 7.1 36.6 3.1 U 0.89 UJ
7041-2 0.11 U 1.5 30.3 0.69 14.2 141 3.0 U 0.84 UJ
7041-2FD 0.11 U 2.6 63 0.95 12.0 77.1 3.0 U 0.86 UJ
DU-3 West of main Re-Con building 37.017049 95.018820 7041-3 0.12 U 8.5 103 1.4 32.9 140 3.2 U 0.90 UJ
DU-4Waste material covering floor of main Re-Con
building37.017006 95.618749 7041-4 0.73 256 597 22.1 197 256 3.2 U 9.0 UJ
DU-5 West of PrimeTime shop 37.016048 95.618863 7041-5 0.11 U 1.9 94.7 1.3 11.7 82.7 3.3 U 0.94 UJ
DU-6 South of PrimeTime shop 37.015749 95.618417 7041-6 0.12 U 3.2 125 2.6 18.0 151 3.3 U 0.93 UJ
DU-7 Near oil well 37.014789 95.618481 7041-7 0.29 3.8 66.5 4.7 69.4 31.9 3.4 U 0.97 UJ
0.017 7.941 NE NE NE 23.226 0.365 NE
46 3.00 2.25E+05 980 NE* 800 5.80E+03 5.80E+03
20 63.2 2.77E+05 965 111** 1.00E+03 1.02E+04 1.02E+04
Notes
Bolded value indicates analyte exceeds one health-based benchmark
Bolded and shaded value indicates analyte exceeds both health-based benchmarks
* No benchmark exists for total chromium
** This value is for total chromium
°N Degrees north
°W Degrees west
DU Decision Unit
EPA U.S. Environmental Protection Agency
ID Identification
KDHE Kansas Department of Health and Environment
mg/kg Milligrams per kilogram
NE Not established
RSL Regional Screening Level
U The analyte was not detected at or above the reporting limit
UJ
USGS United States Geological Survey
The analyte was not detected at or above the reporting limit. The reporting limit is an estimate
USGS Average Background Concentration for Montgomery County
KDHE Tier 2 Risk Based Benchmark for Non-Residential Scenario (soil pathway)
EPA RSL for Industrial Soil
Laboratory
Sample ID
Analyte and Result (mg/kg)
37.017336
TABLE G-3
SUMMARY OF SURFACE SOIL SAMPLE ANALYTICAL DATA
OSAGE AND WALNUT SITE, COFFEYVILLE, KANSAS
Sample Location
North exterior of main Re-Con building, near
paint boothDU-2 95.618499
Sample
NameSample Description